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UV and IR spectra andtheir simple applications.(3) Atomic structure and chemicalBonding :Sommerfelds model, Schrodinger equation(General treatment) Elementry idea of valencybond and Molecular orbital theory (bonding , nonbondingand antibonding orbitals) diplole momentand Molecular structure.(4) Electro Chemistry.Reversible and irreversible electrodes,Nernst equation, Standard hydrogen electrodeand glass electrode, concentration cells with andwithout transference, condutivity of solution(specific, , equipment and molecular conductance),ionic velocity and effect of dilution onconductance, conductometric titrations, Degreeof ionisation and conductivity concept of transportnumber and its determination, Kohlrausch's lawof ionic mobility and its applications. Elementaryidea of theory of strong electrolytes.(5) Thermodynamics :Extensive and intensive properties, isolatedsystem. Intrinsic energy, and enthalpy asproperties of states, Reversible , irreversible andcyclic processes and drive towards equillibrium,Second law of the thermodynamics with referenceto entropy, physical concept of entropy, simpleapplications of thermodyanmics to chemicalprocesses.(6) Nuclear Chemistry :Theory of atomic nucleus and nuclearstability in terms of N/P ratio, binding enegry,packing fraction, mass defect, whole number rule,Effective nuclear charge, atomic disintegration,nuclear section, nuclear cross-section, basicprinciples of nuclear fission and fusion.(7) Chemistry of elements and theircompounds:A comparative study of XIV, XV, XVI,XVII and zero group elements with respect toelectronic configuration,oxidation states ,hydrides, oxides , halides and hydroxides.(8) Transition and inner transitionelements :Electronic configuration, position in theperiodic table, characteristics, oxidation states.spectral and magnetic properties of transitionelements.General study, electronic structure,oxidation states, spectral and magnetic propertiesof lanthanides, lanthanide contraction.(9) Co-ordination Chemistry :Werner's theory of co-ordinationcompounds, its electronic interpretation valencybond theory for explaining metalling and bonding,hybridisation in complexes.(10) Non-aqueous solvents :Classification and characteristics ofsolvents Chemistry of non-aqueous solvents withspecial reference to liquid ammonia and liquidsulphur dioxide.(11) Inorganic Compounds :(i) A detailed study of oxides. oxyacids(including electronic structure ) of nitrogen,phosphorus, and sulphur. Peroxoacids of sulphur.Øe'k%
Oxyacids of chlorinc, thionic acids. Isolation offlourine. Inert gas compounds, interhalogen compoundsand pseudo halogens.(ii) Preparation, properties, uses and theconstitution of the following :- diborane ,hydrazine, hydroxylamine, hyponitrous acid,sodium thiosulphate and hydrogen peroxide.(iii) A detailed study of active nitrogen,nitrides and fertilisers.(iv) Preparation, properties and uses of thefollowing-Hydrazoic acid Tartaremetic, Microcosmicsalt, thionylchloride sulphuryl chloride,potassiumdichromate, Potassium permagnate , ChromalumBleaching powder, Potassium Ferro andferricyanide, chlorosulphonic acid , sodiumbismuthate, sodium cobaltinitrite andcorborundum.PAPER - IIPhysical Organic ChemistryElectronic displacements Inductive,elecromeric, mesomeric and hyper conjugativeeffects, Electronphiles, nucleophiles and freeradicals. Resonance and its applications to organiccompounds, Effect of structure on the dissociationconstants of organic acids and bases.Hydrogen bond and its effects on the propertiesof organic compounds.Modern concepts of reaction mechanismsaddition,substitution, elimination andrearrangement. Reaction involving free radicalmechanisms of aromatic substitution Benzeneintermediates.Aliphatic ChemistryChemistry of simple organic compoundsbelonging to the following classes alkanes, alkenes,alkynes, alkyl halides; alcohols, thiols, aldehydes,ketones, acids and their derivatives, ethers, amines,amino acids, hydroxy acids, unsaturated acids,Dibasic Acids.Synthetic uses of the following :-Acetoacetic and malonic estars,organometallic compounds of magnesium andlithium, and diazomethane.Carbohydrates - Classification,configuration and general reactions of simplemonosaccharides. Chemistry of glucose, fructoseand sucrose.StereochemistryElements of symmetry and simple symmetryoperations. Optical and geometrical isomerism insimple organic molecules. E.Z. and R.S. notationsConformations of simple organic molecules,Stereochemistry of inorganic co-ordinationcompounds.Aromatic ChemistryBenzene, toluene and their halogen,hydroxy, nitro and amino derivatives, Sulphonic(9)acid, Xylenes, Benzaldehyde. Salicylaldehyde,acetophenone,Benzoic, phthalic, sallcylic,cinnamic and mandelic acids.Reduction productsof nitrobenzene, Benzonium salts and their syntheticuses.Structure, synthesis and important reactionsof napthalene, anthracene, phenanthrene, pyridineand quinoline.Dyes belonging to the azo triphenylmethaneand phthalein groups, Modern theories of colourand constitution.General ideas regarding the Chemistry ofnicotine.Basic concepts regarding the followingmaterials of economic and medicinal importance,Cellulose and starch, coaltar chemicals, oils andfats.Chemistry of the following elements andtheir principal compounds Boron, titanium,germanium, Silicon.Nickel, Platinum, Chromiumand Uranium.Elementary idea of Hydrogen bondingVSEPR theory and importance of lone pairstructure of ionic solids, energetics of formationof NaCl. Crystal lattice with-reference toionisation potential, electron , affinity, and latticeenergy. Born Haber cycle. Polarising power.Polorisability Fajan's rules.Acid-Base concept, Lowry Bronstedconcept, Lewis concept, Other theories of acidand bases, Hard and soft Acid base concept,pH and its determination, Buffer solution andBuffer action, Henderson equation.Errors in quantitative analysis, classificationof errors, minimisation of errors, precision andaccuracy, significance of figures, Co-precipitationand post precipitation, optimum conditions forprecipitations,choice of indicators in the acid basetitrations, theories of indicators, Principle of EDTAtitrations.Analytical, Numerical questions on (a)Quantitative estimation of pyrolusite, iodometry,silver coin, acid-base. titrations, Redox-titrations(b) Aliphatic and Aromatic compounds.05-flfoy bathfu;jhbathfu;jh fo"k;ksa ds iz'u i= dsoy vaxzsthesa gksaxsaA vr,o ikB~;Øe dsoy vaxzsth esa gh eqfnzrgS A¼ifjf'k"V ,d&iSjk 4 ¼?k½ ns[ksa ½05 CIVIL ENGINEERINGPAPER - I(A) Structural Analysis :Principles of superposition : reciprocalTheorem unsymmetrical bending.Determinate and indeterminate structures :simple and space frames; degrees of freedom;virtual work; energy theorem, deflection of trusses;redundant frames, three moment equation slopedeflection, moment distribution and kani'smethods; column anology. Energy methods;approximate and numerical methods;Approximate methods. of analysis of rigid frames.Moving loads- Shearing force and Bendingmoment diagrams in fluence line for simple andcontinuous beams and frames;Analysis of determinate and indeterminatearches; spandrel braced arch .Matrix methods of analysis; stiffiness andflexibility matrices. Elements of plastic analysis.(B) Structural Design :(i) Steel Design - Factors of safety andload factors; Design of tension, compression andflexural members; built up beams and plate girders, semi-rigid and rigid connections.Design of stanchions,slab and gussestedbases; gentry girders; roof trusses; industrial andmulti storeyed building; water tanks and towers.Plastic design of continuous frames andportals.(ii) R.C.C. Design- Working stress andlimit state methods of Design of slabs, rectangular, T & L beams simply supported and continuous;column & footings isolated and combined, raftfoundations over -head & under ground watertanks, encased beams and columns.Methods and systems of prestressing;anchorages, losses in prestress; Design ofprestressed beams.(C) Construction , Planning andManagementBuilding estimates and specifications.valuation, contract conditions and agreement,construction scheduling, CPM and PERTmethods.(D) Environmental EngineeringWater quality criteria for various uses e.g.domestic & irrigational . Transmission of water.Unit processes and operations for water treatment-sedimentation, coagulation & floculation,filteration, slow & rapid sand, decao media filters,disinfection sofeting, removal of taste, odour andsalanity.Quantity and characteristic of domesticwaste water sewerage system and sewage pumps,unit processes and operation for domestic wastewater treatment-grit chambers primarysedimentation, biological waste treatment e.g. activatedsludge trickling filters followed bysecondary sedimentation, waste stabilizationponds, sludge treatment byanaerobic digestionand its disposal , waste water disposal and selfpurification of streams septic tanks.Elements of air pollution, primary pollutants& their effects.Rural sanitation, environmental pollution andecologyØe'k%
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