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Glycerol and spent lye clarification - Illinois Institute of Technology

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solution. Chloridea may be removed by the<br />

addition <strong>of</strong> some soluble silver salt such as<br />

the nitrate, or the oxide, silver chloride<br />

being precipitated <strong>and</strong> filtered from the<br />

solution.<br />

Proteins <strong>and</strong> some other organic substances<br />

can <strong>of</strong>ten be removed completely by precipitat-<br />

ing the slightly alkaline solution with zinc<br />

chloride. The precipitate is filtered <strong>of</strong>f<br />

<strong>and</strong> the filtrate rendered slightly acid when<br />

further precipitation will <strong>of</strong>ten occur.<br />

The last traces <strong>of</strong> zinc may be removed from<br />

the solution by adding potassium ferrocyanide,<br />

which is also a very good precipitant <strong>of</strong><br />

albumen.<br />

At the present writing there seems to be<br />

no accurate method for the determination <strong>of</strong><br />

glycerol <strong>of</strong> all percentages in complex<br />

mixtures. In aqueous solutions glycerol can<br />

be determined accurately by means <strong>of</strong> specific<br />

gravity <strong>and</strong> refractive index, Lenz recommends<br />

that the refractive index <strong>of</strong> glycerol solution<br />

17

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