Shimadzu Techno-Research Inc., Japan - UNEP Chemicals

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�� Comprehensive analytical laboratory in Japan as well as in the world. �� Update our work our research team participate in DIOXIN Conference (International Symposium on Halogenated Environmental Organic Pollutants and POPs) every year and presented several of our reports and new methodology developments. �� In addition to international meetings, we presented our analytical results and new methodology developments in the scientific meeting conducted in Japan, especially Symposium on Environmental Chemistry. �� We received a honorable prize of 2nd Technical prize of Environmental Chemistry in 1993, 1993, and Prize of Academic for Environmental Chemistry in 1996. 1996 �� Furthermore, we collaboration with scientists from several universities and institute from Japan as well as from abroad as Joint research program for Government. SHIMADZU TECHNO RESEARCH, Inc. Target Compounds and techniques HRGC-HRMS(EI); HRMS(EI); �� HRGC PCDDs/DFs, PCDDs/DFs PBDDs/DFs, PBDDs/DFs PXDDs/DFs, PXDDs/DFs, PCBs, PCNs Dioxins;PCDDs/DFs & Dioxinlike PCBs POPs; POPs DDTs(p,p‘- DDTs(p,p o,p’-DDT/DDD/DDE) o,p DDT/DDD/DDE) Chlordanes��cis Chlordanes cis/trans /trans-Chlordane, Chlordane, c/t-Nonachlor c/t Nonachlor, Oxychlordane��Heptachlor, Oxychlordane Heptachlor, cis/trans cis/trans- Heptachlor epoxide�� epoxide Cyclodienes(Aldrin, Cyclodienes(Aldrin Dieldrin, Dieldrin Endrin) Endrin HCB Mirex Toxaphene HCHs��-,��-,��-,��-HCH HCHs HCH��, , HCB, Mirex PAHs��CBz PAHs CBz, CPh Organo Tin ; phenyl Tin, Buthyl Tin, Octyl Tin BFR��PBDE BFR PBDE, PBB, PBB, HBCD, PBBz, PBBz PBPh, PBPh, TBBPA, DBDPE, BTBPE�� BTBPE�� Additionally Methabolite OH-PCB, OH PCB, OH-PBDE, OH PBDE, Tribromoanisole, Tribromoanisole, TBBPA dimethylether�� dimethylether Natural formation OMe-PBDE, OMe PBDE, OMe-PBB OMe PBB HRGC-HRMS( HRMS(NCI NCI); ); �� HRGC Toxaphene, Toxaphene Polychlorinated n-Alkanes Alkanes (PCAs PCAs), Short (C10-C13) (C10 C13) Chain, Chain Endsulfan, Endsulfan LC-MS/MS MS/MS �� LC PFOS/PFOA, PFOS/PFOA Chlordecone, Chlordecone PCAs (medium & long chain C14-) C14 ) , Polar comp. PPCP, HRGC-HRTOFMS; HRTOFMS; full characterization for unknown compounds �� HRGC SHIMADZU TECHNO RESEARCH, Inc.
New New POPs POPs proposed POPs �� PBDE (Pentabromodiphenylether ( Pentabromodiphenylether) �� HBB (Hexabromobiohenyl ( Hexabromobiohenyl) �� Chlordecone �� -HCH HCH (Lindane ( Lindane) �� PFOS (and precursor) �� OBDE (Octabromodiphenylether ( Octabromodiphenylether) �� PeCB (Pentachlorobenzene Pentachlorobenzene) �� Short-chain Short chain chlorinated Paraffins �� /��-HCH HCH �� Endosulfane SHIMADZU TECHNO RESEARCH, Inc. DIOXIN Symposium (#presentation) International International Symposium Symposium on on Halogenated Halogenated Organic Organic Pollutants Pollutants and and Persistent Persistent Organic Organic Pollutants Pollutants �� 1980 Rome Italy (52) �� 1998 Stockholm Sweden �� 1981 Arlington USA(55) �� 1999 Venice Italy (641) �� 1982 Salzburg Austria (48) 1984 Ottawa Canada (64) 1985 Bayreuth Germany (201) 1986 Fukuoka Japan (159) 1987 Las Vegas USA (178) �� 2000 Monterey USA (527) 2001 Kyongju Korea (582) 2002 Barcelona Spain (580) �� 1988 Umeå Ume Sweden (285) �� 2003 Boston USA (750) �� 1989 Toronto Canada (308) �� 2004 Berlin Germany(670) �� 1990 Bayreuth Germany (430) �� 1991 Noth Carolina USA (400) �� 1992 Tampere Finland (313) �� 1993 Vienna Austria (195) 1994 Kyoto Japan (327) �� 2005 Toronto Canada(801) 2006 Oslo Norway(700) 2007 Tokyo Japan(763) 2008 Birmingham UK �� 1995 Edmonton Canada (379) �� 2009 2009 Beijing Beijing China China �� 1996 Amsterdam The Netherlands �� (385) �� 1997 Indianapolis USA (399) 2010 2010 USA USA Texas Texas 2011 2011 Bergen Bergen SHIMADZU TECHNO RESEARCH, Inc.
Page 1 and 2: Waters TOF Meeting at Dioxin2008, T
Page 3: Summary of our capability �� 11
Page 7 and 8: Control by Database system �� A
Page 9 and 10: median, NIQR, CV% rob, min., max.,
Page 11 and 12: pg-TEQ 900 850 800 750 700 650 600
Page 13 and 14: Typical Interferences in Dioxin ana
Page 15 and 16: 100% 90% 80% 70% 60% 50% 40% 30% 20
Page 17 and 18: PCB fragment ion and PCDD ion P(n)
Page 19 and 20: Usage in Japan (ton) 1946-1972 1,00
Page 21 and 22: POPs concentrations in air sample
Page 23 and 24: HRGC/HRMS Micromass Autospec Ultima
Page 25 and 26: Native Standard Internal Standard o
Page 27 and 28: 1.20 1.10 1.00 0.90 0.80 0.70 0.60
Page 29 and 30: pg 100 10 1 0.1 0.01 0.02 0.02 TCDD
Page 31 and 32: Internal standard : different bromi
Page 33 and 34: 051019XO1001 19-Oct-2005 14:39:45 V
Page 35 and 36: MDL & MDL of air sample by HRMS sam
Page 37 and 38: �� DMSO/Hex. partioning��ef
Page 39: pg/g lipid Major POPs in Human Bloo

Shimadzu Techno-Research Inc., Japan - UNEP Chemicals

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