Bayer CropScience AG Page 1 of 82 BCS-RD-D ... - IR-4 Project

Bayer CropScience AG Page 37 of 82
BCS-RD-D-ROCS Method-No. 00857
D-40789 Monheim Report No. MR-099/04
5.4 LOQ, LOD, Recovery Rates and Repeatability (contd)
Table 14: Recoveries for BYI08330-ketohydroxy; RSD: Relative Standard Deviation.
Crop
Fortification
Level (FL) (mg/kg)
Recoveries %
(Single Values)
Mean
(%)
per FL
RSD
(%)
Mean
(%)
overall
RSD (%)
overall
Orange
0.01 88 93 71 87 69 82 13.3
Fruit 1.0 90 88 94 91 96 92 3.5 87 10.7
Orange
0.01 96 91 93 93 2.7
Juice 1.0 71 88 93 84 13.7 89 10.2
Orange
0.01 93 107 92 97 8.6
Pomace 1.0 95 83 71 83 14.5 90 13.5
Orange
0.01 97 100 101 99 2.1
Jam 1.0 93 93 98 95 3.0 97 3.5
Sweet Cherry
0.01 98 102 82 94 11.3
Fruit 1.0 95 93 92 93 1.6 94 7.2
Plum
0.01 97 91 100 93 89 94 4.8
Fruit 1.0 94 93 88 85 87 89 4.4 92 5.1
Peach
0.01 89 96 90 92 4.1
Fruit 1.0 97 88 98 94 5.8 93 4.8
Strawberry
0.01 94 88 91 91 3.3
Fruit 1.0 86 89 91 89 2.8 90 3.1
Apple
0.01 90 88 89 79 90 87 5.3
Fruit 1.0 88 90 92 95 92 91 2.9 89 4.7
Apple
0.01 99 98 98 98 0.6
Pomace Dried 1.0 93 95 100 96 3.8 97 2.7
Apple
0.01 89 89 87 83 81 86 4.2
Sauce 1.0 85 80 81 84 82 82 2.5 84 3.9
Tomato
0.01 98 109 106 102 105 104 4.0
Fruit 1.0 101 99 98 99 97 99 1.5 101 4.0
Tomato
0.01 94 99 95 100 93 96 3.2
Juice 1.0 93 91 92 94 92 92 1.2 94 3.2
Tomato
0.01 97 100 94 97 3.1
Preserve 1.0 96 93 97 95 2.2 96 2.6
Grape
0.01 95 97 94 94 97 95 1.6
Bunches of Grape 1.0 98 92 96 94 96 95 2.4 95 1.9
Grape
0.01 98 99 99 99 0.6
Most 1.0 98 96 94 96 2.1 97 2.0
Grape
0.01 102 97 97 99 2.9
Pomace 1.0 92 94 91 92 1.7 96 4.2
Grape
0.01 98 99 96 98 1.6
Wine 1.0 95 91 94 93 2.2 96 3.0
Potato
0.01 95 96 104 95 97 97 3.9
Tuber 1.0 96 96 96 95 96 96 0.5 97 2.8
Melon
0.01 97 95 95 96 1.2
Peel 1.0 90 93 96 93 3.2 94 2.7
Melon
0.01 96 98 102 99 96 98 2.5
Pulp 1.0 92 90 93 93 94 92 1.6 95 3.8
Onion
0.01 96 94 96 91 93 94 2.3
Tuber 1.0 95 94 93 94 92 94 1.2 94 1.7
Hop
0.01 100 90 79 84 101 91 10.7
Beer 1.0 97 94 90 91 96 94 3.3 92 7.5
Hop
0.10 95 94 97 95 1.6
Cone Dried 10.0 93 95 92 93 1.6 94 1.9
Hop
0.10 85 99 110 98 12.8
Cone Green 10.0 84 96 84 88 7.9 93 11.4
Broccoli
0.01 100 105 111 111 91 104 8.1
Curd 1.0 73 92 79 78 93 83 10.8 93 14.6
Cauliflower
0.01 89 98 100 96 6.1
Inflorescence 1.0 89 70 90 83 13.6 89 11.9
Lettuce
0.01 98 80 91 90 10.1
Head 1.0 97 94 86 92 6.2 91 7.6