CLAN LAB METHODS

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50TO SEPARATE REACTIONFunnels and filter paper istypically used to separatethe red phosphorus afterthe reflux, from the water(acid) phase.
ALTERNATE METHOD TO SEPARATEREACTION51• Large labs have been known touse bed sheets and buckets.
Page 1 and 2: 1CLAN LAB METHODS…COOKING WITH CH
Page 3 and 4: 3METHODS WE’LL COVER• METHAMPHE
Page 5 and 6: RED P METHOD5
Page 7 and 8: 7RED P METHODRed phosphorus can bep
Page 9 and 10: 9RED P METHODStriker plates are usu
Page 11 and 12: 11STEP 1 - TABLET EXTRACTION• GRI
Page 13 and 14: 13TABLET EXTRACTIONCoffee grinders
Page 15 and 16: 15TABLET EXTRACTION• EXTRACT-EPHE
Page 17 and 18: 17TABLET EXTRACTION-SOLVENTS• ALC
Page 19 and 20: 19TABLET EXTRACTIONDenatured alcoho
Page 21 and 22: 21TABLET EXTRACTION-SOLVENTSLarge-s
Page 23 and 24: 23TABLET EXTRACTION-SOLVENTSHot pla
Page 25 and 26: 25TABLET EXTRACTION-SOLVENTSMexican
Page 27 and 28: 27TABLET EXTRACTION-WATER•WATER C
Page 29 and 30: TABLET EXTRACTION-WATERFilter out B
Page 31 and 32: 31STEP 2 - COOKING• COMBINE- PSEU
Page 37 and 38: 37STEP 2 - COOKING• COMBINE- PHOS
Page 39 and 40: 39COOKINGRed phosphorus usuallywill
Page 41 and 42: COOKING41
Page 43 and 44: 43SUBSTITUTIONSIodine can be purcha
Page 45 and 46: 45SUBSTITUTIONSHousehold Iodine tin
Page 47 and 48: 47SUBSTITUTIONSHydrogenperoxide ism
Page 49: 49AFTER REFLUX TO SEPARATETHE REACT
Page 53 and 54: 53SEPARATIONSodium hydroxide(lye) i
Page 55 and 56: 55STEP 3 - SEPARATION• RAISE pH >
Page 57 and 58: 57SEPARATIONWhite gas (camp fuel) i
Page 59 and 60: 59METH SOLUBILITYMETH BASE METH HCL
Page 61 and 62: 61SEPARATE LAYERS• POUR THELIQUID
Page 63 and 64: 63STEP 4 - SALTING OUT• BUBBLE HY
Page 65 and 66: 65STEP 4 - SALTING OUT• Separate
Page 67 and 68: 67SALTING OUTHCL acid gas generator
Page 69 and 70: 69SALTING OUTThe tip of the tubing
Page 71 and 72: 71METHODS FOR SALTING OUT• SULFUR
Page 73 and 74: 73METHODS FOR SALTING OUTRock salt(
Page 75 and 76: 75ALTERNATE RED P METHODS• SPORTS
Page 77 and 78: 77ALTERNATE RED P METHOD• PRESSUR
Page 79 and 80: 79ANHYDROUS AMMONIAANHYDROUSMEANSWI
Page 81 and 82: 81AMMONIA SOURCESAmmonia is often p
Page 83 and 84: 83AMMONIA SOURCESAnhydrous ammonia
Page 85 and 86: AMMONIA SOURCESLye can be mixed wit
Page 87 and 88: 87LITHIUM & SODIUM• HIGHLY WATER
Page 89 and 90: 89LITHIUM & SODIUMStripped lithium
Page 91 and 92: 91SODIUM FROM LYE/DRANONaOH-+Na+ -O
Page 93 and 94: SODIUM FROM LYE/DRANO93
Page 95 and 96: 95STEP 1 - TABLETEXTRACTION• SAME
Page 97 and 98: 97STEP 2 - REACTION• TO A CONTAIN
Page 99 and 100: 99REACTION CONTINUED...• ALLOW AM
Page 101 and 102:
101REACTION CONTINUED...• ALLOW A
Page 103 and 104:
103STEP 3 - SEPARATION• ADD ORGAN
Page 105 and 106:
105STEP 4 - SALTING OUT• BUBBLEHY
Page 107 and 108:
107SALTING OUTEpsom salt (magnesium
Page 109 and 110:
109THIONYL HAZARDS• THIONYL CHLOR
Page 111 and 112:
111HOMEMADEHYDROGENATOR
Page 113 and 114:
113HOMEMADEHYDROGENATOR
Page 115 and 116:
115PHENYL-2-PROPANONEMETHOD• PHEN
Page 117 and 118:
117P-2-P REACTION• REACTION ISSLI
Page 119 and 120:
119STEP 2 - SEPARATION• OIL LAYER
Page 121 and 122:
121HAZARD COMPARISONMETHOD• REDPH
Page 123 and 124:
123Begin with Safrole• Sassafras
Page 125 and 126:
125Components of Sassafras OilCompo
Page 127 and 128:
127Safrole to Isosafrole• Combine
Page 129 and 130:
129MDP-2-P Production Cont.5. Disti
Page 131 and 132:
131STEP ONE - REACTION• COMBINE T
Page 133 and 134:
133STEP 3 - SALTING OUT• BUBBLE H
Page 135 and 136:
135GHB MANUFACTURINGButyrolactone i
Page 137 and 138:
137GHB ALTERNATIVES• USERS DISCOV
Page 139 and 140:
GHB ALTERNATIVES139
Page 141:
141CLAN LAB METHODS…WHAT WILL THE
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CLAN LAB METHODS

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