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Chemistry 360 - Athabasca University

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CHEM<strong>360</strong> 2012-14 Exp.14Unknown # <strong>360</strong>-14-7Mol. Wt. = 121.18 g/mol Chemical Formula = C 8 H 11 N Degrees of Unsaturation = ___________________________________b.p. = 210CIR Spectra (liquid film (neat) on KBr Disc)1 H-NMR Spectra (at 90 MHz 10.5 mol% in CDCl 3 )Infrared Spectra (liquid film (neat) on KBr disc):Spectrum Absorp'n Frequency Peak ShapeRegion Band # (cm -1 ) (sharp, broad)Peak Intensity(strong, med.or weak)Functional GroupIndicated1 H-NMR Integration Data: (at 90 MHz 10.5 mol% in CDCl 3 )Signal#Shift Integrat'n Splitting Comment #NeighbouringH1 1.2 3HSignalAssignment2 2.46 2H3 3.47 2H xchangeswith D 2 O4 6.65 2H5 7.0 2HStructure Assigned to Unknown <strong>360</strong>-14-7Compound Name:

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