CLAN LAB METHODS

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THIONYL CHLORIDE METHOD- HAZARDSONLY108• PSEUDOEPHEDRINE ISPRECURSOR• THIONYL CHLORIDE WITHCHLOROFORM• NICKNAMED…– “HYDROGENATION” METHOD– “SHAKE-N-BAKE”• REACTIVE CATALYSTS– RANEY NICKEL– PALLADIUM BLACK
109THIONYL HAZARDS• THIONYL CHLORIDE– WATER REACTIVE- FORMSHYDROCHLORIC AND SULFURICACIDS• HYDROGEN GAS–PRESSURE– FLAMMABLE• CATALYST– WATER REACTIVE• CHLOROFORM– SUSPECTED CARCINOGEN
Page 1 and 2:
1CLAN LAB METHODS…COOKING WITH CH
Page 3 and 4:
3METHODS WE’LL COVER• METHAMPHE
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RED P METHOD5
Page 7 and 8:
7RED P METHODRed phosphorus can bep
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9RED P METHODStriker plates are usu
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11STEP 1 - TABLET EXTRACTION• GRI
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13TABLET EXTRACTIONCoffee grinders
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15TABLET EXTRACTION• EXTRACT-EPHE
Page 17 and 18:
17TABLET EXTRACTION-SOLVENTS• ALC
Page 19 and 20:
19TABLET EXTRACTIONDenatured alcoho
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21TABLET EXTRACTION-SOLVENTSLarge-s
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23TABLET EXTRACTION-SOLVENTSHot pla
Page 25 and 26:
25TABLET EXTRACTION-SOLVENTSMexican
Page 27 and 28:
27TABLET EXTRACTION-WATER•WATER C
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TABLET EXTRACTION-WATERFilter out B
Page 31 and 32:
31STEP 2 - COOKING• COMBINE- PSEU
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Page 37 and 38:
37STEP 2 - COOKING• COMBINE- PHOS
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39COOKINGRed phosphorus usuallywill
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COOKING41
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43SUBSTITUTIONSIodine can be purcha
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45SUBSTITUTIONSHousehold Iodine tin
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47SUBSTITUTIONSHydrogenperoxide ism
Page 49 and 50:
49AFTER REFLUX TO SEPARATETHE REACT
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ALTERNATE METHOD TO SEPARATEREACTIO
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53SEPARATIONSodium hydroxide(lye) i
Page 55 and 56:
55STEP 3 - SEPARATION• RAISE pH >
Page 57 and 58: 57SEPARATIONWhite gas (camp fuel) i
Page 59 and 60: 59METH SOLUBILITYMETH BASE METH HCL
Page 61 and 62: 61SEPARATE LAYERS• POUR THELIQUID
Page 63 and 64: 63STEP 4 - SALTING OUT• BUBBLE HY
Page 65 and 66: 65STEP 4 - SALTING OUT• Separate
Page 67 and 68: 67SALTING OUTHCL acid gas generator
Page 69 and 70: 69SALTING OUTThe tip of the tubing
Page 71 and 72: 71METHODS FOR SALTING OUT• SULFUR
Page 73 and 74: 73METHODS FOR SALTING OUTRock salt(
Page 75 and 76: 75ALTERNATE RED P METHODS• SPORTS
Page 77 and 78: 77ALTERNATE RED P METHOD• PRESSUR
Page 79 and 80: 79ANHYDROUS AMMONIAANHYDROUSMEANSWI
Page 81 and 82: 81AMMONIA SOURCESAmmonia is often p
Page 83 and 84: 83AMMONIA SOURCESAnhydrous ammonia
Page 85 and 86: AMMONIA SOURCESLye can be mixed wit
Page 87 and 88: 87LITHIUM & SODIUM• HIGHLY WATER
Page 89 and 90: 89LITHIUM & SODIUMStripped lithium
Page 91 and 92: 91SODIUM FROM LYE/DRANONaOH-+Na+ -O
Page 93 and 94: SODIUM FROM LYE/DRANO93
Page 95 and 96: 95STEP 1 - TABLETEXTRACTION• SAME
Page 97 and 98: 97STEP 2 - REACTION• TO A CONTAIN
Page 99 and 100: 99REACTION CONTINUED...• ALLOW AM
Page 101 and 102: 101REACTION CONTINUED...• ALLOW A
Page 103 and 104: 103STEP 3 - SEPARATION• ADD ORGAN
Page 105 and 106: 105STEP 4 - SALTING OUT• BUBBLEHY
Page 107: 107SALTING OUTEpsom salt (magnesium
Page 111 and 112: 111HOMEMADEHYDROGENATOR
Page 113 and 114: 113HOMEMADEHYDROGENATOR
Page 115 and 116: 115PHENYL-2-PROPANONEMETHOD• PHEN
Page 117 and 118: 117P-2-P REACTION• REACTION ISSLI
Page 119 and 120: 119STEP 2 - SEPARATION• OIL LAYER
Page 121 and 122: 121HAZARD COMPARISONMETHOD• REDPH
Page 123 and 124: 123Begin with Safrole• Sassafras
Page 125 and 126: 125Components of Sassafras OilCompo
Page 127 and 128: 127Safrole to Isosafrole• Combine
Page 129 and 130: 129MDP-2-P Production Cont.5. Disti
Page 131 and 132: 131STEP ONE - REACTION• COMBINE T
Page 133 and 134: 133STEP 3 - SALTING OUT• BUBBLE H
Page 135 and 136: 135GHB MANUFACTURINGButyrolactone i
Page 137 and 138: 137GHB ALTERNATIVES• USERS DISCOV
Page 139 and 140: GHB ALTERNATIVES139
Page 141: 141CLAN LAB METHODS…WHAT WILL THE
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CLAN LAB METHODS

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