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Glycerol and spent lye clarification - Illinois Institute of Technology

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means must be employed to render them insol-<br />

uble. This is best accomplished by the<br />

addition <strong>of</strong> metallic salts, forming insoluble<br />

metallic oompo-unds, which are coagulated when<br />

the <strong>lye</strong> is neutralized.<br />

The chief aim in using a metallic salt<br />

in the purification <strong>of</strong> soap <strong>lye</strong>s is the removal<br />

<strong>of</strong> the soaps <strong>of</strong> the lower fatty acids, formic,<br />

acetic, butyric, caprylic, etc,.<br />

The amount <strong>of</strong> aluminum sulphate to be<br />

used depends on the cleanliness <strong>of</strong> the <strong>lye</strong><br />

<strong>and</strong> its freedom from soap <strong>and</strong> gelatinous<br />

matters. The least amount that will give a<br />

good cake in the filter press <strong>and</strong> not gum the<br />

cloths is the amount to use. This salt can<br />

bo added either dry or dissolved in water <strong>and</strong><br />

will neutralize about one third its weight <strong>of</strong><br />

caustic soda. An exoess <strong>of</strong> caustic soda in<br />

the <strong>lye</strong> has the tendency to form aluminum<br />

hydrate which will retard filtering.<br />

There are anumber <strong>of</strong> compounds on the<br />

market for which special advantages in <strong>lye</strong>

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