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CHEM<strong>360</strong> Report Book 2012-14Exp.10Procedure: (Reference: use proper format. Any Changes/Modifications?)Procedure for the Fisher esterification of acetic acid with isoamyl alcohol.Procedural StepObservations/Comments/InferencesRecord amounts of reagents used.Table 10.1 Table of Reagents for Experiment 10 Fisher Esterification.Reagent Formula Mwt.(g/mol)Acetic acid, glacial (conc.)17.4 MIsoamyl alcohol(3-methyl -1-butanol)Sulfuric acid, conc.18 Md(g/ml)Mp*(C)Bp*(C)(CH 3 ) 2 CH(CH 2 ) 2 OH 88.15 130 IrritantH 2 SO 4 1.840Distilled water H 2 O 18.02 1.000 0 100 noneDiethyl etherHaz. Properties5% sodium carbonate (aq) Na 2 CO 3 (aq)Sat. sodium chloride (aq)(brine)Calcium chloride (anhydr) CaCl 2acetone, washNaCl (aq)Isoamyl acetate CH 3 CO 2 C 5 H 11 130.19 142*find and record either the melting point if the reagent is a solid at room temperature, or the boiling point if the reagent is a liquidat room temperature.9
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