Monograph - Metrohm

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Non-aqueous titration of acids and baseswith potentiometric endpoint indicationPeter BruttelAll rights reserved, including translation rights.Printed in Switzerland by <strong>Metrohm</strong> Ltd., CH-9101 Herisau08.1999 – 8.024.5003Non-aqueous titration of acids and bases with potentiometric endpoint indication
ContentsContents1. Preface ................................................................................................... 32. Important terms ...................................................................................... 43. Remarks concerning solvents for non-aqueous titrations ....................... 54. Apparatus and accessories used ........................................................... 95. Titration of acids ..................................................................................... 96. Titration of bases .................................................................................. 127. pK A values of some selected acids ....................................................... 148. pK B values of some selected bases ...................................................... 159. Dielectric constants (DC) of some selected solvents............................ 1610. Literature references ............................................................................ 17Compilation of results: bases as titrants ......................................................... 18Standard deviations of the electrode signals ........................................ 24Titration curves obtained with the SolvotrodeLiCl sat. in ethanol ........................................................................... 250.4 mol/L TEA-Br in ethylene glycol ................................................ 31Compilation of results: acids as titrants .......................................................... 37Standard deviations of the electrode signals ........................................ 44Titration curves obtained with the SolvotrodeLiCl sat. in ethanol ........................................................................... 450.4 mol/L TEA-Br in ethylene glycol ................................................ 492 Peter Bruttel
Page 1: MonographNon-aqueous titration of a
Page 5 and 6: Important terms2 Important termsAmp
Page 7 and 8: Remarks concerning solvents for non
Page 9 and 10: Remarks concerning solvents for non
Page 11 and 12: Titration of acidsResultsA) Benzoic
Page 13 and 14: Titration of bases6 Titration of ba
Page 15 and 16: pK Avalues of some selected acids7
Page 17 and 18: Dielectric constants (DC) of some s
Page 19 and 20: Compilation of results: bases as ti
Page 25 and 26: Standard deviations of the electrod
Page 27 and 28: Titration curves obtained with the
Page 39 and 40: Compilation of results: acids as ti
Page 45 and 46: Standard deviations of the electrod
Page 53 and 54:
Titration curves obtained with the
Page 55 and 56:
Page 57:
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Monograph - Metrohm

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