Shimadzu Techno-Research Inc., Japan - UNEP Chemicals
Shimadzu Techno-Research Inc., Japan - UNEP Chemicals
Shimadzu Techno-Research Inc., Japan - UNEP Chemicals
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HRGC/HRMS<br />
Micromass<br />
Autospec Ultima<br />
SP2331, DB-17HT,<br />
DB-5MS, HT-8PCB<br />
�dichloromethane)<br />
PCBs,POPs,PBDEs<br />
PCBs, PBDEs,<br />
(less polar) POPs<br />
HRGC/HRMS SIM<br />
PCBs, PBDEs,<br />
HCHs, HCBz,<br />
Aldrin, Heptachlor,<br />
Chlordanes,<br />
DDTs<br />
sample<br />
�Na2SO4) homogenize<br />
Soxhlet extract.<br />
16hr<br />
concentration<br />
Crude ext.<br />
portion 20%<br />
Lipid<br />
determination<br />
For<br />
PCDDs/DFs<br />
analysis<br />
Crude ext.<br />
Portion 20%<br />
Florisil cleanup<br />
Extraction & cleanup<br />
Biological sample<br />
dichloromethane<br />
DMSO partitioning<br />
Florisil cleanup<br />
13 C-PCBs Mix<br />
13 C12 -PBDE�<br />
(syringe spike)<br />
13C12-2378-TeCDD�OCDD 13C12-2378-TeCDF�OCDF 13C12-PCB� 22mix<br />
13C-POP� 3mix<br />
13C12-PBDE� 9mix<br />
�cleanup spike�<br />
portion 20%<br />
For<br />
PCBs/POPs/PBDEs<br />
analysis<br />
SHIMADZU TECHNO RESEARCH, <strong>Inc</strong>.<br />
13 C-POPs Mix<br />
Cleanup spike<br />
20%-Dichloromethane in Hexane 100% -Dichloromethane<br />
POPs (polar)<br />
HRGC/HRMS SIM<br />
Dieldrin�Endrin�<br />
Heptachlor epoxide<br />
SHIMADZU TECHNO RESEARCH, <strong>Inc</strong>.
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