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FIGURE 3GAS CHROMATOGRAM OF INDIVIDUAL ORGANOCHLORINE PESTICIDE STANDARD MIX BColumn:Temperature program:30 m x 0.25 mm ID, DB-5100EC (hold 2 minutes) to 160EC at 15EC/min, then at 5EC/min to 270EC;carrier He at 16 psi.CD-ROM <strong>8081A</strong> - 40 Revision 1December 1996
FIGURE 4GAS CHROMATOGRAM OF TOXAPHENEToxaphene analyzed on an SPB-608 fused-silica open-tubular column. The GC operating conditions wereas follows: 30 m x 0.53 mm ID SPB-608. Temperature program: 200EC (2 min hold) to 290EC at 6EC/min.CD-ROM <strong>8081A</strong> - 41 Revision 1December 1996
Page 1 and 2: METHOD 8081AORGANOCHLORINE PESTICID
Page 3 and 4: CompoundCAS Registry No.Chloropropy
Page 6 and 7: confirmation techniques may be empl
Page 9 and 10: 5.7.2 1-bromo-2-nitrobenzene is sug
Page 11 and 12: columns. Table 2 lists average rete
Page 13 and 14: mean CF ' CF 'nj CF ii'1nwhere n is
Page 15 and 16: 7.5.6.1 For aqueous samplesConcentr
Page 17 and 18: 7.5.11 Identification of mixtures (
Page 19 and 20: Construct a similar baseline in the
Page 21 and 22: 8.0 QUALITY CONTROL8.1 Refer to Cha
Page 23 and 24: 8000, Sec. 8.0 for information on e
Page 25 and 26: TABLE 1GAS CHROMATOGRAPHIC RETENTIO
Page 27 and 28: TABLE 3aFACTORS FOR DETERMINATION O
Page 29 and 30: TABLE 5GC OPERATING CONDITIONS FOR
Page 31 and 32: TABLE 6 (continued)RETENTION TIMES
Page 33 and 34: TABLE 8GC OPERATING CONDITIONS FOR
Page 35 and 36: TABLE 10ANALYTE RECOVERY FROM DICHL
Page 37 and 38: TABLE 12SINGLE LABORATORY ACCURACY
Page 39: FIGURE 2GAS CHROMATOGRAM OF INDIVID
Page 43 and 44: FIGURE 6GAS CHROMATOGRAM OF ORGANOC

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