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BCS-RD-D-ROCS Method-No. 00857
D-40789 Monheim Report No. MR-099/04
5.4 LOQ, LOD, Recovery Rates and Repeatability (contd)
Table 16: Recoveries for BYI08330-enol-Glc; RSD: Relative Standard Deviation.
Crop
Fortification
Level (FL) (mg/kg)
Recoveries %
(Single Values)
Mean
(%)
per FL
RSD
(%)
Mean
(%)
overall
RSD (%)
overall
Orange
0.01 91 94 70 86 70 82 14.0
Fruit 1.0 85 100 96 101 100 96 6.9 89 13.0
Orange
0.01 91 96 91 93 3.1
Juice 1.0 71 94 95 87 15.7 90 10.5
Orange
0.01 90 89 87 89 1.7
Pomace 1.0 98 90 77 88 12.0 89 7.7
Orange
0.01 100 96 92 96 4.2
Jam 1.0 93 91 90 91 1.7 94 4.0
Sweet Cherry
0.01 99 106 88 98 9.3
Fruit 1.0 89 90 87 89 1.7 93 8.2
Plum
0.01 102 100 96 95 102 99 3.4
Fruit 1.0 94 89 85 83 86 87 4.9 93 7.6
Peach
0.01 91 91 102 95 6.7
Fruit 1.0 98 88 98 95 6.1 95 5.7
Strawberry
0.01 102 94 94 97 4.8
Fruit 1.0 84 90 92 89 4.7 93 6.4
Apple
0.01 86 86 91 75 95 87 8.7
Fruit 1.0 87 85 91 91 92 89 3.4 88 6.3
Apple
0.01 90 95 99 95 4.8
Pomace Dried 1.0 85 86 88 86 1.8 91 6.0
Apple
0.01 94 96 90 92 91 93 2.6
Sauce 1.0 90 89 91 90 91 90 0.9 91 2.3
Tomato
0.01 103 97 99 96 101 99 2.9
Fruit 1.0 97 97 98 97 96 97 0.7 98 2.3
Tomato
0.01 96 100 95 98 98 97 2.0
Juice 1.0 90 91 90 93 91 91 1.3 94 3.9
Tomato
0.01 94 92 85 90 5.2
Preserve 1.0 89 90 91 90 1.1 90 3.4
Grape
0.01 93 95 93 98 93 94 2.3
Bunches of Grape 1.0 93 90 90 92 91 91 1.4 93 2.6
Grape
0.01 93 91 94 93 1.6
Most 1.0 92 92 91 92 0.6 92 1.3
Grape
0.01 94 93 92 93 1.1
Pomace 1.0 78 79 81 79 1.9 86 8.8
Grape
0.01 90 92 92 91 1.3
Wine 1.0 92 94 92 93 1.2 92 1.4
Potato
0.01 89 95 93 96 89 92 3.6
Tuber 1.0 91 89 88 89 87 89 1.7 91 3.4
Melon
0.01 89 89 94 91 3.2
Peel 1.0 88 90 95 91 4.0 91 3.2
Melon
0.01 94 96 91 90 92 93 2.6
Pulp 1.0 87 87 91 90 91 89 2.3 91 3.0
Onion
0.01 90 86 92 85 90 89 3.3
Tuber 1.0 89 88 87 91 89 89 1.7 89 2.5
Hop
0.01 99 83 75 88 97 88 11.2
Beer 1.0 94 97 98 99 92 96 3.0 92 8.7
Hop
0.10 89 92 93 91 2.3
Cone Dried 10.0 88 80 79 82 6.0 87 6.9
Hop
0.10 86 97 97 93 6.8
Cone Green 10.0 81 89 83 84 4.9 89 7.7
Broccoli
0.01 103 100 109 103 83 100 9.9
Curd 1.0 71 86 73 79 88 79 9.5 90 15.1
Cauliflower
0.01 92 104 87 94 9.3
Inflorescence 1.0 81 73 80 78 5.6 86 12.6
Lettuce
0.01 98 82 99 93 10.3
Head 1.0 92 90 85 89 4.1 91 7.5