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Machining of High Strength PM Steels - Höganäs AB

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<strong>Machining</strong> <strong>of</strong> <strong>High</strong> <strong>Strength</strong> <strong>PM</strong> <strong>Steels</strong><br />

Ol<strong>of</strong> Andersson*, Hans Thordenberg**, Sigurd Berg*<br />

*<strong>Höganäs</strong> <strong>AB</strong>, S-26383 <strong>Höganäs</strong>, Sweden<br />

**<strong>AB</strong> Sandvik Coromant, S-811 81, Sandviken, Sweden<br />

Abstract<br />

P/M is a net or near net shape process. <strong>Machining</strong> operations are used for many applications<br />

in order to reach final tolerances or shapes not possible to achieve in the compaction step. The<br />

use <strong>of</strong> high strength <strong>PM</strong> steels have increased in recent time. Guidelines for insert choice and<br />

effect from additives are needed to improve the performance in the machining operation for<br />

these application areas.<br />

This paper describes the machinability <strong>of</strong> a fully bainitic high strength <strong>PM</strong> material. An<br />

optimum is found regarding settings <strong>of</strong> the insert for which properties like insert life time and<br />

surface roughness are improved. Machinability additives performance and their influence on<br />

physical and mechanical properties are shown for machining <strong>of</strong> such <strong>PM</strong> material.<br />

Introduction<br />

<strong>PM</strong> is a well-known method for producing large series <strong>of</strong> complex parts to very close<br />

tolerances. However, today many <strong>PM</strong> components require some type <strong>of</strong> machining operation<br />

to reach final shape, e.g. shapes impossible to create with the compaction exclusively or due<br />

to demands for even higher tolerances.<br />

<strong>PM</strong> materials are <strong>of</strong>ten considered to be difficult to machine, especially compared to<br />

conventional standard steels. However, by choosing a proper combination <strong>of</strong> tool material and<br />

insert geometry together with optimised cutting data, and if also necessary, additives, it is in<br />

many cases possible to reach a productivity level as high as <strong>of</strong> standard steels [1][2].<br />

In this study a turning operation has been performed on a relatively new <strong>PM</strong> material, the<br />

chromium and molybdenum prealloyed AstaloyCrM [3], in a fully bainitic condition with<br />

high strength properties. In this paper the influence <strong>of</strong> tool grades, insert geometries, additives<br />

and cutting data, when machining this type <strong>of</strong> <strong>PM</strong> material will be presented.<br />

Experimental<br />

Three powder mixes [Table 1] were manufactured in order to compact turning test specimens,<br />

with geometry Ø64/Ø35 x 45 mm, and test bars to evaluate mechanical properties. All<br />

specimens were compacted at 700 MPa to a green density <strong>of</strong> 7.0 g/cm³.<br />

Table 1. Powder mixes based on AstaloyCrM<br />

<strong>PM</strong> material Composition<br />

Material 1 Astaloy CrM + 0.37% Graphite + 0.8% Kenolube<br />

Material 2 Astaloy CrM + 0.37% Graphite + 0.8% Kenolube + 0.5% MnS<br />

Material 3 Astaloy CrM + 0.37% Graphite + 0.8% Kenolube + 0.3% MnX<br />

MnX is a patented product <strong>of</strong> <strong>Höganäs</strong> <strong>AB</strong> that has been found effective as a pre-mix additive<br />

in the machining <strong>of</strong> <strong>PM</strong> steels.<br />

Presented at <strong>PM</strong>2004, in Vienna, Austria, October 2004<br />

1


Green specimens were sintered in a laboratory belt furnace at 1120ºC for 30 minutes in an<br />

atmosphere <strong>of</strong> 90% nitrogen/10% hydrogen, and with additional 0.2% methane to maintain a<br />

good carbon control. The cooling rate in the end <strong>of</strong> the sintering cycle was 0.8ºC/s. For all<br />

three material compositions a fully bainitic structure [Fig. 1] was obtained.<br />

Figure 1: Sintered AstaloyCrM + 0.37%C. Etched with nital/picral.<br />

The influence by the additives can be observed in terms <strong>of</strong> minor reductions in strength<br />

[Table 2]. However, the micro hardness <strong>of</strong> the bainitic matrix is independent whether the mix<br />

consists <strong>of</strong> additives or not.<br />

Table 2: Mechanical properties <strong>of</strong> sintered test specimens<br />

<strong>PM</strong> material SD HV10 MHV0.05 DC TS YS MnS IE<br />

Material 1 7.0 236 376 -0.20 833 625 0.6 14<br />

Material 2 7.0 228 370 -0.21 787 571 0.9 13<br />

Material 3 7.0 234 372 -0.17 780 572 0.8 15<br />

SD:<br />

HV10:<br />

Sintered density [g/cm³]<br />

Hardness measured on polished cross section <strong>of</strong> turning test specimen [MPa]<br />

MHV0.05: Micro hardness measured on polished cross section <strong>of</strong> turning test specimen [MPa]<br />

DC:<br />

TS:<br />

YS:<br />

A:<br />

IE:<br />

Dimensional change from as-green to as-sintered [%]<br />

Tensile strength [MPa]<br />

Yield strength [MPa]<br />

Elongation [%]<br />

Impact energy [J]<br />

A CNC lathe (Mazak) was used to face turn the cylinder specimens. The surface to a depth <strong>of</strong><br />

0.5 mm was removed in order to secure the performance <strong>of</strong> the different inserts and<br />

geometries. Influence <strong>of</strong> surface variation, like carburisation, decarburisation or oxidation is<br />

therefore eliminated in comparsion test.<br />

Turning tests <strong>of</strong> AstaloyCrM without additive (Material 1) – Preparatory tests<br />

One <strong>of</strong> the first attempts to machine AstaloyCrM was carried out with a CVD coated<br />

cemented carbide insert, CNMG120408-WF [4]. With start-up cutting data (Vc = 150 m/min,<br />

f = 0.1 mm/r, ap = 0.5 mm) and dry machining the insert was inspected every tenth pass, up to<br />

50 passes. The dominating wear mechanism was found to be adhesion in terms <strong>of</strong> severe built<br />

up edge (BUE) and a heavily smearing effect, i.e. pressure-welded specimen material, on<br />

clearance flank [Fig. 2]<br />

Presented at <strong>PM</strong>2004, in Vienna, Austria, October 2004<br />

2


Figure 2: BUE and smearing on insert CNMG120408-WF<br />

In an attempt to reduce BUE and smearing effects, cutting speed was increased in order to<br />

change cutting edge temperature and in this way s<strong>of</strong>ten the built up layer and replace it with a<br />

flow zone. The BUE can be reduced with an increased cutting speed however, pressuredwelded<br />

material is still heavily smeared on the clearance flank and close to secondary cutting<br />

edge [Fig. 3] which would in the end jeopardize the machined surface quality.<br />

Vc = 200 m/min Vc = 250 m/min Vc = 300 m/min<br />

Figure 3: BUE and smearing on insert CNMG120408-WF. Turning with increased cutting speeds.<br />

In a next step to reduce BUE and smeared material on tool insert, cutting fluid (emulsion <strong>of</strong><br />

water and 5% Castrol Syntilo XPS) was applied. The use <strong>of</strong> cutting fluid was found to be <strong>of</strong><br />

significant importance [Fig. 4] since BUE and a large amount <strong>of</strong> the smearing could be<br />

eliminated.<br />

Vc = 200 m/min Vc = 250 m/min Vc = 300 m/min<br />

Figure 4: CNMG120408-WF. Turning with increased cutting speeds and applied cutting fluid.<br />

Turning tests <strong>of</strong> AstaloyCrM without additive (Material 1) – Optimizations<br />

Two measurements have proven to minimize or eliminate the smearing tendencies; cutting<br />

speed in some remarks but especially the addition <strong>of</strong> cutting fluid with significant result. To<br />

make further optimizations, with regards to an increased tool life, different insert grades [4],<br />

i.e. substrates and coatings, applied on insert CCMT09T308 [4], a positive design compared<br />

with the negative CNMG, were tested. All tests were performed until flank wear on tool insert<br />

had reached the standardized length <strong>of</strong> 0.3 mm. The two most successful grades [Fig. 5] were<br />

grade CT5015 (uncoated WC-Co cermet) and a new developed grade GC3215 (solid carbide,<br />

coated with TiCN, Al2O3 and TiN).<br />

Presented at <strong>PM</strong>2004, in Vienna, Austria, October 2004<br />

3


No <strong>of</strong> passes to Vb = 0.3 mm<br />

Figure 5: Tool life with different insert grades and same tool geometry.<br />

With the cermet grade CT5015 the influence <strong>of</strong> geometry was tested by choosing different<br />

cutting edge designs (-WF, -PF and -<strong>PM</strong>) applied on CCMT09T308 [4]. In this test an insert<br />

with a more improved tolerance by grinding, the CCGT09T308-UM [4], also was tested. The<br />

result [Fig. 6] <strong>of</strong> this test indicates that a well-defined edge radius and sharpness affects the<br />

tool life when machining the AstaloyCrM without additives, i.e. the G-tolerance geometry<br />

CCGT09T308-UM exhibits the best performance.<br />

No <strong>of</strong> passes to Vb = 0.3 mm<br />

150<br />

125<br />

100<br />

75<br />

50<br />

25<br />

0<br />

250<br />

200<br />

150<br />

100<br />

50<br />

0<br />

CCMT09T308 (-KM/<strong>PM</strong>/MM)<br />

Vc = 300 m/min<br />

f = 0.10 mm/r<br />

ap = 0.5 mm<br />

With cutting fluid<br />

GC1025 GC1005 GC4025 GC2015 GC2025 GC4015 GC3215 CT5015<br />

CCMT09T308 (-WF, -PF, <strong>PM</strong>)<br />

CCGT09T308-UM<br />

Vc = 250 m/min, f = 0.1 mm/r<br />

ap = 0.5 mm<br />

With cutting fluid<br />

- WF - PF - <strong>PM</strong> - UM<br />

Figure 6: Tool life with same insert grade and different tool geometries.<br />

Turning tests <strong>of</strong> AstaloyCrM with addition <strong>of</strong> MnS or MnX (Material 2 & 3)<br />

The influence <strong>of</strong> additives in AstaloyCrM was dramatically shown in the first test with tool<br />

insert CNMG120408-WF [Fig. 7]. With the same type <strong>of</strong> tool insert and with the same cutting<br />

data that was used when AstaloyCrM without additive was machined (Vc = 150 m/min, f =<br />

0.1 mm/r, ap = 0.5 mm) the presence <strong>of</strong> BUE and smeared material on clearance flank was<br />

non-existent, even when the machining took place without cutting fluid, i.e. dry.<br />

Without additive With + 0.3% MnX With + 0.5% MnS<br />

Figure 7: Edge integrity <strong>of</strong> CNMG120408-WF.<br />

With the intention to optimize machinability the so far successful grades, CG3215 and<br />

CT5015 were applied on the insert tool CCMT09T308-WF. All tests were done with cutting<br />

fluid. The best machining performance was found for the coated solid carbide GC3215 and<br />

Presented at <strong>PM</strong>2004, in Vienna, Austria, October 2004<br />

4


not, as previous was stated in the case AstaloyCrM without additives, the uncoated cermet<br />

CT5015 [Fig. 8].<br />

No <strong>of</strong> passes to Vb = 0.3 mm<br />

800<br />

700<br />

600<br />

500<br />

400<br />

300<br />

200<br />

100<br />

0<br />

+ MnS<br />

Figure 8: Tool life when machining AstaloyCrM + additive with<br />

different insert grades and same tool geometry.<br />

The additives are beneficial to tool life, especially AstaloyCrM + 0.5% MnS, even at feed<br />

rate 0.3 mm/r. The presence <strong>of</strong> MnX eliminates pressured-welded material but a higher wear<br />

rate, in terms <strong>of</strong> flank and crater wear, can be observed compared to the wear rate with the<br />

addition <strong>of</strong> MnS. Yet, addition <strong>of</strong> MnX will improve the machinability.<br />

Tool life for AstaloyCrM with or without addition <strong>of</strong> MnS (Material 1 & 2)<br />

The Vt-graph [Fig. 9] shows a divided behaviour when AstaloyCrM without additive is<br />

machined, expressed with two alpha-values (curve slopes). At lower cutting speeds, i.e. less<br />

than 250 m/min, the wear process is gradually more and more influenced by smearing and<br />

BUE formation. With increased feed rate (0.3 mm/r) tool life will be heavily reduced.<br />

However, with the addition <strong>of</strong> MnS higher cutting speed (>250 m/min) together with higher<br />

feed rates (up to 0.3 mm/r) can be used with maintained tool life.<br />

Tool life to Vb = 0.3 mm [min]<br />

100<br />

30<br />

20<br />

10<br />

Increased BUE and<br />

smearing<br />

Figure 9: Vt-graph<br />

Gains by optimization <strong>of</strong> inserts and addition <strong>of</strong> MnX or MnS<br />

A comparison <strong>of</strong> gains in tool life (number <strong>of</strong> passes) and productivity (feed rate) shows the<br />

influence <strong>of</strong> additive [Fig. 10]. The gains are relatively to the turning tests <strong>of</strong> AstaloyCrM<br />

without additive, that was turned with insert CCGT09T308-UM (CT5015) and feed rate<br />

0.1 mm/r. The MnS and MnX variants were turned with insert CCMT09T308-WF (GC3215)<br />

and feed rate 0.3 mm/r. With addition <strong>of</strong> MnS the gain in tool life and productivity is<br />

remarkable, three times as high. Even the addition <strong>of</strong> MnX is beneficial with respect to<br />

productivity. Insert geometry and feed rate will by natural causes influence the surface<br />

roughness <strong>of</strong> the machined part. With the wiper geometry CCMT09T308-WF a lasting<br />

5<br />

Presented at <strong>PM</strong>2004, in Vienna, Austria, October 2004<br />

+ MnS<br />

CCMT09T308-WF<br />

Vc = 250 m/min<br />

f = 0.3 mm/r<br />

ap = 0.5 mm<br />

With cutting fluid<br />

+ MnX<br />

CT5015 GC3215 GC3215<br />

f = 0.2mm/r<br />

f = 0.3mm/r<br />

Without additive, insert CCGT09T308-UM (CT5015), f = 0.1 mm/r<br />

With 0.5% MnS, insert CCMT09T308-WF (GC3215)<br />

Without additive, f = 0.3 mm/r<br />

1<br />

100 200 250 300 400<br />

1000<br />

Cutting Speed [m/min]


surface quality will be obtained on parts made <strong>of</strong> AstaloyCrM + 0.5% MnS, even with feed<br />

0.3 mm/r [Fig. 11]<br />

Gain (relatively)<br />

4<br />

3<br />

2<br />

1<br />

0<br />

Gain "Tool life" Gain "Productivity"<br />

Without additive With MnX With MnS<br />

Figure 10: Comparison <strong>of</strong> tool life and productivity.<br />

Vc = 250 m/min, ap = 0.5 mm, with cutting fluid.<br />

Presented at <strong>PM</strong>2004, in Vienna, Austria, October 2004<br />

Surface roughness Ra [µm]<br />

3,5<br />

3,0<br />

2,5<br />

2,0<br />

1,5<br />

1,0<br />

0,5<br />

0,0<br />

GC3215-KM<br />

GC3215-WF<br />

CCMT09T308 (-WF, KM)<br />

Vc = 250 m/min,<br />

f = 0.3 mm/r<br />

ap = 0.5 mm<br />

With cutting fluid<br />

0 5 10 15 20 25<br />

Tool contact time [min]<br />

Figure 11: Surface roughness vs. cutting time.<br />

Astaloy CrM + 0.5% MnS<br />

6


Discussion<br />

The use <strong>of</strong> cutting fluid has in previous investigations not been recommended in turning<br />

operations with <strong>PM</strong> steel material because <strong>of</strong> the observed wear effects [5]. However, with<br />

respect to the bainitic AstaloyCrM without additive, when the choice is between a<br />

predictable and controlled wear (with cutting fluid) or an unpredictable and uncontrolled (dry)<br />

the choice whether cutting fluid should be used or not appears obvious.<br />

For comparative reasons all tool life tests have been performed with cutting fluid. Yet, the<br />

turning operation <strong>of</strong> the additive variants would most likely perform as well, or even better, in<br />

dry condition.<br />

Conclusions<br />

A. Turning <strong>of</strong> bainitic Astloy CrM without additive:<br />

• The dominating wear mechanism is adhesion in terms <strong>of</strong> BUE and pressure-welded<br />

material on clearance flank.<br />

• The adhesion wear is reduced by using as sharp cutting edges as possible, increasing the<br />

cutting speed and the use <strong>of</strong> cutting fluid.<br />

• Best machining performance is achieved by using cermet grade CT5015.<br />

• It is not possible to use high feed rates and productive wiper inserts. A higher load will<br />

increase the adhesion wear.<br />

B. Turning <strong>of</strong> bainitic Astaloy CrM with additive:<br />

• The machining exhibits a completely different behaviour compared to the non additive<br />

variant. BUE and smearing tendencies are in principle eliminated.<br />

• One <strong>of</strong> the general machining recommendations for <strong>PM</strong>-material is to use as sharp cutting<br />

edges as possible. This recommendation is not so important when MnS and MnX are<br />

added to the tested <strong>PM</strong> material.<br />

• Best machining performance is achieved with hard metal grade GC3215.<br />

• Three times higher productivity and tool life is achieved by MnS compared with variant<br />

without additive.<br />

• Three times higher productivity is achieved by additive MnX compared with variant<br />

without additive.<br />

• The best overall performance is obtained with AstaloyCrM + 0.5% MnS. Excellent<br />

results have been achieved, both in tool life and surface roughness, with feed rates up to<br />

0.3 mm/r together with the high productive wiper insert, CCMT09T308-WF.<br />

References:<br />

1. Berg, S. ”Cutting data Recommendations for Turning <strong>of</strong> Various P/M Materials Using<br />

Different Tool Grade and Geometry Selections”. Paper presented at 1998 Powder<br />

Metallurgy World Congress, Granada, Spain October 1998.<br />

2. Berg, S., Måhrs, O. ”Investigating the Relationship Between Machinability Additives and<br />

<strong>Machining</strong> Parameters”. Paper presented at <strong>PM</strong> 2 Tec2001, New Orleans, USA, May 2001.<br />

3. Lindberg, C. ”Mechanical Properties <strong>of</strong> a Water Atomized Fe-Cr-Mo Powder and How to<br />

Sinter it”. Paper presented at <strong>PM</strong> 2 Tec1999, Vancouver, Canada, June 1999.<br />

4. <strong>AB</strong> Sandvik Coromant. Catalogue: “Metal Working Products – Turning Tools 2003”<br />

5. <strong>Höganäs</strong> handbook for sintered components. ”5. <strong>Machining</strong> Guidelines”.<br />

Presented at <strong>PM</strong>2004, in Vienna, Austria, October 2004<br />

7

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