CLAN LAB METHODS

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42SUBSTITUTIONS• RED PHOSPHORUS...– WHITE PHOSPHORUS– HYPOPHOSPHORUS ACID• IODINE...– TINCTURE OF IODINE– HYDRIODIC ACID (IF AVAI<strong>LAB</strong>LE)
43SUBSTITUTIONSIodine can be purchasedin prill (small beads),flakes and BB size shot.
Page 1 and 2: 1CLAN LAB METHODS…COOKING WITH CH
Page 3 and 4: 3METHODS WE’LL COVER• METHAMPHE
Page 5 and 6: RED P METHOD5
Page 7 and 8: 7RED P METHODRed phosphorus can bep
Page 9 and 10: 9RED P METHODStriker plates are usu
Page 11 and 12: 11STEP 1 - TABLET EXTRACTION• GRI
Page 13 and 14: 13TABLET EXTRACTIONCoffee grinders
Page 15 and 16: 15TABLET EXTRACTION• EXTRACT-EPHE
Page 17 and 18: 17TABLET EXTRACTION-SOLVENTS• ALC
Page 19 and 20: 19TABLET EXTRACTIONDenatured alcoho
Page 21 and 22: 21TABLET EXTRACTION-SOLVENTSLarge-s
Page 23 and 24: 23TABLET EXTRACTION-SOLVENTSHot pla
Page 25 and 26: 25TABLET EXTRACTION-SOLVENTSMexican
Page 27 and 28: 27TABLET EXTRACTION-WATER•WATER C
Page 29 and 30: TABLET EXTRACTION-WATERFilter out B
Page 31 and 32: 31STEP 2 - COOKING• COMBINE- PSEU
Page 37 and 38: 37STEP 2 - COOKING• COMBINE- PHOS
Page 39 and 40: 39COOKINGRed phosphorus usuallywill
Page 41: COOKING41
Page 45 and 46: 45SUBSTITUTIONSHousehold Iodine tin
Page 47 and 48: 47SUBSTITUTIONSHydrogenperoxide ism
Page 49 and 50: 49AFTER REFLUX TO SEPARATETHE REACT
Page 51 and 52: ALTERNATE METHOD TO SEPARATEREACTIO
Page 53 and 54: 53SEPARATIONSodium hydroxide(lye) i
Page 55 and 56: 55STEP 3 - SEPARATION• RAISE pH >
Page 57 and 58: 57SEPARATIONWhite gas (camp fuel) i
Page 59 and 60: 59METH SOLUBILITYMETH BASE METH HCL
Page 61 and 62: 61SEPARATE LAYERS• POUR THELIQUID
Page 63 and 64: 63STEP 4 - SALTING OUT• BUBBLE HY
Page 65 and 66: 65STEP 4 - SALTING OUT• Separate
Page 67 and 68: 67SALTING OUTHCL acid gas generator
Page 69 and 70: 69SALTING OUTThe tip of the tubing
Page 71 and 72: 71METHODS FOR SALTING OUT• SULFUR
Page 73 and 74: 73METHODS FOR SALTING OUTRock salt(
Page 75 and 76: 75ALTERNATE RED P METHODS• SPORTS
Page 77 and 78: 77ALTERNATE RED P METHOD• PRESSUR
Page 79 and 80: 79ANHYDROUS AMMONIAANHYDROUSMEANSWI
Page 81 and 82: 81AMMONIA SOURCESAmmonia is often p
Page 83 and 84: 83AMMONIA SOURCESAnhydrous ammonia
Page 85 and 86: AMMONIA SOURCESLye can be mixed wit
Page 87 and 88: 87LITHIUM & SODIUM• HIGHLY WATER
Page 89 and 90: 89LITHIUM & SODIUMStripped lithium
Page 91 and 92: 91SODIUM FROM LYE/DRANONaOH-+Na+ -O
Page 93 and 94:
SODIUM FROM LYE/DRANO93
Page 95 and 96:
95STEP 1 - TABLETEXTRACTION• SAME
Page 97 and 98:
97STEP 2 - REACTION• TO A CONTAIN
Page 99 and 100:
99REACTION CONTINUED...• ALLOW AM
Page 101 and 102:
101REACTION CONTINUED...• ALLOW A
Page 103 and 104:
103STEP 3 - SEPARATION• ADD ORGAN
Page 105 and 106:
105STEP 4 - SALTING OUT• BUBBLEHY
Page 107 and 108:
107SALTING OUTEpsom salt (magnesium
Page 109 and 110:
109THIONYL HAZARDS• THIONYL CHLOR
Page 111 and 112:
111HOMEMADEHYDROGENATOR
Page 113 and 114:
113HOMEMADEHYDROGENATOR
Page 115 and 116:
115PHENYL-2-PROPANONEMETHOD• PHEN
Page 117 and 118:
117P-2-P REACTION• REACTION ISSLI
Page 119 and 120:
119STEP 2 - SEPARATION• OIL LAYER
Page 121 and 122:
121HAZARD COMPARISONMETHOD• REDPH
Page 123 and 124:
123Begin with Safrole• Sassafras
Page 125 and 126:
125Components of Sassafras OilCompo
Page 127 and 128:
127Safrole to Isosafrole• Combine
Page 129 and 130:
129MDP-2-P Production Cont.5. Disti
Page 131 and 132:
131STEP ONE - REACTION• COMBINE T
Page 133 and 134:
133STEP 3 - SALTING OUT• BUBBLE H
Page 135 and 136:
135GHB MANUFACTURINGButyrolactone i
Page 137 and 138:
137GHB ALTERNATIVES• USERS DISCOV
Page 139 and 140:
GHB ALTERNATIVES139
Page 141:
141CLAN LAB METHODS…WHAT WILL THE
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CLAN LAB METHODS

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