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FIGURE 5GAS CHROMATOGRAM OF STROBANEStrobane analyzed on a DB-5/DB-1701 fused-silica open-tubular column pair. The GC operating conditionswere as follows: 30 m x 0.53 mm ID DB-5 (1.5-µm film thickness) and 30 m x 0.53 mm ID DB-1701 (1.0-µmfilm thickness) connected to a J&W Scientific press-fit Y-shaped inlet splitter. Temperature program: 150EC(0.5 min hold) to 190EC (2 min hold) at 12EC/min then to 275EC (10 min hold) at 4EC/min.CD-ROM <strong>8081A</strong> - 42 Revision 1December 1996
FIGURE 6GAS CHROMATOGRAM OF ORGANOCHLORINE PESTICIDESOrganochlorine pesticides analyzed on a DB-5/DB-1701 fused-silica open-tubular column pair. The GCoperating conditions were as follows: 30 m x 0.53 mm ID DB-5 (0.83-µm film thickness) and 30 m x 0.53mm ID DB-1701 (1.0-µm film thickness) connected to an 8 in. injection tee (Supelco Inc.). Temperatureprogram: 140EC (2 min hold) to 270EC (1 min hold) at 2.8EC/min.CD-ROM <strong>8081A</strong> - 43 Revision 1December 1996
Page 1 and 2: METHOD 8081AORGANOCHLORINE PESTICID
Page 3 and 4: CompoundCAS Registry No.Chloropropy
Page 6 and 7: confirmation techniques may be empl
Page 9 and 10: 5.7.2 1-bromo-2-nitrobenzene is sug
Page 11 and 12: columns. Table 2 lists average rete
Page 13 and 14: mean CF ' CF 'nj CF ii'1nwhere n is
Page 15 and 16: 7.5.6.1 For aqueous samplesConcentr
Page 17 and 18: 7.5.11 Identification of mixtures (
Page 19 and 20: Construct a similar baseline in the
Page 21 and 22: 8.0 QUALITY CONTROL8.1 Refer to Cha
Page 23 and 24: 8000, Sec. 8.0 for information on e
Page 25 and 26: TABLE 1GAS CHROMATOGRAPHIC RETENTIO
Page 27 and 28: TABLE 3aFACTORS FOR DETERMINATION O
Page 29 and 30: TABLE 5GC OPERATING CONDITIONS FOR
Page 31 and 32: TABLE 6 (continued)RETENTION TIMES
Page 33 and 34: TABLE 8GC OPERATING CONDITIONS FOR
Page 35 and 36: TABLE 10ANALYTE RECOVERY FROM DICHL
Page 37 and 38: TABLE 12SINGLE LABORATORY ACCURACY
Page 39 and 40: FIGURE 2GAS CHROMATOGRAM OF INDIVID
Page 41: FIGURE 4GAS CHROMATOGRAM OF TOXAPHE

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