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Universidad Nacional Autónoma de México - CNyN

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1st International Symposium on Nanoscience and Nanomaterials<br />

<strong>de</strong>veloped on the metal pow<strong>de</strong>r. This material was introduced in a suspension of Ca(OH) 2 and was ad<strong>de</strong>d<br />

phosphoric acid in a stoichiometric proportion to growth the hydroxyapatite phase on titanium particles.<br />

Once the reaction was finished we aged the solution, subsequently the pow<strong>de</strong>rs were, washed , filtered and<br />

dried and studied by x ray diffraction pattern we observed two principal features an improvement of the<br />

cristallinity as function of the treatment of the titanium and the small size of the nanocystalline composite<br />

pow<strong>de</strong>r hydroxyapatite – titanium formed. The pow<strong>de</strong>rs obtained were pressed and sintered, the material<br />

showed hardness was in the or<strong>de</strong>r of 450HV200 by x ray technique we observed the <strong>de</strong>velopment of a<br />

vitreous phase in the sintered material. By this methodology we arrived to a nanocomposite pow<strong>de</strong>r whose<br />

characteristics favors its possible use in future studies, it means, by the control of the quantity and<br />

composition of components it is possible to <strong>de</strong>velop functionally gra<strong>de</strong>d materials.<br />

P-019<br />

ELECTRICAL PROPERTIES OF THE MULTIWALL CARBON NANOTUBES BUNDLES IN<br />

GLASS TUBING<br />

U. J. Tamayo-Perez 1a , A. Martínez-Ruíz 1b<br />

1 Facultad <strong>de</strong> Ciencias, <strong>Universidad</strong> Autónoma <strong>de</strong> Baja California, Km. 103 Carretera Tijuana-Ensenada, C.P.<br />

22800, Baja California, México<br />

Keywords: bulk Resistivity MWCNT Density bundles<br />

a uli1234567@gmail.com, b alejandro@uabc.edu.mx<br />

Since the discovery of carbon nanotubes (CNTs) by Iijima[1], have been intensively investigated for<br />

their outstanding physical and chemical properties. There are some technical difficulties of electrical<br />

resistivity measurements on an individual CNT, as well as the results are very sample-<strong>de</strong>pen<strong>de</strong>nt. The<br />

electrical properties and the associated measurement techniques of bulk; bundles, ribbons or ropes of CNTs<br />

provi<strong>de</strong> an alternative approach to study a macroscopic scale of both basic science and applications of CNTs<br />

[2]. In this work, a mass known of MWNTs have been placed into the insulating glass cylin<strong>de</strong>r at room<br />

temperature where it is compacted for metal electro<strong>de</strong>s reducing the volume of the bundle, with advances of<br />

066µm, in each advances the <strong>de</strong>nsity is increases and the resistance <strong>de</strong>creases between two electro<strong>de</strong>s. Un<strong>de</strong>r<br />

the maximum compressive stress of 109 MPa the measurements of bulk of MWNTs as the Ohmic I–V<br />

characteristic. This new methodology not only provi<strong>de</strong>s an effective path to measurement electrical properties<br />

is the way to characterization in spongy regime for potential applications as gas sensors [3-4].<br />

Acknowledgments: This work is partially supported through a stu<strong>de</strong>nt grant from CONACyT. We thank to<br />

Dr. Gerardo Soto H., Dr. José Valenzuela B. and Ing. Israel Gradilla M. from <strong>CNyN</strong>-UNAM for helpful<br />

discussions and assistance with the experiments.<br />

[1]S. Iijima, Nature 354 (1991) 56.<br />

[2] R.Z. Ma, C.L. Xu, B.Q.Wei, J. Liang, D.H.Wu, D.J. Li, Mater. Res. Bull. 34 (1999) 741.<br />

[3] P. Singjai ∗ , S. Changsarn, S. Thongtem, Materials Science and Engineering A 443 (2007) 42–46.<br />

[4] Woo-Sung Cho, Seung-Il Moon, Yang-Doo Lee, IEEE Electron Device Letters, VOL. 26, NO. 7, July 2005.<br />

34

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