CLAN LAB METHODS

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126Separate Safrole Oil• Easiest method:1. Wash sassafras oil with 28% aceticacid to removed eugenol, pinene, andcamphor oils.2. Wash remaining oil with water toremove other contaminants.3. Wash oil with denatured alcohol todissolve safrole (leaving phelladrenebehind).4. Heat denatured alcohol until alcoholhas evaporated leaving safrole behind.
127Safrole to Isosafrole• Combine– Safrole oil– Sodium or potassium hydroxide– Denatured alcohol– Reflux at 120 – 140 °C for 12 – 24 hours– Dark colored mixture is isosafrole
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1CLAN LAB METHODS…COOKING WITH CH
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3METHODS WE’LL COVER• METHAMPHE
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RED P METHOD5
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7RED P METHODRed phosphorus can bep
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9RED P METHODStriker plates are usu
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11STEP 1 - TABLET EXTRACTION• GRI
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13TABLET EXTRACTIONCoffee grinders
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15TABLET EXTRACTION• EXTRACT-EPHE
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17TABLET EXTRACTION-SOLVENTS• ALC
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19TABLET EXTRACTIONDenatured alcoho
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21TABLET EXTRACTION-SOLVENTSLarge-s
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23TABLET EXTRACTION-SOLVENTSHot pla
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25TABLET EXTRACTION-SOLVENTSMexican
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27TABLET EXTRACTION-WATER•WATER C
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TABLET EXTRACTION-WATERFilter out B
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31STEP 2 - COOKING• COMBINE- PSEU
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37STEP 2 - COOKING• COMBINE- PHOS
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39COOKINGRed phosphorus usuallywill
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COOKING41
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43SUBSTITUTIONSIodine can be purcha
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45SUBSTITUTIONSHousehold Iodine tin
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47SUBSTITUTIONSHydrogenperoxide ism
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49AFTER REFLUX TO SEPARATETHE REACT
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ALTERNATE METHOD TO SEPARATEREACTIO
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53SEPARATIONSodium hydroxide(lye) i
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55STEP 3 - SEPARATION• RAISE pH >
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57SEPARATIONWhite gas (camp fuel) i
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59METH SOLUBILITYMETH BASE METH HCL
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61SEPARATE LAYERS• POUR THELIQUID
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63STEP 4 - SALTING OUT• BUBBLE HY
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65STEP 4 - SALTING OUT• Separate
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67SALTING OUTHCL acid gas generator
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69SALTING OUTThe tip of the tubing
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71METHODS FOR SALTING OUT• SULFUR
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73METHODS FOR SALTING OUTRock salt(
Page 75 and 76: 75ALTERNATE RED P METHODS• SPORTS
Page 77 and 78: 77ALTERNATE RED P METHOD• PRESSUR
Page 79 and 80: 79ANHYDROUS AMMONIAANHYDROUSMEANSWI
Page 81 and 82: 81AMMONIA SOURCESAmmonia is often p
Page 83 and 84: 83AMMONIA SOURCESAnhydrous ammonia
Page 85 and 86: AMMONIA SOURCESLye can be mixed wit
Page 87 and 88: 87LITHIUM & SODIUM• HIGHLY WATER
Page 89 and 90: 89LITHIUM & SODIUMStripped lithium
Page 91 and 92: 91SODIUM FROM LYE/DRANONaOH-+Na+ -O
Page 93 and 94: SODIUM FROM LYE/DRANO93
Page 95 and 96: 95STEP 1 - TABLETEXTRACTION• SAME
Page 97 and 98: 97STEP 2 - REACTION• TO A CONTAIN
Page 99 and 100: 99REACTION CONTINUED...• ALLOW AM
Page 101 and 102: 101REACTION CONTINUED...• ALLOW A
Page 103 and 104: 103STEP 3 - SEPARATION• ADD ORGAN
Page 105 and 106: 105STEP 4 - SALTING OUT• BUBBLEHY
Page 107 and 108: 107SALTING OUTEpsom salt (magnesium
Page 109 and 110: 109THIONYL HAZARDS• THIONYL CHLOR
Page 111 and 112: 111HOMEMADEHYDROGENATOR
Page 113 and 114: 113HOMEMADEHYDROGENATOR
Page 115 and 116: 115PHENYL-2-PROPANONEMETHOD• PHEN
Page 117 and 118: 117P-2-P REACTION• REACTION ISSLI
Page 119 and 120: 119STEP 2 - SEPARATION• OIL LAYER
Page 121 and 122: 121HAZARD COMPARISONMETHOD• REDPH
Page 123 and 124: 123Begin with Safrole• Sassafras
Page 125: 125Components of Sassafras OilCompo
Page 129 and 130: 129MDP-2-P Production Cont.5. Disti
Page 131 and 132: 131STEP ONE - REACTION• COMBINE T
Page 133 and 134: 133STEP 3 - SALTING OUT• BUBBLE H
Page 135 and 136: 135GHB MANUFACTURINGButyrolactone i
Page 137 and 138: 137GHB ALTERNATIVES• USERS DISCOV
Page 139 and 140: GHB ALTERNATIVES139
Page 141: 141CLAN LAB METHODS…WHAT WILL THE
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CLAN LAB METHODS

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