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ANNUAL <strong>2010</strong>/<strong>2011</strong><br />

OF THE CROATIAN ACADEMY<br />

OF ENGINEERING


CROATIAN ACADEMY OF ENGINEERING<br />

Annu. Croat. Acad. Eng. ISSN 1332-3482<br />

ANNUAL <strong>2010</strong>/<strong>2011</strong><br />

OF THE CROATIAN ACADEMY<br />

OF ENGINEERING<br />

Editor-in-Chief<br />

Vilko Žiljak<br />

Zagreb, 2012


Published by<br />

Croatian Academy <strong>of</strong> Engineering,<br />

28 Kai St., 10000 Zagreb, Croatia<br />

Editor-in-Chief<br />

Pr<strong>of</strong>. Vilko Žiljak, Ph.D.,<br />

Vice president <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Editorial Board<br />

Pr<strong>of</strong>. Stanko Tonkovi, Ph.D.<br />

Pr<strong>of</strong>. Vilko Žiljak, Ph.D.<br />

Pr<strong>of</strong>. emer. Zlatko Kniewald, Ph.D.<br />

ISSN 1332-3482<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Annu. Croat. Acad. Eng.<br />

Prepress and Press<br />

INTERGRAFIKA, Zagreb<br />

Circullation<br />

300


Table <strong>of</strong> contents<br />

B. Pribievi, D. Medak, A. apo<br />

GEODETIC CONTRIBUTION TO THE GEODYNAMIC RESEARCH<br />

OF THE AREA OF THE CITY OF ZAGREB .................................................... 11<br />

Drago Katovi, Andrea Katovi, Marija Krnevi<br />

SPANISH BROOM (SPARTIUM JUNCEUM L.) .............................................. 23<br />

Matanovi Davorin, Moslavac Bojan, Nediljka Gaurina-Meimurec<br />

THE WAY TO REDUCE PIPE WEARING WHILE DRILLING ...................... 38<br />

Dinko Mikuli, Vladimir Koroman<br />

FUNDAMENTALS OF MILITARY PRODUCTION DEVELOPMENT IN<br />

THE CROATIAN WAR FOR INDEPENDENCE FROM 1991 TO 1993 .......... 46<br />

Darko Stipaniev<br />

INTELLIGENT FOREST FIRE MONITORING SYSTEM – FROM<br />

IDEA TO REALIZATION ................................................................................... 58<br />

Igor Petrovi, Davorin Kovai<br />

LABORATORY TESTING AND NUMERICAL MODELLING OF MBT<br />

WASTE DEFORMABILITY ............................................................................... 74<br />

Darko Dujmovi, Boris Androi, Ivan Lukaevi<br />

BEAM-TO-COLUMN JOINT MODELLING TO EC3 ...................................... 89<br />

Darko Dujmovi, Boris Androi, Josip Piskovic<br />

MODELLING OF JOINT BEHAVIOUR IN STEEL FRAMES ...................... 109<br />

Juraj Božievi, Marijan Andrašec<br />

DEVELOPMENT STRATEGY OF ECOINDUSTRAL PARK<br />

RAŠA - EIPR ..................................................................................................... 121<br />

Marijan Bošnjak<br />

POSIBLE MODEL OF MATHEMATICAL EVALUATION OF<br />

BEHAVIOUR DISORDER THERAPY ............................................................ 136


Mario Žagar, Ivica Crnkovi, Darko Stipaniev, Maja Štula, Juraj Feljan, Luka<br />

Lednicki, Josip Maras, Ana Petrii<br />

DICES: DISTRIBUTED COMPONENT-BASED EMBEDDED<br />

SOFTWARE SYSTEMS ................................................................................... 154<br />

Martin Žagar, Hrvoje Mlinari, Josip Knezovi<br />

FRAMEWORK FOR 3D MOTION FIELD ESTIMATION AND<br />

RECONSTRUCTION........................................................................................ 168<br />

Gaurina-Meimurec Nediljka, Pašic Borivoje, Matanovi Davorin<br />

LABORATORY EVALUATION OF MUD DIFFERENTIAL STICKING<br />

TENDENCY AND SPOTTING FLUID EFFECTIVENESS ............................ 184<br />

Ružica unko, Sanja Ercegovi Raži<br />

USE OF PLASMA TECHNOLOGY FOR MODIFICATION<br />

OF TEXTILES ................................................................................................... 199<br />

Žaneta Ugari-Hardi<br />

IMPORTANCE OF SALT CONTENT REDUCTION IN<br />

BAKERY PRODUCTS ...................................................................................... 213


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 7<br />

Croatian Academy <strong>of</strong> Engineering is sponsoring scientic meetings, symposia and<br />

conferences organized by <strong>the</strong> Departments and Centers <strong>of</strong> <strong>the</strong> Academy. Important<br />

events in <strong>the</strong> Croatian Academy <strong>of</strong> Engineering in <strong>2010</strong> and <strong>2011</strong> are:<br />

<strong>2010</strong><br />

25th Annual Assembly <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering was held on<br />

March 27th, <strong>2010</strong> where Awards <strong>of</strong> <strong>the</strong> Academy for 2009 were granted and <strong>the</strong><br />

new Statute <strong>of</strong> <strong>the</strong> Academy adopted.<br />

In accordance with <strong>the</strong> provisions <strong>of</strong> <strong>the</strong> new Statute <strong>of</strong> <strong>the</strong> Academy, a new categorization<br />

<strong>of</strong> membership in <strong>the</strong> Academy was implemented. The most important<br />

innovation is <strong>the</strong> termination <strong>of</strong> Associate Members <strong>of</strong> <strong>the</strong> Academy and <strong>the</strong> transition<br />

<strong>of</strong> Associates and Members into <strong>the</strong> unique status <strong>of</strong> a Full Member <strong>of</strong> <strong>the</strong><br />

Academy.<br />

Annual 2009 <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering with <strong>the</strong> new Who is Who<br />

in <strong>the</strong> Croatian Academy <strong>of</strong> Engineering was published.<br />

President <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia Pr<strong>of</strong>. Ivo Josipovi, Ph.D. visited <strong>the</strong> Academy<br />

on September 15th, <strong>2010</strong>.<br />

In November <strong>2010</strong> <strong>the</strong> Academy submitted its comments on <strong>the</strong> draft <strong>of</strong> <strong>the</strong> Law<br />

on Science to <strong>the</strong> Ministry <strong>of</strong> Science, Education and Sports <strong>of</strong> <strong>the</strong> Republic <strong>of</strong><br />

Croatia.


8<br />

<strong>2011</strong><br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Croatian Academy <strong>of</strong> Engineering became a partner in EU SETA - South East<br />

Transport Axis. The holder <strong>of</strong> <strong>the</strong> project activities from <strong>the</strong> part <strong>of</strong> <strong>the</strong> Academy is<br />

its Center for Trafc Engineering and distinguished experts from <strong>the</strong> Department<br />

<strong>of</strong> Transport <strong>of</strong> <strong>the</strong> Academy have taken part in <strong>the</strong> project.<br />

On January 14th, <strong>2011</strong> <strong>the</strong> Academy organized a conference entitled "Engineering<br />

Ethics and <strong>the</strong> Croatian Economy" at <strong>the</strong> Faculty <strong>of</strong> Electrical Engineering and<br />

Computing in Zagreb.<br />

In <strong>the</strong> organization <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering and <strong>the</strong> Ministry <strong>of</strong><br />

Science, Education and Sports <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia, under <strong>the</strong> auspices <strong>of</strong> <strong>the</strong><br />

President <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia, Central Celebration <strong>of</strong> <strong>the</strong> 300th Anniversary<br />

<strong>of</strong> <strong>the</strong> Birth <strong>of</strong> Ruer Boškovi was held at <strong>the</strong> Vatroslav Lisinski Concert Hall on<br />

May 17, <strong>2011</strong>.<br />

On <strong>the</strong> same day, after <strong>the</strong> celebration, 26th Annual Assembly <strong>of</strong> <strong>the</strong> Croatian<br />

Academy <strong>of</strong> Engineering was held upon which Academy Awards for <strong>2010</strong> were<br />

presented.<br />

Co-organized by <strong>the</strong> Biotechnical Center <strong>of</strong> <strong>the</strong> Academy, Faculty <strong>of</strong> Food Technology<br />

and Biotechnology <strong>of</strong> <strong>the</strong> University <strong>of</strong> Zagreb and <strong>the</strong> Centre for Environment<br />

Protection and Development <strong>of</strong> Sustainable Technologies <strong>of</strong> <strong>the</strong> Academy,<br />

international symposium "The life and Achievements <strong>of</strong> Pr<strong>of</strong>. Emer. Vera Johanides<br />

" was held on September 28th, <strong>2011</strong>, and her memorial bust was unveiled<br />

in front <strong>of</strong> <strong>the</strong> House <strong>of</strong> <strong>the</strong> Academy in 28 Kai St., Zagreb.<br />

Bulletin <strong>of</strong> <strong>the</strong> Academy in Croatian and English "Tehnike znanosti / Engineering<br />

Power vol. 10 (1) <strong>2011</strong> was published.<br />

2012<br />

Bulletin <strong>of</strong> <strong>the</strong> Academy in Croatian and English "Tehnike znanosti / Engineering<br />

Power vol. 10 (special issue) <strong>2011</strong> entirely devoted to Ruer Boškovi and 300th<br />

anniversary <strong>of</strong> his birth was published.<br />

In March 2012 Croatian Academy <strong>of</strong> Engineering signed Agreement on Scientic<br />

and Technical Cooperation with <strong>the</strong> Academy <strong>of</strong> Medical Sciences <strong>of</strong> Croatia,<br />

Croatian Academy <strong>of</strong> Legal Sciences and <strong>the</strong> Academy <strong>of</strong> Forestry Sciences.<br />

Organized by <strong>the</strong> Scientic Committee for Agriculture and Forestry <strong>of</strong> <strong>the</strong> Croatian<br />

Academy <strong>of</strong> Sciences and Arts and Biotechnical Center <strong>of</strong> <strong>the</strong> Croatian Academy<br />

<strong>of</strong> Engineering, a scientic conference "Food as <strong>the</strong> Foundation <strong>of</strong> Health and<br />

Longevity" was held on June 18th 2012.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 9<br />

In September 2012 representatives <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering met<br />

with <strong>the</strong> delegation <strong>of</strong> <strong>the</strong> Chinese Academy <strong>of</strong> Engineering (CAE) in Zagreb.<br />

CAE representatives were: Pr<strong>of</strong>. Pan Yunhe, Executive Vice President <strong>of</strong> CAE,<br />

Pr<strong>of</strong>. Zheng Xiaoguang and Wang Xiaowen, Ph.D., Deputy Directors <strong>of</strong> <strong>the</strong> Department<br />

for International Cooperation <strong>of</strong> CAE, and Ms. Zhang Song, Secretary<br />

to Pr<strong>of</strong>. Pan Yunhea. On behalf <strong>of</strong> <strong>the</strong> Academy Chinese delegation was received<br />

by Pr<strong>of</strong>. V. Žiljak, Ph.D.,Vice President, and members <strong>of</strong> <strong>the</strong> Academy N. Peri,<br />

Dean <strong>of</strong> <strong>the</strong> Faculty <strong>of</strong> Electrical Engineering and Computing, and Pr<strong>of</strong>. M. Cifrek,<br />

Ph.D. The meeting was also attended by a group <strong>of</strong> scientists from <strong>the</strong> Faculty <strong>of</strong><br />

Electrical Engineering and Computing.<br />

At <strong>the</strong> conference “The Future <strong>of</strong> Printing” held in September <strong>of</strong> this year Pr<strong>of</strong>.<br />

Anayath Rejendrakumar from India gave a comprehensive overview <strong>of</strong> <strong>the</strong> state<br />

and development <strong>of</strong> graphics technology in <strong>the</strong> world. The lecture was held at <strong>the</strong><br />

Croatian Chamber <strong>of</strong> Commerce in <strong>the</strong> presence <strong>of</strong> many engineers and members<br />

<strong>of</strong> <strong>the</strong> Academy.


10<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

In November 2012 <strong>the</strong> Department <strong>of</strong> Systems and Cybernetics and <strong>the</strong> Centre for<br />

Development Studies and Projects <strong>of</strong> <strong>the</strong> Academy started "Talks about <strong>the</strong> Present<br />

and Future <strong>of</strong> Engineering and Biotechnological Sciences," as an activity <strong>of</strong> <strong>the</strong><br />

Academy members who would at <strong>the</strong>ir monthly meetings reect upon important<br />

development issues.<br />

Information about <strong>the</strong> events associated with <strong>the</strong> Academy could be found on our<br />

web site: www.hatz.hr


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 11<br />

Geodetic Contribution to <strong>the</strong> Geodynamic Research<br />

<strong>of</strong> <strong>the</strong> Area <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb<br />

B. Pribičević, D. Medak, and A. Đapo<br />

University <strong>of</strong> Zagreb,<br />

Faculty <strong>of</strong> Geodesy<br />

email: {bpribic, dmedak, adapo}@ge<strong>of</strong>.hr<br />

ABSTRACT<br />

Paper presents 11 year long interdisciplinary research <strong>of</strong> geodynamic processes <strong>of</strong> <strong>the</strong> area<br />

<strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb. The Geodynamic GPS-Network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb represents <strong>the</strong><br />

longest and <strong>the</strong> most intensive research effort in <strong>the</strong> eld <strong>of</strong> geodynamics in Croatia. Since<br />

<strong>the</strong> establishment <strong>of</strong> <strong>the</strong> Network in 1997, several series <strong>of</strong> precise GPS measurements<br />

have been conducted on specially stabilized points <strong>of</strong> Geodynamical Network <strong>of</strong> City <strong>of</strong><br />

Zagreb with purpose <strong>of</strong> investigation <strong>of</strong> tectonic movements and related seismic activity <strong>of</strong><br />

<strong>the</strong> wider area <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb. The Network has been densied in 2005 in <strong>the</strong> most<br />

active region <strong>of</strong> nor<strong>the</strong>astern Mount Medvednica. Since <strong>the</strong>n, several GPS campaigns have<br />

been conducted. Processing <strong>of</strong> observation data was done with scientic s<strong>of</strong>tware GAMIT/<br />

GLOBK, developed by MIT. From this series <strong>of</strong> GPS measurements geodetic model <strong>of</strong><br />

tectonic movements has been created. In <strong>the</strong> area <strong>of</strong> interest, independent geological investigations<br />

have been conducted through even longer period <strong>of</strong> time which resulted in<br />

geological model <strong>of</strong> tectonic movements. The correlation coefcient between geodetic and<br />

geologic model has been calculated and shows high degree <strong>of</strong> correlation thus giving credibility<br />

to both methods <strong>of</strong> research. Systematic analysis has been conducted over geodetic<br />

and geologic results giving as a result unique interdisciplinary model <strong>of</strong> crust movements<br />

over wider Zagreb area. This interdisciplinary interpretation <strong>of</strong> obtained geodetic movements<br />

leads to a new scientic insight about geodynamics <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb area. The<br />

results <strong>of</strong> this scientic research will be used to delineate zones <strong>of</strong> potential earthquake<br />

hazard or tectonically caused landslides.<br />

Keywords: geodesy, GPS, geodynamics, GAMIT, tectonics<br />

Introduction<br />

It has been known for a long time that <strong>the</strong> wider area <strong>of</strong> Zagreb is geodynamically active,<br />

(Prelogovi, Cvijanovi 1981) (Kuk et al. 2000), (Kuk et al. 2000a), (Tomljenovi, 2002)<br />

however, <strong>the</strong>re were no data on <strong>the</strong> actual size <strong>of</strong> those movements, nor on <strong>the</strong>ir spatial orientation.<br />

The rst geodetic research in this direction was made through <strong>the</strong> implementation<br />

<strong>of</strong> <strong>the</strong> project <strong>the</strong> “Basic GPS network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb” (oli et al. 1999) (Medak,<br />

Pribievi 2001).<br />

Through <strong>the</strong> realization <strong>of</strong> <strong>the</strong> project “Basic GPS-Network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb” in 1997,<br />

Croatian capital got a modern, geodetic foundation <strong>of</strong> high accuracy. Network was planned<br />

as <strong>the</strong> basis for investigations <strong>of</strong> tectonic movements and related seismic activity <strong>of</strong> <strong>the</strong><br />

wider area <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb. Basic part <strong>of</strong> <strong>the</strong> network consists <strong>of</strong> 43 specially stabilized<br />

geodetic points to meet <strong>the</strong> specic criteria for geodynamic points. After <strong>the</strong> second<br />

series <strong>of</strong> GPS measurements in year 2001, <strong>the</strong> network has become “Geodynamic Network<br />

<strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb” (Medak, Pribievi 2001), (Medak, Pribievi 2002), (Medak,


12<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Pribievi 2003). The City <strong>of</strong> Zagreb has recognized <strong>the</strong> importance <strong>of</strong> this project and<br />

GPS campaigns have been performed in years 2004, 2006, 2007 and in 2008 (Pribievi et<br />

al 2004), (Medak et al 2007a).<br />

After six series <strong>of</strong> GPS-measurements in period from 1997 to 2008, <strong>the</strong> analysis <strong>of</strong> <strong>the</strong> results<br />

with scientic s<strong>of</strong>tware GAMIT/GLOBK show signicant movement on GPS points<br />

as a result <strong>of</strong> geodynamic activity in <strong>the</strong> research area (Medak, Pribievi 2004), (Medak,<br />

Pribievi 2006), (Pribievi et al. 2007), (apo 2005), (apo 2009). From <strong>the</strong> analysis results<br />

<strong>the</strong> geodetic model <strong>of</strong> tectonic movements has been created and scientic comparison<br />

with geologic model created on <strong>the</strong> basis <strong>of</strong> age-long research. The correlation coefcient<br />

between geodetic and geologic model has been calculated and shows high degree <strong>of</strong> correlation<br />

thus giving credibility to both methods <strong>of</strong> research. Systematic analysis has been<br />

conducted over geodetic and geologic results giving as a result unique interdisciplinary<br />

model <strong>of</strong> crust movements over wider Zagreb area (apo et al. 2009), (apo 2009).<br />

Geodynamic Network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb<br />

Underlying network has already in its preliminary design devised a dual role: rst it was<br />

<strong>the</strong> basis for <strong>the</strong> establishment <strong>of</strong> homogeneous GPS network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb, while<br />

since 2001 it has became <strong>the</strong> “Geodynamic Network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb. Such role was<br />

possible primarily due to development <strong>of</strong> GPS technology and achieving high accuracy,<br />

which made possible measurement <strong>of</strong> geodynamic movements (Blewitt 1993), (Bock et al.<br />

1993), (Segall, Davis 1997). This fact now allows geodesy to actively participate toge<strong>the</strong>r<br />

with o<strong>the</strong>r pr<strong>of</strong>essions and disciplines in <strong>the</strong> important interdisciplinary research for <strong>the</strong><br />

City <strong>of</strong> Zagreb.<br />

The aim <strong>of</strong> such a special geodetic network is determination <strong>of</strong> actual geodynamic movements<br />

over a longer period <strong>of</strong> time with very high accuracy. This research represents a<br />

qualitative contribution to <strong>the</strong> geodetic pr<strong>of</strong>ession in a variety <strong>of</strong> interdisciplinary research,<br />

such as monitoring <strong>of</strong> earthquake prediction indicators in Zagreb and its surroundings.<br />

Thus, modern geodesy with its high accuracy enters in an entirely new area <strong>of</strong> research<br />

with purpose <strong>of</strong> determining new parameters microseismic zoning and landslide monitoring<br />

in <strong>the</strong> area <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb. Today, in this type <strong>of</strong> research, toge<strong>the</strong>r with geologists,<br />

seismologists, geotechnicists, geophysicists and o<strong>the</strong>r scientists, <strong>the</strong>ir signicant<br />

contribution may be given by <strong>the</strong> geodesists (Altiner 1999.), (Altiner et al. 2001), (Medak<br />

et al. 2002), (Grenercy, 2005), (Pinter et al. 2004).<br />

It goes without saying that this segment <strong>of</strong> <strong>the</strong> research is <strong>of</strong> great importance because <strong>the</strong><br />

City <strong>of</strong> Zagreb has <strong>the</strong> highest concentration <strong>of</strong> population and industry in <strong>the</strong> Republic <strong>of</strong><br />

Croatia. Therefore, it is certain that even now <strong>the</strong> city administration should think about<br />

measures to be taken in order to preserve human life and property in case <strong>of</strong> natural disasters<br />

such as earthquakes, landslides and similar. Figures 1-7 show cracks and damages on<br />

<strong>the</strong> objects in <strong>the</strong> Zagreb area due to tectonic movements.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 13<br />

Figure 1: a, b) Cracks in <strong>the</strong> wall <strong>of</strong> <strong>the</strong> church <strong>of</strong> St. Marie in Granešina with marked direction<br />

<strong>of</strong> <strong>the</strong> sliding – size <strong>of</strong> <strong>the</strong> cracks is between 5-10 cm (c) Example o <strong>the</strong> cracks parallel to <strong>the</strong><br />

orientation <strong>of</strong> local compression stress above south church window; (d) same crack extended to<br />

<strong>the</strong> road between <strong>the</strong> church and <strong>the</strong> rectory (Medak et al 2007b)<br />

Figure 2. Gornja Planina, Podizeljska Street 12 – a) crack on <strong>the</strong> concrete oor parallel to <strong>the</strong><br />

fault from zone Stubica-Kašina b) In <strong>the</strong> house yard a concrete curb with a crack <strong>of</strong> 1.5 cm in<br />

size, created in just one year. (apo 2005)<br />

Figure 3. Example <strong>of</strong> cracks due to movements in <strong>the</strong> zone <strong>of</strong> Zagreb fault - Vidovec – cracks 4<br />

cm wide (apo 2009)


14<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 4. a) Donja Planina, Planinarska Street 21. Whole house has been cut with <strong>the</strong> crack <strong>of</strong><br />

NNW-SSE direction. On <strong>the</strong> facade a signicant horizontal right shift <strong>of</strong> 2 cm is notable. The<br />

facade was made two years prior; b). Donja Planina 13- south facade – cracks with horizontal<br />

right movement with size 3cm (apo 2009).<br />

Figure 5. During 2006 year in <strong>the</strong> period <strong>of</strong> a relatively larger displacement amplitudes measured<br />

at points Geodynamic network, in fault zone Stubica-Kašina landslides were activated. Particularly<br />

activated was <strong>the</strong> well known landslide in <strong>the</strong> Planina Gornja. Figure shows <strong>the</strong> cracking <strong>of</strong><br />

<strong>the</strong> road (apo 2009).<br />

Figure 6. a) In Gornji Mikulii on <strong>the</strong> route <strong>of</strong> main fault <strong>of</strong> <strong>the</strong> Zagreb zone <strong>the</strong> landslide has<br />

been reactivated in 2008. b) Particularly noticeable are shifts <strong>of</strong> <strong>the</strong> ground north <strong>of</strong> <strong>the</strong> road,<br />

where considerable damage to fences has been recorded (apo 2009).


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 15<br />

Figure 7: In <strong>the</strong> spring <strong>of</strong> 2008 a new landslide in Vidovec was created. Landslide is located<br />

within <strong>the</strong> route <strong>of</strong> <strong>the</strong> main faults <strong>of</strong> <strong>the</strong> Zagreb fault zone. In <strong>the</strong> overlying wing <strong>of</strong> <strong>the</strong> cliffs<br />

<strong>the</strong>re is a fault in <strong>the</strong> relief. Due to tectonic activity <strong>the</strong>re was an escarpment destabilization and<br />

<strong>the</strong> activation <strong>of</strong> landslides (apo 2009).<br />

Design and <strong>the</strong> stabilization <strong>of</strong> <strong>the</strong> Geodynamic Network<br />

Given <strong>the</strong> size <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb and <strong>the</strong> need to encompass <strong>the</strong> wider area, <strong>the</strong> Geodynamic<br />

network covers an area <strong>of</strong> app. 700 km 2 . The main characteristic <strong>of</strong> this mostly raster<br />

formatted network is that <strong>the</strong> distance between points is approximately seven kilometers in<br />

a sparsely populated area, and in urban areas <strong>of</strong> <strong>the</strong> City, density is slightly higher. Namely,<br />

given <strong>the</strong> fact that <strong>the</strong> City <strong>of</strong> Zagreb is seismically very active, <strong>the</strong> Network is designed so<br />

that <strong>the</strong> recent structural fabric <strong>of</strong> <strong>the</strong> Zagreb area is optimally covered. Network points are<br />

placed in relation to fault zones to positions that will show <strong>the</strong> truest geodynamic movements<br />

in <strong>the</strong> research area. Figure 8 shows <strong>the</strong> placement <strong>of</strong> <strong>the</strong> points in <strong>the</strong> Zagreb area<br />

and positions <strong>of</strong> main faults and epicenters <strong>of</strong> largest earthquakes in <strong>the</strong> area.<br />

Figure 8. Locations <strong>of</strong> <strong>the</strong> Geodynamic network points and positions <strong>of</strong> main faults and epicenters<br />

<strong>of</strong> largest earthquakes in <strong>the</strong> area (apo 2005)


16<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Thanks to <strong>the</strong> signicant increase in accuracy, dependence <strong>of</strong> geodetic data on time (<strong>the</strong><br />

fourth dimension) is apparent. That is why special attention has been paid to <strong>the</strong> stabilization<br />

<strong>of</strong> <strong>the</strong> points <strong>of</strong> <strong>the</strong> geodynamic network. The aim was to ensure <strong>the</strong> stability <strong>of</strong> points<br />

over a longer period <strong>of</strong> time and provide accurate reoccupation <strong>of</strong> GPS antenna. In this way<br />

determination <strong>of</strong> actual geodynamic displacements was enabled with very high accuracy<br />

over a longer period (Solari, 1999), (Schmitt, 1985), (Gerasimenko et al. 2000).<br />

Works on <strong>the</strong> stabilization <strong>of</strong> points <strong>of</strong> <strong>the</strong> Geodynamic network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb were<br />

performed according to <strong>the</strong> design created by <strong>the</strong> experts from <strong>the</strong> University <strong>of</strong> Zagreb,<br />

Faculty <strong>of</strong> Geodesy, with <strong>the</strong> interdisciplinary help <strong>of</strong> engineers, geologists and seismologists.<br />

The Geodynamic network consists <strong>of</strong> more than 40 specially stabilized points on wider<br />

area <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb and covers area <strong>of</strong> about 700km2 (oli et al 1999), (Medak,<br />

Pribievi 2002).<br />

In total <strong>the</strong>re were 33 pillars built, 32 <strong>of</strong> which come with <strong>the</strong> above ground stabilization,<br />

and only one with <strong>the</strong> sub terrain stabilization (1028 King Tomislav Square). The remaining<br />

7 points <strong>of</strong> <strong>the</strong> Geodynamic network has a different stabilization, which also meets all<br />

<strong>the</strong> stability requirements that are set before this special network (Medak, Pribievi 2002)<br />

(Pribievi et al 2007).<br />

As shown on <strong>the</strong> gure 1, most <strong>of</strong> <strong>the</strong> monuments have pilots that go up to 14 meters deep<br />

to consolidated ground. On <strong>the</strong> top <strong>of</strong> every monument is a steel mark with winding for <strong>the</strong><br />

special extension thus insuring stability <strong>of</strong> points through long periods <strong>of</strong> time and precise<br />

GPS antenna reoccupation.<br />

Figure 9. Specially stabilized monument on Geodynamic network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb<br />

After seven years <strong>of</strong> intensive research, it became clear that <strong>the</strong> Geodynamic network must<br />

be densied in <strong>the</strong> seismotectonically most active area. Densifying is <strong>of</strong> particular importance<br />

for <strong>the</strong> preliminary assessment <strong>of</strong> <strong>the</strong> landslide susceptibility in those urban areas<br />

that lie on <strong>the</strong> clay layers in <strong>the</strong> nor<strong>the</strong>rn part <strong>of</strong> <strong>the</strong> zone: Šestine Grmošica, Granešina,<br />

Mikulii, Vugrovec and Kašina. In year 2005, ve new geodynamic points were established<br />

in that part <strong>of</strong> Zagreb (Medak et al. 2007a).


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 17<br />

GPS-observations<br />

Since 1997 GPS measurements on <strong>the</strong> Geodynamic network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb were<br />

conducted through GPS measurement campaigns every few years. Each campaign consists<br />

<strong>of</strong> two to three 24 hour sessions. First two campaigns in 1997 and 2001 had tree 24 hour<br />

sessions with 15 second observation interval, thus giving 5670 epochs. All later campaigns<br />

had 24 hour sessions but with 30 second interval, giving 2880 epochs (Medak et al 2007a)<br />

(apo 2009).<br />

Figure 10. Distribution <strong>of</strong> points according to <strong>the</strong> observation sessions (2004, 2006, 2008)<br />

All conducted campaigns had only Trimble GPS receivers and antennas. There were 8<br />

conducted GPS campaigns: 1997, 2001, 2003, 2004, 2005, 2006, 2007 and 2008. Only<br />

ve <strong>of</strong> those were observation <strong>of</strong> complete Geodynamic network: 1997, 2001, 2004, 2006,<br />

and 2008 (41 points). Two campaigns were conducted for observing densication points<br />

2005, 2007 (11 and 21 points) (Pribievi et al. 2007) (apo et al. 2009). Table 1 shows all<br />

conducted campaigns including number <strong>of</strong> points and used instruments<br />

Table 1: GPS campaigns on Geodynamic network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb<br />

Campaign Date sessions points receivers<br />

Zagreb 1997 27.-29.10.1997. 2 43 27<br />

Zagreb 2001 25.-28.06.2001. 3 40 16<br />

Zagreb 2003 22.-23.06.2003. 1 13 13<br />

Zagreb 2004 17.-20.06.2004. 3 39 13<br />

Zagreb 2005 10.-11.09.2005. 1 11 11<br />

Zagreb 2006 22.-25.06.2006. 3 41 13<br />

Zagreb 2007 13.-15.07.2007. 2 21 13<br />

Zagreb 2008 10.-13.06.2008. 3 41 13


18<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 11: Velocity rates and <strong>the</strong>ir error ellipses for period 2006-2007 (apo 2009), (Wessel 2004)<br />

Table 2: Statistical representation <strong>of</strong> absolute values <strong>of</strong> velocity rates for 2006–2007 in mm/yr.<br />

v<br />

v<br />

v hz<br />

mm/yr<br />

v H<br />

mm/yr<br />

min. 0,2 0,57 1,43 0,60<br />

max. 10,70 19,36 19,37 50,27<br />

avg. 3,14 4,86 6,43 16,25<br />

Velocity rates calculated for <strong>the</strong> complete period from 1997 to 2008 are much smaller due<br />

to different active zones <strong>of</strong> <strong>the</strong> Zagreb area from year to year giving thus sometimes opposite<br />

velocity directions for <strong>the</strong> same points. Velocity rates for <strong>the</strong> period 1997 to 2008<br />

are shown in Figure 12 and Table 3 shows statistical representation <strong>of</strong> absolute values <strong>of</strong><br />

velocity rates for period 1997–2008 in mm/yr.<br />

Table 3: Statistical representation <strong>of</strong> absolute values <strong>of</strong> velocity rates for 1997–2008 in mm/yr.<br />

v v<br />

v hz<br />

v H<br />

mm/yr mm/yr<br />

min. 0,03 0,04 0,12 0,02<br />

max. 3,93 3,42 4,34 17,48<br />

avg. 0,83 1,03 1,45 1,97


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 19<br />

Figure 13: Geodetic velocity model created using IDW interpolation<br />

with respect to faults model<br />

(1)<br />

Table 4: Correlation coefcient by Spearman formula<br />

Calculating <strong>of</strong> correlation coefcient by above given formula (1) for Spearman rank correlation<br />

we get rs=0.94 with 1% signicance level (or 99% in Gaussian model).<br />

The correlation coefcient between geodetic and geologic model shows high degree <strong>of</strong> correlation<br />

thus giving credibility to both methods <strong>of</strong> research (apo 2009).


20<br />

CONCLUSION<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Geodynamic study <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb has started in 1997 and since 2008 <strong>the</strong>re has<br />

been seven GPS campaigns for <strong>the</strong> purpose <strong>of</strong> determining geodynamic movements on <strong>the</strong><br />

points <strong>of</strong> <strong>the</strong> Geodynamic network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb.<br />

Through <strong>the</strong> project Geodynamic study <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb, based on independent multiple<br />

precise geodetic and geological measurements, original models <strong>of</strong> tectonic movements<br />

on Zagreb area have been created. Geodetic model is based on precise GPS satellite<br />

measurements, and geological model is based on <strong>the</strong> long-term geologic measurements<br />

and studies. For this purpose data collected through GPS measurements on seven GPS<br />

measurement campaigns in <strong>the</strong> period since 1997 until 2008. Year has been used. GPS<br />

measurements were processed in <strong>the</strong> scientic GAMIT/GLOBK s<strong>of</strong>tware, designed at MIT<br />

specically for processing GPS measurements on <strong>the</strong> geodynamic network. It calculated<br />

<strong>the</strong> geodynamic movements on <strong>the</strong> points <strong>of</strong> <strong>the</strong> Geodynamic network using modern methods<br />

<strong>of</strong> Kalman ltering.<br />

The result <strong>of</strong> <strong>the</strong> velocity models at <strong>the</strong> points Geodynamic network were obtained for <strong>the</strong><br />

period 1997- 2001, 2001-2004, 2004-2006, 2006-2007, 2007-2008, 2006-2007-2008 and<br />

cumulatively for <strong>the</strong> whole period from 1997-2008. The maximum absolute value <strong>of</strong> displacement<br />

for <strong>the</strong> total solution in <strong>the</strong> horizontal direction is 4.3mm/yr in vertical direction<br />

17.5mm/yr. The largest absolute values <strong>of</strong> displacements were obtained during <strong>the</strong> period<br />

2006-2007 and are amounted to 19.4mm/yr and 50.3mm/yr in <strong>the</strong> horizontal and vertical<br />

direction respectively. It is evident that it represents signicant geodynamic movements.<br />

However, it should be noted that <strong>the</strong> mean value <strong>of</strong> velocity is 3 mm/yr.<br />

Velocity model <strong>of</strong> geodynamic movements for <strong>the</strong> whole period <strong>of</strong> <strong>the</strong> study has been created<br />

using IDW interpolation method with <strong>the</strong> inclusion <strong>of</strong> fault models <strong>of</strong> <strong>the</strong> Zagreb area.<br />

In that way <strong>the</strong> original geodetic model <strong>of</strong> <strong>the</strong> velocity eld for <strong>the</strong> wider area <strong>of</strong> <strong>the</strong> City<br />

<strong>of</strong> Zagreb.<br />

Geostatistical analysis has been performed and <strong>the</strong> correlation coefcient has been calculated<br />

for <strong>the</strong> geodetic and geological model <strong>of</strong> <strong>the</strong> geodynamic movements, by using<br />

Spearman correlation coefcient formula. The resulting value <strong>of</strong> 0.94 with signicance<br />

level <strong>of</strong> 1% (or 99% in Gaussian model) indicates a high degree <strong>of</strong> correlation between<br />

<strong>the</strong> geodetic and geological model <strong>of</strong> <strong>the</strong> geodynamic movements in <strong>the</strong> subject area. This<br />

proves <strong>the</strong> credibility <strong>of</strong> eleven year long research independently conducted by geological<br />

and geodetic methods.<br />

In conclusion, it can be stated that as part <strong>of</strong> this research a unique interdisciplinary model<br />

<strong>of</strong> crust movements over wider Zagreb area has been created for <strong>the</strong> rst time. It can be<br />

applied to precisely dene <strong>the</strong> boundaries <strong>of</strong> seismic micro-zoning <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb.<br />

On <strong>the</strong> o<strong>the</strong>r hand, results <strong>of</strong> <strong>the</strong> study can help in decision making process about reconstruction<br />

and adaptation <strong>of</strong> important structures (reinforcement <strong>of</strong> foundations and structural<br />

elements) and also <strong>the</strong>y can be used to more accurately dene <strong>the</strong> zones <strong>of</strong> landslides<br />

caused by tectonic movements.<br />

REFERENCES<br />

1. Altiner, Y. (1999). Analytical Surface Deformation Theory for Detection <strong>of</strong> <strong>the</strong> Earth’s<br />

Crust Movements. Springer Verlag.<br />

2. Altiner, Y., Marjanovi-Kavanagh, R., Medak, D., Medi, Z., Prelogovi, E., Pribievi,<br />

B., et al. (2001). Is Adria a Promontory or does it exist as an Independent Microplate?<br />

In J. Sledzinski (Ed.), Proceedings <strong>of</strong> <strong>the</strong> EDS G9 Symposium “Geodetic and Geodynamic<br />

Programmes <strong>of</strong> <strong>the</strong> CEI (Central European Initiative), 25-30 March 2001.


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Reports on Geodesy (p. 225-229). Nice, France: Warsaw University <strong>of</strong> Technology.<br />

3. Blewitt G. (1993): Advances in Global Positioning System technology for geodynamics<br />

investigations: 1978–1992. In Contrib. Space Geodesy Geodyn.: Technol. Geodyn.,<br />

Geodyn. Ser., ed. DE Smith, DL Turcotte, 25: 195–213. Washington, DC: Am.<br />

Geophys. Union. 213 pp.<br />

4. Bock Y., D., Agnew, Fang, P., Genrich, J., Hager, B., Herring, T., Hudnut, K., et al.<br />

(1993). Detection <strong>of</strong> crustal deformation from <strong>the</strong> Landers earthquake sequence using<br />

continuous geodetic measurements. Nature, 361 , 337-340<br />

5. oli, K., Prelogovi, E., Pribievi, B., Švehla, D. (1999). Hrvatski geodinamiki<br />

projekt CRODYN i GPS mreža Grada Zagreba. In A. Baji (Ed.), Znanstveni skup<br />

Andrija Mohorovii - 140. obljetnica roenja: zbornik radova (p. 141-152). Zagreb:<br />

Državni hidrometeorološki zavod.<br />

6. Dong, D., Herring, T., & King, R. (1998). Estimating regional deformation from a<br />

combination <strong>of</strong> space and terrestrial geodetic data. Journal <strong>of</strong> Geodesy, 72 (4), 200-<br />

214.<br />

7. apo, A. (2005). Obrada i interpretacija geodetskih mjerenja na geodinamikoj mreži<br />

Grada Zagreba. magistarski rad. Zagreb: Geodetski fakultet, 12.05. 2005., 174 str.<br />

Voditelj: Medak, Damir.<br />

8. apo, A (2009): Korelacija geodetskog i geološkog modela tektonskih pomaka na<br />

primjeru šireg podruja Grada Zagreba. doktorska disertacija. Zagreb: Geodetski<br />

fakultet, 08.05. 2009, 199 str. Voditelj: Pribievi, Boško.<br />

9. apo, Almin; Pribievi, Boško; Medak, Damir; Prelogovi, Eduard (2009): Correlation<br />

between Geodetic and Geological Models in <strong>the</strong> Geodynamic Network <strong>of</strong> <strong>the</strong> City<br />

Of Zagreb. Reports on geodesy. 86 (2009), 1; p 115-122.<br />

10. Grenerczy, G., Sella, G., Stein, S., Kenyeres, A. (2005). Tectonic implications <strong>of</strong> <strong>the</strong><br />

GPS velocity eld in <strong>the</strong> nor<strong>the</strong>rn Adriatic region. Geophys. Res. Lett., 32 .<br />

11. Gerasimenko, M. D., Shestakov, N. V., Teruyuki, K. (2000). On optimal geodetic network<br />

design for fault-mechanics studies (Vol. 52). Earth Planets Space.<br />

12. Herring, T., King, R., McClusky, S. (2006a). Documentation for <strong>the</strong> MIT Global Kalman<br />

lter VLBI and GPS analysis program: GLOBK 10.3. Cambridge.<br />

13. Herring, T., King, R., McClusky, S. (2006b). Documentation for <strong>the</strong> MIT GPS analysis<br />

s<strong>of</strong>tware: GAMIT 10.3. Cambridge.<br />

14. Kuk, V., Prelogovi, E., Dragievi, I. (2000). Seismotectonically Active Zones in <strong>the</strong><br />

Dinarides. Geol. Croatica, 53 (2), 295-303.<br />

15. Kuk, V., Prelogovi, E., Sovi, L., Kuk, K., Mari, K. (2000a). Seizmološke i seizmotektonske<br />

znaajke šireg zagrebakog podruja. Graevinar, 52 (11), 647-653.<br />

16. Medak, D., Pribievi, B. (2001). Geodynamic GPS-Network <strong>of</strong> <strong>the</strong> City <strong>of</strong> Zagreb<br />

- First Results. In The Stephan Mueller topical conference <strong>of</strong> <strong>the</strong> European Geophysical<br />

Society: Quantitative neotectonic and seismic hazard assessment: new integrated<br />

approaches for environmental management. Balatonfüred, Hungary.<br />

17. Medak, D., Pribievi, B. (2002). Geodinamika mreža Grada Zagreba. In T. Baši<br />

(Ed.), Zbornik Geodetskog fakulteta Sveuilišta u Zagrebu povodom 40. obljetnice<br />

samostalnog djelovanja 1962-2002. pp. 145-156. Zagreb.<br />

18. Medak, D., Pribievi, B., Prelogovi, E. (2002). Determination <strong>of</strong> <strong>the</strong> recent structural<br />

fabric in <strong>the</strong> Alps-Dinarides area by combination <strong>of</strong> geodetic and geologic methods.<br />

In M. Brilly (Ed.), Raziskave s podroja geodezije in geozike. p. 57-64. Ljubljana:<br />

Slovensko združenje za geodezijo in geoziko.<br />

19. Medak, D., Pribievi, B. (2003). Processing <strong>of</strong> Geodynamic GPSNetworks with<br />

GAMIT S<strong>of</strong>tware. Reports on Geodesy, Warsaw University <strong>of</strong> Technology, 64 (1),<br />

75-84.


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20. Medak, D., Pribievi, B. (2004). Processing <strong>of</strong> Geodynamic GPS networks in Croatia<br />

with GAMIT S<strong>of</strong>tware. In N. Pinter, G. Grenerczy, J. Webber, S. Stein, & D. Medak<br />

(Eds.), The Adria Microplate: GPS Geodesy, Tectonics and Hazards (Vol. 61, p. 247-<br />

256). Veszprem, Hungary: Springer.<br />

21. Medak, D., Pribievi, B. (2006): Processing <strong>of</strong> geodynamic GPS-networks in Croatia<br />

with GAMIT s<strong>of</strong>tware, The Adria Microplate, GPS Geodesy, Tectonics and Hazards /<br />

Pinter, Nicholas et al. (eds).<br />

22. Medak, D., Pribievi, B., apo, A. (2007a). Progušenje toaka Geodinamike mreže<br />

Grada Zagreba u podsljemenskoj zoni. Geodetski list , 61(84)(4), 247-258.<br />

23. Medak, D., Pribievi, B., Prelogovi, E., apo, A. (2007b). Primjene geodetskogeodinamikih<br />

GPS-mjerenja za monitoring tektonski uvjetovanih klizišta. In Simpozij<br />

o inženjerskoj geodeziji (p. 229-241). Beli Manastir.<br />

24. Pinter, N, Grenerczy, G., Webber, J., Stein, S., Medak, D. (Eds.) (2004), The Adria<br />

Microplate: GPS Geodesy, Tectonics and Hazards .Vol. 61. Veszprem, Hungary:<br />

Springer.<br />

25. Prelogovi, E., Cvijanovi, D. (1981). Potres u Medvednici 1880. godine. Geol. vjesnik<br />

(34), 137-146.<br />

26. Pribievi, B., Medak, D., Prelogovi, E. (2004). Geodinamika prostora Grada Zagreba.<br />

Geodetski list , 58(81)(1), 51-65.<br />

27. Pribievi, B., Medak, D., Prelogovi, E., apo, A. (2007). Geodinamika prostora<br />

Grada Zagreba. Zagreb: Geodetski fakultet Sveuilište u Zagrebu. Znanstvena monograja.<br />

28. Schmitt, G. (1985). Review <strong>of</strong> network design: Criteria, risk functions, design ordering.<br />

In Grafarend & F. Sanco (Eds.), Optimization and design <strong>of</strong> geodetic network (p.<br />

610). Berlin etc.: Springer.<br />

29. Segall, P., Davis, L. J. (1997): GPS Applications for Geodynamics and Earthquake<br />

Studies. Annual Review <strong>of</strong> Earth and Planetary Sciences. Vol. 25: 301-336. May 1997.<br />

30. Solari, M. (1999). Suradnja srednje europskih zemalja u geodeziji i geodinamici.<br />

In A. Baji (Ed.), Znanstveni skup Andrija Mohorovii - 140. obljetnica roenja:<br />

zbornik radova (p. 165-177). Zagreb: Državni hidrometeorološki zavod.<br />

31. Šoši, I. (2004). Primijenjena statistika. Zagreb: Školska knjiga, Udžbenici Sveuilišta<br />

u Zagrebu.<br />

32. Tomljenovi, B. (2002). Strukturne znaajke Medvednice i Samoborskog gorja. Doktorska<br />

disertacija. Rudarsko-geološko-naftni fakultet, Zagreb.<br />

33. Wessel, P., Smith, W. H. F. (2004). The Generic Mapping Tools – Technical Reference<br />

and Cookbook (4th ed.).


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 23<br />

Drago Katović, Ph.D.<br />

Spanish Broom (Spartium Junceum L.)<br />

University <strong>of</strong> Zagreb<br />

Faculty <strong>of</strong> Textile Technology<br />

Zagreb, Prilaz baruna Filipovića 28A<br />

e-mail: dkatovic@ttf.hr<br />

Andrea Katović PhD<br />

University <strong>of</strong> Calabria, Faculty <strong>of</strong> Engineering Department <strong>of</strong> Chemical Engineering<br />

and Materials Via P.Bucci, Cubo 44 A, Rende (CS), Italy<br />

(e-mail: katovic@unical.it)<br />

Marija Krnčević B.Sc. <strong>of</strong> Ethnology and Archeology,<br />

Museum <strong>of</strong> Šibenik, Gradska vrata 3<br />

marija.krncevic@muzej-sibenik.hr)<br />

LA GINESTRA<br />

O IL FIORE DEL DESERTO<br />

Qui<br />

su l’arida schiena<br />

Del formidabil monte<br />

Sterminator Vesevo,<br />

La qual null’altro allegra arbor né ore<br />

Tuoi cespi solitari intorno spargi<br />

Odorata ginestra,<br />

Contenta dei deserti …<br />

Giacomo Leopardi<br />

Abstract<br />

The Spanish Broom (Spartium Junceum L.) plant is almost a forgotten textile raw material.<br />

This paper presents a review <strong>of</strong> procedures practiced in <strong>the</strong> past and nowadays for obtaining<br />

bers from this plant. It discusses new discoveries about its use as a component <strong>of</strong><br />

special composite bers, as well as its possible benets in households <strong>of</strong> poorer limestone<br />

areas. It also reports on come chemical and physical properties <strong>of</strong> <strong>the</strong> bers extracted from<br />

local plants.<br />

Key words: Spanish Broom, maceration, composites, ash, Klason lignin, cellulose, hemcellulose,<br />

FTIR, SEM, microwave, composites<br />

Introduction<br />

Whilst ax and hemp have mostly been used as textile raw material <strong>of</strong> cellulosic origin


24<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

in plains, in coastal areas <strong>of</strong> <strong>the</strong> Mediterranean wild Spanish Broom has been used as<br />

raw textile material since ancient times. However, Spanish Broom (Spartium Junceum L.)<br />

(Croatian: žuka or brnistra; Italian: ginestra) is almost completely forgotten today, and it is<br />

only sporadically mentioned as raw textile material. The habitat <strong>of</strong> Spanish Broom is <strong>the</strong><br />

Mediterranean area <strong>of</strong> south Europe, south-west Asia and north-west Africa. In Italy, in <strong>the</strong><br />

Mediterranean area <strong>of</strong> olive groves, it climbs <strong>the</strong> altitude <strong>of</strong> 975 meters. In Turkey, Syria<br />

and Palestine, it reaches altitudes <strong>of</strong> 1,700 meters. It is regarded weed in <strong>the</strong> USA and New<br />

Zealand; where <strong>the</strong>re is a tendency to eradicate it in order to save indigenous plants.<br />

Figure 1 Spartium Junceum L.<br />

There are numerous anatomic adjustments to dry soil visible in microscopic structures <strong>of</strong><br />

Spanish Broom’s vegetative organs. One <strong>of</strong> <strong>the</strong>m is xerophtytic (xerophytes – types <strong>of</strong><br />

plants adjusted to dry climate) adjustment <strong>of</strong> <strong>the</strong> leaf during its short life span and transformation<br />

<strong>of</strong> its internal structure dominated by <strong>the</strong> chain <strong>of</strong> parenchyma. The upper part<br />

<strong>of</strong> <strong>the</strong> stem took over <strong>the</strong> function <strong>of</strong> leaf, whereas sclerenchyma’s bers and conductive<br />

elements take over <strong>the</strong> majority part <strong>of</strong> its secondary units. An unusual feature <strong>of</strong> <strong>the</strong> root’s<br />

primary structure is its underdeveloped endoderm, and <strong>the</strong> secondary structure points to<br />

its storage and mechanical roles. [1]. Morphological structures <strong>of</strong> Spanish Broom, more<br />

precisely its longitudinal and cross-section <strong>of</strong> shoots were recorded with a FE-SEM (Field<br />

Emission-Scanning Electron Microscope) <strong>of</strong> <strong>the</strong> company TESCAN, with a steamer and<br />

unit for EDX analysis (Energy Dispersive X-Ray Analysis). Before <strong>the</strong> microscopic recording,<br />

samples were processed for 180 seconds in a steamer with gold and palladium, using<br />

operative voltage <strong>of</strong> 5-15 kV. The results <strong>of</strong> images show that Spanish Broom’s shoots<br />

have two basic layers: rigid and woody inner layer, porous in <strong>the</strong> middle part, making <strong>the</strong><br />

plant light, and an outer layer, skin intertwined with sinewy bers. The cross-section <strong>of</strong>


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 25<br />

Spanish Broom also points to epidermis, parenchyma <strong>of</strong> <strong>the</strong> bark with chlorophyll, endoderm,<br />

bundles <strong>of</strong> root bers and bundles <strong>of</strong> pericyle bers. Head shaped units <strong>of</strong> root and<br />

pericycle bers, connected in an almost continuous ring, are also visible.<br />

Figure 2 SEM micrograph <strong>of</strong> cross-section <strong>of</strong> Spanish Broom vermenes (SEM) Hitachi S-3400 N<br />

Cross-section <strong>of</strong> <strong>the</strong> woody shoot <strong>of</strong> Spanish Broom, which give rigidness to <strong>the</strong> shoot, and<br />

enables passage <strong>of</strong> cell juices alongside <strong>the</strong> shoot<br />

Figure 3 SEM micrograph <strong>of</strong> Cross-section <strong>of</strong> <strong>the</strong> woody (lignin) part


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 4 SEM micrograph <strong>of</strong> Cross-section <strong>of</strong> bers <strong>of</strong> Spanish Broom<br />

The cross-section <strong>of</strong> technical bers shows <strong>the</strong>ir irregular shape, with visible regular elementary<br />

circular bers in some places.<br />

Figure 5 Longitudinal micrograph SEM <strong>of</strong> Spanish Broom technical bers with visible elementary<br />

bers (SEM FE/Mira Tescan);


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 27<br />

Figure 6 Elementary ber <strong>of</strong> Spanish Broom, recorded with scanning electron microscope (SEM<br />

FE/Mira Tescan);<br />

THE APPLICATION OF SPANISH BROOM IN HISTORY<br />

Spanish Broom is a plant that was known even to <strong>the</strong> ancient Romans. In <strong>the</strong> past, Greeks,<br />

Romans and Carthaginians used it as raw material for <strong>the</strong> manufacture <strong>of</strong> ropes, nets, bags,<br />

sails. They also used it for covering ro<strong>of</strong>s and even clothing. The ower <strong>of</strong> <strong>the</strong> Spanish<br />

Broom is important for <strong>the</strong> coastal apiculture. Aristotle and Pliny praised <strong>the</strong> honey produced<br />

from Spanish Broom. In general, out <strong>of</strong> all ancient writers about Spanish Broom, it<br />

was Pliny Senior who wrote <strong>the</strong> most. He called it genista and he writes: Ginestra quoque<br />

vinculi,… ores apibus gratissimi (Spanish Broom is used for tying and making crumples,…<br />

and bees <strong>of</strong>ten land on its owers).<br />

However, in several places he mentions a plant called Spartum (Latin form <strong>of</strong> <strong>the</strong> Dioskorides’<br />

description <strong>of</strong> <strong>the</strong> plant sparton). After a detailed analysis <strong>of</strong> <strong>the</strong> application and<br />

processing, it is regarded <strong>the</strong> same plant today, or ra<strong>the</strong>r (Spartium Junceum L.). Already in<br />

<strong>the</strong> period <strong>of</strong> <strong>the</strong> ancient Rome, Spanish Broom elds (genestium – or ager in later Latin)<br />

were cultivated as any o<strong>the</strong>r eld, and <strong>the</strong> plant or sprouts were sown in ploughed up furrows,<br />

as <strong>the</strong> Roman agronomist Columella describes. According to Vergil, hedges <strong>of</strong> Spanish<br />

Broom were planted in addition to willow, hazel, elder and o<strong>the</strong>r plants. Pliny wrote<br />

that <strong>the</strong> sowing and planting <strong>of</strong> Spanish Broom was crucial for peasants. Amongst o<strong>the</strong>r<br />

things, its branches provide excellent material for tying vine and young trees.<br />

The most intensive production <strong>of</strong> Spanish Broom as raw material for obtaining textile fabric<br />

was in Italy during <strong>the</strong> 1930’s, when <strong>annual</strong> production <strong>of</strong> Spanish Broom, due to economic<br />

sanctions in Italy (war in Abyssinia) and <strong>the</strong> proclamation policy <strong>of</strong> self-sufciency,<br />

reached 700,000 tones. It was planted on 300,000 hectares and <strong>the</strong>re were 61 processing<br />

factories [2].


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

However, <strong>the</strong> industrial processing <strong>of</strong> <strong>the</strong> textile raw material completely extinguished in<br />

<strong>the</strong> mid 20th century. There were only several associations <strong>of</strong> Spanish Broom producers<br />

left in Europe that obtained subsidized EU projects with <strong>the</strong> goal <strong>of</strong> maintaining and improving<br />

old crafts. However, during <strong>the</strong> past 10 years <strong>the</strong>re has been a growing interest in<br />

Spanish Broom as raw material in <strong>the</strong> production <strong>of</strong> composite materials.<br />

Findings <strong>of</strong> Liburnian ships, named Serilias, dating from <strong>the</strong> 2nd century, prove that Spanish<br />

Broom was used quite early in our parts <strong>of</strong> <strong>the</strong> Adriatic. The special feature <strong>of</strong> this type<br />

<strong>of</strong> ship is <strong>the</strong> way parts <strong>of</strong> its structure were connected by sewing individual elements. All<br />

dilemmas surrounding this type <strong>of</strong> ship building were resolved by ancient writers, who<br />

also transposed <strong>the</strong> name <strong>of</strong> <strong>the</strong> vessel constructed using this sewing technique. Ancient<br />

writers left us with data about <strong>the</strong> special type <strong>of</strong> vessel used by Liburnians and Histrians<br />

and <strong>the</strong>ir construction techniques. Marcus Verrius Flacus, grammarian from <strong>the</strong> Augustan<br />

period, ga<strong>the</strong>red grammatically interesting, but faintly familiar words in his work De verborum<br />

signicatu. He also mentions <strong>the</strong> name serilia for Istrian and Liburnian ships. This<br />

record came to us through Sextus Pompeious Festus, who lived in <strong>the</strong> 200 AD. He writes:<br />

According to Verrius, Serilia is <strong>the</strong> name for Istrian and Liburnian vessels, compressed<br />

with ax and Spanish Broom ropes. Its name thus derives from <strong>the</strong> Latin word conserere<br />

(string toge<strong>the</strong>r) and contexere (to weave). In his play Niptra, Pacuvius writes: No wooden<br />

pin hold <strong>the</strong> ship’s haul toge<strong>the</strong>r. It is ra<strong>the</strong>r sewn using ax and Spanish Broom ropes. He<br />

used a descriptive expression and invented word for ropes spun from Spanish Broom. [1].<br />

In this area, Spanish Broom was used throughout <strong>the</strong> Middle Ages, according to several<br />

historical records. The oldest record, even though it only mentions Spanish Broom, does<br />

point to its processing for textile purposes. This data is recorded in <strong>the</strong> collection <strong>of</strong> laws<br />

and regulations Statuta et leges civitatis et insulae Curzlae (1214 – 1558). According to<br />

chapter XCVIII, it was prohibited to ga<strong>the</strong>r on moles <strong>of</strong> Zavalatica, Prigradica and Blace,<br />

since <strong>the</strong>y were probably places where women came to soak ax and Spanish Broom. Provisions<br />

for <strong>the</strong> protection <strong>of</strong> useful plants were prescribed quite <strong>of</strong>ten. One <strong>of</strong> <strong>the</strong> examples<br />

is <strong>the</strong> Statute <strong>of</strong> Bra from 1656[3].<br />

The next preserved record on Spanish Broom was written in Glagolitic alphabet and dates<br />

from 1674. It describes <strong>the</strong> area <strong>of</strong> Šibenik. It is a testament and reads: Ostavlan Matii<br />

svekrivi jednu kanicu novu i brnistru, ka j(e) g(o)tova. It is not quite clear what does nished<br />

Spanish Broom actually refer to.<br />

In <strong>the</strong> book Viaggio in Dalmazia, written by <strong>the</strong> famous Italian travel writer Alberto Fortis<br />

in 1774, he describes his visit to <strong>the</strong> island <strong>of</strong> Murter including <strong>the</strong> processing and use <strong>of</strong><br />

Spanish Broom: “The favorite craft <strong>of</strong> Betinjans, population <strong>of</strong> <strong>the</strong> western part <strong>of</strong> <strong>the</strong> island,<br />

is picking, soaking and weaving <strong>of</strong> Spanish Broom which <strong>the</strong>y nd on <strong>the</strong> coast <strong>of</strong> Istria<br />

and islands <strong>of</strong> Kvarner. They make fabric from it, which <strong>the</strong>y use for making sacks and<br />

sometimes shirts and skirts for peasants. There is no doubt this plant could produce far better<br />

artifacts if processed in a more rened manner. They use <strong>the</strong> sea to soak <strong>the</strong> bundles.”<br />

The cultivation <strong>of</strong> Spanish Broom is unfamiliar today in our parts. However, it was widely<br />

spread in <strong>the</strong> past. The shortage <strong>of</strong> textile in 1916 motivated Friar Andrija Rajkovi to use<br />

<strong>the</strong> people’s experience in Spanish Broom processing and use it to a greater extent, even<br />

in industry. He explained to authorities at that time <strong>the</strong> need, benet and possibilities <strong>of</strong><br />

processing Spanish Broom, sending several samples <strong>of</strong> ready-made fabric. In <strong>the</strong> same<br />

memo he writes: For <strong>the</strong> past 40 or 50 years, Spanish Broom has been widely used, but now<br />

manufacturing <strong>of</strong> this type <strong>of</strong> fabric is completely neglected. He also attached a guide How


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 29<br />

to process Spanish broom fabric. [3]<br />

During <strong>the</strong> ‘30s <strong>of</strong> <strong>the</strong> past century, foresters widely recommended <strong>the</strong> cultivation <strong>of</strong> Spanish<br />

Broom (Spartium junceum) in <strong>the</strong> coastal karst areas, more precisely M. Ani Ph. D<br />

in Forest Journal in 1937 and engineer Stane Benko in his booklet on Spanish Broom,<br />

published by <strong>the</strong> Ministry <strong>of</strong> Industry and Mining, in Zagreb, 1946. Member <strong>of</strong> <strong>the</strong> Institute<br />

for Forestry Research Ante Premuži explains <strong>the</strong> possibility <strong>of</strong> using Spanish Broom<br />

for economic purposes in his report Systematic cultivation <strong>of</strong> Spanish broom in our karst<br />

areas, published in <strong>the</strong> Forest Journal. He wrote that diverse biological properties could<br />

be put to good use for forestation <strong>of</strong> poor soil <strong>of</strong> <strong>the</strong> coastal limestone area since Spanish<br />

Broom grows on clay and limestone soil <strong>of</strong> neutral, acid and alkali reaction. Positive sides<br />

<strong>of</strong> its cultivation were highly praised, giving <strong>the</strong>se studies a more propaganda character.<br />

Alongside <strong>the</strong> coast <strong>of</strong> east Adriatic, people used and processed Spanish Broom in various<br />

ways, but it was also harvested in Istria and <strong>the</strong> coastal area <strong>of</strong> Dubrovnik in <strong>the</strong> period <strong>of</strong><br />

Austrian-Hungarian Monarchy, and later between <strong>the</strong> two World Wars. It was <strong>the</strong>n harvested<br />

by <strong>the</strong> army, tied up in bundles and exported to Italy for manufacturing military suits.<br />

There were many attempts <strong>of</strong> industrial processing in our country. Let us remember <strong>the</strong><br />

previously mentioned initiative <strong>of</strong> Rajkovi, which spread across <strong>the</strong> entire Adriatic, gaining<br />

<strong>the</strong> status <strong>of</strong> industrial processing. Immediately after <strong>the</strong> World War I in 1919, <strong>the</strong>re<br />

was an attempt in Omiš to process Spanish Broom in bulk. A factory was also built for its<br />

processing. However, <strong>the</strong> rst attempt failed since Spanish Broom had been soaked in <strong>the</strong><br />

sea for six months, <strong>the</strong>reby rotting. There were no fur<strong>the</strong>r attempts from <strong>the</strong>n on. Only<br />

after <strong>the</strong> end <strong>of</strong> World War II, Spanish Broom was rediscovered, mostly due to a shortage<br />

<strong>of</strong> textile raw material during <strong>the</strong> post-war period.<br />

The processing actually started two years after <strong>the</strong> W. W. II (1947). Around two trucks <strong>of</strong><br />

Spanish Broom, harvested near Rabac and Labin (Istria), were turned over to <strong>the</strong> district <strong>of</strong><br />

Pula to send it for processing in <strong>the</strong> factory in Fažana. It was also decided to build factories<br />

in Vodice and Zakuac near Omiš. There was a second attempt to revive <strong>the</strong> production,<br />

this time using state-<strong>of</strong>-<strong>the</strong> art methods, quite near where <strong>the</strong> rst plant had been constructed<br />

in 1919. The process <strong>of</strong> maceration was chemical, and a device for hot-air drying was<br />

used. In <strong>the</strong> paper factory in Rijeka, a department was turned into a laboratory for testing.<br />

In order to save on transport <strong>of</strong> raw material, someone suggested turning an old ship into a<br />

oating factory, which would cruise in <strong>the</strong> Adriatic and process Spanish Broom, quite expensive<br />

to harvest. The results <strong>of</strong> this test production were taken over for fur<strong>the</strong>r processing<br />

by certain spinning mills in Croatia and Slovenia, and so rst test products were actually<br />

produced. However, <strong>the</strong> process stops <strong>the</strong>re. The whole initiative, which had started positively,<br />

stopped abruptly, allegedly due to high purchasing price, and so traditional processing<br />

remained in <strong>the</strong> hands <strong>of</strong> <strong>the</strong> people. [3].<br />

There were o<strong>the</strong>r attempts to process Spanish Broom industrially. In Vodice, between 1946<br />

and 1949, a factory was built for <strong>the</strong> processing <strong>of</strong> Spanish Broom. It worked until 1954,<br />

when it was shut down due to unprotability. The same factory is scheduled for demolition<br />

today.<br />

According to former workers <strong>of</strong> <strong>the</strong> factory (Tvornica Žuke) in Vodice <strong>the</strong> technological<br />

procedure for obtaining bbers was as follows: branches <strong>of</strong> Spanish Broom with <strong>the</strong>ir<br />

shoots were soaked in sodium alkali for several days. After resting in pools with <strong>the</strong> alkali,<br />

bers would separate from <strong>the</strong> o<strong>the</strong>r parts. Bundles <strong>of</strong> Spanish Broom would be subject<br />

to water jets under pressure <strong>of</strong> four to six atmospheres. The water jets would separate b-


30<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

ers from <strong>the</strong> connective tissue, transferring <strong>the</strong>m to pools for rinsing <strong>of</strong>f <strong>the</strong> alkali. After<br />

air drying, periodic exposure to rain would have a positive effect on <strong>the</strong> quality. Fibers in<br />

<strong>the</strong> shape <strong>of</strong> hemp were <strong>the</strong>n mechanically cleansed from any eventual remainders <strong>of</strong> <strong>the</strong><br />

connective tissue. They were pressed in bales and sent for fur<strong>the</strong>r processing in <strong>the</strong> factory<br />

Duga Resa. The resulting technical bers <strong>of</strong> Spanish Broom were used for producing ropes.<br />

The original use <strong>of</strong> Spanish Broom can be found in Petriani near Zadar. Freshly cut shoots<br />

were chopped and beaten into powder. This powder was sprinkled on a wet mesh, and <strong>the</strong><br />

ingredients which it would absorb, would protect it against rotting. Spanish Broom shoots<br />

were also used for manufacturing smaller-sized coops. [3]<br />

Several associations <strong>of</strong> Spanish Broom producers remain in Europe today. The European<br />

Union allocated subsidies to Italy with a goal <strong>of</strong> preserving and developing old trades.<br />

There is also a craft shop which produces sails made <strong>of</strong> Spanish Broom for <strong>the</strong> reconstruction<br />

<strong>of</strong> old boats. In Pirovac, <strong>the</strong> Porart Association organizes traditional harvesting and<br />

maceration <strong>of</strong> Spanish Broom, once practiced in our parts. (Figure 7-9).<br />

Figure 7 Harvesting <strong>of</strong> Spanish Broom<br />

Figure 8 Tying shoots in bundles - fašine


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 31<br />

Figure 9 Maceration <strong>of</strong> Spanish Broom in <strong>the</strong> sea<br />

There are several items made from Spanish Broom in our museums, or ra<strong>the</strong>r its combination<br />

<strong>of</strong> o<strong>the</strong>r bers. The sheet – lancun – from <strong>the</strong> Island <strong>of</strong> Pag (Jakišnica), 207x160 cm, was<br />

weaved in four threads in approximately 1945. It consists <strong>of</strong> two parts and it was washed and<br />

whitened by damping in dew and sun exposure. It is in good shape, with a few smears.<br />

Figure 10 Lancun (sheet) made <strong>of</strong> Spanish Broom from Pag (collection <strong>of</strong> <strong>the</strong> Museum <strong>of</strong><br />

Ethnography in Split)<br />

Figure 11 Sheet (collection <strong>of</strong> <strong>the</strong> Town Museum <strong>of</strong> Šibenik)


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Cover from <strong>the</strong> Island <strong>of</strong> Capri (local name: klašnje), 130x80 cm. It is mostly made <strong>of</strong><br />

Spanish Broom, whilst old pieces <strong>of</strong> cloth were used for weft. They were <strong>of</strong> uniformed<br />

size, depending on <strong>the</strong> width <strong>of</strong> <strong>the</strong> weaving loom.<br />

Figure 12 Cover (basically Spanish Broom) from Capri (collection <strong>of</strong> <strong>the</strong> Town Museum <strong>of</strong><br />

Šibenik)<br />

The Faculty <strong>of</strong> Textile Technology, within <strong>the</strong> framework <strong>of</strong> <strong>the</strong> Textile Science Research<br />

Center, analyzed a sample <strong>of</strong> a fuse from a Roman ceramic oil lamp found in Split. The<br />

oil lamp dates from <strong>the</strong> 3rd or 4th century AD. Considering this item is so rare, we were<br />

interested from which material <strong>the</strong> fuse was made <strong>of</strong>.<br />

Figure 13 Roman ceramic oil lamp (lucerna)<br />

For <strong>the</strong> purpose <strong>of</strong> <strong>the</strong> fuse analysis, several images were taken with a scanning electron<br />

microscope (SEM) <strong>of</strong> <strong>the</strong> company Tescan Mira/FE .


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 33<br />

Figure 14 - 20 SEM images <strong>of</strong> <strong>the</strong> fuse (variations in zoom)


34<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

The images show bers covered with ashes, but not completely burned (grey part <strong>of</strong> <strong>the</strong><br />

sample). O<strong>the</strong>rwise, <strong>the</strong>y would not be identiable with precision. There are also black<br />

clumps <strong>of</strong> dirt (larger shapeless pieces)<br />

For <strong>the</strong> purpose <strong>of</strong> analyzing <strong>the</strong> fuse FTIR (Fourier Transform Infra Red) specters <strong>of</strong> bers<br />

were also recorded, which might have been used in <strong>the</strong> 3 rd or 4 th century AD in our parts:<br />

cotton, ax, hemp and Spanish Broom. The resulting curves <strong>of</strong> <strong>the</strong> mentioned bers were<br />

compared with <strong>the</strong> spectrum <strong>of</strong> <strong>the</strong> fuse sample.<br />

Figure 21 Fuse spectrum<br />

After attempts <strong>of</strong> separating parts <strong>of</strong> <strong>the</strong> fuse (grey part) from <strong>the</strong> black part, which mostly<br />

contains dirt, <strong>the</strong> difference in FTIR specters was evident, although insufcient for a denite<br />

conclusion. The differences, which relate to a total <strong>of</strong> spikes, double spike at wavelength<br />

ca. 2900 cm -1 , and at 1700 cm -1 (arc) and 1540 cm -1 (spike), represent <strong>the</strong> existence<br />

<strong>of</strong> non-cellulose natural bers (wax, pectin, lignin). At rst glance that would mean it is not<br />

cotton or Spanish Broom. However, this would be acceptable only if we take into consideration<br />

special methods for ber processing, practiced after <strong>the</strong> 19 th century.<br />

It was <strong>the</strong>n assumed, based on <strong>the</strong> color and SEM images, that <strong>the</strong> fuse was actually a<br />

remainder <strong>of</strong> incomplete burning process. FTIR ber specters were <strong>the</strong>n recorded after<br />

burning, and it was concluded it was probably not cotton.<br />

THE APPLICATION OF SPANISH BROOM IN FUTURE<br />

In <strong>the</strong> past, natural bers were not taken into account as reinforcements for polymeric<br />

materials because <strong>of</strong> some problems associated with <strong>the</strong>ir use. Lack <strong>of</strong> good interfacial<br />

adhesion, low degradation temperature, properties variability depending on <strong>the</strong> quality <strong>of</strong><br />

harvest, age and body <strong>of</strong> <strong>the</strong> plant, as well poor resistance against moisture make <strong>the</strong> use<br />

<strong>of</strong> natural ber reinforced composites less attractive than syn<strong>the</strong>tic. However, <strong>the</strong> production<br />

<strong>of</strong> composites reinforced with syn<strong>the</strong>tic bers and matrices (glass, carbon, aramid)<br />

requires a large amount <strong>of</strong> energy, and <strong>the</strong>y are difcult to recycle or <strong>the</strong>y are completely<br />

unrecyclable. Moreover, natural bers in cases <strong>of</strong> re decrease <strong>the</strong> content <strong>of</strong> toxic gases<br />

<strong>of</strong> combustion. [10].<br />

For <strong>the</strong> past several years <strong>the</strong>re has been an increase in <strong>the</strong> number <strong>of</strong> scientic studies


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 35<br />

relating to <strong>the</strong> production <strong>of</strong> Spanish Broom as raw material for composite materials [6-<br />

8]. The advantage <strong>of</strong> Spanish Broom over ax and hemp is that it can grow in <strong>the</strong> most<br />

unfavorable limestone soil; it is resilient to draught; and once planted it can be used during<br />

a period <strong>of</strong> up to twenty years, whilst ax and hemp demand high quality soil each<br />

year. Its cultivation on rocky areas would have several benets. For <strong>the</strong> purpose <strong>of</strong> analyzing<br />

<strong>the</strong> possibility <strong>of</strong> using Spanish Broom as composite material, inborn samples were<br />

harvested in <strong>the</strong> surroundings <strong>of</strong> Šibenik. Freshly picked shoots contained up to 35% <strong>of</strong><br />

moisture, compared with <strong>the</strong> mass <strong>of</strong> samples dried in standard conditions. Samples were<br />

tied in bundles, soaked in sea water for 21 days and <strong>the</strong>n bers were separated from <strong>the</strong><br />

remaining woody part, using a mechanical procedure. This traditional procedure <strong>of</strong> extracting<br />

Spanish Broom was compared with several contemporary processes, using NaOH,<br />

with subsequent <strong>the</strong>rmal processing at 130 °C and rapid decompression. [9]. Processing<br />

would last for approximately six hours, which is signicantly less compared with water<br />

processing between 20 and 80 days. According to <strong>the</strong> latest studies <strong>of</strong> <strong>the</strong> Faculty <strong>of</strong> Textile<br />

Technology – Institute for Textile Technology and Ecology – <strong>the</strong> possibility <strong>of</strong> microwave<br />

processing is currently undergoing research. According to present and promising results,<br />

total maceration period was reduced to 10 minutes, with a signicant decrease in <strong>the</strong> use<br />

<strong>of</strong> applied chemicals.<br />

Figure 22 Energy for production <strong>of</strong> some bers<br />

Energy for production <strong>of</strong> Spanish Broom depends on <strong>the</strong> type <strong>of</strong> applied maceration and<br />

ranges within <strong>the</strong> framework <strong>of</strong> o<strong>the</strong>r natural bers, according to our research.<br />

Cotton Flax Hemp Spanish broom<br />

Tensile strength (MPa) 300-700 500-900 310-750 750<br />

Figure 23 Some natural bers properties<br />

Spanish Broom bers were extracted from <strong>the</strong> plant’s branches harvested in Dalmatia<br />

(Šibenik area) which contained 35 % <strong>of</strong> moisture compared with branches dried under


36<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

standard conditions. The IR spectra <strong>of</strong> <strong>the</strong> ber sample obtained after alkaline extraction<br />

was recorded on <strong>the</strong> ATR-FTIR spectrometer (Spectrum 100, Perkin Elmer), while cotton,<br />

ax and hemp bers were taken as reference samples. From <strong>the</strong> recorded FT-IR spectra <strong>of</strong><br />

<strong>the</strong> ber samples it is visible that all bers have peak characteristic <strong>of</strong> cellulose although<br />

<strong>the</strong>y present some differences (Fig. 24.) The intensity <strong>of</strong> signal at 1734 cm-1 corresponding<br />

to <strong>the</strong> C=C es<strong>the</strong>r band related to pectin is higher in ax than in hemp bers while this<br />

band is not found in Spanish Broom ber sample. On <strong>the</strong> contrary, only a weak peak at<br />

ca. 1500 cm-1 corresponding to <strong>the</strong> C=C in-plane aromatic vibrations from lignin can be<br />

observed in <strong>the</strong> case <strong>of</strong> Spanish Broom bers, providing an ulterior evidence <strong>the</strong> applied<br />

chemical treatment was adequate for <strong>the</strong> almost complete removal <strong>of</strong> non-cellulosic compounds<br />

from <strong>the</strong> Broom bers. On <strong>the</strong> o<strong>the</strong>r hand, <strong>the</strong> two little sharp peaks observed over<br />

a broader peak in <strong>the</strong> area <strong>of</strong> 2850 to 2950 cm -1 , attributed to <strong>the</strong> CH 2<br />

and CH groups <strong>of</strong><br />

long alkyl chains <strong>of</strong> waxes, are present in <strong>the</strong> spectra <strong>of</strong> ax and hemp.<br />

Figure 24 FTIR (Fourier Transform Infra Red) spectra <strong>of</strong> some bast bers compared to <strong>the</strong> cotton<br />

ber<br />

In Fig. 25 <strong>the</strong> FTIR spectra <strong>of</strong> Spanish Broom bers obtained after four different extraction<br />

procedures are presented. According to <strong>the</strong> previously highlighted peaks that point <strong>the</strong><br />

presence <strong>of</strong> pectin, lignin and/or wax, it can be seen that <strong>the</strong> procedures B and D resulted<br />

in <strong>the</strong> best removal <strong>of</strong> <strong>the</strong> non-cellulosic compounds <strong>of</strong> <strong>the</strong> ber. Fiber treatment (B) with<br />

sodium hydroxide at 105 °C for 2 h removes completely wax and lignin while a weak peak<br />

related to pectin at 1740 cm -1 is still visible. On <strong>the</strong> o<strong>the</strong>r hand, ber treatment (D) with<br />

<strong>the</strong> same alkaline solution but heated in a microwave oven for only 10 minutes (900 W)<br />

resulted in greater removal <strong>of</strong> pectins and maybe not total elimination <strong>of</strong> waxes. The latter<br />

treatment seems very promising, especially from <strong>the</strong> economical point <strong>of</strong> view.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 37<br />

Figure 25 FTIR spectrum <strong>of</strong> bers obtained from Spanish Broom applying four different procedures<br />

compared to <strong>the</strong> cotton ber.<br />

REFERENCES<br />

1. Kovaevi Z., Krnevi M., Katovi A. Katovi D.: Brnistra – zaboravljena tekstilna<br />

sirovina Tekstil <strong>2010</strong> –in press<br />

2. http://www.lammatest.rete.toscana.it/lammatest/documenti/ginestra_manuale.pdf<br />

Accessed November <strong>2010</strong><br />

3. Stojanovi A.: Brnestra (Žuka- Spartium Junceum) (1962) Etnološki Zavod Filoz<strong>of</strong>skog<br />

fakelteta Sveuilišta u Zagrebu, 4, 3-45<br />

4. Katovi D., Katovi A., Krnevi M.: Spanish Broom - History and Perspective (Spartium<br />

Junceum), Journal <strong>of</strong> Natural Fibers <strong>2011</strong> - in press<br />

5. Nekkaa S., Chebira F., Haddaoui N.(2006): Effect <strong>of</strong> Fiber Treatment on <strong>the</strong> Mechanical<br />

and Rheological Properties <strong>of</strong> Polypropylene/Broom Fiber Spartium Junceum<br />

Composites Journal <strong>of</strong> Engineering and Applied Sciences 1(3), 278-283<br />

6. Cerchiara,T., Chidichimo G., Ragusa, M.I., Belsito E.L., Liguorib, A. Arioli A. (<strong>2010</strong>):<br />

Characterization and utilization <strong>of</strong> Spanish Broom (Spartium junceum L.) seed oil Industrial<br />

Crops and Products 31, 423–426<br />

7. Avella M., Casale L., Dell’Erba R., Focher B., Martuscelli E., Marzetti A.M. (1998):<br />

Broom Fibers as Reinforcing Materials for Polypropylene-Based Composites J. Appl<br />

Polym Sci 68, 1077–1089<br />

8. Gabriele B., Teresa Cerchiara T., Salerno G., Chidichimo G., Vetere M.V. Alampi C,<br />

Gallucci M.C., Conidi C., Cassano A.( <strong>2010</strong>): A new physical-chemical process for<br />

<strong>the</strong> efcient production <strong>of</strong> cellulose bers from (Spartium junceum L.) Bioresource<br />

Technology 101, 724–729<br />

9. Cerchiara T., Chidichimo G., Gallucci M.C. Vuono D., (<strong>2010</strong>): Effects <strong>of</strong> Extraction<br />

(Spartium junceum L.) Fibres, Fibres & Textiles in Eastern Europe 2(79) 13-16<br />

10. Cristaldi G. Latteri A. Recca G., Cicala G. (<strong>2010</strong>) : Woven Fabric Engineering , Composites<br />

Based on Natursal Fibre Fabrics, Sciyo, Rijeka, pp.317-342, ISBN 978-953-<br />

307-194-7


38<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

THE WAY TO REDUCE PIPE WEARING WHILE DRILLING<br />

Matanović Davorin, Moslavac Bojan, Nediljka Gaurina-Međimurec<br />

University <strong>of</strong> Zagreb<br />

Faculty <strong>of</strong> Mining, Geology and Petroleum Engineering<br />

Pierottijeva 6, 10000 Zagreb, Republic <strong>of</strong> Croatia<br />

Tel. +385 1 5535 835; fax: +385 1 48 36 074<br />

E-mail: dmatan@rgn.hr<br />

Abstract<br />

While drilling <strong>the</strong>re is an additional load on <strong>the</strong> coiled tubing due to friction with <strong>the</strong> well<br />

walls/rocks regardless <strong>the</strong> drilling mode; rotating or sliding. According to recent investigations<br />

fatigue is <strong>the</strong> major factor controlling <strong>the</strong> service life <strong>of</strong> coiled tubing. The rate<br />

<strong>of</strong> fatigue damage accumulation is affected by a number <strong>of</strong> operating factors: mechanical<br />

damage, corrosion damage, damage incurred by exceeding <strong>the</strong> ultimate capacity <strong>of</strong> <strong>the</strong><br />

string, and damage due to cycling plastic strain or fatigue.<br />

Determination <strong>of</strong> <strong>the</strong> actual friction coefcient is essential in dening <strong>the</strong> project technical<br />

feasibility. As <strong>the</strong> part <strong>of</strong> drilling system, drilling uid can impact on <strong>the</strong> reduction <strong>of</strong> friction<br />

coefcient by implementation <strong>of</strong> lubricants. Selection <strong>of</strong> lubricants, <strong>the</strong>ir compatibility<br />

with drilling uid and rocks was determined through laboratory testing. The results are<br />

shown and elaborated in <strong>the</strong> paper.<br />

Key words: drilling, pipe wearing, lubricants<br />

Introduction<br />

Horizontal wells are more expensive to drill than vertical wells so increased production<br />

must <strong>of</strong>fset increased drilling costs. In drilling horizontal or highly deviated wells, more<br />

serious problems appear than in drilling vertical wells. These problems are: poor hole<br />

cleaning, excessive torque and drag, hole lling, pipe sticking, well bore instability, loss <strong>of</strong><br />

circulation, formation damage, poor cement job, and difculties at logging jobs. From that<br />

reason, <strong>the</strong> principle factors that require extra consideration for choosing a uid for drilling<br />

a horizontal well are: formation damages, hole cleaning, hole stability and lubricity. Good<br />

lubricating properties <strong>of</strong> <strong>the</strong> drilling uid can improve greatly drilling operation efciency.<br />

When drilling long sections <strong>of</strong> highly deviated wells, <strong>the</strong>re is considerable contact between<br />

<strong>the</strong> drill string and <strong>the</strong> borehole wall, generating frictional resistance to movement. The<br />

friction between <strong>the</strong> drill pipe and <strong>the</strong> wall will increase torque and power required to rotate<br />

<strong>the</strong> drill pipe and <strong>the</strong> stress on <strong>the</strong> drill pipe. It could also interfere with running <strong>the</strong> pipe<br />

in and out <strong>of</strong> <strong>the</strong> hole. The frictional resistance to movement can be large enough to be <strong>the</strong><br />

limiting factor in horizontal and extended-reach drilling. Since <strong>the</strong>re are many factors that<br />

affect torque and drag, it is sometimes difcult to detect what is causing increased down<br />

hole friction.<br />

Regardless <strong>of</strong> <strong>the</strong> drilling uid or lubricant used, down hole friction can be reduced by


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 39<br />

conditioning <strong>the</strong> uid to achieve a thin, slick, compressible lter cake, and by practicing<br />

good hole-cleaning techniques to minimize <strong>the</strong> cuttings bed. In order to design <strong>the</strong> best<br />

suitable drill-in uid for horizontal well, drilling problems generally encountered in each<br />

eld should be studied and laboratory tests planned and conducted.<br />

Systematic approach to drilling optimization<br />

To optimize a drilling process <strong>the</strong>re is a need to develop methods and processes that will<br />

improve drilling efciency. The method must be systematic, logical and must have quantiable<br />

approach. The applicable method is one that denes and quanties two sets <strong>of</strong><br />

parameters for <strong>the</strong> drilling operation: performance objectives and requirements, as shown<br />

in Fig. 1. The gure is taken from reference [1] but is slightly changed to apply for coiled<br />

tubing drilling with down hole positive displacement motor.<br />

Fig. 1 Systematic approach inuence diagram<br />

To achieve minimal interval cost we have to maximize on-bottom time and effective rate <strong>of</strong><br />

penetration. First branch determines parameters that are not direct drilling parameters, but<br />

depend on well path and used equipment. Second branch determines parameters that are<br />

<strong>of</strong> greatest inuence in drilling process. Bit design and used down hole motor combination<br />

efciency according to observed formation characteristics are essential. To obtain optimal<br />

performance <strong>of</strong> bit-motor combination optimal ow rate must be obtained and proper uid<br />

used.<br />

In deviated or horizontal wells proper determination <strong>of</strong> weight on bit in any moment or<br />

point <strong>of</strong> <strong>the</strong> well trajectory is essential. The determination <strong>of</strong> compressive load in vertical<br />

section, build section or horizontal section depends on well trajectory and coiled tubing<br />

dimensions. Buckling <strong>of</strong> coiled tubing and lock-up condition is <strong>the</strong> next limitation that<br />

must be considered.<br />

Because <strong>of</strong> different possible well paths and segment length and slope (Fig. 2) it is necessary<br />

to determine forces and stresses in coiled tubing.


40<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Fig 2. Possible well paths and pipe buckling in <strong>the</strong>m<br />

When coiled tubing is run into horizontal section, it is subjected to compressive load due<br />

to frictional drag. The axial compressive load is highest at <strong>the</strong> end <strong>of</strong> <strong>the</strong> built section and<br />

lowest at <strong>the</strong> far end <strong>of</strong> <strong>the</strong> well. When compressive load exceeds <strong>the</strong> critical buckling load,<br />

<strong>the</strong> coiled tubing will initiate a sinusoidal buckling. Fur<strong>the</strong>r increase <strong>of</strong> <strong>the</strong> compressive<br />

load can result in a helical buckling <strong>of</strong> <strong>the</strong> coiled tubing. Helical buckling can also occur in<br />

<strong>the</strong> vertical section when “slacking-<strong>of</strong>f” weight at <strong>the</strong> surface to push coiled tubing through<br />

<strong>the</strong> well. In horizontal section coiled tubing will buckle when <strong>the</strong> axial compressive load<br />

exceeds critical (sinusoidal) buckling load. When <strong>the</strong> axial compressive load reaches helical<br />

buckling load, helical buckling occurs, and is fully formed.<br />

In <strong>the</strong> build-up section, coiled tubing under axial compression will be pushed against <strong>the</strong><br />

lower side <strong>of</strong> <strong>the</strong> well bore before <strong>the</strong> onset <strong>of</strong> sinusoidal or helical buckling. In this section<br />

buckling will not easily occur because <strong>of</strong> distributed lateral force, and <strong>the</strong> need <strong>of</strong> larger<br />

buckling load in build-up section than in straight well bore.<br />

When pushing coiled tubing into horizontal section with no helical buckling present, <strong>the</strong><br />

axial load simply increases linearly along <strong>the</strong> tubular. This is due to <strong>the</strong> friction drag from<br />

<strong>the</strong> tubular weight, without considering any additional frictional force from sinusoidal<br />

buckling, since usually it is very small. In vertical section without helical buckling <strong>the</strong>re<br />

is <strong>the</strong>oretically no frictional drag and <strong>the</strong> axial compressive load decreases linear. If helical<br />

buckling occurs in <strong>the</strong> vertical section due to “slack-<strong>of</strong>f”, <strong>the</strong> axial load distribution<br />

decreases nonlinear:


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 41<br />

Maximum axial compressive load that is transmitted to <strong>the</strong> bottom <strong>of</strong> vertical section to<br />

kick-<strong>of</strong>f point (KOP) by “slacking-<strong>of</strong>f” is [2]:<br />

(1)<br />

Where: (F b,max<br />

) is maximal axial compressive load at <strong>the</strong> bottom <strong>of</strong> vertical section, (E) is<br />

Young’s modulus <strong>of</strong> elasticity, (I) is moment <strong>of</strong> inertia <strong>of</strong> tubular, (we)- tubular weight in<br />

uid, (r) is radial clearance between well bore and tubular, () is coefcient <strong>of</strong> friction and<br />

(H) is vertical well bore depth.<br />

The compressive axial load at <strong>the</strong> end <strong>of</strong> <strong>the</strong> build section (EOC) is:<br />

(2)<br />

Where: (F eoc<br />

) is axial load at <strong>the</strong> end <strong>of</strong> build section, (F kf)<br />

is axial load at <strong>the</strong> kick<strong>of</strong>f point,<br />

(R) is radius <strong>of</strong> well bore curvature and (e) is natural logarithm base.<br />

“Lockup” refers to situation where <strong>the</strong> bit or packer load can not be increased by “slacking<strong>of</strong>f”<br />

weight at <strong>the</strong> surface, or <strong>the</strong> tubulars can not be pushed fur<strong>the</strong>r in <strong>the</strong> well bore. And<br />

<strong>the</strong> maximal horizontal reach without helical buckling in horizontal section will be:<br />

(3)<br />

Where: (L h<br />

) is horizontal section length.<br />

It is obvious that coefcient <strong>of</strong> friction is <strong>of</strong> importance when calculating loads on tubular.<br />

Measurements conducted by Johancsik at all [3] have shown that it can vary from 0,2 to 0,4<br />

in real well bore situations. The reduction <strong>of</strong> friction will allow greater horizontal lengths<br />

with smaller pipe wearing. The capability to do so has two main benets. First, deep,<br />

highly deviated wells can be planned to minimize torque and drag by selection <strong>of</strong> most<br />

appropriate well path. Second, more complete knowledge <strong>of</strong> drill string loading allows<br />

choose <strong>of</strong> drill string components according to systematic approach that considers <strong>the</strong> extra<br />

forces involved. They have showed that tension increment and torsion increment depend<br />

on coefcient <strong>of</strong> friction and normal force:<br />

Where: (F t<br />

) is axial tension acting at lower end <strong>of</strong> element, ( ) is average inclination<br />

angle <strong>of</strong> element, (F n<br />

) is normal force acting on element, (M) is increase in torsion over<br />

length <strong>of</strong> element, and (r p<br />

) is characteristic radius <strong>of</strong> drill string element. In Eq. 4, <strong>the</strong> plus<br />

sign is for upward motion and <strong>the</strong> minus sign is for downward motion.<br />

(4)<br />

(5)


42<br />

LUBRICANTS<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Friction reduction can be achieved by using a drilling uid with good lubricating qualities<br />

such as oil-base uids, polymer uids, and glycol-derivative systems [4]. Oil-based uids<br />

<strong>of</strong>ten are chosen for extended reach wells because <strong>the</strong>y are highly inhibitive and exhibit<br />

good lubrication properties. Unfortunately, <strong>the</strong>ir use in environmentally sensitive areas is<br />

discouraged or even prohibited [5]. There are also a large number <strong>of</strong> lubricant additives<br />

available; <strong>the</strong>se should be tested for uid and formation compatibility as some <strong>of</strong> <strong>the</strong>m<br />

can have detrimental effects. In general, lubricants may be <strong>of</strong> a mechanical nature (beads,<br />

nut plug, etc.), general borehole or lm lubricants, or extreme-pressure (metal-to-metal)<br />

lubricants.<br />

Natural grease and oils abandoned because <strong>of</strong> cheaper oxidant stable mineral oils, are now,<br />

because <strong>of</strong> ecological aspect, used again. Rape oil and castor oil are used in production <strong>of</strong><br />

biodegradable lubricants. Rape oil has also o<strong>the</strong>r favorable properties: good lubricity, high<br />

viscosity, good adhesion on metal surfaces and very good load bearing. Problems on high<br />

and low temperatures and with foaming can be solved by adding additives. When added<br />

in water based mud (WBM) such problems are solved with <strong>the</strong> use <strong>of</strong> emulsiers, antifoaming<br />

agents and for warehouse purposes pour point depressants.<br />

Lubricants are designed to reduce torque to increase horsepower at <strong>the</strong> bit by reducing <strong>the</strong><br />

coefcient <strong>of</strong> friction. In water based drilling uids certain oils, graphite powder, glycols<br />

and soaps are used for this purpose. To be economic, a drilling uid lubricant must reduce<br />

torque and drag, and operating costs by performing <strong>the</strong> following functions:<br />

• reduce possibilities <strong>of</strong> twist-<strong>of</strong>fs,<br />

• shorten trip time,<br />

• lessen <strong>the</strong> conditions for differential sticking, and<br />

• lower <strong>the</strong> amount <strong>of</strong> energy necessary to run <strong>the</strong> rig.<br />

Depending on <strong>the</strong>ir chemical composition and state <strong>of</strong> dispersion or solubility in <strong>the</strong> base<br />

drilling uid, lubricants:<br />

• can coat metal surfaces, reducing <strong>the</strong> adhesion <strong>of</strong> steel to <strong>the</strong> lter cake;<br />

• can be incorporated into <strong>the</strong> lter cake and provide better uid-loss control (resulting in<br />

thinner cakes); and<br />

• can be incorporated into <strong>the</strong> lter cake to reduce <strong>the</strong> yield stress <strong>of</strong> <strong>the</strong> cake.<br />

In many uid systems, it was found that <strong>the</strong> most effective additives are those operating by<br />

more than one <strong>of</strong> <strong>the</strong> above mechanisms.<br />

LABORATORY TESTS AND RESULTS<br />

Laboratory tests <strong>of</strong> <strong>the</strong> effect <strong>of</strong> two commercially available lubricants L1 and L2, and new<br />

developed lubricant Horma-138 [7] on rheological, ltration and lubricating properties <strong>of</strong><br />

selected drill-in uids were carried out. They are water-dispersible lubricants designed to<br />

decrease <strong>the</strong> coefcient <strong>of</strong> friction in all water-base muds, reducing torque and drag. They<br />

also have a unique wettability characteristic which lowers <strong>the</strong> potential <strong>of</strong> BHA balling [7].<br />

Inuence <strong>of</strong> addition different concentrations (0%, 2%, 3%) <strong>of</strong> three lubricants on rheological<br />

and ltration properties in different drill-in uids were carried out according API<br />

standard using Fann viscometer and API lter press. The three unweighted, water based


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 43<br />

drill-in uid systems were tested. Fluids are designated as WBM 1, WBM 2 and WBM 3<br />

(Table 1).<br />

Lubricating properties were studied using <strong>the</strong> Lubricity Tester. Briey a steel test block that<br />

simulates <strong>the</strong> wall <strong>of</strong> <strong>the</strong> hole is pressed against <strong>the</strong> test ring by a torque arm. The torque is<br />

measured by <strong>the</strong> intensity <strong>of</strong> current that is required to turn <strong>the</strong> ring at a constant rotation<br />

when immersed in <strong>the</strong> uid that is tested. The API procedure (RP 13B) was followed for<br />

<strong>the</strong> tests, in laboratory tests <strong>the</strong> rotational velocity was 60 min-1 (60 rpm) and <strong>the</strong> force applied<br />

was 16,95 Nm (150 lb/inch). Results are given as a torque value that can vary from 0<br />

to 50. The lower <strong>the</strong> value, <strong>the</strong> better <strong>the</strong> lubricating properties. The coefcient <strong>of</strong> friction<br />

is calculated from torque reading using adequate formulas.<br />

Table 1. Effect <strong>of</strong> various lubricants on mud properties and lubricating ability<br />

It is obvious that adding <strong>of</strong> HORMA-138 lubricant has <strong>the</strong> greatest inuence on plastic<br />

viscosity and yield point in comparison to uid without lubricants. For all three lubricants<br />

<strong>the</strong>re is an signicant reduction <strong>of</strong> coefcient <strong>of</strong> friction (COF). Fig. 3 is an illustration <strong>of</strong><br />

<strong>the</strong> inuence <strong>of</strong> lubricant concentration on COF in selected water based muds.


44<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Fig. 3. Efciency <strong>of</strong> selected lubricants in mud WBM 1<br />

The comparison <strong>of</strong> different lubricants inuence on lubricating properties <strong>of</strong> WBM is<br />

shown in Fig. 4. It can be seen that with 3% <strong>of</strong> HORMA-138 lubricant in WBM 1 and<br />

WBM 2 <strong>the</strong>re is a 60% reduction <strong>of</strong> COF. In WBM 3 because <strong>of</strong> original excellent lubricating<br />

properties <strong>the</strong>re is only 12% <strong>of</strong> COF reduction.<br />

Conclusions<br />

Fig. 4. Comparison <strong>of</strong> various lubricants impact on mud lubricating ability<br />

All used lubricants have certain but not important impact on rheological and ltration properties<br />

<strong>of</strong> tested uids, which is o<strong>the</strong>rwise desirable.<br />

By adding 2 to 3% <strong>of</strong> lubricant in WBM satisfactory reduction <strong>of</strong> COF is achieved.<br />

New developed lubricant HORMA-138 is in range <strong>of</strong> commercially available lubricants<br />

and is applicable for eld testing.<br />

Achieved COF reduction when implemented in force and horizontal reach calculations


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 45<br />

shows that for <strong>the</strong> same horizontal reach <strong>the</strong>re is <strong>the</strong> need for smaller axial loads on pipe,<br />

that means smaller amount <strong>of</strong> stresses imposed on pipe while drilling.<br />

Nomenclature<br />

E - Young’s modulus <strong>of</strong> elasticity, Pa<br />

e - natural logarithm base, 2,21828<br />

F b,max<br />

- maximal axial compressive load at <strong>the</strong> bottom <strong>of</strong> vertical section, N<br />

F eoc<br />

-axial load at <strong>the</strong> end <strong>of</strong> build section, N<br />

F n<br />

- axial load acting on element, N<br />

F kf<br />

- axial load at <strong>the</strong> kick<strong>of</strong>f point, N<br />

F t<br />

- axial tension acting at lower end <strong>of</strong> element, N<br />

H - vertical well bore depth, m<br />

I - moment <strong>of</strong> inertia <strong>of</strong> tubulars, m4<br />

L h<br />

- horizontal section length, m<br />

M - increase in torsion over length <strong>of</strong> element, N•m<br />

r - radial clearance between well bore and tubulars, m<br />

r p<br />

- characteristic radius <strong>of</strong> drill string element, m<br />

R - radius <strong>of</strong> well bore curvature, m<br />

w e<br />

- tubular weight in uid, N/m<br />

- friction factor<br />

- Ludolf’s number, 3,14<br />

References<br />

1. Wolfson L, Mensa-Wilmot G, Coolidge R. ( 1998) Systematic Approach Enhances<br />

Drilling Optimization and PDC Bit Performance in North Slope ERD Program, SPE<br />

50557, SPE Annual Technical Conference and Exhibition, New Orleans, 27-30 September,<br />

p. 1-12<br />

2. Wu J, Juvkam-Wold HC. (1993) Drilling and Completing Horizontal Wells With<br />

Coiled Tubing, SPE 26336, 68th Annual Conference and Exhibition, Houston, 3-6<br />

October, p. 221-233<br />

3. Johancsik CA, Friesen DB, Dawson R. (1984) Torque and Drag in Directional Wells-<br />

Prediction and Measurement, Journal <strong>of</strong> Petroleum Technology, June, p. 987-992<br />

4. Argillier J-F, Audibert A, Janssen M, Demoulin A. (1996) Development <strong>of</strong> a New<br />

Non-Polluting Ester Based Lubricant for Water Based Muds: Laboratory and Field<br />

Tests Results, SPE 36862, European Petroleum Conference, Milan, Italy, October 22-<br />

24, p. 401-410<br />

5. Bol GM. (1986) Effect <strong>of</strong> Mud Composition on Wear and Friction on Casing and Tool<br />

Joints, SPE Drilling Engineering, October, p. 369-376<br />

6. Evans N, Langlois B, Audibert-Hayet A, Dalmazzone C, Deballe E. High Performance<br />

Emulsiers for Syn<strong>the</strong>tic Based Muds, SPE 63101, SPE Annual Technical Conference<br />

and Exhibition, Dallas, TX, October 1-4, p. 1-11<br />

7. Gaurina-Meimurec N. (1998) Horizontal Well Drill-In Fluids, The Mining, Geological,<br />

Petroleum Engineering Bulletin, vol. 10, Zagreb, Croatia, p. 73-76


46<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

FUNDAMENTALS OF MILITARY PRODUCTION<br />

DEVELOPMENT IN THE CROATIAN WAR FOR<br />

INDEPENDENCE FROM 1991 TO 1993<br />

Dinko Mikulić<br />

University <strong>of</strong> Apllied Sciences Velika Gorica<br />

Zagrebačka cesta 5, 10410 Velika Gorica, Croatia<br />

e-mail: dinko.mikulic@vvg.hr<br />

Tel. 01/6230-761, Mob. 099 6222-503<br />

Vladimir Koroman<br />

Brodarski institut d.o.o.,<br />

Av. V. Holjevca 20, 10020 Zagreb, Croatia<br />

e-mail: vladimir.koroman@hrbi.hr<br />

Tel. 01/6504-401, Mob. 098 211-324<br />

Summary<br />

There were several phases in organizing <strong>the</strong> military production during <strong>the</strong> Homeland War<br />

from 1991 to 1993. In <strong>the</strong> rst phase, emphasis was placed on human creativity and top<br />

level improvisation in producing armoured vehicles and light arms. In <strong>the</strong> second stage, <strong>the</strong><br />

military armament and equipment production development fundamentals were established<br />

by forming The Sector for Development, Production and Scientic Research. In <strong>the</strong> third<br />

phase, a systematically organised massive arms and equipment military production and<br />

overhaul had begun by forming The Production Department. In this paper, based on an<br />

example <strong>of</strong> armoured vehicles development, <strong>the</strong> fundamentals <strong>of</strong> Croatian military production<br />

are explained, which fullled <strong>the</strong> military missions and reconciled <strong>the</strong> requests, thus<br />

serving <strong>the</strong> purpose <strong>of</strong> <strong>the</strong> country's liberation.<br />

Key words: armoured vehicles, development and production, Croatian War <strong>of</strong> Independence<br />

(Homeland war)<br />

Introduction<br />

The production <strong>of</strong> military equipment for Croatian National Guard (Zbor narodne garde,<br />

ZNG) soldiers began in <strong>the</strong> summer <strong>of</strong> 1991, a year <strong>of</strong> war. The equipment was produced<br />

manually in small and large plants as well as in workshops and garages. Firstly, trucks<br />

were armoured and given as present to <strong>the</strong> Croatian soldier who ghts for freedom. It was<br />

a help to <strong>the</strong> police in <strong>the</strong> rst place, <strong>the</strong>n to <strong>the</strong> Croatian National Guard. Such improvised<br />

vehicles gave protection from infantry weapons and enabled <strong>the</strong> completion <strong>of</strong> various<br />

logistic tasks, from food and ammunition transport to <strong>the</strong> transport <strong>of</strong> <strong>the</strong> wounded.<br />

Since Croatia didn't have any armoured vehicles at its disposal, excluding a part <strong>of</strong> <strong>the</strong><br />

police personnel carriers, <strong>the</strong>se handcrafted armoured vehicles in <strong>the</strong> hands <strong>of</strong> <strong>the</strong> brave<br />

Croatian Homeland War defenders as seen on TV screens, strongly raised people's morale<br />

and gave a huge impetus to faster production and o<strong>the</strong>r defence nances. Approximately<br />

fty rms participated in <strong>the</strong>ir production, mostly in Zagreb, <strong>the</strong>n in Split, Slavonski Brod,<br />

Rijeka etc.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 47<br />

1 The beginning <strong>of</strong> organized production<br />

First it began in <strong>the</strong> Croatian Parliament and <strong>the</strong> Government <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia.<br />

Direct contacts between <strong>the</strong> Headquarters <strong>of</strong> <strong>the</strong> military command and <strong>the</strong> economy resulted<br />

in <strong>the</strong> admission <strong>of</strong> company's leaders to <strong>the</strong> Croatian Parliament, as well as <strong>the</strong> Defence<br />

Minister, lieutenant general Martin Špegelj, and associates. Defence Minister Deputy<br />

V. Kikerec and Mr M. Hlad, a Parliament representative, accepted in <strong>the</strong>ir <strong>of</strong>ces persons<br />

and company requests for development and production <strong>of</strong> military equipment among<br />

which were also <strong>the</strong> <strong>of</strong>fers for <strong>the</strong> production <strong>of</strong> armoured vehicles.<br />

Having graduated from <strong>the</strong> Technical Military Academy from rnomerec in Zagreb, volunteers,<br />

military-technical experts <strong>of</strong>fered <strong>the</strong>ir pr<strong>of</strong>essional services to <strong>the</strong> Ministry <strong>of</strong><br />

Defence leaders. As pr<strong>of</strong>essional advisers, <strong>the</strong>y took over <strong>the</strong> coordination <strong>of</strong> development<br />

and production <strong>of</strong> various equipment. The development coordination at Zagreb-based<br />

companies TAZ, Hidroelektra-Mehanizacija, Autodubrava, Autoservis-Borongaj and o<strong>the</strong>rs<br />

soon followed as well as <strong>of</strong>fering pr<strong>of</strong>essional instructions for vehicle armouring, body<br />

armours, small individual weapons, etc.<br />

1.1 The sector for Development, Production and Scientific Research<br />

Systematic development <strong>of</strong> defence funding began by forming The Sector for Development,<br />

Production and Scientic Research. President <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia Franjo<br />

Tuman, PhD, issued <strong>the</strong> Decision on <strong>the</strong> Appointment <strong>of</strong> Gojko Šušak as <strong>the</strong> Defence<br />

Minister on 16 September 1991, while Croatian Prime Minister Franjo Greguri, PhD,<br />

passed <strong>the</strong> Decision on <strong>the</strong> Appointment <strong>of</strong> Vladimir Volarevi, PhD, as <strong>the</strong> Defence Minister<br />

Deputy, who took over <strong>the</strong> organization <strong>of</strong> military equipment and armaments development<br />

and production and also formed The Sector for Development, Production and<br />

Scientic Research (temporary department at <strong>the</strong> Ministry <strong>of</strong> Defence).<br />

The rst staff <strong>of</strong> <strong>the</strong> just formed sector comprised military experts, mostly lecturers from<br />

<strong>the</strong> Technical Military Academy from rnomerec in Zagreb and experts from <strong>the</strong> Army<br />

Depot Mainentance Bregana, who as volunteers enlisted for Croatian military service, and<br />

who were competent for specic eld <strong>of</strong> military equipment and armaments development.<br />

These were <strong>the</strong> following Croatian army <strong>of</strong>cers:<br />

Dinko Mikuli, MSc, motor vehicles; Zdenko Matijaši, MSc, motor vehicles; Vjekoslav<br />

Stojkovi, PhD, motor vehicles; Mijo Vrhovski, PhD, motor vehicles; Simeon Kovaev,<br />

PhD, motor vehicles; Nikola Gambiroža, PhD, explosives; Mirjana Gambiroža Juki,<br />

PhD, explosives, Milan Prpi, MSc, explosives, Mladen Pleše, PhD, explosives; Mladen<br />

Barkovi, PhD, electronic devices; Artur Gorianin, MSc, electronic devices; Aljoša<br />

Božikovi, MSc, radars; Mirko Jukl, MSc, radars; Mihalj Strmeki, MSc, air defence;<br />

Vladimir Lebinac, MSc, electronic devices, Goran Prokopec, MSc, telecommunication;<br />

Ivan Pokaz, MSc; Mirko Kukolj, MSc, armaments; Milan Ivanuševi, MSc, NBC equipment;<br />

Josip Petrovi, electronic devices; Josip Vinter, overhaul; Vinko Turk, artillery<br />

weapons; Ivan Peica, air defence, Vitoš Bebi, <strong>engineering</strong>; Zdravko Paveli, armaments;<br />

Petar Radonji, navy.<br />

The cooperation was established between The Sector for Development, Production and<br />

Scientic Research <strong>of</strong> <strong>the</strong> Croatian Ministry <strong>of</strong> Defence and <strong>the</strong> Department <strong>of</strong> Energy <strong>of</strong><br />

<strong>the</strong> Croatian Ministry <strong>of</strong> Industry for <strong>the</strong> purpose <strong>of</strong> coordination and unobstructed work <strong>of</strong><br />

pr<strong>of</strong>essional advisers <strong>of</strong> <strong>the</strong> Ministry <strong>of</strong> Defence in companies.


48<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

1.2 The list <strong>of</strong> some companies working on <strong>the</strong> production <strong>of</strong> armoured vehicles<br />

Autodubrava, Zagreb, Brodosplit, Split, TAZ – Bus Factory Zagreb, Autoservis Borongaj,<br />

Zagreb, Hidroelektra-Niskogradnja-Mehanizacija, Zagreb, Industrogradnja, Zagreb,<br />

Tehnika, Zagreb, TPK, Zagreb, J.Gredelj, HŽP Zagreb, Jedinstvo, Zagreb, Tehnomehanika,<br />

Marija Bistrica, .akovi Specijalna vozila, Sl.Brod, elik/TVIL, Križevci, Torpedo,<br />

Rijeka, Rijekaprojekt, and o<strong>the</strong>rs.<br />

Production <strong>of</strong> some armoured vehicles, Semptember-December, 1991<br />

Key meetings at companies<br />

Key meetings <strong>of</strong> <strong>the</strong> representatives <strong>of</strong> The Sector for Development, Production and Scientic<br />

Research <strong>of</strong> <strong>the</strong> Croatian Ministry <strong>of</strong> Defence and <strong>the</strong> Department <strong>of</strong> Energy <strong>of</strong> <strong>the</strong><br />

Croatian Ministry <strong>of</strong> Industry with representatives <strong>of</strong> <strong>the</strong> rms which <strong>of</strong>fer <strong>the</strong> military<br />

production <strong>of</strong> armoured vehicles, were held as follows:<br />

Meeting in <strong>the</strong> factory Torpedo Rijeka, 1 October 1991<br />

Meeting in <strong>the</strong> factory . akovi, Slavonski Brod, 15 October 1991<br />

Meeting in <strong>the</strong> shipyard Brodosplit, Split, 4 December 1991<br />

The basic manufacturers' questions were about <strong>the</strong> necessary number <strong>of</strong> vehicles and <strong>the</strong><br />

way or <strong>the</strong>ir development as well as <strong>the</strong> possibility <strong>of</strong> project nancing. In <strong>the</strong> production<br />

<strong>of</strong> armoured personnel carrier based on <strong>the</strong> truck chassis, emphasis must be put on chas-


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 49<br />

sis standardization while for armouring <strong>the</strong> usage <strong>of</strong> steel plates (plates for ship) 8-10 mm<br />

thick. As a technical institute Brodarski institut <strong>of</strong>fered <strong>the</strong> help <strong>of</strong> its experts for <strong>the</strong> purpose<br />

<strong>of</strong> superstructure and certain systems development.<br />

Fig. 1. Armoured personnel carriers, Otoac, Gacka, Krešimir i Domagoj; Industrogradnja,<br />

Zagreb, 1991<br />

1.3 A letter to <strong>the</strong> producers <strong>of</strong> military equipment and armament, 10 November 1991<br />

In cooperation with <strong>the</strong> Ministry <strong>of</strong> Industry and after talks with potential armaments and<br />

military equipment manufacturers, Defence Minister Deputy V. Volarevi sent <strong>the</strong> manufacturers<br />

<strong>the</strong> following letter:<br />

The Republic <strong>of</strong> Croatia<br />

The Ministry <strong>of</strong> Defence<br />

Zagreb, 10 November 1991<br />

Class: 213-01/91-01/30<br />

Reg. no.: 512-08-91-1<br />

Armaments and military equipment production<br />

Please activate all available capacities for mass production <strong>of</strong> <strong>the</strong> assigned – arranged<br />

armaments and military equipment assortment for <strong>the</strong> needs <strong>of</strong> <strong>the</strong> armed battle and<br />

war operations. All produced quantities with <strong>the</strong> highest degree <strong>of</strong> achieved reliability –<br />

quality should be delivered to <strong>the</strong> commanders <strong>of</strong> <strong>the</strong> units in your territories, while <strong>the</strong><br />

necessary documentation should be made about <strong>the</strong> delivery.<br />

Defence Minister Deputy<br />

Vladimir Volarevi, PhD


50<br />

Typical example <strong>of</strong> Commands’ requests<br />

The Republic <strong>of</strong> Croatia<br />

Starigrad-Paklenica Command <strong>of</strong> <strong>the</strong> Croatian Army<br />

No.: 155-1-9/<br />

Date: 13 November 1991<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

The Ministry <strong>of</strong> Defence<br />

Fax 041 451-882<br />

Dinko Mikuli<br />

For <strong>the</strong> purposes <strong>of</strong> our command, please assign us one armoured vehicle with <strong>the</strong> following<br />

characteristics:<br />

- It must be protected against <strong>the</strong> shooting and cumulative effects<br />

- The possibility <strong>of</strong> mounting <strong>the</strong> machine-gun<br />

- Such vehicle is urgent to us<br />

Ivan Cerovac<br />

Commander<br />

1.4 Report on motor vehicles production and development, 20 November 1991, to <strong>the</strong><br />

Defence Minister Deputy<br />

1. The production <strong>of</strong> an armoured <strong>engineering</strong> vehicle Straško is running according to<br />

<strong>the</strong> delivery plan (15 delivered)<br />

2. The production <strong>of</strong> armoured personnel carriers in Brodosplit rms is nished. The<br />

works are nished at Hidroelektra, Tehnika-Bjelovar.<br />

3. Armour steel HPA-10 <strong>of</strong> various thicknesses is provided for vehicle armouring, placed<br />

in <strong>the</strong> vicinity <strong>of</strong> TAZ (Tvornica autobusa Zagreb)<br />

4. The production <strong>of</strong> safety car tires with lling mass, placed and examined in Hidroelektra-Mehanizacija,<br />

Žitnjak, Zagreb.<br />

5. The development <strong>of</strong> mine cleaner with disks, <strong>the</strong> examination <strong>of</strong> its effectiveness is<br />

under way<br />

6. The project <strong>of</strong> multi-purpose armoured vehicle is prepared in cooperation with Brodarski<br />

Institute Zagreb, on <strong>the</strong> TAM 150 T11 6x6 chassis<br />

7. Tactical-technical requirements are prepared for development <strong>of</strong> armoured light vehicle.<br />

8. Preparations for <strong>the</strong> possibility <strong>of</strong> cooperation on terrain vehicle are being made<br />

9. The project <strong>of</strong> shielded medical buses in TAZ is being prepared.<br />

10. The production <strong>of</strong> military truck on TAM 110 T7 4x 4 chassis is being prepared.<br />

After production <strong>of</strong> rst armoured vehicles, <strong>the</strong> manufacturers gained a valuable experience,<br />

so <strong>the</strong>y asked for new available armoured vehicles, trucks type TAM 260, TAM<br />

170, TAM 190 and similar. However, <strong>the</strong>re wasn't a sufcient number <strong>of</strong> such vehicles<br />

at disposal because a huge number <strong>of</strong> vehicles was mobilized, besides building companies<br />

which had <strong>the</strong> most trucks would be left without work resources. It is estimated that<br />

approximately 200 various armoured vehicles are handcrafted and <strong>the</strong>re were over 1000<br />

people working on <strong>the</strong>m, in more than 50 rms and workshops in <strong>the</strong> Republic <strong>of</strong> Croatia.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 51<br />

2 Croatian Army requirements and organized production <strong>of</strong> armoured<br />

vehicles<br />

Considering <strong>the</strong> war situation, <strong>the</strong> Croatian Army required increasingly better military<br />

equipment, with better technical protection characteristics, with greater mobility and better<br />

possibility <strong>of</strong> combat activity as well as <strong>the</strong>ir supporting logistics, spare parts and intervention<br />

team. In this way <strong>the</strong> Croatian Army wanted to increase tactical and strategic mobility<br />

<strong>of</strong> <strong>the</strong> Croatian Army at <strong>the</strong> whole operation zone <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia.<br />

Requirements for better equipment were based upon three important factors: armour protection,<br />

mobility and repower. Commanders demand <strong>the</strong> mobility <strong>of</strong> repower and this<br />

is possible only by means <strong>of</strong> armoured combat vehicles for it can lead to faster change in<br />

conducting combat operations. It was not enough anymore that <strong>the</strong> soldier could only be<br />

transported at <strong>the</strong> battleeld protected by armour, moreover repower from various arms<br />

was required as well as supporting technical logistics. Such vehicles from which infantry<br />

can lead <strong>the</strong> battle should be produced and leave <strong>the</strong> vehicle only in emergency case and<br />

reconnaissance. The basis <strong>of</strong> it can be multi-purpose light combat vehicles on wheels intended<br />

for various combat activities in <strong>the</strong> system <strong>of</strong> mechanized reconnaissance units,<br />

forces for fast activities and general support forces. Thus, armoured vehicles on wheels<br />

complement with armoured vehicles on tracks during tactical activity.<br />

Means <strong>of</strong> transport for troop transport, military trucks, ambulance vehicles, towing vehicles<br />

for MB-120 mm heavy mortars were required from <strong>the</strong> Croatian army as a priority,<br />

and <strong>the</strong>n requiring better armoured vehicles with <strong>the</strong> possibility to apply weapons. For <strong>the</strong><br />

purpose <strong>of</strong> vehicle standardization for <strong>the</strong> army multi-purpose vehicles are recommended<br />

in order to be used for various tasks.<br />

The Sector for Development, Production and Scientic Research intensies development<br />

and production for defence, which speeds up <strong>the</strong> implementation <strong>of</strong> projects for armoured<br />

vehicles and supporting logistics development.<br />

During <strong>the</strong> 1991 - 1993 period <strong>the</strong> following production <strong>of</strong> armoured vehicles, trucks and<br />

overhaul support was established and realized:<br />

- 120 mm Self-propelled mortar, year 1991<br />

- Military truck TK 130 T-7 4x 4 Torpedo, year 1992<br />

- Light Armoured Vehicle (LAV) 4x 4, year 1993<br />

- Army Maintenance Depot, Zagreb, year 1991<br />

2.1 Development and production <strong>of</strong> 120 mm self-propelled mortars<br />

It is estimated that <strong>the</strong> Croatian Army has at its disposal a sufcient number <strong>of</strong> terrain vehicles<br />

(TAM 150 T11 6x6) which can meet tactical-technical requirements <strong>of</strong> multi-purpose<br />

armoured vehicle production. The project was given to a scientic-research institution –<br />

Brodarski Institute Zagreb, which already has experts and experience in <strong>the</strong> development<br />

<strong>of</strong> complex military objects. It was <strong>the</strong> rst complex development project <strong>of</strong> <strong>the</strong> Ministry<br />

<strong>of</strong> Defence which was initiated with <strong>the</strong> scientic-research institution. The complete<br />

preparation <strong>of</strong> <strong>the</strong> project was led by pr<strong>of</strong>essional adviser in The Sector for Development,<br />

Production and Scientic Research, Dinko Mikuli, MSc, and <strong>the</strong> head <strong>of</strong> <strong>the</strong> Special Projects<br />

Department in Brodarski Institute, Vladimir Koroman, MSc. The implementing body<br />

– Brodarski Institute obliged to design, construct and deliver <strong>the</strong> prototype and establish<br />

<strong>the</strong> production <strong>of</strong> <strong>the</strong> multi-purpose armoured vehicle with a built-in MB-120 mm mortar<br />

and PAM 12.7 mm heavy machine-gun. There are three project phases:<br />

1. The construction <strong>of</strong> a functional model to full functionality


52<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

2. The construction <strong>of</strong> a prototype based on <strong>the</strong> approved functional model<br />

3. The organization <strong>of</strong> production based on <strong>the</strong> approved prototype<br />

Deadline for <strong>the</strong> completion <strong>of</strong> <strong>the</strong> 1st phase works was 10 December 1991. Within <strong>the</strong><br />

Institute, people specialising in various technical elds worked day and night in <strong>the</strong> preparation<br />

<strong>of</strong> <strong>the</strong> rst functional model and prototype. Technical documentation was prepared<br />

according to <strong>the</strong> simultaneous <strong>engineering</strong> principle (simultaneous phase overlap), regarding<br />

<strong>the</strong> armour design, as well as hydraulic suspension for <strong>the</strong> impact amortization, mortar<br />

tting and ammunition storage. The vehicle is designed for endurance according to possible<br />

impacts <strong>of</strong> <strong>the</strong> MB-120 mm heavy mortar, produced by “Prvomajska-Alatni strojevi<br />

/ INAS”- Žitnjak.<br />

Several manufacturers participated in <strong>the</strong> 1st and 2nd development phase: TAZ Zagreb(for<br />

armour), Strojogradnja Samobor (for hydraulics), Rade Konar – special devices and systems<br />

(laser cutting <strong>of</strong> sheet metal), Obrada Rovinj (mortar chassis at <strong>the</strong> vehicle), Elmech<br />

(inert mines – mines for testing) and o<strong>the</strong>r manufacturers. The testing <strong>of</strong> <strong>the</strong> self-propelled<br />

mortar functional model was carried out on 22 November 1991 on Velešec polygon in <strong>the</strong><br />

vicinity <strong>of</strong> Velika Gorica.<br />

SoMB-120 mm self-propelled mortar model was placed on hydraulic props and levelled.<br />

Recording equipment was connected as well. The usage <strong>of</strong> mortars was carried out by a<br />

group <strong>of</strong> military <strong>of</strong>cers <strong>of</strong> <strong>the</strong> General Staff <strong>of</strong> <strong>the</strong> Croatian Armed Forces. 9 inert mines<br />

were red. The vehicle was checked and <strong>the</strong>re weren’t any deformations on it. With <strong>the</strong><br />

change <strong>of</strong> functional model to prototype, a prototype was completely nished and prepared<br />

for nal testing on endurance and accuracy <strong>of</strong> targets shooting, with 99 red inert mines.<br />

Fur<strong>the</strong>r testings on mortar endurance and accuracy showed <strong>the</strong> correctness <strong>of</strong> suspension<br />

solution and <strong>the</strong> way <strong>of</strong> re control system. At <strong>the</strong> beginning <strong>of</strong> 1992, <strong>the</strong> prototype was<br />

given to <strong>the</strong> 108th Brigade ZNG, Slavonski Brod. A self-propelled mortar prototype was<br />

used during <strong>the</strong> Homeland War.<br />

According to <strong>the</strong> 3 rd phase <strong>of</strong> <strong>the</strong> contract - <strong>the</strong> organization <strong>of</strong> production based on <strong>the</strong> approved<br />

prototype – two more SoMB-120 mm self-propelled mortars were produced in TAZ<br />

factory according to <strong>the</strong> documentation and supervision <strong>of</strong> works by Brodarski Institut.<br />

Note:<br />

In time <strong>of</strong> completion <strong>of</strong> self-propelled mortar production, Ivan ermak was appointed<br />

as <strong>the</strong> Defence Minister Deputy for logistics and forms Logistics Sector which includes<br />

several departments: Department for Production, which takes over <strong>the</strong> organization <strong>of</strong> military<br />

production (from The Sector for Development, Production and Scientic Research),<br />

Procurement Department, Technical and Trade Department, Construction Department and<br />

Telecommunications Department. Colonel Nikola Gambiroža, PhD, was appointed as<br />

Head <strong>of</strong> The Department for Production on 9 January 1992.<br />

Both just produced SoMB-120 mm self-propelled mortars were delivered to <strong>the</strong> Croatian<br />

Army on 7 January 1991 before Operation ''Maslenica'' in which self-propelled mortars<br />

were successfully used in liberating operation <strong>of</strong> Zadar hinterland.<br />

The contribution <strong>of</strong> Brodarski Institute to <strong>the</strong> development <strong>of</strong> Croatian Army equipment<br />

and armaments, among which was also SoMB self-propelled mortar, was shown when<br />

Croatian President Franjo Tuman and Minister <strong>of</strong> Defence Gojko Šušak came to visit<br />

Brodarski Institute on 31 March 1993.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 53<br />

Fig.2. Functional model <strong>of</strong> SoMB 120 mm self-propelled mortar with 12.7 mm,<br />

Kiseli, Brodarski Institut, Zagreb, 1991<br />

Fig.3. The testing <strong>of</strong> SoMB 120 mm self-propelled mortar prototype, Velešec, 1992<br />

2.2 Development and production <strong>of</strong> military trucks TK 130 T-7 4x4 Torpedo<br />

The idea <strong>of</strong> military truck production based on TAM 110 T7 4x 4 chassis fell on fertile<br />

ground in <strong>the</strong> tractor and construction machines factory Torpedo, Rijeka. After <strong>the</strong> production<br />

<strong>of</strong> armoured <strong>engineering</strong> vehicle Straško/HIAV on <strong>the</strong> universal excavator chassis, <strong>the</strong><br />

management board decided to make preparations for <strong>the</strong> domestic production <strong>of</strong> military<br />

trucks in cooperation with <strong>the</strong> factory TAM Maribor. For <strong>the</strong> purpose <strong>of</strong> domestic production<br />

share increase, Boženko Vukovi, MSc and Zdenko Novak, MSc, reconstructed<br />

<strong>the</strong> cabin and cargo crate, which was completely produced in Progres rm-Jastrebarsko.<br />

Nedjeljko Ški, MSc, proposed <strong>the</strong> tting <strong>of</strong> 130 HP. domestic diesel-engine Torpedo,<br />

which would be technically and logistically better than 110 HP engine. Feasibility study<br />

justied <strong>the</strong> truck domestic production. A new manufacturing department for vehicle production<br />

was prepared within <strong>the</strong> factory. In <strong>the</strong> production system Director Neven Dedi<br />

and Head <strong>of</strong> Procurement Department Marelo Jurman worked out a plan for mounting


54<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

parts procurement, thus <strong>the</strong> production in <strong>the</strong> new manufacturing department could start.<br />

A part <strong>of</strong> <strong>the</strong> chassis (frame, axle, gear box) must have been imported from <strong>the</strong> manufacturer<br />

TAM Maribor, while everything else was manufactured in Croatia (diesel engine<br />

Torpedo, <strong>the</strong> cabin, cargo crate, tarpaulin, o<strong>the</strong>r parts). Thus, vehicle price around 50% <strong>of</strong><br />

purchase price <strong>of</strong> <strong>the</strong> similar imported vehicle was acceptable. A domestic share <strong>of</strong> approximately<br />

60 % <strong>of</strong> product price was relevant. Product Quality Regulation was made, while<br />

all vehicles before <strong>the</strong> delivery passed all necessary polygon tests on Šljunara polygon,<br />

under <strong>the</strong> Grobnik automobile race-track. The vehicles had provided logistical support, a<br />

2-year guarantee and spare parts for <strong>the</strong> next ten-year-period. It was a successful decision<br />

in truck production, according to <strong>the</strong> guidelines <strong>of</strong> war industry, <strong>the</strong> reduction <strong>of</strong> costs and<br />

vehicle standardization in <strong>the</strong> Croatian Army.<br />

First ''0'' series vehicles comprising 20 trucks were delivered at <strong>the</strong> end <strong>of</strong> 1992, <strong>the</strong>n series<br />

comprising 200 trucks were delivered in 1993-1994 period. It provided <strong>the</strong> tactical and<br />

strategic mobility <strong>of</strong> <strong>the</strong> Croatian Army during <strong>the</strong> Homeland War. In this time Torpedo<br />

TK-130 4x 4 military vehicles could be mostly seen on Croatian roads. This means that <strong>the</strong><br />

production <strong>of</strong> Torpedo TK-130 4x 4 trucks with <strong>the</strong> capacity <strong>of</strong> 3 tons(it can accommodate<br />

12 soldiers with complete equipment) was a very important factor <strong>of</strong> <strong>the</strong> Croatian Army<br />

capability during <strong>the</strong> Homeland War. Besides, a series production <strong>of</strong> military trucks proves<br />

that <strong>the</strong> cooperation with foreign partners on <strong>the</strong> basis <strong>of</strong> economical protability is possible<br />

even during <strong>the</strong> laid embargo.<br />

2.3 Development and production <strong>of</strong> light armoured vehicles LOV 4x4<br />

On <strong>the</strong> basis <strong>of</strong> good experience <strong>of</strong> ‘’0’’ series military truck production, an initiative was<br />

accepted that <strong>the</strong> manufacturer Torpedo <strong>of</strong>fers <strong>the</strong> solution <strong>of</strong> <strong>the</strong> Light Armoured Vehicle<br />

on <strong>the</strong> same TK 130 T7 4x 4 vehicle chassis. A huge degree <strong>of</strong> unication <strong>of</strong> both products<br />

was achieved in this way, as well as <strong>the</strong> low price <strong>of</strong> development and production. After<br />

that, appropriate tactical-technical requirements for light armoured vehicles (LOV 4x4)<br />

were prepared. The weight <strong>of</strong> 6.5 tons light armoured vehicles will be propelled by an<br />

intensied 150 HP diesel engine, with <strong>the</strong> maximum vehicle speed 120 km/h. The vehicle<br />

crew is made <strong>of</strong> 2 + 8 soldiers.<br />

Two items <strong>of</strong> ''0'' series LOV OP are developed in 1992. Main engineer Zdenko Novak,<br />

MSc, designed a modern form <strong>of</strong> Armoured Combat Vehicle. The vehicle height was below<br />

2 metres (1860 mm). The front part <strong>of</strong> <strong>the</strong> vehicle was well designed, <strong>the</strong> door construction<br />

for fast and easy entering and exiting <strong>of</strong> <strong>the</strong> driver, <strong>the</strong>n for fast entering and exiting <strong>of</strong> <strong>the</strong><br />

crew. The power <strong>of</strong> diesel engine was increased to150 HP, so that <strong>the</strong> vehicle got more<br />

available power for terrain mobility. In cooperation with experts from Brodarski Institut,<br />

contemporary methods were used to check <strong>the</strong> rmness <strong>of</strong> <strong>the</strong> armour with regard to vibrations.<br />

The capacity <strong>of</strong> LOV OP include 2 tons artillery and 8 soldiers.<br />

The main protection <strong>of</strong> Light Armoured Vehicles is <strong>the</strong> armour made <strong>of</strong> special steel which<br />

protects <strong>the</strong> crew from all types 7.62 x 51 AP (NATO protection) ammunition which would<br />

be red from <strong>the</strong> distance <strong>of</strong> 30 metres as well as <strong>the</strong> 155 mm shell fragments. 6-8-9 mm<br />

thick Armox special steel plates are applied as well as <strong>the</strong> safety glass. Due to <strong>the</strong> greater<br />

re exposure <strong>of</strong> <strong>the</strong> armoured surfaces, <strong>the</strong> vehicle got <strong>the</strong> greater armour thickness. On <strong>the</strong><br />

bottom side <strong>of</strong> <strong>the</strong> vehicle an additional two-layered antitank mines protection was made.<br />

Trial factory testings <strong>of</strong> <strong>the</strong> Light Armoured Vehicles are carried out on Šljunara polygon,<br />

above Rijeka. The representatives <strong>of</strong> <strong>the</strong> factory, <strong>the</strong> Ministry <strong>of</strong> Defence, <strong>the</strong> Faculty <strong>of</strong><br />

Mechanical Engineering and Naval Architecture and Brodarski Institute were present. The<br />

vehicle demonstration was very good. It is dened that <strong>the</strong> braking regulator must be tted<br />

on <strong>the</strong> rear axle, Run Flat tires must be provided and making <strong>the</strong> opening <strong>of</strong> <strong>the</strong> ro<strong>of</strong> doors


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 55<br />

and rotation <strong>of</strong> turret easier.<br />

The nal testing <strong>of</strong> light armoured vehicles as a type LOV IZV 4x4 with <strong>the</strong> 12.7 mm<br />

heavy machine-gun was carried out on polygon <strong>of</strong> Jastrebarsko barracks. During <strong>the</strong> testing<br />

Chief <strong>of</strong> General Staff <strong>of</strong> Armed Forces Anton Tus and representatives <strong>of</strong> Armoured<br />

units <strong>of</strong> <strong>the</strong> Croatian Army were present and very satised with <strong>the</strong> possibilities <strong>of</strong> barriers<br />

overcoming, especially cross water-trench capability as well as <strong>the</strong> speed <strong>of</strong> entering and<br />

exiting <strong>of</strong> <strong>the</strong> soldiers from <strong>the</strong> armoured vehicles.<br />

Fig. 4. The testing <strong>of</strong> LOV 4x4 OP prototype, Jastrebarsko, 13 February 1993.<br />

Fig. 5. Testing <strong>of</strong> LOV RAK 24/128 mm prototype, Zeevo, Šibenik, 1993.


56<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

After <strong>the</strong> operational capacity <strong>of</strong> <strong>the</strong> armoured vehicle was shown, a serial quantity <strong>of</strong> different<br />

types <strong>of</strong> vehicles was arranged. The delivery <strong>of</strong> <strong>the</strong>se vehicles increased <strong>the</strong> tactical<br />

and strategic capability <strong>of</strong> <strong>the</strong> Croatian Army and its readiness to reject <strong>the</strong> enemy forces<br />

and end <strong>the</strong> war. Light Armoured Vehicle was developed in <strong>the</strong> following types: Armoured<br />

Personnel Carrier (LOV OP 4x4), Reconnaissance Vehicle (LOV IZV 4x4), Electronic<br />

Warfare Vehicle (LOV ED 4x4), Command Vehicle (LOV Z 4x4), Multiple rocket launcher<br />

(LOV RAK 24/128 4x4), Nuclear-Biological Vehicle (LOV ABK 4x4) and Reconnaissance<br />

patrol and artillery re control system (LOV UP).<br />

12.7 mm air-defence machine-gun is a part <strong>of</strong> <strong>the</strong> standard equipment <strong>of</strong> all Light Armoured<br />

Vehicles. The Reconnaissance Vehicle for electronic warfare uses an additional<br />

armaments – 20 mm RT-20 hand gun and 8-tube launcher system Obad (8 RL 60 M93),<br />

60 mm calibre, with range <strong>of</strong> 8000 m. In order to increase artillery repower or artillery<br />

rocket combat a type <strong>of</strong> RAK 24/128 Light Armoured Vehicle is developed. This vehicle is<br />

equipped with <strong>the</strong> multiple rocket launcher with 28 tubes <strong>of</strong> 128 mm diameter. The rocket<br />

range is 8.550 m, up to 13.500 m. A prototype LOV-2 as an improved type <strong>of</strong> previous series<br />

is developed. It comprised covered winch on <strong>the</strong> front part, easier vehicle conducting,<br />

better brakes, better electronic equipment, telecommunications system and working area.<br />

A complex development project <strong>of</strong> military LOV 4x4 Torpedo linked 4 important factors:<br />

construction, technical, conducting and economic. It gave its logistic identity. Logistic <strong>engineering</strong><br />

requirements were set already in <strong>the</strong> 1st phase <strong>of</strong> tactical-technical requirements<br />

setting so that <strong>the</strong> total logistic support for lime time is assessed through <strong>the</strong> ’’iceberg’’<br />

costs. Production and service price <strong>of</strong> such vehicles is more acceptable than <strong>the</strong> price <strong>of</strong><br />

such imported vehicles. The price <strong>of</strong> <strong>the</strong> basic LOV OP 4x4 is 6 times lower than <strong>the</strong> <strong>of</strong>fered<br />

price <strong>of</strong> basic Piranha 6x6 armoured vehicle, which is <strong>the</strong> pro<strong>of</strong> <strong>of</strong> <strong>the</strong> possible costeffectiveness<br />

<strong>of</strong> <strong>the</strong> fur<strong>the</strong>r production.<br />

This project <strong>of</strong> <strong>the</strong> original LOV design, low contour and domestic production proved <strong>the</strong><br />

sufcient domestic pr<strong>of</strong>essional knowledge and it showed that <strong>the</strong> army can rely on <strong>the</strong><br />

domestic science and production in dealing with <strong>the</strong> complex military systems in <strong>the</strong> hardest<br />

war conditions.<br />

2.4 Army Maintenance Depot<br />

Staff <strong>of</strong> The Sector for Development, Production and Scientic Research examined <strong>the</strong><br />

disposable halls used for manufacture in Jedinstvo company in Jankomir in Zagreb and<br />

prepared <strong>the</strong> necessary documentation on maintenance realization and <strong>the</strong> overhaul <strong>of</strong> <strong>the</strong><br />

Croatian Army military technology. Colonel Mijo Vrhovski, Col. Josip Vinter, Zdenko<br />

Matijaši, Col. Vjekoslav Stojkovi, Col. Josip Petrovi and o<strong>the</strong>r military <strong>of</strong>cers <strong>of</strong> <strong>the</strong><br />

Croatian Army were working on this project.<br />

A unit <strong>of</strong> army maintenance depot support was formed on <strong>the</strong> basis <strong>of</strong> this project on 14<br />

October 1991, rst for <strong>the</strong> overhaul <strong>of</strong> armoured means. The development <strong>of</strong> technical support<br />

system for <strong>the</strong> development <strong>of</strong> armoured vehicles began in this way, <strong>the</strong>n began <strong>the</strong><br />

formation <strong>of</strong> <strong>the</strong> 310th logistic support brigade.<br />

The 310th logistic support brigade signicantly contributed to <strong>the</strong> development and<br />

maintenance <strong>of</strong> military equipment and armaments. Among o<strong>the</strong>r things, it maintained<br />

<strong>the</strong> armoured vehicles <strong>of</strong> different manufacturers and it gave help at <strong>the</strong> lowlands elds<br />

throughout <strong>the</strong> Republic <strong>of</strong> Croatia. Army Maintenance Depot, as a part <strong>of</strong> <strong>the</strong> Logistics<br />

Command, became a unit <strong>of</strong> <strong>the</strong> Armed Forces responsible for <strong>the</strong> implementation <strong>of</strong> <strong>the</strong><br />

overhaul highest level (<strong>the</strong> 3rd level) <strong>of</strong> armaments means, Croatian Army military equipment<br />

and it is also a support to <strong>the</strong> units <strong>of</strong> <strong>the</strong> Croatian Armed Forces which take part in<br />

<strong>the</strong> international peacekeeping missions.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 57<br />

3 Conclusion<br />

During <strong>the</strong> Serbian aggression against <strong>the</strong> independent Republic <strong>of</strong> Croatia, people’s motivation<br />

and organized directing <strong>of</strong> equipment and armaments projects enabled <strong>the</strong> production<br />

<strong>of</strong> improvised combat means. The units <strong>of</strong> <strong>the</strong> Croatian Army required <strong>the</strong>se vehicles<br />

in <strong>the</strong> rst 3 years <strong>of</strong> <strong>the</strong> Homeland war. The rst quantities <strong>of</strong> <strong>the</strong> armoured personnel<br />

carriers justied <strong>the</strong>ir purpose. Regarding <strong>the</strong> direct commanders' demand and soldiers' information<br />

from <strong>the</strong> eld, <strong>the</strong> Croatian Army was satised. Around 1000 people from many<br />

rms and workshops took part in <strong>the</strong> handcrafted production <strong>of</strong> 200 armoured vehicles.<br />

Requirements for military equipment caused <strong>the</strong> need for war industry directing in order to<br />

ensure <strong>the</strong> logistics <strong>of</strong> Croatian Army equipment in a faster and more rational way. Apart<br />

from <strong>the</strong> protection <strong>of</strong> people from infantry weapons using <strong>the</strong> sandwich armour, <strong>the</strong>se<br />

vehicles could not provide <strong>the</strong> necessary mobility <strong>of</strong> repower. Therefore, <strong>the</strong> development<br />

projects <strong>of</strong> contemporary armoured vehicles with armaments on chassis <strong>of</strong> <strong>the</strong> highly<br />

mobile military trucks, SoMB-120 (6x6) self-propelled mortars and Light Armoured Vehicles<br />

(LOV 4x4) were initiated. The developed domestic armoured vehicles were used<br />

in <strong>the</strong> three crucial country liberating operations ’’Maslenica ’’, ’’Bljesak ’’ and ’’Oluja ’’.<br />

Their usage in <strong>the</strong> hands <strong>of</strong> <strong>the</strong> Croatian Army soldiers, <strong>the</strong>ir operation and <strong>the</strong>ir production<br />

is carried out with regard to military tasks as well as in view <strong>of</strong> foreign contemporary<br />

solutions. A series production <strong>of</strong> military trucks proves that <strong>the</strong> cooperation with foreign<br />

partners is possible even during <strong>the</strong> embargo.<br />

In <strong>the</strong> end, <strong>the</strong>re were several phases in organizing <strong>the</strong> military production during <strong>the</strong><br />

Homeland War from 1991 to 1993. In <strong>the</strong> rst phase, emphasis was placed on human creativity<br />

and top level improvisation in producing armoured vehicles and light arms. In <strong>the</strong><br />

second stage, <strong>the</strong> military armament and equipment production development fundamentals<br />

were established by forming The Sector for Development, Production and Scientic Research.<br />

In <strong>the</strong> third phase, a systematically organised massive arms and equipment military<br />

production and overhaul had begun by forming The Production Department. In this paper,<br />

based on an example <strong>of</strong> armoured vehicles development, <strong>the</strong> fundamentals <strong>of</strong> Croatian<br />

military production are explained, which fullled <strong>the</strong> military missions and reconciled <strong>the</strong><br />

requests, thus serving <strong>the</strong> purpose <strong>of</strong> <strong>the</strong> country's liberation.<br />

4 References<br />

1. Ivkovi Z (2001) Hrvatski oklopnjaci 1991.-1993.: Ministarstvo obrane Republike<br />

Hrvatske, Zagreb, 2001.<br />

2. Poster (1996) Runo izraena oklopna vozila Hrvatske vojske 1991-1992: Galerija<br />

Zvonimir, Zagreb, 1996.<br />

3. Gambiroža N (1992) Proizvedeno u Hrvatskoj: Hrvatski vojnik, br. 17/92, Zagreb,1992.<br />

4. Bandula D (1997) Hrvatska vojna industrija: Velebit, 31.12.1997, Zagreb.<br />

5. Mallet J (1998) Croatian tanks and rocket launchers hits <strong>of</strong> Eurosatory 1998: DAILY,<br />

Janes Defence Weekly, Le Bourget, Pariz, 1998.<br />

6. Mikuli D (1991/1992) Kolegij blok: vlastite bilješke, Zagreb, 1992.<br />

7. Mikuli D (1991/1992) Oklopljena vozila: slikovni album, Zagreb, 1992.<br />

8. Mikuli D (1992/1993) Oklopna borbena vozila: slikovni album, Zagreb, 1993.


58<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Intelligent Forest Fire Monitoring System – from idea<br />

to realization<br />

Darko Stipaničev<br />

Department for Modeling and Intelligent Systems & Center for Wildfire Research<br />

University <strong>of</strong> Split Faculty <strong>of</strong> Electrical Engineering,<br />

Mechanical Engineering and Naval Architecture<br />

R.Boškovića 32, 21000 Split, Croatia<br />

darko.stipnaicev@fesb.hr<br />

Abstract<br />

Wildres, including forest res, are natural phenomena that cause signicant economic<br />

damage and have quite devastating effect to <strong>the</strong> environment all over <strong>the</strong> world. Early re<br />

detection on one side and quick and appropriate intervention on <strong>the</strong> o<strong>the</strong>r one, are <strong>of</strong> vital<br />

importance for wildre damage minimization. The re season 2003 was quite severe one,<br />

particularly in Split and Dalmatia County. Provoked by great damages caused by 2003<br />

wildres in autumn 2003 a project was initiated at University <strong>of</strong> Split Faculty <strong>of</strong> Electrical<br />

Engineering, Mechanical Engineering and Naval Architecture Department for Modeling<br />

and Intelligent Systems, having <strong>the</strong> main goal to nd a way how advanced information –<br />

communication technologies (ICT) could be used to improve wildre prevention and protection.<br />

After three years <strong>of</strong> research and testing in 2006 <strong>the</strong> Intelligent Forest Fire Monitoring<br />

System called iForestFire was presented. iForestFire belongs to <strong>the</strong> last generation<br />

<strong>of</strong> wildre monitoring and surveillance systems, having a lot <strong>of</strong> innovative and advanced<br />

features. Since 2006 it has been applied in various Croatian national and nature parks, but<br />

also <strong>the</strong> whole Istria region is covered by iForestFire network having 29 monitoring stations<br />

and 7 operational centers. The paper describes main features <strong>of</strong> iForestFire system<br />

with emphasize on its development and implementation.<br />

Key words: wildre, wildre detection, smoke detection, intelligent system<br />

1 Introduction<br />

Wildre or wildland re is any uncontrolled burning <strong>of</strong> natural vegetation (grass, shrub,<br />

forest timber, litter and slash) in <strong>the</strong> wilderness area. When <strong>the</strong> vegetation layer is more<br />

precisely known, <strong>the</strong> more specic names could be used like forest re, grass re or bush-<br />

re. Wildres represent a constant threat to ecological systems, infrastructure and human<br />

lives. According to prognoses, wildres, including re clearing in tropical rain forest, will<br />

halve <strong>the</strong> world forest stand by <strong>the</strong> year 2030. In Europe, up to 10,000 km2 <strong>of</strong> vegetation is<br />

destroyed by res every year, and up to 100,000 km2 in North America and Russia. Wild-<br />

res are responsible for approximately 20% <strong>of</strong> CO2 emission into <strong>the</strong> atmosphere (Kührt<br />

et al, 2001).<br />

Croatia belongs to countries with high wildre risk. In summer season, seven coastal<br />

counties in Croatia, including in particular <strong>the</strong> Adriatic islands, are permanently exposed<br />

from high to very high re risks. This is due to meteorological conditions, densely spaced<br />

conifer forests and a lot <strong>of</strong> tourists. According to Croatian Forests data (Žaja, 2008) from


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 59<br />

1992 to 2007 <strong>the</strong>re were 4.851 wildres in Croatia and <strong>the</strong> burning area was 251.910 ha.<br />

Fire seasons 2000 and 2003 were particularly severe with 706 and 532 wildres and <strong>the</strong><br />

total damage caused by wildres was huge. For example in 2003 only in Split and Dalmatia<br />

County <strong>the</strong>re were 130 wildres, <strong>the</strong> total burned area was 9.700 ha, <strong>the</strong> direct damage<br />

caused by wildres (reghters interventions and post-re terrain recovery) was 16 mil.€,<br />

and <strong>the</strong> indirect damage, taking into account energetic equivalent <strong>of</strong> lost woody biomass,<br />

was assessed to 66 mil.€ (Stipaniev et al., 2004, Stipaniev et al. 2007). Wildres in<br />

2003 were particularly catastrophic on Split and Dalmatia County islands. For example,<br />

on islands Hvar and Bra <strong>the</strong> burning area was between 1/4 and 1/3 <strong>of</strong> total islands area<br />

and <strong>the</strong> small island Biševo near Vis has been totally burnt. Figure 1 shows photos <strong>of</strong> few<br />

2003 res on Split and Dalmatia County islands photographed by <strong>the</strong> author <strong>of</strong> this paper.<br />

Figure 1 – Wildres on Dalmatian islands in 2003<br />

Provoked by great damages caused by 2003 wildres in autumn 2003, a project was initiated<br />

at Department for Modeling and Intelligent Systems University <strong>of</strong> Split Faculty <strong>of</strong><br />

Electrical Engineering, Mechanical Engineering and Naval Architecture, having <strong>the</strong> main<br />

goal to nd a way how advanced information – communication technologies (ICT) could<br />

be used to improve wildre prevention and protection. After detailed survey <strong>of</strong> research<br />

topics and implementation <strong>of</strong> ICT systems in wildre prevention task in o<strong>the</strong>r countries<br />

subjected to wildres, we have focused ourselves primarily on <strong>the</strong>se three topics:<br />

- Automatic early wildre detection,<br />

- Calculation <strong>of</strong> micro location wildre risk index, and<br />

- Wildre behavior and propagation simulation.<br />

The rst topic is <strong>the</strong> most important one, because <strong>the</strong> only effective way to minimize damage<br />

caused by wildres is wildre early detection and fast and appropriate reaction, apart<br />

from preventive measures. Great efforts are <strong>the</strong>refore made to achieve early wildre detection,<br />

which is traditionally based on human wildre surveillance, realized by 24 hours observation<br />

by human observers located on selected monitoring spots. In Croatia <strong>the</strong> human<br />

wildres surveillance is mainly organized by Croatian Forests – <strong>the</strong> governmental organization<br />

responsible for protection and exploitation <strong>of</strong> forests in state ownership. Human observers<br />

are usually equipped only with standard binoculars and communication equipment<br />

and <strong>the</strong>ir observation area is only <strong>the</strong> area covered by <strong>the</strong>ir sight <strong>of</strong> view.<br />

A ra<strong>the</strong>r new, technically more advanced approach to human wildre surveillance is video<br />

cameras based human wildre surveillance and monitoring when remotely controlled<br />

video cameras are installed on monitoring spots, and <strong>the</strong> human observer is located in <strong>the</strong><br />

observation center. Such system could be used not only for early re detection, but also for


60<br />

distant video presence on re remote location.<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 2 – The difference between human wildre surveillance (left) and video camera based<br />

human wildre surveillance (right)<br />

The video cameras based human wildres surveillance has many advantages in comparison<br />

to direct human observation from monitoring spots. Few <strong>of</strong> <strong>the</strong>m are:<br />

- A wider area could be covered, because one human observer could monitor few video<br />

monitoring eld units.<br />

- Cameras are usually equipped with power zoom (optical zoom with 22 x magnication)<br />

so <strong>the</strong> observer could easily inspect suspected areas.<br />

- System usually has video storing capabilities, at least for <strong>the</strong> last couple <strong>of</strong> days, and that<br />

is quite useful for post-re analysis.<br />

The main limitation <strong>of</strong> video cameras based human surveillance is that re detection depends<br />

entirely on <strong>the</strong> human observation. The observer is located in more comfortable environment,<br />

<strong>the</strong> observation center, but he (or she) has to carefully watch multiple computer<br />

monitors at <strong>the</strong> same time, so problems like fatigue, boredom and loss <strong>of</strong> concentration<br />

could be encountered. That was <strong>the</strong> main reason for introduction <strong>of</strong> various forms <strong>of</strong> automatic<br />

and advanced automatic wildre surveillance and monitoring systems and networks.<br />

The system described in this paper, named iForestFire ® – Intelligent Forest Fire Monitoring<br />

System (Croatian name is IPNAS ® – Inteligentni Protupožarni NAdzorni Sustav) (iForest-<br />

Fire, <strong>2011</strong>), belongs to <strong>the</strong> last generation <strong>of</strong> advanced automatic wildre surveillance and<br />

monitoring systems, having a lot <strong>of</strong> innovative and advance features. It was entirely developed<br />

at University <strong>of</strong> Split Faculty <strong>of</strong> Electrical Engineering, Mechanical Engineering and<br />

Naval Architecture, so iForestFire is a good example <strong>of</strong> university – industry cooperation,<br />

because today it is a successful commercial product installed in various Croatian national<br />

and nature parks and Istria County, but also a product that have signicant export opportunities.<br />

In <strong>the</strong> rest <strong>of</strong> this paper, a short introduction to automatic wildre monitoring and surveillance<br />

systems will be given, main features <strong>of</strong> iForestFire system will be described with<br />

emphasis to its advanced and innovative aspects and nally a short discussion about iForestFire<br />

development, implementation and commercialization will be added.<br />

2 Automatic wildfire surveillance and monitoring system<br />

The research and system development in <strong>the</strong> area <strong>of</strong> automatic wildre surveillance system<br />

was extended in <strong>the</strong> last couple <strong>of</strong> years. There are two main types <strong>of</strong> automatic wildre


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 61<br />

surveillance systems: satellite systems based on satellite wildre monitoring and terrestrial<br />

systems based on wildre monitoring from ground monitoring stations. In this moment<br />

terrestrial systems are more useful because early re detection is not <strong>the</strong> only one task that<br />

contemporary automatic wildre surveillance and monitoring system has to fulll. Beside<br />

<strong>the</strong> automatic detection <strong>of</strong> wildres, <strong>the</strong> distance video presence on re remote location is<br />

almost <strong>of</strong> equal importance and today’s satellite systems could not fulll that task. Satellite<br />

systems could be used only for wildre detection with limited spatial and time resolution.<br />

Therefore <strong>the</strong> automatic wildre surveillance and monitoring ground-based or terrestrial<br />

system used as an enhancement <strong>of</strong> human based wildre surveillance are dominant today.<br />

In ground-based or terrestrial systems different kinds <strong>of</strong> re detection sensors could be<br />

used:<br />

- Video cameras sensitive in visible spectra where wildre detection is based on smoke<br />

recognition during <strong>the</strong> day and re ames recognition during <strong>the</strong> night.<br />

- Infrared (IR) <strong>the</strong>rmal imaging cameras where wildre detection is based on detection <strong>of</strong><br />

heat ux from <strong>the</strong> re (Arrue et al, 2000).<br />

- Optical spectrometry that identies <strong>the</strong> spectral characteristics <strong>of</strong> smoke (Forest Fire<br />

Finder, <strong>2010</strong>).<br />

- Light detection and ranging (LIDAR) systems that measure laser light backscattered by<br />

<strong>the</strong> smoke particles (Utkin et al, 2003)<br />

- Radio-Acoustic Sounding System (RASS) for remote temperature measurements and<br />

<strong>the</strong>rmal sensing <strong>of</strong> a particular forest region (Sahin et al, 2009).<br />

- Acoustic Volumetric Scanner (VAS) that recognizes <strong>the</strong> re acoustic emission spectrum<br />

as a results <strong>of</strong> acoustic re sensing (Viegas et al., 2008).<br />

- Sensor network based system, where a number <strong>of</strong> sensor nodes (in most cases wireless<br />

sensors) are deployed in forest, measuring different environmental variables used for re<br />

detection. There are lot <strong>of</strong> different approaches, from more or less standard wireless sensor<br />

network (Byungrak et al, 2006), application <strong>of</strong> so called Fiber Optic Sensor Network<br />

(FOSN) developed within <strong>the</strong> EU-FIRE project (Viegas et al, 2008) to exotic proposals<br />

where animals have to be used as mobile biological sensors equipped with sensor devices<br />

(Sahin, 2008).<br />

Each technology has its advantages and disadvantages. Most <strong>of</strong> <strong>the</strong>m are promising, but<br />

<strong>the</strong>y are still in experimental stage, particularly sensor networks, VAS, RASS and LIDAR<br />

systems. For example LIDAR - light detection and ranging system is used to carry out<br />

chemical detection from great distances and has <strong>the</strong> potential to be an efcient system for<br />

wildre detection. However, it requires <strong>the</strong> lighting <strong>of</strong> <strong>the</strong> horizon with a laser beam that<br />

causes public health risks, besides not being very feasible from <strong>the</strong> economic point <strong>of</strong> view.<br />

Because <strong>of</strong> that, today in commercial use are mostly video based system equipped with<br />

cameras sensitive in visible spectra and/or infrared spectra and systems based on optical<br />

spectrometry. Optical spectrometry is ra<strong>the</strong>r new technology. It is based on a chemical<br />

analysis <strong>of</strong> <strong>the</strong> atmosphere by an optical spectrometry system. A telescope is coupled with<br />

optical sensor connected to a spectrometer unit with optical cable. The system analyzes<br />

<strong>the</strong> way <strong>the</strong> sunlight is absorbed by <strong>the</strong> atmosphere. It is quite efcient having <strong>the</strong> smallest<br />

number <strong>of</strong> false alarms, but <strong>of</strong> course it has a lot <strong>of</strong> disadvantages too. The main one is that<br />

it scans <strong>the</strong> space above <strong>the</strong> tree crowns on horizon, so <strong>the</strong> smoke has to be higher than <strong>the</strong><br />

horizon. The second one is dubious night detection when standard video camera is used<br />

rst to detect light and <strong>the</strong>n optical spectrometry is used to detect re ames. Because <strong>of</strong><br />

that in commercial optical spectrometry based systems, <strong>the</strong> video cameras in visible spectra<br />

are also included. Infrared systems are good choice for wildre detection, but <strong>the</strong>ir price<br />

is still quite high in comparison to video cameras sensitive in visible spectra, <strong>the</strong>y have<br />

limited space resolution and <strong>the</strong>y could not be used for distant video presence. Therefore,


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

contemporary systems for wildre detection based on infrared cameras are usually also<br />

equipped with cameras sensitive in visible spectra.<br />

The conclusion is that almost in all commercially available systems, <strong>the</strong> camera sensitive<br />

in visible spectra is also present. As an old adage said: “The best hunting solution is<br />

to kill two rabbits with one shot.” we think that today <strong>the</strong> most suitable solution for terrestrial<br />

automatic wildre detection and monitoring systems is to use cameras sensitive<br />

in visible spectra, particularly from <strong>the</strong> price/quality point <strong>of</strong> view. If you want to build a<br />

network, you need a lot <strong>of</strong> monitoring devices and <strong>the</strong> price <strong>of</strong> various advanced re detection<br />

systems are much higher than today’s high quality video cameras. Additional feature<br />

<strong>of</strong> today’s video cameras is <strong>the</strong>ir dual sensitivity. They are usually color cameras sensitive<br />

in visible spectra during <strong>the</strong> day, and black and white cameras sensitive in near IR spectra<br />

during <strong>the</strong> night, so <strong>the</strong> detection capabilities, particularly in sunrise/sunset parts <strong>of</strong> <strong>the</strong><br />

day are greatly improved. The second reason why visible spectra video cameras based<br />

system are <strong>the</strong> best choice is because <strong>the</strong>ir way <strong>of</strong> detecting wildres is <strong>the</strong> most close to<br />

human based wildre detection. Human wildre observers primarily use his (or her) vision<br />

sensor (eyes) to detect wildre. Sometimes humans use additional visual enhancement<br />

devices like binocular to check suspicious areas, but humans never use o<strong>the</strong>r sensors for<br />

early wildre detection. During our research and development phase we have spoken with<br />

a lot various human wildre observers and no one <strong>of</strong> <strong>the</strong>m said that he (or she) is using<br />

for example hearing (ears) to detect wildres. That was <strong>the</strong> reason why our efforts from<br />

<strong>the</strong> beginning were to develop ground-based wildre monitoring system based on visible<br />

cameras sensitive in visible spectra.<br />

Off course we were not <strong>the</strong> only ones who have thought <strong>of</strong> that way. In various countries<br />

that encounter high risk <strong>of</strong> wildres, various terrestrial systems based on cameras sensitive<br />

in visible spectra were developed and proposed. In all <strong>of</strong> <strong>the</strong>m automatic wildre detection<br />

was based on smoke recognition during <strong>the</strong> day and ame recognition during <strong>the</strong> night.<br />

The main disadvantage <strong>of</strong> those systems is ra<strong>the</strong>r high false alarms rate, due to atmospheric<br />

conditions (clouds, shadows, dust particles), light reections and human activities. Therefore,<br />

systems are usually designed as semi-automatic systems, which means that a human<br />

operator supervises <strong>the</strong> automatic wildre detection and his (or her) decision is <strong>the</strong> nal<br />

one. After <strong>the</strong> re alarm is generated and suspicious part <strong>of</strong> <strong>the</strong> image is marked, <strong>the</strong> human<br />

operator conrms or discards <strong>the</strong> alarm. The task <strong>of</strong> a human operator is not to monitor<br />

camera displays all <strong>the</strong> time, like in video cameras based human wildre surveillance<br />

mentioned in previous section, but only to conrm or discard possible re alarms. If <strong>the</strong><br />

human operator is not sure about a re alarm, he (or she) could switch <strong>the</strong> system to manual<br />

operation and make additional inspections using camera pan, tilt and zoom features. Using<br />

such semi-automatic surveillance system, human operator efciency is highly improved.<br />

One operator can manage more video monitoring units but also his (or her) fatigue is<br />

greatly reduced.<br />

iForestFire - Intelligent Forest Fire Monitoring System belongs to this category. It is an<br />

innovative, cloud computing based, semi-automatic wildre detection system with quite<br />

advance distant video presence capabilities.<br />

3 Main features <strong>of</strong> iForestFire - Intelligent Forest Fire Monitoring Systems<br />

iForestFire is integrated and intelligent video based wildre surveillance and monitoring<br />

system. Wildres are detected in incipient stage using advanced image processing and<br />

image analyses methods. Intelligent re recognition algorithms analyze images automatically,<br />

trying to nd visual signs <strong>of</strong> wildres, particularly wildre smoke during <strong>the</strong> day and<br />

wildre ames during <strong>the</strong> night. If something suspicious is found, pre-alarm is generated


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 63<br />

and appropriate image parts are visibly marked. The operator inspects suspicious image<br />

parts and decides is it really <strong>the</strong> wildre or not. The system is capable to work with both<br />

types <strong>of</strong> cameras: video cameras sensitive in visible and near IR spectra and real IR <strong>the</strong>rmal<br />

imaging cameras, but video cameras sensitive in visible spectra are preferred.<br />

Theoretical background <strong>of</strong> iForestFire is innovative and newly introduced wildre observer<br />

network <strong>the</strong>ory based on three-layer sensor network architecture, formal <strong>the</strong>ory <strong>of</strong><br />

perception and notation <strong>of</strong> observer (Stipaniev et al, 2007a; Šeri et al, 2009). Wildre<br />

observer, illustrated in Figure 3, is <strong>the</strong> core element <strong>of</strong> iForestFire system. It has three horizontal<br />

layers: data or sensor layer, information or service layer and knowledge or application<br />

layer, vertically interconnected by low-level or data observer working as proprioception<br />

unit (syntactic and semantic validation <strong>of</strong> sensors and sensors data) and two high-level<br />

observers, <strong>the</strong> image re observer and <strong>the</strong> decision re observer, working as exteroception<br />

units (making conclusions based on sensory data).<br />

Figure 3 – Wildre observer is organized as three-layer observer network<br />

iForestFire is a cloud computing or Web Information System (WIS) which means that <strong>the</strong><br />

operator could be located on any location with broadband Internet connection and his (or<br />

her) user interface is standard Web browser. The system is based on eld units and a central<br />

processing unit. The eld unit includes <strong>the</strong> day & night, pan/tilt/zoom controlled IP based<br />

video camera and IP based mini meteorological stations connected by wired or wireless<br />

LAN to a central processing unit where all analysis, calculation, presentation, image and<br />

data archiving are done. The system is also an example <strong>of</strong> Future Generation Communication<br />

Environment (FGCA) where all applications and services are focused on users,<br />

and “user” in our case is <strong>the</strong> natural environment, having <strong>the</strong> main task its own wildre<br />

protection. For such environment behavior <strong>the</strong> term environmental intelligence (EI) was<br />

introduced (Stipaniev et al, 2007a; Šeri et al, 2009).


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iForestFire is both integral and intelligent user friendly system. Its organizational structure<br />

is shown in Figure 4.<br />

Figure 4 – The structure <strong>of</strong> iForestFire system<br />

It has three data bases: data warehouse with input images and alarm images, SQL database<br />

with meteorological data and temporal information <strong>of</strong> alarm images and GIS database with<br />

all relevant GIS data. iForestFire has ve working modes:<br />

- Manual Mode – user-friendly camera manual control by pan, tilt and zoom.<br />

- Automatic Mode – automatic re detection based on images captured by video cameras<br />

in <strong>the</strong> visible and near infrared spectra.<br />

- Archive Mode – video and meteorological data archive retrieval using various userfriendly<br />

procedures.<br />

- Simulation Mode – re behavior modeling and re-spread simulation using meteorological<br />

data and various GIS layers.<br />

- Fire Risk Calculation Mode - micro location re risk index calculation using, not only<br />

meteorological data, but sociological parameters connected with forest res too.<br />

iForestFire is integral because it is based on three different types <strong>of</strong> data:<br />

- Real time video data. Digital video stream is used in both, automatic and manual system<br />

modes. In automatic mode <strong>the</strong> video stream is a source <strong>of</strong> images for automatic wildre<br />

detection and in manual mode <strong>the</strong> video stream is used for distant video presence and distant<br />

video inspection.<br />

- Real time meteorological data. The meteorological data is used in <strong>the</strong> post-processing<br />

unit for false alarm reduction, but it is important for wildre risk calculation during <strong>the</strong><br />

monitoring phase and wildre spread behavior modeling during <strong>the</strong> re-ghting phase.<br />

Main meteorological parameters are measured using high tech IP based ultra sound mini<br />

meteorological station (iMeteo, <strong>2011</strong>), also developed during iForestFire project.<br />

- GIS (Geographical Information System) database. GIS system stores not only informa-


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 65<br />

tion on pure geographical data (elevations, road locations, water resources etc.), but also<br />

all o<strong>the</strong>r relevant forest re information related to a geographic position, like re history,<br />

land cover – land use, roads and forest corridors and similar. These data are used for userfriendly<br />

camera pan/tilt control but also <strong>the</strong>y are quite useful for reghting management<br />

activities. GIS data is essential for Simulation Mode and Fire Risk Calculation Mode.<br />

iForestFire is intelligent because it is based on articial intelligence (AI), computational<br />

intelligence (CI) and distributed intelligence (DI) technologies like:<br />

- Multi - agent based architecture. The system s<strong>of</strong>tware organization is based on agent<br />

architecture. Intelligent s<strong>of</strong>tware agents are responsible for sensors integrity testing, image<br />

and meteorological data collecting, syntactic and semantic image and data validation, image<br />

and data storing, image pre-processing processing and post-processing and pre-alarms<br />

and alarms generation. All agents share <strong>the</strong> same ontology and speak <strong>the</strong> same agent communication<br />

language (ACL) (Šeri et al, 2009). To demonstrate <strong>the</strong> system complexity, let<br />

us mention that on one server having 5 monitoring locations with 16 preset positions on<br />

each video unit, more <strong>the</strong>n 300 agents are working in parallel.<br />

- Advanced image processing and analyses algorithms. In its automatic mode, <strong>the</strong> wildre<br />

detection is based on various advanced image processing, image analyzing and image understanding<br />

algorithms. Various algorithms work in parallel based on advanced motion detection,<br />

advanced image segmentation, res smoke dynamic pattern analysis, color-space<br />

analysis and texture analysis (Krstini et al,2009; Krstini et al, <strong>2011</strong>). Typical detection<br />

result for monitoring station located in Buzet region (Istria) is shown in Figure 5.<br />

- Advanced procedures for false alarms reduction. In post-processing analysis, various<br />

methods derived from intelligent technologies eld are used to reduce <strong>the</strong> number <strong>of</strong> false<br />

alarms, as for example advanced image processing techniques (Jakovevi et al, 2009),<br />

rule-based expert system, data fusion algorithms (Stipaniev et al, 2007b) and integration<br />

<strong>of</strong> re risk index calculation with automatic adjustment <strong>of</strong> detection sensitivity (Bugari<br />

et al, 2009). Algorithms have a number <strong>of</strong> tuning parameters, but our experience was that<br />

users adjust <strong>the</strong>m rarely. The poorly adjusted parameters sometimes cause overly false<br />

alarm generation. That was <strong>the</strong> reason why we have introduced <strong>the</strong> possibility <strong>of</strong> automatic<br />

parameter adjustment based on meteorological data fusion and augmented reality features.<br />

Results <strong>of</strong> re risk index calculation are used to automatically increase or decrease system<br />

detection sensitivity on various image regions. Also a powerful QoS (Quality <strong>of</strong> service)<br />

was developed, particularly related to wildre observer detection quality evaluation<br />

(Jakovevi et al, <strong>2010</strong>). QoS is used particularly as a tool for fur<strong>the</strong>r improvements <strong>of</strong><br />

detection quality.<br />

- Augmented reality. The system is geo-referenced, so for every image pixel <strong>the</strong> corresponding<br />

geo-coordinate could be known and vice versa. The augmented reality features,<br />

now in experimental phase, based on fusion and integration <strong>of</strong> GIS information and real<br />

time video images are used in both, automatic and manual mode. Two examples <strong>of</strong> augmented<br />

reality use in automatic mode are automatic adjustment <strong>of</strong> detection sensitivity and<br />

determination <strong>of</strong> smoke location geo-coordinates. In manual mode important GIS information<br />

could be shown on video screen like toponyms, coordinates, altitudes, but GIS data are<br />

also used in advanced cameras manual control.<br />

In system design phase particular attention was given to create a user-friendly system. All<br />

iForestFire modules and components could be reached and administrated through dynamic<br />

and interactive Web pages, where real time video and meteorological data are shown toge<strong>the</strong>r<br />

with GIS data and user friendly interface for camera pan/tilt/zoom camera control.<br />

From <strong>the</strong> beginning, <strong>the</strong> reghters were involved in experiments with iForestFire system<br />

prototype, so <strong>the</strong> nal user interface was designed taking into account <strong>the</strong>ir advices. Figure<br />

5 shows a typical camera control screen, and a typical re alarm screen.


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Figure 5 - iForestFire camera control screen with various manual control modes and typical re<br />

alarm screen at location Buzet in Istria. The user can accept or discard <strong>the</strong> generated alarm.<br />

For right decision about reghting intervention, both <strong>the</strong> early re detection and appropriate<br />

judgment about <strong>the</strong> potential re danger are important. That is <strong>the</strong> reason why from <strong>the</strong><br />

reghters’ point <strong>of</strong> view, both automatic detection <strong>of</strong> wildres and manual camera control<br />

modes are <strong>of</strong> equal importance. Because <strong>of</strong> that, we have implemented in iForestFire various<br />

user-friendly procedures for cameras manual control like:<br />

- Geo-referenced camera map control. The user can control camera pan movement by<br />

simple clicking on geo-referenced map. The camera control system is integrated with GIS,<br />

so it automatically detects and informs <strong>the</strong> user is <strong>the</strong> chosen point visible from <strong>the</strong> camera<br />

location or not.<br />

- Geo-referenced one-click multiple cameras map control. In regions where <strong>the</strong> monitoring<br />

cameras network is established (like Istria County) <strong>the</strong> so-called one-click multiple cameras<br />

control was implemented. The user simply click on geo-referenced map and in background<br />

visibility <strong>of</strong> that location is calculated for all cameras in neighborhood, appropriate<br />

azimuth and elevation angles are calculated and all cameras are automatically pan and tilt<br />

moved to show chosen location (Stipaniev et al, 2009).<br />

- Camera control using panorama image. In left upper corner <strong>of</strong> Figure 5 <strong>the</strong> 360o panorama<br />

image is shown. By simply clicking on panoramic image camera moves to chosen<br />

position by both pan and tilt.<br />

- Camera control using preset positions. Camera could by simple click on preset thumbs,<br />

moved to preset positions, pre-dened by pan, tilt and zoom.<br />

- Virtual pan-tilt-zoom commands and joystick emulation. Virtual commands are shown<br />

in upper right part <strong>of</strong> Figure 5. Simple, self-explaining virtual commands for pan tilt and<br />

zoom camera control were implemented, toge<strong>the</strong>r with joystick s<strong>of</strong>tware emulation.<br />

iForestFire has a powerful archive retrieval methods for input images, generated alarm images<br />

and meteorological data. All <strong>of</strong> <strong>the</strong>m could be easily reached and analyzed using various<br />

image and image data retrieval procedures based on advanced Internet technologies.<br />

Each monitoring station is equipped with advanced IP based ultra sound mini meteorological<br />

station used for measuring <strong>the</strong> most important meteorological parameters: air<br />

temperature, relative humidity, air pressure, wind speed, wind direction and wind gust.<br />

Additionally it is possible to measure o<strong>the</strong>r meteorological parameters important for wild-


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 67<br />

re behavior and system performances, as for example isolation, precipitation, moisture,<br />

ground temperature or lighting activity. Meteorological data are used in Automatic Mode<br />

for false alarms reductions in post-processing procedures, but also in our experimental Fire<br />

Risk Calculation Mode and Simulation Mode. Figure 6 shows <strong>the</strong> system interfaces for<br />

micro-location wildre risk calculation and simulation <strong>of</strong> wildre propagation.<br />

Figure 6 – Experimental system for micro-location wildre risk calculation (left) and simulation<br />

<strong>of</strong> wildre propagation (right)<br />

In Fire Risk Calculation and Simulation Mode external meteorological services are also<br />

used, for example <strong>the</strong> results <strong>of</strong> meteorological simulations performed by simulation model<br />

ALADIN-HR. These data are automatically collected from <strong>the</strong> servers <strong>of</strong> Meteorological<br />

and Hydrological Service <strong>of</strong> Croatia twice a day. Figure 6 shows ALADIN-HR wind data<br />

superimposed on re risk and simulation <strong>of</strong> re propagation maps.<br />

iForestFire is also award wining ICT project. In 2008 iForestFire won rst price (Tesla<br />

Golden Egg) on VIDI e-novation award, competition founded by VIDI publication and<br />

Rudjer Boskovic institute. It was elected as <strong>the</strong> most prominent and innovative ICT project<br />

in Croatia in 2008.<br />

4 Development and commercialization <strong>of</strong> iForestFire system<br />

Development <strong>of</strong> Intelligent Forest Fire Monitoring System started in autumn 2003 as a<br />

seminar on <strong>the</strong> postgraduate (Mr.Sc.) study at Faculty <strong>of</strong> Electrical Engineering, Mechanical<br />

Engineering and Naval Architecture, provoked by great damages caused by 2003 wild-<br />

res. The student Damir Krstini (who was also <strong>the</strong> voluntary reghter at island Hvar) enrolled<br />

<strong>the</strong> course Digital Image Processing and Analyses. The results <strong>of</strong> his seminar entitled<br />

“Wildre smoke segmentation” were more than promising, so we have decided to apply for<br />

technology project, and in 2003 we have received a grant TP-03/0023-09 ''System for early<br />

forest re detection based on cameras in visible spectra" supported by <strong>the</strong> Ministry <strong>of</strong> Science,<br />

Education and Sport <strong>of</strong> Republic Croatia. The grant funds were enough to start more<br />

intensive research, but not enough to nished it, so a part <strong>of</strong> our research were also funded<br />

by ordinary project 023-0232005-2003 "AgISEco Agent-based intelligent environmental<br />

monitoring and protection systems", by support <strong>of</strong> Split and Dalmatia County authorities<br />

through a study "Holistic approach to forest re protection in Split and Dalmatia County"<br />

and by our own resources.<br />

In initial system development four researchers were involved - Darko Stipaniev as a team<br />

leader, Maja Štula as a designer <strong>of</strong> overall Web based information system, Damir Krstini


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

as a designer <strong>of</strong> wildre detection algorithms and Ljiljana Šeri as a designer <strong>of</strong> wildre<br />

observer agent architecture. From <strong>the</strong> beginning <strong>the</strong> main reghters adviser was Tomislav<br />

Vuko, <strong>the</strong> vice commander <strong>of</strong> Croatian reghters for Adriatic Coast and Islands.<br />

Research started in 2003 with wildres video materials collecting necessary for detection<br />

algorithm development. Controlled res were burned at island Hvar in cooperation with<br />

voluntary reghters. Lot <strong>of</strong> video material was recorded and soon <strong>the</strong> rst version <strong>of</strong> <strong>of</strong>fline<br />

detection algorithm was developed. Figure 7 shows examples <strong>of</strong> rst algorithm detections<br />

in <strong>the</strong> typical landscape <strong>of</strong> island Hvar.<br />

Recording and collecting wildre images and video sequences is quite important for detection<br />

algorithm development and testing so this activity was carried out all <strong>the</strong> time. Today<br />

our database has more than 2.500 images selected and segmented by reference (ground<br />

truth) human observer. Figure 8 shows one typical example. On manually segmented image<br />

all regions were distinguished, because in <strong>the</strong> latest version <strong>of</strong> our detection algorithm<br />

region context based wildre alarm reduction has been applied so it was important to have<br />

manually segmented, not only wildre smoke – no smoke regions, but also o<strong>the</strong>r regions<br />

like sky, water, vegetation, man-made objects etc.<br />

Figure 7 – Examples <strong>of</strong> detection images in <strong>the</strong> typical landscape for Croatian coasts and islands<br />

(island Hvar 2003)<br />

Figure 8 – Input image and corresponding manually segmented image regions represented by<br />

various gray tonalities


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 69<br />

After successful laboratory implementation, <strong>the</strong> real life eld-testing was performed during<br />

re seasons 2004 and 2005. Three experimental monitoring stations were installed on<br />

Marjan Hill near Split, Vidova gora on island Bra and FESB faculty building in Split.<br />

These eld tests were performed in cooperation with Fire Brigade Administration for <strong>the</strong><br />

Coast, Protection and Rescue Operations Administration, Ministry <strong>of</strong> Interiors in Divulje<br />

so <strong>the</strong> main monitoring centers were in Divulje and <strong>the</strong> second one in our laboratory. Figure<br />

9 shows <strong>the</strong> experimental system layout and Figure 10 <strong>the</strong> experimental station on<br />

Marjan hill.<br />

Figure 9 – The experimental system layout used for iForestFire prototype<br />

testing in 2004 and 2005<br />

After <strong>the</strong> testing period a lot <strong>of</strong> improvements in both, hardware and s<strong>of</strong>tware design were<br />

implemented and in 2006 <strong>the</strong> commercialization phase has started and <strong>the</strong> rst real life<br />

monitoring system was installed in National Park Paklenica supported by Ministry <strong>of</strong> Culture<br />

<strong>of</strong> Republic Croatia. The system was partially developed as a technological project<br />

supported by Ministry <strong>of</strong> Science, Education and Sport <strong>of</strong> Republic Croatia and in contract<br />

signed with <strong>the</strong>m our obligations were also <strong>the</strong> system commercialization. Two models<br />

were possible – to establish a new spin-<strong>of</strong>f company or to nd a strategic partner. In that<br />

moment, <strong>the</strong> second option was more convenient for us, so we found <strong>the</strong> strategic partner<br />

in company Lama d.o.o. from Split (iForesFire, <strong>2011</strong>). Lama was responsible for system<br />

promotion, selling, installation and maintenance, but fur<strong>the</strong>r system improvements, development<br />

and research were and remain until today our obligations.<br />

The development <strong>of</strong> system like iForetFire is a never-ending story. The system version<br />

is now 2.7 (October <strong>2010</strong>) and beside <strong>the</strong> initial researchers involved in system development<br />

from <strong>the</strong> begineeng, in today’s version signicant contributions were given also by<br />

Toni Jakovevi (advanced IP based meteorological station, detection algorithm), Marin<br />

Bugari (Web GIS based system features), Josip Maras (component based system architecture),<br />

Petar Jeri (s<strong>of</strong>tware developement) and Kaja Radi (electronic components design<br />

and realization).


70<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 10 – The experimental station on Marjan hill<br />

Since 2006 <strong>the</strong> system was successfully applied in various Croatian national and nature<br />

parks (7 monitoring stations and 5 operational centers), but <strong>the</strong> most advanced is network<br />

application in Istria County. Istria system called Istria iForestFire Net (Stipaniev et al,<br />

<strong>2010</strong>) has 29 monitoring stations and 7 operational centers, mutually interconnected using<br />

encrypted VPN and hardware rewalls developed by our strategic partner – <strong>the</strong> company<br />

Lama. Figure 11 shows system layout and few screen prints <strong>of</strong> that system. iForestFire also<br />

has a quite promising export potentials. In March <strong>2011</strong> two demo units are in installation<br />

phase, one in Greece and <strong>the</strong> o<strong>the</strong>r in Portugal.<br />

Last but not least it is important to emphasize that iForestFire has initiated a lot <strong>of</strong> scientic<br />

research, too. As a result <strong>of</strong> research connected with system development three PhD <strong>the</strong>ses<br />

were written and defended (D.Krstini, Lj.Šeri and T.Jakovcevic), two PhD <strong>the</strong>ses are in<br />

preparation phase and lot <strong>of</strong> scientic papers were published in journals, books and conference<br />

proceedings. A specialized Web portal dedicated to wildre observers and smoke<br />

recognition has been created and maintained (http://wildre.fesb.hr), but also our interest<br />

in more general scientic wildre research has resulted in establishment <strong>of</strong> Center for<br />

Wildre Research (http://cipop.fesb.hr).


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 71<br />

Figure 11 – Istria iForestFire Net – advanced wildre monitoring network in Istria County<br />

5 Conclusion<br />

The only effective way to minimize damages caused by wildres is wildre early detection<br />

and fast and appropriate reaction, apart from preventive measures. Great efforts are<br />

<strong>the</strong>refore made to achieve early forest re detection, which is traditionally based on human<br />

surveillance. This paper shows how modern ICT technologies could be used for automatic<br />

wildre detection and monitoring. It describes <strong>the</strong> advanced wildre surveillance and monitoring<br />

system named iForestFire and entirely developed at University <strong>of</strong> Split Faculty <strong>of</strong><br />

Electrical Engineering, Mechanical Engineering and Naval Architecture.<br />

iForestFire is a practical realization <strong>of</strong> <strong>the</strong> observer network <strong>the</strong>ory. Observer network<br />

was dened as an advanced sensor network described using formal <strong>the</strong>ory <strong>of</strong> perception<br />

and a notation <strong>of</strong> <strong>the</strong> observer. iForestFire is both integral and intelligent system. Integral<br />

because it is based on various data types (images, meteorological data, GIS data) and intelligent<br />

because it has a lot <strong>of</strong> features derived from various intelligent technologies (multiagent<br />

architecture, advanced image analysis and image recognition algorithms, advanced<br />

procedures for false alarm reduction, augmented reality).<br />

The system was developed as a technological and scientic research project, but today it is<br />

commercial system widely used for advanced wildre surveillance and monitoring in various<br />

Croatian national and nature parks and Istria region, so it is a good example <strong>of</strong> successful<br />

university – industry cooperation, particularly because its development has provoked a<br />

lot <strong>of</strong> scientic research activities resulting in a number <strong>of</strong> PhD <strong>the</strong>sis and published papers<br />

in journals, books and conference proceedings.


72<br />

References<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

1. Arrue B C, Ollero A, Martinez de Dios J R (2000) An intelligent system for false alarm<br />

reduction in infrared forest-re detection. IEEE Int. Systems, May/June 2000, 64-72.<br />

2. Bugari M, Jakovevi T, Stipaniev D (2009) Automatic adjustement <strong>of</strong> detection<br />

parameters in forest re video monitoring system, MIPRO, May 2009, Opatija, pp.<br />

270-275<br />

3. Byungrak S, Yong-Sork H, and Jung-Gyu K, (2006) A Design and Implementation<br />

<strong>of</strong> Forest-Fires Surveillance System based on Wireless Sensor Networks for South<br />

Korea Mountains, IJCSNS Int. Journal <strong>of</strong> Computer Science and Network Security,<br />

V.6 No.9B, pp.124-130<br />

4. Forest Fire Finder NGNS IS, http://www.ngns-is.com/html/orestas/fff_intro_eng.<br />

html (Accessed March, 1 <strong>2011</strong>)<br />

5. iForestFire (<strong>2011</strong>) Itelligent Forest Fire Monitorig System, http://iforestre.fesb.hr<br />

(Accessed March, 1 <strong>2011</strong>)<br />

6. iMeteo (<strong>2011</strong>) Advance Ultrasound IP based Mini Meteorological Station, http://imeteo.fesb.hr<br />

(Accessed March, 1 <strong>2011</strong>)<br />

7. Jakovevi T, Stipaniev D, Krstini D, (2009) False alarm reduction in forest re<br />

video monitoring system, MIPRO 2009, May 25-29, Opatija, 264-269<br />

8. Jakovevi T, Šeri Lj, Stipaniev D, Krstini D, (<strong>2010</strong>) Wildre smoke detection algorithms<br />

evaluation, VI Int. Conf. on Forest Fire Research, Coimbra, Nov 15-18 <strong>2010</strong>.<br />

9. Krstini D, Jakovevi T, Stipaniev D, (2009) Histogram-Based Smoke Segmentation<br />

in Forest Fire Detection System, Information Technology and Control, Vol.38,<br />

No.3, 2009. 237-244<br />

10. Krstini D, Kuzmani Skelin A, Slapniar I (<strong>2011</strong>) Fast Two-Step Histogram-Based<br />

Image Segmentation, IET image processing. 5 (<strong>2011</strong>), 1; 63-72<br />

11. Kührt E, Knollenberg J, Mertens V (2001) An automatic early warning system for forest<br />

res, Annals <strong>of</strong> Burns and Fire Disasters, vol. XIV, n. 3, Sept. 2001<br />

12. Sahin Y, Animals as Mobile Biological Sensors for Forest Fire Detection, Sensors<br />

2007, 7, 3084-3099<br />

13. Sahin Y G, Turker Ince S, Early Forest Fire Detection Using Radio-Acoustic Sounding<br />

System, Sensors 2009, 9, 1485-1498<br />

14. Stipaniev D, Hrasnik B (2004) Integral, holistic model <strong>of</strong> wildre prevention in Split<br />

and Dalmatia County, Expert Study for Split and Dalmatia County, FESB Split, 2004.<br />

(231 pages) (in Croatian)<br />

15. Stipaniev D, Hrastnik B, Vuji R (2007) Holistic Approach to Forest Fire Protection<br />

in Split and Dalmatia County <strong>of</strong> Croatia, Wildre 2007 Int.Conference, Sevilla, Spain,<br />

May 2007.<br />

16. Stipaniev D, Bodroži Lj, Štula M (2007a) Environmental Intelligence based on Advanced<br />

Sensor Networks, Proc.<strong>of</strong> 14th Int.Conference on Systems, Signals and Image<br />

Processing, Maribor, Slovenija, 27-30.6.2007<br />

17. Stipaniev D, Bodroži Lj, Štula M (2007b) Data Fusion in Observer Networks, Proc.<br />

<strong>of</strong> Second (IEEE) International Workshop on Information Fusion and Dissemination<br />

in Wireless Sensor Networks. Pisa, Italia, 08.10.2007, 1-6<br />

18. Stipaniev D, Bugari M, Bodroži Lj (2009) Integration <strong>of</strong> Forest Fire Video Monitoring<br />

System and Geographic Information System, Proc. <strong>of</strong> 51st Int.Symp ELMAR<br />

2009, Zadar, Sept 2009, pp.49-52<br />

19. Stipaniev D, Štula M, Krstini D, Šeri Lj, Jakovevi T, Bugari M (<strong>2010</strong>) Advanced<br />

automatic wildre surveillance and monitoring network, VI International Conference<br />

on Forest Fire Research, Coimbra, Porugal, Nov. 15 – 18, <strong>2010</strong>, 053, 15 pages


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 73<br />

20. Šeri Lj, Stipaniev D, Štula M (2009) Observer network and forest re detection,<br />

Information Fusion, DOI: 10.1016/j.inffus.2009.12.003, on-line from Dec 28, 2009.<br />

21. Utkin A, Vilar R, Feasibility <strong>of</strong> forest-re smoke detection using lidar, International<br />

Journal <strong>of</strong> Wildland Fire 2003, 12(2) 159 – 166<br />

22. Viegas X, Pita L P, Nielsen F, Haddad K, Calisti Tassini C, D’Altrui G, Quaranta<br />

V, Dimino I, Acoustic and <strong>the</strong>rmal characterization <strong>of</strong> a forest re event, Proceedings<br />

<strong>of</strong> SPIE, Remote sensing <strong>of</strong> re, San Diego CA , 2008, vol. 7089, pp. 708904.1-<br />

708904.12<br />

23. Žaja D (2008) The role <strong>of</strong> Croatian Forests d.o.o. in ghtings again wildres, International<br />

Workshop – new Methodes and Approaches to Wildres Prevention and Protection,<br />

Dec, 8-11 2008., Makarska (in Croatian)


74<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Laboratory testing and numerical modelling <strong>of</strong> MBT<br />

waste deformability<br />

Igor Petrović, Ph.D.<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Geotechnical Engineering<br />

Hallerova aleja 7, Varaždin, Croatia<br />

e-mail: igor.petrovic@gfv.hr<br />

Pr<strong>of</strong>. Davorin Kovačić, Ph.D.<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Geotechnical Engineering<br />

Hallerova aleja 7, Varaždin, Croatia<br />

e-mail: davorin.kovacic@gfv.hr<br />

Abstract<br />

The paper deals with <strong>the</strong> experimental investigation and numerical simulation <strong>of</strong> <strong>the</strong> mechanical<br />

behaviour <strong>of</strong> samples from a “Mechanical Biological Treatment” waste deposit<br />

(MBT waste deposit). Laboratory tests with samples <strong>of</strong> different moisture contents were<br />

conducted to determine <strong>the</strong> basic geotechnical characteristics as well as <strong>the</strong> stress-strain<br />

relations under loading and reloading conditions. When it is required to evaluate <strong>the</strong> loaddeformation<br />

characteristics <strong>of</strong> specimens containing relatively large-diameter grain particles,<br />

like MBT waste for example, <strong>the</strong> standard oedometric apparatus with cell (sample)<br />

diameter <strong>of</strong> 56 mm is evidently inadequate. Therefore, at <strong>the</strong> University <strong>of</strong> Zagreb, an<br />

oedometer <strong>of</strong> 500 mm in internal diameter was designed, fabricated, assembled and evaluated.<br />

As only limited experimental results were available, for numerical simulations a simplied<br />

hypoplastic model was used. For <strong>the</strong> calibration <strong>of</strong> this model it was sufcient to conduct<br />

oedometer tests and to use a simple procedure to estimate <strong>the</strong> angle <strong>of</strong> friction. The model<br />

proved to be satisfactory for modelling <strong>the</strong> compaction behaviour <strong>of</strong> MBT waste observed<br />

in experiments.<br />

Key words: compressibility, hypoplasticity, MBT waste, oedometer, stiffness<br />

1 Introduction<br />

The waste management is actually one <strong>of</strong> <strong>the</strong> most important issues related to <strong>the</strong> protection<br />

<strong>of</strong> <strong>the</strong> environment. Remarkably high amount <strong>of</strong> money is invested in waste management,<br />

including <strong>the</strong> separation, recycling, transport and permanent landlling <strong>of</strong> municipal solid<br />

waste. According to <strong>the</strong> Waste Management Strategy <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia (2005), a<br />

more intensive process <strong>of</strong> rehabilitation and improvement <strong>of</strong> sanitary conditions on a large<br />

number <strong>of</strong> uncontrolled waste dumps started in 1990s.<br />

The objective <strong>of</strong> <strong>the</strong> Strategy is to establish framework within which Croatia should reduce<br />

<strong>the</strong> amounts <strong>of</strong> waste it produces, and to be able to manage it in a sustainable manner. Taking<br />

<strong>the</strong> assessment <strong>of</strong> current situation and a vision <strong>of</strong> an appropriate waste management<br />

system as a starting point, <strong>the</strong> Strategy sets <strong>the</strong> objectives and <strong>of</strong>fers suggestions for <strong>the</strong>ir<br />

gradual achievement by 2025.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 75<br />

An ideal project <strong>of</strong> waste management in <strong>the</strong> Republic <strong>of</strong> Croatia corresponds to <strong>the</strong> socalled<br />

non-landll concept. In order to achieve this project it would be necessary to close<br />

<strong>the</strong> circle starting from avoidance <strong>of</strong> waste production, reduction <strong>of</strong> quantities and harmfulness,<br />

recycling and recovery (mechanical, biological, energy recovery) to <strong>the</strong> use <strong>of</strong> inert<br />

residue.<br />

The Strategy has set quantitative targets that determine <strong>the</strong> dynamics <strong>of</strong> meeting strategic<br />

objectives (Table 1). Deadlines are determined with <strong>the</strong> expected time delays in relation to<br />

EU regulations.<br />

Therefore <strong>the</strong> following basic activities are to be performed:<br />

- rehabilitation and closure <strong>of</strong> <strong>the</strong> existing open dumps,<br />

- extension and improvement <strong>of</strong> those landlls which will remain in operation,<br />

- construction <strong>of</strong> new waste management centres in which <strong>the</strong> inevitable waste should be<br />

landlled.<br />

Table 1. Quantitative targets for landlls<br />

Targets<br />

Year<br />

2005. <strong>2010</strong>. 2015. 2020. 2025.<br />

Regional centres for waste<br />

management<br />

0 1-2 2-3 3 4<br />

County centres for waste management<br />

0 3-7 7-10 10-14 14-21<br />

“Ofcial landlls” * 187 100 50 30 14-21<br />

Percentage <strong>of</strong> remedied landlls<br />

(% from <strong>the</strong> number determined<br />

in 2000).<br />

5 65 75 85 100<br />

*Group “Ofcial landlls“ consists <strong>of</strong> <strong>the</strong> following categories dened above: legal land-<br />

lls, landlls in <strong>the</strong> process <strong>of</strong> legalization, <strong>of</strong>cial landlls, and landlls by agreement<br />

A waste landll has to be regarded as an engineered structure for which long-term safety<br />

has to be proved on <strong>the</strong> basis <strong>of</strong> an appropriate geotechnical design. This means that <strong>the</strong><br />

waste body has to be stable against slope failure. Fur<strong>the</strong>rmore, <strong>the</strong> deformations behaviour<br />

and stresses imposed on subsoil, liner systems and internal structures have to be assessed.<br />

Figure 1 gives schematic illustration <strong>of</strong> possible failure mechanisms and deformations<br />

problems (Jessberger et al., 1995)


76<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 1. Stability and deformation <strong>of</strong> a landll<br />

The study <strong>of</strong> <strong>the</strong> mechanical behaviour <strong>of</strong> municipal solid waste by monitoring <strong>the</strong> existing<br />

landlls and by laboratory testing <strong>of</strong> waste samples was named “waste mechanics” in<br />

<strong>the</strong> handbook issued by German Geotechnical Society in <strong>the</strong> chapter: Principles <strong>of</strong> Waste<br />

Mechanics in <strong>the</strong> Geotechnical Design <strong>of</strong> Landlls (1993).<br />

The results <strong>of</strong> a survey conducted in <strong>the</strong> period 1992 - 2000 (for both continental and coastal<br />

parts <strong>of</strong> <strong>the</strong> Croatia) show that <strong>the</strong> average <strong>annual</strong> composition <strong>of</strong> municipal solid waste<br />

has a biodegradable portion <strong>of</strong> 74,5 % (Domanovac et al., 2002). Waste Management Plan<br />

<strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia for 2007-2015 (2007) requires that until 2020, <strong>the</strong> biodegradable<br />

portion <strong>of</strong> municipal solid waste should be reduced to 35 % <strong>of</strong> <strong>the</strong> mass portion <strong>of</strong> biodegradable<br />

municipal solid waste produced in 1997. According to Ordinance on <strong>the</strong> methods<br />

and conditions for <strong>the</strong> landll <strong>of</strong> waste categories and operational requirements for waste<br />

landlls (2007), which is based on Council Directive 1999/31/EC <strong>of</strong> 26 April 1999 on <strong>the</strong><br />

landll waste, only pre-treated waste is allowed to be dumped in landlls. Most <strong>of</strong> county<br />

waste management plans anticipated mechanical biological treatment (MBT) as <strong>the</strong> optimum<br />

waste treatment method.<br />

The goal <strong>of</strong> mechanical biological waste treatment is <strong>the</strong> recycling <strong>of</strong> separated fractions<br />

(which leads to <strong>the</strong> reduction <strong>of</strong> landll volume) on one side, and <strong>the</strong> biological stabilisation<br />

<strong>of</strong> <strong>the</strong> waste on <strong>the</strong> o<strong>the</strong>r side. One <strong>of</strong> <strong>the</strong> consequences <strong>of</strong> <strong>the</strong> waste treatment is <strong>the</strong><br />

change <strong>of</strong> physical, biological and chemical properties <strong>of</strong> <strong>the</strong> material to be landlled,<br />

compared with <strong>the</strong> wastes which have been landlled before. It can be concluded that <strong>the</strong><br />

knowledge <strong>of</strong> mechanical parameters <strong>of</strong> MBT waste for <strong>the</strong> design <strong>of</strong> landlls, which will<br />

be built within waste management centres, is necessary. The extended operation period <strong>of</strong><br />

a landll due to <strong>the</strong> reduction <strong>of</strong> landll volume is directly dependent on <strong>the</strong> deformability<br />

properties <strong>of</strong> MBT waste which are in <strong>the</strong> focus <strong>of</strong> <strong>the</strong> present research.<br />

Most commercial geotechnical laboratories have been utilizing some kind <strong>of</strong> Casagrandetype<br />

oedometer (Casagrande, 1936) for routine measurements <strong>of</strong> deformability parameters<br />

<strong>of</strong> ne-grained soils for decades. O<strong>the</strong>r names for this test are: one-dimensional compression<br />

test, <strong>the</strong> conned compression test and <strong>the</strong> consolidation test. The apparatus contains<br />

an oedometer cell that can be installed in a loading frame so that a predetermined vertical<br />

consolidation stress can be applied to <strong>the</strong> specimen. The soil specimen is restrained laterally<br />

by a steel oedometer cell. The top and bottom surface <strong>of</strong> <strong>the</strong> specimen are in contact


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 77<br />

with porous stone discs, so that <strong>the</strong> excess pore water pressure induced in <strong>the</strong> specimen by<br />

<strong>the</strong> applied loading can be dissipated through simultaneous upward and downward drainage<br />

during consolidation. The specimen has to be fully submerged in water during <strong>the</strong> test<br />

to eliminate <strong>the</strong> surface tension <strong>of</strong> water at <strong>the</strong> drainage surfaces, so as to allow unrestricted<br />

drainage <strong>of</strong> water. The test is considered to be one dimensional as both specimen deformation<br />

and drainage occur in <strong>the</strong> vertical direction only. Oedometer samples usually have a<br />

diameter <strong>of</strong> 56 mm and <strong>the</strong> thickness-diameter ratio 1:3 to 1:4.<br />

Based on <strong>the</strong> above mentioned consideration, <strong>the</strong> manufacturing <strong>of</strong> large oedometer <strong>of</strong><br />

500 mm in internal diameter, suitable for testing MBT waste samples, was initiated within<br />

<strong>the</strong> scientic project “Characterization <strong>of</strong> municipal solid waste”. The basic outline <strong>of</strong> <strong>the</strong><br />

project was given by Petrovi (2008). The manufacturing <strong>of</strong> large oedometer started in<br />

September 2008 and lasted until March 2009 when it was assembled at <strong>the</strong> Faculty <strong>of</strong><br />

Geotechnical Engineering.<br />

2 Basic geotechnical characteristics <strong>of</strong> tested MBT waste material<br />

The MBT waste samples used for testing were imported from an MBT waste landll in<br />

Austria as in <strong>the</strong> Republic <strong>of</strong> Croatia <strong>the</strong>re is no MBT facility yet installed. Naturally <strong>the</strong>re<br />

was no experience in laboratory testing <strong>of</strong> MBT samples so far.<br />

Prior to laboratory testing <strong>the</strong> waste was dried in <strong>the</strong> open air for two weeks. After drying<br />

<strong>the</strong> equilibrium moisture content was determined according to ASTM D 2974 as in case <strong>of</strong><br />

organic soil samples. The samples were dried in <strong>the</strong> oven at <strong>the</strong> temperature 1050C. The<br />

equilibrium water content was 7 %.<br />

Figure 2 shows <strong>the</strong> particle size distribution curve for <strong>the</strong> air dried MBT waste material according<br />

to HRN.U.B1.018. It can be seen that <strong>the</strong> largest particle diameter does not exceed<br />

30 mm and <strong>the</strong>refore fulls <strong>the</strong> requirement that <strong>the</strong> largest particle diameter should not<br />

exceed <strong>the</strong> 1/5 <strong>of</strong> <strong>the</strong> sample height which, for <strong>the</strong> oedometer used, is 40 mm. Since <strong>the</strong><br />

ne-grained portion <strong>of</strong> <strong>the</strong> waste material is less than 10 %, a particle size analysis using<br />

<strong>the</strong> hydrometer test procedure was not conducted. According to <strong>the</strong> Unied Soil Classication<br />

System (USCS), <strong>the</strong> MBT waste can be classied as a coarse grained material, as<br />

<strong>the</strong> particle sizes lie in <strong>the</strong> range between 0.05 and 30 mm. The uniformity coefcient and<br />

coefcient <strong>of</strong> curvature are Cu = 26 and Cc = 1.5, respectively. Therefore <strong>the</strong> tested MBT<br />

waste is a well-graded material and it can be well compacted.<br />

Figure 2. Particle size distribution curve <strong>of</strong> MBT waste


78<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

The average density <strong>of</strong> <strong>the</strong> solid particles, s, was determined according to <strong>the</strong> ASTM D<br />

854 on <strong>the</strong> air free samples with maximum particle size <strong>of</strong> 4.75 mm using a pycnometer <strong>of</strong><br />

a known volume. The particles larger than 4.75 mm were removed by sieving. The value<br />

s = 2147 [kg/m 3 ] was determined.<br />

Detailed description <strong>of</strong> <strong>the</strong> laboratory testing <strong>of</strong> basic MBT waste parameters is given by<br />

Petrovi et al. (<strong>2011</strong>b).<br />

3 Design, fabrication and assembly <strong>of</strong> a large oedometer<br />

Since standards for testing compressibility behaviour <strong>of</strong> MBT waste do not exist it was<br />

concluded that a large oedometer must be designed, manufactured, assembled and evaluated<br />

in accordance with standards for testing compressibility behaviour <strong>of</strong> soils. This is quite<br />

in line with <strong>the</strong> fact that waste mechanics had been developed on <strong>the</strong> basis <strong>of</strong> soil mechanics<br />

principles. The most relevant standards used for dening <strong>the</strong> technical specications<br />

<strong>of</strong> large oedoemeter are British (BS 1377: Part 5: 1990) and American (ASTM D 2435)<br />

standards for compressibility testing as well as Croatian standard Eurocode 7: Geotechnical<br />

design – Part 2 - Ground investigation and testing (HRN EN 1997-2:2008). Technical<br />

specications <strong>of</strong> new oedometer were dened in collaboration with several mechanical<br />

<strong>engineering</strong>, industrial management and IT companies from Varaždin.<br />

The diameter <strong>of</strong> <strong>the</strong> new oedometer cell is 500 mm and <strong>the</strong> height is 200 mm. It means that<br />

minimum height-diameter ratio 1:2,5 required by <strong>the</strong> British standard in order to minimize<br />

<strong>the</strong> effect <strong>of</strong> <strong>the</strong> side friction forces, is satised. Maximum vertical pressure on sample is<br />

2000 kN/m 2 . The force (pressure) on specimen is transmitted by means <strong>of</strong> hydraulic loading<br />

actuator. Pressure transducer has a minimum accuracy ± 0,05 % <strong>of</strong> full range output<br />

(FRO). Displacement transducer has a minimum accuracy ± 0,05 % FRO and minimum<br />

stroke <strong>of</strong> 9 cm. The lower and upper lids, as well as <strong>the</strong> pressure plate, are made from<br />

structural steel (all protected against corrosion). Compression tests are fully automated<br />

(computer-controlled).<br />

Figure 3 shows a nal set-up <strong>of</strong> <strong>the</strong> large oedometer system while Figures 4, 5, 6 and 7<br />

present selected parts <strong>of</strong> a large oedometer during <strong>the</strong> production phase.<br />

Figure 3. Final set-up <strong>of</strong> <strong>the</strong> large oedometer system


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 79<br />

Figure 4 presents an upper and lower lid <strong>of</strong> oedometric cell. Maximum deformation <strong>of</strong> lids<br />

at highest load should not exceeds 0,7 mm. Figure 5 presents hydraulic loading actuator<br />

while Figure 6 presents oedometric cell ring polished to burnish so that friction between<br />

sample and cell ring is reduced to minimum. Figure 7 presents drainage porous plates<br />

which are required for dissipation <strong>of</strong> <strong>the</strong> excess pore pressure. Drainage porous plates<br />

are made from 1 mm thick stainless steel. The clogging <strong>of</strong> <strong>the</strong> drainage holes should be<br />

prevented with <strong>the</strong> use <strong>of</strong> <strong>the</strong> lter paper or geotextile placed between <strong>the</strong> specimen and<br />

drainage plate.<br />

Figure 4. An upper and lower lid <strong>of</strong> oedometric cell<br />

Figure 5. Hydraulic loading actuator<br />

Figure 6. Cell ring


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 7. Porous drainage plate<br />

As <strong>the</strong> innovative parts <strong>of</strong> <strong>the</strong> large oedometer are still subject <strong>of</strong> legal protection (patent<br />

registration), detailed technical description <strong>of</strong> <strong>the</strong> apparatus can not be given before <strong>the</strong><br />

completion <strong>of</strong> <strong>the</strong> legal procedure.<br />

4 Oedometric compression tests and friction angle<br />

4.1 Sample preparation<br />

In <strong>the</strong> present paper <strong>the</strong> properties <strong>of</strong> two MBT waste samples are presented, where Sample<br />

A is characterized by an initial moisture content <strong>of</strong> w = 65 % and Sample B is characterized<br />

by an initial moisture content <strong>of</strong> w = 41 %.<br />

In order to obtain a homogenous distribution <strong>of</strong> moisture content through <strong>the</strong> whole specimen<br />

after mixing with water, <strong>the</strong> wetted samples were left untouched for <strong>the</strong> next 24 hours.<br />

Then <strong>the</strong> samples were installed in <strong>the</strong> oedometer cell in ve layers. On average, each layer<br />

was 4 cm thick and pre-compacted to a dened initial void ratio.<br />

The basic geotechnical parameters for both samples at <strong>the</strong> beginning <strong>of</strong> <strong>the</strong> test are presented<br />

in Table 2 respectively. Herein denotes <strong>the</strong> density, w <strong>the</strong> moisture content, d <strong>the</strong><br />

dry density, s <strong>the</strong> average density <strong>of</strong> solid particles, e <strong>the</strong> void ratio and S <strong>the</strong> degree <strong>of</strong><br />

saturation.<br />

Table 2 Basic geotechnical parameters <strong>of</strong> tested samples<br />

w d s e0 S<br />

[kg/m 3 ] [%] [kg/m 3 ] [kg/m 3 ] / [%]<br />

Sample A 1366 65 828 2147 1,59 88<br />

Sample B 1093 31 834 2147 1,57 42<br />

4.2 Consolidation procedure<br />

The initial pressure obtained from <strong>the</strong> pressure plate was 4,7 kN/m 2 . A sequence <strong>of</strong> loadings<br />

was applied, where <strong>the</strong> next load step was applied after <strong>the</strong> completion <strong>of</strong> consolidation<br />

<strong>of</strong> <strong>the</strong> preceding loading step. The loading steps are 36, 82 and 180 kN/m 2 , followed<br />

by unloading to 36 kN/m 2 , <strong>the</strong>n reloading to 365 kN/m 2 and nally unloading to 4,7 kN/m 2 .


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 81<br />

4.3 Oedometric test results and <strong>the</strong>ir evaluation<br />

Figure 8 presents stress-strain relationship for samples A and B respectively.<br />

Figure 8. Stress-strain relationship for one-dimensional compression<br />

The graphs on Figure 8 can be used in order to determine secant compressibility moduli for<br />

usual load increments (Table 3)<br />

Table 3. Secant compressibility moduli<br />

Load 4,7-50 50-100 100-200 200-360<br />

Increment [kN/m 2 ] [kN/m 2 ] [kN/m 2 ] [kN/m 2 ]<br />

Sample A 566 1190 1515 3666<br />

Sample B 657 1316 1639 2860<br />

The values from Table 3 are compared with test results published by o<strong>the</strong>r researchers<br />

(Table 4).<br />

Table 4. Compressibility moduli published by o<strong>the</strong>r researchers<br />

Load (0) 25-50 50-100 100-200 200-400 400-600 280-420 Fraction<br />

increment/<br />

Ref.<br />

[kN/m 2 ] [kN/m 2 ] [kN/m 2 ] [kN/m 2 ] [kN/m 2 ] [kN/m 2 ] [mm]<br />

Duelmann<br />

(2002)<br />

730 1480 2460 4920 / / 0-30<br />

840 1990 1870 3290 / / 0-20<br />

800 1000 1800 / / / 0-20<br />

Kuehle- 1070 1590 1680 2880 / / 0-40<br />

Weidemeier<br />

(2003)<br />

500 1100 1600 2800 / / 0-40<br />

940 1490 2440 3030 / / 0-60<br />

600 1300 2000 2800 / / 0-60


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et al. (1999)<br />

Ziehmann<br />

(1999)<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

355 1670 1947 2904 4514 / < 60<br />

239 905 1570 2973 4977 / < 100<br />

/ / / / / 5100 /<br />

/ / / / / 7900 < 60<br />

By comparison <strong>of</strong> <strong>the</strong> values <strong>of</strong> compressibility moduli from Table 3 and Table 4 it can be<br />

concluded that <strong>the</strong> values obtained for <strong>the</strong> load increments 0 – 50 (25-50), 50 – 100 and<br />

100 – 200 kN/m2 t well with <strong>the</strong> values <strong>of</strong> compressibility moduli by o<strong>the</strong>r researchers.<br />

The values obtained for load increment 200 – 360 kN/m 2 are somewhat higher than <strong>the</strong><br />

values published by Bidlingmaier et al. (1999) and by Kuehle-Weidemeier (2003). Yet according<br />

to Duellmann (2002) i Ziehmann (1999) it is possible to obtain even higher values<br />

<strong>of</strong> compressibility moduli for approximately same load increment.<br />

In addition, Figure 9 presents comparison <strong>of</strong> measured stress-strain curves with stress-strain<br />

curves <strong>of</strong> MBT waste published by Duelmann (2002) and Kuehle-Weidemeier (2003).<br />

Figure 9 Comparison <strong>of</strong> measured stress-strain relationships with stress-strain relationships<br />

published by o<strong>the</strong>r researchers<br />

Figure 9 shows a good agreement, with respect to <strong>the</strong> relative deformation, <strong>of</strong> <strong>the</strong> selected<br />

stress-strain relationships with stress-strain relationships published by Duelmann (2002)<br />

and Kuehle-Weidemeier (2003). It should be also emphasized that <strong>the</strong> largest particle size<br />

<strong>of</strong> MBT samples used by Duelmann (2002) and Kuehle-Weidemeier (2003) corresponds<br />

well to <strong>the</strong> largest particle size <strong>of</strong> <strong>the</strong> tested MBT waste material. The elasto-plastic behaviour<br />

<strong>of</strong> MBT waste dened by Duelmann (2002) has been also conrmed.<br />

Detailed description <strong>of</strong> <strong>the</strong> oedometric compression tests <strong>of</strong> MBT waste samples is given<br />

by Petrovi et al. (<strong>2010</strong>) and Petrovi et al. (<strong>2011</strong>c).<br />

4.4 Friction angle<br />

In order to estimate <strong>the</strong> critical friction angle c, <strong>the</strong> angle <strong>of</strong> repose <strong>of</strong> <strong>the</strong> dry waste material<br />

was determined. The measurements were conducted on two separate samples at <strong>the</strong><br />

bottom and at <strong>the</strong> top <strong>of</strong> <strong>the</strong> repose in twelve different points. The values measured were<br />

as follows: 370, 310, 310, 410, 380, 380, 350, 400, 410, 380, 500, 430. If <strong>the</strong> highest and<br />

lowest values are considered to be unrealistic and are disregarded, <strong>the</strong>n <strong>the</strong> mean value is<br />

390 with a standard deviation <strong>of</strong> ± 2.450.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 83<br />

5 Constitutive model<br />

In order to model <strong>the</strong> behaviour under oedometric conditions rst a relation between <strong>the</strong><br />

void ratio e and <strong>the</strong> mean effective pressure p for monotonic compression is considered. In<br />

particular, <strong>the</strong> decrease <strong>of</strong> e with an increase <strong>of</strong> p is described by <strong>the</strong> following exponential<br />

function:<br />

(1)<br />

where <strong>the</strong> constant e0 denotes <strong>the</strong> void ratio for p 0, hoe has <strong>the</strong> dimension <strong>of</strong> stress and n<br />

is a dimensionless constant. It can be noted that function (1) is similar to <strong>the</strong> approximation<br />

function for isotropic compression proposed by Bauer (1996), i.e.<br />

(2)<br />

While in <strong>the</strong> function by Bauer <strong>the</strong> quantities eio, , and hs are dened for <strong>the</strong> isotropic<br />

compression curve starting from <strong>the</strong> loosest possible state <strong>of</strong> <strong>the</strong> grain skeleton, <strong>the</strong> parameters<br />

eo, p, n and hoe in Eq. (1) are related to monotonic oedometric compression. Herein<br />

<strong>the</strong> mean pressure reads p = - (11+ 22+ 33)/3 = -(1+2K0) 11/3, where 11 is <strong>the</strong> vertical<br />

stress, 22 = 33 <strong>the</strong> lateral stress under zero lateral strain and K0 denotes <strong>the</strong> pressure<br />

coefcient at rest, i.e. K0= 22 / 11= 33 / 11. Usually K0 is obtained in experiments<br />

by measuring <strong>the</strong> vertical and horizontal stresses simultaneously. As this was not carried<br />

out in <strong>the</strong> experiments conducted, it is necessary to make estimation for <strong>the</strong> value <strong>of</strong> K0.<br />

The most established semi-empirical function in <strong>engineering</strong> practice is <strong>the</strong> relation proposed<br />

by Jaky (1944), where K0 is related to <strong>the</strong> critical friction angle c according to: K0<br />

= 1 - sin c.<br />

A comprehensive review <strong>of</strong> experimental data obtained from different soils, however,<br />

shows that K0 not only depends on <strong>the</strong> friction angle but also on <strong>the</strong> current density and<br />

<strong>the</strong> pressure level. Bauer (1997), for instance, reported a remarkable agreement between<br />

experiments carried out under different densities and <strong>the</strong> corresponding predictions with<br />

<strong>the</strong> hypoplastic model proposed by Bauer (1996) and Gudehus (1996). The framework<br />

<strong>of</strong> hypoplasticity is <strong>the</strong>refore suitable to get an approximation for K0 and to model <strong>the</strong><br />

inelastic and non-linear stress strain behaviour under axisymmetric loading and unloading.<br />

In particular for oedometric boundary conditions <strong>the</strong> constitutive equations (3-4) are<br />

proposed, which present a simplied version <strong>of</strong> <strong>the</strong> hypoplastic model by Bauer (1996) and<br />

Gudehus (1996).<br />

(3)<br />

(4)


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Assuming a constant grain density, <strong>the</strong> balance equation <strong>of</strong> mass leads to a relation between<br />

<strong>the</strong> rate <strong>of</strong> <strong>the</strong> void rate, , and <strong>the</strong> volumetric strain rate, , i.e. equation (5) can<br />

be derived:<br />

(5)<br />

Herein, is <strong>the</strong> time derivative <strong>of</strong> <strong>the</strong> Cauchy stress are normalized<br />

quantities, is <strong>the</strong> strain rate, and is <strong>the</strong> rate <strong>of</strong> void ratio. Factor is related to <strong>the</strong> critical<br />

friction angle c and for general stress paths also depends on <strong>the</strong> Lode angle in <strong>the</strong><br />

deviator plane (Bauer, 2000). For axisymmetric loading paths factor reduces to (Bauer<br />

& Herle, 2000):<br />

(6)<br />

In Eq. (3) and Eq. (4) <strong>the</strong> density factor >0 is related to <strong>the</strong> limit void ratios as outlined<br />

in more detail by Bauer (1996) and Gudehus (1996). In particular 1 for a loose material. In <strong>the</strong> present paper is assumed to be constant.<br />

The compression law (1) is embedded in <strong>the</strong> stiffness factor using <strong>the</strong> consistency condition<br />

for oedometric compression, which leads to <strong>the</strong> following relation:<br />

(7)<br />

Under monotonic oedometric compression <strong>the</strong> following expression is obtained from Eq.<br />

(3) and Eq. (4) for <strong>the</strong> stress ratio<br />

(8)<br />

K 0<br />

in Eq. (8) is also called <strong>the</strong> pressure coefcient at rest. It depends on <strong>the</strong> critical friction<br />

angle c and <strong>the</strong> density factor . From Figure 10 it can be seen that Eq. (8) allows a ner<br />

adaptation <strong>of</strong> K 0<br />

. In particular higher friction angles c and lower values <strong>of</strong> <strong>the</strong> density<br />

factor give signicantly lower values for K 0<br />

while Jaky’s relation is independent <strong>of</strong> <strong>the</strong><br />

current density.<br />

The hypoplastic model proposed for MBT waste material includes ve constants. Taking<br />

into account Eq. (8) for K 0<br />

, a critical friction angle <strong>of</strong> c = 39º and =1.1, <strong>the</strong> values e o<br />

,<br />

h oe<br />

and n <strong>of</strong> <strong>the</strong> approximation function (1) can be calibrated. For Sample A, a comparison<br />

<strong>of</strong> <strong>the</strong> results obtained from Eq. (1) with <strong>the</strong> experiments is shown in Figure 11. For <strong>the</strong><br />

numerical simulations discussed in Section 6 <strong>the</strong> constants used are presented in Table 5.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 85<br />

Figure 10. Comparison <strong>of</strong> K 0<br />

values obtained with <strong>the</strong> hypoplastic constitutive model (HM) for<br />

different density factor and friction angles c with <strong>the</strong> function by Jaky (1944)<br />

Table 5. Constants used for numerical simulations<br />

hs<br />

[kN/m 2 ]<br />

n e0 fd<br />

[0]<br />

Sample A 3519 0.389 1.75 1.1 39<br />

Figure 11. Comparison <strong>of</strong> <strong>the</strong> oedometric compression relation according to Eq. (1) with <strong>the</strong><br />

experimental results for Sample A<br />

6 Comparison <strong>of</strong> numerical simulations with experiments<br />

In <strong>the</strong> following <strong>the</strong> results obtained from numerical simulations <strong>of</strong> oedometric compression<br />

tests are compared with <strong>the</strong> corresponding experiments by Petrovi (<strong>2010</strong>). All simulations<br />

are conducted under drained conditions. Figure 12 show a good agreement between<br />

<strong>the</strong> results obtained from <strong>the</strong> numerical simulation (solid curve) and <strong>the</strong> experimental data<br />

(dots). Is should be noticed that with <strong>the</strong> presented hypoplastic model only loading and<br />

unloading can be modelled. For <strong>the</strong> simulation <strong>of</strong> loading cycles an extension <strong>of</strong> <strong>the</strong> constitutive<br />

model is needed as proposed for instance by Bauer & Wu (1992), Niemunis &<br />

Herle (1997).


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 12. Oedometric compression and extension <strong>of</strong> Sample A<br />

Detailed description <strong>of</strong> <strong>the</strong> numerical modelling <strong>of</strong> MBT waste deformability is given by<br />

Petrovi et al. (<strong>2011</strong>a).<br />

7 Conclusions<br />

A 500 mm internal diameter Casagrande-type oedometer has been designed, manufactured,<br />

and assembled at <strong>the</strong> University <strong>of</strong> Zagreb. The manufacturing costs were about 17.000,00<br />

EUR. It was a ra<strong>the</strong>r demanding task to produce a laboratory device capable to give reliable<br />

results with very limited nancial resources. In order to achieve this goal many innovative<br />

and unusual technical solutions were applied. Some <strong>of</strong> <strong>the</strong> innovative parts <strong>of</strong> <strong>the</strong><br />

large oedometer are currently in <strong>the</strong> process <strong>of</strong> legal protection (patent registration). The<br />

laboratory results obtained with <strong>the</strong> new device prove that even with limited resources it is<br />

still possible to achieve a respectable scientic result as long as scientists keep <strong>the</strong>ir minds<br />

wide open.<br />

The results obtained from <strong>the</strong> evaluation program indicate that <strong>the</strong>y are comparable to <strong>the</strong><br />

results published by o<strong>the</strong>r authors. The particle size distribution curve conrmed that <strong>the</strong><br />

MBT waste can be classied as a coarse grained material. A good agreement <strong>of</strong> stressstrain<br />

curves for samples A and B proves that new apparatus can provide repeatability <strong>of</strong><br />

<strong>the</strong> oedometer test. It has been veried that <strong>the</strong> magnitude <strong>of</strong> vertical relative deformation<br />

is in <strong>the</strong> range 15 - 25 % for given load range. The elasto-plastic behaviour <strong>of</strong> MBT waste<br />

has been also conrmed. Simplied hypoplastic model proved to be satisfactory for modelling<br />

<strong>the</strong> compaction behaviour <strong>of</strong> MBT waste observed in experiments<br />

A complete presentation <strong>of</strong> <strong>the</strong> laboratory testing and numerical modelling <strong>of</strong> MBT waste<br />

deformability toge<strong>the</strong>r with <strong>the</strong> recommendations for future research is given by Petrovi<br />

(<strong>2010</strong>).<br />

8 Acknowledgements<br />

The nancial support <strong>of</strong> <strong>the</strong> Ministry <strong>of</strong> Science, Education and Sports <strong>of</strong> <strong>the</strong> Republic <strong>of</strong><br />

Croatia for <strong>the</strong> project "Characterization <strong>of</strong> municipal solid waste" (160-0831529-3031) is<br />

gratefully acknowledged.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 87<br />

References<br />

1. Bauer E (1996) Calibration <strong>of</strong> a comprehensive hypoplastic model for granular materials.<br />

Soils and Foundations., Vol. 36(1), pp 13-26<br />

2. Bauer E (1997) The critical state concept in hypoplasticity. 9th International Conference<br />

on Computer Methods and Advances in Geomechanics, IACMAG 97, Wuhan,<br />

China, Balkema, pp 691–696.<br />

3. Bauer E (2000) Conditions for embedding Casagrande’s critical states into hypoplasticity.<br />

Mechanics <strong>of</strong> Cohesive-Frictional Materials, 5. pp 125-148<br />

4. Bauer E, Wu W (1992) A hypoplastic model for granular soils under cyclic loading, In:<br />

Kolymbas (ed.) Proceedings <strong>of</strong> <strong>the</strong> International Workshop on Modern Approaches to<br />

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8. Domanovac T, Orašanin R (2002) Municipal solid waste composition for continental<br />

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Symposium Waste Management Zagreb 2002, mtg-topgraf, Zagreb, pp 61-68 (in Croatian)<br />

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Zentraldeponie Hannover, Laboruntersuchungen zum Verdichtungs-, Durchlaessigkeits-,<br />

Last-Setzungs- und Scherverhalten. Februar 2002. Im Auftrag des Abfallwirtschaftsbetriebes<br />

Hannover<br />

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GLR, Second Edition, Ernst & Sohn, Berlin, 1993.<br />

11. Gudehus G (1996) A comprehensive constitutive equation for granular materials. Soils<br />

and Foundations, Vol 36(1), pp 1-12<br />

12. Jaky J (1944) The Coefcient <strong>of</strong> Earth Pressure at Rest. Journal for Society <strong>of</strong> Hungarian<br />

Architects and Engineers, pp 355-358<br />

13. Jessberger HL, Kockel R (1995) Determination and assessment <strong>of</strong> <strong>the</strong> mechanical properties<br />

<strong>of</strong> waste materials. In: Sarsby (ed.) Waste Disposal by Landlls – GREEN'93,<br />

Balkema, Bolton, pp 313-322<br />

14. Kuehle-Weidemeier M. (2003) Landlling and properties <strong>of</strong> MBP waste, Proceedings<br />

Sardinia 2003, Ninth International Waste Management and Landll Symposium, S.<br />

Margherita di Pula, Cagliari, Italy<br />

15. Niemunis A, Herle I (1997) Hypoplastic model for cohesionless soils with elastic<br />

16. strain range. Mechanics <strong>of</strong> Cohesive-Frictional Materials, Vol. 2(4), pp 279-299<br />

17. Ordinance on <strong>the</strong> methods and conditions for <strong>the</strong> landll <strong>of</strong> waste, categories and<br />

operational requirements for waste landlls (2007) Ofcial Gazette <strong>of</strong> <strong>the</strong> Republic <strong>of</strong><br />

Croatia, No. 117/07 (in Croatian)<br />

18. Petrovi I (2008) Deformability <strong>of</strong> mechanically and biologically treated municipal<br />

solid waste, In: Milanovi Z. (ed.) Proceedings <strong>of</strong> Xth International Symposium Waste<br />

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19. Petrovi I (<strong>2010</strong>) Modelling <strong>the</strong> behaviour <strong>of</strong> mechanically and biologically treated<br />

municipal solid waste. PhD Thesis, University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Civil Engineering,<br />

Zagreb, Croatia (in Croatian)<br />

20. Petrovi I, Kovai D (<strong>2010</strong>) Measurement <strong>of</strong> stiffness modulus <strong>of</strong> mechanically and<br />

biologically treated waste, In: Milanovi Z. (ed.) Proceedings <strong>of</strong> XIth International<br />

Symposium Waste Management Zagreb <strong>2010</strong>, Udruga za gospodarenje otpadom,<br />

Zagreb,(in Croatian)<br />

21. Petrovi I, Bauer E (<strong>2011</strong>a) A simple hypoplastic model for simulating <strong>the</strong> mechanical<br />

behaviour <strong>of</strong> MBT waste, In: The Second International Symposium on Computational<br />

Geomechanics (ComGeo II), Cavtat, Croatia, 27-29 April, <strong>2011</strong><br />

22. Petrovi I, Szavits-Nossan V, Štuhec D (<strong>2011</strong>b) Laboratory testing <strong>of</strong> waste after biomechanical<br />

treatment. Graevinar 63(1), pp 43-53 (in Croatian)<br />

23. Petrovi I, Szavits-Nossan V, Kovai D (<strong>2011</strong>c) Deformability <strong>of</strong> mechanically and<br />

biologically treated municipal solid waste, Graevinar 63(3), pp 255-264 (in Croatian)<br />

24. Waste Management Strategy <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia (2005) Ofcial Gazette <strong>of</strong> <strong>the</strong><br />

Republic <strong>of</strong> Croatia, No. 130/05 (in Croatian)<br />

25. Waste Management Plan <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia for <strong>the</strong> period 2007-2015 (2007)<br />

Ofcial Gazette <strong>of</strong> <strong>the</strong> Republic <strong>of</strong> Croatia, No. 85/07 (in Croatian)<br />

26. Ziehmann G (1999) Veraenderung des mechanischen Verhaltens durch die mechanische<br />

und biologische Vorbehandlung, Deponierung von vorbehandelten Siedlungsabfaellen.<br />

Veroeffentlichungen des Zentrums fuer Abfallforschung der Technischen<br />

Universitaet Braunschweig, Heft 14, S. 1 – 9


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 89<br />

BEAM-TO-COLUMN JOINT MODELLING TO EC3<br />

Darko Dujmović<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Civil Engineering; Croatian Academy <strong>of</strong> Engineering,<br />

Zagreb, Croatia<br />

Boris Androić<br />

IA Projektiranje Structural Engineering L.t.d.; Croatian Academy <strong>of</strong> Engineering, Zagreb,<br />

Croatia<br />

Ivan Lukačević<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Civil Engineering, Zagreb, Croatia<br />

ABSTRACT<br />

The modelling <strong>of</strong> beam to column joints is analyzed taking into account real behaviour<br />

<strong>of</strong> such joints as described by <strong>the</strong> Mj- curve. General considerations relating to <strong>the</strong> new<br />

joint design philosophy, as based on Eurocode 3, are given in <strong>the</strong> initial part <strong>of</strong> <strong>the</strong> paper.<br />

The method <strong>of</strong> components, an analytical method for characterization <strong>of</strong> joints, is <strong>the</strong>n described.<br />

Components enabling bolted joint between beams and columns are identied and<br />

analyzed. The use <strong>of</strong> <strong>the</strong> described modelling procedure is shown by means <strong>of</strong> a specially<br />

devised computer program CoP (Connection Program).<br />

Key words: beam to column joint, modelling, component method, bolted joint, application<br />

<strong>of</strong> <strong>the</strong> new approach<br />

1 INTRODUCTION<br />

Laboratory research and <strong>the</strong> progress <strong>of</strong> numeric methods have stimulated <strong>the</strong> development<br />

<strong>of</strong> a more realistic approach to dividing joints for everyday <strong>engineering</strong> practice. The component<br />

method is an efcient way <strong>of</strong> solving complex behaviour <strong>of</strong> steel structure joint.<br />

The component method, as well as <strong>the</strong> mechanical models which describe individual joint<br />

types can be used to dene basic joint characteristics. These are: stiffness, bending resistance<br />

and rotation capacity.<br />

2 BEAM-TO-COLUMN JOINT MODEL<br />

Joint analysis requires <strong>the</strong> following to be taken into consideration:<br />

• material non-linearity (plasticity, strain-hardening),<br />

• non-linear contact and slip,<br />

• geometrical non-linearity (local instability),<br />

• residual stresses,<br />

• complex geometrical congurations.<br />

For practical purposes, <strong>the</strong> joint analysis is conducted on simpler models. This is <strong>the</strong> reason<br />

<strong>the</strong> design procedure known as <strong>the</strong> components method has been adopted in Eurocode 3<br />

(EC3). The method suits <strong>the</strong> simplied mechanical spring and rigid links model very well.<br />

The joint is represented by adequate rigid and exible components. They represent individual<br />

joint parts, Fig. 1.


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Fig. 1. Component model <strong>of</strong> beam-to-column joint<br />

Typical bolted joint components are:<br />

• column web panel in shear,<br />

• end-plate in bending,<br />

• beam ange in bending,<br />

• beam web in tension,<br />

• beam ange and web in compression,<br />

• bolts in tension<br />

• welds.<br />

When using <strong>the</strong> component method, <strong>the</strong> rst characteristics to be considered are those <strong>of</strong><br />

resistance, stiffness and ductility in individual components. These characteristics are combined<br />

to reach an estimate <strong>of</strong> mechanical joint behaviour.<br />

A non-linear force-deformation (F-) curve can be used to show individual joint behaviour,<br />

Fig. 2.<br />

Fig. 2. Force-deformation (F-) curve <strong>of</strong> ductile component: a) actual behaviour and b) bi-linear<br />

approximation<br />

Simpler behaviour idealisations are possible. The simplied components model <strong>of</strong> EN<br />

1993-1-8, for instance, combines <strong>the</strong> joint bending response with <strong>the</strong> column web panel<br />

response to shear. This type <strong>of</strong> equivalent rotational spring has been shown in Fig. 3.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 91<br />

Fig. 3. Equivalent rotational spring model<br />

Fig. 4. Application <strong>of</strong> <strong>the</strong> component method to a welded joint<br />

The application <strong>of</strong> <strong>the</strong> component method requires <strong>the</strong> following steps:<br />

• Identication <strong>of</strong> <strong>the</strong> active components from a global list <strong>of</strong> components (20 different<br />

components currently codied in EN 1993-1-8).<br />

• Evaluation <strong>of</strong> <strong>the</strong> force deformation response (F-) <strong>of</strong> each individual basic component<br />

(initial stiffness, design resistance etc.).<br />

• Assembly <strong>of</strong> <strong>the</strong> active components, using representative mechanical model shown in<br />

Fig. 2, for <strong>the</strong> evaluation <strong>of</strong> <strong>the</strong> mechanical characteristics <strong>of</strong> <strong>the</strong> whole joint (initial stiffness,<br />

design resistance etc. or <strong>the</strong> whole deformability M- curve).<br />

These steps are illustrated in Fig. 4. in simple case <strong>of</strong> a beam-to-column welded joint.


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Understanding <strong>the</strong> mechanical behaviour <strong>of</strong> different joint components allows <strong>the</strong> analysis<br />

<strong>of</strong> a large number <strong>of</strong> different joint congurations. The purpose <strong>of</strong> <strong>the</strong> component method<br />

is to determine <strong>the</strong> F- curve for each individual spring. Only <strong>the</strong> linear stiffness <strong>of</strong> each<br />

component is required to estimate initial joint stiffness. The ductility estimate, however,<br />

requires knowledge <strong>of</strong> <strong>the</strong> non-linear F- response for each component.<br />

The following points encompass only <strong>the</strong> components that are relevant for <strong>the</strong> beam-tocolumn<br />

joint. For <strong>the</strong> joint ductility estimate, <strong>the</strong> joint components are divided into three<br />

groups, analogous with <strong>the</strong> cross-section classication:<br />

• components with high ductility,<br />

• components with limited ductility,<br />

• components with brittle failure.<br />

3 DESIGN RESISTANCE OF COMPONENTS<br />

3.1 Components with high ductility<br />

These components are represented by <strong>the</strong> F- curve which in <strong>the</strong> rst part shows linear<br />

elastic behaviour and in <strong>the</strong> second part allows an increase in deformation with an increase<br />

in force. The component deformation capacity is very large.<br />

• Column web panel in shear<br />

Extensive tests show <strong>the</strong> column web having a resistance reserve in shear. The following<br />

equation gives <strong>the</strong> design shear resistance <strong>of</strong> unstiffened column web panel, V wp,Rd<br />

, for<br />

single-sided framed joints:<br />

(1)<br />

where:<br />

f y,wc<br />

A vc<br />

M0<br />

<strong>the</strong> yield strength <strong>of</strong> <strong>the</strong> column web,<br />

<strong>the</strong> shear area <strong>of</strong> <strong>the</strong> column,<br />

<strong>the</strong> partial factor for resistance <strong>of</strong> cross-sections whatever <strong>the</strong> class is.<br />

In <strong>the</strong> case <strong>of</strong> welded cross-sections, <strong>the</strong> shear column area, Avc, coincides with <strong>the</strong> web<br />

area, whereas in <strong>the</strong> case <strong>of</strong> rolled sections it is given by:<br />

(2)<br />

where:<br />

A c<br />

b c<br />

t fc<br />

t wc<br />

r c<br />

<strong>the</strong> total area <strong>of</strong> <strong>the</strong> column,<br />

<strong>the</strong> ange width,<br />

<strong>the</strong> ange thickness,<br />

<strong>the</strong> web thickness,<br />

<strong>the</strong> root-radius <strong>of</strong> <strong>the</strong> web-ange junction.<br />

Eq. (1) disregards <strong>the</strong> axial force in <strong>the</strong> column. Using <strong>the</strong> Von Mises yield criterion it is<br />

possible to determine <strong>the</strong> reduced resistance value which takes into consideration <strong>the</strong> axial<br />

column force. The 0,9 reduction coefcient partially solves this problem, which has also


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 93<br />

been accepted into EN 1993-1-8. The resistance <strong>of</strong> <strong>the</strong> unstiffened column web in shear for<br />

single-sided joints, V wp,Rd<br />

, is:<br />

(3)<br />

The shear deformation <strong>of</strong> <strong>the</strong> column web, s<br />

, in <strong>the</strong> overall initial rotation <strong>of</strong> joint is given<br />

by:<br />

(4)<br />

where:<br />

V<br />

G<br />

<strong>the</strong> shear force on <strong>the</strong> column web taken as 2F i<br />

(F i<br />

denoting <strong>the</strong> force in each<br />

bolt row and i <strong>the</strong> bolt row),<br />

<strong>the</strong> shear modulus.<br />

Thus <strong>the</strong> corresponding axial stiffness, K wp<br />

, is:<br />

(5)<br />

where:<br />

z<br />

E<br />

<strong>the</strong> lever arm between <strong>the</strong> compressive and <strong>the</strong> tensile areas,<br />

<strong>the</strong> modulus <strong>of</strong> elasticity.<br />

Dividing <strong>the</strong> axial stiffness, K wp<br />

, with <strong>the</strong> modulus <strong>of</strong> elasticity E <strong>the</strong> Eq. (5) is:<br />

(5a)<br />

where:<br />

k wp<br />

<strong>the</strong> stiffness coefcient <strong>of</strong> column web in shear, <strong>the</strong> designation in EN 1993-1-8<br />

is k1.<br />

From Eq. (4) it can be observed that <strong>the</strong> stiffness <strong>of</strong> this component depends on <strong>the</strong> applied<br />

shear force on <strong>the</strong> column web. Given that, in general, internal forces transmitted by<br />

<strong>the</strong> lower and upper column and (for internal nodes with unbalanced moments) left beam<br />

may also be present, <strong>the</strong> applied shear force must also be modied by a transformation<br />

parameter , EN 1993-1-8, to deal with this effect. For different joint congurations and<br />

unbalanced bending moments, <strong>the</strong> stiffness coefcient, k<br />

WP<br />

, Eq. (5a), must be modied by<br />

<strong>the</strong> transformation parameter :


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

(6)<br />

For stiffened column web shear deformation can be disregarded (k wp<br />

= ). It ought to be<br />

noted that in slender webs instability becomes relevant, but has so far not been included<br />

in EC 3.<br />

• End-plate in bending<br />

The deformation <strong>of</strong> this component is evaluated using <strong>the</strong> simple substitute model, T-stub.<br />

It represents <strong>the</strong> tension joint zone behaviour, and is shown in Fig. 5.<br />

Fig. 5. Substitute model, <strong>the</strong> T-stub<br />

Three possible failure modes <strong>of</strong> <strong>the</strong> equivalent T-stub ange are assumed, as shown in Fig.<br />

6.<br />

The following failure modes are possible:<br />

Fig. 6. Failure modes <strong>of</strong> <strong>the</strong> T-stub ange<br />

Mode 1: End-plate yielding without bolt failure


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 95<br />

(7a)<br />

Mode 2: Simultaneous yielding <strong>of</strong> end-plate with bolt failure<br />

(7b)<br />

Mode 3: Bolt failure without end-plate yielding<br />

where:<br />

m <strong>the</strong> distance between <strong>the</strong> bolt centreline and <strong>the</strong> face <strong>of</strong> <strong>the</strong> weld connecting <strong>the</strong><br />

beam web to <strong>the</strong> end-plate, see Fig. 7,<br />

n <strong>the</strong> effective distance to <strong>the</strong> free edge, , but , see Fig. 7,<br />

F t,Rd<br />

<strong>the</strong> design tension resistance <strong>of</strong> a bolt,<br />

<strong>the</strong> total value <strong>of</strong> F t,Rd<br />

for all bolts in <strong>the</strong> T-stub.<br />

F t,Rd<br />

Design bending resistance <strong>of</strong> an end-plate depending on failure mode is:<br />

(7c)<br />

(8a)<br />

(8b)<br />

where:<br />

tf<br />

fy<br />

<strong>the</strong> effective width <strong>of</strong> <strong>the</strong> end-plate in bending,<br />

<strong>the</strong> thickness <strong>of</strong> <strong>the</strong> end-plate,<br />

<strong>the</strong> yield strength <strong>of</strong> <strong>the</strong> end-plate.<br />

Dimensions <strong>of</strong> an equivalent T-stub ange are shown in Fig. 7.<br />

For end-plate bending resistance, <strong>of</strong> <strong>the</strong> possible three failure modes, <strong>the</strong> minimum value<br />

is used.<br />

The T-stub stiffness coefcient analytical equations can be derived from classical beam<br />

<strong>the</strong>ory, when <strong>the</strong> effective width is correctly estimated, so that:<br />

(9)


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

where:<br />

k b,p<br />

<strong>the</strong> stiffness coefcient <strong>of</strong> <strong>the</strong> end-plate in bending, <strong>the</strong> designation in EN 1993-<br />

1-8 is k5,<br />

t p<br />

is <strong>the</strong> thickness <strong>of</strong> a end-plate.<br />

Fig. 7. Dimensions <strong>of</strong> an equivalent T-stub ange<br />

• Column ange in bending<br />

This component behaves similarly to <strong>the</strong> end-plate in bending, so <strong>the</strong> equivalent T-stub<br />

approach can also be utilized. The exception is <strong>the</strong> case when <strong>the</strong> ange is stiffened. The<br />

unstiffened ange is supposed to have <strong>the</strong> same levels <strong>of</strong> ductility and stiffness. The resistance<br />

equations dependent on failure modes are given in <strong>the</strong> following:<br />

Mode 1: Column ange yielding without bolt failure<br />

(10a)<br />

Mode 2: Simultaneous yielding <strong>of</strong> column ange with bolt failure<br />

(10b)<br />

Mode 3: Bolt failure without column ange yielding<br />

(10c)<br />

For column ange bending resistance <strong>the</strong> value which is used is <strong>the</strong> minimum out <strong>of</strong> <strong>the</strong><br />

three failure modes.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 97<br />

The component stiffness coefcient is:<br />

(11)<br />

The symbols have <strong>the</strong> same meaning as in <strong>the</strong> case <strong>of</strong> <strong>the</strong> end-plate, with <strong>the</strong> exception that<br />

<strong>the</strong> column and not <strong>the</strong> end-plate ange characteristics are used. The designation <strong>of</strong> this<br />

stiffness coefcient in EN 1993-1-8 is k4.<br />

• Beam web in tension<br />

For bolted end-plate joints, <strong>the</strong> design tension resistance <strong>of</strong> <strong>the</strong> beam web, Ft,wb,Rd, is:<br />

(12)<br />

where:<br />

b eff,t,wb<br />

t wb<br />

f y,wb<br />

<strong>the</strong> effective width <strong>of</strong> <strong>the</strong> beam web in tension, equal to <strong>the</strong> effective length <strong>of</strong><br />

<strong>the</strong> equivalent T-stub representing <strong>the</strong> end-plate in bending,<br />

<strong>the</strong> thickness <strong>of</strong> beam web,<br />

<strong>the</strong> yield strength <strong>of</strong> <strong>the</strong> beam web.<br />

The initial stiffness for this component can be taken to be innite.<br />

3.2 Components with limited ductility<br />

These components are characterized by an F- curve with limit point after which <strong>the</strong> curve<br />

falls.<br />

• Column web in compression<br />

This component achieves limited ductile behaviour when <strong>the</strong> curve falls after <strong>the</strong> maximum<br />

resistance has been reached. The resistance for this component can be grouped according<br />

to two different types <strong>of</strong> criteria:<br />

- crushing resistance,<br />

- buckling resistance.<br />

The crushing resistance must take into account <strong>the</strong> interaction between:<br />

- <strong>the</strong> local stresses that arise from <strong>the</strong> shear stresses in <strong>the</strong> panel zone,<br />

- <strong>the</strong> vertical normal stresses due to axial load and bending moment in <strong>the</strong> column,<br />

- <strong>the</strong> horizontal normal stresses transmitted by <strong>the</strong> beam anges.<br />

Using <strong>the</strong> von Mises yield criterion, <strong>the</strong> design crushing resistance, Fc,wc,Rd, is:<br />

(13)<br />

The effective width <strong>of</strong> <strong>the</strong> column web in compression, b eff,c,wc<br />

, for bolted end-plate joints<br />

is:


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

(14)<br />

where:<br />

a p<br />

<strong>the</strong> effective thickness <strong>of</strong> <strong>the</strong> weld, Fig. 8,<br />

s = r for rolled column sections,<br />

<strong>the</strong> length obtained by dispersion at 45º through <strong>the</strong> end-plate.<br />

s p<br />

Fig. 8. Transverse compression on an unstiffened column<br />

Reduction factor, k wc<br />

, accounts for <strong>the</strong> inuence <strong>of</strong> vertical normal stress due to axial force<br />

and <strong>the</strong> bending moment, com,Ed<br />

, and is given in <strong>the</strong> following:<br />

(15)<br />

Reduction factor accounts for <strong>the</strong> shear interaction, and equals:


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 99<br />

(16)<br />

with<br />

(17a)<br />

(17b)<br />

where:<br />

is <strong>the</strong> transformation parameter from EN 1993-1-8.<br />

The buckling resistance, F c,wc,Rd<br />

, is taken approximately using <strong>the</strong> Winter equation:<br />

(18)<br />

The reduction factor for plate buckling (column web panel), , is:<br />

or<br />

(19a)<br />

(19b)<br />

The normalised plate slenderness (column web panel),<br />

, is:<br />

(20)<br />

The initial deformation <strong>of</strong> <strong>the</strong> c component is:


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

(21)<br />

where:<br />

N<br />

A c<br />

d c<br />

h c<br />

<strong>the</strong> resultant compressive force, taken as 2Fi (Fi denote <strong>the</strong> force in each bolt<br />

row and i <strong>the</strong> bolt row),<br />

<strong>the</strong> effective web area in compression zone, Ac = twc•beff,c,wc,<br />

<strong>the</strong> depth between column llets,<br />

<strong>the</strong> beam depth minus beam ange thickness.<br />

So that <strong>the</strong> initial (axial) stiffness becomes:<br />

(22)<br />

Dividing <strong>the</strong> axial stiffness, K c,wc<br />

, with <strong>the</strong> modulus <strong>of</strong> elasticity E <strong>the</strong> Eq. (22) is:<br />

(22a)<br />

It must be noted that for <strong>the</strong> calculation <strong>of</strong> <strong>the</strong> stiffness coefcient, kc,wc, a reduction <strong>of</strong> <strong>the</strong><br />

effective width used for <strong>the</strong> resistance calculation is adopted (0,7×b eff,c,wc<br />

). The designation<br />

<strong>of</strong> this stiffness coefcient in EN 1993-1-8 is k 2<br />

.<br />

• Column web in tension<br />

Excluding instability occurrences, <strong>the</strong> resistance <strong>of</strong> this component approaches <strong>the</strong> column<br />

web in compression. The design resistance <strong>of</strong> an unstiffened column web, F t,wc,Rd<br />

, equals:<br />

(23)<br />

where <strong>the</strong> symbols mean <strong>the</strong> same as earlier, with t (tension) replacing c (compression). It<br />

shall be noted that EN 1993-1-8 disregards <strong>the</strong> inuence <strong>of</strong> vertical stresses arising from<br />

<strong>the</strong> column.<br />

Analogous to <strong>the</strong> preceding case, <strong>the</strong> initial deformation <strong>of</strong> this component w<br />

is:<br />

(24)<br />

where:<br />

T <strong>the</strong> resultant tensile force, taken as 2Fi (Fi denoting <strong>the</strong> force in each bolt row<br />

and i <strong>the</strong> bolt row),<br />

A t<br />

<strong>the</strong> effective web area in <strong>the</strong> tensile zone, A t<br />

= t wc<br />

×b eff,t,wc<br />

,


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 101<br />

d c<br />

h t<br />

<strong>the</strong> depth between column llets,<br />

<strong>the</strong> distance from <strong>the</strong> tensile force to <strong>the</strong> centre <strong>of</strong> compression.<br />

Initial (axial) stiffness equals:<br />

(25)<br />

Dividing <strong>the</strong> axial stiffness, K t,wc<br />

, with <strong>the</strong> modulus <strong>of</strong> elasticity E <strong>the</strong> Eq. (25) is:<br />

(25a)<br />

This means that Eq. (25a) provides <strong>the</strong> stiffness coefcient, k t,wc<br />

, <strong>of</strong> <strong>the</strong> column web in tension.<br />

The designation <strong>of</strong> this stiffness coefcient in EN 1993-1-8 is k3.<br />

• Beam ange and beam web in compression<br />

This component, <strong>the</strong> beam ange and web in compression adjacent to <strong>the</strong> connection <strong>of</strong><br />

beam, provides a limitation to <strong>the</strong> resistance <strong>of</strong> <strong>the</strong> joint. It is <strong>the</strong>refore necessary to determine<br />

maximum component resistance, using:<br />

(26)<br />

Its initial stiffness is taken as innity.<br />

3.3 Components with brittle failure<br />

These components behave linearly until collapse. Before failure <strong>the</strong>y show very small deformation.<br />

• Bolts in tension<br />

The bolts show a linear force-deformation (F-) response up to failure. The resistance and<br />

initial stiffness <strong>of</strong> each bolt are:<br />

(27)<br />

(28)<br />

where:<br />

A s<br />

f ub<br />

L b<br />

<strong>the</strong> tensile area <strong>of</strong> <strong>the</strong> bolt,<br />

<strong>the</strong> ultimate tensile strength <strong>of</strong> bolts,<br />

<strong>the</strong> sum <strong>of</strong> <strong>the</strong> thickness <strong>of</strong> <strong>the</strong> connected plates (<strong>the</strong> column ange and <strong>the</strong> endplate),<br />

<strong>the</strong> thickness <strong>of</strong> <strong>the</strong> washers and <strong>the</strong> half thickness <strong>of</strong> <strong>the</strong> nut and <strong>the</strong> bolt<br />

head.


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• Welds<br />

Welds are virtually undeformable (Kw = ). A rigid-plastic model is adopted as adequate,<br />

and <strong>the</strong> design resistance is:<br />

(29)<br />

where:<br />

a<br />

f u<br />

w<br />

<strong>the</strong> effective thickness <strong>of</strong> <strong>the</strong> weld,<br />

<strong>the</strong> ultimate tensile strength <strong>of</strong> <strong>the</strong> weld,<br />

<strong>the</strong> correlation factor.<br />

4 ASSEMBLY OF THE COMPONENTS<br />

Components assembly is <strong>the</strong> third and <strong>the</strong> last step <strong>of</strong> <strong>the</strong> components method. It consists<br />

<strong>of</strong> assembling components in such a way that <strong>the</strong> mechanical characteristics <strong>of</strong> <strong>the</strong> entire<br />

joint can be reached. The relationship between <strong>the</strong> components characteristics and <strong>the</strong> joint<br />

components is based on “<strong>the</strong> distribution <strong>of</strong> internal forces in <strong>the</strong> joint”. The manner in<br />

which <strong>the</strong> external forces bearing on <strong>the</strong> joint are distributed to joint components is determined<br />

for <strong>the</strong> given set (analogy with structural member cross-section).<br />

Fig. 9 shows <strong>the</strong> example <strong>of</strong> a spring model for bolted joint with end-plate. Each component<br />

possesses stiffness coefcient, k i<br />

. The springs are connected serially and/or parallely,<br />

and <strong>the</strong> initial rotational stiffness, S j,ini<br />

, is:<br />

(30)<br />

The bending resistance <strong>of</strong> <strong>the</strong> joint, M j,Rd<br />

, equals:<br />

(31)<br />

where:<br />

F tr,Rd<br />

<strong>the</strong> effective design tension resistance <strong>of</strong> bolt-row r,<br />

h r<br />

<strong>the</strong> distance from bolt-row r to <strong>the</strong> centre <strong>of</strong> compression,<br />

r <strong>the</strong> bolt-row number.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 103<br />

Fig. 9. Components represented by springs on bolted beam to column joint<br />

5 PRACTICAL APPLICATION OF THE COMPONENTS METHOD<br />

The example shows <strong>the</strong> new approach to steel beam-to-column joint design adopted in<br />

EC3, in practical application. The beam to column joint in Fig. 10 is a real industrial portal<br />

frame joint with an inclined beam ( = 5°), <strong>the</strong> length <strong>of</strong> L = 19,5 m, and h = 6,32 high (in<br />

<strong>the</strong> ridge H = 7,20 m). A haunch 1,5 m long supports <strong>the</strong> beam. The design <strong>of</strong> this kind <strong>of</strong><br />

joint is based on <strong>the</strong> traditional approach and was intuitively held to be rigid.<br />

The second step is <strong>the</strong> design <strong>of</strong> mechanical joint characteristics (joint No. 1) conducted<br />

based on <strong>the</strong> EC3, Part 1.8, and <strong>the</strong> values are:<br />

• Initial rotational stiffness S j,ini = 260 863 kNm/rad,<br />

• Bending resistance M j,Rd = 554 kNm.<br />

In order to agree with <strong>the</strong> designer’s expectations, every value has to be higher than:<br />

• <strong>the</strong> inexibility limit, based on <strong>the</strong> rotational stiffness 129 769 kNm/rad,<br />

• <strong>the</strong> maximum bending moment, transferred to <strong>the</strong> joint in global frames analysis, equals<br />

M j,Ed<br />

= 416 kNm.<br />

Since both conditions were fullled, <strong>the</strong> joint design can be considered satisfactory.


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Fig. 10. Detail <strong>of</strong> <strong>the</strong> joint<br />

The joint stiffness pro<strong>of</strong> based on <strong>the</strong> EN 1993-1-8 has not been conducted, and <strong>the</strong> joint<br />

was simply taken as inexible based on <strong>the</strong> designer’s experience.<br />

According to <strong>the</strong> EC3 additional efforts are needed to check whe<strong>the</strong>r <strong>the</strong> rigid joint could<br />

be considered unnecessary.<br />

Before any fur<strong>the</strong>r discussion, <strong>the</strong> following needs to be established:<br />

• A lack <strong>of</strong> knowledge necessary to design joints, when <strong>the</strong> designer’s joint geometry is<br />

dened, leads to a systematic application <strong>of</strong> transversal stiffeners <strong>of</strong> <strong>the</strong> column (in both<br />

<strong>the</strong> tension and compression joint zones), toge<strong>the</strong>r with thick end-plates,<br />

• As a result <strong>of</strong> excessive stiffening <strong>the</strong> internal force distribution is <strong>of</strong> a linear kind, which<br />

explains why <strong>the</strong> elastic design approach has traditionally been used for determining bolt<br />

forces,<br />

In such design procedures, <strong>the</strong> bolts are weak joint components and <strong>the</strong> plate approach to<br />

design can be considered valid, but it <strong>of</strong>ten results in an excessive dimensioning <strong>of</strong> joints<br />

and uneconomical joint framings, since <strong>the</strong> execution depends on <strong>the</strong> stiffness level to such<br />

an extent. Stiffness even prevents easy assembly at site. Finally, <strong>the</strong> lack <strong>of</strong> ductility related<br />

to bolt failure is far from satisfactory, when joint ductility is taken into consideration.<br />

Part 1.8 <strong>of</strong> <strong>the</strong> EC 3 suggests as an alternative a set <strong>of</strong> rules for design, where <strong>the</strong> type <strong>of</strong><br />

failure has not been chosen in advance. The stiffness and resistance characteristics for all<br />

participating components have been taken into account in <strong>the</strong> design. In o<strong>the</strong>r words, real<br />

joint characteristics are calculated, and <strong>the</strong> designer is left with <strong>the</strong> decisions to change <strong>the</strong><br />

joint geometry as needed, choosing a ductile type <strong>of</strong> failure, thus making <strong>the</strong> joint more<br />

resistant, stiffer and more ductile.<br />

In <strong>the</strong> case at hand, <strong>the</strong> joint characteristics exceed requirements (<strong>the</strong> resistance is higher<br />

than required, and <strong>the</strong> rotational stiffness <strong>of</strong> 129 769 kNm/rad is enough to secure rigidity<br />

in <strong>the</strong> joint, as was supposed in <strong>the</strong> frame analysis). Simplifying joint geometry thus<br />

decreases <strong>the</strong> joint execution costs, and those <strong>of</strong> <strong>the</strong> entire structure based on that. A more<br />

signicant fact here is that in this way we design joints that will achieve <strong>the</strong> required levels<br />

<strong>of</strong> reliability. Intuitive stiffness forecasts, though made to create a more reliable joint, may<br />

have an effect that is just <strong>the</strong> opposite.<br />

The following table shows different structural joint congurations. They are under consideration<br />

with <strong>the</strong> goal <strong>of</strong> simplifying joint geometry, taking into account <strong>the</strong> frame analysis<br />

requirements.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 105<br />

• Joint No. 1: 6 bolt rows, leng<strong>the</strong>ned end-plate, 6 stiffeners <strong>of</strong> column web (three pairs).<br />

• Joint No. 2: 5 bolt rows, 6 stiffeners <strong>of</strong> column web.<br />

• Joint No. 3: 5 bolt rows, 4 stiffeners <strong>of</strong> column web (compression and tension zone).<br />

• Joint No. 4: 5 bolt rows, 2 stiffeners <strong>of</strong> column web (compression zone).<br />

• Joint No. 5: 5 bolt rows, no stiffeners <strong>of</strong> column web.<br />

• Joint No. 6: 4 bolt rows, 2 stiffeners <strong>of</strong> column web (compression zone).<br />

• Joint No. 7: 3 bolt rows, 2 stiffeners <strong>of</strong> column web (compression zone).<br />

• Joint No. 1, which <strong>the</strong> designer has suggested, fulls <strong>the</strong> frame structure analysis requirements,<br />

where <strong>the</strong> stiffness is such that <strong>the</strong> joint can be considered rigid, and <strong>the</strong> bending<br />

resistance is greater than <strong>the</strong> bending moment, which was reached through global frame<br />

analysis.<br />

• Since <strong>the</strong> joint resistance is signicantly greater than required, it is concluded that <strong>the</strong><br />

extended end-plate is unnecessary, and <strong>the</strong> upper bolt row is eliminated, joint No. 2. This<br />

decreases joint stiffness, but within rigidity limits.<br />

• The third step (joint No. 3) is to reduce <strong>the</strong> number <strong>of</strong> stiffeners, by nei<strong>the</strong>r eliminating <strong>the</strong><br />

middle stiffener, which does not decrease joint stiffness nor bending resistance. The middle<br />

stiffener is thus ineffective.<br />

• Next, <strong>the</strong> stiffener is eliminated from <strong>the</strong> tension zone (joint No. 4), and joint bending<br />

resistance and stiffness are reduced, although still completing <strong>the</strong> requirements <strong>of</strong> global<br />

analysis.<br />

• Following that, <strong>the</strong> stiffener would also be eliminated from <strong>the</strong> compression zone. That<br />

sort <strong>of</strong> joint, however (joint No. 5), does not satisfy requirements, since <strong>the</strong> resistance is<br />

lower than <strong>the</strong> action effect.<br />

• Because <strong>the</strong> relevant mode <strong>of</strong> failure is <strong>the</strong> column web in compression, now a step is<br />

taken back to joint No. 4 with stiffeners in <strong>the</strong> compression zone, with <strong>the</strong> elimination <strong>of</strong> 1<br />

row <strong>of</strong> bolts. That kind <strong>of</strong> joint (joint No. 6) is entirely satisfactory.<br />

• The number <strong>of</strong> bolts is <strong>the</strong>n reduced to 3, and joint no. 7 is no longer satisfactory as far as<br />

bending resistance is concerned (<strong>the</strong> spacing between <strong>the</strong> rst and <strong>the</strong> second row <strong>of</strong> bolts<br />

have been increased from 90 to 120 mm).


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Table 1. Joint congurations with corresponding resistance and stiffness values, as<br />

well as frame analysis requirement fullment<br />

Joint No. 6 represents <strong>the</strong> solution. Bending resistance is reduced to an acceptable level,<br />

and as far as stiffness goes, <strong>the</strong> joint still belongs to <strong>the</strong> rigid joint.<br />

For each <strong>of</strong> <strong>the</strong>se structural solutions, Table 1 gives <strong>the</strong> resistance and stiffness values, as<br />

well as whe<strong>the</strong>r <strong>the</strong> frame analysis requirements have been fullled.<br />

This analysis shows very clearly that even for rigid joints, <strong>the</strong> new approach to joint design<br />

based on EC 3 can have serious benets. This is <strong>the</strong> result <strong>of</strong> <strong>the</strong> clearer denition <strong>of</strong> <strong>the</strong><br />

inexibility notion, and <strong>the</strong> usage <strong>of</strong> advanced design models for joint stiffness and resistance<br />

determination.<br />

6 CONCLUSION<br />

An entirely different approach that consists in a realistic representation <strong>of</strong> joints in structure<br />

modelling is shown. Joints in a broader sense connect all types <strong>of</strong> non-monolithic<br />

structural elements and are <strong>the</strong>refore <strong>the</strong> most important within structural elements and


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 107<br />

within <strong>the</strong> entire structure. In spite <strong>of</strong> that and owing to <strong>the</strong> lack <strong>of</strong> knowledge about <strong>the</strong>ir<br />

actual characteristics and <strong>the</strong> way <strong>of</strong> modelling, joints have been so far neglected and very<br />

simplied assumptions related to forming <strong>of</strong> models have been adopted. This has resulted<br />

in expensive structural solutions that <strong>of</strong>ten have very low reliability.<br />

This new approach can be successfully applied in every-day <strong>engineering</strong> practice and fur<strong>the</strong>r<br />

savings can be made due to <strong>the</strong> decrease in <strong>the</strong> self weight <strong>of</strong> structures or reduced<br />

costs <strong>of</strong> execution and assembly. The shown example represents <strong>the</strong> practical application<br />

<strong>of</strong> <strong>the</strong> new approach according to EC 3.<br />

Fur<strong>the</strong>r research <strong>of</strong> joint behaviour should be conducted by use <strong>of</strong> methods <strong>of</strong> structural<br />

reliability <strong>the</strong>ory. With <strong>the</strong> collection <strong>of</strong> statistical data on joint components that would be<br />

obtained in laboratory, <strong>the</strong>ir stochastic models could be established. By solving <strong>the</strong> limit<br />

state equations <strong>the</strong> comparison <strong>of</strong> <strong>the</strong> reliability level <strong>of</strong> different types <strong>of</strong> joints would be<br />

make possible. This way optimal solutions can be chosen in line with general reliability<br />

requirements according to EN 1990: 2001, Eurocode: Basis <strong>of</strong> structural design.<br />

REFERENCES<br />

1. Zoetemeijer, P. (1974) A design method for <strong>the</strong> tension side <strong>of</strong> statically-loaded bolted<br />

beam-to-column joints, Heron, pp 1-59<br />

2. Yee, Y.L.; Melchers, R.E. (1986) Moment-rotation curves for bolted connections,<br />

Journal <strong>of</strong> Structural Engineering 112 3, pp 615-635<br />

3. Janss, J.; Jaspart, J.P. (1987) Strength and behaviour <strong>of</strong> in plane weak axis joints and<br />

<strong>of</strong> 3-D joints, In: Bjorhovde, R.; Colson, A.; Zandonini, R. (Editors): Connections in<br />

steel structures, Proceedings <strong>of</strong> <strong>the</strong> International Workshop on Joints, Elsevier Applied<br />

Science, New York<br />

4. Zoetemeijer, P. (1990) Summary <strong>of</strong> <strong>the</strong> research on bolted beam-to-column connections,<br />

Report 25-6-90-2. Faculty <strong>of</strong> Civil Engineering, Stevin Laboratory - Steel Structures,<br />

Delft University <strong>of</strong> Technology, Delft<br />

5. European Convention for Constructional Steelwork (1992) Analysis Design <strong>of</strong> Steel<br />

Frames with Semi-rigid Joints, Publication 67, Brussels: ECCS<br />

6. Weinand, K. (1992) SERICON – Databank on Joints in Building Frames, Proceedings<br />

<strong>of</strong> <strong>the</strong> 1st COST C1 Workshop, Strasbourg, pp 28-30<br />

7. Shi, Y.J.; Chan, S.L.; Wong, Y.L. (1996) Modelling for moment rotations characteristic<br />

for end-plate joints, Journal <strong>of</strong> Structural Engineering 122 11, pp 1300-1306<br />

8. Bursi, O. S.; Jaspart, J. P. (1997) Benchmarks for Finite Element Modelling <strong>of</strong> Bolted<br />

Steel Connections; Journal <strong>of</strong> Constructional Steel Research, Vol. 43, No. 1-3, pp 17-<br />

42<br />

9. Cruz, P. J.S; da Silva, L. S.; Rodrigues, D. S; Simões, R. A. D. (1998) Database for <strong>the</strong><br />

semi-rigid behaviour <strong>of</strong> beam-to-column connections in seismic regions, Journal <strong>of</strong><br />

Constructional Steel Research 46 1-3, pp 233-234<br />

10. Huber, G.; Tschemmernegg, F. (1998) Modelling <strong>of</strong> steel connections, Journal <strong>of</strong> Constructional<br />

Steel Research 45 2, pp 199-216<br />

11. Kuhlmann, U.; Davison, J.B.; Kattner, M. (1998) Structural systems and rotation capacity,<br />

Proceeding <strong>of</strong> COST Conference on Control <strong>of</strong> <strong>the</strong> Semi-rigid Behaviour <strong>of</strong><br />

Civil Engineering Structural Connections, Liège, pp 167-176<br />

12. Weynand, K.; Jaspart, J.-P.; Steenhuis, M. (1998) Economy Studies <strong>of</strong> Steel Building<br />

Frames with Semi-Rigid Joints, Journal <strong>of</strong> Constructional Steel Research 46 1-3<br />

13. Kuhlmann U. (1999) Inuence <strong>of</strong> axial forces on <strong>the</strong> component: web under compression,<br />

Proceeding <strong>of</strong> COST-C1 Working Group Meeting, C1/WG2/99-01, Thessaloniki<br />

14. Faella, C.; Piluso, V.; Rizzano, G. (2000) Structural Steel Semirigid Connections, The-


108<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

ory, Design and S<strong>of</strong>tware, CRC Press LLC, 2000 N.W. Corporate Blvd., Boca Raton,<br />

Florida 33431<br />

15. CoP S<strong>of</strong>tware, (2002) Version 2002R03, RWTH Aachen, MSM Liège, ICCS Ho<strong>of</strong>ddorp<br />

16. da Silva, L. S.; Lima, L.; Vellasco, S.; Andrade, S. (2002) Experimental behaviour <strong>of</strong><br />

end-plate beam-to-column joints under bending and axial force, Database reporting<br />

and discussion <strong>of</strong> results. Report on ECCS-TC10, Meeting in Ljubljana<br />

17. European Committee for Standardization (CEN) (2002) “EN 1990: 2002, Eurocode 0:<br />

Basis <strong>of</strong> structural design“, Final draft, Brussels<br />

18. Dujmovi, D.; Androi, B.; Skeji, D. (2003) Modeliranje prikljuaka elinih okvirnih<br />

konstrukcija, Graevinar 55 6, pp 339-348<br />

19. Dujmovi, D.; Skeji, D.; Androi, B. (2003) Modeliranje prikljuka nosa-stup prema<br />

Eurokodu 3, Graevinar 55 7, pp 397-405<br />

20. Girão Coelho, A.M. (2004) Characterization <strong>of</strong> <strong>the</strong> ductility <strong>of</strong> bolted end plate beamto-column<br />

steel connections, PhD Thesis. University <strong>of</strong> Coimbra, Coimbra, Portugal<br />

21. Girão Coelho, A. M.; Bijlaard, F. S. K.; da Silva, L. S. (2004) Experimental assessment<br />

<strong>of</strong> <strong>the</strong> ductility <strong>of</strong> extended end plate connections, Engineering Structures 26, pp<br />

1185-1206<br />

22. European Committee for Standardization (CEN) (2005) EN 1993-1-8:2005, Eurocode<br />

3: Design <strong>of</strong> steel structures, Part 1.8: Design <strong>of</strong> joints, May 2005, Brussels<br />

23. Skeji, D.; Dujmovi, D.; Androi, B. (2008) Reliability <strong>of</strong> <strong>the</strong> bending resistance<br />

<strong>of</strong> welded beam-to-column joints, Journal <strong>of</strong> Constructional Steel Research, Vol.64,<br />

No.4, pp 388-399


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 109<br />

MODELLING OF JOINT BEHAVIOUR IN STEEL FRAMES<br />

Darko Dujmovic<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Civil Engineering;<br />

Croatian Academy <strong>of</strong> Engineering<br />

Zagreb, Croatia.<br />

Boris Androic<br />

IA Projektiranje Structural Engineering L.t.d.,<br />

Croatian Academy <strong>of</strong> Engineering,<br />

Zagreb, Croatia<br />

Josip Piskovic<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Civil Engineering,<br />

Department for Structural Engineering,<br />

Zagreb, Croatia.<br />

ABSTRACT<br />

The interaction between steel frames and <strong>the</strong>ir joints is explained, and <strong>the</strong> joint dimensioning<br />

method according to EC 3 is presented. Four basic terms related to novel approach to<br />

joint dimensioning are described. These terms are: characterization, classication, modelling<br />

and idealisation. An emphasis is placed on <strong>the</strong> advantages <strong>of</strong> component method,<br />

adopted in EC 3, when compared to <strong>the</strong> procedure currently used for joint modelling. Economic<br />

bases for <strong>the</strong> use <strong>of</strong> <strong>the</strong> new joint dimensioning method are also explained.<br />

KEY WORDS: Joints, frame structures, component method, characterization, execution<br />

costs<br />

1 INTRODUCTION<br />

Traditionally <strong>the</strong> beam-column joints have been considered as pinned without any resistance<br />

and stiffness (simple joints) or as completely rigid with full resistance (continuous<br />

joints). This approach is especially convenient for frame structures that are classied as<br />

braced and non-sway, where most beam-column joints do not demand for a moment transfer<br />

(pinned joints). Joints that must transfer moments are usually a constituent part <strong>of</strong> a<br />

bracing system. Therefore, <strong>the</strong>y must be completely rigid. In reality, both <strong>of</strong> <strong>the</strong>se assumptions<br />

for simple and continuous joints can be incorrect and uneconomical, and <strong>the</strong>y present<br />

only <strong>the</strong> limit cases <strong>of</strong> realistic behaviour <strong>of</strong> joints described by <strong>the</strong> relationship <strong>of</strong> <strong>the</strong><br />

bending moment M and <strong>the</strong> rotation angle .<br />

Because <strong>of</strong> insufcient knowledge about <strong>the</strong> behaviour <strong>of</strong> joints in <strong>the</strong> region between limit<br />

cases, procedures have been adopted within <strong>the</strong> traditional approach to designing which<br />

completely neglected this range, and in many cases <strong>the</strong>y provide uneconomical solutions<br />

or solutions that are not so reliable.<br />

The basic problem was <strong>the</strong> fact that had not been taken into consideration and that is that<br />

<strong>the</strong> structural properties <strong>of</strong> joints must be harmonised with structural properties <strong>of</strong> elements<br />

that are being considered. That means that this insufciency was a particular problem in<br />

terms <strong>of</strong> global structural analysis. By introducing a new <strong>engineering</strong> discipline called<br />

structural modelling, <strong>the</strong> insufciencies <strong>of</strong> <strong>the</strong> traditional approach had began to be consid-


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ered. Numerous laboratory researches and <strong>the</strong> development <strong>of</strong> numerical methods encouraged<br />

a faster development <strong>of</strong> <strong>the</strong> idea regarding a more realistic division <strong>of</strong> joints for <strong>the</strong><br />

needs <strong>of</strong> every-day <strong>engineering</strong> practice.<br />

European standards for structures prescribed a system <strong>of</strong> joint division that classies joints<br />

regarding stiffness (nominally pinned, semi-rigid and rigid), and resistance (nominally<br />

pinned, partial-strength and full-strength). Also, joints can be classied regarding ductility,<br />

although <strong>the</strong> criteria for this classication have not clearly been prescribed within Eurocode<br />

3 yet.<br />

2 STRUCTURAL BEHAVIOUR OF JOINTS<br />

A connection is dened as a set <strong>of</strong> physical components that mechanically fastens <strong>the</strong><br />

elements that it connects. It is considered that <strong>the</strong> connection is concentrated at <strong>the</strong> place<br />

where fastening is realized, for example, where <strong>the</strong> end <strong>of</strong> <strong>the</strong> beam and <strong>the</strong> column for <strong>the</strong><br />

beam-column joint around <strong>the</strong> stronger axis meet. When <strong>the</strong> connection and <strong>the</strong> appropriate<br />

zone <strong>of</strong> interaction between <strong>the</strong> connected structural elements are considered toge<strong>the</strong>r,<br />

<strong>the</strong> expression joint is used, Figure 1. Depending on <strong>the</strong> number <strong>of</strong> elements in <strong>the</strong> plane<br />

that are connected, single-sided, Figure 1.a), and double-sided joints congurations, Figure<br />

1.b), are dened.<br />

It is a well-known fact that rotational behaviour <strong>of</strong> actual joints ranges between two limits:<br />

xed and pinned. Figure 2. illustrates such behaviour in an elastic area <strong>of</strong> a single-sided<br />

joint <strong>of</strong> a column and a beam.<br />

Fig. 1. Joints and connections<br />

Fig. 2. Classication <strong>of</strong> joints according to rotational stiffness<br />

Figure 2.a) presents a rigid joint. It is assumed that all elements <strong>of</strong> <strong>the</strong> joint are stiff enough.<br />

There is no difference between rotations at <strong>the</strong> ends <strong>of</strong> <strong>the</strong> structural elements connected


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 111<br />

in <strong>the</strong> joint. The joint rotation is a node rotation usually used in frame structure analysis<br />

methods. A joint that does not have stiffness, Figure 2.b), is nominally pinned. A connected<br />

beam behaves like a simple supported beam. For cases in between, <strong>the</strong> stiffness <strong>of</strong> a joint<br />

is nei<strong>the</strong>r zero nor innite. The moment that <strong>the</strong> joint transfers will have as a consequence<br />

<strong>the</strong> difference <strong>of</strong> between absolute rotations <strong>of</strong> two connected structural elements, Figure<br />

2.c). In this case this concerns a semi-rigid joint.<br />

The simplest way <strong>of</strong> introducing <strong>the</strong>se notions within global analysis is by means <strong>of</strong> a rotational<br />

spring placed between <strong>the</strong> ends <strong>of</strong> <strong>the</strong> structural elements that are being connected.<br />

Rotational stiffness <strong>of</strong> spring S is <strong>the</strong> parameter which links <strong>the</strong> carried-over moment M j<br />

with <strong>the</strong> appropriate rotation , which in turn is <strong>the</strong> difference between absolute rotations<br />

<strong>of</strong> two connected structural elements. Rotational stiffness is dened as <strong>the</strong> slope <strong>of</strong> curve<br />

M j<br />

- which depends on <strong>the</strong> properties <strong>of</strong> <strong>the</strong> joint.<br />

When this rotational stiffness equals zero, or when it is relatively low, <strong>the</strong> joint is in <strong>the</strong><br />

class nominally pinned. On <strong>the</strong> o<strong>the</strong>r hand, when rotational stiffness S is innite, or relatively<br />

large, <strong>the</strong> joint is in <strong>the</strong> class <strong>of</strong> a rigid joint. In all o<strong>the</strong>r in-between cases, <strong>the</strong> joint<br />

belongs to <strong>the</strong> class <strong>of</strong> semi-rigid joints.<br />

Fig. 3. Modelling <strong>of</strong> joints for <strong>the</strong> case <strong>of</strong> an elastic global analysis<br />

For semi-rigid joints, loads will cause <strong>the</strong> bending moment M j<br />

as well as <strong>the</strong> appropriate<br />

rotation between <strong>the</strong> connected structural elements. The moment and <strong>the</strong> appropriate<br />

rotation are linked by a relationship whic depends on <strong>the</strong> structural properties <strong>of</strong> <strong>the</strong> joint.<br />

This relationship is illustrated in Figure 3, where, for <strong>the</strong> purpose <strong>of</strong> simplication, it is<br />

presumed that <strong>the</strong> global analysis was performed with linear elastic assumptions.<br />

Within <strong>the</strong> global analysis, <strong>the</strong> effect that semi-rigid joints have in relation to <strong>the</strong> effect<br />

<strong>of</strong> rigid joints or nominally pinned ones, is not only <strong>the</strong> modication <strong>of</strong> displacement but<br />

also <strong>the</strong> distribution and size <strong>of</strong> internal forces and bending moments in <strong>the</strong> structure. The<br />

concept <strong>of</strong> semi-rigid joints has been introduced into Eurocode 3 for <strong>the</strong> design <strong>of</strong> steel<br />

structures regarding static loads.<br />

3 JOINT REPRESENTATION<br />

3.1 Introduction<br />

Research regarding joints was focused mostly on <strong>the</strong> following aspects:


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• evaluation <strong>of</strong> mechanical properties <strong>of</strong> joints by means <strong>of</strong> rotational stiffness, moment<br />

resistance and rotational capacity,<br />

• procedures <strong>of</strong> analysis and dimensioning <strong>of</strong> frames including <strong>the</strong> behaviour <strong>of</strong> joints.<br />

From this approach it had been understood that <strong>the</strong>re is a step in between <strong>the</strong>se ones that is<br />

to be taken into consideration, with <strong>the</strong> goal <strong>of</strong> consistent integration <strong>of</strong> <strong>the</strong> actual response<br />

<strong>of</strong> <strong>the</strong> joint within <strong>the</strong> frame analysis, and it is called <strong>the</strong> joint representation.<br />

The joint representation includes four steps as follows:<br />

• joint characterisation: determination <strong>of</strong> stiffness, resistance and ductility <strong>of</strong> <strong>the</strong> joint with<br />

<strong>the</strong> help <strong>of</strong> <strong>the</strong> Mj - curve that describes its behaviour,<br />

• classication <strong>of</strong> joints: provides boundary conditions for <strong>the</strong> application <strong>of</strong> traditional<br />

joint modelling types, i.e. pinned or rigid,<br />

• joint idealisation: derivation <strong>of</strong> a simplied Mj - curve so that it is adjusted to <strong>the</strong> specic<br />

procedures <strong>of</strong> frame global analysis, e.g. <strong>the</strong> linear idealisation for <strong>the</strong> elastic analysis,<br />

• joint modelling: <strong>the</strong> manner in which <strong>the</strong> joint is physically presented in lieu <strong>of</strong> <strong>the</strong> frame<br />

analysis.<br />

3.2 Joint characterisation<br />

A more exact yet also more expensive way to characterisation <strong>of</strong> deformability and resistance<br />

<strong>of</strong> joints is laboratory research. This way is basically limited to research activities<br />

and is not recommended for every day practice. On <strong>the</strong> o<strong>the</strong>r hand, numerous ma<strong>the</strong>matical<br />

models have been developed that can be placed into four major sets as follows:<br />

• curve tting,<br />

• simplied analytical models,<br />

• mechanical models,<br />

• analysis by means <strong>of</strong> nite elements.<br />

The procedure for <strong>the</strong> characterisation <strong>of</strong> mechanical properties <strong>of</strong> joints adopted by Eurocode<br />

3, Part 1.8, is based on <strong>the</strong> component method. The identication <strong>of</strong> various components<br />

that constitute <strong>the</strong> joint (bolts, welds, stiffeners) provides a good picture <strong>of</strong> <strong>the</strong><br />

complexity <strong>of</strong> <strong>the</strong> joint analysis. The analysis <strong>of</strong> a joint requires exact consideration <strong>of</strong><br />

many occurrences: non-linearity <strong>of</strong> materials (plasticity, strain-hardening), non-linear contact<br />

and slip, geometrical non-linearity (local instability), residual stresses and complex<br />

geometrical congurations. Although numerical procedures that apply non-linear nite elements<br />

can take into consideration all <strong>the</strong>se complexities, <strong>the</strong>y require long-lasting procedures<br />

and are very sensitive to <strong>the</strong> possibility <strong>of</strong> modelling and analysis.<br />

Therefore, for practical reasons, <strong>the</strong> planned approach must be based on simple models that<br />

leave out many variables. The component method precisely ts <strong>the</strong> simplied mechanical<br />

model consisting <strong>of</strong> springs and rigid links. In this <strong>the</strong> joint is simulated by means <strong>of</strong> <strong>the</strong> appropriate<br />

selection <strong>of</strong> rigid and exible components. These components represent specic<br />

parts <strong>of</strong> <strong>the</strong> joint that, depending on <strong>the</strong> type <strong>of</strong> loading, make an identied contribution to<br />

one or more <strong>of</strong> its structural properties.<br />

Basic components that are included in Eurocode 3 are as follows:<br />

1. Column web panel in shear<br />

2. Column web in transverse compression<br />

3. Column web in transverse tension<br />

4. Column ange in bending<br />

5. End-plate in bending<br />

6. Flange cleat in bending<br />

7. Beam or column ange and web in compression


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8. Beam web in tension<br />

9. Plate in tension or compression<br />

10. Bolts in tension<br />

11. Bolts in shear<br />

12. Bolts in bearing (on beam ange, column ange, end-plate or cleat)<br />

13. Concrete in compression including grout<br />

14. Base plate in bending under compression<br />

15. Base plate in bending under tension<br />

16. Anchor bolts in tension<br />

17. Anchor bolts in shear<br />

18. Anchor bolts in bearing<br />

19. Welds<br />

20. Haunched beam.<br />

When using <strong>the</strong> component method, <strong>the</strong> characteristics <strong>of</strong> resistance, stiffness and ductility<br />

<strong>of</strong> basic components are evaluated rst. These characteristics are <strong>the</strong>n combined with <strong>the</strong><br />

goal <strong>of</strong> achieving <strong>the</strong> mechanical characteristics <strong>of</strong> <strong>the</strong> entire joint. As a result, <strong>the</strong> application<br />

<strong>of</strong> <strong>the</strong> component method is according to that fairly wide, since it can be applied to<br />

all steel joints for which <strong>the</strong> characteristics <strong>of</strong> constituent components can be identied. In<br />

general, each <strong>of</strong> <strong>the</strong>se components is characterized by a non-linear relationship between<br />

<strong>the</strong> force and deformation (F-), although more simple idealisations are also possible.<br />

Several models made <strong>of</strong> spring and rigid links are proposed, which consist <strong>of</strong> <strong>the</strong> same<br />

basic components.<br />

The application <strong>of</strong> <strong>the</strong> component method on steel joints requires <strong>the</strong> following steps:<br />

1. Selection <strong>of</strong> <strong>the</strong> relevant (active) components from <strong>the</strong> general list <strong>of</strong> components (20<br />

different components have thus been fur<strong>the</strong>r dened in Part 1.8, EC 3).<br />

2. Evaluation <strong>of</strong> <strong>the</strong> force-deformation response <strong>of</strong> each component.<br />

3. “Assembly” <strong>of</strong> <strong>the</strong> active components for <strong>the</strong> evaluation <strong>of</strong> <strong>the</strong> moment-rotation (Mj -)<br />

joint response, by means <strong>of</strong> a representative mechanical model.<br />

Its application can suit various levels <strong>of</strong> element “processing”, e.g. a simplied characterisation<br />

<strong>of</strong> components is possible whenever only <strong>the</strong> resistance or <strong>the</strong> initial stiffness <strong>of</strong> a<br />

joint is sought.<br />

Familiarization with <strong>the</strong> mechanical behaviour <strong>of</strong> various joint components enables <strong>the</strong><br />

analysis <strong>of</strong> a large number <strong>of</strong> various joint congurations with a relatively low number <strong>of</strong><br />

components. The key element in <strong>the</strong> component method <strong>the</strong>refore relates to <strong>the</strong> characterisation<br />

<strong>of</strong> <strong>the</strong> F- relationship for each particular spring (component). For <strong>the</strong> evaluation<br />

<strong>of</strong> <strong>the</strong> initial stiffness <strong>of</strong> a joint only <strong>the</strong> linear stiffness <strong>of</strong> each component is necessary,<br />

while for <strong>the</strong> evaluation <strong>of</strong> ductility it is necessary to know <strong>the</strong> non-linear F- relationship<br />

<strong>of</strong> each component. Classication <strong>of</strong> joints<br />

3.2.1 Classification according to stiffness<br />

Classication according to stiffness for rigid, semi-rigid and pinned joints is performed by<br />

simply comparing <strong>the</strong> design stiffness <strong>of</strong> <strong>the</strong> joint with two stiffness boundaries, Figure 4.<br />

With <strong>the</strong> goal <strong>of</strong> simplication, <strong>the</strong> stiffness boundaries are set in such a way that <strong>the</strong>y allow<br />

a direct comparison with <strong>the</strong> calculated initial stiffness Sj,ini <strong>of</strong> <strong>the</strong> joint, for any type<br />

<strong>of</strong> joint idealisation that is being used in <strong>the</strong> analysis and is presumed beforehand.<br />

The boundaries <strong>of</strong> classication according to stiffness are as follows:


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• rigid joint<br />

(unbraced frames),<br />

(braced frames),<br />

• semi-rigid joint<br />

(unbraced frames),<br />

(braced frames),<br />

• pinned joint<br />

EI/L denotes <strong>the</strong> exural stiffness <strong>of</strong> <strong>the</strong> connected beam.<br />

Fig. 4. Boundaries <strong>of</strong> classication according to joint stiffness<br />

3.2.2 Classification according to resistance<br />

Classication according to resistance consists <strong>of</strong> comparing <strong>the</strong> design joint resistance moment,<br />

M j,Rd<br />

, with <strong>the</strong> boundaries <strong>of</strong> “full-strength” and “pinned”, Figure 5.<br />

Boundaries <strong>of</strong> classication according to resistance are as follows:<br />

• full strength joint<br />

• partial-strength joint<br />

• pinned joint<br />

M full strength<br />

denotes <strong>the</strong> design resistance <strong>of</strong> <strong>the</strong> weaker structural element in <strong>the</strong> connection.<br />

It shall be noted that <strong>the</strong> classication based on experimental Mj- joint characteristics was<br />

not taken into consideration because only <strong>the</strong> design properties were considered.


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3.2.3 Classification according to ductility<br />

Fig. 5. Boundaries <strong>of</strong> classication <strong>of</strong> joint stiffness<br />

Adequate experience and appropriate detailing result in <strong>the</strong> so-called pinned joints that<br />

exhibit a sufcient rotation capacity. That means <strong>the</strong>y can sustain <strong>the</strong> rotations imposed<br />

on <strong>the</strong>m.<br />

In <strong>the</strong> case <strong>of</strong> moment resistant joints a notion <strong>of</strong> ductility class that includes rotation capacity<br />

is introduced. This problem has not been dealt with in more detail within Eurocode<br />

3, although extensive research is being done regarding this problem. In order to evaluate<br />

<strong>the</strong> ductility <strong>of</strong> a joint one can apply an analogy with <strong>the</strong> classication <strong>of</strong> cross-sections<br />

according to rotation capacity. Thus, joints can be classied into three classes concerning<br />

ductility, see Figure 6.<br />

Fig. 6. Ductility classes <strong>of</strong> joints – classication according to rotation capacity


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Class 1 - Able to reach MRd and with a sufciently good rotation capacity to allow plastic<br />

design <strong>of</strong> <strong>the</strong> frame.<br />

Class 2 - Able to reach MRd but with a reduced plastic rotation capacity. A plastic verication<br />

<strong>of</strong> <strong>the</strong> section is anyway allowed.<br />

Class 3 - Where brittle failure (or instability) limits <strong>the</strong> moment resistance and does not<br />

allow full redistribution <strong>of</strong> <strong>the</strong> internal forces in <strong>the</strong> joint.<br />

3.3 Joint modelling<br />

The following types <strong>of</strong> joint modelling have traditionally been considered:<br />

• for rotational stiffness: rigid or pinned;<br />

• for resistance: full-strength or pinned.<br />

However, as far as joint rotational stiffness and economical joint dimensioning are concerned,<br />

<strong>the</strong>y can be semi-rigid. This provides a new possibility <strong>of</strong> joint modelling: semirigid/full-strength<br />

and semi-rigid/partial-strength. Eurocode 3 takes into consideration<br />

<strong>the</strong>se possibilities with three joint modelling types, Table 1:<br />

• continuous:<br />

covers only <strong>the</strong> rigid/full-strength case,<br />

• semi-continuous: covers <strong>the</strong> rigid/partial-strength, semi-rigid/full strength and<br />

semi-rigid/partial-strength cases.<br />

• simple:<br />

covers only <strong>the</strong> pinned case.<br />

Table 1. Joint modelling types<br />

Stiffness<br />

Resistance<br />

Full-strength Partial-strength Pinned<br />

Rigid Continuous Semi-continuous -<br />

Semi-rigid Semi-continuous Semi-continuous -<br />

Pinned - - Simple<br />

The notions continuous, semi-continuous and simple have <strong>the</strong> following meaning:<br />

• continuous:<br />

<strong>the</strong> joint ensures a full rotational continuity between <strong>the</strong> ele<br />

ments it connects;<br />

• semi-continuous: <strong>the</strong> joint ensures only a partial rotational continuity between<br />

<strong>the</strong> elements it connects (connecting elements);<br />

• simple:<br />

<strong>the</strong> joint prevents any rotational continuity between <strong>the</strong><br />

elements it connects.<br />

These meanings are linked to <strong>the</strong> type <strong>of</strong> <strong>the</strong> global analysis <strong>of</strong> <strong>the</strong> frame. In <strong>the</strong> case <strong>of</strong> an<br />

elastic global analysis <strong>of</strong> <strong>the</strong> frame, only <strong>the</strong> stiffness properties <strong>of</strong> <strong>the</strong> joint are important<br />

for joint modelling<br />

In <strong>the</strong> case <strong>of</strong> an ideal plastic analysis, <strong>the</strong> main characteristic <strong>of</strong> <strong>the</strong> joint is resistance. In<br />

all o<strong>the</strong>r cases, <strong>the</strong> properties <strong>of</strong> stiffness as well as resistance are a guide for <strong>the</strong> manner in<br />

which joints are to be modelled.<br />

The above listed possibilities as well as <strong>the</strong>ir physical interpretation for analysis are provided<br />

in Table 2 and in Figure 7, respectively


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Table 2: Joint modelling and frame analysis<br />

Type <strong>of</strong> frame analysis<br />

Joint modelling<br />

Elastic-perfectly<br />

Elastic<br />

Rigid plastic plastic and elastoplastic<br />

Continuous Rigid Full-strength Rigid/full-strength<br />

Semi-continuous Semi-rigid Partial-strength<br />

Rigid/partialstrength<br />

Semi-rigid/fullstrength<br />

Semi-rigid/partial<br />

strength<br />

Simple Pinned Pinned Pinned<br />

Fig. 7. Simplied joint modelling for frame analysis<br />

3.4 Joint idealisation<br />

The Mj- curve that describes non-linear behaviour <strong>of</strong> joints is not convenient for everyday<br />

practice. However, it can be idealised without a more signicant loss <strong>of</strong> exactness.<br />

One <strong>of</strong> <strong>the</strong> simplest idealisations is <strong>the</strong> one done by means <strong>of</strong> <strong>the</strong> elastic-perfectly plastic<br />

relationship, Figure 8. The advantage <strong>of</strong> such modelling is in <strong>the</strong> fact that it is similar to <strong>the</strong><br />

one that is applied for modelling <strong>of</strong> member cross-sections that are subjected to bending.<br />

The M j,Rd<br />

moment that corresponds to <strong>the</strong> yield plateau is within EC 3 called design moment<br />

resistance. It can be considered as a pseudo-plastic moment resistance <strong>of</strong> <strong>the</strong> joint.<br />

The effects <strong>of</strong> strain-hardening and <strong>the</strong> possible membrane effects are neglected, which<br />

explains <strong>the</strong> difference in Figure 8 between <strong>the</strong> actual M- curve and <strong>the</strong> yield plateau in<br />

<strong>the</strong> idealisation.<br />

The value <strong>of</strong> constant stiffness <strong>of</strong> joint S j.ini/<br />

has been explained in a number <strong>of</strong> papers,<br />

and practical values are provided in EC 3, Part 1.8. The coefcient results from a highly


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expressed non-linearity <strong>of</strong> <strong>the</strong> Mj- joint curves in comparison to <strong>the</strong> M- curves for structural<br />

elements.<br />

Fig. 8. Bi-linearisation <strong>of</strong> <strong>the</strong> M- curves<br />

Actually <strong>the</strong>re are different possibilities <strong>of</strong> Mj- joint curve idealisations. The choice <strong>of</strong><br />

one <strong>of</strong> <strong>the</strong>m depends on <strong>the</strong> type <strong>of</strong> global analysis <strong>of</strong> <strong>the</strong> frame used, and EC 3 lists <strong>the</strong>m<br />

according to <strong>the</strong> following:<br />

• elastic idealisation for <strong>the</strong> elastic analysis,<br />

• perfectly plastic idealisation for <strong>the</strong> perfectly plastic analysis,<br />

• non-linear idealisation for <strong>the</strong> elastic-plastic analysis.<br />

4 CHOICE OF A JOINT MODEL<br />

Joints presented as rigid or pinned in an analysis should be dimensioned in such a way that<br />

<strong>the</strong>y satisfy <strong>the</strong> conditions for a classication <strong>of</strong> a rigid or pinned joint. The model for a<br />

semi-rigid joint can be more or less complex. It can be modelled as a spring for which M-<br />

relationship is in <strong>the</strong> range between linear elastic and non-linear, see Figure 9. The elastic<br />

global analysis requires that <strong>the</strong> behaviour <strong>of</strong> a joint be modelled as linear elastic. The elastic<br />

– perfectly plastic analysis requires a bi-linear joint model. So, <strong>the</strong> type <strong>of</strong> global analysis<br />

directly inuences <strong>the</strong> complexity <strong>of</strong> <strong>the</strong> adopted joint model. It should be mentioned<br />

that formation <strong>of</strong> plastic hinges in <strong>the</strong> joints is allowed in <strong>the</strong> application <strong>of</strong> plastic analysis.<br />

Fig. 9. Presentation <strong>of</strong> different Mj- relationships<br />

5 ECONOMIC JUSTIFICATION OF THE NEW APPROACH<br />

A modern approach to <strong>the</strong> behaviour <strong>of</strong> joints is based on <strong>the</strong> realistic behaviour <strong>of</strong> joints<br />

as semi-rigid. It is founded on economic justication <strong>of</strong> a structure in which <strong>the</strong> joints have<br />

been considered as semi-rigid. To obtain <strong>the</strong> minimum price <strong>of</strong> a steel structure two design


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strategies are possible regarding <strong>the</strong> execution <strong>of</strong> <strong>the</strong> joint:<br />

• Simplication <strong>of</strong> joint details which results in reducing <strong>the</strong> costs <strong>of</strong> workshop execution.<br />

It is important for unbraced frames where joints transfer signicant moments and those are<br />

rigid joints.<br />

• By reducing cross-sections <strong>of</strong> elements which results in decreasing <strong>the</strong> expenses for material.<br />

It is signicant for braced frames with nominally pinned joints.<br />

Generally speaking both strategies will lead to <strong>the</strong> application <strong>of</strong> semi-rigid joints. In <strong>the</strong><br />

case <strong>of</strong> rigid joints an economic solution can be achieved if <strong>the</strong> stiffness <strong>of</strong> joint is close to<br />

<strong>the</strong> classication limit <strong>of</strong> semi-rigid joint.<br />

Different economic studies show that <strong>the</strong>re is a possibility <strong>of</strong> saving with <strong>the</strong> application<br />

<strong>of</strong> semi-rigid joints and <strong>the</strong> adequate design <strong>of</strong> 20-25% in <strong>the</strong> case <strong>of</strong> unbraced frames<br />

and 5-9% in <strong>the</strong> case <strong>of</strong> braced frames. With <strong>the</strong> assumption that <strong>the</strong> price <strong>of</strong> steel frames<br />

amounts to about 10% <strong>of</strong> <strong>the</strong> total price <strong>of</strong> a commercial building and about 20% for an<br />

industrial building a decrease in total costs can be estimated to 4-5% for unbraced frames.<br />

For braced frame systems saving <strong>of</strong> 1-2% is possible. The costs <strong>of</strong> material and workshop<br />

execution depend on <strong>the</strong> relative stiffness <strong>of</strong> <strong>the</strong> joint, Figure 10.<br />

Fig. 10. Qualitative relation <strong>of</strong> a steel structure depending on <strong>the</strong> relative stiffness <strong>of</strong> <strong>the</strong> joint<br />

With an increase <strong>of</strong> <strong>the</strong> relative stiffness <strong>of</strong> joints <strong>the</strong> costs <strong>of</strong> material is decreased, curve<br />

A, whereas <strong>the</strong> costs <strong>of</strong> labour grow, curve B. For <strong>the</strong> total costs that are a sum <strong>of</strong> <strong>the</strong> costs<br />

<strong>of</strong> curves A and B, <strong>the</strong> minimum can be found and <strong>the</strong>refore <strong>the</strong> optimum relative stiffness<br />

as well. In many cases <strong>the</strong> value that leads to <strong>the</strong> optimum design <strong>of</strong> a structural system by<br />

taking into consideration <strong>the</strong> minimum <strong>of</strong> <strong>the</strong> total costs does not lie in <strong>the</strong> area <strong>of</strong> nominally<br />

pinned nor in <strong>the</strong> area <strong>of</strong> semi-rigid joints.<br />

Looking at <strong>the</strong> trends in <strong>the</strong> past few decades it is obvious that <strong>the</strong> costs <strong>of</strong> labour grow<br />

compared to <strong>the</strong> costs <strong>of</strong> <strong>the</strong> used material (see curve B*). As a result, see Figure 10, it is<br />

clear that a fast development <strong>of</strong> <strong>the</strong> optimum stiffness <strong>of</strong> joints shifts more towards semirigid<br />

joints. Therefore, in an attempt to nd an economic solution for steel structures <strong>the</strong><br />

use <strong>of</strong> semi-rigid joints will become increasingly more interesting.<br />

6 CONCLUSION<br />

The design <strong>of</strong> structural joints that is proposed in Eurocode 3, is based on <strong>the</strong> research<br />

conducted over <strong>the</strong> past few decades. Eurocode 3 gives practical guidelines for <strong>the</strong> characterisation<br />

<strong>of</strong> most <strong>of</strong> steel joints (beam-to-column joints, beam and column splices, column<br />

base plates etc.) <strong>of</strong> frames made <strong>of</strong> I or H cross sections, loaded by static load. Fur<strong>the</strong>r<br />

research is focused on extending <strong>the</strong> guidelines for characterisation <strong>of</strong> joints as composite


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joints (concrete and steel) and joints made <strong>of</strong> o<strong>the</strong>r types <strong>of</strong> cross sections and o<strong>the</strong>r types<br />

<strong>of</strong> load.<br />

The new approach, semi-rigid joints – semi-continuous structure, gives more possibilities<br />

than <strong>the</strong> traditional approach in type <strong>of</strong> framing. This is based on <strong>the</strong> fact that <strong>the</strong> joint<br />

characteristics in <strong>the</strong> design have been considered as variables that are chosen to comply<br />

with <strong>the</strong> particular requirements <strong>of</strong> a specic project.<br />

For braced frames, <strong>the</strong> new approach allows <strong>the</strong> use <strong>of</strong> smaller cross sections <strong>of</strong> beams<br />

and a reduction <strong>of</strong> <strong>the</strong> costs <strong>of</strong> <strong>the</strong> structural frame. For unbraced frames <strong>the</strong> new approach<br />

reduces <strong>the</strong> complexity <strong>of</strong> <strong>the</strong> joint geometry and thus results in major saving in <strong>the</strong> execution<br />

costs.<br />

REFERENCES<br />

1. Eurocode 3, Design <strong>of</strong> Steel Structures, Part 1.1: General Rules and Rules for Buildings,<br />

European Prestandard ENV 1993-1-1, Brussels: CEN, 1992.<br />

2. Revised Annex J <strong>of</strong> Eurocode 3. Joints in Building Frames, European Prestandard<br />

ENV 1993-1-1: 1992/A2, Brussels: CEN, 1998.<br />

3. Eurocode 3, Design <strong>of</strong> Steel Structures, Part 1.8: Design <strong>of</strong> Joints, European Prestandard<br />

prEN 1993-1-8, Final Draft, Brussels: CEN, 2001.<br />

4. Maquoi, R.; Chabrolin, B.: Frame Design Including Joint Behaviour, ECSC Report<br />

18563, Luxembourg, Ofce for Ofcial Publications <strong>of</strong> <strong>the</strong> European Communities,<br />

1998.<br />

5. Ne<strong>the</strong>rcot, D.; Zandonini, R.: Methods <strong>of</strong> prediction <strong>of</strong> joint behaviour – Beam to<br />

column connections, In: Naranayan, R. (ed.) Structural Connections – Stability and<br />

Strength, Elsevier Applied Science, 1989., 23-62<br />

6. European Convention for Constructional Steelwork, Analysis Design <strong>of</strong> Steel Frames<br />

with Semi-rigid Joints, Publication 67, Brussels: ECCS, 1992.<br />

7. Zoetemeijer, P.: A design method for <strong>the</strong> tension side <strong>of</strong> statically-loaded bolted beamto-column<br />

joints, Heron 1974; 1-59<br />

8. Weynand, K.; Jaspart, J.-P.; Steenhuis, M.: The stiffnes model <strong>of</strong> revised Annex J <strong>of</strong><br />

Eurocode 3, In: Bjorhovde, R.; Colson, A.; Zandonini, R., (editors): Connections in<br />

steel structures, Trento, 1995., 441-452<br />

9. Huber, G.; Tschemmernegg, F.: Modelling <strong>of</strong> steel connections, Journal <strong>of</strong> Constructional<br />

Steel Research 45 (1998) 2, 199-216<br />

10. Weynand, K.; Jaspart, J.-P.; Steenhuis, M.: Economy Studies <strong>of</strong> Steel Building Frames<br />

with Semi-Rigid Joints, Journal <strong>of</strong> Constructional Steel Research 46:1-3 (1998)<br />

11. Giro Coelho, A. M.; Bijlaard, F. S. K.; da Silva, L. S.:Experimental assessment <strong>of</strong> <strong>the</strong><br />

ductility <strong>of</strong> extended end plateconnections. Engineering Structures 26 (2004), 1185-<br />

1206.<br />

12. da Silva, L. S.; Lima, L.; Vellasco, S.; Andrade, S.: Experimental behaviour <strong>of</strong> endplate<br />

beam-to-column joints under bending and axial force, Database reporting and<br />

discussion <strong>of</strong> results. Report on ECCS-TC10, Meeting in Ljubljana, April 2002.<br />

13. Faella, C.; Piluso, V.; Rizzano, G.: Structural Steel Semirigid Connections, Theory,<br />

Design and S<strong>of</strong>tware, CRC Press LLC, 2000 N.W. Corporate Blvd., Boca Raton, Florida<br />

33431, 2000.<br />

14. Cruz, P. J.S; da Silva, L. S.; Rodrigues, D. S; Simes, R. A. D.: Database for <strong>the</strong><br />

semi-rigid behaviour <strong>of</strong> beam-to-column connections in seismic regions, Journal <strong>of</strong><br />

Constructional Steel Research 46 (1998) 1-3, 233-234<br />

15. Robot Millennium Program - Version 17.5: User's Manual, RoboBAT, June 2004.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 121<br />

Development strategy <strong>of</strong><br />

ECOINDUSTRAL PARK RAŠA – EIPR<br />

Pr<strong>of</strong>.dr.sc. Juraj Božičević<br />

Elitech Ltd.<br />

Trg kralja Tomislava 18 Zagreb 10000, Croatia<br />

juraj.bozicevic1@zg.t-com.hr, Tel. 00385 1 4922264<br />

Dr.sc. Marijan Andrašec<br />

Ecooleum Ltd.<br />

Trg kralja Tomislava 18, Zagreb 10000, Croatia<br />

marijan.andrasec@zg.t-com.hr, Tel. 00385 98 404755<br />

Abstract<br />

The pith <strong>of</strong> <strong>the</strong> strategy <strong>of</strong> development <strong>of</strong> <strong>the</strong> Ecoindustrial Park Raša is presented. The<br />

Park is situated in <strong>the</strong> bay <strong>of</strong> Raša, unique but improperly used and maintained Croatian<br />

fjord. The starting point in conceiving <strong>of</strong> <strong>the</strong> Ecoindustrial Park Raša is synergy <strong>of</strong> service<br />

and production activities, successful cooperation <strong>of</strong> companies aiming to achieve results on<br />

<strong>the</strong> following principle: unity is more successful than <strong>the</strong> amount <strong>of</strong> successfully combined<br />

activity <strong>of</strong> singular companies, units <strong>of</strong> <strong>the</strong> system. The contribution will be <strong>the</strong> care about<br />

industrial ecology, streng<strong>the</strong>ning <strong>of</strong> <strong>the</strong> integration <strong>of</strong> economic raise and protection <strong>of</strong><br />

environment as well as industrial symbiosis that will improve <strong>the</strong> economy and <strong>the</strong> quality<br />

<strong>of</strong> life in <strong>the</strong> Community <strong>of</strong> Raša.<br />

Key words: ecoindustrial park, sustainable development, Port Raša, Community <strong>of</strong> Raša<br />

Contents<br />

1.0 Introduction<br />

2.0 The Community <strong>of</strong> Raša<br />

2.1 Geography<br />

2.2 Present situation<br />

3.0 Ecoindustrial Park Raša – EIPR - conceptualization<br />

3.1 What is an Ecoindustrial Park – EIP?<br />

3.2 Basics for conceptualization <strong>of</strong> EIPR<br />

3.3 Projects in EIPR proposed for realization<br />

3.4 Ecoindustrial Park and <strong>the</strong> Community <strong>of</strong> Raša<br />

3.5 Stakeholders<br />

3.6 Knowledge and experience on which venture relies<br />

4.0 Ecoindustrial Park Raša – EIPR - realization<br />

4.1 The way <strong>of</strong> achieving realization <strong>of</strong> EIPR<br />

4.2 Economy <strong>of</strong> <strong>the</strong> project EIPR<br />

4.3 Risks<br />

4.4 Development effects achieved with EIPR<br />

4.5 Priority tasks


122<br />

5.0 Conclusion<br />

6.0 References<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

1 Introduction<br />

When, during <strong>the</strong> early 1990s, more precisely, in 1993, Croatian System Society has organized<br />

<strong>the</strong> rst conference called The Port as a Complex System, our guiding idea was<br />

<strong>the</strong> promotion <strong>of</strong> knowledge about <strong>the</strong> importance <strong>of</strong> <strong>the</strong> modernization <strong>of</strong> <strong>the</strong> Croatian<br />

ports and <strong>the</strong> strategic consideration about <strong>the</strong> role <strong>of</strong> <strong>the</strong> ports in <strong>the</strong> development <strong>of</strong> <strong>the</strong><br />

economy. At that time <strong>the</strong> rst author was, as <strong>the</strong> Associate Minister for higher education<br />

in <strong>the</strong> Ministry <strong>of</strong> Education and Sports, participated at <strong>the</strong> rst Croatian – Ne<strong>the</strong>rlands negotiations<br />

about <strong>the</strong> cooperation in education area... so he took <strong>the</strong> opportunity to visit <strong>the</strong><br />

Rotterdam port and learn on higher maritime education, as well as on <strong>the</strong> training equipment<br />

at <strong>the</strong> High Maritime College, with <strong>the</strong> intention to transfer gained experiences to<br />

<strong>the</strong> Maritime Faculty in Rijeka. He was accompanied by a host, a Dutchman, who was <strong>the</strong><br />

member <strong>of</strong> <strong>the</strong> management board <strong>of</strong> <strong>the</strong> Rotterdam port and who presented him numerous<br />

data which illustrated <strong>the</strong> importance <strong>of</strong> <strong>the</strong> port and its industrial area for <strong>the</strong> economy <strong>of</strong><br />

<strong>the</strong> Ne<strong>the</strong>rlands. The host was especially interested in Croatia’s plans – in which way will<br />

Croatia, after has gained independence, use its maritime position, and how Croatian strategic<br />

plan <strong>of</strong> development <strong>of</strong> economy and <strong>the</strong> ports will be conceived. We shall quote <strong>the</strong><br />

private communication <strong>of</strong> <strong>the</strong> rst author (3): The Dutchman emphasized <strong>the</strong> extraordinary<br />

geographical position and maritime features <strong>of</strong> <strong>the</strong> Port <strong>of</strong> Rijeka and neighboring ports<br />

within its jurisdiction. He had excellent knowledge <strong>of</strong> Croatian possibilities, and, since I<br />

was preparing for <strong>the</strong> conference „Port as a complex system“ in Rijeka, I presented him<br />

ambitiously <strong>the</strong> vision <strong>of</strong> <strong>the</strong> Conference Program board and our idea about ports development<br />

in Croatia... He asked me if we really have full understanding <strong>of</strong> <strong>the</strong> geo-strategic importance<br />

<strong>of</strong> <strong>the</strong> Port <strong>of</strong> Rijeka and its possible competitiveness in relation to <strong>the</strong> Rotterdam<br />

port. When we shaked hands during <strong>the</strong> parting, he said to me, half-jokingly, something<br />

which stunned me: «I will kill myself if <strong>the</strong> Port <strong>of</strong> Rijeka takes even 1% <strong>of</strong> <strong>the</strong> middle-<br />

European traf c from <strong>the</strong> Port <strong>of</strong> Rotterdam.»<br />

That was <strong>the</strong> war time in Croatia. The Port <strong>of</strong> Rijeka was destination <strong>of</strong> just a few ships.<br />

When I talked about this event to my closest cooperate in <strong>the</strong> project „Port as <strong>the</strong> Complex<br />

System“, dr. Juraj Maari, he suggested me not to talk about <strong>the</strong> Dutchman’s statement,<br />

because no one will understand... However, he proposed that we talk about this in inner<br />

circle as a very serious topic, and that <strong>the</strong> program <strong>of</strong> our future conferences should be<br />

gradually developed in such way that, in <strong>the</strong> sphere <strong>of</strong> <strong>the</strong> economic decision making, we<br />

could develop <strong>the</strong> awareness about <strong>the</strong> need for <strong>the</strong> strategy <strong>of</strong> <strong>the</strong> economic development<br />

which is leaning upon <strong>the</strong> maritime orientation.<br />

The fourth conference ”Port as a Complex System”“ held in 1999, was dedicated to strategic<br />

topics:<br />

„Rijeka – <strong>the</strong> Main Croatian Port and joined Rijeka and Zagreb – Croatian and European<br />

economic Focus“. (4, 5) However, since 2000, <strong>the</strong>re was no more interest for <strong>the</strong> Conferences....<br />

I was introduced to <strong>the</strong> operations <strong>of</strong> <strong>the</strong> Port <strong>of</strong> Rijeka ve years later, when I started to<br />

cooperate with <strong>the</strong> Community <strong>of</strong> Raša. The talks with <strong>the</strong> mayor <strong>of</strong> <strong>the</strong> Community encouraged<br />

me to think about <strong>the</strong> sustainable development <strong>of</strong> <strong>the</strong> port area <strong>of</strong> Raša, which is in<br />

concession <strong>of</strong> <strong>the</strong> Port <strong>of</strong> Rijeka. Really, about very strategic Task.<br />

The mayor <strong>of</strong> Raša accepted <strong>the</strong> idea <strong>of</strong> consulting company Elitech Ltd. to make <strong>the</strong> development<br />

concept <strong>of</strong> <strong>the</strong> Community <strong>of</strong> Raša as socially responsible community, <strong>the</strong> basis<br />

<strong>of</strong> <strong>the</strong> wise exploration <strong>of</strong> its natural resources, revitalisation and fur<strong>the</strong>r development <strong>of</strong>


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 123<br />

its economy, based upon <strong>the</strong> idea <strong>of</strong> eco-industrial society.<br />

The following agreement was accepted as <strong>the</strong> frame work: The target <strong>of</strong> sustainable development<br />

is to facilitate and fulll <strong>of</strong> basic necessities and quality lives to all <strong>the</strong> citizens <strong>of</strong><br />

<strong>the</strong> Community, having in mind not to risk <strong>the</strong> quality <strong>of</strong> life <strong>of</strong> future generations. If we<br />

don’t take care about sustainable development we could face an insecure future. Therefore<br />

<strong>the</strong> sustainable development is our best long-term interest.<br />

We started with work in autumn 2005. We had number <strong>of</strong> meetings with <strong>the</strong> mayor and <strong>the</strong><br />

head <strong>of</strong> <strong>the</strong> County <strong>of</strong> Istria, who suggested that <strong>the</strong> Community <strong>of</strong> Raša, in cooperation<br />

with consulting company Elitech Ltd., should establish <strong>the</strong> Working group for strategic<br />

development <strong>of</strong> port area and sign an agreement upon it.<br />

With <strong>the</strong> acceptance <strong>of</strong> Letter <strong>of</strong> Intent, signed by Community <strong>of</strong> Raša, County <strong>of</strong> Istria,<br />

Port <strong>of</strong> Rijeka, Port Authority <strong>of</strong> Rijeka and Elitech Ltd. on 15th December 2006, Working<br />

group started with meetings and discussions in early 2007.<br />

As a basis for discussions has been <strong>the</strong> study „Development <strong>of</strong> Eco-energy Valley <strong>of</strong> Raša<br />

and Port area Raša based upon <strong>the</strong> production <strong>of</strong> bi<strong>of</strong>uel”, made by Naval Research Institute<br />

in Zagreb in cooperation with <strong>the</strong> company Elitech Ltd. and <strong>the</strong> company Ecooleum<br />

Ltd., which joined <strong>the</strong> Working group. Ecooleum Ltd was established with <strong>the</strong> purpose to<br />

realize conceived projects.<br />

The idea <strong>of</strong> technological platform Ecoenergy Valley was developed and presented to <strong>the</strong><br />

Croatian Institute for Technology as a possible EU-project in order to nance <strong>the</strong> project.<br />

Aside to eco-energy production, <strong>the</strong> particular attention was focused upon trafc infrastructure,<br />

especially in revitalizing <strong>of</strong> <strong>the</strong> railway as important support to port activity.<br />

In <strong>the</strong> period from 2008 to <strong>2010</strong> <strong>the</strong> idea <strong>of</strong> Eco-industrial society has been developed in<br />

nal form, and <strong>the</strong> basic conception is presented in this paper.<br />

In 2008. <strong>the</strong> Forum for Social Responsible Activity was founded to facilitate communication<br />

with local community. The companies Holcim and Murexin - Istarska tvornica vapna<br />

joined <strong>the</strong> Forum, and <strong>the</strong> consultations were held upon <strong>the</strong> Sustainable Development <strong>of</strong><br />

Community <strong>of</strong> Raša. Initially, <strong>the</strong> important contribute was made by Croatian Systems<br />

Society and <strong>the</strong>ir study Ecoproduct areas <strong>of</strong> Croatia and <strong>the</strong>n with <strong>the</strong>ir project Systemic<br />

considerations <strong>of</strong> social responsibility in <strong>the</strong> living area (2008-9), nanced by Ministry <strong>of</strong><br />

Environment Protection, Space Planning and Construction.<br />

In <strong>the</strong> case <strong>of</strong> Ecoindustrial park <strong>of</strong> Raša it has been conceived <strong>the</strong> interaction <strong>of</strong> portrelated,<br />

industrial, energy, agricultural, maricultural and touristic activities that rely on<br />

restructured and highly functional communal and trafc infrastructure – port, road and<br />

railway. We would like to emphasize <strong>the</strong> part <strong>of</strong> activities in management <strong>of</strong> eco-industrial<br />

park that will be very important for successful achievement <strong>of</strong> sustainable development<br />

and industrial symbiosis, for <strong>the</strong> reduction <strong>of</strong> costs, common use <strong>of</strong> information, services,<br />

energy and byproducts as raw material for number <strong>of</strong> users.<br />

From <strong>the</strong> point <strong>of</strong> view <strong>of</strong> <strong>the</strong> Community <strong>of</strong> Raša, it was particularly important to motivate<br />

enterprising spirit in <strong>the</strong> development <strong>of</strong> port activity. It is presumable that <strong>the</strong> building <strong>of</strong><br />

<strong>the</strong> Park will be especially benecial and a big impulse on port activity, and <strong>the</strong> Port <strong>of</strong><br />

Rijeka, which is <strong>the</strong> concessionaire, should be encouraged to show more responsibility on<br />

that valuable national resource.


124<br />

2 The Community <strong>of</strong> Raša<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

2.1 Geography<br />

The Community <strong>of</strong> Raša is situated on south-eastern side <strong>of</strong> Istrian peninsula. Its surface is<br />

7.954 ha, it contains 23 settlements with 3535 inhabitants and <strong>the</strong> shore length <strong>of</strong> 48 km.<br />

It is part <strong>of</strong> Region <strong>of</strong> Istria.<br />

The Community <strong>of</strong> Raša have got high quality land for agricultural production that is partly<br />

owned by private persons, and partly is property <strong>of</strong> Republic <strong>of</strong> Croatia and <strong>of</strong> <strong>the</strong> Community.<br />

It is planted with fodder, vegetable in lowlands, and with grapes, fruits and medicinal<br />

cultures and olives on <strong>the</strong> sunny positions. Forests are mostly <strong>of</strong> private property, and <strong>the</strong><br />

rest <strong>of</strong> it is property <strong>of</strong> Republic <strong>of</strong> Croatia and are managed by Croatian Forests.<br />

The forests are not important for exploitation but are very important for ecological balance,<br />

prevention <strong>of</strong> erosion, improvement <strong>of</strong> microclimatic conditions and development <strong>of</strong><br />

agrotourismus and recreation.<br />

Climatic conditions in Community <strong>of</strong> Raša are characterized with bigger quantity <strong>of</strong> rains<br />

than <strong>the</strong> west side <strong>of</strong> Istria. Rainy period is at its peak in October and minimum in July.<br />

The most signicant winds are nor<strong>the</strong>astern, especially bura in winter period and summer’s<br />

night wind in most part <strong>of</strong> shore territory, sou<strong>the</strong>astern – especially jugo (sirocco) in spring<br />

and autumn, northwestern – especially during summer period.<br />

Soils are shallow and stony, and smaller areas <strong>of</strong> deep soil we can nd in typical karstic<br />

forms – short lanes and karstic heights, predominantly red and brown soil. In <strong>the</strong> area <strong>of</strong><br />

<strong>the</strong> river Raša we nd hidromorc (gley) soil, and on <strong>the</strong> edges aluvial-coluvial soils that<br />

are salinized on <strong>the</strong> estuary <strong>of</strong> river. The river <strong>of</strong> Raša is <strong>the</strong> main and <strong>the</strong> most important<br />

water-current in water-supply-system “Raša-Boljunica“. Its characteristic is <strong>the</strong> frequent<br />

torrents, so at times extremely high water is to be expected. The main water sources are<br />

Fonte Gaj and Kokoti. The town <strong>of</strong> Raša with 1800 inhabitants does not have waste water<br />

purication facility.<br />

Across <strong>the</strong> Community <strong>of</strong> Raša <strong>the</strong>re is state road D21 Pula-Labin, number <strong>of</strong> regional and<br />

local roads. Numbers <strong>of</strong> unclassied roads are under community’s jurisdiction.<br />

Railroad Lupoglav-Štalije is used exclusively for transport; it’s not electried, it’s in group<br />

<strong>of</strong> mountain railways and is qualied for average speed <strong>of</strong> 60 km/h. Railway station is in<br />

Most Raša.<br />

There are several ports on <strong>the</strong> territory <strong>of</strong> <strong>the</strong> Community <strong>of</strong> Raša. The port Bršica is <strong>the</strong><br />

only one classied for international sea shipping (state-level port). The port <strong>of</strong> Koromano<br />

is special purpose port – industrial port. The ports Sveta Marina, Trget and Tunarica are <strong>of</strong><br />

local importance (shery).<br />

The main direction <strong>of</strong> magistral gas pipeline (for international transport) <strong>of</strong> national importance<br />

Casal Borsetti – Karlovac DN700, transits along eastern shore <strong>of</strong> Istria and is passing<br />

through a part <strong>of</strong> Community’s territory.<br />

2.2 Present situation<br />

Once industrially developed and supported by mining (coal mines, coal power plant) and<br />

by production <strong>of</strong> machine-tools (Prvomajska factory), <strong>the</strong> Community <strong>of</strong> Raša became<br />

poor with <strong>the</strong> closure <strong>of</strong> coal mine and failure <strong>of</strong> Prvomajska, leaning nowadays on companies<br />

Holcim, ITV Murexin and hardly active Port.<br />

The territory <strong>of</strong> <strong>the</strong> Port <strong>of</strong> Raša, <strong>the</strong> most valuable industrial zone in Istria, has long tradition<br />

in energetic sector (coal), and <strong>the</strong> industrial culture <strong>of</strong> inhabitants was developed. In


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 125<br />

<strong>the</strong> past it was mostly used to support local industry, and <strong>the</strong>refore never had signicant<br />

value as transit port for Middle-European area, although it was connected by railroad to<br />

Trieste and fur<strong>the</strong>r to North Italy and Middle Europe.<br />

The port is used for stone and timber transport. Port installations and operative quay are in<br />

dilapidated conditions so <strong>the</strong> new one should be made, o<strong>the</strong>r trafc, energy and water infrastructure<br />

should be made too and operative and warehousing surface should be widened.<br />

The bottom <strong>of</strong> <strong>the</strong> bay should be cleaned from <strong>the</strong> mud.<br />

On <strong>the</strong> location <strong>of</strong> Bršica a stone pit existed, that was closed in 1978, so this area should<br />

be revitalized by removing <strong>the</strong> part <strong>of</strong> <strong>the</strong> hill between microlocations Bršica and Štalije.<br />

Agricultural land in river Raša valley and along <strong>the</strong> channels are poorly used, because <strong>of</strong><br />

<strong>the</strong> irresponsible maintenance <strong>of</strong> <strong>the</strong> channels, non resolved water overow protection and<br />

salinization.<br />

The territory <strong>of</strong> Raša is rich with high quality lime stone, so <strong>the</strong> stone exploitation, as well<br />

as in o<strong>the</strong>r parts <strong>of</strong> Istria, is a part <strong>of</strong> traditional exploitation. On that basis <strong>the</strong> production <strong>of</strong><br />

lime (ITV – Istrian Lime Factory) and cement (Holcim) were established, so <strong>the</strong> fur<strong>the</strong>r establishment<br />

<strong>of</strong> complementary production with higher grade <strong>of</strong> material processing would<br />

be natural development <strong>of</strong> this industry.<br />

The project <strong>of</strong> waste water drainage should be replaced with improved project with which<br />

should be projected high quality equipment for depuration and obtained technical water for<br />

agricultural production on uncultivated agricultural land.<br />

The urban plan <strong>of</strong> Community <strong>of</strong> Raša in <strong>the</strong> past did not provide for appropriate development<br />

<strong>of</strong> <strong>the</strong> Community <strong>of</strong> Raša, as well as <strong>of</strong> <strong>the</strong> port-area. It should be upgraded in <strong>the</strong><br />

new urban plan.<br />

3 Ecoindustrial Park Raša – EIPR - conceptualization<br />

3.1 What is an Ecoindustrial Park – EIP?<br />

An Ecoindustrial Park is unity <strong>of</strong> production and service activities that cultivate cooperation<br />

and with emphasized care about environment and materials, harmonizing energy,<br />

water and materials ows. Acting toge<strong>the</strong>r, <strong>the</strong> members <strong>of</strong> business units take care <strong>of</strong> <strong>the</strong><br />

common prot, which is bigger than amount <strong>of</strong> single prot that <strong>the</strong> single company would<br />

achieve optimizing proper activity independently. In that way economic success <strong>of</strong> <strong>the</strong><br />

companies increases and minimizes its inuence on environment. That is a new concept<br />

<strong>of</strong> sustainable development <strong>of</strong> <strong>the</strong> local community which protects <strong>the</strong> economy <strong>of</strong> local<br />

society from undesired inuences <strong>of</strong> globalization.<br />

EIP has rich and different possibilities <strong>of</strong> development including diversity <strong>of</strong> environment<br />

cultivation, infrastructure, single outt and resources, common services etc.<br />

Since <strong>the</strong> beginning <strong>of</strong> 90s, a number <strong>of</strong> ecoindustrial parks were established all over <strong>the</strong><br />

world, and <strong>the</strong>ir activities proved that public and private sector is interested in such concept<br />

<strong>of</strong> sustainable development. (8, 9, 10, 11, 12)<br />

Ecoindustrial parks are developed in three basic forms:<br />

Transformation <strong>of</strong> an existing industrial park,<br />

Revitalization <strong>of</strong> previously used sites (brownelds development).<br />

New industrial site development.


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Often <strong>the</strong>se appear in combination. When existing industrial parks undergo expansion, this<br />

can be developed as an eco-industrial park.<br />

The form <strong>of</strong> ElP development brings certain preconditions that affect <strong>the</strong> whole planning<br />

process: Existing industrial parks have <strong>the</strong> companies for potential synergies, but <strong>of</strong>ten <strong>the</strong><br />

interaction between <strong>the</strong> companies is not developed, making it difcult to get to know companies<br />

and <strong>the</strong>ir potential in detail. Park management and local authorities have to invest<br />

time in community interaction among <strong>the</strong> companies.<br />

As in developing traditional industrial parks, similar strategies can be used to establish ecoindustrial<br />

parks. The most commonly practiced or researched strategies are:<br />

Anchor tenant; This involves having a large industrial user, <strong>of</strong>ten a power plant, sugar<br />

renery or o<strong>the</strong>r types <strong>of</strong> operation with large-scale material ows, which <strong>the</strong> industrial<br />

park will be developed around.<br />

Materials or By-product exchange; This can occur ei<strong>the</strong>r in an eco-industrial park or in a<br />

regional network <strong>of</strong> businesses, including industrial parks. This involves using one industry’s<br />

waste or “by products” as ano<strong>the</strong>r industry’s raw materials.<br />

Resource Recovery System; is an expanded concept <strong>of</strong> <strong>the</strong> byproduct exchange and includes<br />

all forms <strong>of</strong> material and product recovery in an industrial complex (waste management,<br />

by-product exchange, recycling and remanufacturing).<br />

Energy connections; involves maximizing energy efciency through design or rehabilitation,<br />

co-generation, and energy cascading. It can also include <strong>the</strong> utilization <strong>of</strong> renewable<br />

energy.<br />

Thematic Park; a number <strong>of</strong> ElPs focus on co-locating a specic type <strong>of</strong> industry. Examples<br />

<strong>of</strong> such <strong>the</strong>matic parks are:<br />

Agriculture-based EIP or Agro-ElP; provides support for sustainable farming and<br />

food processing and includes several basic types <strong>of</strong> rms and agencies which may be recruited<br />

as tenants. Farms and food processing industries have a high ow <strong>of</strong> organic material<br />

that can easily be fur<strong>the</strong>r processed and maximized in its resource value.<br />

Chemical EIP; <strong>the</strong> chemical industry uses co-location <strong>of</strong> production units and<br />

upstream-downstream synergies as <strong>the</strong>ir core business.<br />

Sector-specic EIP (Textile, Electronics etc.); a number <strong>of</strong> regions have historical<br />

industrial areas with an agglomeration <strong>of</strong> sector industries, <strong>of</strong>ten as industrial clusters, but<br />

also as industrial parks. Companies located <strong>the</strong>re usually have similar problems and less<br />

potential for synergies, but strong links between companies (associations) can stimulate<br />

joint problem solving and innovation concepts.<br />

Resource Recovery EIP; companies involved in recycling, reuse, remanufacturing,<br />

niche collection <strong>of</strong> materials, and manufacturing from recovered materials form a cluster<br />

with good synergies among <strong>the</strong>m.<br />

Environmental Technology Parks/EIP; <strong>the</strong> concept focuses on <strong>the</strong> promotion <strong>of</strong><br />

environmental technology industries. Aside from possible innovation synergies, <strong>the</strong>ir colocation<br />

does not necessarily provide any benet in industrial symbiosis. Many environmental<br />

technology companies produce like ordinary manufacturing businesses.<br />

3.2 Basics for conceptualization <strong>of</strong> EIPR<br />

Considering <strong>the</strong> past experiences and <strong>the</strong> present situation it is natural wish <strong>of</strong> Community’s<br />

management to initiate development on new basis and use extraordinary natural<br />

resources, especially port-area, with <strong>the</strong> special attention on sustainable development approach.<br />

The proposed study should bring <strong>the</strong> strategy <strong>of</strong> development <strong>of</strong> Ecoindustrial Park <strong>of</strong>


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 127<br />

Raša as <strong>the</strong> basis <strong>of</strong> sustainable development <strong>of</strong> <strong>the</strong> Community <strong>of</strong> Raša.<br />

The conditions relevant for conceptualization <strong>of</strong> EIPR are:<br />

<strong>the</strong>re are existing old industrial zone and economically weakly developed port,<br />

not connected all subjects in space and do not cooperate, so <strong>the</strong>y should be brought to create<br />

new relations through new ideas,<br />

local community is interested in forming EIPR, because it should solve its infrastructural<br />

and ecological difculties and economical development,<br />

present entities could be netted with new projects,<br />

location is important also on Croatian level (state port!), and at North Adriatic area is <strong>the</strong><br />

only free and high quality industrial space.<br />

Extraordinary convenient trafc settlement: port, road and railway should be natural encouragement<br />

for <strong>the</strong> logistic support <strong>of</strong> activities in EIPR. With planning and restoring<br />

<strong>of</strong> <strong>the</strong> railway and in <strong>the</strong> future with <strong>the</strong> tunneling <strong>of</strong> <strong>the</strong> mountain Uka, EIPR will have<br />

additional value.<br />

The activities on settling <strong>of</strong> <strong>the</strong> port area, removal <strong>of</strong> ruins <strong>of</strong> <strong>the</strong> abandoned separation <strong>of</strong><br />

<strong>the</strong> coal and <strong>the</strong> formation <strong>of</strong> initial industrial plateaus will be important initial activities,<br />

followed by necessary reconstruction <strong>of</strong> quay and removal <strong>of</strong> mud from <strong>the</strong> bay.<br />

One <strong>of</strong> <strong>the</strong> rst and important steps in realization <strong>of</strong> this unique Croatian project is settlement<br />

<strong>of</strong> <strong>the</strong> neglected port area and forming <strong>of</strong> landscape and horticulturally shaped industrial<br />

area and reconstruction <strong>of</strong> quay.<br />

In order to manage <strong>the</strong> activities in Park, a social, non-prot Company for environment<br />

economy should be established, against <strong>the</strong> model <strong>of</strong> public-private partnership, as a common<br />

model <strong>of</strong> <strong>the</strong> management in eco-industrial parks.<br />

Besides institutional co-property <strong>of</strong> local community, <strong>the</strong> idea is that local inhabitants<br />

should become shareholders, and this should favor acceptance <strong>of</strong> <strong>the</strong> project and increase<br />

<strong>the</strong> possibilities for long-term successful and sustainable development <strong>of</strong> port, transport<br />

and industrial activities, as well as provide attractive benets for internal and foreign investors.<br />

The company for management <strong>of</strong> <strong>the</strong> Park will take care about <strong>the</strong> development and building<br />

<strong>of</strong> EIPR, so acting in concordance with <strong>the</strong> targets dened with this strategy will implement<br />

<strong>the</strong> model <strong>of</strong> <strong>the</strong> Park and will select <strong>the</strong> participating companies, investors and act as<br />

coordinator, manage and coordinate closely with <strong>the</strong> Community <strong>of</strong> Raša. For <strong>the</strong> success<br />

<strong>of</strong> <strong>the</strong> project it is important to clearly dene WHAT and HOW a support <strong>of</strong> <strong>the</strong> citizens<br />

should give <strong>the</strong> impulse for general development.<br />

We have to establish multidisciplinary team in <strong>the</strong> company for <strong>the</strong> management <strong>of</strong> EIPR,<br />

in which <strong>the</strong>re would participate, toge<strong>the</strong>r with <strong>the</strong> experts in branches <strong>of</strong> business, people<br />

from <strong>the</strong> executive authorities. Such expert team should, in accordance with <strong>the</strong> rules <strong>of</strong><br />

business, start working on <strong>the</strong> plan <strong>of</strong> development beginning with <strong>the</strong> denition <strong>of</strong> development<br />

targets, available human resources through <strong>the</strong> ways <strong>of</strong> its executing, from planning<br />

<strong>the</strong> future development till <strong>the</strong> preparation <strong>of</strong> <strong>the</strong> conditions for its achievement.<br />

Large amount <strong>of</strong> funds should be invested in port space design, but it should be emphasized<br />

that this project should, with wisely designed project <strong>of</strong> environment design and use<br />

<strong>of</strong> obtained material, bring prot to use in fur<strong>the</strong>r investments in space and infrastructure<br />

development <strong>of</strong> <strong>the</strong> Park. So <strong>the</strong> conditions to attract investors should be created gradually,<br />

and <strong>the</strong> interest for <strong>the</strong> project has been already shown from <strong>the</strong> investors from Austria,<br />

Italy, Sweden, Denmark and Malaysia.<br />

It should be taken into account that <strong>the</strong> Croatian economy is in big difculties: huge public<br />

debt, unemployment, <strong>the</strong> deprivation <strong>of</strong> quality <strong>of</strong> life, but also <strong>the</strong> leak <strong>of</strong> <strong>the</strong> current<br />

knowledge and skills. In such circumstances <strong>the</strong> development should be conceived considering<br />

existence and fast initialization with new economic initiatives.


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Also, it should be kept in mind that <strong>the</strong> business conditions have changed in last ten years<br />

both in Croatia and in <strong>the</strong> world. There is number <strong>of</strong> barriers in business development<br />

and creative and highly innovative business penetrations will be needed as well as wellconceived<br />

marketing, and organized care for maintaining <strong>the</strong> human resources above all.<br />

Elaboration <strong>of</strong> <strong>the</strong> program <strong>of</strong> development should be <strong>the</strong> beginning. Well-conceived projects<br />

should attract investors. It is important to emphasize that projects cannot be accomplished<br />

just through <strong>the</strong> preparation <strong>of</strong> <strong>the</strong> area <strong>of</strong> industrial zone and calling <strong>the</strong> investors<br />

to come and fulll <strong>the</strong>ir interest, which is <strong>the</strong> present Croatian practice. We should act<br />

completely different from <strong>the</strong> way it’s done actually.<br />

3.3 Projects in EIPR proposed for realization<br />

Territory <strong>of</strong> EIPR covers <strong>the</strong> port <strong>of</strong> Bršica with port area with particular accentuation on<br />

industrial microlocations: Bršica, Štalije and Vlaška, and areas surrounding port area along<br />

<strong>the</strong> river Raša and lime factory, areas along <strong>the</strong> channels to <strong>the</strong> industrial location Vlaška<br />

and <strong>the</strong> city <strong>of</strong> Raša (see picture).<br />

In <strong>the</strong> period from <strong>the</strong> establishment <strong>of</strong> Working group and presentation <strong>of</strong> <strong>the</strong> basic ideas<br />

about settlement <strong>of</strong> <strong>the</strong> eco production in port territory, <strong>the</strong> concept <strong>of</strong> <strong>the</strong> Park was gradually<br />

built. During <strong>the</strong> study based on industrial ecology as <strong>the</strong> basis <strong>of</strong> <strong>the</strong> project, different<br />

industrial, agricultural and service activities came to <strong>the</strong> surface, which could be connected<br />

in <strong>the</strong> community on <strong>the</strong> principles <strong>of</strong> modern eco industrial parks. Special<br />

attention was paid on bi<strong>of</strong>uel production based on imported raw materials, and on <strong>the</strong><br />

o<strong>the</strong>r hand <strong>the</strong> development <strong>of</strong> agricultural production on poorly tended land and processing<br />

agricultural products, as well as on waste water purication and reuse.<br />

There were various ideas about energy, production <strong>of</strong> biogas, wind power station Goli<br />

project and o<strong>the</strong>r useful and complementary ventures, in order to settle operative port and<br />

industrial synergic system.<br />

We will present <strong>the</strong> most important tasks:<br />

The building-up <strong>of</strong> <strong>the</strong> operative port and industrial surface, which will be cleaned <strong>of</strong> <strong>the</strong><br />

ruins from previous industrial period, and <strong>the</strong>n <strong>the</strong> hill between ex quarry Bršica and Štalije<br />

will be removed. For that task <strong>the</strong> Community <strong>of</strong> Raša and Port authority <strong>of</strong> Rijeka should<br />

jointly prepare <strong>the</strong> tende. Stone exploitation as building material with fur<strong>the</strong>r processing<br />

should provide important initial income for development <strong>of</strong> EIPR.<br />

Production <strong>of</strong> bi<strong>of</strong>uel on <strong>the</strong> bio-material basis<br />

Biodiesel as a modern ecological fuel guarantees good positioning <strong>of</strong> <strong>the</strong> Park and connection<br />

with o<strong>the</strong>r economies in Croatia and Middle Europe.<br />

The idea <strong>of</strong> this clue project is supported by knowledge and experience in Biodiesel production<br />

in Croatia. Croatian and foreign experts and business partners were consulted and<br />

<strong>the</strong> whole width was taken in consideration: technical, technological, microeconomics, energetic,<br />

political, organisational and markets knowledge relevant for <strong>the</strong> project realisation,<br />

Croatian, European and global situation and trends have been considered.<br />

With <strong>the</strong> increase <strong>of</strong> bioethanol use, which is mostly imported in Europe from overseas<br />

countries, it opens <strong>the</strong> possibility <strong>of</strong> logistic activity in that direction. Bioenergy business<br />

means creating nal products or semi-products, and could be realized in Štalije location,<br />

and means higher (and more protable) phase <strong>of</strong> technological development in that eld.


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Industrial power plant on bi<strong>of</strong>uels<br />

Industrial location with big production plants should have proper power plant that brings<br />

supplying security, but uses by-products from energy production plant (hot water, steam,<br />

energy power..). Considering great delicacy <strong>of</strong> <strong>the</strong> relation between electro-energy projects<br />

and environment, <strong>the</strong> particular attention was paid to <strong>the</strong> power station on bi<strong>of</strong>uel. The<br />

basic idea is that it should be exclusively in function for local society:<br />

use <strong>of</strong> biodiesel and bio-oils; „green energy“<br />

use <strong>of</strong> biogas as a product in cleaning <strong>of</strong> waste water from Raša and Labin<br />

high level <strong>of</strong> work exibility: industrial power plant<br />

netting with local heat and electric energy consumers; for example food production (greenhouses)<br />

and food processing (dryers, refrigeration plants…)<br />

Water management<br />

Raša and all Labin territory have a large quantity <strong>of</strong> water from <strong>the</strong> coal-mine galleries that<br />

could be used as technical water for irrigation in agriculture. In case it will be shown that<br />

this water could be supplied continuously in necessary clean level, it could be used as an<br />

export product for Adriatic islands and South Italy.<br />

Labin and Raša do have a problem <strong>of</strong> waste water processing, but with <strong>the</strong> use <strong>of</strong> modern<br />

technology where waste is used to produce biogas, and puried water for agricultural irrigation,<br />

we would create a system that should economically and ecologically friendly bring<br />

several benets: purication <strong>of</strong> waste water, produced energy could be used for pumping<br />

water for irrigation in agriculture, puried water could be used for irrigation, ecologically<br />

contaminated channels in valley could be cleaned and used for aquacultural production.<br />

Processing <strong>of</strong> mineral raw materials<br />

Some <strong>of</strong> Istria producers <strong>of</strong> white cement and o<strong>the</strong>r products stopped <strong>the</strong> production or<br />

have uncertain future, because <strong>of</strong> <strong>the</strong> location or lousy industrial politics. The location <strong>of</strong><br />

EIPR is by all means favorable for development <strong>of</strong> complementary production with higher<br />

level <strong>of</strong> processing <strong>of</strong> raw minerals, and means natural development through cooperation<br />

with existing factories.<br />

The micro- and nano-technology allow a wide range <strong>of</strong> products from lime-stone mineral<br />

basis and usefull in processing <strong>of</strong> plastic in food, in metallurgy, in agriculture, in medicine<br />

etc. Building development strategy in that segment is very important task in EIPR project.<br />

Agricultural production and processing<br />

There is a huge potential in vegetable and ower cultivation through modern technology.<br />

To get economically successful project <strong>the</strong> following is important: production direction and<br />

market availability, <strong>the</strong> use <strong>of</strong> new cultivating technologies, surface, quantity <strong>of</strong> production,<br />

irrigation water and irrigation system availability, costs <strong>of</strong> energy for winter period<br />

heating and for product processing, for example drying. On <strong>the</strong> o<strong>the</strong>r hand, <strong>the</strong> production<br />

and processing <strong>of</strong> industrial cultures as hemp might be very protable.<br />

The availability <strong>of</strong> waste heating from energy station might be good condition for economic<br />

success <strong>of</strong> <strong>the</strong> project. In Raša valley <strong>the</strong> conditions: water availability, as well as<br />

possibility <strong>of</strong> <strong>the</strong> building <strong>of</strong> <strong>the</strong> processing facilities for agricultural products are very<br />

good. The port and railway facilitate transportation on <strong>the</strong> market.<br />

3.4 Ecoindustrial Park and <strong>the</strong> Community <strong>of</strong> Raša<br />

Every industrial park is in interaction with its living space (surroundings) and depends on it<br />

from <strong>the</strong> point <strong>of</strong> view <strong>of</strong> natural resources, services and social development and values. It<br />

is extremely important that <strong>the</strong> cooperation and understanding <strong>of</strong> <strong>the</strong> Community’s leadership<br />

and EIPR management is established since <strong>the</strong> initial phase <strong>of</strong> EIPR. The inhabitants


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are included from <strong>the</strong> beginning through <strong>the</strong> public discussions in <strong>the</strong> project and its inuence<br />

on living space, and number <strong>of</strong> benets: contributions to <strong>the</strong> economical and social<br />

development, improvement <strong>of</strong> infrastructure, improvement <strong>of</strong> life quality are accepted as<br />

logical result.<br />

For that purpose <strong>the</strong> consultations are organized, and Forum for socially responsible teritory,<br />

which is stimulating discussions about actual problems <strong>of</strong> sustainable development <strong>of</strong><br />

<strong>the</strong> Community, has been established.<br />

EIPR will be <strong>the</strong> impulse for <strong>the</strong> development <strong>of</strong> educational institutions, and will stimulate<br />

employment and attract working force from <strong>the</strong> surroundings and <strong>the</strong>refore stimulate<br />

residential building. It leads on streng<strong>the</strong>ning and diversication <strong>of</strong> existing infrastructure<br />

and services. Social activities will be developed, cultural institutions will be built, and it is<br />

to be expected that Raša becomes a friendly place for <strong>the</strong> start <strong>of</strong> new businesses, a place<br />

with high quality <strong>of</strong> life.<br />

Following are <strong>the</strong> goals <strong>of</strong> <strong>the</strong> Project<br />

Long term goals<br />

Realisation <strong>of</strong> highly efcient and economically sustainable and efcient ecoindustrial<br />

park <strong>of</strong> manufacturing and service industries, which would be based on principles <strong>of</strong> industrial<br />

symbiosis and realizing benets for <strong>the</strong> inhabitants <strong>of</strong> Raša and Labinština.<br />

Short term goals<br />

Enterprise management in <strong>the</strong> life space and management <strong>of</strong> EIPR<br />

Environment design <strong>of</strong> EIPR, landscape and horticultural design<br />

Renewal <strong>of</strong> <strong>the</strong> transport infrastructure<br />

Renewal and equipment <strong>of</strong> port area Trget – Bršica – Štalije<br />

Management <strong>of</strong> storm water and inundation protection<br />

Ecologically efcient management with waste water from Raša and Labin and with production<br />

<strong>of</strong> biogas<br />

Processing <strong>of</strong> <strong>the</strong> mineral raw material<br />

Agricultural production and processing <strong>of</strong> agricultural products<br />

Production <strong>of</strong> bi<strong>of</strong>uel and management <strong>of</strong> bioenergy<br />

Mariculture<br />

Water from deserted mine galleries as market product<br />

Building <strong>of</strong> Marina and Wind power station Goli as collaborative projects will support ef-<br />

ciency <strong>of</strong> EIPR, so <strong>the</strong>y are considered as <strong>the</strong> additional targets<br />

The development <strong>of</strong> tourism should be designed in harmony with EIPR and leaning on<br />

original ideas and innovation as separately important target<br />

3.5 Stakeholders<br />

We will point out initial statement <strong>of</strong> <strong>the</strong> major <strong>of</strong> Raša in <strong>the</strong> publication Prosperity towards<br />

sustainable development (7):<br />

A set <strong>of</strong> synergy related projects based on production <strong>of</strong> bi<strong>of</strong>uel, management <strong>of</strong> water<br />

and agricultural production, logistic support, commodity business tailored to <strong>the</strong> needs <strong>of</strong><br />

development <strong>of</strong> <strong>the</strong> Community <strong>of</strong> Raša, Istria and Croatia is in complete spirit <strong>of</strong> strategy<br />

<strong>of</strong> EU and Croatia on realisation <strong>of</strong> sustainable development, energy ef ciency and protection<br />

<strong>of</strong> nature with reduction <strong>of</strong> emission. The program will be realized with emphasis on<br />

practice <strong>of</strong> public – private partnership and is consistent with Croatian strategy <strong>of</strong> export<br />

support, and is its important contribution. Local community, Labin area and Istria are<br />

naturally interested for good solutions in activating <strong>the</strong> port <strong>of</strong> Raša, for use <strong>of</strong> industrial<br />

areas and for <strong>the</strong> prosperity <strong>of</strong> <strong>the</strong> economy in that space.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 131<br />

Local entities that are leaning on available resources (raw material, water, energy, transport)<br />

with this project will gain great developing impulse and support, and location and<br />

market advantages that ensure <strong>the</strong> future prosperity.<br />

Republic <strong>of</strong> Croatia with this project will gain a rounded conception <strong>of</strong> development <strong>of</strong> <strong>the</strong><br />

ports in basin <strong>of</strong> Rijeka, <strong>the</strong> solution for neglected port <strong>of</strong> Raša and impulses for <strong>the</strong> development<br />

<strong>of</strong> <strong>the</strong> rail transport route on <strong>the</strong> eastern part <strong>of</strong> Uka-mountain.<br />

In Middle European area <strong>the</strong> interest for port <strong>of</strong> Raša exists as <strong>the</strong> port specialized for<br />

biomaterial with <strong>the</strong> possibility for <strong>the</strong>ir processing in area settled for industrial plants.<br />

The main reason for such thinking is <strong>the</strong> fact that in o<strong>the</strong>r north Adriatic ports <strong>the</strong>re is no<br />

possibility to accept additional liquid cargo and to supply big biodiesel plants in middle<br />

Europe with vegetable oils, <strong>the</strong>re is a need for sea transport, as well as for supplement <strong>of</strong><br />

bi<strong>of</strong>uel (biodiesel, ethanol). The interest for <strong>the</strong> port <strong>of</strong> Raša has been shown from <strong>the</strong><br />

entrepreneurs from Italy and several Asiatic countries, especially from Malaysia and India.<br />

3.6 Knowledge and experience on which venture relies<br />

The suggested strategy is based on <strong>the</strong> synergy <strong>of</strong> knowledge and experience <strong>of</strong> <strong>the</strong>ir authors,<br />

who participated as individuals in number <strong>of</strong> projects and solved number <strong>of</strong> <strong>engineering</strong><br />

and economic development tasks.<br />

We should emphasize <strong>the</strong> knowledge and experience by which <strong>the</strong> mayor <strong>of</strong> Raša supported<br />

<strong>the</strong> designing <strong>of</strong> <strong>the</strong> strategy, because knowing local society and its wide environment is<br />

especially important for strategy development.<br />

All this knowledge and experience has been implemented in <strong>the</strong> idea <strong>of</strong> this strategy. There<br />

exist huge literature dedicated to development and building <strong>of</strong> ecoindustrial parks, but it<br />

can be understood and implemented just with wide experience and understanding <strong>of</strong> systemic<br />

thinking.<br />

4 Ecoindustrial Park Raša – EIPR - realization<br />

4.1 The way <strong>of</strong> achieving realization <strong>of</strong> EIPR<br />

Good cooperation <strong>of</strong> interested institutions, economic entities and management through<br />

<strong>the</strong> activity <strong>of</strong> Working group, Forum for socially responsible activity and public presentations<br />

and discussions, as well as good cooperation with Croatian System Society, form <strong>the</strong><br />

basis <strong>of</strong> friendly surroundings for realization <strong>of</strong> <strong>the</strong> project EIPR.<br />

Everything mentioned above, toge<strong>the</strong>r with learned experiences, particular knowledge and<br />

information, as well as ga<strong>the</strong>red circle <strong>of</strong> experts, constitutes <strong>the</strong> intellectual capital without<br />

which would it be impossible to initiate realization <strong>of</strong> <strong>the</strong> project EIPR on <strong>the</strong> current<br />

cognitive and project level.<br />

The idea is for <strong>the</strong> Working group to continue its activity as a part <strong>of</strong> expert advisory panel<br />

<strong>of</strong> <strong>the</strong> company for <strong>the</strong> economy in life space and EIPR management.<br />

The rst development task is appointment <strong>of</strong> project manager and establishment <strong>of</strong> <strong>the</strong><br />

management <strong>of</strong> Ecoindustrial Park <strong>of</strong> Raša. This rst in order <strong>of</strong> priority tasks will realize<br />

<strong>the</strong> Working group for strategy <strong>of</strong> development in cooperation with <strong>the</strong><br />

Community <strong>of</strong> Raša and will create a multidisciplinary body – Expert working group or<br />

Expert advisory council <strong>of</strong> appropriate size and competence. It will be a support to <strong>the</strong> project<br />

manager (leader) and will jointly establish and operate <strong>the</strong> Park management. Expert<br />

working group will continue with technical work, dene methodology <strong>of</strong> work, and prepare<br />

necessary documentation and detailed operational plan. Toge<strong>the</strong>r with <strong>the</strong> Forum for<br />

socially responsible activity will promote <strong>the</strong> idea <strong>of</strong> EIPR and report to <strong>the</strong> public about


132<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

progress <strong>of</strong> activities. With <strong>the</strong> progress and raise <strong>of</strong> EIPR it will be established consortium<br />

<strong>of</strong> companies, members <strong>of</strong> Park, which will be important support to <strong>the</strong> activity <strong>of</strong> Park<br />

management.<br />

4.2 Economy <strong>of</strong> <strong>the</strong> project EIPR<br />

Generally it can be predicted that potential <strong>of</strong> <strong>the</strong> space and suggested projects expressed<br />

as an <strong>annual</strong> income is around 200 million €.<br />

In different phases <strong>of</strong> realization <strong>of</strong> EIPR <strong>the</strong> projects need different amount <strong>of</strong> funds, in<br />

relation with actual structure <strong>of</strong> project realization, and are provided from public and private<br />

sources.<br />

In initial activities <strong>the</strong> needs for funds generally are:<br />

execution <strong>of</strong> Preliminary feasibility studies and preliminary <strong>engineering</strong> studies<br />

execution <strong>of</strong> EIP’s infrastructure and marketing activities for attraction <strong>of</strong> investors<br />

execution <strong>of</strong> possible pilot-plant and building <strong>of</strong> objects for initial settlement <strong>of</strong> entrepreneurs<br />

in rent<br />

establishment <strong>of</strong> <strong>the</strong> institutions that support development <strong>of</strong> EIP, as business incubators<br />

and development centers<br />

activities with which local / wider community supports <strong>the</strong> development <strong>of</strong> EIP and acts in<br />

accordance with projected targets<br />

The idea <strong>of</strong> EIPR could be realized if foreign investors with capital are attracted, that will<br />

be driving force <strong>of</strong> <strong>the</strong> project. It should also be considered nancing from EU and Croatian<br />

funds.<br />

4.3 Risks<br />

The hardest thing is to predict, minimize and solve potential risks that could endanger<br />

project. But risk is a part <strong>of</strong> every day’s life and <strong>the</strong> causes should be individuated and separated.<br />

The suggested project is complex and includes number <strong>of</strong> subprojects and <strong>the</strong>refore<br />

different risk causes. We are listing <strong>the</strong> more important possible causes, and in more detailed<br />

way <strong>the</strong> causes will be analyzed during <strong>the</strong> elaboration <strong>of</strong> <strong>the</strong> singular project tasks:<br />

<strong>the</strong> success <strong>of</strong> <strong>the</strong> management <strong>of</strong> <strong>the</strong> EIPR<br />

careful choice <strong>of</strong> collaborative companies<br />

non favorable economic circumstances<br />

competition inuence<br />

Investors are loath to <strong>the</strong> risks, so it is important to decrease <strong>the</strong>ir exposure to <strong>the</strong> risks<br />

through wisely dened conditions <strong>of</strong> investments. Let’s emphasize that, for example, public<br />

private partnership cannot signicantly decrease exposure to risks, but <strong>the</strong>re are several<br />

o<strong>the</strong>r useful approaches <strong>of</strong> decreasing risks that should be examined.<br />

Thinking <strong>the</strong> past and <strong>the</strong> present we cannot think good enough and live <strong>the</strong> already present<br />

future: informatic, biotechnological, nanotechnological that has already begun in highly<br />

developed countries greatly progressed and moved away. Is it possible to think and organize<br />

overcoming <strong>of</strong> <strong>the</strong> technical gap?<br />

Therefore positive thinking should be promoted, which is focused to <strong>the</strong> future, creativeness<br />

and permanent innovation, <strong>the</strong> understanding <strong>of</strong> our exible and creative abilities; it<br />

should wisely be open to <strong>the</strong> most developed world and its permanently changeable life.<br />

Let’s point that <strong>the</strong> old saying which states that mental blockade is <strong>the</strong> biggest obstacle on<br />

progress towards <strong>the</strong> future is true that is so called „embedded human resistance against<br />

anything new“, and <strong>the</strong> Europeans are <strong>the</strong> biggest slaves <strong>of</strong> such resistance and <strong>the</strong>ir lag<br />

behind Americans and Japanese is partly caused because <strong>of</strong> it. We are Europeans as well,


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 133<br />

and we also carry this defect, not so much when spending is concerned, but true when it<br />

concerns work and production. We hardly see <strong>the</strong> embryo <strong>of</strong> big changes, and <strong>the</strong>refore we<br />

defer too late. As a useful example we should examine <strong>the</strong> unsuccessful Lisabon strategy<br />

because <strong>of</strong> which EU Council in 2000 thought EU as „<strong>the</strong> most dynamic and competitive<br />

economy on <strong>the</strong> world…“ and <strong>the</strong> majority <strong>of</strong> targets was not reached till <strong>the</strong> predicted<br />

data, <strong>2010</strong> year.<br />

European culture is one <strong>of</strong> <strong>the</strong> basic risks to <strong>the</strong> possible success <strong>of</strong> our project, and we<br />

can list number <strong>of</strong> o<strong>the</strong>rs. In <strong>the</strong> rst line <strong>the</strong>re is <strong>the</strong> possibility <strong>of</strong> initial nancing <strong>of</strong> <strong>the</strong><br />

venture, understanding <strong>of</strong> <strong>the</strong> surroundings, choice <strong>of</strong> <strong>the</strong> project management, <strong>the</strong>n understanding<br />

<strong>of</strong> <strong>the</strong> surrounding community about <strong>the</strong> need <strong>of</strong> its achievement.<br />

4.4 Development effects achieved with EIPR<br />

On macro plan - Excellently organized community <strong>of</strong> producing agricultural and service<br />

activities taking care <strong>of</strong> industrial ecology by principles <strong>of</strong> ecoindustrial park, dependent<br />

on highly developed infrastructure: sea, road, rail and air.<br />

On micro plan - Support to <strong>the</strong> sustainable development <strong>of</strong> <strong>the</strong> living space and economy<br />

<strong>of</strong> <strong>the</strong> Community <strong>of</strong> Raša, employment and rich social life, work and family life, achieving<br />

reputation <strong>of</strong> <strong>the</strong> place <strong>of</strong> possible business success and quality <strong>of</strong> life.<br />

4.5 Priority tasks<br />

Realization <strong>of</strong> <strong>the</strong> whole EIPR project, as well as partial project courses inside <strong>of</strong> <strong>the</strong> system<br />

starts with <strong>the</strong> realization <strong>of</strong> project documentation and forming <strong>of</strong> singular project<br />

courses with all <strong>the</strong> necessary elements explained that are needed for initiate <strong>the</strong> realization,<br />

as it is used in pr<strong>of</strong>ession. We are mentioning here <strong>the</strong> tasks that should be executed<br />

in short term period, in order to initiate <strong>the</strong> project:<br />

Preliminary project management with life space EIPR and coordination <strong>of</strong> activities<br />

Conceptual space design planning in EIPR<br />

Preliminary project <strong>of</strong> restoring and furnishing <strong>of</strong> <strong>the</strong> Port <strong>of</strong> Raša<br />

Preliminary project <strong>of</strong> activity and management with waste water from Labin and Raša<br />

Preliminary project <strong>of</strong> Cluster for <strong>the</strong> processing <strong>of</strong> <strong>the</strong> mineral raw material<br />

Preliminary project <strong>of</strong> agricultural production<br />

5 Conclusion<br />

The above described idea <strong>of</strong> sustainable development <strong>of</strong> <strong>the</strong> Community <strong>of</strong> Raša and<br />

preparations for development <strong>of</strong> <strong>the</strong> Ecoindustrial Park <strong>of</strong> Raša, as well as description <strong>of</strong><br />

circumstances in which <strong>the</strong> development tasks should be accomplished, tell us about a vision<br />

<strong>of</strong> a Park as rst such Croatian venture: with wise management it can become widely<br />

recognized and accepted successful business model.<br />

During <strong>the</strong> deliberation <strong>of</strong> <strong>the</strong> Strategy <strong>of</strong> development <strong>of</strong> port area Raša points <strong>of</strong> view<br />

were dened, that are starting points <strong>of</strong> sustainable development and with which development<br />

projects and activities should harmonize:<br />

System <strong>of</strong> projects thought on <strong>the</strong> basis <strong>of</strong> space, natural, infrastructural and technological<br />

resources<br />

Activating <strong>of</strong> <strong>the</strong> port <strong>of</strong> Raša and port area <strong>of</strong> Raša and its surroundings, as „anchorage“<br />

<strong>of</strong> EIPR, that will through specializing operations have advantage to <strong>the</strong> o<strong>the</strong>r ports <strong>of</strong><br />

Nor<strong>the</strong>rn Adriatic.<br />

Planned activities in port area won’t disturb o<strong>the</strong>r development projects in spaces or tour-


134<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

istic programs<br />

The area <strong>of</strong> EIPR will be designed by cleaning <strong>of</strong> <strong>the</strong> remained ruins from previous industrial<br />

periods and o<strong>the</strong>r activities (Bršica, Štalije, Vlaška, agricultural land along channel3)<br />

and by removing <strong>the</strong> stones (hill) between <strong>the</strong> deserted stone mine Bršica and Štalije area<br />

operational and industrial space will be formed.<br />

The basis is created for <strong>the</strong> development <strong>of</strong> strategically important and clean activities, <strong>the</strong><br />

production that will in good way place Raša in regional environment (transport, bioenergy,<br />

food, water).<br />

Realization <strong>of</strong> <strong>the</strong> exemplary management with water: storm water and inundation protection,<br />

using <strong>the</strong> water from mine galleries from Raša and Labin, and <strong>the</strong> water from purication<br />

<strong>of</strong> waste water.<br />

It predicts netted system <strong>of</strong> energy management with emphasis on renewable sources <strong>of</strong><br />

energy (biodiesel, biogas, wind power stations)<br />

Revitalisation and realization <strong>of</strong> ecological agricultural production in <strong>the</strong> valley <strong>of</strong> Raša,<br />

considering good climatic conditions, availability <strong>of</strong> water, energetic and o<strong>the</strong>r support <strong>of</strong><br />

industrial systems<br />

Compliance to <strong>the</strong> rigorous norms <strong>of</strong> landscape conservation should harmonize with touristic<br />

activity and harmony with landscape beauty in nearby area.<br />

Realization <strong>of</strong> EIPR project follows usual procedure and phases <strong>of</strong> development for such<br />

project with predicted tasks and subprojects have to be realized:<br />

Company for space management (PGP) and management <strong>of</strong> EIPR<br />

Designing <strong>the</strong> space <strong>of</strong> EIPR: functional, landscape and horticultural design<br />

Renewal <strong>of</strong> trafc infrastructure<br />

Renewal and furnishing <strong>of</strong> <strong>the</strong> port-area Bršica-Štalije<br />

Management <strong>of</strong> storm water and inundation protection<br />

Ecologically efcient treatment <strong>of</strong> waste water from Labin and Raša with biogas production<br />

Basis for forming <strong>of</strong> a Cluster for mineral raw material processing and strategy <strong>of</strong> development<br />

in that segment<br />

Agricultural production and processing <strong>of</strong> agricultural products<br />

Production <strong>of</strong> bi<strong>of</strong>uel and management <strong>of</strong> bio energy<br />

Mariculture<br />

Water from deserted mine galleries as market product<br />

Building <strong>of</strong> marina and wind power station Goli as collaborative projects that would be<br />

supportive to <strong>the</strong> success <strong>of</strong> EIPR, so are emphasized as possible additional targets<br />

Realization <strong>of</strong> <strong>the</strong> whole project EIPR as well as singular units inside <strong>the</strong> Park will start<br />

with design <strong>of</strong> project documentation.<br />

6 References<br />

1. Andrašec M. (2009), Tehnologijske platforme, hrvatski razvojni projekti u EU<br />

okruženju. In: Božievi J. (eds) Inovacijska kultura i tehnologijski razvoj, CROSS,<br />

Zagreb, pp 109-114<br />

2. Baas L. (2008), Industrial Symbiosis in <strong>the</strong> Rotterdam Harbour and Industrial Complex,<br />

Bus. Strat. Env 17, pp 330-340<br />

3. Božicevic J. (1993), Private communication, Zagreb<br />

4. Božievi J. (ed) (1999), Luka kao složen sustav, Rijeka – glavna hrvatska luka,<br />

<strong>HATZ</strong>-CROSS, Zagreb


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 135<br />

5. Božievi J. (ed) (1999), Povezani Rijeka i Zagreb hrvatsko i europsko gospodarsko<br />

žarište, <strong>HATZ</strong>, Zagreb<br />

6. Božievi J., Andrašec M. (2009), Opina Raša – Mudra zajednica, Opina Raša,<br />

Raša<br />

7. Božievi J., Andrašec M. (2009), Napredak prema održivom razvoju, Opina Raša,<br />

Raša<br />

8. Doyle B. et al. (1996), Eco-industrial Parks, TRI, Research Triangle Park, NC, USA<br />

9. Fleig A. K. (2000), Eco industrial Parks, Deutsche Gesellschaft fur Technische Zusamanarbeit<br />

GmbH, Eschborn, Deutschland<br />

10. Lowe E. A. (2001), Eco-industrial Park Handbook for Asian Developing Countries,<br />

Report to Asian Development Bank, Indigo Development, Hidden Valley Lake, CA,<br />

USA<br />

11. Koenig A.W. (ed.) (2005), The Eco-Industrial Park Development, A Guide for Chinese<br />

Government Ofcials and Industrial Park Managers, EU-China Environmental<br />

Management Cooperation Programme - Industry Development, Beijing<br />

12. Tarantini M., Paolo A., Dominici A., Peruzzi A., Dell’Isola M. (2007), Guidelines for<br />

<strong>the</strong> Settlement and <strong>the</strong> Management <strong>of</strong> <strong>the</strong> Sustainable Industrial Areas, The Experience<br />

<strong>of</strong> <strong>the</strong> LIFE SIAM Project, Bologna


136<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

POSIBLE MODEL OF MATHEMATICAL EVALUATION OF<br />

BEHAVIOUR DISORDER THERAPY<br />

Pr<strong>of</strong>. Dr. sc. Marijan Bošnjak, retired;<br />

member emeritus <strong>of</strong> Croatian Academy <strong>of</strong> Engineering (<strong>HATZ</strong>),<br />

HR-10000 Zagreb, Croatia;<br />

Summary<br />

Because <strong>of</strong> enormous complexity <strong>of</strong> mental and behavioural disorders and illnesses <strong>the</strong>re<br />

is still continuous need for fur<strong>the</strong>r advances in <strong>the</strong>ir treatment. Treatment frequently asks<br />

<strong>the</strong> application <strong>of</strong> chemo<strong>the</strong>rapeutic agents in addition to o<strong>the</strong>r conventional <strong>the</strong>rapeutic<br />

actions. The effects <strong>of</strong> treatments should be adequately evaluated. In this work special<br />

emphasis is given to medical treatments when chemo<strong>the</strong>rapeutic agents are applied.<br />

Therefore, <strong>the</strong> major importance was given to chemo<strong>the</strong>rapeutic agent pharmacokinetics.<br />

Consequently, <strong>the</strong> ma<strong>the</strong>matical model composed from more than twenty differential<br />

equations was applied to describe pharmacokinetics <strong>of</strong> chemo<strong>the</strong>rapeutic agent distribution<br />

in human body, kinetics <strong>of</strong> development <strong>of</strong> positive and negative effects <strong>of</strong> applied<br />

chemo<strong>the</strong>rapeutic treatment, effects on body viability and development <strong>of</strong> compounds<br />

inhibiting <strong>the</strong> effects <strong>of</strong> present chemo-<strong>the</strong>rapeutic agent and causing <strong>the</strong> organism<br />

dependence on applied substances. Computer simulation was applied to test ma<strong>the</strong>matical<br />

model convenience. Obtained computer simulation data con rmed <strong>the</strong> model adequacy<br />

suggesting its application in explaining real cases <strong>of</strong> combined psycho<strong>the</strong>rapy treatments.<br />

Special convenience <strong>of</strong> proposed ma<strong>the</strong>matical model type showed to be its con rmation<br />

<strong>of</strong> necessity for controlling chemo<strong>the</strong>rapeutic substance distribution in bodies <strong>of</strong> treated<br />

patients as a prerequisite for more reliable successful patient treatments with reduced<br />

accompanied negative side effects.<br />

Key words: Psycho<strong>the</strong>rapy pharmacokinetics. Ma<strong>the</strong>matical modelling. Computer<br />

simulation application.<br />

1 Introduction<br />

Despite <strong>the</strong> evident advances in discovering <strong>the</strong> causes <strong>of</strong> mental and behavioural disorders<br />

and illnesses as well as in increasing <strong>the</strong> frequency <strong>of</strong> successful patient disorder and<br />

illness treatments, resulting in patient recoveries, <strong>the</strong>re is still continuous need for fur<strong>the</strong>r<br />

advances in this area <strong>of</strong> medicine, because <strong>of</strong> enormous complexity <strong>of</strong> problems asking to<br />

be successfully solved. One <strong>of</strong> important prerequisites for fur<strong>the</strong>r advances appears to be<br />

<strong>the</strong> application <strong>of</strong> appropriate approaches to <strong>the</strong> evaluation <strong>of</strong> results <strong>of</strong> medical treatments.<br />

Some consequences (positive and/or negative) <strong>of</strong> applied medical treatment can appear<br />

even very fast after its start, <strong>the</strong> o<strong>the</strong>rs one can observe much later, whereas it can also<br />

happen that <strong>the</strong> desired effects cannot appear at all. Of course, <strong>the</strong> best situation can be<br />

considered that when desired positive effects appear already during <strong>the</strong> beginning phase <strong>of</strong><br />

medical treatment.<br />

Since, in addition to direct communications <strong>of</strong> psychiatrists and employed personnel with<br />

patients <strong>the</strong> psycho<strong>the</strong>rapy includes also different psychophysical activities and frequently


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 137<br />

an application <strong>of</strong> chemo<strong>the</strong>rapeutic agents, <strong>the</strong> particular effects <strong>of</strong> all mentioned <strong>the</strong>rapeutic<br />

actions should be appropriately evaluated prior to <strong>the</strong> conclusions referring to <strong>the</strong> answer<br />

on <strong>the</strong> question whe<strong>the</strong>r <strong>the</strong> applied <strong>the</strong>rapy was adequate and whe<strong>the</strong>r it can be considered<br />

as successful with respect to patient recovery and his health improvement.<br />

This work refers to an attempt <strong>of</strong> advancing medical treatment by developing <strong>the</strong> one <strong>of</strong><br />

possible models for ma<strong>the</strong>matical evaluation <strong>of</strong> results <strong>of</strong> applied psycho<strong>the</strong>rapy. Although<br />

<strong>the</strong> present approach to <strong>the</strong> development <strong>of</strong> ma<strong>the</strong>matical model does not neglect a decisive<br />

role <strong>of</strong> engaged psychiatrists and o<strong>the</strong>r pr<strong>of</strong>essional persons, <strong>the</strong> emphasis is given to <strong>the</strong><br />

role <strong>of</strong> applied chemo<strong>the</strong>rapeutic agents and <strong>the</strong>ir effects on patients subjected to <strong>the</strong><br />

<strong>the</strong>rapy. The impression based on <strong>the</strong> real practice <strong>of</strong> neglecting <strong>the</strong> relevance for assaying<br />

or estimating amounts <strong>of</strong> chemo<strong>the</strong>rapeutic agents in particular compartments <strong>of</strong> patient<br />

body (mainly caused by nancial reasons) provoked such an orientation to ma<strong>the</strong>matical<br />

modelling.<br />

2 Ma<strong>the</strong>matical modelling<br />

2.1 Development <strong>of</strong> fundamental model<br />

As already long time known 1, 2, 10, 14, different approaches to <strong>the</strong> ma<strong>the</strong>matical<br />

modelling <strong>of</strong> biochemical reaction systems can be applied. In <strong>the</strong> case <strong>of</strong> biological<br />

systems <strong>the</strong> frequent practice is to describe <strong>the</strong>m by systems <strong>of</strong> differential equations 1-<br />

10, 12-15. These can be relatively simple (composed from 2 – 3 differential equations)<br />

or complex ones characterised with series <strong>of</strong> differential equations. Commonly, <strong>the</strong> simple<br />

systems <strong>of</strong> differential equations can be solved analytically or by applying computer<br />

simulation, whereas for complex systems <strong>the</strong> best choice appears to be <strong>the</strong> application<br />

<strong>of</strong> computer simulations. As pointed out in recent publication 2A, <strong>the</strong> whole system <strong>of</strong><br />

human organism certainly is so complex that one can consider illusory to expect that one<br />

can perfectly describe it by adequate ma<strong>the</strong>matical model. It is also pointed out that <strong>the</strong><br />

accepted practice became <strong>the</strong> description only <strong>of</strong> parts <strong>of</strong> realty and mainly more or less<br />

approximately. Consequently, process events in live organisms can be described by series<br />

<strong>of</strong> appropriate differential equations, as demonstrated with reference to microbial cells<br />

and/or microbial biomass 2-6, 8-10, 12-15 and specically with reference to mammalian<br />

bodies 2, 8, 9, 15. The data published recently 2 could be considered to be <strong>the</strong> most<br />

relevant ones in forming <strong>the</strong> ma<strong>the</strong>matical model <strong>of</strong> this work.<br />

Prior to <strong>the</strong> beginning <strong>of</strong> possible ma<strong>the</strong>matical model formation one should select and<br />

group <strong>the</strong> most relevant patient body process events assumed to happen during <strong>the</strong> applied<br />

<strong>the</strong>rapy and to indicate (at least roughly) <strong>the</strong> most probable <strong>the</strong>rapy consequences. In<br />

any case <strong>the</strong> <strong>the</strong>rapy effects on patient survival and viability maintenance should not be<br />

neglected in forming a ma<strong>the</strong>matical model. The emphasis given to <strong>the</strong> evaluation <strong>of</strong> applied<br />

chemo<strong>the</strong>rapeutic agent effects asks a more detailed consideration <strong>of</strong> chemo<strong>the</strong>rapeutic<br />

agent pharmacokinetics. Data and explanations expressed in <strong>the</strong> recent work 2A suggest<br />

a similar approach in this work.<br />

Usual practice is to apply chemo<strong>the</strong>rapeutic agents orally, although in some cases a<br />

parenteral application can be recommended. When applying chemo<strong>the</strong>rapeutic agents<br />

orally one <strong>of</strong> possibilities is to consider that ventricular-intestinal organism compartment<br />

is composed from two sub-compartments. Then one can start ma<strong>the</strong>matical modelling by<br />

putting differential equations:<br />

dF ve<br />

/dt =-k 1<br />

F ve<br />

/1/


138<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

dF it<br />

/dt =k 1<br />

F ve<br />

–k 2<br />

F it<br />

–k 3<br />

F it<br />

/2/<br />

if neglecting chemo<strong>the</strong>rapeutic drug resorption rate value in ventricular part (Such<br />

oversimplication cannot be recommended in every case), and if supposing that some part<br />

<strong>of</strong> drug would be excreted through faeces, i. e. if one can apply <strong>the</strong> equation<br />

dF fc<br />

/dt =k 2<br />

F it<br />

/3/<br />

If, however, a chemo<strong>the</strong>rapeutic agent resorption rate is enough signicant already in<br />

ventricular part, <strong>the</strong>n instead <strong>of</strong> equation /1/ <strong>the</strong> following equation should be applied:<br />

dF ve<br />

/dt =-k 1<br />

F ve<br />

–aF ve<br />

/1a/<br />

All organism parts are interconnected adequately and <strong>the</strong>refore communication between<br />

<strong>the</strong>m is well established when one considers normal viable organism. However, with<br />

respect to organism survival and communications between organism parts <strong>the</strong> main role<br />

could be assigned to <strong>the</strong> cardio-vascular system and its connection with respiratory system,<br />

if respecting <strong>the</strong> control role <strong>of</strong> cerebral-neural system.<br />

Since <strong>the</strong> blood communicates with all organism compartments <strong>the</strong> rate <strong>of</strong> changes <strong>of</strong><br />

chemo<strong>the</strong>rapeutic drug mass in <strong>the</strong> blood could be expressed by equation<br />

dF sng<br />

/dt =k 3<br />

F it<br />

–(k 4<br />

+k 6<br />

+k 7<br />

+k 9<br />

+k k<br />

) F sng<br />

+k 5<br />

F cr<br />

+k 8<br />

F hp<br />

+k a<br />

F t<br />

+<br />

+k i<br />

F men<br />

/4/<br />

or by equation<br />

dF sng<br />

/dt =a F ve<br />

+k 3<br />

F it<br />

–(k 4<br />

+k 6<br />

+k 7<br />

+k 9<br />

+k k<br />

) F sng<br />

+k 5<br />

F cr<br />

+k 8<br />

F hp<br />

+k a<br />

F t<br />

+<br />

+k i<br />

F men<br />

/4a/<br />

Communication with nephritic-urinary system is mainly irreversible and <strong>the</strong>refore drug<br />

transfer rate towards this system can be presented by applying <strong>the</strong> equation<br />

dF nu<br />

/dt =k 6<br />

F sng<br />

/5/<br />

The liver has important role and communicates reversibly with blood. The equation<br />

dF hp<br />

/dt =k 7<br />

F sng<br />

–k 8<br />

F hp<br />

/6/<br />

is considered to be ma<strong>the</strong>matically adequate.<br />

For <strong>the</strong> main part <strong>of</strong> tissue one can apply <strong>the</strong> equations:<br />

dF t<br />

/dt =k 9<br />

F sng<br />

–(k a<br />

+k d<br />

) F t<br />

+k e<br />

F tr<br />

/7/<br />

dF tr<br />

/dt =k d<br />

F t<br />

–k e<br />

F tr<br />

/8/<br />

if drug transfer to tissue receptor happens reversibly.<br />

The hearth communicates reversibly with <strong>the</strong> blood, as <strong>the</strong> engine <strong>of</strong> blood circulation<br />

and as <strong>the</strong> main part <strong>of</strong> cardio-vascular system. Its reversible communication with <strong>the</strong>


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 139<br />

respiratory system is necessary and is a prerequisite <strong>of</strong> body survival. The equations<br />

and<br />

dF cr<br />

/dt =k 4<br />

F sng<br />

–(k 5<br />

+k b<br />

) F cr<br />

+k c<br />

F rsp<br />

/9/<br />

dF rsp<br />

/dt =k b<br />

F cr<br />

–k c<br />

F rsp<br />

/10/<br />

appear to be adequate for application.<br />

Cerebral-neural and consequently mental system should be obligatorily considered. The<br />

rate <strong>of</strong> changes <strong>of</strong> drug amount in this system can be represented by equation<br />

dF men<br />

/dt =k k<br />

F sng<br />

–k i<br />

F men<br />

/11/<br />

Presence <strong>of</strong> chemo<strong>the</strong>rapeutic substance in <strong>the</strong> cerebral-neural system can induce positive<br />

and/or negative effects inuencing <strong>the</strong>ir intensities. One <strong>of</strong> possibilities to express <strong>the</strong>se<br />

consequences could be by applying <strong>the</strong> equations<br />

dMenp/dt =k u<br />

F men<br />

(1-Menp/Mpm) /12/<br />

dMenn/dt =k v<br />

F men<br />

(1-Menn/Mnm) /13/<br />

Equations /12/ and /13/ determine <strong>the</strong> maximal values which can be attained during<br />

medication, if neglecting <strong>the</strong> probable inhibitory effects <strong>of</strong> increased F men<br />

quantities. Since<br />

it is much more probable that <strong>the</strong> inhibitory effects would reect ra<strong>the</strong>r on positive than<br />

negative consequences, it seems to be sufcient to modify <strong>the</strong> equation /12/ with taking<br />

into account inhibitory effects <strong>of</strong> increasing F men<br />

quantities. The equation,<br />

dMenp/dt =k u<br />

F men<br />

(1-fF men<br />

-Menp/Mpm)<br />

/12a/<br />

can be considered adequate one for an explanation <strong>of</strong> expected consequences.<br />

The experience and experts recommendations concerning <strong>the</strong> application <strong>of</strong> chemo<strong>the</strong>rapeutic<br />

agents in psycho<strong>the</strong>rapy suggest us to be cautious, especially in cases <strong>of</strong> longterm<br />

<strong>the</strong>ir application. As mentioned recently 7, none <strong>of</strong> known antipsychotics used to<br />

treat patients is quite adequate. Those called <strong>the</strong> typical antipsychotics are regarded as<br />

efcacious at ameliorating positive symptoms, but generally ineffective against negative<br />

symptoms and with accompanied displaying <strong>of</strong> extra-pyramidal side effects. Atypical<br />

antipsychotics are also ineffective against negative symptoms. Therefore, one should<br />

consider possible negative effects <strong>of</strong> applied chemical substances on organism body <strong>of</strong><br />

patients subjected to psycho<strong>the</strong>rapy. One <strong>of</strong> ways <strong>of</strong> evaluating <strong>the</strong> consequences is by<br />

estimating values <strong>of</strong> arbitrarily dened body viability, Bv, and body non-viability, Bnv. In<br />

present approach it is supposed that differential equations<br />

dB v<br />

/dt =-k s<br />

.B v<br />

F sng<br />

+k r<br />

S rv<br />

B nv<br />

/14/<br />

dB nv<br />

/dt =k s<br />

B v<br />

F sng<br />

–k r<br />

S rv<br />

B nv<br />

/15/<br />

dS rv<br />

/dt =-k r<br />

S rv<br />

B nv<br />

+k rv<br />

(1-S rv<br />

) /16/


140<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

can serve adequately to such a purpose, if one considers that live organism by his metabolism<br />

supplies continuously <strong>the</strong> own body with energy and appropriate substances in necessary<br />

amounts for survival, and that “revitalization substrate”, S rv<br />

, as <strong>the</strong> notion represents <strong>the</strong>m.<br />

The effects <strong>of</strong> psycho<strong>the</strong>rapy on patient recovery and his health improvement should be<br />

evaluated. However, one cannot say that actually reliable and exactly dened methods are<br />

applied systematically. Therefore, every attempt in approaching to <strong>the</strong> problem solution<br />

can be useful. One <strong>of</strong> possibilities seems to be by proposing <strong>the</strong> ma<strong>the</strong>matical expression<br />

in which <strong>the</strong> recognised effects are considered with respect to <strong>the</strong> participation <strong>of</strong><br />

particular factors <strong>of</strong> inuence. No doubt, both <strong>the</strong> efciency <strong>of</strong> psychiatrists and employed<br />

pr<strong>of</strong>essional personnel and effects <strong>of</strong> applied chemo<strong>the</strong>rapeutic substances should be<br />

evaluated on appropriate ways. As <strong>the</strong> rst step in searching an acceptable ma<strong>the</strong>matical<br />

model could be <strong>the</strong> investigation <strong>of</strong> application convenience <strong>of</strong> equations<br />

dPs/dt =z(1-Ps) /17/<br />

dUt/dt =wPs+xMenp-yMenn /18/<br />

Since <strong>the</strong> decision on <strong>the</strong> choice and dosing psycho<strong>the</strong>rapeutic agents essentially depends<br />

on psychiatrists, perhaps it is more adequate instead <strong>of</strong> equation /17/ to apply <strong>the</strong> equation<br />

dPs/dt =z(1-Ps)(1+Menp)/(1+Menn)<br />

/17a/<br />

The idea to propose equations /17/, /17a/ and /18/ is based on <strong>the</strong> assumption that engaged<br />

psychiatrists and pr<strong>of</strong>essional personnel are ethically and by <strong>the</strong>ir education and experience<br />

quite adequate to act efciently in positive sense. It is also supposed that both positive and<br />

negative consequences should be evaluated, primarily without an investigation whe<strong>the</strong>r <strong>the</strong><br />

applied chemo<strong>the</strong>rapeutic agent acts as reaction substance in biochemical processes or as<br />

signal substance inducing <strong>the</strong> biochemical processes which lead to desired patient behaviour<br />

and health improvements. Although <strong>the</strong>re is series <strong>of</strong> o<strong>the</strong>r factors playing important roles<br />

in people <strong>the</strong>rapies (religion, meteorological factors, environmental conditions in general,<br />

etc.), <strong>the</strong> evaluation <strong>of</strong> consequences <strong>of</strong> <strong>the</strong>ir inuence cannot be recommended for detailed<br />

consideration in this work, because <strong>of</strong> actual insufcient knowledge to dene and estimate<br />

exactly <strong>the</strong> effects <strong>of</strong> <strong>the</strong>ir inuence.<br />

2.2 Modelling <strong>of</strong> <strong>the</strong> development <strong>of</strong> organism dependence on applied drugs<br />

Frequently, organism dependence on applied drug can be induced to develop. Then it<br />

can be produced even with danger and irreversible consequences. Various mechanisms<br />

<strong>of</strong> induction and development <strong>of</strong> organism dependence on drugs can be supposed. With<br />

respect to ma<strong>the</strong>matical modelling one <strong>of</strong> possibilities is to suppose that a dependence<br />

product, Dp, is produced in proportion to <strong>the</strong> rate <strong>of</strong> negative effects, Menn production<br />

and that it acts as an inhibitor <strong>of</strong> positive effects and/or as a drug inactivation factor. If,<br />

supposedly, one could consider that induction and development <strong>of</strong> dependence product<br />

formation mainly happen in <strong>the</strong> cerebral-neural compartment, and if roughly it could be<br />

sufcient to focus our interest to events taking place in cerebral-neural system, <strong>the</strong>n <strong>the</strong><br />

following approach could be applied in transforming <strong>the</strong> discussed ma<strong>the</strong>matical model:<br />

Let suppose that <strong>the</strong> dependence product, Dp inactivates <strong>the</strong> applied drug to high extent<br />

irreversibly, i.e. in accordance to <strong>the</strong> scheme:


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 141<br />

Dp + Fmen Fmni<br />

/Sh-1/<br />

If <strong>the</strong> expressed reduction rate <strong>of</strong> positive effects becomes proportional to Dp amount, <strong>the</strong>n<br />

<strong>the</strong> applicability <strong>of</strong> following equations can be expected:<br />

dD p<br />

/dt =b dMenn/dt –c D p<br />

F men<br />

/19/<br />

dF mni<br />

/dt =c D p<br />

F men<br />

/20/<br />

dF men<br />

/dt =k k<br />

F sng<br />

–k i<br />

F men<br />

- c D p<br />

F men<br />

/21/<br />

2.3 When one can stop to apply chemo<strong>the</strong>rapeutic agent?<br />

If one observes that positive effects do not show a tendency to decrease, <strong>the</strong>n one can<br />

recommend a starting <strong>of</strong> <strong>the</strong> procedure <strong>of</strong> decreasing drug doses, or even <strong>of</strong> stopping a<br />

given drug application, especially if with stopping drug application negative effects would<br />

start to reduce. Therefore, it appears that instead <strong>of</strong> equation /12a/ <strong>the</strong> equation /22/ can be<br />

recommended for application, i.e.<br />

dMenp/dt =k u<br />

F men<br />

(1-fF men<br />

-Menp/M pm<br />

) –d D p<br />

/22/<br />

Such a consideration does not ask detailed discussion referring to <strong>the</strong> kinetics <strong>of</strong> inactivated<br />

drug, F mni<br />

. If both positive and negative effects will spontaneously reduce in proportion to<br />

<strong>the</strong>ir specic rates, <strong>the</strong>n instead <strong>of</strong> equation /22/ and equation /13/ one can propose <strong>the</strong><br />

equations:<br />

dMenp/dt =k u<br />

F men<br />

(1-fF men<br />

-Menp/M pm<br />

) –d D p<br />

–g Menp /23/<br />

dMenn/dt =k v<br />

F men<br />

(1-Menn/M nm<br />

) –h Menn /24/<br />

Equations /23/ and /24/ suggest <strong>the</strong> drugs with higher h/g values should be preferred for<br />

application under a condition <strong>the</strong>y do not differ with respect to o<strong>the</strong>r <strong>the</strong>ir properties.<br />

To facilitate <strong>the</strong> understanding <strong>of</strong> properties <strong>of</strong> transformed ma<strong>the</strong>matical model some<br />

simplications can be introduced in order to have more convenient nal model. It seems<br />

that lumping <strong>of</strong> <strong>the</strong> terms F ve<br />

and F it<br />

into common F it<br />

, as well as <strong>of</strong> F hp<br />

, F tr<br />

and F t<br />

into<br />

common term F t<br />

could markedly correspond to <strong>the</strong> desired goal. Then <strong>the</strong> equations /1/,<br />

/1a/, /6/ and /8/ could be neglected, whereas instead <strong>of</strong> equations /2/, /4/, /4a/ and /7/ <strong>the</strong><br />

corresponding equations /25/, /26/ and /27/ could be applied:<br />

dF it<br />

/dt =-k 1<br />

.F it<br />

–k 2<br />

.F it<br />

/25/<br />

dF sng<br />

/dt =k 1<br />

F it<br />

–(k 4<br />

+k 6<br />

+k 9<br />

+k k<br />

) F sng<br />

+k 5<br />

F cr<br />

+k a<br />

F t<br />

+k i<br />

F men<br />

/26/<br />

dF t<br />

/dt =k 9<br />

F sng<br />

–k a<br />

F t<br />

/27/<br />

2.4 Modelling <strong>of</strong> <strong>the</strong> psycho<strong>the</strong>rapeutic substance transformation<br />

The applied psycho<strong>the</strong>rapeutic agent, depending on its chemical structure and its


142<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

instantaneous position in organism body, can be and usually is transformed into degradation<br />

products, at least partly. Degree and <strong>the</strong> rate <strong>of</strong> transformation depend on both substance<br />

characteristics and biodegradative capability <strong>of</strong> particular organism, especially <strong>of</strong> organism<br />

corresponding parts. The formed degradation products can be <strong>the</strong>rapeutically inactive,<br />

more or less toxic, <strong>of</strong> higher or lower <strong>the</strong>rapeutic effects, when compared with original<br />

substance, etc. Commonly, signicant or even <strong>the</strong> main part <strong>of</strong> applied substance mass<br />

is eliminated from organism body as <strong>the</strong> substance <strong>of</strong> original structure, while <strong>the</strong> o<strong>the</strong>r<br />

part is eliminated as applied substance degradation products. In many cases, <strong>the</strong> applied<br />

substance is primarily converted into <strong>the</strong> product (metabolite) <strong>of</strong> similar <strong>the</strong>rapeutic effects<br />

as original substance. Of course, <strong>the</strong>re is spectrum <strong>of</strong> efciency which could be expressed<br />

by formed metabolites. In this work, pharmacokinetics <strong>of</strong> formed <strong>the</strong>rapeutically active<br />

product is considered to demonstrate how some specic situations can be described by<br />

corresponding ma<strong>the</strong>matical model. Substance transformation can be considered as to<br />

happen in organism body in general, or as to happen mainly in <strong>the</strong> specic tissue (e.g.<br />

in liver), or in body tissue in general. Since cardiovascular system communicate with<br />

every particular body compartment, one can consider <strong>the</strong> substance transformation quickly<br />

reected to <strong>the</strong> state in cardiovascular system. Therefore, in <strong>the</strong> extended ma<strong>the</strong>matical<br />

model, instead <strong>of</strong> equation /26/ <strong>the</strong> equations<br />

dF sng<br />

/dt =k 1<br />

Fit-(k 4<br />

+k 6<br />

+k 9<br />

+k k<br />

+j)F sng<br />

+k 5<br />

F cr<br />

+k a<br />

F t<br />

+k i<br />

F men<br />

/26a/<br />

dF tsng<br />

/dt =jF sng<br />

-(k 6<br />

+k k<br />

)F tsng<br />

+k a<br />

F tt<br />

+k i<br />

F mt<br />

/28/<br />

should be applied, if neglecting <strong>the</strong> formed product afnity to <strong>the</strong> hearth and if supposing<br />

its transfers concerning o<strong>the</strong>r body compartments happen with same specic rates as<br />

those referring to transfers <strong>of</strong> <strong>the</strong> original substance. In addition, <strong>the</strong> corresponding new<br />

equations should be also included:<br />

dF nut<br />

/dt =k 6<br />

F tsng<br />

/29/<br />

dF tt<br />

/dt =k 9<br />

F tsng<br />

-k a<br />

F tt<br />

/30/<br />

dF mt<br />

/dt =k k<br />

F tsng<br />

-k i<br />

F mt<br />

/31/<br />

It is supposed that formed product inuences also positive and negative effects <strong>of</strong> patient<br />

behaviour as well as body viability. Therefore, instead <strong>of</strong> equations /12/, /12a/, /13/, /14/<br />

and /15/ <strong>the</strong> following equations should be applied:<br />

dMenp/dt =k u<br />

(F men<br />

+F mt<br />

)(1-fF men<br />

-Menp/M pm<br />

) /32/<br />

dMenn/dt =k v<br />

(F men<br />

+F mt<br />

)(1-Menn/M nm<br />

) /33/<br />

dB v<br />

/dt =-k s<br />

B v<br />

(F sng<br />

+F tsng<br />

)+k r<br />

S rv<br />

B nv<br />

/34/<br />

dB nv<br />

/dt =k s<br />

B v<br />

(F sng<br />

+F tsng<br />

)-k r<br />

S rv<br />

B nv<br />

/35/<br />

Of course, <strong>the</strong> o<strong>the</strong>r possibilities could be supposed. However, <strong>the</strong>re is no need to consider<br />

<strong>the</strong>m now.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 143<br />

2.5 Relevance <strong>of</strong> drug application method and pharmaceutical product form<br />

It is known that different drug application methods are practised. Parenteral application<br />

is preferred when fast effects are desired and/or when active substance is sensitive to <strong>the</strong><br />

action <strong>of</strong> active factors present in ventricular-intestinal compartment. Active substance<br />

stability and pharmaceutical drug form properties play important role in applied drug<br />

convenience and <strong>the</strong>rapeutic efciency. Active substance half-life time is considered to<br />

be one <strong>of</strong> very relevant pharmacokinetics parameters, especially when different active<br />

substances should be applied during <strong>the</strong>rapy. In <strong>the</strong> case <strong>of</strong> per oral drug application <strong>the</strong><br />

resorption rate <strong>of</strong> active substance markedly affects its pharmacokinetics and <strong>the</strong>refore<br />

<strong>the</strong>rapeutic consequences. The fast resorption rate is desired when <strong>the</strong> fast <strong>the</strong>rapeutic<br />

effects should result (e.g. when applying hypnotics). However, for longer <strong>the</strong>rapy periods<br />

and for maintenance <strong>of</strong> more stable active substance concentrations with minimal<br />

oscillations <strong>of</strong> active substance concentrations in corresponding organism compartments<br />

<strong>the</strong> slower active substance resorption rates could be recommended to be realised. Some <strong>of</strong><br />

computer simulation data demonstrating <strong>the</strong> effects <strong>of</strong> different substance resorption rates<br />

are shown in Tables 2 – 3 and Figs 3a,b.<br />

3 Computer simulations<br />

Computer programme Scientist enables a solving <strong>of</strong> number <strong>of</strong> different scientic problems.<br />

Based on previous and especially <strong>of</strong> recent experience 2, 5, 6 it was applied also in this<br />

work.<br />

4 Results and discussion<br />

4.1 Fundamental comments<br />

Chosen examples <strong>of</strong> computer simulations are presented in Fig. 1 to Fig. 3. To see how <strong>the</strong><br />

estimated consequences relate to quantities in particular organism body compartment <strong>the</strong><br />

calculation results are presented in Table 1.<br />

Table 1<br />

Effects <strong>of</strong> some psycho<strong>the</strong>rapeutic parameters (k u<br />

, k v<br />

, w, x, y, z) on <strong>the</strong> psycho<strong>the</strong>rapy<br />

efciency (Ut). Ut values refer to <strong>the</strong> 50 th hour <strong>of</strong> <strong>the</strong> computer simulation process.<br />

Parameter<br />

name<br />

Values<br />

ku kv w x y z Ut<br />

0.02 0.015 0.001 0.001 0.001 0.001 0.00492<br />

0.022 0.025 0.001 0.001 0.001 0.001 -0.000525<br />

0.02 0.02 0.001 0.001 0.001 0.001 0.00123<br />

0.02 0.02 0.001 0.002 0.001 0.001 0.0218<br />

0.02 0.02 0.001 0.001 0.002 0.001 -0.01934<br />

0.02 0.02 0.002 0.001 0.002 0.001 -0.01811<br />

0.02 0.02 0.002 0.001 0.002 0.002 -0.01573<br />

0.02 0.01 0.002 0.001 0.002 0.002 0.000668<br />

0.02 0.01 0.002 0.002 0.001 0.002 0.033608<br />

It is known that distribution <strong>of</strong> pharmacokinetic substances depends on substance properties,


144<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

way <strong>of</strong> its application and its applied amount, afnity <strong>of</strong> organism compartments to accept<br />

it and to retain its quantity, particular organism compartment mass and physiological state,<br />

whole organism viability and activity, etc. In this work, values <strong>of</strong> computer simulation<br />

parameters were chosen arbitrarily in order to demonstrate acceptability <strong>of</strong> proposed<br />

approach and possible applicability <strong>of</strong> supposed ma<strong>the</strong>matical model, expecting for both<br />

to be conditionally adequate. Chosen computer simulation examples demonstrated in Fig.<br />

1 to Fig. 3 show how parameter values reect on distribution <strong>of</strong> pharmacokinetic substance<br />

in treated patient organism. Psycho<strong>the</strong>rapy experts know well that rarely one can expect<br />

evident patient health improvement during very short time <strong>of</strong> treatment. Therefore, one can<br />

suggest considering <strong>the</strong> consequences <strong>of</strong> longer patient treatment periods. Some insight<br />

one can obtain by observing Fig. 1.<br />

Y (mg)<br />

Psycho<strong>the</strong>rapy pharmacokinetics<br />

10.0<br />

1.00 0.200<br />

9.5<br />

9.0<br />

8.5<br />

8.0<br />

7.5<br />

0.75 0.149<br />

7.0<br />

6.5<br />

6.0<br />

5.5<br />

5.0<br />

0.50 0.098<br />

4.5<br />

4.0<br />

3.5<br />

3.0<br />

2.5<br />

0.25 0.046<br />

2.0<br />

1.5<br />

1.0<br />

0.5<br />

0.0<br />

0.00 -0.005<br />

0 10 20 30 40 50<br />

Time (h)<br />

FVE_CALC vs T<br />

FIT_CALC vs T<br />

FFC_CALC vs T<br />

FSNG_CALC vs T<br />

FCR_CALC vs T<br />

FNU_CALC vs T<br />

FHP_CALC vs T<br />

FT_CALC vs T<br />

FTR_CALC vs T<br />

FMEN_CALC vs T<br />

FPL_CALC vs T<br />

MENP_CALC vs T<br />

MENN_CALC vs T<br />

BV_CALC vs T<br />

BNV_CALC vs T<br />

SRV_CALC vs T<br />

UT_CALC vs T<br />

PS_CALC vs T<br />

Bv,Bnv,Srv,Menp,Menn (nor.units)<br />

Ut,Ps (units)<br />

Y (mg)<br />

10.0<br />

9.5<br />

9.0<br />

8.5<br />

8.0<br />

7.5<br />

7.0<br />

6.5<br />

6.0<br />

5.5<br />

5.0<br />

4.5<br />

4.0<br />

3.5<br />

3.0<br />

2.5<br />

2.0<br />

1.5<br />

1.0<br />

0.5<br />

0.0<br />

Psycho<strong>the</strong>rapy pharmacokinetics<br />

0 10 20 30 40 50<br />

Time (h)<br />

1.00<br />

0.65<br />

0.30<br />

-0.05<br />

-0.40<br />

Bv,Bnv,Srv,Menp,Menn (nor.units)<br />

0.200<br />

0.138<br />

0.075<br />

0.012<br />

-0.050<br />

Ut,Ps (units)<br />

FVE_CALC vs T<br />

FIT_CALC vs T<br />

FFC_CALC vs T<br />

FSNG_CALC vs T<br />

FCR_CALC vs T<br />

FNU_CALC vs T<br />

FHP_CALC vs T<br />

FT_CALC vs T<br />

FTR_CALC vs T<br />

FMEN_CALC vs T<br />

FPL_CALC vs T<br />

MENP_CALC vs T<br />

MENN_CALC vs T<br />

BV_CALC vs T<br />

BNV_CALC vs T<br />

SRV_CALC vs T<br />

UT_CALC vs T<br />

PS_CALC vs T<br />

a) b)<br />

Fig. 1a,b<br />

Simulated psycho<strong>the</strong>rapy course for applied same computer simulation parameters during<br />

two consecutive cycles: k 1<br />

=0.3; k 2<br />

=0.01; k 3<br />

=0.8; k 4<br />

=0.1; k 5<br />

=0.5; k 6<br />

=0.02; k 7<br />

=0.05; k 8<br />

=0.08;<br />

k 9<br />

=0.1; k a<br />

=0.1; k b<br />

=0.05; k c<br />

=0.03; k d<br />

=0.1; k e<br />

=0.05; K k<br />

=0.1; k i<br />

=0.15; k u<br />

=0.02; k v<br />

=0.01;<br />

M pm<br />

=1.0; M nm<br />

=1.0; k s<br />

=0.005; k r<br />

=0.1; k rv<br />

=0.5; w=0.002; x=0.002; y=0.001; z=0.002; f =0.65.<br />

Initial value for F ve<br />

was <strong>the</strong> same for both a) and b) cycles; o<strong>the</strong>r initial independent variable<br />

quantities <strong>of</strong> <strong>the</strong> 2 nd cycle (b) were those at <strong>the</strong> 50 th hour <strong>of</strong> <strong>the</strong> simulated rst (a) cycle;<br />

As shown, some relative improvement one can expect if chosen substance can induce<br />

or cause an improvement and if it cannot lead to negative consequences <strong>of</strong> applied<br />

chemo<strong>the</strong>rapeutic treatment. Results suggest <strong>the</strong> giving <strong>of</strong> more importance to <strong>the</strong> role <strong>of</strong><br />

experts whenever <strong>the</strong> experts can inuence <strong>the</strong> patients by inducing positive consequences<br />

at <strong>the</strong>m. Data presented in Table 1 can explain <strong>the</strong> reasons why one can recommend <strong>the</strong><br />

estimations and/or assaying <strong>of</strong> chemo<strong>the</strong>rapeutic quantities in particular patient organism


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 145<br />

compartments. Fig. 1a, 1b demonstrate that equation /12a/ can be applied in explaining<br />

negative consequences <strong>of</strong> increasing <strong>the</strong> amounts <strong>of</strong> pharmacokinetic substances in<br />

cerebral-neural tissues. Evidently, data in Fig. 1a, 1b support <strong>the</strong> reasons why one should<br />

recommend <strong>the</strong> assaying and/or estimating <strong>of</strong> quantity distribution <strong>of</strong> chemo<strong>the</strong>rapeutic<br />

agents in particular compartments <strong>of</strong> human organism body. The organism dependence<br />

on applied drugs can be explained if applying <strong>the</strong> transformed ma<strong>the</strong>matical models. One<br />

example <strong>of</strong> computer simulation is demonstrated in Fig. 2a, 2b.<br />

Y (mg)<br />

Psycho- <strong>the</strong>rapy pharmacokinetics<br />

6.0<br />

1.00 0.050<br />

5.7<br />

5.4<br />

5.1<br />

4.8<br />

4.5<br />

0.75 0.038<br />

4.2<br />

3.9<br />

3.6<br />

3.3<br />

3.0<br />

0.50 0.025<br />

2.7<br />

2.4<br />

2.1<br />

1.8<br />

1.5<br />

0.25 0.013<br />

1.2<br />

0.9<br />

0.6<br />

0.3<br />

0.0<br />

0.00 0.000<br />

0.0 4.8 9.6 14.4 19.2 24.0<br />

FIT_CALC vs T<br />

Time (h)<br />

FF_CALC vs T<br />

FSG_CALC vs T<br />

FC_CALC vs T<br />

FTSG_CALC vs T<br />

FNU_CALC vs T<br />

FT_CALC vs T<br />

FM_CALC vs T<br />

FR_CALC vs T<br />

MEP_CALC vs T<br />

MEN_CALC vs T<br />

BV_CALC vs T<br />

BNV_CALC vs T<br />

SRV_CALC vs T<br />

U_CALC vs T<br />

PS_CALC vs T<br />

DP_CALC vs T<br />

FMI_CALC vs T<br />

FTT_CALC vs T<br />

FMT_CALC vs T<br />

FUT_CALC vs T<br />

Mep,Men,Bv,Srv (nor.units)<br />

Y3-U,Ps,Dp (arb.units)<br />

Y (mg)<br />

6.0<br />

5.7<br />

5.4<br />

5.1<br />

4.8<br />

4.5<br />

4.2<br />

3.9<br />

3.6<br />

3.3<br />

3.0<br />

2.7<br />

2.4<br />

2.1<br />

1.8<br />

1.5<br />

1.2<br />

0.9<br />

0.6<br />

0.3<br />

0.0<br />

Psycho- <strong>the</strong>rapy pharmacokinetics<br />

0.0 4.8 9.6 14.4 19.2 24.0<br />

Time (h)<br />

1.00<br />

0.75<br />

0.50<br />

0.25<br />

0.00<br />

Mep,Men,Bv,Srv (nor.units)<br />

0.100<br />

0.075<br />

0.050<br />

0.025<br />

0.000<br />

Y3-U,Ps,Dp (arb.units)<br />

FIT_CALC vs T<br />

FF_CALC vs T<br />

FSG_CALC vs T<br />

FC_CALC vs T<br />

FTSG_CALC vs T<br />

FNU_CALC vs T<br />

FT_CALC vs T<br />

FM_CALC vs T<br />

FR_CALC vs T<br />

MEP_CALC vs T<br />

MEN_CALC vs T<br />

BV_CALC vs T<br />

BNV_CALC vs T<br />

SRV_CALC vs T<br />

U_CALC vs T<br />

PS_CALC vs T<br />

DP_CALC vs T<br />

FMI_CALC vs T<br />

FTT_CALC vs T<br />

FMT_CALC vs T<br />

FUT_CALC vs T<br />

a) b)<br />

Fig. 2a,b:<br />

Simulation <strong>of</strong> active degradation product formation by applied drug transformation.<br />

Computer simulation based on transformed extended ma<strong>the</strong>matical model. Applied values<br />

<strong>of</strong> computer simulation parameters: k 1<br />

=0.8; k 2<br />

=0.01; k 4<br />

=0.1; k 5<br />

=0.5; k 6<br />

=0.02; k 9<br />

=0.1;<br />

K k<br />

=0.1; k a<br />

=0.1; b=0.01; c=0.03; d=0.0001; k i<br />

=0.15; k u<br />

=0.02; f=0.5; k v<br />

=0.01; g=0.0001;<br />

h=0.1; M pm<br />

=1.0; M nm<br />

=1.0; k s<br />

=0.005; k r<br />

=0.1; k rv<br />

=0.5; w=0.002; x=0.002; y=0.001; z=0.002;<br />

New parameter j=0.12 was applied. Initial drug quantity for both a) and b) was <strong>the</strong> same;<br />

<strong>the</strong> o<strong>the</strong>r quantities applied for b) were those nal for a);<br />

In practice, patients are frequently classied as belonging to different groups or types,<br />

based on <strong>the</strong> criteria <strong>of</strong> debatable reliability and <strong>the</strong>refore sometimes wrongly or even with<br />

danger consequences. Here, perhaps is reasonable to mention <strong>the</strong> Latina sentence: Quot<br />

homines tot sententiae, which refers to all people in general and <strong>the</strong>refore it certainly can<br />

be applicable to patients as well. Therefore, it follows that <strong>the</strong> best patient classication<br />

criterion seems to be by considering every patient as individual asking specic treatment<br />

and strong control <strong>of</strong> drug quantity distribution during <strong>the</strong>rapy. Data in Tables 2 – 3 and<br />

Figs. 3a,b show one <strong>of</strong> possible ways for <strong>the</strong>rapy improvements or even optimisation.


146<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

As demonstrated, slowed resorption leads to benecial consequences. Therefore, <strong>the</strong>re<br />

is reason for production <strong>of</strong> pharmaceutical products <strong>of</strong> properties which correspond to<br />

desired active substance resorption rate.<br />

Table 2<br />

Effects <strong>of</strong> active substance resorption rate (value <strong>of</strong> resorption rate constant k 1<br />

) on values<br />

<strong>of</strong> pharmacokinetics parameters at 10th hour after drug application.<br />

Parameter name Initial Value at 10th hour for given k 1<br />

value<br />

value<br />

k 1<br />

=0.8/h k 1<br />

=0.08/h<br />

FIT 100.0 0.030354 40.657<br />

FF 0.0 1.2342 6.5937<br />

FSG 0.0 16.699* 15.413**<br />

FC 0.0 3.8810 2.8076<br />

FTSG 0.0 17.915 8.5609<br />

FNU 0.0 6.2270 2.5503<br />

FT 0.0 18.144 8.6117<br />

FM 0.0 14.235 7.2429<br />

FR 0.0 2.1823 0.82074<br />

MEP 0.0 -5.8849 -1.1067<br />

MEN 0.0 0.59911 0.28760<br />

BV 0.99 0.33840 0.57298<br />

BNV 0.01 0.66160 0.42702<br />

SRV 1.0 0.88626 0.93331<br />

U 0.0 -0.058650 -0.005600<br />

PS 0.0 -0.022766 0.014274<br />

DP 0.0 0.0011259 0.0016591<br />

FMI 0.0 0.0048652 0.0012169<br />

FTT 0.0 9.0919 3.1410<br />

FMT 0.0 7.7490 2.75743<br />

FUT 0.0 2.6062 0.84128<br />

*<br />

**<br />

maximum attained during <strong>the</strong> 2nd<br />

hour,<br />

maximum attained during <strong>the</strong> 8th hour<br />

Table 3<br />

Effect <strong>of</strong> active substance repeated per-oral additions on pharmacokinetics quantities.<br />

Application <strong>of</strong> drug form adapted for active substance resorption rate dened with k 1<br />

=<br />

0.08/h.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 147<br />

Quantity<br />

name<br />

Initial<br />

value<br />

Simulated value<br />

after 8 th hour<br />

Simulated value<br />

after 25 mg active<br />

substance addition<br />

at 8 th hour and after<br />

16 hours<br />

Simulated values after<br />

50 mg active substance<br />

additions at 8 th and at 16 th<br />

hour<br />

Value after<br />

16 th hour<br />

Value after<br />

24 th hour<br />

FIT 100.0 48.675 35.861 48.030 47.716<br />

FF 0.0 5.7028 9.9043 11.330 16.920<br />

FSG 0.0 15.600 17.548 21.448 25.419<br />

FC 0.0 2.6998 3.3293 4.0042 4.8585<br />

FTSG 0.0 7.0583 13.705 15.469 24.329<br />

FNU 0.0 1.9287 4.7860 5.2682 9.3740<br />

FT 0.0 7.0789 13.049 14.819 20.868<br />

FM 0.0 6.1546 10.210 11.749 15.583<br />

FR 0.0 0.58643 1.5909 1.7375 3.0097<br />

MEP 0.0 -0.54687 -3.2256 -3.7939 -6.4175<br />

MEN 0.0 0.19988 0.51099 0.53363 0.69866<br />

BV 0.99 0.63995 0.42220 0.38628 0.27897<br />

BNV 0.01 0.36005 0.57780 0.61372 0.72103<br />

SRV 1.0 0.94798 0.90219 0.89739 0.87648<br />

U 0.0 -0.0018992 -0.034447 -0.037620 -0.12630<br />

PS 0.0 0.013684 0.0042820 0.0022673 -0.039698<br />

DP 0.0 0.0014112 0.0013068 0.0012736 0.00039878<br />

FMI 0.0 0.00058767 0.0038032 0.0040628 0.0065879<br />

FTT 0.0 2.0975 7.0013 7.5256 14.736<br />

FMT 0.0 1.8886 5.7933 6.2655 11.627<br />

FUT 0.0 0.52811 2.2175 2.3495 5.5524


148<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Y (mg)<br />

100<br />

95<br />

90<br />

85<br />

80<br />

75<br />

70<br />

65<br />

60<br />

55<br />

50<br />

45<br />

40<br />

35<br />

30<br />

25<br />

20<br />

15<br />

10<br />

5<br />

0<br />

Psycho- <strong>the</strong>rapy pharmacokinetics<br />

0 2 4 6 8 10<br />

Time (h)<br />

1.0<br />

0.8<br />

0.5<br />

0.3<br />

0.0<br />

Mep,Men,Bv,Srv (nor.units)<br />

0.100<br />

0.075<br />

0.050<br />

0.025<br />

0.000<br />

Y3-U,Ps,Dp (arb.units)<br />

FIT_CALC vs T<br />

FF_CALC vs T<br />

FSG_CALC vs T<br />

FC_CALC vs T<br />

FTSG_CALC vs T<br />

FNU_CALC vs T<br />

FT_CALC vs T<br />

FM_CALC vs T<br />

FR_CALC vs T<br />

MEP_CALC vs T<br />

MEN_CALC vs T<br />

BV_CALC vs T<br />

BNV_CALC vs T<br />

SRV_CALC vs T<br />

U_CALC vs T<br />

PS_CALC vs T<br />

DP_CALC vs T<br />

FMI_CALC vs T<br />

FTT_CALC vs T<br />

FMT_CALC vs T<br />

FUT_CALC vs T<br />

Y (mg)<br />

100<br />

95<br />

90<br />

85<br />

80<br />

75<br />

70<br />

65<br />

60<br />

55<br />

50<br />

45<br />

40<br />

35<br />

30<br />

25<br />

20<br />

15<br />

10<br />

5<br />

0<br />

Psycho- <strong>the</strong>rapy pharmacokinetics<br />

0 2 4 6 8 10<br />

Time (h)<br />

1.00<br />

0.75<br />

0.50<br />

0.25<br />

0.00<br />

Mep,Men,Bv,Srv (nor.units)<br />

0.100<br />

0.075<br />

0.050<br />

0.025<br />

0.000<br />

Y3-U,Ps,Dp (arb.units)<br />

FIT_CALC vs T<br />

FF_CALC vs T<br />

FSG_CALC vs T<br />

FC_CALC vs T<br />

FTSG_CALC vs T<br />

FNU_CALC vs T<br />

FT_CALC vs T<br />

FM_CALC vs T<br />

FR_CALC vs T<br />

MEP_CALC vs T<br />

MEN_CALC vs T<br />

BV_CALC vs T<br />

BNV_CALC vs T<br />

SRV_CALC vs T<br />

U_CALC vs T<br />

PS_CALC vs T<br />

DP_CALC vs T<br />

FMI_CALC vs T<br />

FTT_CALC vs T<br />

FMT_CALC vs T<br />

FUT_CALC vs T<br />

a) b)<br />

Fig. 3a,b.<br />

Effect <strong>of</strong> active substance resorption rate on pharmacokinetics quantities: a) k 1<br />

=0.8; b)<br />

k 1<br />

=0.08;<br />

Concerning a chemo<strong>the</strong>rapeutic substance distribution in organism body one should point<br />

out that in <strong>the</strong> proposed ma<strong>the</strong>matical model <strong>the</strong> chemo<strong>the</strong>rapeutic substance quantities<br />

represent chemo<strong>the</strong>rapeutic substance masses in particular compartments, not <strong>the</strong>ir<br />

mass concentrations in corresponding compartments. Such an approach to expressing<br />

chemo<strong>the</strong>rapeutic substance distribution can be considered as more convenient than that<br />

referring to chemo<strong>the</strong>rapeutic substance mass concentrations, since at given time <strong>the</strong><br />

corresponding substance mass concentration cannot be considered to be constant with<br />

reference to every compartment part.<br />

4.2 Speculative comments (conclusions)<br />

Enormous complexity <strong>of</strong> psycho<strong>the</strong>rapy asks serious comments. Some questions one can<br />

put here: Are we capable to recognise, in every case, which part <strong>of</strong> patient behaviour can be<br />

and should be changed, and how to proceed in order to realise desired positive changes?!<br />

Are we always sure that chosen chemo<strong>the</strong>rapeutic agent is adequate one?! Whe<strong>the</strong>r at<br />

all <strong>the</strong> application <strong>of</strong> any chemo<strong>the</strong>rapeutic agent can be recommended?! Is it reasonable<br />

a neglecting <strong>of</strong> prayers?! Religious and spiritual factors in general certainly should be<br />

taken into account with giving <strong>the</strong>m adequate relevance. Which degree <strong>of</strong> tranquilisation<br />

<strong>of</strong> particular patient could be considered as optimal one for his health?! How to enhance<br />

<strong>the</strong> endogenous production <strong>of</strong> tranquilisation factors (endorphin, e.g.) in improving <strong>the</strong>


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 149<br />

dreaming and sleeping in order to reduce <strong>the</strong> need for an application <strong>of</strong> hypnotics?!<br />

Why not to consider that particular effect <strong>of</strong> any factor can be quantitatively evaluated,<br />

at least approximately?! Is it possible to dene <strong>the</strong> position <strong>of</strong> psychiatrists, since <strong>the</strong><br />

most frequent situation is that <strong>the</strong>y are simultaneously engaged in treating relatively<br />

large number <strong>of</strong> patients?! One <strong>of</strong> answers on all mentioned questions certainly should<br />

be that exact information on chemo<strong>the</strong>rapeutic substance distribution in organism body<br />

is <strong>of</strong> essential importance for achieving <strong>of</strong> positive results <strong>of</strong> psycho<strong>the</strong>rapeutic treatment<br />

which includes <strong>the</strong> application <strong>of</strong> chemo<strong>the</strong>rapeutic substances. Therefore, methods <strong>of</strong><br />

assaying and estimating <strong>of</strong> chemo<strong>the</strong>rapeutic substance contents in particular human<br />

organism compartments should be available for application whenever one estimates that<br />

such information could be helpful.<br />

Application <strong>of</strong> chemo<strong>the</strong>rapeutic substances in general can induce or cause different<br />

undesired side effects. These can refer to particular organism body compartments or to <strong>the</strong><br />

whole organism. Live organism body can be induced, and frequently is capable to degrade<br />

and/or transform <strong>the</strong> used substance. As a result <strong>of</strong> organism body answer could be <strong>the</strong><br />

overproduction <strong>of</strong> some products asking <strong>the</strong>rapeutic action as well. Therefore, one suggests<br />

a serious consideration <strong>of</strong> all <strong>the</strong>se effects and possible <strong>the</strong>ir description. The extended<br />

ma<strong>the</strong>matical model can enable a more exact expression <strong>of</strong> particular side effect causes<br />

and consequences. The approach similar to that applied for cerebral-neural compartment<br />

can be also applied for any considered compartment. Then, particular positive and/or<br />

undesired negative effects could be evaluated with reference to <strong>the</strong> whole organism body<br />

or to particular its organs or tissues.<br />

As shown recently 2A by expressing roughly <strong>the</strong> decisive role <strong>of</strong> cardio-vascular and<br />

respiratory compartments in affecting <strong>the</strong> quantity <strong>of</strong> “revitalisation substrate”, Srv, in this<br />

work one can focus onto evaluation <strong>of</strong> consequences referring to vital functions <strong>of</strong> liver, or<br />

<strong>of</strong> nephritic-urinary and o<strong>the</strong>r organism body compartments.<br />

Concerning nephritic-urinary system it should be pointed out that <strong>the</strong> total amounts <strong>of</strong><br />

pharmacokinetic agent transferred to it differ from those present in it at given time, because<br />

<strong>of</strong> periodic withdrawals <strong>of</strong> urine from nephritic-urinary system. Therefore, <strong>the</strong> amounts<br />

<strong>of</strong> pharmacokinetic substances actually present in <strong>the</strong> nephritic-urinary system represent<br />

<strong>the</strong> difference between <strong>the</strong> total amounts transferred into <strong>the</strong> system and <strong>the</strong> total amounts<br />

withdrawn from <strong>the</strong> system. Similar consideration as for nephritic-urinary system can also<br />

be applied concerning <strong>the</strong> pharmacokinetic substance quantity present in <strong>the</strong> faeces <strong>of</strong> large<br />

intestine.<br />

The advantages <strong>of</strong> developed ma<strong>the</strong>matical model application can become especially<br />

evident if one tends to estimate consequences <strong>of</strong> simultaneous application <strong>of</strong> different<br />

drugs in <strong>the</strong> <strong>the</strong>rapy. Based on <strong>the</strong> kinetic relationships established for particular substance<br />

one can predict <strong>the</strong> consequences <strong>of</strong> simultaneous applications <strong>of</strong> two or more different<br />

substances during <strong>the</strong> planned psycho<strong>the</strong>rapy treatments, if applying computer simulations.<br />

These could be performed with reference to every patient. It is important to point out that<br />

our possibilities to represent <strong>the</strong> events in organism body by ma<strong>the</strong>matical models are not<br />

limited only on models presented here. Our knowledge referring to o<strong>the</strong>r events can also be<br />

translated into corresponding ma<strong>the</strong>matical models, and <strong>the</strong>refore in those convenient for<br />

<strong>the</strong> use in performing desired computer simulations. By <strong>the</strong> way, it is important to point out<br />

that presented ma<strong>the</strong>matical model can simply be transformed into much simpler models<br />

by neglecting relevance <strong>of</strong> those events which should not be obligatory considered for<br />

evaluation <strong>of</strong> consequences <strong>of</strong> more relevant events.<br />

Finally, <strong>the</strong>re are questions which should not be avoided. One <strong>of</strong> <strong>the</strong>m is how to estimate<br />

normalised values <strong>of</strong> quantities <strong>of</strong> B v<br />

, B nv<br />

, S rv<br />

, Menp, Menn, etc. No doubt, a reliability


150<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

<strong>of</strong> estimations will markedly depend on <strong>the</strong> experience <strong>of</strong> psycho<strong>the</strong>rapy experts and on<br />

<strong>the</strong> availability <strong>of</strong> acceptable evaluation methods. However, <strong>the</strong> experts certainly can and<br />

know dene, at least approximately, <strong>the</strong> maximal specic quantity values, and compare<br />

<strong>the</strong>m with values estimated during <strong>the</strong> patient observation and treatments. Therefore,<br />

<strong>the</strong>re is a certain possibility for at least slight advances in evaluating <strong>the</strong> efciency <strong>of</strong><br />

psycho<strong>the</strong>rapy treatments. Of course, evaluations should be performed in <strong>the</strong> right time.<br />

One cannot recommend e.g. a postponing <strong>of</strong> B nv<br />

evaluations till a situation when <strong>the</strong><br />

pathologist opinion would become <strong>the</strong> most relevant. On <strong>the</strong> o<strong>the</strong>r hand, we should always<br />

take into account <strong>the</strong> fact that <strong>the</strong> frequency <strong>of</strong> successful <strong>the</strong>rapy cases shows positive<br />

trend. Moreover, relevant pharmaceutical companies (e.g. LILLY USA, LLC. 11) give<br />

enough data for optimal approach to <strong>the</strong> use <strong>of</strong> psycho<strong>the</strong>rapeutic agents. Therefore, <strong>the</strong>re<br />

is no doubt for a need <strong>of</strong> controlling drug distribution in human body during <strong>the</strong>rapy.<br />

Already long time introduced practice <strong>of</strong> determination <strong>of</strong> alcohol concentrations in blood<br />

samples <strong>of</strong> persons causing trafc accidents justify <strong>the</strong> giving adequate relevance to <strong>the</strong><br />

control <strong>of</strong> psycho<strong>the</strong>rapeutic drugs distribution in <strong>the</strong> body <strong>of</strong> every patient subjected to<br />

psycho<strong>the</strong>rapy which includes <strong>the</strong> drug application.<br />

Symbols<br />

a kinetic constant, h -1 (T -1 )<br />

B v<br />

body vitality, dimensionless<br />

B nv<br />

body non-vitality, dimensionless<br />

b kinetic constant, dimensionless<br />

c kinetic constant, h -1 (T -1 )<br />

Dp dependence product normalised mass, dimensionless<br />

d kinetic constant, h -1 (T -1 )<br />

F cr<br />

pharmacokinetic substance mass in hearth, mg (M)<br />

F fc<br />

pharmacokinetic substance mass in faeces, mg (M)<br />

F hp<br />

pharmacokinetic substance mass in liver, mg (M)<br />

F men<br />

pharmacokinetic substance mass in neural-brain system, mg (M)<br />

F mni<br />

inhibited F men<br />

, mg (M)<br />

F mt<br />

transformed pharmacokinetic substance mass in neural-brain system, mg (M)<br />

F nu<br />

pharmacokinetic substance mass in nephritic–urinary system, mg (M)<br />

F nut<br />

transformed pharmacokinetic substance mass in nephritic–urinary system, mg (M)<br />

F rsp<br />

, F plm<br />

pharmacokinetic substance mass in respiratory system, mg<br />

(M)<br />

F sng<br />

pharmacokinetic substance mass in blood, mg (M)<br />

F tsng<br />

transformed pharmacokinetic substance mass in blood, mg (M)<br />

F t<br />

pharmacokinetic substance mass in tissue, mg (M)<br />

F tt<br />

transformed pharmacokinetic substance mass in tissue, mg (M)<br />

F tr<br />

pharmacokinetic substance mass in tissue receptor, mg (M)<br />

F ve,<br />

F it<br />

pharmacokinetic substance mass in ventricular (F ve<br />

)-intestinal (F it<br />

) compartment,<br />

mg<br />

(M)<br />

g kinetic constant, h -1 (T -1 )<br />

h kinetic constant, h -1 (T -1 )<br />

j kinetic constant, h -1 (T -1 )<br />

k 1<br />

kinetic constant with reference to F ve<br />

, h -1 (T -1 )<br />

k 2<br />

kinetic constant with reference to F it<br />

, h -1 (T -1 )<br />

k 3<br />

kinetic constant with reference to Fit, h -1 (T -1 )<br />

k 4<br />

kinetic constant with reference to F sng<br />

, h -1 (T -1 )<br />

k 5<br />

kinetic constant with reference to F cr<br />

, h -1 (T -1 )


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 151<br />

k 6<br />

kinetic constant with reference to F sng<br />

, h -1 (T -1 )<br />

k 7<br />

kinetic constant with reference to F sng<br />

, h -1 (T -1 )<br />

k 8<br />

kinetic constant with reference to F hp<br />

, h -1 (T -1 )<br />

k 9<br />

kinetic constant with reference to F sng<br />

, , h -1 (T -1 )<br />

k a<br />

kinetic constant with reference to Ft, h -1 (T -1 )<br />

k b<br />

kinetic constant with reference to F cr<br />

, h -1 (T -1 )<br />

k c<br />

kinetic constant with reference to F rsp<br />

, h -1 (T -1 )<br />

k d<br />

kinetic constant with reference to Ft, h -1 (T -1 )<br />

ke kinetic constant with reference to F tr,<br />

h -1 (T -1 )<br />

ki kinetic constant with reference to F men<br />

,h -1 (T -1 )<br />

k k<br />

kinetic constant with reference to F sng,<br />

,h -1 (T -1 )<br />

k r<br />

kinetic constant with reference to B nv<br />

and Srv, h -1 (T -1 )<br />

k rv<br />

kinetic constant with reference to Srv, h -1 (T -1 )<br />

k s<br />

kinetic constant with reference to Bv and F sng<br />

, mg -1 h -1 (M -1 T -1 )<br />

k u<br />

kinetic constant with reference to F men<br />

and Menp, mg -1 h -1 (M -1 T -1 )<br />

k v<br />

kinetic constant with reference to F men<br />

and Menn, mg -1 h -1 (M -1 T -1 )<br />

Menn normalised quantity <strong>of</strong> negative effects caused by F men<br />

, dimensionless<br />

Menp normalised quantity <strong>of</strong> positive effects caused by F men<br />

, dimensionless<br />

Mnm maximal value <strong>of</strong> Menn, dimensionless<br />

Mpm maximal value <strong>of</strong> Menp, dimensionless<br />

Ps normalised effect <strong>of</strong> psychiatrist and personnel, dimensionless<br />

S rv<br />

normalised quantity <strong>of</strong> revitalisation substrate, dimensionless<br />

Ut normalised psycho<strong>the</strong>rapy efciency, dimensionless<br />

w kinetic constant with reference to Ps, h -1 (T -1 )<br />

x kinetic constant with reference to Menp, h -1 (T -1 )<br />

y kinetic constant with reference to Menn, h -1 (T -1 )<br />

z kinetic constant with reference to Ps, h -1 (T -1 )<br />

References<br />

1. Bošnjak M. (1982) Ma<strong>the</strong>matical modelling <strong>of</strong> biochemical reaction systems (in<br />

Croatian) Kem. Ind. 31 545 -559<br />

2. Bošnjak M. (2009) Introduction to Kinetics <strong>of</strong> Microbial Processes ( in Croatian:<br />

Uvod u kinetiku mikrobnih procesa), Graphis, Zagreb, (2A= pp. 275-306, Appendix)<br />

3. Bošnjak M., Topolovec V., Vrana M. (1978), Growth kinetics <strong>of</strong> Streptomyces<br />

erythreus during erythromycin biosyn<strong>the</strong>sis, J. Appl. Chem. Biotechnol. 28 791- 798<br />

4. Bošnjak M., Topolovec V., Johanides V. (1979), Growth kinetics and antibiotic<br />

syn<strong>the</strong>sis during <strong>the</strong> repeated fed batch culture <strong>of</strong> streptomycetes, In: Armiger W. B.<br />

(ed.), Computer Applications in Fermentation Technology, Biotechnol. Bioeng. Symp.<br />

No. 9 155 -165, Wiley & Sons<br />

5. Bošnjak M., Bago Joksovi A., Pigac J., Bošnjak Cihlar Ž., Hranueli D., (2006)<br />

Applicability <strong>of</strong> ma<strong>the</strong>matical models in dening <strong>the</strong> behaviour kinetics distinction<br />

among microbial strains, Chem. Biochem. Eng. Q. 20 375 -388<br />

6. Bošnjak M., Udikovi Koli N., Petri I., Cihlar D., Hršak D., (<strong>2010</strong>) Integrated<br />

approach to ma<strong>the</strong>matical modelling <strong>of</strong> atrazine degradation in different reaction<br />

systems, Food Technol. Biotechnol.48 392-403<br />

7. Ci<strong>of</strong> Ch. L., Liu Sh., Wolf M. A., (<strong>2010</strong>) Recent development in glycine transporter-1<br />

inhibitors, In: J. E. Macor (Ed.), Annual Reports in Medicinal Chemistry,Vol.45, pp.<br />

19-35, Academic Press, Burlington, MA 01803, USA<br />

8. Karba R., Mrhar A., Bremšak F., Kozjak F., (1977) Estimation <strong>of</strong> pharmacokinetics


152<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

parameters <strong>of</strong> amoxicillin and ampicilline by identication (in Slovenian: Doloevanje<br />

farmakokinetinih parametrov amoksicilina in ampicilina s pomojo identikacije),<br />

In: Informatica 77, Proc. Yug. Intern. Symp. 6 218, Slov. Soc. Informatika, Ljubljana<br />

9. van der Kleijin E., Guelen P. J. M., van Wijk C., Baars I., (1975) Clinical<br />

pharmacokinetics in monitoring chronic medication with anti-epileptic drugs, In:<br />

Schneider H., Janz D., Gardner-Thorpe C., Meinardi H., Shervin A. L. (eds.), Clinical<br />

Pharmacology <strong>of</strong> Anti-Epileptic Drugs, Springer, Berlin- Heidelberg –New York, pp.<br />

11 -13<br />

10. Kossen N. W., (1979) Ma<strong>the</strong>matical modelling <strong>of</strong> fermentation processes: Scope and<br />

limitation, In: Bull A. T., Elwood D. C., Ratledge C. (eds.) Microbial Technology:<br />

Current State, Future Prospects, 29 th Symp. Soc. Gen. Microb., Cambridge, University<br />

Press, Cambridge, , pp. 327 -35<br />

11. LILLY USA, LLC Internet sites.<br />

12. Li R. C., Nix D. E., Schentag J. J., (2006) Pharmacodynamic modelling <strong>of</strong> bacterial<br />

kinetics: -Lactam antibiotics against Escherichia coli, J. Pharm. Sciences 83 970<br />

-975<br />

13. Nikolaou M., Schilling A. N., Vo Giao, Chang Kai-tai, Tam V. H., (2007) Modeling<br />

<strong>of</strong> microbial population responses to time-periodic concentrations <strong>of</strong> antimicrobial<br />

agents, Anuals Biomed. Eng. 35 1458 -1470<br />

14. Ramkrishna D., (1979) Statistical models <strong>of</strong> cell populations, In: Ghose T. K., Fiechter<br />

A., Blakebrough N. (eds.), Advances in Biochemical Engineering, Vol. 11, Springer,<br />

Berlin-Heidelberg-New York, pp. 1 -47<br />

15. Roepke H. und Riemann J.,(1979) Analog Computer in Chemie und Biologie, Springer,<br />

Berlin, 1969<br />

Appendix<br />

Spirituality based <strong>the</strong>rapy and its possible relevance with reference to behaviour disorder<br />

treatments<br />

There are cases <strong>of</strong> health improvements observed after patients being subjected to<br />

spirituality based <strong>the</strong>rapy. Therefore, its relevance should not be neglected regardless<br />

whe<strong>the</strong>r somebody is religious or not. However, <strong>the</strong> evaluation <strong>of</strong> effects based on such a<br />

<strong>the</strong>rapy probably asks <strong>the</strong> specic approach and explanations. Certainly <strong>the</strong>re is no need to<br />

explain why <strong>the</strong> health <strong>of</strong> those religious was improved, while <strong>the</strong> cases <strong>of</strong> those declared<br />

as not being religious ask some comments. In this work <strong>the</strong> effects <strong>of</strong> signals were not<br />

discussed. The source <strong>of</strong> signals can be <strong>of</strong> different characters, but possible explanation<br />

<strong>of</strong> <strong>the</strong>ir effects could be similar. One <strong>of</strong> explanation possibilities is to suppose that signals<br />

activate some biochemical mechanisms capable to repair <strong>the</strong> organism normal behaviour.<br />

Applied drug dose titration<br />

In psycho<strong>the</strong>rapy, depending on particular patient, one or more different drugs can be<br />

applied. In cases when applied drug reliably showed adequate positive effects with absence<br />

or with minimal negative side effects <strong>the</strong> estimation and maintenance <strong>of</strong> optimal drug<br />

dosing do not represent problem, if necessary information on drug properties is available.<br />

More complicate situation appears when <strong>the</strong> quite adequate drug for particular patient is<br />

not available, or when patient behaviour asks <strong>the</strong> searching <strong>of</strong> adequacy <strong>of</strong> known and<br />

available different drugs. Then it can happen that none <strong>of</strong> available known drugs is quite<br />

adequate and that <strong>the</strong> combination <strong>of</strong> different available drugs should be applied. If <strong>the</strong> most


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 153<br />

convenient <strong>of</strong> available drugs is chosen for starting treatment is applied on appropriate way,<br />

<strong>the</strong>n it is recommendable to monitor <strong>the</strong> consequences to decide how to continue, taking<br />

into account drug properties referring to drug half-life time and resorption rate as well as<br />

character and intensity <strong>of</strong> observed consequences. The observed side effects could suggest<br />

additional application <strong>of</strong> ano<strong>the</strong>r drug suitable to suppress observed negative effects. If<br />

such a drug can induce side effects reducing <strong>the</strong> positive effects <strong>of</strong> applied starting drug,<br />

<strong>the</strong>n careful titration become obligate. If this would not be done adequately, <strong>the</strong>n it can<br />

happen that due to overdosing instead <strong>of</strong> health improvement <strong>the</strong> health aggravation could<br />

result. Therefore, in addition to commonly applied trial and error methods in optimizing<br />

chemo<strong>the</strong>rapeutic treatment <strong>the</strong> computer simulation <strong>of</strong> applied drugs pharmacokinetics<br />

and supplying some necessary experimental data could be recommended in order to<br />

optimise <strong>the</strong>rapy.<br />

Information on <strong>the</strong> author:<br />

Pr<strong>of</strong>. Dr. sc. Marijan Bošnjak, retired; member emeritus <strong>of</strong> Croatian Academy <strong>of</strong><br />

Engineering (<strong>HATZ</strong>), HR-10000 Zagreb, Croatia;<br />

E-mail: marijan.bosnjak@hatz.hr<br />

Home address:<br />

HR-10000 Zagreb, Slovenska 19, Croatia<br />

Tel. (385)-1-3702507


154<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

DICES: Distributed Component-based Embedded<br />

S<strong>of</strong>tware Systems<br />

Mario Žagar<br />

Faculty <strong>of</strong> Electrical Engineering and Computing<br />

University <strong>of</strong> Zagreb, Zagreb, Croatia<br />

mario.zagar@fer.hr<br />

Ivica Crnković<br />

Mälardalen Real-Time Research Centre<br />

Mälerdalen University, Västerås, Sweden<br />

ivica.crnkovic@mdh.se<br />

Darko Stipaničev<br />

Faculty <strong>of</strong> Electrical Engineering, Mechanical Engineering and Naval Architecture<br />

University <strong>of</strong> Split, Split, Croatia<br />

darko.stipanicev@fesb.hr<br />

Maja Štula<br />

Faculty <strong>of</strong> Electrical Engineering, Mechanical Engineering and Naval Architecture<br />

University <strong>of</strong> Split, Split, Croatia<br />

maja.stula@fesb.hr<br />

Juraj Feljan<br />

Mälardalen Real-Time Research Centre<br />

Mälerdalen University, Västerås, Sweden<br />

juraj.feljan@mdh.se<br />

Luka Lednicki<br />

Faculty <strong>of</strong> Electrical Engineering and Computing<br />

University <strong>of</strong> Zagreb, Zagreb, Croatia<br />

luka.lednicki@fer.hr<br />

Josip Maras<br />

Faculty <strong>of</strong> Electrical Engineering, Mechanical Engineering and Naval Architecture<br />

University <strong>of</strong> Split, Split, Croatia<br />

josip.maras@fesb.hr<br />

Ana Petričić<br />

Faculty <strong>of</strong> Electrical Engineering and Computing<br />

University <strong>of</strong> Zagreb, Zagreb, Croatia<br />

ana.petricic@fer.hr<br />

Abstract<br />

This article gives a short overview <strong>of</strong> <strong>the</strong> contribution <strong>of</strong> DICES project. The goal <strong>of</strong> <strong>the</strong><br />

project is to advance <strong>the</strong>ories and technologies used in development <strong>of</strong> distributed embedded<br />

systems. Three examples <strong>of</strong> <strong>the</strong> contributions are presented: a) reverse <strong>engineering</strong> <strong>of</strong> webbased<br />

applications, design extraction and extraction <strong>of</strong> reusable user-interface controls,


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 155<br />

b) a fretwork for building systems that use UPnP devices and treat <strong>the</strong>m as components<br />

in <strong>the</strong> same way as s<strong>of</strong>tware components, and c) PRIDE – development environment for<br />

designing, modeling and developing embedded systems, based on ProCom technology.<br />

Keywords: S<strong>of</strong>tware components, embedded systems, web-based applications, reverse<br />

<strong>engineering</strong><br />

1 Introduction<br />

DICES (Distributed Component-based Embedded S<strong>of</strong>tware Systems) is a project<br />

funded by UKF (Unity Through Knowledge Fund) with contributions from Faculty <strong>of</strong><br />

Electrical Engineering and Computing (FER) - University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Electrical<br />

Engineering, Mechanical Engineering and Naval Architecture (FESB), University <strong>of</strong> Split,<br />

School <strong>of</strong> Innovation, Design and Engineering - Mälardalen University (MDU) in Sweden,<br />

and Ericsson Nikola Tesla. The project was performed during three years, from 2007 to<br />

<strong>2011</strong>.<br />

The DICES project goal is to advance development <strong>of</strong> distributed embedded s<strong>of</strong>tware<br />

systems with emphasis on s<strong>of</strong>tware reusability and predictability <strong>of</strong> s<strong>of</strong>tware quality.<br />

The aim <strong>of</strong> <strong>the</strong> project is increasing <strong>the</strong> s<strong>of</strong>tware development efciency and quality by<br />

applying service-oriented and component-based approaches.<br />

The overall presence <strong>of</strong> distributed embedded systems in <strong>the</strong> modern society is a fact.<br />

Examples <strong>of</strong> such systems are telecommunication systems, grid systems, control and<br />

information systems <strong>of</strong> vehicular systems (cars, trains), environmental monitoring<br />

systems. Embedded systems development is one <strong>of</strong> <strong>the</strong> strategic research areas <strong>of</strong> EU-FP7<br />

programmes. It is also <strong>of</strong> signicant importance in Croatia, since many leading companies<br />

in Croatia ei<strong>the</strong>r produce such systems (e.g. Konar, Ericsson Nikola Tesla) or use such<br />

systems (e.g. Pliva, or many small companies).<br />

DICES is addressing efcient reusability <strong>of</strong> s<strong>of</strong>tware components and prediction <strong>of</strong> <strong>the</strong><br />

important properties for embedded systems: resource utilization, and performance,<br />

by applying <strong>the</strong> service-oriented s<strong>of</strong>tware <strong>engineering</strong> and component-based s<strong>of</strong>tware<br />

<strong>engineering</strong> methods and technologies.<br />

The main contribution <strong>of</strong> DICES is provided in two directions: a) analysis <strong>of</strong> legacy webbased<br />

systems, extraction <strong>of</strong> its design and its automatic modeling, and extraction <strong>of</strong> user<br />

interface controls and packaging <strong>the</strong>m as reusable units, and development <strong>of</strong> componentbased<br />

technology appropriate for design <strong>of</strong> embedded systems.<br />

The reverse <strong>engineering</strong>, architecture recovery and extraction <strong>of</strong> reusable UI units is applied<br />

on “iForestFire - Intelligent Forest Fire System” system developed at FESB Split, which<br />

enables thorough validation <strong>of</strong> <strong>the</strong> approach and provides input for fur<strong>the</strong>r development <strong>of</strong><br />

this system and possible commercialization <strong>of</strong> <strong>the</strong> improved product.<br />

Development <strong>of</strong> component-based technology is done in cooperation with Swedish Strategic<br />

Research Centre, PROGRESS that has developed <strong>the</strong>ories and methods for modeling<br />

component-based embedded systems. DICES contribution was in development <strong>of</strong> PRIDE,<br />

PROGRESS Integrated Development Environment, a tool modeling component-based<br />

embedded systems, simulation and analysis <strong>of</strong> resource utilization.<br />

In this article we give a short overview <strong>of</strong> <strong>the</strong>se contributions as follows. In section 2 we<br />

describe Componentizing Web Information Systems, including phpModeller, a tool for<br />

design extraction and its presentation in UML. Section 3 shows a component model that<br />

includes both, s<strong>of</strong>tware and hardware components based on UPnP devices and enables a<br />

unique treatment for s<strong>of</strong>tware and hardware components. Section 4 describes PRIDE.


156<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

2 Analysis and Componenitization <strong>of</strong> Web-based systems<br />

Web-based systems are systems that use <strong>the</strong> Internet as its core infrastructure and are<br />

accessible from anywhere in <strong>the</strong> world via <strong>the</strong> Web. Often <strong>the</strong>se systems extensively<br />

communicate with databases and third-party information sources. In some cases <strong>the</strong>y even<br />

communicate with embedded devices such as cameras or meteo-stations in order to provide<br />

real-time information about <strong>the</strong> environment. One <strong>of</strong> <strong>the</strong>se systems is <strong>the</strong> iForestFire system<br />

developed at <strong>the</strong> University <strong>of</strong> Split, Croatia. iForestFire is an intelligent and integrated<br />

video based monitoring system for early detection <strong>of</strong> forest re. The main idea is that<br />

forest res are detected in incipient stage using advanced image processing and image<br />

analyses methods. The system is based on eld units and central processing unit. The eld<br />

units are embedded devices and include day & night, pan/tilt/zoom controlled IP based<br />

video cameras and IP based mini meteorological stations connected by wired or wireless<br />

LAN to <strong>the</strong> central processing unit where all analysis, calculation, presentation, image<br />

and data archiving is done. In <strong>the</strong> scope <strong>of</strong> <strong>the</strong> DICES project, iForestFire was chosen as<br />

a case study application in order to test <strong>the</strong> ideas <strong>of</strong> componentization <strong>of</strong> Web Information<br />

Systems that extensively communicate with embedded devices.<br />

Since one <strong>of</strong> <strong>the</strong> goals <strong>of</strong> <strong>the</strong> DICES project was <strong>the</strong> analysis <strong>of</strong> legacy web-based systems,<br />

extraction <strong>of</strong> its design and its automatic modeling, extraction <strong>of</strong> User Interface controls<br />

and packaging <strong>the</strong>m as reusable units in this section, we will describe two approaches that<br />

we have developed in order to achieve those goals: phpModeler – an approach for reverse<br />

<strong>engineering</strong> <strong>of</strong> legacy web applications, and Firecrow, an approach for extracting reusable<br />

Web User Interface controls.<br />

2.1 PhpModeler – Reverse Engineering Legacy Web Applications<br />

In order to componentize web information systems, rst a correct assessment <strong>of</strong> <strong>the</strong> current<br />

state is necessary. Web information systems, especially ones that are communicating with<br />

complex embedded devices can be hard to understand because a single behavior can be<br />

realized by code executed on a large number <strong>of</strong> nodes (embedded devices, web servers,<br />

clients, etc.). Also, <strong>the</strong>re usually exist many inter-dependencies between certain parts <strong>of</strong><br />

<strong>the</strong> system that are hard to track and manage manually, and naturally <strong>the</strong> complexity <strong>of</strong><br />

<strong>the</strong>se inter-dependencies grows with <strong>the</strong> size <strong>of</strong> <strong>the</strong> web application. In order to tackle this<br />

problem and to improve development and maintenance efciency, <strong>the</strong>se applications need<br />

to be modeled on a high level <strong>of</strong> abstraction. One <strong>of</strong> <strong>the</strong> ways to achieve this goal is to use<br />

a process called Reverse Engineering (RE).<br />

Reverse Engineering (RE) is used for information extraction from source artifacts (primarily<br />

source code) and <strong>the</strong>ir transformation to easily understandable abstract representations (e.g.<br />

standard UML diagrams). Even though <strong>the</strong>re exists a certain number <strong>of</strong> already available<br />

tools for reverse <strong>engineering</strong> Web Information Systems (WARE [6], WebUml [3], ReWeb<br />

[10], etc.), none <strong>of</strong> <strong>the</strong>m have <strong>the</strong> following functionalities:<br />

• Static analysis <strong>of</strong> web application source code which as an end result produces UML<br />

diagrams that can be used for architecture recovery<br />

• Generates dependency models that show inter-dependence between web application<br />

elements<br />

• Visualizes Web application evolution.<br />

In order to tackle this problem we have developed a plugin for <strong>the</strong> Eclipse IDE (Integrated<br />

Development Environment) that facilitates modeling and web application architecture<br />

recovery called phpModeler. It has three main features: page modeling, dependency<br />

modeling and model comparison.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 157<br />

In order to be able to build page UML models, <strong>the</strong> information important for those models<br />

has to be extracted. phpModeler ga<strong>the</strong>rs this information by parsing PHP, HTML, and<br />

JavaScript code responsible for <strong>the</strong> behavior <strong>of</strong> <strong>the</strong> web application. Once this information<br />

has been collected fur<strong>the</strong>r analysis techniques can be used to establish dependencies<br />

between parts <strong>of</strong> <strong>the</strong> system. For every web page entity (JavaScript library, database<br />

table, le, PHP library, web page), <strong>the</strong> analysis nds all o<strong>the</strong>r entities dependent on it.<br />

For example, for every database table this means locating all web pages that access <strong>the</strong>m<br />

and for function libraries all web pages that use those functions. Naturally, all information<br />

ga<strong>the</strong>red in <strong>the</strong> analysis process can be generated to UML diagrams.<br />

Figure 1: Reverse Engineering Web applications with phpModeler.<br />

Web information systems evolve with <strong>the</strong> addition <strong>of</strong> new functionalities. This usually<br />

means that <strong>the</strong> existing code is modied to support <strong>the</strong> new user requirements. At different<br />

steps <strong>of</strong> <strong>the</strong> WIS evolution <strong>the</strong> system is represented with different models, so phpModeler<br />

provides a way to track <strong>the</strong> differences between two existing models. This gives a simpler,<br />

and more visual representation <strong>of</strong> <strong>the</strong> evolution <strong>of</strong> <strong>the</strong> target system. The whole process is<br />

shown in Figure 1.<br />

We used phpModeler in <strong>the</strong> reverse <strong>engineering</strong> process <strong>of</strong> <strong>the</strong> iForestFire system in order<br />

to recover <strong>the</strong> architecture and gain better understanding <strong>of</strong> <strong>the</strong> system.<br />

2.2 Firecrow – reusing Web User Interface controls<br />

Important part <strong>of</strong> <strong>the</strong> web application code is <strong>the</strong> code that is used to realize <strong>the</strong> userinterface<br />

<strong>of</strong> <strong>the</strong> web application. Web application user-interface (UI) is <strong>of</strong>ten composed<br />

<strong>of</strong> distinctive UI elements, <strong>the</strong> so called UI controls. Similar controls are <strong>of</strong>ten used in<br />

different parts <strong>of</strong> web applications (and even in different web applications) and facilitating<br />

<strong>the</strong>ir reuse could lead to faster development. Unfortunately, preparing code for reuse is a<br />

slow process which is <strong>of</strong>ten not a priority.<br />

Often, when developers encounter problems that have already been solved in <strong>the</strong> past,<br />

ra<strong>the</strong>r than re-inventing <strong>the</strong> wheel, or spending time componentizing, <strong>the</strong>y reuse <strong>the</strong> code<br />

that is already functioning in ano<strong>the</strong>r context [4]. Reuse tasks are complex and prone to<br />

errors, primarily because it is difcult to establish <strong>the</strong> minimum amount <strong>of</strong> code responsible


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for implementing <strong>the</strong> desired behavior [8].<br />

In <strong>the</strong> web application domain, reuse is especially difcult: <strong>the</strong>re is no trivial mapping<br />

between source code and <strong>the</strong> page displayed in <strong>the</strong> browser, responsible code is <strong>of</strong>ten<br />

scattered between several les and is found in between code that is not important from <strong>the</strong><br />

reuse perspective. Next, <strong>the</strong> developer has to locate and download <strong>the</strong> necessary resources,<br />

source code, and adjust for <strong>the</strong> changes so that <strong>the</strong> component can be easily integrated into<br />

an already existing system.<br />

The structure <strong>of</strong> a web page is dened by HTML code, <strong>the</strong> presentation by CSS (Cascading<br />

Style Sheets) code, and <strong>the</strong> behavior by JavaScript code. In addition, a web page usually<br />

contains various resources such as images or fonts. The interplay <strong>of</strong> <strong>the</strong>se four basic elements<br />

produces <strong>the</strong> end result displayed in <strong>the</strong> user’s web browser. Visually and behaviorally a<br />

web page can be viewed as a collection <strong>of</strong> UI controls, where each control is dened by a<br />

combination <strong>of</strong> HTML, CSS, JavaScript and resources (images, videos, fonts, etc.) that are<br />

intermixed with code and resources dening o<strong>the</strong>r parts <strong>of</strong> <strong>the</strong> web page.<br />

In order to reuse a web UI control, we have to extract all that is necessary for <strong>the</strong> control<br />

to be visually and functionally autonomous. This means extracting all HTML, CSS,<br />

JavaScript and resources that are used in <strong>the</strong> visual presentation and <strong>the</strong> desired behavior<br />

<strong>of</strong> <strong>the</strong> control. The process can be separated into three phases: 1) Interaction recording, 2)<br />

Resource extraction, and 3) UI control reuse (Figure 2).<br />

Figure 2: Extracting Web User-Interface controls.<br />

The rst step <strong>of</strong> <strong>the</strong> Interaction recording phase is to select <strong>the</strong> HTML node that denes<br />

<strong>the</strong> chosen UI control. Next, <strong>the</strong> user performs a series <strong>of</strong> interactions that represent <strong>the</strong><br />

behavior <strong>of</strong> <strong>the</strong> control. The purpose <strong>of</strong> this phase is to ga<strong>the</strong>r a log <strong>of</strong> all resources required<br />

for replicating visual and behavioral aspects <strong>of</strong> <strong>the</strong> control. This is done by logging all<br />

executed code, all CSS styles and all resources used in <strong>the</strong> lifecycle <strong>of</strong> <strong>the</strong> control.


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When <strong>the</strong> user chooses to end <strong>the</strong> recording, <strong>the</strong> process enters <strong>the</strong> Resource extraction<br />

phase, where code models for all code les (HTML, CSS, and JavaScript) are built. Based<br />

on those models and logs ga<strong>the</strong>red during <strong>the</strong> recording phase, <strong>the</strong> code necessary for<br />

replicating <strong>the</strong> visuals and <strong>the</strong> demonstrated behavior is extracted.<br />

After <strong>the</strong> extraction phase is completed, <strong>the</strong> user can enter <strong>the</strong> Reuse phase and automatically<br />

integrate <strong>the</strong> extracted control in an already existing web page, ei<strong>the</strong>r by replacing, or by<br />

embedding it inside an existing node. With this, a full cycle is completed: from seeing <strong>the</strong><br />

potential for reuse, through control extraction, all <strong>the</strong> way to actual reuse and gaining new<br />

functionalities on <strong>the</strong> target web application.<br />

The whole process is currently supported by <strong>the</strong> Firecrow tool, which is an extension for <strong>the</strong><br />

Firebug web debugger. Currently, <strong>the</strong> tool can be used from <strong>the</strong> Firefox web browser, but<br />

it can be ported to any o<strong>the</strong>r web browser that provides communication with a JavaScript<br />

debugger, and a DOM explorer (e.g. IE, Chrome, Opera). The interaction recording phase<br />

is <strong>the</strong> only part <strong>of</strong> <strong>the</strong> process that is browser dependent; building source models, extracting<br />

code, downloading resources, merging code and resources are all functionalities that are all<br />

encapsulated in a library that can be called from any browser on any operating system. The<br />

whole source <strong>of</strong> <strong>the</strong> program can be downloaded from [18].<br />

3 Hardware and S<strong>of</strong>tware Components<br />

The main purpose <strong>of</strong> embedded systems is to monitor or control processes in <strong>the</strong>ir<br />

environment. This interaction <strong>of</strong> s<strong>of</strong>tware with <strong>the</strong> real world requires integration <strong>of</strong><br />

s<strong>of</strong>tware components with hardware components such as sensors and actuators. However,<br />

coping with <strong>the</strong>se two different parts <strong>of</strong> embedded systems simultaneously is still a<br />

challenge. Current component models for embedded systems mostly focus on s<strong>of</strong>tware<br />

components and rarely try to provide extensive support hardware component [7]. In DICES<br />

project we have also addressed this aspect <strong>of</strong> component-based s<strong>of</strong>tware development. One<br />

<strong>of</strong> <strong>the</strong> results <strong>of</strong> our research is UComp component model and supporting technology [9].<br />

3.1 UComp – component-based development for hardware and s<strong>of</strong>tware components<br />

The focus <strong>of</strong> UComp is on distributed systems whose functionality is implemented using<br />

various devices connected to a computer network. These devices may ei<strong>the</strong>r be physical, i.e.<br />

realized using hardware, or virtual, i.e. realized using s<strong>of</strong>tware applications. Main goal <strong>of</strong><br />

UComp is to utilise <strong>the</strong> component-based approach and manage <strong>the</strong> hardware and s<strong>of</strong>tware<br />

components in a uniform way. Fur<strong>the</strong>r, our goal is to apply <strong>the</strong> component-based approach<br />

during whole life-cycle <strong>of</strong> a system, including run-time phase. By having <strong>the</strong> components<br />

available at run-time, systems can be extremely exible because any modications can be<br />

done while <strong>the</strong> system is running and <strong>the</strong> embedded devices are deployed. In addition, this<br />

would allow easier late deployment <strong>of</strong> new devices (i.e. components) or replacement <strong>of</strong><br />

existing ones during run-time.<br />

3.1.1 The UComp component model<br />

UComp distinguishes between two types <strong>of</strong> components: Device components and s<strong>of</strong>tware<br />

components. Device components are used to communicate with hardware or virtual network<br />

devices and provide <strong>the</strong>ir functionalities in a component-based manner. Functionality <strong>of</strong><br />

s<strong>of</strong>tware components is fully implemented in program code, and <strong>the</strong>se components are not<br />

associated with any devices. They are used for additional computations in order to avoid<br />

<strong>the</strong> need for “glue code”.


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Component interfaces consist <strong>of</strong> input and output ports. Ports can be considered as<br />

component access points, used for a component to exchange data and control (triggering)<br />

signals. System execution follows <strong>the</strong> pipes and lter pattern. Data and triggering signals<br />

from output port <strong>of</strong> one component can be directed to input ports <strong>of</strong> one or more components.<br />

When an input port receives a signal from <strong>the</strong> output port it is connected to, it becomes<br />

active. A component can be congured to start it’s execution when ei<strong>the</strong>r all or just selected<br />

ports are activated. This is done by selecting activation types for ports. There are three<br />

activation types for input ports:<br />

• Trigger. A component is activated if all input ports with activation type set to trigger<br />

are active.<br />

• Priority trigger. A component is activated if any <strong>of</strong> its input port with activation type<br />

set to priority trigger is active.<br />

• Data. If port’s activation type is set to data, it is only used to receive data, and does not<br />

affect <strong>the</strong> triggering <strong>of</strong> <strong>the</strong> component.<br />

The graphical representation <strong>of</strong> output ports and all input port types can be seen in Figure<br />

3. The gure shows an instance <strong>of</strong> Component A having input ports a (data port), b (trigger<br />

port) and c (priority trigger port), and an output port out.<br />

Figure 3: Graphical representation <strong>of</strong> an UComp component and its input and output ports.<br />

3.1.2 Device Components<br />

Device components are <strong>the</strong> base for accomplishing <strong>the</strong> uniform treatment <strong>of</strong> components <strong>of</strong><br />

a system, which is not dependant on component realization (hardware or s<strong>of</strong>tware). They<br />

represent hardware (physical) and virtual (realized using s<strong>of</strong>tware applications) network<br />

devices.<br />

Device components, toge<strong>the</strong>r with <strong>the</strong>ir input and output ports, are automatically generated<br />

by <strong>the</strong> UComp framework using device descriptions. Automatic generation <strong>of</strong> devices<br />

and <strong>the</strong>ir ports eliminates need for specialized drivers or manual conguration <strong>of</strong> such<br />

components by <strong>the</strong> developer <strong>of</strong> <strong>the</strong> system.<br />

Every device component signals if <strong>the</strong> actual device is available on <strong>the</strong> network. This<br />

information can be very useful in distributed systems where connection between<br />

components is not reliable and some <strong>of</strong> <strong>the</strong>m can be temporarily unavailable.<br />

Device components can represent actions (synchronous request-response communication)<br />

or events (asynchronous publish-subscribe messaging) <strong>of</strong> network devices. Therefore, we<br />

have dened two types <strong>of</strong> device components: action components and event components.<br />

Action Components. Action components are designed to wrap around synchronous action<br />

invocations or data queries <strong>of</strong> a device connected to <strong>the</strong> network.<br />

When an action component is triggered, action invocation is performed, using values <strong>of</strong><br />

its input ports as arguments. When <strong>the</strong> invocation nishes, results <strong>of</strong> <strong>the</strong> invocation are


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propagated to output ports <strong>of</strong> <strong>the</strong> components.<br />

Event Components. Event components allow receiving asynchronous messages from<br />

devices. These messages may signal data changes or o<strong>the</strong>r events that device may provide.<br />

Interfaces <strong>of</strong> event components have only output ports, which obtain <strong>the</strong>ir values from<br />

event notications provided by <strong>the</strong> network device.<br />

3.1.3 S<strong>of</strong>tware Components<br />

Functionality <strong>of</strong> s<strong>of</strong>tware components is fully implemented by program code, and <strong>the</strong>y are<br />

not bound to any hardware elements. They are used to process <strong>the</strong> data received from, or<br />

sent to, device components or manipulate <strong>the</strong> execution <strong>of</strong> components. Their function can<br />

vary from very simple (for example addition <strong>of</strong> two numbers) to complex data processing.<br />

Execution Semantics<br />

Initially, all components in <strong>the</strong> system are in an idle state waiting to be activated for<br />

execution. Activation can be caused ei<strong>the</strong>r by <strong>the</strong> triggering signals received at <strong>the</strong> input<br />

ports <strong>of</strong> <strong>the</strong> component, or by its internal events. Action components and most s<strong>of</strong>tware<br />

components are passive, meaning that <strong>the</strong>y execute only when <strong>the</strong>y are triggered by signals<br />

received from o<strong>the</strong>r components, while event components and some s<strong>of</strong>tware components<br />

are active and thus may start <strong>the</strong>ir execution by an internal event.<br />

Realisation <strong>of</strong> UComp Component Model<br />

The UComp architecture, shown in Figure 4, is realised as Java application that implements<br />

<strong>the</strong> Universal Plug and Play (UpnP) [16] technology to control devices available on <strong>the</strong><br />

network, process <strong>the</strong>ir data, and relay data between <strong>the</strong>m. The application communicates<br />

with devices through a single UPnP control point implemented using CyberLink UPnP<br />

stack [11]. Centralized architecture allows us to process data received from a device by<br />

UComp application before it is forwarded to o<strong>the</strong>r devices, making <strong>the</strong> system much more<br />

exible and eliminating <strong>the</strong> need to change <strong>the</strong> code <strong>of</strong> devices to adapt <strong>the</strong>m to <strong>the</strong> needs<br />

<strong>of</strong> <strong>the</strong> developed system. Also, run-time modication <strong>of</strong> systems is much easier. System’s<br />

behaviour can be modied by simple changes in <strong>the</strong> interconnection <strong>of</strong> components (or by<br />

changing <strong>the</strong> components <strong>the</strong>mselves) in <strong>the</strong> central application.<br />

4 Development environment<br />

Figure 4: The UComp architecture.


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To facilitate <strong>the</strong> development we have created a tool for visual development <strong>of</strong> UComp<br />

systems - UComp Developer. The UComp Developer enables browsing available device<br />

and s<strong>of</strong>tware components using a tree structure, visual representation <strong>of</strong> components on a<br />

development panel, modifying connections between <strong>the</strong>m, setting <strong>the</strong>ir properties and <strong>the</strong><br />

properties <strong>of</strong> <strong>the</strong>ir ports, and starting and stopping <strong>the</strong> execution <strong>of</strong> <strong>the</strong> developed system.<br />

Systems developed with this tool are saved or restored from XML les.<br />

A screen-shot <strong>of</strong> UComp Developer is shown in Figure 5.<br />

5 An overview <strong>of</strong> <strong>the</strong> PRIDE tool<br />

Figure 5: Screenshot <strong>of</strong> UComp Developer tool.<br />

PROGRESS-IDE (PRIDE) is an integrated development environment used for s<strong>of</strong>tware<br />

development <strong>of</strong> distributed embedded systems (ES), primarily in <strong>the</strong> automotive,<br />

automation and telecom domains. The grand vision <strong>of</strong> Progress-IDE is to cover <strong>the</strong> whole<br />

s<strong>of</strong>tware development cycle <strong>of</strong> distributed embedded systems, from early system design<br />

to deployment and syn<strong>the</strong>sis. The development process <strong>of</strong> ES requires a strong emphasis<br />

on analysis, verication and validation in order to ensure <strong>the</strong> necessary quality <strong>of</strong> <strong>the</strong><br />

delivered product, <strong>the</strong>refore PRIDE integrates various analysis tools. Compared to <strong>the</strong><br />

majority <strong>of</strong> existing IDEs that focus mainly on <strong>the</strong> programming aspect, PRIDE uses <strong>the</strong><br />

notion <strong>of</strong> component as a rst-class concept allowing <strong>the</strong> manipulation and modelling <strong>of</strong><br />

components, with reusability as one <strong>of</strong> <strong>the</strong> key concerns and supporting:<br />

• Component and system design using <strong>the</strong> ProCom component model [13],<br />

• System analysis (worst-case execution time, model checking <strong>of</strong> behavioural models<br />

and fault propagation and transformation calculus),<br />

• Deployment modelling<br />

• Code syn<strong>the</strong>sis.


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In <strong>the</strong> following list we give some overall reections that apply to Progress-IDE.<br />

• Progress-IDE covers <strong>the</strong> whole system development process,<br />

• Progress-IDE is developed as a stand-alone application on top <strong>of</strong> Eclipse RCP,<br />

• Progress-IDE consists <strong>of</strong> a number <strong>of</strong> editors: architectural editors, attribute editor, node<br />

description (virtual/physical), allocation editor, code generation, various analysis editors,<br />

• Progress-IDE is user-friendly by providing a user interface respecting <strong>the</strong> usability<br />

features, partial auto-completion features, default values etc.<br />

5.1 The PRIDE approach<br />

In <strong>the</strong> recent years ES development has changed signicantly due to <strong>the</strong> rapid increase <strong>of</strong><br />

s<strong>of</strong>tware in <strong>the</strong>se systems and s<strong>of</strong>tware becoming as complex as in conventional systems.<br />

In non-embedded domains, new approaches such as model-based, component-based, and<br />

service-oriented development have been proposed to manage s<strong>of</strong>tware complexity and<br />

<strong>the</strong>re is a trend to apply <strong>the</strong>se approaches also in ES development. ES correctness is strongly<br />

correlated to specic extra-functional properties (EFPs) such as timing (e.g. execution and<br />

response time) or dependability (e.g. reliability and safety) under constrained resources<br />

such as memory, energy, or computation speed. This calls for additional domain-specic<br />

technologies that provide support not only for functional development but also for analysis<br />

and verication <strong>of</strong> EFPs.<br />

As a possible solution, we have been developing a new component-based approach [5]<br />

built around a two-layer component model - ProCom, which addresses <strong>the</strong> particularity<br />

<strong>of</strong> ES development from big complex functionalities, to small, close to control loop<br />

functionalities. This approach requires specic tool support that enables:<br />

Efcient system design by using existing components,<br />

Seamless integration <strong>of</strong> different tools to provide <strong>the</strong> analysis and verication required for<br />

system correctness, and<br />

Ef cient EFP management <strong>of</strong> components and systems.<br />

PRIDE uses reusable s<strong>of</strong>tware components as <strong>the</strong> central development units, and as a<br />

means to support and aggregate various analysis and verication techniques. In difference<br />

to similar approaches [1, 2, 17], PRIDE puts emphasis on EFPs during <strong>the</strong> entire lifecycle<br />

- from early specication to deployment and syn<strong>the</strong>sis.<br />

PRIDE has been designed to support four design strategies that are especially important to<br />

consider for having an efcient component-based development <strong>of</strong> ES.<br />

Levels <strong>of</strong> abstraction<br />

Using components throughout <strong>the</strong> whole development process implies that <strong>the</strong> component<br />

concept spans a wide range <strong>of</strong> abstractions, from a vague and incomplete early specication,<br />

to very “concrete” with a xed specication, a corresponding implementation and<br />

information about <strong>the</strong>ir EFPs. This means that components at different levels <strong>of</strong> abstraction<br />

must be able to co-exist within <strong>the</strong> same model.<br />

Component granularity<br />

In distributed ES, components span a large variety in size and complexity; <strong>the</strong> larger<br />

components are typically active (i.e. with <strong>the</strong>ir own thread <strong>of</strong> execution) with an<br />

asynchronous message passing communication style, whereas <strong>the</strong> smaller components are<br />

responsible for a part <strong>of</strong> control functionality with a strong synchronization. For an efcient<br />

development, a support for handling different types <strong>of</strong> components must be provided.<br />

Component vs. system development<br />

The common distinction between component development and system development brings


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issues in ES development, where <strong>the</strong> coupling between <strong>the</strong> hardware platform and <strong>the</strong><br />

s<strong>of</strong>tware is particularly tight. As a consequence, component development needs some<br />

knowledge <strong>of</strong> where <strong>the</strong> components are to be deployed. This requires support to handle<br />

<strong>the</strong> coupling between components, system and target platform, while still allowing separate<br />

development <strong>of</strong> components and systems.<br />

Extra-functional properties<br />

The correctness <strong>of</strong> ES is ascertained based on both <strong>the</strong> functional and extra-functional<br />

aspects. However, many EFPs typically encountered in ES are assessed through different<br />

methods during <strong>the</strong> development lifecycle (from early estimation to precise measurements)<br />

and different values may be obtained according to <strong>the</strong> characteristics <strong>of</strong> <strong>the</strong> resources <strong>of</strong><br />

<strong>the</strong> platform on which <strong>the</strong> components are to be deployed. For this reason, an efcient<br />

ES development should provide a means for specifying, managing and verifying <strong>the</strong>se<br />

properties with respect to <strong>the</strong> context in which <strong>the</strong>ir values are provided.<br />

To comply with <strong>the</strong> design strategies, <strong>the</strong> following requirements have been identied as<br />

principles that guided <strong>the</strong> design and development <strong>of</strong> PRIDE:<br />

Allowing to move freely between any development stages,<br />

Displaying <strong>the</strong> consequences <strong>of</strong> a change in <strong>the</strong> system or within a component,<br />

Supporting <strong>the</strong> coupling with <strong>the</strong> hardware platform, and<br />

Enabling and enforcing <strong>the</strong> analysis, validation and verication steps.<br />

In addition, a central requirement relates to <strong>the</strong> notion <strong>of</strong> component. Components are <strong>the</strong><br />

main units <strong>of</strong> development and seen as rich-design artifacts that exist throughout <strong>the</strong> whole<br />

development lifecycle, from early design stage, in which little information about <strong>the</strong>m<br />

exists, to deployment and syn<strong>the</strong>sis stages, in which <strong>the</strong>y are fully implemented. PRIDE<br />

views a component as a collection <strong>of</strong> all <strong>the</strong> development artefacts (requirements, models,<br />

EFPs, documentation, tests, source code, etc.), and enables <strong>the</strong>ir manipulation in a uniform<br />

way.<br />

Driven by <strong>the</strong> aforementioned principles, several tools have been developed and tightly<br />

integrated into PRIDE. Since <strong>the</strong> PRIDE is built as an Eclipse RCP application, it can be<br />

easily extended with addition <strong>of</strong> new plugins.<br />

5.2 Implementation <strong>of</strong> PRIDE<br />

The Eclipse platform is chosen as <strong>the</strong> supporting architecture for PRIDE. In order to reduce<br />

<strong>the</strong> overhead which exists when using Eclipse directly as <strong>the</strong> main integration environment,<br />

it has been decided that <strong>the</strong> PRIDE will be developed as a stand-alone application built on<br />

top <strong>of</strong> <strong>the</strong> Eclipse Rich Client Platform (Eclipse RCP). This decision is driven by <strong>the</strong> will<br />

to keep <strong>the</strong> control over <strong>the</strong> features present in <strong>the</strong> environment such as, for example,<br />

avoiding <strong>the</strong> presence <strong>of</strong> menus not directly related to <strong>the</strong> particular use <strong>of</strong> <strong>the</strong> PRIDE.<br />

When using Eclipse RCP, only <strong>the</strong> features explicitly added to <strong>the</strong> environment are present.<br />

In o<strong>the</strong>r words, <strong>the</strong> layout and function <strong>of</strong> <strong>the</strong> environment are fully controlled by <strong>the</strong><br />

plugin developers.<br />

The component architecture design part <strong>of</strong> <strong>the</strong> environment was implemented using EMF<br />

[14] and GMF [15]. EMF is a modelling framework and code generation facility for<br />

building tools based on a structured data model. It <strong>of</strong>fers a graphical editor for describing<br />

metamodels. With <strong>the</strong> aid <strong>of</strong> this, <strong>the</strong> ProCom metamodel (model <strong>of</strong> <strong>the</strong> ProCom model)<br />

was dened. From this graphical description <strong>of</strong> <strong>the</strong> metamodel, EMF automatically<br />

generates Java classes representing <strong>the</strong> model, classes used for modifying <strong>the</strong> model and<br />

textual tree editors for <strong>the</strong> model. GEF <strong>the</strong>n takes this existing application model (i.e.<br />

<strong>the</strong> model generated using EMF) and quickly creates a rich graphical editor. However,<br />

this automatically generated editor has rudimentary functionality and needs to be fur<strong>the</strong>r


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 165<br />

manually modied and tweaked in order to achieve <strong>the</strong> desired functionality.<br />

S<strong>of</strong>tware architecture modelling and analysis<br />

As already mentioned, PRIDE uses component-based approach which allows components<br />

to be developed independently and reused in different contexts. Reusability is one <strong>of</strong><br />

<strong>the</strong> main concepts in PRIDE aiming to signicantly shorten development time. The tool<br />

makes a distinction between a component type and a component instance. Each reusage<br />

<strong>of</strong> a component creates a component instance <strong>of</strong> <strong>the</strong> given component type. By editing <strong>the</strong><br />

component all <strong>of</strong> its instances are affected.<br />

In PRIDE components are rich design entities encapsulating a collection <strong>of</strong> development<br />

artefacts; requirements, various models (e.g. architectural, behavioural, resource usage<br />

etc.), EFPs, documentation, tests and source code.<br />

Figure 6 shows a screenshot from PRIDE with main parts highlighted. PRIDE’s modelling<br />

part consists <strong>of</strong> a component explorer and component editors.<br />

Figure 6: A screenshot from PRIDE showing a) <strong>the</strong> component explorer; b) <strong>the</strong> component editor;<br />

c) <strong>the</strong> code editor; d) <strong>the</strong> repository browser; and e) <strong>the</strong> attribute framework.<br />

Component Explorer<br />

Enables browsing <strong>the</strong> list <strong>of</strong> <strong>the</strong> components available in <strong>the</strong> current development project.<br />

In it a component owns a predened and extensible information structure corresponding<br />

to a rich component concept. It also provides a support for component versioning and<br />

importing and exporting from a project to a component repository making <strong>the</strong>m available<br />

to o<strong>the</strong>r projects thus facilitating <strong>the</strong> component reusability.<br />

Component Editors<br />

Although <strong>the</strong> ProCom component model distinguishes between two different types <strong>of</strong><br />

components (ProSave and ProSys), in <strong>the</strong> component editors all components are treated<br />

in a uniform way. Component editors provide two independent views on a component,<br />

external and internal view. The external view manages <strong>the</strong> component specication<br />

and interface such as <strong>the</strong> information about <strong>the</strong> component name, its interface (services<br />

and ports) and EFPs. The internal view focus on component’s internal structure i.e. its<br />

realization and implementation and it depends in <strong>the</strong> component realization type. For<br />

primitive components, <strong>the</strong> internal view is linked to <strong>the</strong> component implementation and


166<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

<strong>the</strong> source code is displayed. For composite components, <strong>the</strong> internal view corresponds<br />

to an interconnection <strong>of</strong> subcomponent instances and a graphical form is made available<br />

allowing to make modications in this inner structure (addition/deletion <strong>of</strong> component<br />

instances, connectors, change in <strong>the</strong> connections, etc.).<br />

The analysis support in PRIDE is based on two main parts, an attribute framework and an<br />

analysis framework.<br />

Attribute Framework<br />

The purpose <strong>of</strong> <strong>the</strong> attribute framework [12] is to provide a uniform and user-friendly<br />

structure to seamlessly manage EFPs in a systematic way. The attribute framework enables<br />

attaching extra-functional properties to any architectural element such as a specic port,<br />

service or <strong>the</strong> component as a whole. Attributes are dened by attribute types, and include<br />

attribute values with metadata and <strong>the</strong> specication <strong>of</strong> <strong>the</strong> conditions under which <strong>the</strong><br />

attribute value is valid. One key feature is that <strong>the</strong> attribute framework allows an attribute<br />

to be given additional values during <strong>the</strong> development without replacing old values.<br />

This allows dening <strong>of</strong> early estimates for EFPs even before <strong>the</strong> component has been<br />

implemented and use it for analysis in early stages <strong>of</strong> system development. New, userdened<br />

attribute types can also be added to <strong>the</strong> model.<br />

Analysis framework<br />

The analysis framework provides a common platform for integrating in a consistent<br />

way various analysis techniques, ranging from simple constraint checking and attribute<br />

derivation (e.g., propagating port type information over connections), to complex external<br />

analysis tools. Analysis results can ei<strong>the</strong>r be presented to <strong>the</strong> user directly, or stored as<br />

component attributes. They are also added to a common analysis result log, allowing <strong>the</strong><br />

user easy access to earlier analysis results. PRIDE also allows to easily integrate new<br />

analysis techniques toge<strong>the</strong>r with <strong>the</strong>ir associated EFPs.<br />

6 Conclusion<br />

In this paper we gave an overview <strong>of</strong> some <strong>of</strong> <strong>the</strong> results <strong>of</strong> DICES project. The project<br />

focus was on distributed embedded systems and <strong>the</strong> overview shows that a large variety<br />

<strong>of</strong> technologies and approaches are needed for an efcient development and maintenance<br />

<strong>of</strong> embedded systems. The project is focused on several phases in <strong>the</strong> lifecycle: a) reverse<br />

<strong>engineering</strong> and analysis <strong>of</strong> <strong>the</strong> existing legacy code that helps in reusability in development<br />

<strong>of</strong> new systems from existing components; b) modelling and designing embedded systems<br />

that include both s<strong>of</strong>tware and hardware components, and ability to perform different<br />

types <strong>of</strong> analysis important for embedded systems (e.g. resources utilization, performance,<br />

timing characteristics). The work done shows that <strong>the</strong> embedded systems <strong>of</strong> today are<br />

complex system, in <strong>the</strong> rst hand with complex s<strong>of</strong>tware that is approaching in size and<br />

complexity s<strong>of</strong>tware from o<strong>the</strong>r domains.<br />

Acknowledgment<br />

This work was supported by <strong>the</strong> Swedish Foundation for Strategic Research via <strong>the</strong><br />

strategic research centre Progress, Croatian Ministry <strong>of</strong> science, education and sports via<br />

<strong>the</strong> research project S<strong>of</strong>tware <strong>engineering</strong> in ubiquitous computing, and <strong>the</strong> Unity Through<br />

Knowledge Fund via <strong>the</strong> Dices project.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 167<br />

References<br />

1. Akerholm M., Carlson J., Fredriksson J., Hansson H., Hakansson J., Möller A., Pettersson<br />

P., Tivoli M. (2007) The SAVE Approach to Component-Based Development <strong>of</strong> Vehicular<br />

Systems, In: Journal <strong>of</strong> Systems and S<strong>of</strong>tware, Elsevier Science, pp. 655-667<br />

2. Articus Systems, Rubus S<strong>of</strong>tware Components, http://www.arcticus-systems.com ,<br />

Accessed 7 March <strong>2011</strong><br />

3. Bellettini C., Marchetto A., Trentini A. (2004) WebUml: reverse <strong>engineering</strong> <strong>of</strong> web<br />

applications, In: Symposium on Applied computing, ACM New York, NY, USA, 1662-<br />

1669<br />

4. Brandt J., Guo J.P., Lewenstein J., Klemmer S.R. (2008) Opportunistic programming:<br />

How rapid ideation and prototyping occur in practice, In: Workshop on End-user s<strong>of</strong>tware<br />

<strong>engineering</strong>, ACM New York, NY, USA, pp. 1-5<br />

5. Bureš T., Carlson J., Sentilles S., Vulgarakis A. (2008) A Component Model Family<br />

for Vehicular Embedded Systems, In: The Third International Conference on S<strong>of</strong>tware<br />

Engineering Advances, IEEE Computer Society Washington, DC, USA, pp. 437-444<br />

6. Di Lucca G., Fasolino A.r., Tramontana P. (2004) Reverse <strong>engineering</strong> Web applications:<br />

<strong>the</strong> WARE approach, In: Journal <strong>of</strong> S<strong>of</strong>tware Maintenance and Evolution: Research and<br />

Practice - Special issue: Web site evolution Volume 16 Issue 1-2, John Wiley & Sons, Inc.<br />

New York, NY, USA, pp. 71-101<br />

7. Feljan J., Lednicki L., Maras J., Petricic A., Crnkovi I. (2009) Classication and survey <strong>of</strong><br />

component models, MRTC report ISSN 1404-3041 ISRN MDH-MRTC-242/2009-1-SE,<br />

Mälardalen Real-Time Research Centre, Mälardalen University<br />

8. Holmes R.(2008) Pragmatic S<strong>of</strong>tware Reuse, Ph.D. Dissertation, University <strong>of</strong> Calgary<br />

9. Lednicki, L. and Petricic, A. and Zagar, M. (2009) A Component-Based Technology<br />

for Hardware and S<strong>of</strong>tware Components, In: S<strong>of</strong>tware Engineering and Advanced<br />

Applications, 2009. SEAA ‘09. 35th Euromicro Conference on, IEEE Computer Society<br />

Washington, DC, USA, pp. 450 -453<br />

10. Ricca F., Tonella P. (2001) Understanding and Restructuring Web Sites with ReWeb, IEEE<br />

Multimedia, Vol 8, Issue 2, pp. 40-51<br />

11. Satoshi Konno, CyberLink for Java, http://www.cybergarage.org/twiki/bin/view/Main/<br />

CyberLinkForJava , Accessed 7 March <strong>2011</strong><br />

12. Sentilles S., Štpán P., Carlson J., Crnkovi I. (2009) Integration <strong>of</strong> Extra-Functional<br />

Properties in Component Models, In: Proceedings <strong>of</strong> <strong>the</strong> 12th International Symposium on<br />

Component-Based S<strong>of</strong>tware Engineering (CBSE ‘09), Springer-Verlag Berlin, Heidelberg,<br />

pp. 173-190<br />

13. Sentilles S., Vulgarakis A., Bureš T., Carlson J., Crnkovi I. (2008) A Component Model<br />

for Control-Intensive Distributed Embedded Systems, In: Proceedings <strong>of</strong> <strong>the</strong> 11th<br />

International Symposium on Component-Based S<strong>of</strong>tware Engineering (CBSE ‘08),<br />

Springer-Verlag Berlin, Heidelberg, pp. 310-317<br />

14. The Eclipse Foundation, Eclipse Modeling Framework Project, http://www.eclipse.org/<br />

emf/ , Accessed 7 March <strong>2011</strong><br />

15. The Eclipse Fundation, Graphical Modeling Framework, http://http://www.eclipse.org/<br />

gmf , Accessed 7 March <strong>2011</strong><br />

16. UPnP forum, Universal Plug and Play, http://www.upnp.org , Accessed 7 March <strong>2011</strong><br />

17. van Ommering R., van der Linden F., Kramer J., Magee J. (2000) The Koala component<br />

model for consumer electronics s<strong>of</strong>tware, In: IEEE Computer, , IEEE Computer Society<br />

Washington, DC, USA, pp. 78-85<br />

18. Maras J., Štula M., Carlson J, Crnkovi I. (<strong>2011</strong>). Firecrow web page, http://www.fesb.<br />

hr/~jomaras/?id=Firecrow, Accessed 7 March <strong>2011</strong>


168<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Framework for 3D Motion Field Estimation and<br />

Reconstruction<br />

Martin Žagar, Hrvoje Mlinarić, Josip Knezović<br />

Department <strong>of</strong> Control and Computer Engineering, Faculty <strong>of</strong> Electrical Engineering<br />

and Computing, Unska 3, HR-10000 Zagreb, Croatia<br />

Abstract:<br />

We propose <strong>the</strong> framework for <strong>the</strong> motion estimation <strong>of</strong> 3D objects based on <strong>the</strong> motion<br />

vectors that form motion elds and <strong>the</strong> motion reconstruction based on <strong>the</strong> 3D rotations<br />

and <strong>the</strong> factorization method. The classical two-dimensional motion eld approach is<br />

extended to three dimensions, e.g. on <strong>the</strong> volumetric objects that are moving in time. When<br />

dealing with <strong>the</strong> real world multiple moving objects and <strong>the</strong> complex scenes, lots <strong>of</strong> objects<br />

are moving with different motions, both in space and in time. In this context, an object<br />

can be described as a part <strong>of</strong> a scene that moves with a coherent motion and <strong>the</strong> scene can<br />

be broken down into a number <strong>of</strong> regions, each <strong>of</strong> which can be well approximated by its<br />

own motion. The rst part <strong>of</strong> this paper describes <strong>the</strong> motion vectors based techniques<br />

which are used for <strong>the</strong> motion estimation, and <strong>the</strong> second part addresses problems with <strong>the</strong><br />

reconstruction <strong>of</strong> <strong>the</strong> 3D motion and structure. Proposed methods estimate reconstruction<br />

from a sparse set <strong>of</strong> <strong>the</strong> matched volume features on <strong>the</strong> 3D neuroimage in NIfTI format.<br />

We evaluate <strong>the</strong>se techniques according to <strong>the</strong> different problems <strong>the</strong>y address.<br />

Keywords: 3D motion estimation, differential techniques, matching techniques, motion<br />

and structure reconstruction, factorization method.<br />

1 INTRODUCTION<br />

The motion estimation is used to eliminate a large amount <strong>of</strong> temporal and spatial<br />

redundancy that exists in sequences <strong>of</strong> 3D data. Most video encoders perform <strong>the</strong> motion<br />

estimation in video sequences to search for <strong>the</strong> motion information in sequential video<br />

frames that can improve compression. The difference between <strong>the</strong> current frame and <strong>the</strong><br />

predicted frame in motion estimation and motion reconstruction (based on previous and/or<br />

future frames) is coded and transmitted. The better <strong>the</strong> prediction is, <strong>the</strong> smaller <strong>the</strong> error<br />

and hence <strong>the</strong> transmission bit rates are. If a scene is still, <strong>the</strong>n a good prediction for <strong>the</strong><br />

particular object in <strong>the</strong> current frame is <strong>the</strong> same as object in <strong>the</strong> previous frame and <strong>the</strong><br />

error is close to zero. However, when <strong>the</strong>re is a motion in a sequence, an estimation <strong>of</strong> <strong>the</strong><br />

predicted position <strong>of</strong> <strong>the</strong> object in <strong>the</strong> current frame can be made with <strong>the</strong> motion vectors<br />

[7], [10]. Many techniques based on <strong>the</strong> motion vectors that form motion elds can be<br />

roughly divided into two major classes: differential techniques and feature-based matching<br />

techniques [9]. The differential techniques are based on <strong>the</strong> spatial and temporal variations<br />

<strong>of</strong> <strong>the</strong> volume brightness at all voxels, and can be regarded as methods for computing<br />

optical ow. The matching techniques, instead, estimate <strong>the</strong> disparity <strong>of</strong> special volume<br />

points (features) between frames. Proposed methods are evaluated on 3D neuroimages<br />

in NIfTI (Neuroimaging Informatics Technology Initiative) format which is designed to


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 169<br />

maximize <strong>the</strong> usability <strong>of</strong> neuroimaging computing tools and provide a common resource<br />

for researches in magnetic resonance imaging (MRI). It is used for <strong>the</strong> detailed visualization<br />

<strong>of</strong> internal structure and functions <strong>of</strong> <strong>the</strong> human body. The main purpose <strong>of</strong> determining<br />

motion in MRI is to reduce a vast amount <strong>of</strong> acquired data in coding process. For different<br />

types <strong>of</strong> MRI, different motion techniques should be used for motion estimation and motion<br />

reconstruction. Estimation <strong>of</strong> 3D motion eld is based on <strong>the</strong> motion vectors and is used to<br />

predict and to describe motion between <strong>the</strong> current and <strong>the</strong> next frame. With coding only<br />

motion vectors instead <strong>of</strong> whole dataset, higher compression ratio can be achieved. On <strong>the</strong><br />

o<strong>the</strong>r hand, in <strong>the</strong> motion reconstruction, 3D motion is reconstructed from a sparse set <strong>of</strong><br />

matched volume features.<br />

The paper is organized as follows. Our proposed differential and matching techniques are<br />

described in Section 2. We adapted motion vectors based techniques as one <strong>of</strong> appropriate<br />

techniques for motion estimation and factorization method for 3D motion reconstruction.<br />

Factorization method is described in Section 3.2, while <strong>the</strong> beginning <strong>of</strong> Section 3 presents<br />

our 3D edge detection method for segmentation, based on Canny 2D edge detection [11].<br />

The segmentation is necessary when dealing with multiple moving objects to detect and<br />

to segment objects that are moving with different motions in space in time. Experimental<br />

results <strong>of</strong> proposed methods and techniques are presented in Section 4 and concluded in<br />

Section 5.<br />

2 MOTION VECTORS BASED TECHNIQUES<br />

2.1 Differential Techniques based on Optical Flow<br />

A large number <strong>of</strong> differential techniques for computing <strong>the</strong> optical ow have been proposed<br />

[1], [3], [8]. Some <strong>of</strong> <strong>the</strong>m require <strong>the</strong> solution <strong>of</strong> a system <strong>of</strong> partial differential equations,<br />

o<strong>the</strong>rs <strong>the</strong> computation <strong>of</strong> second and higher-order derivatives <strong>of</strong> <strong>the</strong> volume brightness<br />

and some <strong>of</strong> <strong>the</strong>m require <strong>the</strong> least-squares estimates <strong>of</strong> <strong>the</strong> parameters characterizing <strong>the</strong><br />

optical ow. Methods in <strong>the</strong> latter class have at least two advantages over those in <strong>the</strong> rst<br />

two:<br />

• They are not iterative; <strong>the</strong>refore <strong>the</strong>y are genuinely local and less biased by possible<br />

discontinuities <strong>of</strong> <strong>the</strong> motion eld than iterative methods.<br />

• They do not involve derivatives <strong>of</strong> order higher than <strong>the</strong> rst; <strong>the</strong>refore, <strong>the</strong>y are less<br />

sensitive to noise than methods requiring higher-order derivatives.<br />

2.1.1 Optical flow<br />

Our proposed differential technique is <strong>the</strong> extension <strong>of</strong> 2D motion eld estimation ([3],<br />

[11]) to 3D. It is based on <strong>the</strong> least-squares estimates <strong>of</strong> <strong>the</strong> parameters characterizing<br />

<strong>the</strong> optical ow. The basic assumption is that <strong>the</strong> motion eld is well approximated by a<br />

constant vector eld velocity v r<br />

within any small region <strong>of</strong> <strong>the</strong> volume plane. The optical<br />

ow is <strong>the</strong> approximation <strong>of</strong> <strong>the</strong> motion eld which can be computed from time-varying<br />

volume sequences. For each point p i<br />

within a small patch Q <strong>of</strong> size N x N x N, it can be<br />

written<br />

∂E<br />

( ∇E) T r<br />

v + = 0<br />

(1)<br />

∂t<br />

where E = E(x,y,z,t) is volumetric brightness for voxel at point p(x,y,z) at time t. The spatial<br />

and <strong>the</strong> temporal derivatives <strong>of</strong> <strong>the</strong> volumetric brightness are computed at points (voxels)


170<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

p , p , p ∈<br />

1 2<br />

K , 3 Q . Therefore, <strong>the</strong> optical ow can be estimated within Q as<br />

N<br />

<strong>the</strong> constant vector, v r that minimizes <strong>the</strong> functional<br />

2<br />

T E<br />

<br />

v E<br />

v . (2)<br />

<br />

p Q<br />

t<br />

<br />

i<br />

The solution <strong>of</strong> <strong>the</strong> least squares problem can be found by solving <strong>the</strong> linear system<br />

T<br />

T<br />

A Av = A b [3]. The i-th row <strong>of</strong> <strong>the</strong> N 3 x 3 matrix A is <strong>the</strong> spatial gradient evaluated<br />

at point p i<br />

:<br />

⎡∇E<br />

⎢<br />

⎢<br />

∇E<br />

A =<br />

⎢M<br />

⎢<br />

⎣∇E<br />

( p1<br />

)<br />

( p )<br />

2<br />

⎤<br />

( p ) ⎥⎥⎥⎥ NxNxN ⎦<br />

and b is <strong>the</strong> N 3 -dimensional vector <strong>of</strong> partial temporal derivatives <strong>of</strong> <strong>the</strong> volumetric<br />

brightness, evaluated at p , p2 , K , p 3 after a sign change:<br />

1 N<br />

∂E<br />

⎤<br />

( ) ( ) T<br />

p ,<br />

⎡∂E<br />

b = −<br />

⎢ 1<br />

K , p NxNxN<br />

⎣ ∂t<br />

∂t<br />

⎥ . (4)<br />

⎦<br />

The least squares solution <strong>of</strong> <strong>the</strong> constrained system can be obtained as<br />

r<br />

v =<br />

T −1<br />

T<br />

( A A) A b<br />

(3)<br />

. (5)<br />

ψ [] v r is <strong>the</strong> optical ow (<strong>the</strong> estimate <strong>of</strong> <strong>the</strong> motion eld) at <strong>the</strong> centre <strong>of</strong> patch Q. By<br />

repeating this procedure for all cubic patches, a dense optical ow is obtained. This<br />

algorithm can be summarized as follows. The input is a time-varying sequence <strong>of</strong> n volumes<br />

E 1<br />

, E 2<br />

, …, E n<br />

. Let Q be a sub-volume region <strong>of</strong> N x N x N voxels.<br />

1. Filter each image <strong>of</strong> <strong>the</strong> sequence along each spatial dimension with a Gaussian lter<br />

<strong>of</strong> standard deviation equal to σ s .<br />

2. Filter each image <strong>of</strong> <strong>the</strong> sequence along <strong>the</strong> temporal dimension with a Gaussian<br />

lter <strong>of</strong> standard deviation σ t .<br />

3. For each voxel <strong>of</strong> each volume <strong>of</strong> <strong>the</strong> sequence:<br />

(a) Compute <strong>the</strong> matrix A and <strong>the</strong> vector b using (3) and (4)<br />

(b) Compute <strong>the</strong> optical ow using (5)<br />

Values σ<br />

s and σ<br />

t are set to 1,5 voxels and 1,5 frames respectively, because <strong>of</strong> <strong>the</strong><br />

smoothness. The output is <strong>the</strong> optical ow computed in <strong>the</strong> last step.<br />

2.2 Feature-based Matching Techniques<br />

The second class <strong>of</strong> methods for estimating <strong>the</strong> motion eld is formed by <strong>the</strong> so-called<br />

matching techniques, which estimate <strong>the</strong> motion eld at feature points only. The result is<br />

a sparse motion eld [7]. One proposed solution is a two-frame analysis (nding feature<br />

disparities between consecutive volumetric frames). The robustness <strong>of</strong> frame-to-frame<br />

matching can be improved by motion tracking <strong>of</strong> a feature across a long volumetric


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 171<br />

sequence. We will now describe and adapt two different feature-based matching techniques<br />

from 2D to 3D: <strong>the</strong> constant ow algorithm and <strong>the</strong> feature tracking tracking.<br />

2.2.1 Constant Flow Algorithm<br />

Features can be dened as centres <strong>of</strong> those regions for which <strong>the</strong> smallest eigenvalue <strong>of</strong> A T A<br />

computed over small, cubic regions, is greater than a threshold. The idea <strong>of</strong> <strong>the</strong> matching<br />

method is simple; <strong>the</strong> displacement <strong>of</strong> such feature points can be computed by iterating <strong>the</strong><br />

constant ow algorithm [4].<br />

The input is formed by two frames <strong>of</strong> a volumetric sequence, I 1<br />

and I 2<br />

and a set <strong>of</strong><br />

corresponding feature points in <strong>the</strong> two frames. Let Q 1<br />

, Q 2<br />

, and Q’ be three N x N x N cubic<br />

regions. Let d be <strong>the</strong> unknown displacement between I 1<br />

and I 2<br />

<strong>of</strong> a feature point p on which<br />

Q 1<br />

is centred. Feature point p is centre point <strong>of</strong> <strong>the</strong> shape segmented and dened by <strong>the</strong><br />

edge and corner detection described in Section 3.1. The procedure consists <strong>of</strong> three steps.<br />

First, <strong>the</strong> uniform displacement <strong>of</strong> <strong>the</strong> cube region Q 2<br />

is estimated through constant ow,<br />

and added to <strong>the</strong> current displacement estimate (initially set to 0). Second, <strong>the</strong> patch Q 2<br />

is<br />

wrapped according to <strong>the</strong> estimated ow. This means that Q 2<br />

is displaced according to <strong>the</strong><br />

estimated ow, and <strong>the</strong> resulting patch, Q’, is restored in <strong>the</strong> voxel grid <strong>of</strong> frame I 2<br />

. If <strong>the</strong><br />

estimated ow normalized in time equals (v x<br />

, v y<br />

, v z<br />

), <strong>the</strong> grey value at voxel (i, j, k) <strong>of</strong> Q’<br />

can be obtained from <strong>the</strong> values <strong>of</strong> <strong>the</strong> voxels <strong>of</strong> Q 2<br />

close to (i – v x<br />

, j – v y<br />

, k – v z<br />

). Third, <strong>the</strong><br />

rst and second steps are iterated until a stopping criterion is met. For all feature points p:<br />

1. Set d = 0 and centre Q 1<br />

on p.<br />

2. Estimate <strong>the</strong> displacement d 0<br />

<strong>of</strong> p, centre <strong>of</strong> Q 1<br />

, and let d = d + d 0<br />

.<br />

Let Q’ be <strong>the</strong> patch obtained by warping Q1 according to d0. Compute S, <strong>the</strong> sum <strong>of</strong><br />

<strong>the</strong> squared differences between <strong>the</strong> new patch Q’ and <strong>the</strong> corresponding patch Q2<br />

in <strong>the</strong> frame I2. If S > τ , where τ is <strong>the</strong> threshold, set Q1 = Q’ and go to step 1;<br />

o<strong>the</strong>rwise exit.<br />

The output is an estimate <strong>of</strong> d for all feature points. In reality, long volumetric sequences<br />

ra<strong>the</strong>r than just pairs <strong>of</strong> frames have to be analyzed. The motion <strong>of</strong> feature points is expected<br />

to be continuous, and <strong>the</strong>refore predictable, in most cases. The disparities computed between<br />

frames I i-1<br />

and I i-2<br />

, I i-2<br />

and I i-3<br />

and so on, can be used to make predictions on <strong>the</strong> disparities<br />

between I i-1<br />

and I i<br />

, before observing frame I i<br />

. This algorithm gives satisfying results only<br />

for continuous, predictable motions which can be computed based on disparities between<br />

pairs <strong>of</strong> frames only. To improve <strong>the</strong> algorithm results for long volumetric sequences we<br />

propose to use <strong>the</strong> feature tracking.<br />

2.2.2 Feature Tracking<br />

The feature tracking solves <strong>the</strong> problem <strong>of</strong> matching features from frame to frame in a<br />

long sequence <strong>of</strong> volumes. Our approach is based on [2] and [5] and extended on 3D.<br />

First, it is necessary to formalize <strong>the</strong> tracking problem. A new frame <strong>of</strong> <strong>the</strong> volumetric<br />

sequence is acquired and processed at each instant ti<br />

= ti<br />

0<br />

+ kΔT<br />

, where k is a natural<br />

number and ΔT = 1 is denoted as a sampling interval. Discrete equally-spaced time instants<br />

can be indicated with t i assumed that, for simplicity, ΔT = 1 is small enough to capture<br />

<strong>the</strong> system’s dynamics. The state does not change much between consecutive time instants,<br />

and a linear system model is an adequate approximation <strong>of</strong> <strong>the</strong> state change within ΔT = 1<br />

, i.e. <strong>the</strong> motion <strong>of</strong> feature points from frame to frame is considered to be linear. If only one<br />

feature point, [ ] T<br />

p = x , y , z is considered, in <strong>the</strong> frame acquired at instant t i<br />

, moving<br />

i<br />

i<br />

i<br />

i


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with vector eld velocity v [ ] T<br />

i<br />

= vx, i<br />

, v<br />

y,<br />

i<br />

, v , <strong>the</strong> motion on <strong>the</strong> cubic plane is described<br />

z,<br />

i<br />

with <strong>the</strong> state vector s [ ] T<br />

i<br />

= xi<br />

, yi<br />

, zi<br />

, vx, i<br />

, vy,<br />

i<br />

, v .<br />

z,<br />

i<br />

i<br />

A physical system is modelled by a state vector s , <strong>of</strong>ten called simply <strong>the</strong> state, and a set<br />

s<br />

<strong>of</strong> equations, called <strong>the</strong> system model. The state is a time-dependent vector, i<br />

is stated<br />

as s ( t i<br />

) , <strong>the</strong> components <strong>of</strong> which are system variables, in a sufcient number to capture<br />

<strong>the</strong> dynamic properties <strong>of</strong> <strong>the</strong> system. The system model is a vector equation describing<br />

<strong>the</strong> evolution <strong>of</strong> <strong>the</strong> state in time. Assuming a sufciently small sampling interval (and<br />

<strong>the</strong>refore constant feature velocity between <strong>the</strong> frames), <strong>the</strong> system model can be written as<br />

p ξ (6)<br />

i<br />

= pi− 1<br />

+ vi−<br />

1<br />

+<br />

i−1<br />

v η (7)<br />

= +<br />

i<br />

v i − 1 i−1<br />

where ξi−<br />

1 and η<br />

i−1<br />

are zero-mean, random, vector-modelling additive system noise. In<br />

terms <strong>of</strong> <strong>the</strong> state vector s<br />

i rewrites si<br />

= φ<br />

i− 1si−1<br />

+ wi−<br />

1 with<br />

⎡1<br />

0 0 1 0 0⎤<br />

⎢<br />

⎥<br />

⎢<br />

0 1 0 0 1 0<br />

⎥<br />

⎢0<br />

0 1 0 0 1⎥<br />

φ<br />

i−1<br />

= ⎢<br />

⎥<br />

(8)<br />

⎢0<br />

0 0 1 0 0⎥<br />

⎢0<br />

0 0 0 1 0⎥<br />

⎢<br />

⎥<br />

⎣0<br />

0 0 0 0 1<br />

⎦<br />

and<br />

w i −1<br />

⎡ξ<br />

i−1<br />

⎤<br />

= ⎢ ⎥<br />

⎣η<br />

i−1<br />

⎦<br />

. (9)<br />

The difference between <strong>the</strong> predicted state and <strong>the</strong> real state is measured with <strong>the</strong> state<br />

correction via <strong>the</strong> lter gain factor K t<br />

, known from Kalman ltering. Estimation step, a<br />

priori estimation, estimation error variance and correction step are calculated based on [6].<br />

3 3D MOTION RECONSTRUCTION<br />

When dealing with <strong>the</strong> real world multiple moving objects and complex scenes, lots <strong>of</strong><br />

objects are moving with <strong>the</strong> different motions. In this context, an object can be described<br />

as a part <strong>of</strong> a scene that moves with a coherent motion and <strong>the</strong> scene can be broken down<br />

into a number <strong>of</strong> regions, each <strong>of</strong> which can be well approximated by its own motion.<br />

Segmenting objects against xed background, based on <strong>the</strong> edge detection, as a solution <strong>of</strong><br />

nding <strong>the</strong> regions <strong>of</strong> <strong>the</strong> object corresponding to <strong>the</strong> different moving objects is presented<br />

in Section 3.1. The 3D motion can be reconstructed from a sparse set <strong>of</strong> matched features.<br />

If <strong>the</strong> average disparity between consecutive frames is small, <strong>the</strong> reconstruction can gain in<br />

stability and robustness from <strong>the</strong> time integration <strong>of</strong> long sequences <strong>of</strong> frames. Moreover, in<br />

this case, motion can be dened as a combination <strong>of</strong> small 3D rotations around coordinate<br />

axes and axis and angle. This method is described in Section 3.2. If, on <strong>the</strong> contrary, <strong>the</strong>


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 173<br />

average disparity between frames is large, this problem can be dealt with by using a stereolike<br />

algorithm, applied to a pair <strong>of</strong> frames. The factorization method as a typical example<br />

<strong>of</strong> stereo-like algorithm is described in Section 3.3.<br />

3.1 Segmentation based on <strong>the</strong> Edge Detection<br />

Relax <strong>the</strong> assumption that <strong>the</strong> object motion is described by a single general 3D motion<br />

to deal with <strong>the</strong> problem <strong>of</strong> multiple motions. Identifying moving objects can be seen as<br />

a problem <strong>of</strong> detecting and segmenting objects against a xed background. The goal is to<br />

nd <strong>the</strong> regions <strong>of</strong> <strong>the</strong> volume corresponding to <strong>the</strong> different moving objects. This problem<br />

can be thought <strong>of</strong> as a classication problem. One has to classify <strong>the</strong> voxels <strong>of</strong> each frame<br />

within objects that are detected. The Canny edge detector is, at <strong>the</strong> moment, <strong>the</strong> most widely<br />

used edge detection algorithm in multimedia systems. Constructing a Canny detector<br />

requires <strong>the</strong> formulation <strong>of</strong> a ma<strong>the</strong>matical model <strong>of</strong> <strong>the</strong> edges and <strong>the</strong> corners. The edges<br />

<strong>of</strong> <strong>the</strong> intensity volumes can be modelled according to <strong>the</strong>ir intensity values and proles.<br />

The edge detection operator returns a value for <strong>the</strong> rst derivative in <strong>the</strong> horizontal and <strong>the</strong><br />

vertical direction. The depth dimension (<strong>the</strong> third dimension) can be achieved by modifying<br />

a regular Canny 2D detector [11]. The edge gradient <strong>of</strong> a 3D volumetric object G can be<br />

∂G<br />

determined by computing <strong>the</strong> magnitude gradient components G x =<br />

∂G<br />

∂x<br />

, G y =<br />

∂y<br />

∂G<br />

and G z =<br />

∂z<br />

for each voxel point p(x,y,z) and can be displayed as an volume which<br />

intensity levels are proportional to <strong>the</strong> magnitude <strong>of</strong> <strong>the</strong> local intensity changes. The second<br />

step is to estimate <strong>the</strong> edge strength with<br />

2 2 2<br />

d ( x,<br />

y,<br />

z)<br />

Gx<br />

+ Gy<br />

Gz<br />

e = + as well as <strong>the</strong><br />

orientation <strong>of</strong> <strong>the</strong> edge normal.<br />

Figure 1 Orientation <strong>of</strong> edge normal.<br />

As shown in Figure 1, <strong>the</strong> orientation <strong>of</strong> <strong>the</strong> edge normal is specied by angles and ϕ


174<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

that can be computed by equations<br />

G y<br />

tan θ =<br />

(10)<br />

Gx<br />

and<br />

Gz<br />

tanϕ =<br />

. (11)<br />

( G ) 2 + ( G ) 2<br />

x<br />

y<br />

Weighted summations <strong>of</strong> <strong>the</strong> voxel intensities in local neighbourhoods can be listed as a<br />

numerical array. Intensity gradients which are large are more likely to correspond to edges<br />

than if <strong>the</strong>y are small. Making <strong>the</strong> assumption that <strong>the</strong> important edges should be along<br />

continuous curves in <strong>the</strong> volume allows us to follow a faint section <strong>of</strong> a given line and to<br />

discard a few noisy pixels that do not constitute a line but have produced large gradients.<br />

This marks out <strong>the</strong> edges we can be fairly sure are genuine. Starting from <strong>the</strong>se, using <strong>the</strong><br />

directional information derived earlier, edges can be traced through <strong>the</strong> frames. The output<br />

<strong>of</strong> gradient based edge detection is a binary volume indicating where <strong>the</strong> edges are in order<br />

to decide whe<strong>the</strong>r an edge has been found. From complementary output from <strong>the</strong> edge<br />

tracing step, <strong>the</strong> binary edge map obtained in this way can also be treated as a set <strong>of</strong> edge<br />

curves.<br />

3.2 3D Rotations<br />

This section addresses 3D rotations as a base for reconstruction <strong>of</strong> 3D motions. In most<br />

cases it is useful to represent a rotation by means <strong>of</strong> more natural parameterization. Two<br />

parameterizations are proposed: rotations around <strong>the</strong> coordinate axes and axis and angle.<br />

Rotations around <strong>the</strong> coordinate axes can be expressed as <strong>the</strong> result <strong>of</strong> three consecutive<br />

rotations around <strong>the</strong> coordinate axes, e 1<br />

, e 2<br />

and e 3<br />

, by angles , and respectively. The<br />

angles are <strong>the</strong>n <strong>the</strong> three free parameters <strong>of</strong> linear transformation represented by a 3x3<br />

matrix R and each rotation is expressed as a rotation matrix, R j<br />

, rotating vectors around e j<br />

,<br />

that is,<br />

⎡1<br />

0 0 ⎤<br />

R ( ⎢<br />

⎥<br />

1<br />

α)<br />

= 0 cosα<br />

− sinα<br />

⎢<br />

⎥<br />

(12)<br />

⎢⎣<br />

0 sinα<br />

cosα<br />

⎥⎦<br />

⎡ cos β 0 sin β ⎤<br />

R<br />

⎢<br />

⎥<br />

2( β ) = 0 1 0<br />

(13)<br />

⎢<br />

⎥<br />

⎢⎣<br />

− sin β 0 cos β ⎥⎦<br />

⎡cosγ<br />

− sin γ 0⎤<br />

R =<br />

⎢<br />

⎥<br />

3(<br />

γ ) sin γ cosγ<br />

0 . (14)<br />

⎢<br />

⎥<br />

⎢⎣<br />

0 0 1⎥⎦


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 175<br />

The matrix R describing <strong>the</strong> overall rotation is <strong>the</strong> product <strong>of</strong> <strong>the</strong> R j<br />

(<strong>the</strong> order <strong>of</strong> overall<br />

multiplications matters; different sequences give different results with <strong>the</strong> same triplet <strong>of</strong><br />

angles):<br />

R = R R<br />

1 2R3<br />

=<br />

⎡ cos β cosγ<br />

=<br />

⎢<br />

sinα<br />

sin β cosγ<br />

+ cosα<br />

sinγ<br />

⎢<br />

⎢⎣<br />

− cosα<br />

sin β cosγ<br />

+ sinα<br />

sinγ<br />

− cos β sinγ<br />

− sinα<br />

sin β sinγ<br />

+ cosα<br />

cosγ<br />

cosα<br />

sin β sinγ<br />

+ sinα<br />

cosγ<br />

sin β ⎤<br />

− sinα<br />

cos β<br />

⎥<br />

⎥<br />

cosα<br />

cosγ<br />

⎥⎦<br />

(15)<br />

Second parameterization is as follows. According to Euler’s <strong>the</strong>orem, any 3D rotation<br />

can be described as a rotation by an angle, , around an axis identied by a unit vector<br />

r<br />

n = [ n n n ] T . The corresponding rotation matrix R can <strong>the</strong>n be obtained in terms<br />

1 2 3<br />

<strong>of</strong> and <strong>the</strong> components <strong>of</strong> n which gives a total <strong>of</strong> four parameters. The redundancy <strong>of</strong> this<br />

parameterization (four parameters for three degrees <strong>of</strong> freedom) is eliminated by adding<br />

2 2 2<br />

<strong>the</strong> constraint that n has a unit norm, that is by dividing each n i<br />

by n<br />

1<br />

+ n2<br />

+ n3<br />

[5].<br />

The matrix R in terms <strong>of</strong> and n is given by<br />

2<br />

⎡ n1<br />

n1n2<br />

n1n3<br />

⎤ ⎡ 0 − n3<br />

n2<br />

⎤<br />

⎢<br />

2 ⎥<br />

R = I cosθ + ( 1 − cosθ<br />

)<br />

+<br />

⎢<br />

−<br />

⎥<br />

⎢<br />

n2n1<br />

n2<br />

n2n3⎥<br />

sinθ<br />

n 0<br />

⎢<br />

3<br />

n1⎥<br />

(16)<br />

2<br />

⎢<br />

⎥<br />

⎣n3n1<br />

n3n2<br />

n3<br />

⎦ ⎢⎣<br />

− n2<br />

n1<br />

0 ⎥⎦<br />

Conversely, both and n can be obtained from <strong>the</strong> eigenvalues and <strong>the</strong> eigenvectors <strong>of</strong> R.<br />

The three eigenvalues <strong>of</strong> R are 1, cosθ<br />

+ i sin θ and cosθ<br />

− i sin θ , where i is <strong>the</strong><br />

imaginary unit. The unit vector n is proportional to <strong>the</strong> eigenvector <strong>of</strong> R, corresponding<br />

<strong>the</strong> eigenvalue 1; <strong>the</strong> angle can be obtained from ei<strong>the</strong>r <strong>of</strong> <strong>the</strong> two complex eigenvalues.<br />

3.3 Factorization Method for Motion Reconstruction<br />

Of <strong>the</strong> many methods proposed in <strong>the</strong> literature for <strong>the</strong> case <strong>of</strong> large average disparity<br />

between frames, <strong>the</strong> most used is <strong>the</strong> factorization method, which is simple to implement<br />

and gives very good (and numerically stable) results for objects viewed from ra<strong>the</strong>r large<br />

distances [8]. In this paper it is adopted to three dimensions. The necessary assumption is<br />

that <strong>the</strong> position <strong>of</strong> n volume points corresponding to <strong>the</strong> feature points p 1<br />

, p 2<br />

, ..., p n<br />

, has<br />

been tracked in N frames, with N > 3. This is equivalent to acquiring <strong>the</strong> entire sequence<br />

before starting any processing. Tracking method is described in Section 2.2.2.<br />

If p [ ] T<br />

ij<br />

= xij<br />

, yij<br />

, z denote <strong>the</strong> j-th voxel (j = 1, ..., n) at <strong>the</strong> i-th frame (i = 1, ..., N),<br />

ij<br />

and think <strong>of</strong> <strong>the</strong> x ij<br />

, y ij<br />

and z ij<br />

as entries <strong>of</strong> three N x n matrices, X, Y and Z, respectively, <strong>the</strong><br />

measurement matrix 3N x n can be formed as<br />

⎡X<br />

⎤<br />

W =<br />

⎢<br />

Y<br />

⎥<br />

⎢ ⎥ . (17)<br />

⎢⎣<br />

Z ⎥⎦


176<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

For use in <strong>the</strong> rank <strong>the</strong>orem, <strong>the</strong> mean <strong>of</strong> <strong>the</strong> entries on <strong>the</strong> same row is subtracted from<br />

each x ij<br />

, y ij<br />

and z ij<br />

:<br />

~ xij<br />

= xij<br />

− x<br />

(18)<br />

~ i<br />

yij<br />

= yij<br />

− y<br />

(19)<br />

~ i<br />

(20)<br />

z<br />

ij<br />

= z<br />

ij<br />

− z<br />

i<br />

where<br />

1<br />

x =<br />

n<br />

∑<br />

i<br />

x ij<br />

n j=<br />

1<br />

1<br />

y =<br />

n<br />

∑<br />

i<br />

y ij<br />

n j=<br />

1<br />

(21)<br />

(22)<br />

1<br />

z =<br />

n<br />

∑<br />

i<br />

z ij<br />

n j=<br />

1<br />

are <strong>the</strong> coordinates <strong>of</strong> p<br />

i , <strong>the</strong> centroid <strong>of</strong> <strong>the</strong> voxels in <strong>the</strong> i-th frame. Fur<strong>the</strong>rmore, x~ ,<br />

ij<br />

y~<br />

ij<br />

and z~ can be denoted as entries <strong>of</strong> three N x n matrices, X ~ , Y ~ and Z ~ , and form <strong>the</strong> 3N x<br />

ij<br />

n matrix W, called <strong>the</strong> registered measurement matrix:<br />

(23)<br />

~<br />

⎡X<br />

⎤<br />

~ ⎢ ~ ⎥<br />

W = ⎢Y<br />

⎥<br />

⎢ ~ ⎥<br />

⎣Z<br />

⎦<br />

. (24)<br />

The factorization method is based on <strong>the</strong> pro<strong>of</strong> <strong>of</strong> a simple but fundamental result that <strong>the</strong><br />

registered measurement matrix without noise has at most <strong>the</strong> rank 3 [8]. The pro<strong>of</strong> is based<br />

on <strong>the</strong> decomposition (factorization <strong>of</strong> W ~ ) into <strong>the</strong> product <strong>of</strong> a 3N x 3 matrix, R, and a<br />

3 x n matrix, C. R describes <strong>the</strong> frame-to-frame rotation with respect to <strong>the</strong> points p i<br />

. C<br />

describes <strong>the</strong> structure <strong>of</strong> points (coordinates).<br />

Figure 2 Factorization method.<br />

Consider all quantities expressed in an object-centred reference frame with <strong>the</strong> origin in


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 177<br />

<strong>the</strong> centroid <strong>of</strong> p 1<br />

, ..., p n<br />

(Figure 2), and let i i<br />

, j i<br />

and k i<br />

denote <strong>the</strong> unit vectors <strong>of</strong> <strong>the</strong> i-th<br />

frame (at time instant i). It can be seen from Figure 2 that<br />

x<br />

y<br />

z<br />

ij<br />

ij<br />

ij<br />

T<br />

i<br />

( p − d )<br />

= i<br />

(25)<br />

T<br />

i<br />

j<br />

( p − d )<br />

j<br />

i<br />

= j<br />

(26)<br />

T<br />

i<br />

( p − d )<br />

j<br />

i<br />

i<br />

= k<br />

(27)<br />

where d i<br />

is <strong>the</strong> vector from <strong>the</strong> original reference frame to <strong>the</strong> origin <strong>of</strong> <strong>the</strong> i-th frame;<br />

moreover as <strong>the</strong> origin is in <strong>the</strong> centroid <strong>of</strong> <strong>the</strong> points,<br />

n<br />

1<br />

∑ p j<br />

= 0 . (28)<br />

n 1<br />

j=<br />

Now, it can be rewritten<br />

n<br />

1 T<br />

T<br />

( p − d ) − i ( p − d ) ii<br />

p<br />

j<br />

~ x =<br />

T<br />

ij<br />

= ii<br />

j i ∑ i<br />

n m=1<br />

n<br />

1 T<br />

T<br />

( p<br />

j<br />

− di<br />

) − ji<br />

( pm<br />

− di<br />

) ji<br />

p<br />

j<br />

~ y =<br />

T<br />

ij<br />

= ji<br />

∑<br />

n m=1<br />

n<br />

1 T<br />

T<br />

( p<br />

j<br />

− di<br />

) − ki<br />

( pm<br />

− di<br />

) ki<br />

p<br />

j<br />

~ z =<br />

T<br />

ij<br />

= ki<br />

∑<br />

n m=1<br />

Therefore, <strong>the</strong> rotation matrix R size <strong>of</strong> 3N x 3 can be dened as<br />

m<br />

i<br />

(29)<br />

(30)<br />

. (31)<br />

T<br />

⎡i<br />

⎤<br />

1<br />

⎢ ⎥<br />

⎢ M ⎥<br />

⎢<br />

T<br />

i ⎥<br />

n<br />

⎢ T ⎥<br />

⎢<br />

j1<br />

⎥<br />

R = ⎢ M ⎥<br />

⎢ T ⎥<br />

⎢ jn<br />

⎥<br />

T<br />

⎢k<br />

⎥<br />

1<br />

⎢ ⎥<br />

⎢ M ⎥<br />

⎢<br />

T<br />

⎥<br />

⎣kn<br />

⎦<br />

(32)<br />

and a 3 x n shape matrix C as<br />

[ p K ]<br />

C = (33)<br />

so it can be written that<br />

1<br />

p n<br />

~<br />

W =<br />

RC .


178<br />

4 EXPERIMENTAL EVALUATION<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

This section gives <strong>the</strong> experimental details <strong>of</strong> <strong>the</strong> implemented methods and algorithms<br />

on <strong>the</strong> four-dimensional data sets (3D objects that change in time) collected from an MRI<br />

scanner (i.e. MRI brain volumes). Each dataset is representing <strong>the</strong> brain motion in an MRI<br />

scanner. The framework for <strong>the</strong> estimation <strong>of</strong> different 3D motions is represented in Figure<br />

3. Different types <strong>of</strong> <strong>the</strong> 3D motion are estimated with <strong>the</strong> different techniques. For <strong>the</strong><br />

typical linear motion, such as translation, we propose use <strong>of</strong> <strong>the</strong> constant ow algorithm.<br />

Rotations in space in time are approximated with <strong>the</strong> 3D rotation methods. The optical<br />

ow and <strong>the</strong> feature tracking are proposed for estimation <strong>of</strong> a long sequence <strong>of</strong> data or<br />

accelerating motion. In case <strong>of</strong> large disparity between frames we propose <strong>the</strong> factorization<br />

method. The whole process is semi-automated because a medical expert should know what<br />

kind <strong>of</strong> <strong>the</strong> input data collected from MRI scanner is analyzed, and based on that, <strong>the</strong><br />

system will select an appropriate technique for given 3D motion.<br />

Figure 3 Proposed framework for 3D motion.<br />

Three consecutive frames <strong>of</strong> <strong>the</strong> original experimental dataset (size <strong>of</strong> 429 kB) are<br />

shown in Figure 4. For motion estimation between two frames we use <strong>the</strong> constant<br />

ow algorithm (Figure 4). The resulting displacement between <strong>the</strong> rst and <strong>the</strong><br />

second frame is computed as d = [ ( i − vx<br />

), ( j − vy<br />

)( , k − vz<br />

) ] = [ 153,2,0]<br />

2<br />

2<br />

2<br />

d ( i − v ) + ( j − v ) + ( k − v ) = 153, 013<br />

=<br />

x<br />

y<br />

z<br />

used to estimate <strong>the</strong> movement between <strong>the</strong> second and <strong>the</strong> third frame.<br />

and<br />

. The resulting displacement d is<br />

Figure 4 Example <strong>of</strong> motion between three consecutive frames. Motion between <strong>the</strong> second and <strong>the</strong><br />

third frame is determined by <strong>the</strong> constant ow algorithm.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 179<br />

Figure 5 Example <strong>of</strong> motion between three consecutive frames. Motion between <strong>the</strong> second and <strong>the</strong><br />

third frame is determined by <strong>the</strong> optical ow.<br />

In Figure 5 <strong>the</strong> same procedure <strong>of</strong> motion estimation between <strong>the</strong> second and <strong>the</strong> third frame<br />

is repeated by using <strong>of</strong> <strong>the</strong> optical ow algorithm. There is a signicant visual difference<br />

between <strong>the</strong> estimated and real position <strong>of</strong> 3D object. Also, in case <strong>of</strong> <strong>the</strong> constant ow<br />

algorithm, we have to code only <strong>the</strong> displacement d which is signicantly less (for three<br />

consecutive frames 151 kB) than coding <strong>the</strong> whole optical ow for <strong>the</strong> each voxel (386<br />

kB).<br />

Figure 6 Motion in long sequence <strong>of</strong> volumes.<br />

Second example is a long sequence <strong>of</strong> volumes (shown in Figure 6). In this case <strong>the</strong><br />

feature tracking is <strong>the</strong> most appropriate technique for <strong>the</strong> motion estimation, because <strong>the</strong><br />

displacement in a long sequence <strong>of</strong> data is not a constant value. In this example feature<br />

tracking is described with p = [ 517 ,38, 92] T<br />

and [ ] T<br />

i<br />

v = − 5,0, 1 , <strong>the</strong> motion on <strong>the</strong><br />

volume plane is described with <strong>the</strong> state vector [ ] T<br />

i<br />

i<br />

s = 517 ,38,92, −5,0,<br />

1 . Estimated


180<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

state vector s<br />

i+ 1 , with assumed = 1<br />

si<br />

1<br />

= 512 ,38,94, −52,6,<br />

−14<br />

Estimated state vectors for consecutive 8 frames are stated below:<br />

ΔT , gives values [ ] T<br />

[ 512 ,38,94, 52,6, ] T<br />

+ 1<br />

= − s = [ 460,44,108, −37,2,<br />

1] T<br />

,<br />

s 14<br />

i<br />

i+<br />

2<br />

−<br />

[ ] T<br />

, s 13<br />

i+ 3<br />

= 423,46,107, −11,<br />

−12,<br />

s [ ] T<br />

,<br />

i+4 = 412 ,34,120,1,0, 2<br />

[ ] T<br />

, s 1<br />

i+ 5<br />

= 413 ,34,122,9,6, − s [ ] T<br />

,<br />

i 6<br />

= 422,40,121,17 ,8, 5<br />

s [ ] T<br />

i+ 7<br />

= 439,48,126,6,24, −2<br />

s [ ] T<br />

,<br />

i 8<br />

= 445,72,124,0,0, 0<br />

+<br />

,<br />

+<br />

.<br />

+<br />

.<br />

To recreate motion on <strong>the</strong> syn<strong>the</strong>sized 3D-models, it is necessary to nd a ma<strong>the</strong>matical<br />

solution to tie <strong>the</strong> analysis to <strong>the</strong> syn<strong>the</strong>sis. To extract motion information from <strong>the</strong> specic<br />

features <strong>of</strong> multiple moving objects, <strong>the</strong> parameters <strong>of</strong> <strong>the</strong> visualization semantics <strong>of</strong> <strong>the</strong><br />

system that will syn<strong>the</strong>size <strong>the</strong> motion, should be known. To do this we rst separate <strong>the</strong><br />

objects with methods described in Section 3.1. Results are shown in Figure 7.<br />

Figure 7 Example <strong>of</strong> segmentation; upper left is <strong>the</strong> original frame; upper right <strong>the</strong> segmented<br />

frame based on <strong>the</strong> edge and <strong>the</strong> corner detection <strong>of</strong> <strong>the</strong> outer shape; lower left all edges detected<br />

based on <strong>the</strong> methods described in Section 3.1; lower right <strong>the</strong> nal segmentation <strong>of</strong> <strong>the</strong> brain with<br />

<strong>the</strong> inner cavities.<br />

It is also necessary to relate <strong>the</strong>se parameters to <strong>the</strong> actions that must be applied to <strong>the</strong><br />

3D-model in order to recreate motion. These motion models translate <strong>the</strong> results into an<br />

object-visualization parameters building motion elds <strong>of</strong> <strong>the</strong> sub-objects in a 3D rotation


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 181<br />

and <strong>the</strong> factorization method for <strong>the</strong> motion reconstruction.<br />

Figure 8 3D rotation.<br />

Example shown in Figure 8 represents a rigid motion eld that is simply described by a<br />

rotation matrix R<br />

R = R R<br />

1 2R3<br />

=<br />

cos( −13°<br />

) cos( 29°<br />

) − cos( −13°<br />

) sin( 29°<br />

) sin( −13°<br />

)<br />

( 8°<br />

) sin( −13°<br />

) cos( 29°<br />

) + cos( 8°<br />

) sin( 29°<br />

) − sin( 8°<br />

) sin( −13°<br />

) sin( 29°<br />

) + cos( 8°<br />

) cos( 29°<br />

) − sin( 8°<br />

) cos( −13°<br />

)<br />

( 8°<br />

) sin( −13°<br />

) cos( 29°<br />

) + sin( 8°<br />

) sin( 29°<br />

) cos( 8°<br />

) sin( −13°<br />

) sin( 29°<br />

) + sin( 8°<br />

) cos( 29°<br />

) cos( 8°<br />

) cos( 29°<br />

)<br />

⎡<br />

⎢<br />

⎢<br />

sin<br />

⎢⎣<br />

− cos<br />

⎡0,1478<br />

− 0,1478<br />

=<br />

⎢<br />

⎢<br />

0,8509 0,8813<br />

⎢⎣<br />

0,2623 − 0,0015<br />

− 0,225 ⎤<br />

− 0,1356<br />

⎥<br />

⎥<br />

0,866 ⎥⎦<br />

⎤<br />

⎥<br />

⎥<br />

⎥⎦<br />

Example <strong>of</strong> <strong>the</strong> factorization method is shown in Figure 9. Aim is to form a registration<br />

measurement matrix. In this example, <strong>the</strong>re is a large average disparity between <strong>the</strong> current<br />

and <strong>the</strong> reference frame. The registered measurement matrix, <strong>the</strong> rotation matrix and <strong>the</strong><br />

shape matrix are<br />

T<br />

⎡−<br />

2,84 ⎤ ⎡i<br />

⎤<br />

1 ⎡−<br />

0,27 − 0,76 0,9 ⎤<br />

⎢ ⎥ ⎢ T ⎥ ⎢<br />

⎥<br />

⎢<br />

−1,13<br />

⎥ ⎢ j1<br />

⎥ ⎢<br />

− 0,73 0,58 − 0,24<br />

⎥<br />

⎢−<br />

2,13 ⎥ ⎢<br />

T<br />

k ⎥<br />

1 ⎢−<br />

0,82 0,24 0,31 ⎥<br />

⎢ ⎥ ⎢ ⎥<br />

T ⎢<br />

⎥<br />

⎢−<br />

3,065⎥<br />

⎢i2<br />

⎥ ⎢−<br />

0,35 − 0,69 0,75 ⎥<br />

⎡ 4 ⎤<br />

~<br />

W = ⎢ − 0,55 ⎥ , ⎢ T<br />

R = j<br />

⎥<br />

= ⎢−<br />

0,69 0,72 − 0,31 ⎥ and C =<br />

⎢ ⎥<br />

⎢ ⎥ ⎢<br />

2<br />

⎥ ⎢<br />

⎥<br />

⎢<br />

3,5<br />

⎥.<br />

T<br />

⎢−<br />

2,875 ⎥ ⎢k<br />

⎥ ⎢−<br />

0,91 0,15 0,24<br />

⎢<br />

2<br />

⎥<br />

⎣ 1 ⎥⎦<br />

⎢−<br />

3,515 ⎥ ⎢<br />

T<br />

⎥ ⎢−<br />

−<br />

⎥<br />

⎢ ⎥ ⎢i<br />

⎥ 0,49 0,61 0,58<br />

3<br />

⎢<br />

⎥<br />

⎢ 0,015 ⎥ ⎢ T<br />

j ⎥ ⎢−<br />

0,59 0,79 − 0,39<br />

3<br />

⎥<br />

⎢ ⎥ ⎢ ⎥<br />

T<br />

⎣−<br />

3,515<br />

⎢<br />

⎥<br />

⎦ ⎢ ⎥ ⎣−<br />

0,97 0,07 0,12<br />

⎣k3<br />

⎦<br />


182<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 9 Example <strong>of</strong> factorization method.<br />

The factorization <strong>of</strong> <strong>the</strong> registered measurement matrix W ~ as <strong>the</strong> product <strong>of</strong> R and C<br />

suggests a method for <strong>the</strong> reconstruction <strong>of</strong> structure and motion from a sequence <strong>of</strong><br />

tracked voxels.<br />

5 CONCLUSION<br />

In this paper we have applied different algorithms for <strong>the</strong> 3D motion estimation and<br />

reconstruction. For <strong>the</strong> estimation <strong>of</strong> <strong>the</strong> constant motion eld between only two consecutive<br />

frames, <strong>the</strong> constant ow algorithm is satisfying enough, and it is not computational<br />

extensive as <strong>the</strong> differential techniques because it is oriented only on a sparse set <strong>of</strong> <strong>the</strong><br />

volume points, denoted as <strong>the</strong> feature points. For estimating motion in long sequence <strong>of</strong><br />

3D objects it is more appropriate to use <strong>the</strong> feature tracking. The main purpose <strong>of</strong> this<br />

framework for <strong>the</strong> 3D motion eld estimation in 3D MRI data is to reduce a vast amount <strong>of</strong><br />

acquired data, in coding process. For different types <strong>of</strong> MRI, different motion techniques<br />

should be used for <strong>the</strong> motion estimation and <strong>the</strong> motion reconstruction. By coding only<br />

a sparse set <strong>of</strong> information about <strong>the</strong> volume motion, higher compression ratios can be<br />

achieved. For example, size <strong>of</strong> <strong>the</strong> original dataset is 429 kB, and with coding only <strong>the</strong><br />

reference frame and <strong>the</strong> motion eld based on <strong>the</strong> combination <strong>of</strong> proposed algorithms<br />

for different kind <strong>of</strong> 3D motions, <strong>the</strong> size can be reduced on only 56 kB which gives <strong>the</strong><br />

compression ratio <strong>of</strong> 1 : 8.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 183<br />

6 REFERENCES<br />

1. Aubert G, Deriche R, Kornprobst P (1999) Computing Optical Flow via Variational<br />

Techniques. SIAM Journal <strong>of</strong> Applied Ma<strong>the</strong>matics, Vol. 60, Issue 1: 156-182<br />

2. Black MJ, Anandan P (1996) The robust estimation <strong>of</strong> multiple motions: parametric<br />

and piecewise-smooth ow elds. Computer Vision and Image Understanding, Vol.<br />

63, Issue 1: 75-104<br />

3. Fashandi H, Fazel-Rezai R, Pistorius S (2007) Optical Flow and Total Least Squares<br />

Solution for Multi-scale Data in an Over-Determined System. Lecture Notes in<br />

Computer Science, Advances in Visual Computing, Springer Berlin/Heidelberg, Vol.<br />

4842: 33-42<br />

4. Favaro P, Soatto S (2007) 3-D Shape Estimation and Image Restoration: Exploiting<br />

Defocus and Motion Blur. Springer-Verlag, London, pp 240-292<br />

5. Furht B, Greenberg J, Westwater R (1997) Motion Estimation Algorithms for Video<br />

Compression. Kluwer Academic Publishers, Boston, pp 120-156<br />

6. Messelodi S, Modena CM, Segata N, Zanin M (2005) A Kalman Filter Based<br />

Background Updating Algorithm Robust to Sharp Illumination Changes. Lecture<br />

Notes in Computer Science, Vol. 3617: 163–170<br />

7. Su Y, Sun MT, Hsu V (2005) Global motion estimation from coarsely sampled motion<br />

vector eld and <strong>the</strong> applications. Circuits and Systems for Video Technology, IEEE<br />

Transactions on, Vol. 15, Issue 2: 232-242<br />

8. Ueshiba T, Tomita F (2000) A factorization method for multiple perspective views via<br />

iterative depth estimation. Systems and Computers in Japan, Vol. 31, Issue 13:87-95<br />

9. Yuille AL, Hallinan PW, Cohen DS (1992) Feature extraction from faces using<br />

deformable templates. International Journal <strong>of</strong> Computer Vision, Springer Ne<strong>the</strong>rlands,<br />

Vol. 8, Issue 2: 99-111<br />

10. Wills J, Agarwal S, Belongie S (2006) A Feature-based Approach for Dense<br />

Segmentation and Estimation <strong>of</strong> Large Disparity Motion. International Journal <strong>of</strong><br />

Computer Vision, Springer Ne<strong>the</strong>rlands, Vol. 68, Issue 2: 125-143<br />

11. Žagar M (2009) 4D Medical Data Compression Architecture. PhD Thesis, University<br />

<strong>of</strong> Zagreb, Zagreb, Croatia


184<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Laboratory Evaluation <strong>of</strong> Mud Differential Sticking<br />

Tendency and Spotting Fluid Effectiveness<br />

Gaurina-Međimurec Nediljka<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Mining, Geology and Petroleum Engineering<br />

Pierottijeva 6, Zagreb, Croatia<br />

nediljka.gaurina-medjimurec@rgn.hr, Tel. +385 1 5535 825<br />

Pašic Borivoje<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Mining, Geology and Petroleum Engineering<br />

Pierottijeva 6, Zagreb, Croatia<br />

borivoje.pasic@rgn.hr, Tel. +385 1 5535 840<br />

Matanović Davorin<br />

University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Mining, Geology and Petroleum Engineering<br />

Pierottijeva 6, Zagreb, Croatia<br />

davorin.matanovic@rgn.hr, Tel. +385 1 5535 835<br />

Abstract<br />

Differential-pressure pipe sticking occurs when a portion <strong>of</strong> <strong>the</strong> drill string becomes<br />

embedded in a lter cake that creates on <strong>the</strong> wall <strong>of</strong> a permeable formation during drilling.<br />

The dominant force is usually associated with a difference in pressures between <strong>the</strong><br />

hydrostatic pressure <strong>of</strong> <strong>the</strong> mud and <strong>the</strong> pore pressure in <strong>the</strong> contact area, though adhesion<br />

and cohesion may also contribute some resistance to pipe movement. Some level <strong>of</strong> sticking<br />

occurs routinely in drilling operations and differential-pressure-pipe-sticking problems<br />

may not be totally prevented. These events only became problematic if <strong>the</strong> force required<br />

to pull <strong>the</strong> pipe free exceeds <strong>the</strong> pipe strength.<br />

If sticking does occur, several methods can be used for freeing <strong>the</strong> stuck pipe but <strong>the</strong> most<br />

common approach is to place a small volume <strong>of</strong> oil, or special spotting uid in a wellbore<br />

annulus to free differentially stuck pipe. Spotting uid reduces <strong>the</strong> stuck area and <strong>the</strong> forces<br />

<strong>of</strong> cohesion between <strong>the</strong> pipe and cake, and allowing pipe to be pulled free.<br />

Differential sticking tendency <strong>of</strong> different drilling uids has been determined in laboratory<br />

using sticking tester as well as inuence <strong>of</strong> spotting uids on freeing differentially stuck<br />

pipe. Results <strong>of</strong> <strong>the</strong> testing are presented in <strong>the</strong> paper.<br />

Key words: differential sticking, stuck pipe, spotting uid, lter cake, drilling<br />

1 INTRODUCTION<br />

Pipe sticking is, for most drilling organizations, <strong>the</strong> greatest drilling problem worldwide.<br />

It results in a signicant amount <strong>of</strong> non-productive time and ends up as one <strong>of</strong> <strong>the</strong> major<br />

causes <strong>of</strong> increased well costs (Reid et al., 2000; Pal et al., 2000). Pipe sticking may result<br />

in abandonment <strong>of</strong> <strong>the</strong> current hole and force a sidetrack, It is estimated that <strong>the</strong> cost <strong>of</strong><br />

stuck pipe in deep oil and gas wells can be approximately 25% <strong>of</strong> <strong>the</strong> overall budget.<br />

In some areas, events related to differentially stuck pipe can be responsible for as much<br />

as 40% <strong>of</strong> <strong>the</strong> total well cost (Reid et al, 2000). Causes <strong>of</strong> stuck pipe can be devided in


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 185<br />

two categories (Isambourg, et al., 1999): (a) mechanical (key seating, formation-related<br />

wellbore instability, wellbore geometry (deviation and ledges), inadequate hole cleaning,<br />

junk in hole or collapsed casing, cement related) and (b) differential pressure (wall sticking).<br />

Differential pressure sticking is usually indicated when <strong>the</strong> drill string cannot be rotated,<br />

raised or lowered, but full circulation at normal pressure can be established (Bushnell-<br />

Watson and Panesar, 1991). The force required to pull <strong>the</strong> pipe free can exceed <strong>the</strong> strength<br />

<strong>of</strong> <strong>the</strong> pipe. Usually, even if <strong>the</strong> stuck condition starts with <strong>the</strong> possibility <strong>of</strong> limited pipe<br />

rotation or vertical movement, it will degrade to <strong>the</strong> inability to move <strong>the</strong> pipe at all.<br />

The risk <strong>of</strong> differentially stuck pipe increases when drilling depleted reservoirs and avoids<br />

when drilling underbalanced. Stuck pipe causes and methods for <strong>the</strong>ir freeing are shown<br />

in Figure 1 (BHI, 1998).<br />

STUCK PIPE CAUSE<br />

MECHANICAL<br />

DIFFERENTIAL STICKING<br />

KEY SEATING<br />

WELLBORE<br />

GEOMETRY<br />

INADEQUATE HOLE<br />

CLEANING<br />

JUNK OR COLLAPSED CASING<br />

CEMENT RELATED<br />

DRILLSTRING<br />

JAMMED<br />

DRILLSTRING<br />

JAMMED<br />

HOLE PACKED<br />

OFF<br />

DRILLSTRING<br />

JAMMED<br />

DRILLSTRING<br />

JAMMED<br />

WORK STRING<br />

DOWN AND<br />

ROTATE<br />

WORK STRING UP IF<br />

RIH.<br />

WORK STRING<br />

DOWN IF P.O.O.H.<br />

WORK STRING<br />

DOWN TO<br />

ESTABLISH OR<br />

IMPROVE<br />

CIRCULATION<br />

WORK STRING UP AND DOWN<br />

WORK STRING UP<br />

AND DOWN. PUMP<br />

ACID IF AVAILABLE<br />

DRILLSTRING<br />

JAMMED<br />

SLUMP STRING AND ROTATE. REDUCE<br />

FLUID WEIGHT. UTILIZE SPOTTING<br />

FLUID<br />

Figure 1. Stuck pipe causes and methods for <strong>the</strong>ir freeing (BHI, 1998.)<br />

2 MECHANISMS OF DIFFERENTIAL STICKING<br />

Differential sticking by denition is a situation in which <strong>the</strong> drilling assembly (pipe, drill<br />

collars and bottomhole assembly) is stuck in lter cake that was previously deposited on a<br />

permeable zone (Figure 2a). A signicant overbalance must also exist and <strong>the</strong> pipe must be<br />

stationary, or almost stationary, to allow <strong>the</strong> bond between <strong>the</strong> cake and <strong>the</strong> pipe to develop.


186<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

The pipe is held in <strong>the</strong> cake by a difference in pressures (P) between <strong>the</strong> hydrostatic<br />

pressure <strong>of</strong> <strong>the</strong> mud (P m<br />

) and <strong>the</strong> formation (pore) pressure (P f<br />

) in <strong>the</strong> permeable zone.<br />

This pressure (P) acts upon <strong>the</strong> area <strong>of</strong> <strong>the</strong> pipe in contact with lter cake and isolated from<br />

<strong>the</strong> pressure <strong>of</strong> <strong>the</strong> mud in <strong>the</strong> hole by new lter cake (Figure 2b). There must be a minimum<br />

penetration <strong>of</strong> <strong>the</strong> drill pipe before a signicant change <strong>of</strong> pressure at pipe/cake interface<br />

can occur. Therefore if lter cake can be made thin enough, sticking can be avoided. Three<br />

differential forces have been used to free <strong>the</strong> pipe: axial (equivalent to working <strong>the</strong> pipe up<br />

or down), radial (equivalent to pulling <strong>the</strong> pipe across <strong>the</strong> wellbore) and torque (rotation <strong>of</strong><br />

<strong>the</strong> pipe) (Figure 2c). In practice it is likely to be a combination <strong>of</strong> an axial force and torque<br />

which is used to free <strong>the</strong> pipe. The force required to free differentially stuck pipe must<br />

overcome adhesion and <strong>the</strong> differential pressure exerted by <strong>the</strong> mud. It has tendency to<br />

increase with time until all water is expelled from <strong>the</strong> lter cake. Once sticking is established,<br />

a signicant force is required to free <strong>the</strong> pipe, even if <strong>the</strong> mud overbalance is removed.<br />

At best, several hours <strong>of</strong> rig time can be spent in various freeing operations. In more<br />

serious cases, <strong>the</strong> pipe cannot be freed and <strong>the</strong> well has to be sidetracked or abondoned.<br />

Pullout force needed to free a stuck pipe is equal to:<br />

F = P·A· (Eq. 1)<br />

where<br />

F - pullout force, N<br />

P - differential pressure, Pa<br />

A - contacta area, m 2<br />

- coefcient <strong>of</strong> friction (adhesion) between <strong>the</strong> collars and <strong>the</strong> cake<br />

Value <strong>of</strong> F is also increased with compressibility and thickness <strong>of</strong> <strong>the</strong> lter cake, hole<br />

deviation, and diameter <strong>of</strong> <strong>the</strong> drill collars. It is decreased with increase in diametar <strong>of</strong> <strong>the</strong><br />

hole. The pullout force is time-dependent since contact area (A) and coefcient <strong>of</strong> friction<br />

() increases with time.<br />

Figure 2. Pipe before stuck (a), stuck pipe (b) and forces to free <strong>the</strong> pipe (c)


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 187<br />

3 DIFFERENTIAL STICKING CAUSES<br />

Differential sticking causes could be: (a) relatively high differential pressure and (b)<br />

mud cake characteristics (thickness, permeability, lubricity). In <strong>the</strong> situations when is not<br />

possible to reduce <strong>the</strong> differential pressure by reducing <strong>the</strong> mud weight <strong>the</strong> option is to act<br />

on <strong>the</strong> mud cake (Outmans, 1974). In situation when pipe is rotating, dynamic lter cake<br />

is formed and drill collar penetrates only a short distance into mud lter cake (Figure 3a)<br />

but when pipe is stationary, static mud lter cake is formed and drill collar is pushed into<br />

mud lter cake by differential pressure (Figure 3b). In highly deviated wellbores, with pipe<br />

being stationary, pressure between mud lter cake and drill collar varies from zero to P<br />

(Figure 3c).<br />

Figure 3. Situation in wellbore with pipe rotating (a) and pipe stationary (b and c)<br />

3.1 Methods <strong>of</strong> reducing <strong>the</strong> risk <strong>of</strong> differential sticking<br />

Differential sticking tendencies <strong>of</strong> mud depend on mud lter cake properties: thickness,<br />

shear strenght, and lubricity. These lter cake properties are inuenced by a combination<br />

<strong>of</strong> variables such as: mud overbalance, solids content <strong>of</strong> <strong>the</strong> mud (both high-gravity and<br />

low-gravity solids), mud type (e.g., oil-based, polymer water-based, gel water-based),<br />

specic mud composition, and uid loss. Early detection <strong>of</strong> differential pressure sticking<br />

risks could be made through observation <strong>of</strong> torque and drag levels while drilling to detect<br />

any sign <strong>of</strong> deviation from a normal trend for <strong>the</strong> well. The objective <strong>of</strong> <strong>the</strong> stuck pipe<br />

avoidance practices is to ensure conditions are maintained at all times that allow pulling<br />

force to exceed sticking force (shear strenght) (Dupriest et al, <strong>2010</strong>). To mitigate differential<br />

pressure sticking events, operators <strong>of</strong>ten (Montgomery et al., 2007, Simon et al., 2005):<br />

• Minimize <strong>the</strong> overbalance (by decreasing mud weight),<br />

• Minimize stationary time (drill string rotates at all times),<br />

• Minimize drilled length through low pressure formations,<br />

• Increase drill collar and drill string stabilization,<br />

• Optimize uid properties in attempts to minimize <strong>the</strong> risk <strong>of</strong> sticking, and<br />

• Select a drilling uid that will yield smooth lter cake with low coefcient <strong>of</strong> friction.<br />

The addition <strong>of</strong> certain lubricants to water- and oil- based muds will reduce <strong>the</strong> risk <strong>of</strong><br />

differential sticking and, should sticking still occur, reduce <strong>the</strong> force needed to free <strong>the</strong><br />

stuck pipe or tool. Lubricants are designed to reduce <strong>the</strong> coefcient <strong>of</strong> friction <strong>of</strong> drilling<br />

uid which decreases torque and drag. Depending on <strong>the</strong>ir chemical composition and state<br />

<strong>of</strong> dispersion or solubility in <strong>the</strong> base mud, lubricants can: (a) coat metal surfaces, reducing


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<strong>the</strong> adhesion <strong>of</strong> steel to <strong>the</strong> mud cake, (b) be incorporated into <strong>the</strong> lter cake and provide<br />

better uid-loss control (resulting in thinner cakes), and (c) be incorporated into <strong>the</strong> lter<br />

cake to reduce <strong>the</strong> yield stress <strong>of</strong> <strong>the</strong> cake.<br />

However, despite <strong>the</strong> best efforts <strong>of</strong> operators a differential pressure sticking event may<br />

still occur (Ayers et al., 1989). The best cure for differential sticking is to prevent it by use<br />

<strong>of</strong> drill-collar stabilizers and, more important, conscientiouslly shortening <strong>the</strong> intervals <strong>of</strong><br />

rest when pipe is opposite permeable formations (Dupriest et al., <strong>2010</strong>).<br />

3.2 Methods <strong>of</strong> freeing <strong>the</strong> stuck pipe<br />

Methods used to get <strong>the</strong> pipe free, in addition to pulling and torquing <strong>the</strong> pipe, include:<br />

(a) lowering hydrostatic pressure in <strong>the</strong> wellbore (by reducing <strong>the</strong> mud weight; this will<br />

reduce <strong>the</strong> differential pressure; should not be used if well control is a problem), (b) placing<br />

a spotting uid next to <strong>the</strong> stuck zone and (c) applying shock force just above <strong>the</strong> stuck<br />

point by mechanical jarring, or (d) all <strong>the</strong> above. The most common approach, however,<br />

to getting pipe free is to pump a chemical spotting uid in a wellbore annulus. Before<br />

placement <strong>of</strong> spotting uid, <strong>the</strong> depth (free point) to where <strong>the</strong> drill string is free and where<br />

sticking starts must be determined. This free point can be calculated using measurements<br />

taken on <strong>the</strong> rig oor. Knowing <strong>the</strong> stretch L and <strong>the</strong> forces applied F 1<br />

and F 2<br />

, Hooke’s<br />

law, <strong>the</strong> length <strong>of</strong> <strong>the</strong> drill string from <strong>the</strong> surface to <strong>the</strong> free point (L f<br />

) is equal to:<br />

(Eq. 2)<br />

where<br />

• E is <strong>the</strong> Elastic Modulus (Young’s Modulus) <strong>of</strong> steel (i.e., 200 GPa),<br />

• A is <strong>the</strong> cross-sectional area <strong>of</strong> <strong>the</strong> pipe body (m 2 ),<br />

• L is <strong>the</strong> stretch distance (elastical stretch <strong>of</strong> <strong>the</strong> free portion <strong>of</strong> <strong>the</strong> drill string (m),<br />

• F1 is <strong>the</strong> force to place <strong>the</strong> entire drill string in tension (N),<br />

• F2 is a force greater than F1 but less that <strong>the</strong> force limited by <strong>the</strong> yield stress <strong>of</strong> <strong>the</strong><br />

pipe grade (N).<br />

3.3 Spotting fluid<br />

A spotting uid (spot) is a small volume or pill <strong>of</strong> any substance, oil or water base, that is<br />

positioned in <strong>the</strong> wellbore to achieve a specic purpose. Most service companies provide<br />

multiple spotting uid options. The purpose <strong>of</strong> <strong>the</strong> spotting uid is to dissolve or break<br />

down <strong>the</strong> lter cake so <strong>the</strong> pipe can be freed. Possible mechanisms <strong>of</strong> spotting uid action<br />

to help free differentially stuck pipe are (Montgomery et al., 2007):<br />

• Breaks <strong>the</strong> capillary forces that hold <strong>the</strong> drillstring against <strong>the</strong> wellbore wall,<br />

• Penetrates, dehydrates and cracks (breaks up) <strong>the</strong> mud lter cake,<br />

• Reduces <strong>the</strong> contact (stuck) area between pipe and wall,<br />

• Reduces <strong>the</strong> forces needed to work <strong>the</strong> pipe free,<br />

• Increases drillstring lubricity throughout stuck zone.<br />

• Allows pipe to be pulled free.<br />

Spotting uids need to be in place as quickly as possible (within six hours after pipe<br />

becoming stuck). Figure 4 shows free drill collar in <strong>the</strong> center <strong>of</strong> hole (a), initial (b) and nal<br />

(c) position <strong>of</strong> drill collar in contact with wall, before spotting uid. When pipe sticking


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 189<br />

occurs, pupming <strong>of</strong> spotting uid has to be as quickly as possible to minimize continued<br />

lter cake buildup which leads to higher contact angle and pull free forces (Fig. 4c).<br />

Mud lter cake shrunk after spotting uid (Fig. 4d) and drill collar is freed (Fig. 4e).<br />

Figure 4. Position <strong>of</strong> drill collar in <strong>the</strong> hole before and after spotting uid<br />

Spotting uids could be devided into four main categories: (a) water-based spotting uids,<br />

(b) diesel-based spotting uids, (c) syn<strong>the</strong>tic-based spotting uids, and (d) acid based<br />

spotting uid. They could be unweighted or weighted (spotting uid, viscosier and<br />

weighting material) and consist <strong>of</strong> detergents, soaps, oils, surfactants and o<strong>the</strong>r chemicals<br />

(wall cake cracking material). Oil-based mud is <strong>the</strong> traditional spotting uid (Krol, 1981;<br />

Ayers et al., 1989). Because <strong>of</strong> concern about mud disposal, spotting uids used <strong>of</strong>fshore<br />

are ei<strong>the</strong>r syn<strong>the</strong>tic-based uids or benign water-based uids (such as drill-in uids<br />

and salt solutions) (Kercheville et al.,1986). Drill-in uids are low and ultra-low solids<br />

uids; <strong>the</strong> sealing mechanism is generated inside <strong>the</strong> rock, so <strong>the</strong>y are leaving just a thin<br />

lm on <strong>the</strong> borehole walls. Salt solutions with a low activity coefcient combined with<br />

environmentally-safe lubricants (two-phase spot) produce low torque levels.<br />

4 LABORATORY RESEARCH<br />

Laboratory tests were carried out to determine <strong>the</strong> effectiveness <strong>of</strong> mud system additives<br />

in minimizing differential pressure sticking <strong>of</strong> drill pipe. Differential sticking tendency <strong>of</strong><br />

<strong>the</strong> tested lignosulfonate mud was evaluated using differential sticking tester marketed by<br />

OFI Testing Equipment International (Figure 5). The test device consists <strong>of</strong> ltration cell<br />

capable <strong>of</strong> holding 200 mL <strong>of</strong> uid, perforated bottom capable <strong>of</strong> holding lter paper and<br />

screen, plate (on a plunger) and torque wrench. Torque necessary to break <strong>the</strong> plate free is<br />

measured. Tests were carried out at room temperature and pressure <strong>of</strong>: 3 292.2 kPa (477.5<br />

PSI). Differential sticking tester measures <strong>the</strong> stuck pipe tendency coefcient <strong>of</strong> drilling<br />

uids, and also determines how effective lubricants or treatments might be with any given<br />

drilling uid.


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Figure 5. OFITE Differential sticking tester<br />

This coefcient takes into account both <strong>the</strong> friction, or “stickiness”, <strong>of</strong> <strong>the</strong> lter cake, as<br />

well as <strong>the</strong> amount <strong>of</strong> cake building that must occur in order to freeze or stick <strong>the</strong> pipe in <strong>the</strong><br />

hole. By measuring <strong>the</strong> area <strong>of</strong> cake building during a test, <strong>the</strong> bulk sticking coefcient is<br />

obtained and read directly at <strong>the</strong> end <strong>of</strong> <strong>the</strong> test. How likely a given uid will be to produce<br />

a stuck pipe situation and how effective a given treatment may be, can be immediately<br />

determined on-site. The bulk sticking coefcient (K sc<br />

) is calculated by dividing <strong>the</strong> sliding<br />

force (F s<br />

) by <strong>the</strong> normal force (F n<br />

):<br />

K sc<br />

= F s<br />

/ F n<br />

(Eq. 3)<br />

For radius <strong>of</strong> plate r = 25.4 mm (1”):<br />

The sliding force (F s<br />

) <strong>of</strong> <strong>the</strong> plate is a function <strong>of</strong> <strong>the</strong> measured torque (T u<br />

).<br />

F s<br />

= 1.5 × T u<br />

(Eq. 4)<br />

The normal force (F n<br />

) on <strong>the</strong> plate is determined by multiplying <strong>the</strong> area by <strong>the</strong> differential<br />

pressure (This assumes that a pressure <strong>of</strong> 477.5 PSI was used during <strong>the</strong> test) (Eq. 5)<br />

Fn = 1 500 × r 2 (Eq. 5)<br />

Finally, <strong>the</strong> bulk sticking coefcient (Ksc) is equal to:<br />

K sc<br />

= 0.001 × T n<br />

(Eq. 6)


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 191<br />

Where T u<br />

is torque reading (lb f<br />

-inch or 0.1129 N·m).<br />

The stuck tendency coefcient (K st<br />

) is equal to <strong>the</strong> bulk sticking coefcient (K sc<br />

) multiplied<br />

by <strong>the</strong> variable stuck area (Eq. 7):<br />

K st<br />

= K sc<br />

× (Variable Stuck Area) (Eq. 7)<br />

Laboratory tests were run to evaluate <strong>the</strong> effectiveness <strong>of</strong> mud system additives:<br />

Carboxymethylcellulose - CMC (ltration control additive) and lubricant on differential<br />

sticking tendency <strong>of</strong> <strong>the</strong> tested uids (Gaurina-Meimurec et al., <strong>2010</strong>.). Formulations<br />

<strong>of</strong> tested lignosulphonate mud is shown in Table 1. To determine inuence <strong>of</strong> CMC and<br />

lubricant on mud properties, especially on differential sticking tendency, amount <strong>of</strong> CMC<br />

and lubricant (Lube 167) in base lignosulphonate mud was varied. The numbers included<br />

in <strong>the</strong> mud sign implies CMC concentration in grams per 1 L <strong>of</strong> <strong>the</strong> mud (C0, C3, C5)<br />

and lubricant concentration in ml per 1 L <strong>of</strong> <strong>the</strong> mud (L0, L20, L40). Mud properties such<br />

as API uid loss, cake thickness, rheological properties and pH value were determined<br />

according to API RP13B (API Recommended Practice Standard Procedure for Testing<br />

Drilling Fluids). Spotting uid was composed <strong>of</strong> 620 ml Diesel oil, 80 ml Pipe Lax W, 280<br />

ml water and 73 g barite. Spotting time was 16 hours.<br />

Composition Units C0L0 C3L0 C5L0 C0L20 C3L20 C5L20 C0L40 C3L40 C5L40<br />

Water ml 1000 1000 1000 1000 1000 1000 1000 1000 1000<br />

Bentonite g L -1 80 80 80 80 80 80 80 80 80<br />

FCL g L -1 20 20 20 20 20 20 20 20 20<br />

NaOH g L -1 3 3 3 3 3 3 3 3 3<br />

CMC g L -1 0 3 5 0 3 5 0 3 5<br />

Viscosifer g L -1 5 5 5 5 5 5 5 5 5<br />

Biocide g L -1 0,6 0,6 0,6 0,6 0,6 0,6 0,6 0,6 0,6<br />

Lubricant ml L -1 0 0 0 20 20 20 40 40 40<br />

Defoamer ml L -1 1 1 1 1 1 1 1 1 1<br />

Barite g L -1 500 500 500 500 500 500 500 500 500<br />

Table 1. Formulation <strong>of</strong> <strong>the</strong> tested lignosulphonate mud<br />

Laboratory results are shown in gures from 6 to 15. Torque increases with time regardless<br />

<strong>of</strong> concentration <strong>of</strong> CMC and lubricant, but for specied time decreases with increasing<br />

concentration <strong>of</strong> CMC and lubricant. In addition, torque decreases after placement <strong>of</strong><br />

spotting uid for16-hours (Fig. 6).


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Figure 6. Effect <strong>of</strong> time and additives on torque<br />

Bulk sticking coefcient after 300 min sticking time is decreased with increasing<br />

concentration <strong>of</strong> CMC and lubricant. For instance, <strong>the</strong> value <strong>of</strong> bulk sticking coefcient <strong>of</strong><br />

C5L40 mud is 35,3 % lesser than <strong>of</strong> C0L0 mud, and for C5L40 bulk sticking coefcient is<br />

2,3 times less after 16 hours spotting time (Fig. 7).<br />

Figure 7. Effect <strong>of</strong> CMC and lubricant on bulk sticking coefcient<br />

Bulk sticking coefcient is decreased with increasing concentration <strong>of</strong> CMC but increased<br />

with time regardless <strong>of</strong> concentration <strong>of</strong> CMC (mud without lubricant) (Fig 8).


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 193<br />

Figure 8. Effect <strong>of</strong> time and concentration <strong>of</strong> CMC on bulk sticking coefcient<br />

Bulk sticking coefcient <strong>of</strong> mud without lubricant and with 5 g CMC after 300 min is 9,2<br />

% less than without CMC but 2,4 times higher than after 60 min (Fig. 9). The bulk sticking<br />

coefcient <strong>of</strong> mud with 5 g CMC and with 4% lubricant after 300 min test is 29 % less than<br />

without lubricant.<br />

Figure 9. Effect <strong>of</strong> lubricant on bulk sticking coefcient<br />

The corelation between torque after 60 min and mud properties (uid loss, cake thicknes,<br />

plastic viscosity, gel strengts and pH value) is observed. The lower uid loss value <strong>the</strong><br />

lower value <strong>of</strong> torque (Fig. 10). In addition, API Fluid loss decreases with addition <strong>of</strong> CMC


194<br />

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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 10. The corelation between torque and uid loss <strong>of</strong> tested muds<br />

Cake thickness and torque decreases with increasing concentration <strong>of</strong> CMC and lubricant.<br />

The thiner cake <strong>the</strong> lower torque (Fig. 11).<br />

Figure 11. The corelation between torque and cake thickness <strong>of</strong> tested muds<br />

Plastic viscosity and yield point increase with increasing concentration <strong>of</strong> CMC and


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 195<br />

lubricant (Fig. 12 and 13).<br />

Figure 12. The corelation between torque and plastic viscosity <strong>of</strong> tested muds<br />

Figure 13. The corelation between torque yield point <strong>of</strong> tested muds<br />

Gel strenght increases and pH value decreases with increasing concentration <strong>of</strong> CMC and<br />

lubricant (Fig. 14 and 15).


196<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Figure 14. The corelation between torque and gel strenght <strong>of</strong> tested muds<br />

Figure 15. The corelation between torque and pH value <strong>of</strong> tested muds<br />

5 CONCLUSIONS<br />

The sticking tendency <strong>of</strong> mud can be estimated using differential sticking tester. Use <strong>of</strong><br />

<strong>the</strong> test at <strong>the</strong> well-site allows <strong>the</strong> mud engineer to identify <strong>the</strong> problem before <strong>the</strong> sticking


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 197<br />

occurs, and to select and implement <strong>the</strong> most effective treatment option.<br />

According to performed tests torque and bulk sticking coecient constantly increase with<br />

sticking time regardless <strong>of</strong> concentration <strong>of</strong> CMC and lubricant in tested lignosulphonate<br />

mud, but for any specied sticking time (60 min, 120 min, 180 min, 240 min or 300 min)<br />

<strong>the</strong>ir values decrease with increasing concentration <strong>of</strong> CMC and lubricant. After placement<br />

<strong>of</strong> spotting uid for16-hours torque signicantly decreases. In addition, <strong>the</strong> corelation between<br />

mud composition, torque and mud properties is observed. API uid loss, lter cake<br />

thickness and pH value decrease but plastic viscosity, yield point and gel strenght increase<br />

with increasing concentration <strong>of</strong> CMC and lubricant. Fluid loss and lter cake thickness<br />

have a direct inuence on values <strong>of</strong> <strong>the</strong> torque and sticking coefcient (reducing sticking<br />

area). The lower uid loss and <strong>the</strong> thiner cake <strong>the</strong> lower values <strong>of</strong> <strong>the</strong> torque and <strong>the</strong> bulk<br />

sticking coefcient. Therefore using <strong>the</strong> lignosulphonate mud signed C5L40 with 5 gL-1<br />

CMC and 40 mlL-1 lubricant sticking pipe can be avoided or if it still occurs <strong>the</strong> force<br />

required to free differentially stuck pipe will be less.<br />

6 REFERENCES<br />

1. Ayers, R.C., O´Reilly, J.E., Henry, L.R. (1989.) Offshore Operators Committee Gulf<br />

<strong>of</strong> Mexico Spotting Fluid Survey, paper SPE/IADC 18683, presented at <strong>the</strong> 1989 SPE/<br />

IADC Drilling Conference, New Orleans, Louisiana, February 28-March 3, 517-519.<br />

2. Bushnell-Watson, Y.M., Panesar, S.S. (1991) Differential Sticking Laboratory Tasts<br />

Can Improve Mud Design, paper SPE 22549 presented at <strong>the</strong> 66th Annual Technical<br />

Conference and Exhibition <strong>of</strong> <strong>the</strong> Society <strong>of</strong> Petroleum Engineers, Dallas, TX,<br />

October 6-9.147-156.<br />

3. Dupriest, F.E., Elks Jr., W.C., Ottesen, S. (<strong>2010</strong>.) Design Methodology and Operational<br />

Practices Eliminate Differential Sticking, paper IADC/SPE 128129, presented at<br />

<strong>the</strong> <strong>2010</strong> IADC/SPE Drilling Conference and Exhibition, New Orleans, Louisiana,<br />

February 2-4. 5-13.<br />

4. Gaurina-Meimurec, N., Paši, B., Matanovi, D. (<strong>2010</strong>.) Spotting Fluids for<br />

Freeing Differentially Stuck Pipe, The 1st Annual Congress <strong>of</strong> Oil Field Chemicals,<br />

Conference Proceedings, Beijing, China, November 15-17, 57.<br />

5. Isambourg, P., Ottesen, S., Benaissa, S., Marti, J. (1999.) Down-Hole Simulation Cell<br />

for Measurement <strong>of</strong> Lubricity and Differential Pressure Sticking, paper SPE/IADC<br />

52816, presented at <strong>the</strong> 1999 SPE/IADC Drilling Conference, Amsterdam, Holland,<br />

March 9-11, 1-12.<br />

6. Kercheville, J.D., Hinds, A.A., Clements, W.R. (1986.) Comparison <strong>of</strong> Environmentally<br />

Acceptable Materials with Diesel Oil for Drilling Mud Lubricity and Spotting Fluid<br />

Formulations, paper IADC/SPE 14797, presented at <strong>the</strong> 1986 IADC/SPE Drilling<br />

Conference, Dallas, Texas, February 10-12, 611-615.<br />

7. Krol, A.D. (1981.) Laboratory Evaluation <strong>of</strong> Stuck Pipe Spotting Fluid Effectiveness,<br />

paper SPE 10096, presented at <strong>the</strong> 56th Annual Fall Technical Conference and<br />

Exhibition <strong>of</strong> Society <strong>of</strong> Petroleum Engineers <strong>of</strong> AIME, San Antonio, Texas, October<br />

5-7.1-13.<br />

8. Montgomery, J.K., Keller, S.R., Krahel, N., Smith, M.V. (2007) Improved Method for<br />

Use <strong>of</strong> Chelation to Free Stuck Pipe and Enhance Treatment <strong>of</strong> Lost Returns, paper<br />

SPE/IADC 105567 presented at <strong>the</strong> 2007 SPE/IADC Drilling Conference,Amsterdam,<br />

The Ne<strong>the</strong>rlands, 20-22 February, pp 1-7.<br />

9. Outmans, H.D. (1974.) Spot Fluid Quickly to Free Differentially Stuck Pipe, The Oil<br />

and Gas Journal, July 15, 65-68.<br />

10. Pal, K., Mangla, V.K., Joshi, N.P., Tewari, P.P., Bose, U.N. (2000.) A New Approach


198<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Solves Differential Sticking Problems in Geleki and Ahmedabad Fields, paper SPE<br />

63055, presented at <strong>the</strong> 2000 SPE Annual Technical Conference and Exhibition,<br />

Dallas, Texas, October 1-4.1-8.<br />

11. Reid, P.I., Meeten, G.H., Way, P.W., Clark, P., Chambers, B.D., Gilmour, A., Sanders,<br />

M.W. (2000.) Differential-Sticking Mechanisms and a Simple Wellsite Test for<br />

Monitoring and Optimizing Drilling Mud Properties, SPE Drilling & Completion,<br />

Vol. 15, No. 2, June, 97-104.<br />

12. Simon, K., Gaurina-Meimurec, N.; Paši, B. (2005) Drilling Fluids Differential<br />

Sticking Tendency Determination, Rudarsko-geološko-naftni zbornik, Vol.17, Faculty<br />

<strong>of</strong> Mining, Geology and Petroleum Engineering, Zagreb, 31-35.<br />

13. ***, (1998) FLUID Facts – Engineering Handbook, Baker Hughes Inteq, Houston,<br />

TX, March 1998.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 199<br />

Use <strong>of</strong> Plasma Technology for Modification <strong>of</strong> Textiles<br />

Pr<strong>of</strong>. dr. Ružica Čunko<br />

Faculty <strong>of</strong> Textile Technology, University <strong>of</strong> Zagreb<br />

Prilaz baruna Filipovića 28a, Zagreb<br />

rcunko@ttf.hr<br />

tel. 01/3712-523<br />

Dr. Sanja Ercegović Ražić<br />

Faculty <strong>of</strong> Textile Technology, Univesity <strong>of</strong> Zagreb<br />

Prilaz baruna Filipovića 28a, Zagreb<br />

Abstract<br />

The use <strong>of</strong> non-<strong>the</strong>rmal, oxygen and argon low-presser plasmas for modication <strong>of</strong> cellulose<br />

textiles is discussed. The emphasis is given to <strong>the</strong> characterization <strong>of</strong> <strong>the</strong> complex micromorphology<br />

and physical-chemical changes <strong>of</strong> <strong>the</strong> textile surface after plasma treatments,<br />

as well as on dening <strong>the</strong> impacts <strong>of</strong> <strong>the</strong>se changes on <strong>the</strong> obtained nal properties <strong>of</strong><br />

textile materials treated in this way. SEM and AFM results conrmed <strong>the</strong> <strong>the</strong>sis that using<br />

oxygen and argon plasmas, two, essentially different, processes <strong>of</strong> textile surface ablation<br />

occurred; <strong>the</strong> rst is chemical etching and <strong>the</strong> second physical sputtering. Using <strong>the</strong> AFM,<br />

<strong>the</strong> bre surface morphology was estimated at nanoscale. The measurements <strong>of</strong> <strong>the</strong> vertical<br />

rise <strong>of</strong> water in fabric sample and <strong>the</strong> results <strong>of</strong> <strong>the</strong> wetting time (vertical test and drop<br />

test) indicate <strong>the</strong> improvement <strong>of</strong> hydrophilic properties <strong>of</strong> all tested samples after lowpressure<br />

oxygen plasma treatment. The presented results conrm that <strong>the</strong> low-pressure<br />

plasma treatment is an acceptable and appropriate method <strong>of</strong> textile surface modication<br />

and an eco-friendly method at <strong>the</strong> same time.<br />

Keywords: low-pressure plasma, surface functionalization, cellulose fabric modication.<br />

1 Introduction<br />

The textile and clothing industries in Europe, USA, Japan and some o<strong>the</strong>r developed<br />

countries are facing some big challenges today, largely because <strong>of</strong> <strong>the</strong> globalization process.<br />

Therefore, <strong>the</strong> shift to high- and multifunctional, added value, luxury and technical textiles<br />

is deemed to be essential for <strong>the</strong>ir sustainable growth. The growing environmental and<br />

energy-saving conditions will also lead to <strong>the</strong> gradual replacement <strong>of</strong> many traditional wet<br />

chemistry-based textile processing, using large amounts <strong>of</strong> water, energy and efuents,<br />

by various forms <strong>of</strong> low-liquor and dry-nishing processes. Plasma technology, when<br />

developed at a commercially viable level, has strong potential to <strong>of</strong>fer in an attractive way<br />

achievement <strong>of</strong> new functionalities in textiles.<br />

The signicant research work on introduction <strong>of</strong> plasma technology in <strong>the</strong> textile eld has<br />

been going since <strong>the</strong> early 1980s and recently <strong>the</strong> application <strong>of</strong> plasma treatments for<br />

textile modication has become more and more signicant. In many laboratories across<br />

<strong>the</strong> world <strong>the</strong> researches are dealing with plasma treatments <strong>of</strong> variety <strong>of</strong> brous materials<br />

in order to improve <strong>the</strong>ir functional properties. A variety <strong>of</strong> low-pressure and atmospheric<br />

plasma machines, mostly in prototype form, have been <strong>of</strong>fered for industrial processing <strong>of</strong>


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textiles. In recent years, considerable efforts have been made by many plasma technology<br />

suppliers, as well as researches, to impart broad range <strong>of</strong> new functionalities and textile<br />

properties by plasma treatment [2, 7, 10, 23, 24, 27, 28].<br />

In <strong>the</strong> recent point <strong>of</strong> view, a desired ber surface characteristics and textiles modication<br />

by plasma seem very promising. Plasma treatments can be used both in substitutions<br />

<strong>of</strong> conventional processes and for <strong>the</strong> production <strong>of</strong> innovative textile materials with<br />

properties that cannot be achieved via wet processing. They are applicable to different<br />

textile substrates, even to those that cannot be modied by conventional methods. It is<br />

important to note, that plasma agency is limited to <strong>the</strong> top surface layer and no signicant<br />

alteration <strong>of</strong> bulk properties <strong>of</strong> <strong>the</strong> ber is produced. Plasma treatments are fast and<br />

extremely gentle, as well as environmentally friendly, being dry processes characterized<br />

by low consumption <strong>of</strong> chemicals and energy [3, 15]. If plasmas are used as pre-treatment,<br />

<strong>the</strong>y can reduce <strong>the</strong> amount <strong>of</strong> chemicals required by <strong>the</strong> conventional process and <strong>the</strong><br />

concentration <strong>of</strong> pollutants in <strong>the</strong> efuents.<br />

The rst investigation <strong>of</strong> possibilities and phenomenology <strong>of</strong> textiles modication by<br />

plasma treatment in Croatia was carried out within <strong>the</strong> scope <strong>of</strong> <strong>the</strong> research project<br />

Multifunctional textile materials for personal protection (Faculty <strong>of</strong> Textile Technology,<br />

Department <strong>of</strong> materials, bres and textile testing, 1997-<strong>2011</strong>). The results <strong>of</strong> a part <strong>of</strong> this<br />

research are presented in this paper.<br />

2 Possibilities and phenomenology <strong>of</strong> cellulose textiles modification<br />

by plasma treatment<br />

2.1 What is plasma?<br />

Plasma was rst identied (as “radiant matter”) by Sir W. Crookes in 1879; Sir J. J. Thomson<br />

identied <strong>the</strong> nature <strong>of</strong> <strong>the</strong> matter in 1897, and in 1928. I. Langmuir has introduced <strong>the</strong><br />

term “plasma”. In physics plasma is dened as distinct phase <strong>of</strong> matter, separate from<br />

<strong>the</strong> traditional solids, liquids, and gases. It comprises a dynamic mix <strong>of</strong> ions, electrons,<br />

neutrons, photons, free radicals, meta-stable excited species and molecular fragments.<br />

Since <strong>the</strong> particles in plasma are electrically charged (generally by being stripped <strong>of</strong><br />

electrons), it is frequently described as an “ionized gas.” Energy is needed to strip electrons<br />

from atoms to make plasma. The energy can be <strong>of</strong> various origins: <strong>the</strong>rmal, electrical, or<br />

light (ultraviolet light or intense visible light from a laser). With insufcient sustaining<br />

power, plasmas recombine into neutral gas.<br />

Plasma is electrically conductive and can be manipulated by magnetic elds. It is odd to<br />

consider that plasma is actually <strong>the</strong> most common phase <strong>of</strong> matter, especially since it was<br />

<strong>the</strong> last one discovered. Flame, lightning, interstellar nebulae, stars, and even <strong>the</strong> empty<br />

vastness <strong>of</strong> space are all examples <strong>of</strong> <strong>the</strong> plasma state <strong>of</strong> matter.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 201<br />

Figure 1 Plasma lamp [13]<br />

The colors are a result <strong>of</strong> relaxation <strong>of</strong> electrons in excited states to lower energy states<br />

after <strong>the</strong>y have recombined with ions. These processes emit light in<br />

a spectrum characteristic <strong>of</strong> <strong>the</strong> gas being excited.<br />

2.2 Principles <strong>of</strong> plasma processes and application <strong>of</strong> plasma<br />

in <strong>the</strong> field <strong>of</strong> textiles<br />

Plasmas are generally classied as <strong>the</strong>rmal and non-<strong>the</strong>rmal. Thermal (“hot”) plasmas are<br />

characterized by a condition <strong>of</strong> <strong>the</strong>rmal equilibrium between different species contained<br />

in <strong>the</strong> gas and <strong>the</strong>ir temperature raise <strong>of</strong> several thousand degrees. It is clear that <strong>the</strong>se<br />

plasmas due to <strong>the</strong>ir destructive nature, are not suitable for textile treatment.<br />

Contrary to <strong>the</strong>rmal plasmas, non-<strong>the</strong>rmal plasmas are “cold” plasmas and are produced<br />

at room temperature or little above room temperature. In this case, electrons have higher<br />

energies than ions and molecules (<strong>the</strong>ir energies ranging from 0.1 to some electron volts),<br />

and, due to <strong>the</strong> low density <strong>of</strong> <strong>the</strong> gas, collisions with <strong>the</strong> o<strong>the</strong>r species are relatively rare<br />

and <strong>the</strong>rmal equilibrium is not reached. The bulk temperature <strong>of</strong> <strong>the</strong> gas is comparable to<br />

room temperature. Electron collisions with neutral species produce additional electrons<br />

and ions. Thanks to <strong>the</strong> low operating temperatures, cold plasmas are suitable for textile<br />

treatment. The most important for this purpose are low-pressure plasma and atmospheric<br />

pressure plasma [11, 17, 20, 22, 23].<br />

Using <strong>of</strong> high vacuum pumps, <strong>the</strong> low-pressure plasma reactors are working in <strong>the</strong> pressure<br />

range <strong>of</strong> 10 -2 to 10 -3 mbar (vacuum vessel). The gas which is <strong>the</strong>n introduced in <strong>the</strong> vessel<br />

is ionized with <strong>the</strong> help <strong>of</strong> high frequency generator. For radi<strong>of</strong>requency range (typically<br />

40 KHz or 13, 56 MHz), normally <strong>the</strong> working gas pressure is kept in <strong>the</strong> lower 0.1 mbar<br />

range, whereas for micro-wave sources (915 MHz or 2.45 GHz), a working pressure<br />

between 0.5 and 1 mbar is <strong>of</strong>ten used.<br />

The interaction between <strong>the</strong> very active chemical species and photons present in <strong>the</strong> plasma<br />

gas and a textile substrate is <strong>the</strong> basis <strong>of</strong> dissimilar industrial applications. As a consequence<br />

<strong>of</strong> <strong>the</strong> very complex and non-equilibrium nature <strong>of</strong> cold plasmas, a multiplicity <strong>of</strong> very<br />

different phenomena can occur, depending on <strong>the</strong> art <strong>of</strong> <strong>the</strong> gas and <strong>the</strong> operating conditions<br />

[11, 12, 17, 18, 28]. The most important plasma/textile interaction processes are: cleaning<br />

or etching, surface activation, grafting, polymerization and deposition (Fig. 2). All <strong>the</strong>se<br />

phenomena occur at <strong>the</strong> bre surface and are limited to <strong>the</strong> most external layer <strong>of</strong> <strong>the</strong><br />

substrate. Normally, <strong>the</strong> effects do not involve layers deeper than 10 -100 nm.


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Figure 2 Cold plasma processes [19]<br />

2.3 Mechanisms <strong>of</strong> interactions between plasmas and cellulose fibres<br />

Cellulose is <strong>the</strong> most widely known brous polysaccharides and <strong>the</strong> basic building polymer<br />

<strong>of</strong> agricultural bres (cotton, ax, hemp) as well as <strong>of</strong> various man-made bres (viscose,<br />

modal, lyocell, bamboo). The basic structural repeating unit for cellulose is <strong>the</strong> cellobiose<br />

unit, composed <strong>of</strong> two anhydroglucose rings e.g. anhydroglucose units. Each unit contains<br />

three alcohol hydroxyls groups (-OH). These hydroxyls form hydrogen bonds inside<br />

<strong>the</strong> macromolecule itself (intra-molecular) and between o<strong>the</strong>r cellulose macromolecules<br />

(intermolecular). Cellulose in bres is highly crystalline polymer with tight packing <strong>of</strong><br />

ordered chains wherein <strong>the</strong> hydrogen bonding is very strong. Cellulose bre also contains<br />

amorphous regions in which <strong>the</strong>re can be a variation from complete disorder <strong>of</strong> <strong>the</strong><br />

cellulose chains to some order. Owing to <strong>the</strong> hydroxyl groups, cellulose can be traditionally<br />

modied through reactions <strong>of</strong> esterication and e<strong>the</strong>rication. It has been determined that<br />

<strong>the</strong> accessibility <strong>of</strong> <strong>the</strong> -OH groups is controlled by <strong>the</strong> relative ratios <strong>of</strong> crystalline and<br />

amorphous regions <strong>of</strong> <strong>the</strong> cellulose bre superstructure. Amorphous cellulose can be<br />

functionalized much more readily than <strong>the</strong>ir crystalline counterparts.<br />

Cellulose modication using cold plasma differs signicantly from <strong>the</strong> traditional<br />

esterication and e<strong>the</strong>rication reaction. Reactive plasma gas components (particles)<br />

can react directly with <strong>the</strong> anhydroglucose units by abstraction <strong>of</strong> hydrogen atoms from<br />

ei<strong>the</strong>r carbon or oxygen atoms in <strong>the</strong> plasma reactor. Thus, cellulose can be oxidized,<br />

reduced and/or substituted in new ways. XPS data collected from plasma treated cellulose<br />

samples indicate that new functionalities are formed compared with unmodied cellulose.<br />

In addition to C-OH and C-O-C, <strong>the</strong> existence <strong>of</strong> O=C=O, O-CO-O, O=C-O, C=O and<br />

O-CO-O functionalities are detected [6, 27].<br />

The interaction <strong>of</strong> <strong>the</strong> active species <strong>of</strong> plasma with cellulose in bre surface, involves<br />

several electron-mediated processes, as well as positive ion-induced reactions. Some <strong>of</strong><br />

<strong>the</strong>se reactions can promote hemolytic cleavages leading to <strong>the</strong> formation <strong>of</strong> free-radical


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sites. These reactive centers can lead to a variety <strong>of</strong> functionalization mechanisms.<br />

Cellulose can be grafted by monomer introduced in plasma gas and <strong>the</strong> grafting process<br />

is restricted to <strong>the</strong> surface layer [2, 4, 12, 21, 26]. By using specic molecules, a process<br />

known as plasma-enhanced chemical vapor deposition (PE-CVD) may occur, as well as<br />

metal nanoparticles can be deposed on bre surface using plasma gas. All <strong>the</strong>se processes<br />

are by-product free. The reactions are not accompanied by <strong>the</strong> deposition <strong>of</strong> undesired<br />

macromolecular layers on <strong>the</strong> reactor walls. Plasma treatments usually do not create<br />

signicant environmental problems.<br />

3 Experimental, materials and methods<br />

The emphasis in this investigation is given to <strong>the</strong> characterization <strong>of</strong> <strong>the</strong> complex micromorphology<br />

and physical-chemical changes <strong>of</strong> <strong>the</strong> textile surface after plasma treatments,<br />

as well as on dening <strong>the</strong> impacts <strong>of</strong> <strong>the</strong>se changes on <strong>the</strong> obtained nal properties <strong>of</strong><br />

textile materials treated in this way.<br />

3.1 Materials<br />

The textile substrate used was <strong>the</strong> cellulose fabrics woven in plain wave, using threads<br />

spun from lyocell and modal man-made cellulose bres and from cotton. The structural<br />

characteristics <strong>of</strong> sample fabrics are presented in Table 1. Before plasma treatment, <strong>the</strong> raw<br />

cotton fabric was undergoes to desizing and scouring treatments according to <strong>the</strong> industrial<br />

process conditions (sample CO sc).<br />

Table 1: Basic characteristic <strong>of</strong> tested fabric samples woven in plain weave<br />

Samples<br />

Yarn<br />

neness<br />

(warp/<br />

weft) / tex<br />

Numb. <strong>of</strong> threads<br />

(warp/weft) / cm<br />

Volume mass / gcm -3<br />

Mass per unit area /<br />

gm -2<br />

UT O 2<br />

-p Ar-p UT O 2<br />

-p Ar-p<br />

Cotton<br />

(CO sc)<br />

Lyocell<br />

(CLY I)<br />

Modal<br />

(CMD I)<br />

29.4/25.0 25/20 0.369 0.367 0.362 130.6 128.1 128.3<br />

31.3/25.0<br />

21/19<br />

0.409 0.431 0.444 120.1 126.8 129.8<br />

31.3/25.0 23/19 0.420 0.429 0.444 121.8 123.9 126.0<br />

UT = untreated sample, O 2<br />

-p = oxygen plasma treated, Ar-p = argon plasma treated sample<br />

3.2 Plasma treatment <strong>of</strong> fabric samples<br />

Plasma system<br />

Low-pressure (LP) - plasma NANO LF laboratory system (Diener Electronic GmbH,<br />

Germany, Fig 3) <strong>of</strong> 40 kHz low-frequency generator and maximum power <strong>of</strong> 300 W<br />

was used for fabric treatments. One electrode and <strong>the</strong> four trays were placed inside <strong>the</strong><br />

cylindrical vacuum chamber <strong>of</strong> 24 L volume. A standard part <strong>of</strong> <strong>the</strong> plasma system was a<br />

conventional rotary vane pump, type D8B, suction power <strong>of</strong> <strong>the</strong> approx. 8 m 3 /hour, with an<br />

electromagnetic valve, which prevented <strong>the</strong> return <strong>of</strong> <strong>the</strong> oil vapor into <strong>the</strong> vacuum chamber.<br />

Brass needle valves (max. ow rate <strong>of</strong> 400 sccm), with pressure reducers specied for each<br />

type <strong>of</strong> gases applied, provided constant gas ow rate during plasma processes performed.<br />

The plasma treatments were controlled fully automatically.


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Figure 3 Plasma system LP-Nano LF-40kHz, Diener Electronic GmbH<br />

Surface activation with oxygen and argon plasma<br />

Before plasma treatment, <strong>the</strong> fabric samples (dimensions 340x200 mm) were dried to<br />

remove <strong>the</strong> moisture and afterwards treated (separately with oxygen and argon plasma)<br />

under <strong>the</strong> optimum process conditions, determined by preliminary work [6]: <strong>the</strong> gas ow<br />

rate <strong>of</strong> 40 sccm, working pressure <strong>of</strong> 0.34 - 0.4 mbar, operating power <strong>of</strong> 300 W and<br />

treatment time <strong>of</strong> 5 min.<br />

3.3 Method <strong>of</strong> analysis<br />

Surface Analysis<br />

The bre surface micro-morphology characteristics <strong>of</strong> untreated and plasma treated fabrics<br />

were investigated using JEOL 6060LV Scanning Electron Microscopy (SEM) technique.<br />

Before analysis all <strong>the</strong> samples were coated with carbon and a 90% Au/10%Pd alloy layer.<br />

Magnication <strong>of</strong> 1000x and 7000x was used for analysis <strong>of</strong> surface changes depending on<br />

<strong>the</strong> tested bre type and applied plasma gas.<br />

The topography <strong>of</strong> bre surface roughness caused by oxygen and argon plasma treatment<br />

was analyzed using <strong>the</strong> most recent Atomic force microscopy (AFM). The concept on<br />

which AFM is based is <strong>the</strong> generation <strong>of</strong> <strong>the</strong> images <strong>of</strong> <strong>the</strong> bre surface by measuring <strong>the</strong><br />

physical interactions (forces) between a sharp tip <strong>of</strong> AFM cantilever and <strong>the</strong> sample (Fig<br />

4). When <strong>the</strong> tip is brought into proximity <strong>of</strong> a sample surface, forces between <strong>the</strong> tip and<br />

<strong>the</strong> sample lead to a deection <strong>of</strong> <strong>the</strong> cantilever according to Hooke´s law. Depending on<br />

<strong>the</strong> situation and surface topography, forces that are measured in AFM include mechanical<br />

contact force, Van der Waals forces, capillary forces, chemical bonding, electrostatic forces,<br />

magnetic forces, etc. Registered values <strong>of</strong> cantilever deection are electronically converted<br />

into pseudo three-dimensional (3D) image <strong>of</strong> a sample.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 205<br />

Figure 4 Basic schematic principle <strong>of</strong> <strong>the</strong> AFM in contact mode [14]<br />

An important feature <strong>of</strong> <strong>the</strong> AFM technique is based on <strong>the</strong> fact that, apart from <strong>the</strong><br />

qualitative characterization, it also allows <strong>the</strong> quantitative assessment <strong>of</strong> bre surface<br />

topography at <strong>the</strong> nano-scale, where <strong>the</strong> changes caused by plasma action are expected.<br />

AFM imaging was performed in contact mode, using a Multimode AFM with Nanoscope<br />

IIIa controller (Veeco Instruments, Santa Barbara, CA) with a vertical engagement (JV)<br />

125 m scanner. Contact mode imaging was performed using silicon-nitride tips (NP-<br />

20, Veeco, nom. freq. 56 KHz, nom. spring constant <strong>of</strong> 0.32 N/m); with <strong>the</strong> highest scan<br />

resolution <strong>of</strong> 512 samples per line. Processing and analysis <strong>of</strong> images were carried out<br />

using <strong>the</strong> NanoScope s<strong>of</strong>tware (Digital Instruments, version V531r1).<br />

Wet ability properties<br />

Wet ability properties were analyzed using vertical test and drop test.<br />

The Vertical test [16] was used to measure <strong>the</strong> rate <strong>of</strong> vertical capillary rise <strong>of</strong> distilled<br />

water in a woven specimen strip suspended in <strong>the</strong> distilled water (at 152 mm below <strong>the</strong><br />

water surface). The vertical rise <strong>of</strong> distilled water in fabric sample was measured in weftand<br />

warp direction. In order to achieve <strong>the</strong> better visibility <strong>of</strong> <strong>the</strong> water front rise, <strong>the</strong><br />

methylene-blue as a water colorant was used. All test specimens were conditioned at <strong>the</strong><br />

standard atmosphere, according to HRN ISO 139. Test was performed in accordance with<br />

EN ISO 9073-6:2000. In order to improve reproducibility and reliability <strong>of</strong> measurement<br />

results, all <strong>the</strong> measurements were recorded by digital video camera recorder SONY DCR-<br />

DVD304E.<br />

The Drop test was carried out as a measure <strong>of</strong> absorbency <strong>of</strong> fabric samples. The absorbency<br />

is dened as <strong>the</strong> propensity <strong>of</strong> a material to take in and retain a liquid, usually water, in <strong>the</strong><br />

pores and interstices <strong>of</strong> <strong>the</strong> material.<br />

Test was performed in accordance with AATCC e.g. TEGEWA prescription [1, 25]. A drop<br />

<strong>of</strong> water <strong>of</strong> a dened volume is allowed to fall from a xed height onto <strong>the</strong> taut surface <strong>of</strong><br />

a test specimen. The time required for full absorption <strong>of</strong> water drop (e. g. time to disappear<br />

<strong>of</strong> drop) is measured and recorded as wetting time (seconds, stopwatch).<br />

The shorter <strong>the</strong> time, <strong>the</strong> more absorbent is <strong>the</strong> textile material. Five seconds or less is<br />

generally considered to represent adequate absorbency.


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4 Results and discussion<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Surface analysis by Scanning Electron Microscopy<br />

SEM analysis <strong>of</strong> <strong>the</strong> lyocell and modal cellulose bres in <strong>the</strong> fabric sample surface were<br />

carried out with magnication <strong>of</strong> 1000x and 7000x. A part <strong>of</strong> obtained results [9] are<br />

presented in Fig. 5 and 6.<br />

Untreated lyocell bres<br />

Oxygen-plasma treated lyocell<br />

bres<br />

Argon-plasma treated lyocell<br />

bres<br />

Figure 5 SEM photographs <strong>of</strong> untreated, oxygen and argon plasma treated lyocell bres<br />

Untreated modal bres Oxygen treated modal bres Argon treated modal bres<br />

Figure 6 SEM photographs <strong>of</strong> untreated, oxygen and argon plasma treated modal bres<br />

The obtained results with SEM technique indicate that <strong>the</strong> oxygen plasma treatment<br />

certainly clean <strong>the</strong> bres surface, removing <strong>the</strong> organic contaminants from surface. The<br />

treatment with argon plasma results in sputtering <strong>of</strong> <strong>the</strong> bre surface layer increasing <strong>the</strong><br />

roughness and brillations-effect (especially by lyocell) <strong>of</strong> <strong>the</strong> bres. Thereby <strong>the</strong> specic<br />

area <strong>of</strong> bres increases and <strong>the</strong> size <strong>of</strong> bre area accessible to reactions increases to.<br />

Surface topography analysis by atomic force microscopy (AFM)<br />

The examples <strong>of</strong> bre surface topography images <strong>of</strong> untreated, as well as oxygen- and<br />

argon-plasma treated lyocell bres, observed by AFM [6, 8], are shown in Fig. 7 - 9. The<br />

results are presented in a standard form, e.g. as 3D plot <strong>of</strong> bre surface (a), <strong>the</strong> height data<br />

image (b), and section analysis <strong>of</strong> bre along marked lines (c). The vertical distance <strong>of</strong><br />

scanned topographic elements, are given as a measure <strong>of</strong> roughness <strong>of</strong> imaged surface area<br />

<strong>of</strong> bre.


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 207<br />

a<br />

Figure 7 The AFM <strong>of</strong> untreated lyocell bres:<br />

a - Surface plot - 3D topographic image; b - Section analysis along <strong>the</strong> marked line vertical to <strong>the</strong><br />

axis <strong>of</strong> <strong>the</strong> tested bre (imaged area is 25 m × 25 m with vertical scale <strong>of</strong> 3000 nm).<br />

Vertical distance marked on <strong>the</strong> c: approx. 122 nm<br />

b<br />

a<br />

Figure 8 The AFM <strong>of</strong> oxygen plasma treated lyocell bres:<br />

a - Surface plot - 3D topographic image; b - Section analysis along <strong>the</strong> marked line vertical to <strong>the</strong><br />

axis <strong>of</strong> tested bre (imaged area is 15 m x 15 m with vertical scale <strong>of</strong> 1500 nm)<br />

Vertical distance marked on <strong>the</strong> c: approx. 24 nm<br />

b<br />

a<br />

b<br />

Figure 9 The AFM <strong>of</strong> argon plasma treated lyocell bres:<br />

a - Surface plot - 3D topographic image; b - Section analysis along <strong>the</strong> marked line vertical to <strong>the</strong><br />

axis <strong>of</strong> tested bre (imaged area is 10 m × 10 m with vertical scale <strong>of</strong> 2000 nm)<br />

Vertical distance marked on <strong>the</strong> c: size range from approx. 23 nm to 59 nm


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

The results <strong>of</strong> surface roughness noticeable on <strong>the</strong> surface plots (Fig. 7 - 9) and <strong>the</strong> results<br />

obtaining by section analysis point to a different effect <strong>of</strong> oxygen and argon plasma on <strong>the</strong><br />

tested bres, as compared to <strong>the</strong> untreated ones. Surface roughness <strong>of</strong> <strong>the</strong> oxygen plasma<br />

treated bres was considerably lower (approx. 24 nm) compared to <strong>the</strong> untreated samples,<br />

where bre surface roughness was approximately 122 nm. These results additionally prove<br />

that oxygen, as a reactive gas, changes <strong>the</strong> outermost bre surface layers, resulting in <strong>the</strong><br />

removal <strong>of</strong> surface impurities and leading to smoo<strong>the</strong>r surface layer, as can be seen in Fig. 8.<br />

As opposed to oxygen, argon, as an inert gas, caused increased bre surface roughness<br />

and ruptures along <strong>the</strong> longitudinal axis <strong>of</strong> <strong>the</strong> tested bres, as can be seen in Fig. 9. The<br />

surface <strong>of</strong> <strong>the</strong> argon plasma treated sample was altered and ruptures appeared, visible on<br />

<strong>the</strong> surface and oriented in <strong>the</strong> direction <strong>of</strong> bre axis. Their size was in <strong>the</strong> range from 23<br />

to 59 nm at <strong>the</strong> imaged area as well.<br />

AFM results conrmed <strong>the</strong> <strong>the</strong>sis that using oxygen and argon plasmas, two essentially<br />

different processes <strong>of</strong> textile surface ablation occurred; <strong>the</strong> rst is chemical etching and <strong>the</strong><br />

second physical sputtering.<br />

Capillary rise <strong>of</strong> water by vertical test<br />

The capillarity method measures <strong>the</strong> rate <strong>of</strong> vertical capillary rise in a specimen strip<br />

suspended in <strong>the</strong> distilled water. The part <strong>of</strong> obtained results [5] is presented on <strong>the</strong> graphs,<br />

Fig. 10 – 12.<br />

Height <strong>of</strong> <strong>the</strong> water front, h [mm]<br />

150<br />

140<br />

130<br />

120<br />

110<br />

100<br />

90<br />

80<br />

70<br />

60<br />

50<br />

40<br />

CLY I ut (warp)<br />

CLY I O2 plasma, 5 min (warp)<br />

30<br />

CLY I O2 plasma, 5 min (weft) CLY I Ar plasma, 5 min (warp)<br />

20<br />

CLY I Ar plasma, 5 min (weft) CLY I ut (weft)<br />

10<br />

0<br />

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30<br />

Time, t [min]<br />

Figure 10 Results <strong>of</strong> <strong>the</strong> capillary rise <strong>of</strong> water measured on untreated and plasma treated lyocell<br />

fabrics in warp and weft direction


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 209<br />

Height <strong>of</strong> <strong>the</strong> water front, h [mm]<br />

150<br />

140<br />

130<br />

120<br />

110<br />

100<br />

90<br />

80<br />

70<br />

60<br />

50<br />

40<br />

30<br />

20<br />

10<br />

CMD I ut (weft)<br />

CMD I Ar plasma, 5 min (warp)<br />

CMD I O2 plasma, 5 min (weft)<br />

0<br />

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30<br />

Time, t [min]<br />

CMD I O2 plasma, 5 min (warp)<br />

CMD I Ar plasma, 5 min (weft)<br />

CMD I ut (warp)<br />

Figure 11 Results <strong>of</strong> <strong>the</strong> capillary rise <strong>of</strong> water measured on untreated and plasma treated modal<br />

fabrics in warp and weft direction<br />

Height <strong>of</strong> <strong>the</strong> water front, h [mm]<br />

150<br />

140<br />

130<br />

120<br />

110<br />

100<br />

90<br />

80<br />

70<br />

60<br />

50<br />

40<br />

CO I O2 plasma, 5min (warp) CO I Ar plasma, 5min (warp)<br />

30<br />

CO I ut (warp)<br />

CO I ut (weft)<br />

20<br />

CO I O2, 5min (weft)<br />

CO I Ar plasma, 5min (weft)<br />

10<br />

0<br />

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30<br />

Time, t [min]<br />

Figure 12 Results <strong>of</strong> <strong>the</strong> capillary rise <strong>of</strong> water measured on untreated and plasma treated cotton<br />

fabrics in warp and weft direction<br />

It is important to emphasize that several <strong>of</strong> aspects affect <strong>the</strong> wettability <strong>of</strong> treated samples,<br />

such as: bre superstructure, bre diameter, bre surface irregularity and surface chemical<br />

composition. Micro- and macrostructure <strong>of</strong> fabric is very important to. In this respect, <strong>the</strong><br />

increase <strong>of</strong> fabric structure density during plasma treatment cud be reason <strong>of</strong> <strong>the</strong> capillary<br />

force raising and better vertically rise <strong>of</strong> water through fabric.


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

Absorption time <strong>of</strong> water drop by dropt test<br />

Results <strong>of</strong> <strong>the</strong> water drop absorption time <strong>of</strong> tested fabrics are presented in Tab. 2.<br />

Table 2: Results <strong>of</strong> <strong>the</strong> water drops absorption time [s] <strong>of</strong> tested fabrics<br />

Sample<br />

Treatment<br />

Cotton<br />

(Co raw)<br />

Cotton<br />

(Co sc)<br />

Lyocell<br />

(CLY I)<br />

Modal<br />

(CMD I)<br />

Untreated > 3600 5.1 2 1.2<br />

O 2<br />

plasma, 5 min 10.0 0.8 1 0.8<br />

Ar plasma, 5 min > 3600 37.8 0.8 0.8<br />

Obtained results presented in Table 2 indicate <strong>the</strong> improvement <strong>of</strong> wetting and wicking<br />

properties <strong>of</strong> all tested samples by low-pressure oxygen plasma treatment. The oxygen<br />

plasma treatment is especially effective for raw cotton fabric. In this case <strong>the</strong> oxygen<br />

plasma treatment could be recommended as eco-friendly substitution for <strong>the</strong> wet scouring<br />

process, in order to achieve good soak properties (wettability).<br />

Plasma treatments with argon as an inert gas are not enough effective to improve wettability<br />

<strong>of</strong> cotton fabrics; <strong>the</strong> drop absorption time (s) determined for raw cotton fabric is extremely<br />

high (characteristic for hydrophobic surface). Hydrophilic property <strong>of</strong> scoured cotton<br />

fabric after argon plasma treatment still decreases (drop absorption time was increased<br />

from 5.1 to 37.8 s). Could be supposed that supercial primary wall <strong>of</strong> cotton bres is thick<br />

enough to protect bers <strong>of</strong> plasma ionized particles attacks. Contrary, <strong>the</strong> low-pressure<br />

argon plasma treatments <strong>of</strong> lyocell and modal fabrics additionally improve <strong>the</strong>ir original<br />

high hydrophilic properties.<br />

5 Conclusions<br />

Presented results are a part <strong>of</strong> investigation <strong>of</strong> <strong>the</strong> nature <strong>of</strong> low-pressure plasma inuence<br />

on <strong>the</strong> bre surface characteristics and <strong>the</strong>ir effects on <strong>the</strong> properties modication <strong>of</strong><br />

cellulose based textile materials.<br />

• The results obtained using <strong>the</strong> SEM technique indicate that <strong>the</strong> oxygen plasma<br />

treatment leads to <strong>the</strong> cleaning and etching <strong>of</strong> <strong>the</strong> bre surface, in contrary to <strong>the</strong> argon<br />

plasma treatment which resulting in sputtering <strong>of</strong> <strong>the</strong> cellulose bre surface layer. This<br />

results in increasing <strong>the</strong> roughness <strong>of</strong> <strong>the</strong> bres and contributes to <strong>the</strong> enhancement <strong>of</strong><br />

bre specic area (ratio: surface area/volume).<br />

• The AFM results conrmed <strong>the</strong> <strong>the</strong>sis that using oxygen and argon plasmas, two<br />

essentially different processes <strong>of</strong> textile surface ablation occurred; <strong>the</strong> rst is chemical<br />

etching and <strong>the</strong> second physical sputtering. The estimated vertical altitude <strong>of</strong> surface<br />

topographic elements <strong>of</strong> <strong>the</strong> oxygen plasma treated bres was considerably lower<br />

compared to <strong>the</strong> untreated samples (i.e. 24 nm in relation to 122 nm for untreated<br />

sample). The surface <strong>of</strong> <strong>the</strong> argon plasma treated sample was altered and <strong>the</strong> visible<br />

ruptures appeared on <strong>the</strong> surface. The cracks at <strong>the</strong> imaged area are oriented in <strong>the</strong><br />

direction <strong>of</strong> bre axis and <strong>the</strong>ir vertical altitude range <strong>of</strong> 22 to 59 nm as well.<br />

• The results <strong>of</strong> <strong>the</strong> vertical test and <strong>the</strong> drop test conrm <strong>the</strong> improvement <strong>of</strong> hydrophilic<br />

properties <strong>of</strong> all tested samples after low-pressure oxygen plasma treatment. Plasma<br />

treatment with inert gas argon, at <strong>the</strong> given process parameters, was not enough effective<br />

to improve wettability <strong>of</strong> cotton fabrics. Contrary, <strong>the</strong> argon plasma treatments <strong>of</strong><br />

lyocell and modal fabrics additionally improve <strong>the</strong>ir original high hydrophilic surface


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 211<br />

properties.<br />

• It could be concluded that presented investigation results conrm that <strong>the</strong> plasma<br />

treatment is an acceptable and appropriate method <strong>of</strong> textile surface modication,<br />

avoiding bre damage, and an eco-friendly method at <strong>the</strong> same time.<br />

References<br />

1. AATCC Test Method 79:2000 - Drop test<br />

2. Chen P, Wang J, Wang B, Li W, Zhang C, Li H, Sun B (2009) Improvement <strong>of</strong><br />

interfacial adhesion for plasma-treated aramid ber-reinforced poly(phthalazinone<br />

e<strong>the</strong>r sulfone ketone) composite and ber surface aging effects. Surface and Interface<br />

Analysis 41 (1) pp 38-43<br />

3. Demir A, Özdogan E, Özdil N, Gürel A (<strong>2011</strong>) Ecological materials and methods in <strong>the</strong><br />

textile industry: Atmospheric-plasma treatments <strong>of</strong> naturally colored cotton. Journal<br />

<strong>of</strong> Applied Polymer Science 119 (3) pp 1410-1416<br />

4. Denes F, Young RA (1998) Surface modication <strong>of</strong> polysaccharides under coldplasma<br />

conditions. In: Dumitriu S (Ed.) Structural Diversity and Functional Versatility <strong>of</strong><br />

Polysaccharides, New York, Basel, Hong Kong, Marcel Dekker Inc<br />

5. Ercegovi Raži S, unko R, Bautista L, Mota J, Crespo L (<strong>2010</strong>) Ageing Effect<br />

on Wettability Properties <strong>of</strong> Low-Pressure Plasma-Treated Cellulosic Fabrics. In:<br />

Dragevi Z (Ed) Proceedings <strong>of</strong> <strong>the</strong> 5th International Textile, Clothing & Design<br />

Conference - Magic World <strong>of</strong> Textiles, Faculty <strong>of</strong> Textile Technology, University <strong>of</strong><br />

Zagreb, Zagreb, pp 570-575<br />

6. Ercegovi Raži S (<strong>2010</strong>) Ciljana modikacija svojstava tekstilija primjenom plazme<br />

i metalnih spojeva. PhD Thesis, University <strong>of</strong> Zagreb, Faculty <strong>of</strong> Textile Technology,<br />

Zagreb, Croatia<br />

7. Ercegovi Raži S, unko R (2009) Modikacija svojstava tekstilija primjenom<br />

plazme. Tekstil 58 (3) pp 55-74<br />

8. Ercegovi Raži S, unko R, Svetlii V, Šegota S (<strong>2011</strong>) Application <strong>of</strong> AFM<br />

Microscopy for Identication <strong>of</strong> Fibres Surface Changes after Plasma Treatments.<br />

Materials Technology (accepted for publishing)<br />

9. Ercegovi Raži S, unko R, Bukošek V, Rolich T (210) Hydrophilicity Improvement<br />

<strong>of</strong> Cellulose Based Materials by Plasma. In: Proceedindgs <strong>of</strong> <strong>the</strong> 41th International<br />

Symposium on Novelties in Textiles, Faculty <strong>of</strong> Natural Sciences and Engineering,<br />

University <strong>of</strong> Ljubljana, Ljubljana, pp 344-350<br />

10. Guimond S, Hanselmann B, Amberg M, Hegemann D (<strong>2010</strong>) Plasma processing <strong>of</strong><br />

textiles: Perspectives. Melliand International 16 (4) pp 182-183<br />

11. Hauser P J, El-Shafei A (<strong>2011</strong>) Atmospheric pressure plasma treatments for repellent<br />

textiles. AATCC Review 11 (1) pp 70-74<br />

12. Horrocks AR, Nazaré S, Masood R, Kandola B, Price D (<strong>2011</strong>) Surface modication<br />

<strong>of</strong> fabrics for improved ash-re resistance using atmospheric pressure plasma<br />

in <strong>the</strong> presence <strong>of</strong> a functionalized clay and polysiloxane. Polymers for Advanced<br />

Technologies 22 (1) pp 22-29<br />

13. http://en.wikipedia.org/wiki/File:Plasma-lamp_2.jpg (visited 14.01.<strong>2011</strong>.)<br />

14. http://www.scientec.fr/include/surface/agilent/options/EN-mode_contact_friction.<br />

html (visited 14.01.<strong>2011</strong>.)<br />

15. Ibrahim NA, Hashem MM, Eid MA, Refai R, El-Hossamy M, Eid BM (<strong>2010</strong>) Ec<strong>of</strong>riendly<br />

plasma treatment <strong>of</strong> linen-containing fabrics. Journal <strong>of</strong> <strong>the</strong> textile Institute101<br />

(12) pp 1035-1049<br />

16. ISO 9073-6:200 Textiles – Test methods for nonwovens – Part 6: Absorption (Liquid


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wicking rate)<br />

17. Wei QF (2005) Functinalization <strong>of</strong> textile bres using plasma-based technology.<br />

Technical Textiles int. 2005 International Newsletter pp 27-29<br />

18. Jimenez M, Bellayer S, Duquesne S, Bourbigot S (<strong>2010</strong>) Improvement <strong>of</strong> heat<br />

resistance <strong>of</strong> high performance bers using a cold plasma polymerization process.<br />

Surface and Coatings Technology 205 (3) pp 745-758<br />

19. Marchandalli B, Riccardi C (2007) Plasma treatments <strong>of</strong> bres and textiles. In: Shishoo<br />

R (Ed) Plasma technologies for textiles Woodhead Publishing Ltd, Cambidge, pp 282-<br />

298<br />

20. Mehta R (<strong>2010</strong>) Plasma Treatment in <strong>the</strong> textile industry. Colourage 57 (7) pp 45-48<br />

21. Morent R, De Geyter N, Vershuren J, De Clerck K, Kickenes P, Leys C (2008) Non<strong>the</strong>rmal<br />

plasma treatment <strong>of</strong> textiles. Surface &Coatings Technology 202 pp 3427<br />

-3449<br />

22. Nath K (<strong>2010</strong>) Atmospheric pressure plasma systems in textile application.<br />

International Dyer 195 (9) pp 25-31<br />

23. Severich B (2008) Atmospheric pressure plasma - A new technology for modifying<br />

textile fabrics. Melliand International 14 (2), pp 120-121<br />

24. Shahidi S, Rashidi A, Ghoranneviss M, Anvari A, Wiener J (<strong>2010</strong>) Plasma effects on<br />

anti-felting properties <strong>of</strong> wool fabrics. Surface and Coatings Technology 205 (SUPPL.<br />

1) pp S349-S354<br />

25. TEGEWA Bericht (1987) Tropftest - eine Methode zur schnellen Bestimung der<br />

Saugfähigkeit an textile Flächengebilden Melliand Textilberichte 68 pp 581-583<br />

26. Tseng HJ, Hsu SH, Wu MW, Hsueh TH, Tu PC (2009) Nylon textiles grafted with<br />

chitosan by open air plasma and <strong>the</strong>ir antimicrobial effect. Fibers and Polymers 10<br />

(1) pp 53-59<br />

27. Vesel A (2008) XPS study <strong>of</strong> surface modication <strong>of</strong> different polymer materials by<br />

oxygen plasma treatment. Informacije MIDEM 38 (4) pp 257-265<br />

28. Vesel A, Mozetic M, Strnad S, Peršin Z, Kleinschek S, Hauptman N (2009) Plasma<br />

modication <strong>of</strong> viscose textile. Vacuum 84 (1) pp 79-82


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 213<br />

Importance <strong>of</strong> salt content reduction<br />

in bakery products<br />

Žaneta Ugarčić-Hardi<br />

Josip Juraj Strossmayer University <strong>of</strong> Osijek, Faculty <strong>of</strong> Food Technology<br />

F. Kuhača 20, Osijek<br />

zaneta.ugarcic-hardi@ptfos.hr<br />

Abstract<br />

Studies have shown that <strong>the</strong> excessive intake <strong>of</strong> sodium/salt has a negative effect on health,<br />

primarily on <strong>the</strong> cardiovascular system.The average daily salt intakes <strong>of</strong> <strong>the</strong> European<br />

population are high (10-20 g salt/day) and surpass quantity <strong>of</strong> physiological requirements<br />

(5-6 g salt/day). Therefore, many international and national bodies set an aim to reduce<br />

<strong>the</strong> salt intake in diet. Since <strong>the</strong> average daily salt intake <strong>of</strong> Croatian population is 13-<br />

16g/day, <strong>the</strong> Croatian Academy <strong>of</strong> Medical Science launched national programme for<br />

reducing salt intake. The rst task <strong>of</strong> Croatian programme is to obtain <strong>the</strong> exact data on<br />

salt consumption. It is estimated that 70-75% <strong>of</strong> total salt comes from manufactured foods.<br />

Since <strong>the</strong> salt intake from bread is signicant (~30%), <strong>the</strong> bakery industry is joining <strong>the</strong><br />

national initiative to salt reduction. The aim <strong>of</strong> this paper was to estimate <strong>the</strong> salt content in<br />

23 samples <strong>of</strong> commercial bread and 20 samples <strong>of</strong> different rolls taken from <strong>the</strong> market in<br />

Osijek-Baranja County (East Croatia). The obtained results showed that <strong>the</strong> salt content in<br />

bread varied in <strong>the</strong> range from 0.96 to 2.05%. This share is even higher in products strewed<br />

with salt (2.04 to extremely 4.76).<br />

Key words: salt reduction, bakery product, salt content in bakery product<br />

1 Introduction<br />

Cardiovascular diseases including heart disease and stroke cause more than 50% <strong>of</strong> all<br />

deaths in <strong>the</strong> world. The major risk factors include high blood pressure, high cholesterol<br />

level obesity and smoking (Skupnjak, 2007, Reiner, 2008, Drenjanevi-Peri, <strong>2010</strong>,<br />

EFSA 2005).<br />

High salt consumption can raise blood pressure and lead to cardiovascular diseases. Too<br />

much salt in food carriees also <strong>the</strong> risk <strong>of</strong> kidney disorders, osteoporoses or stomach<br />

cancer. Studies indicate that it is possible to lower blood pressure by cutting sodium/salt<br />

intake in diet. Salt and sodium are currently one <strong>of</strong> <strong>the</strong> top issues for healthy reformulation<br />

efforts by food and beverage manufactures (Heidolph et al, <strong>2011</strong>). On a global basis, <strong>the</strong><br />

population has a dietary intake <strong>of</strong> sodium that exceeds <strong>the</strong> required level. The current daily<br />

dietary guideline for sodium is 2,300 mg/day (5-6g/day salt) (IOM, 2004). This amount<br />

<strong>of</strong> salt intake should be much lower for children depending on age. In most countries <strong>the</strong><br />

average daily sodium consumption has increased to 10-20 g salt (MacGregor, 2008). Males<br />

in general, consume more sodium than females (Dietary Guidelines Advisory Committee,<br />

<strong>2010</strong>). In Croatian population <strong>the</strong> average daily salt intake accounts 13-16 g/day. Average<br />

daily intakes <strong>of</strong> salt are 13.3 ± 4.3 g for men and 10.2 ± 4.2 g for women (Premuži et al,<br />

<strong>2010</strong>, Miškulin et al, <strong>2010</strong>).


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Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

1.1 Salt sources<br />

10% from total daily consumption <strong>of</strong> sodium is coming from natural food that contains salt<br />

in <strong>the</strong>ir origin (meat, sh, eggs, vegetables). 15-20% salt in our daily diet is originates from<br />

cooked food or meal consumption (salt shaker).<br />

70-75% <strong>of</strong> <strong>the</strong> sodium in <strong>the</strong> diet in Europe, 77% in <strong>the</strong> U.S. and 88% in Australia (Heidolph<br />

et al <strong>2011</strong>), comes from processed foods („Hidden salt“), for which <strong>the</strong> consumers have<br />

little control. Salt intake from bread and bakery products, according to some investigations<br />

accounts for 30-35%.<br />

Table1. Share <strong>of</strong> salt intake from food<br />

Products %<br />

Bread and bakery products 34<br />

Meat and meat products 28<br />

Cheese, cream, eggs 10<br />

Fish and sh products 7<br />

Milk and milk products 5<br />

Fruits and products 5<br />

Fat, confectionary, drinks 11<br />

Source: Bundesforschungsanstalt für Getreide–und Kart<strong>of</strong>felverarbeitung (1989)<br />

As <strong>the</strong> cost <strong>of</strong> health care rises, with cardiovascular disease, health experts, health agencies,<br />

and medical societies are looking for ways <strong>of</strong> improving health <strong>of</strong> <strong>the</strong>ir nations. It is<br />

believed that reduction in sodium may help in diminishing health care costs by reducing<br />

<strong>the</strong> risks <strong>of</strong> cardiovascular-related diseases and o<strong>the</strong>r sodium-impacted illnesses, such as<br />

kidney damage, stomach cancer, and osteoporosis. Although <strong>the</strong> direct cause and effect<br />

with regard to high blood pressure and sodium is not clear, <strong>the</strong>re are many international and<br />

national bodies that set an aim to reduce <strong>the</strong> salt intake in diet.<br />

Among <strong>the</strong>m, Consensus Action on Salt and Health – CASH, provides recommendations,<br />

follows developments, looking for consensus among medical pr<strong>of</strong>essionals and <strong>the</strong> public.<br />

The sodium-reduction strategies have been adopted in Finland, <strong>the</strong> United Kingdom,<br />

Ireland, France, <strong>the</strong> European Union, Switzerland, Canada and USA and <strong>the</strong>y emerge<br />

globally (IOM 2004, EFSA 2005).<br />

Finland is <strong>the</strong> only country that has im plemented a sodium-reduction policy that is<br />

considered to be “mandatory“. In 1993, Finland adopted a more aggressive sodiumreduction<br />

strategy which established mandatory labeling requirements for food products.<br />

Currently, <strong>the</strong> most comprehensive such “voluntary” program is being implemented in <strong>the</strong><br />

United Kingdom, and employs a strategy consisting <strong>of</strong>:<br />

a) programs designed to encourage <strong>the</strong> food industry to reformulate products to<br />

reduce sodium levels on a voluntary basis,<br />

b) a public relations campaign aimed at in creasing public awareness concerning <strong>the</strong><br />

relationship between sodium intake and HTN risk and ways to reduce sodium in<br />

take, and<br />

c) “voluntary” front-<strong>of</strong>-package “trafc light” labeling, which employs a colorcoded<br />

signaling system to inform consumers whe<strong>the</strong>r <strong>the</strong> sodium levels in food<br />

are deemed to be “high” (red), “medium” (amber), or “low” (green) by public<br />

health <strong>of</strong>cials (Heidolph et al, <strong>2011</strong>)


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 215<br />

In <strong>the</strong> UK salt intake has already fallen from 9.5 to 8.6 g/day (i.e. 10% reduction) from when<br />

salt reduction rst started in 2004 to <strong>the</strong> end <strong>of</strong> 2006 (MacGregor ,2008).<br />

In 2006 Croatian Action on Salt and Health (CRASH) was established by Croatian Academy<br />

<strong>of</strong> medical Sciences and an alliance <strong>of</strong> societies including Croatian Hypertension Society,<br />

Croatian A<strong>the</strong>rosclerosis Society and Croatian Cardiac Society, launching an initiative to<br />

reduce salt intake in Croatian population and developing a National program for salt intake<br />

reduction ( Reiner, 2008, Jelakovi, 2008).<br />

Croatian Ministry <strong>of</strong> Health and Social Care supports <strong>the</strong>se activities, and CRASH is<br />

included in <strong>the</strong> action <strong>of</strong> <strong>the</strong> World Health Organization on mapping sodium intake in<br />

European countries.<br />

Since <strong>the</strong> salt intake from bread is signicant (~30%), <strong>the</strong> bakery industry is joining <strong>the</strong><br />

national initiative for salt reduction. The bakery manufacturers have been <strong>the</strong> rst that<br />

joined this action gaining information on <strong>the</strong> “Flour-Bread ‘07” Congress in October<br />

2007 (Ugari-Hardi et al, 2007). In order to encourage and educate <strong>the</strong> manufacturers to<br />

produce food and meals with low or reduced salt content, Croatian Food Agency, Faculty<br />

<strong>of</strong> Food Technology in Osijek, Medical Faculty and Croatian National Institute <strong>of</strong> public<br />

Health in Osijek have organized seminars for bakers and public.<br />

The levels <strong>of</strong> salt used in baking are variable and it is very difcult to obtain absolute levels<br />

<strong>of</strong> salt in bread. The rst task <strong>of</strong> <strong>the</strong> Croatian programme is to obtain <strong>the</strong> exact data on salt<br />

consumption in different parts <strong>of</strong> Croatia (Reiner, 2008). Therefore, <strong>the</strong> aim <strong>of</strong> this paper<br />

was to estimate <strong>the</strong> salt content in bakery products in Osijek-Baranja County in Croatia.<br />

2 Why is salt added to bread dough?<br />

Salt content in bakery products varies from country to country from 1 – 2%. In Croatia salt<br />

addition amounts from 2 to 2.5%, (20g/kg our = 13g/kg bread; 5g Na/kg bread).<br />

The primary reason to salt addition is to improve <strong>the</strong> taste. Unsalted bread is tasteless.<br />

Salt has also a signicant technical effect on <strong>the</strong> properties <strong>of</strong> wheat gluten by streng<strong>the</strong>ning<br />

<strong>the</strong> gluten network in dough. It inuences gluten development, <strong>the</strong> rheology <strong>of</strong> dough<br />

and <strong>the</strong> speed <strong>of</strong> fermentation. (Slumier, 2005). Salt increases <strong>the</strong> resistance, extensibility<br />

and elasticity <strong>of</strong> <strong>the</strong> wheat gluten (Hlinka, 1962, He et al, 1992, Fisher et al, 1994.). Salt<br />

decreases <strong>the</strong> amount <strong>of</strong> water required to produce dough <strong>of</strong> xed consistency (Cauvain<br />

and Young, 1998). The investigation conducted by <strong>the</strong> Ger man Research Center for Food<br />

Chemistry and <strong>the</strong> Technical University <strong>of</strong> Munich shows that salt appears to increase<br />

<strong>the</strong> osmotic pressure leading to a reduction in yeast activity and a decrease in <strong>the</strong> crumb<br />

pore size. Salt also increased <strong>the</strong> mixing time and dough resistance. A maximum loaf<br />

volume was achieved at 0.5% salt per 100 g <strong>of</strong> our. Sensory considerations show that salt<br />

affects <strong>the</strong> overall avor pro le <strong>of</strong> wheat bread. Sodium recognition strongly depends on<br />

salt content (Heidolph et al, <strong>2011</strong>).<br />

Although <strong>the</strong> salt addition has an impact on sensory and technological properties,<br />

investigations showed that salt addition in bakery products can be reduced up to 25%<br />

without negative effect on quality (Forschung hilft dem Backgewerbe, 1989).<br />

Currently <strong>the</strong> investigation shows that bread and bread products can be manufactured<br />

satisfactorily at levels <strong>of</strong> 1% salt on a our basis. (Linko et al, 1984, EFSA, 2005).<br />

2.1 Sodium replacement<br />

Replacement <strong>of</strong> sodium chloride is <strong>the</strong> next best method to reduce salt in a prod uct. Cations<br />

similar to sodium such as potassium work best. However, a bitter or metallic <strong>of</strong>f-avor<br />

is <strong>of</strong>ten sensed when potassium chloride is used. O<strong>the</strong>r mineral salts can partially replace


216<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

salt in a cost-effective manner as well, but, <strong>the</strong>y <strong>of</strong>ten deliver <strong>of</strong>f-avors which can limit<br />

<strong>the</strong>ir use. Replacement with NH 3<br />

Cl tastes <strong>of</strong> plant licorice, and replacement with CaCl<br />

has a negative effect on dough rheology. Although articial salt does not exist, <strong>the</strong> most<br />

common strategy is to replace sodium salts by o<strong>the</strong>r inorganic salts such as potassium<br />

chloride. It has been demonstrated that replacing 20% <strong>of</strong> sodium by potassium results in<br />

bread with an accept-able taste, whereas 40% replacement re sults in unacceptable <strong>of</strong>f-taste<br />

(Salovaara, 1982). As a consequence, sodium replacement is limited. With <strong>the</strong> growing<br />

market <strong>of</strong> salt reduced food products, <strong>the</strong>re is also an increasing demand for salt substitutes<br />

or salt taste enhancing agents. In <strong>the</strong> recent years a lot <strong>of</strong> commercial mixtures <strong>of</strong> NaCl and<br />

KCl can be found on <strong>the</strong> market. Such a commercial products are “Pansalt”, “Sub4salt”and<br />

“Sanusol”. They should give 25-50% reduction in sodium.<br />

3 Material and methods<br />

The salt content was estimated in different bakery products taken from <strong>the</strong> market in<br />

“Osijek-Baranja” County, (East Croatia): 23 samples <strong>of</strong> commercial bread and 20 samples<br />

<strong>of</strong> different rolls strewed with salt. Chloride ion was determined by Volhard’s titration.<br />

This method determines <strong>the</strong> salinity <strong>of</strong> foods based on <strong>the</strong> concentration <strong>of</strong> <strong>the</strong> chloride ion<br />

titrated with silver nitrate solution.<br />

The analyses were provided in <strong>the</strong> Croatian National Institute <strong>of</strong> Public Health in Osijek<br />

and <strong>the</strong> Faculty <strong>of</strong> Food Technology in Osijek.<br />

4 Results and discussion<br />

Table 2. Salt content in different bread types<br />

Bread types Salt content (%)<br />

Wheat French bread (White baguette) 1.75<br />

Wheat Easter braided bread 1.41<br />

“Sovital” bread 1.79<br />

Wheat water bread 1.49<br />

“Krunovit” bread 1.57<br />

“Drava vital” bread 1.31<br />

Family bread 1.30<br />

“Monastery sun” bread I 1.90<br />

“Monastery sun” bread II 2.01<br />

“Grandmo<strong>the</strong>r mix” bread 1.01<br />

Bread with onion 0.96<br />

Corn baguette 1.76<br />

White bread with inulin 1.29<br />

Extra white bread 1.52<br />

White ciabatta 1.73<br />

White bread I 1.58<br />

Roll bread 2.02<br />

White bread II 1.58<br />

White bread III 1.03<br />

White bread IV 2.05<br />

Brown bread 1.61<br />

Baguette 1.84<br />

Water bread 1.29<br />

Average 1.56


Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering 217<br />

The obtained results showed that <strong>the</strong> salt content in bread in <strong>the</strong> Osijek-Baranja County<br />

varied in <strong>the</strong> range from 0.96 to 2.05%, (Table 2). The average is 15.6 g /kg bread, which<br />

is higher than <strong>the</strong> average value for salt content in bread in EU. It means that eating only<br />

2 slices <strong>of</strong> bread (100 g), salt intake amounts to 1.56 g. According to some investigations<br />

<strong>the</strong> most frequently consumed type <strong>of</strong> bread is <strong>the</strong> white wheat one (>4 slices), (Pucarin-<br />

Cvetkovi, et al, 2008).<br />

This share <strong>of</strong> salt is even higher in products strewed with salt (from 2.04 to extremely<br />

4.76%, average value 2.84), (Table 3). Consumption <strong>of</strong> 1 roll bread (70 g) gives <strong>the</strong><br />

salt intake amounts <strong>of</strong> 2.09 g, which is 1/3 <strong>of</strong> <strong>the</strong> total recommended daily intake (5-6 g).<br />

Most consumers <strong>of</strong> those products (breakfast rolls) are younger, who get a habit <strong>of</strong> eating<br />

salty food from childhood The investigation <strong>of</strong> <strong>the</strong> diet habits <strong>of</strong> school children in Osijek<br />

has shown that 32.0% <strong>of</strong> school children population has a habit to eat daily some <strong>of</strong> <strong>the</strong><br />

bread products, 28.3% (154/545) girls and 35.9% (191/532) boys. Sample was stratied by<br />

settlements population, size 1077 pupils, 545 girls and 532 boys (Miškulin et al, 2009). The<br />

high salt intake in childhood leads to higher blood pressure and an increased risk <strong>of</strong> stroke<br />

and heart disease in later life.<br />

Table 3. Salt content in rolls strewed with salt<br />

Type <strong>of</strong> bakery products strewed with salt Salt content (%)<br />

Finger stick (Baguette ngers) 4.76<br />

Pretzel 3.04<br />

Salt stick 5.98<br />

Finger stick (Baguette ngers) 2.20<br />

Pretzel 2.41<br />

Salt stick 2.60<br />

Roll (Baguette roll) 2.04<br />

Finger stick (Baguette ngers) 2.08<br />

Pretzel 2.14<br />

Salt stick 2.51<br />

Salt stick 2.28<br />

Pretzel 3.44<br />

Finger stick (Baguette ngers) 2.45<br />

Roll (Baguette roll) 2.40<br />

Pretzel 4.57<br />

Finger stick (Baguette ngers) 2.17<br />

Salt stick 2.53<br />

Roll (Baguette roll) 2.34<br />

Pretzel 2.26<br />

Roll (Baguette roll) 2.71<br />

Average 2.84<br />

Very high salt content was determined in snack products, up to 5%. Average salt content<br />

<strong>of</strong> <strong>the</strong>se products is 2.81%. Eating 100 g (1 package) <strong>of</strong> such products, 1/2 <strong>of</strong> total salt<br />

quantity <strong>of</strong> physiological requirements will be taken, without being conscious <strong>of</strong> that fact<br />

(Ugari-Hardi et al, <strong>2010</strong>). Therefore, it is important to raise consumer awareness abut<br />

<strong>the</strong> association between salt consumption and health in order for people to assume more<br />

responsibility for <strong>the</strong>mselves. One <strong>of</strong> <strong>the</strong> preconditions for this is <strong>the</strong> improved labelling <strong>of</strong><br />

foods with nutrition and health information, including details <strong>of</strong> salt content. Salt labelling


218<br />

Annual <strong>2010</strong>/<strong>2011</strong> <strong>of</strong> <strong>the</strong> Croatian Academy <strong>of</strong> Engineering<br />

should detail <strong>the</strong> salt content per serving with <strong>the</strong> recommended intake per day. Some<br />

products in Croatia are labelling on this way. Fig.1.<br />

Fig.1. Recommended daily intake <strong>of</strong> nutrition’s and percentage <strong>of</strong> each nutrition in product<br />

The bakery and o<strong>the</strong>r food industries are invited to support <strong>the</strong> national action on salt<br />

reducing. The bakery industry is recommended to provide that gradually in two steps. The<br />

rst step should be 10% salt reduction, which means addition <strong>of</strong> 1.8 g salt/100 g our.<br />

In <strong>the</strong> second step <strong>the</strong> reduction should be up to 25% (1.5 g salt/100 g our). 25% salt<br />

reduction would not affect <strong>the</strong> taste and technical properties. This target could be achieved<br />

across <strong>the</strong> next three years.<br />

5 Conclusion<br />

The results on salt content in different bakery products show that reduction on salt amounts<br />

is necessary. The salt content in bread in <strong>the</strong> Osijek-Baranja County varied in <strong>the</strong> range<br />

from 0.96 to 2.05%, and in special products from 2.04 to extremely 4.76%. Although <strong>the</strong><br />

salt addition has an impact on sensory and technological properties, investigation showed<br />

that salt addition in bakery products can be reduced up to 25% without negative effect on<br />

quality.<br />

It may be possible to set an average target <strong>of</strong> salt reduction in bakery products gradually<br />

from 10 to 25% in <strong>the</strong> next three years, with <strong>the</strong> aim <strong>of</strong> getting used <strong>the</strong> food with less salt,<br />

which should contribute to long-term prevention <strong>of</strong> cardiovascular diseases.<br />

Discussions with <strong>the</strong> bakery products industry and <strong>the</strong> government would be needed to<br />

dene a way to achieve <strong>the</strong> reduction in salt level consistent with technological and sensory<br />

needs.<br />

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Podupirajui lanovi:<br />

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Centar za vozila Hrvatske d. d., www.cvh.hr<br />

Elektrotehniki fakultet, Osijek, www.etfos.hr<br />

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Fakultet elektrotehnike i raunarstva, Zagreb, www.fer.unizg.hr<br />

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Graki fakultet, Zagreb, www.grf.hr<br />

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Hrvatska zajednica tehnike kulture, Zagreb , www.hztk.hr<br />

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Odašiljai i veze d.o.o., Zagreb, www.oiv.hr<br />

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