Chemistry 360 - Athabasca University

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$Experimental Design - Math Site$

CHEM<strong>360</strong> Report Book 2012-14Exp.16Procedure: (cont.)Table 16.1. Table of Reagents for Experiment 16.Reagent Formula Mwt. d mp bp Haz. PropertiesBromobenzeneC 6 H 5 BrMagnesium 24.31 1.75 649 1090Ethyl benzoate C 6 H 5 CO 2 C 2 H 5Diethyl ether C 2 H 5 OC 2 H 5 74.12 0.7138 -116 34.5Sulfuric acid, 2M 98.07Sodium H carbonate 84.01 2.159 270Sodium sulfate, anhyd 142.04 2.68Dichloromethane 84.93 1.325 -95.1 40.1Biphenyl (C 6 H 5 ) 2 154.21 0.992 71 255.9Ligroin(high bp pet. ether)0.656 60-80alkane mixt.Iodine 253.8 4.930 133Methanol CH 3 OH 32.04 0.7914 -94 65Ethanol C 2 H 5 OH 46.07 0.7893 -117 78.5Triphenylmethanol(C 6 H 5 ) 3 COH67
CHEM<strong>360</strong> Report Book 2012-14Exp.16SAMPLE EXPERIMENT 16 FLOW CHART Part AREAGENT PROCEDURE / STEP OBSERVATIONDry all glassware___g Mg (s)___ mLdiethyl ether___ molbromobenzene___ mLdiethyl etherKeep warm andreflux for a further20-30 min.Proceed to Part B68
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Chemistry 360Organic Chemistry II__
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Chemistry 360 - Athabasca University

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