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New Scientific Opportunities at the European Synchrotron Radiation ...

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<strong>European</strong> <strong>Synchrotron</strong> Radi<strong>at</strong>ion Facility Long-Term Str<strong>at</strong>egy 7 July 2006<br />

• regular organis<strong>at</strong>ion of intern<strong>at</strong>ional nanoscience meetings<br />

• setting up a central d<strong>at</strong>abase for various nanofocusing optics (CRL, Fresnel<br />

zone pl<strong>at</strong>es, mirrors, crystals etc.).<br />

Combin<strong>at</strong>ion of microanalytical techniques include:<br />

• Microtomography combined with various spectroscopic techniques (e.g.<br />

XRF/XRD/XANES/EXAFS) should be pursued with nanoscopic resolution. In<br />

this respect <strong>the</strong> stability of micro- (nano-) EXAFS represents a serious<br />

problem even on <strong>the</strong> micrometer scale, which should be taken into account<br />

during <strong>the</strong> developments of micro-spectroscopy beam lines.<br />

• Combin<strong>at</strong>ion of X-ray imaging with electron microscopy, which would be very<br />

useful for nanoimaging and sample visualis<strong>at</strong>ion when optical microscopy<br />

reaches its <strong>the</strong>oretical limits of resolution.<br />

Fur<strong>the</strong>r developments are needed in <strong>the</strong> field of d<strong>at</strong>a evalu<strong>at</strong>ion for phase-contrast<br />

imaging techniques. A task-force should be cre<strong>at</strong>ed for improving <strong>the</strong> coordin<strong>at</strong>ion<br />

among phase-retrieval techniques developments. On-line d<strong>at</strong>a reduction/evalu<strong>at</strong>ion<br />

in general is an important issue for imaging and scanning micro-spectroscopy, and its<br />

development should be fur<strong>the</strong>r pursued.<br />

Oversubscription is a serious issue <strong>at</strong> imaging beamlines, <strong>the</strong>refore <strong>the</strong> increase in<br />

<strong>the</strong> number of end-st<strong>at</strong>ions will be a positive development. The possibility of external<br />

staffing via partnerships should be considered, possibly via 7 th framework EUprojects.<br />

Report on <strong>the</strong> discussion held during <strong>the</strong> parallel session of <strong>the</strong> Surface and<br />

Interface Science Group: Chris Lucas (UO), Joerg Zegenhagen (ESRF)<br />

Christian Mocuta (ID1) gave <strong>the</strong> first present<strong>at</strong>ion showing examples of micro-beam<br />

diffraction studies of nanotubes and Ge pyramids on Si and coherent X-ray diffraction<br />

measurements from Au microcrystals. Joerg Zegenhagen <strong>the</strong>n summarised <strong>the</strong><br />

group activities on beamlines ID1, ID3 and ID32. Olaf Magnussen (University of Kiel),<br />

gave an excellent introduction to <strong>the</strong> electrochemical interface and <strong>the</strong>n described<br />

some recent results concerning Au homoepitaxy, hydrogen evolution on Pt and liquid<br />

mercury electrodes.<br />

The talks were followed by detailed question and answer sessions from a packed<br />

audience. The ESRF long term str<strong>at</strong>egy (LTS) document was summarised by Chris<br />

Lucas as a lead-in to <strong>the</strong> discussion session where <strong>the</strong> questions summarised <strong>at</strong> <strong>the</strong><br />

head of this Section were addressed.<br />

This gener<strong>at</strong>ed a gre<strong>at</strong> deal of discussion as to <strong>the</strong> potential limit<strong>at</strong>ions in studying<br />

single nanoparticles and exactly how long a beamline would have to be in order to<br />

have sufficient space around a sample. The highest priority for infrastructure support<br />

was deemed to be detector development. It was pointed out th<strong>at</strong> <strong>the</strong>re appeared to<br />

be a gap in <strong>the</strong> accessible energy range of synchrotron sources in <strong>the</strong> range 20-50<br />

keV and <strong>the</strong> ESRF could fill this gap. Looking <strong>at</strong> <strong>the</strong> future it was noted th<strong>at</strong> <strong>the</strong> LTS<br />

describes a str<strong>at</strong>egy th<strong>at</strong> would be governing experiments performed in 5-10 years. It<br />

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