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Brian Pilk<strong>in</strong>g<strong>to</strong>n<br />

In situ measurements <strong>of</strong> build<strong>in</strong>g materials us<strong>in</strong>g a <strong>the</strong>rmal probe<br />

Abstract<br />

This work concerns <strong>the</strong> <strong>in</strong> situ measurement <strong>of</strong> <strong>the</strong>rmal conductivity and <strong>the</strong>rmal<br />

diffusivity <strong>of</strong> build<strong>in</strong>g materials, so as <strong>to</strong> provide improved data for <strong>the</strong><br />

estimation and prediction <strong>of</strong> energy efficiency <strong>in</strong> build<strong>in</strong>gs. Thermal data<br />

sources and measurement methods currently used <strong>by</strong> <strong>in</strong>dustry <strong>to</strong> <strong>in</strong>form<br />

build<strong>in</strong>g design were found <strong>to</strong> give flawed values for <strong>the</strong> <strong>the</strong>rmal properties <strong>of</strong><br />

materials as found <strong>in</strong> situ. A transient measurement technique, carried out <strong>by</strong><br />

means <strong>of</strong> a <strong>the</strong>rmal probe, and used <strong>in</strong> various o<strong>the</strong>r <strong>in</strong>dustries, was<br />

<strong>in</strong>vestigated as an alternative, relatively non-destructive, rapid and economic<br />

means <strong>of</strong> obta<strong>in</strong><strong>in</strong>g representative results.<br />

An analysis <strong>of</strong> <strong>the</strong> literature associated with <strong>the</strong> technique's his<strong>to</strong>ry, <strong>the</strong>ory and<br />

practice was carried out. Four strands <strong>of</strong> scientific research were undertaken:<br />

traditional <strong>the</strong>rmal probe solutions were assessed; computer simulations were<br />

used <strong>to</strong> model probe behaviour while avoid<strong>in</strong>g practical, experimental error;<br />

labora<strong>to</strong>ry based measurements were carried out with materials <strong>of</strong> known and<br />

unknown <strong>the</strong>rmal properties us<strong>in</strong>g varied parameters, <strong>in</strong>clud<strong>in</strong>g moisture<br />

content; an apparatus was developed for fieldwork, and <strong>in</strong> situ measurements<br />

were carried out on real build<strong>in</strong>gs, us<strong>in</strong>g novel analysis rout<strong>in</strong>es.<br />

Results for <strong>the</strong>rmal diffusivity values achieved <strong>by</strong> <strong>the</strong> <strong>the</strong>rmal probe method<br />

were found <strong>to</strong> be unreliable. Representative <strong>the</strong>rmal conductivity values were<br />

achieved for structural materials with varied moisture content, both <strong>in</strong> controlled<br />

labora<strong>to</strong>ry environments and <strong>in</strong> situ under diverse environmental conditions,<br />

which had not previously been achieved. Heat losses from <strong>the</strong> probe open end<br />

and <strong>the</strong> material adjacent <strong>to</strong> it were shown <strong>to</strong> currently prevent reliable values<br />

be<strong>in</strong>g obta<strong>in</strong>ed for build<strong>in</strong>g <strong>in</strong>sulation materials.<br />

The <strong>the</strong>rmal probe technique was successfully transferred from labora<strong>to</strong>ry <strong>to</strong> <strong>in</strong><br />

situ measurements. It was shown that various calibration fac<strong>to</strong>rs reported <strong>in</strong> <strong>the</strong><br />

literature could not be relied upon <strong>to</strong> transfer successfully between material<br />

types. A significant cause <strong>of</strong> error <strong>in</strong> <strong>the</strong> measurement <strong>of</strong> <strong>in</strong>sulation materials<br />

was identified and a guarded probe was proposed <strong>to</strong> overcome this. The<br />

technique was shown <strong>to</strong> provide much improved <strong>the</strong>rmal conductivity data for<br />

structural build<strong>in</strong>g materials, whe<strong>the</strong>r as samples or <strong>in</strong> situ, with <strong>the</strong> potential <strong>to</strong><br />

expand this success <strong>to</strong> <strong>in</strong>sulation materials <strong>in</strong> <strong>the</strong> future.<br />

V

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