108139-1 Study Title Data Requirements Author Study ... - IR-4 Project

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Bayer Corporation <strong>108139</strong>-1 Agriculture Division — Pipets — Pasteur transfer, 5.75-in — Separatory funnels, 125-mL — Spatulas, stainless steel — Volumetric flask, class A, 50-mL Balances — Top-loader electronic, accurate to 0.00001 g (AT 20, Mettler Toledo, Columbus, OH) or equivalent — Top-loader electronic, accurate to 0.001 g (FX-200, A&D Engineering, INC., Milpitas, CA) or equivalent — Top-loader electronic, accurate to 0.01 g (Precisa 1000C-3000D, Precisa, Dietikon, Switzerland) or equivalent Chromatography columns, low-medium pressure with reservoir, 200-mL, 250-mL, (Kimble/Kontes, Vineland, New Jersey, P/N K420280-0213 and P/N K420280-0222) or equivalent Evaporators — Rotary evaporator, Büchi Rotovapor, Model RE 120 with Büchi 461(Brinkman Instruments Inc., Wesbury, NY) or equivalent. — Turbo Vap LV with 60-mL ASE vial conversion kit (Zymark, Hopkinton, MA) or equivalent GC Column — HP- P /HQJWK PP , ' P ILOP WKLFNQHVV $JLOHQW 7HFKQRORJLHV 3DOR Alto, CA) or equivalent — DB- 06 P /HQJWK PP , ' P ILOP WKLFNQHVV $JLOHQW 7HFKQRORJLHV 3DOR Alto, CA) or equivalent Mass spectrometer, 5973 mass selective detector with EI/CI source, (Agilent Technologies, Palo Alto, CA) or equivalent containing the following components — Auto sampler, 7683 series injector, (Agilent Technologies, Palo Alto, CA) — Gas chromatograph, 6890, (Agilent Technologies, Palo Alto, CA) — Software, chemstation G1701BA version B.01.00, (Agilent Technologies, Palo Alto, CA) Pipetter, Fisherbrand Finnpipettes 0.20 mL to 10 mL range (Fisher, Pittsburgh, PA) or equivalent Soxtec system HT 1043, (Foss North America, Praire, MN) or equivalent Tissumizer, model T-25 Basic with SDT-182EN probe (Tekmar, Cincinnati, OH) or equivalent Tumbler, Model A-R2, (Tru-Square Metal Products, Auburn, WA) or equivalent 26
Bayer Corporation <strong>108139</strong>-1 Agriculture Division Vials — 60 mL, (I-CHEM, New Castle, DE, P/N S236-0060) or equivalent — Auto sampler, clear glass with inserts and Viton® lined septum caps, 1.8 mL) — Sample storage, clear glass with Teflon lined caps, 4-mL 3.2.2 Reagents/Supplies Celite® 545 filter aid, (Fisher Chemicals, Pittsburgh, PA) or equivalent Compressed gases, helium and methane, purity • Filters — GF/A, 5.5-cm (Whatman Inc., Clifton, NJ) or equivalent — GHP Acrodisc, 13-PP P 3DOO *HOPDQ /DERUDWRULHV $QQ $UERU 0, 3 1 RU equivalent Florisil, 60-100 mesh, 2.5% deactivated. Prepared by adding 25 mL of water to 975 g of florisil that has been dried overnight at 110° C. Florisil was tumbled overnight to equilibrate moisture. (Fisher, Pittsburg, PA) or equivalent Sodium sulfate , anhydrous, (Fisher Chemicals, Pittsburgh, PA) or equivalent Solvents: Methanol (MeOH), acetone, acetonitrile (ACN), methylene chloride (DCM), hexane, and toluene (Fisher Chemical, Pittsburgh, PA, Optima Grade) or equivalent Solvent solutions (all solutions are volume to volume) — aqueous 1.2 N HCl. Prepared by adding 100 mL of concentrated HCl to a 1000-mL graduated cylinder and diluting to 1000 mL with water. — MeOH/aqueous 1.2 N HCL (4:1). Prepared by mixing 3200 mL of MeOH with 800 mL of aqueous 1.2 N HCl in a 4 L glass bottle. — acetone/DCM (1:2). Prepared by mixing 1300 mL of acetone with 2600 mL of DCM in a 4 L glass bottle. — acetone/hexane (1:9). Prepared by mixing 400 mL of acetone with 3600 mL of hexane in a 4 L glass bottle. — ACN presaturated with hexane. Prepared by shaking equal amounts of ACN and hexane. — Hexane presaturated with ACN. Prepared by shaking equal amounts of hexane and ACN. Syringes — Luer lok single use, 3-mL (Becton Dickinson and Co., Franklin Lakes, NJ) or equivalent — Hamilton 1700 series gas tight, 0.10 mL, 0.25 mL, 0.50 mL, (Hamilton Company, Reno, NV) or equivalent 27
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108139-1 Study Title Data Requirements Author Study ... - IR-4 Project

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