Shimadzu Techno-Research Inc., Japan - UNEP Chemicals

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Toxaphene Fish sample (sea bass) �� Matsukami, H. et. al., Organohalogen Compounds, 66, 217-223 (2004) SHIMADZU TECHNO RESEARCH, Inc. Toxaphene Comparison of resolution �� Still limitation R>10,000 high levels of HpCB #185 >100pg Better to check HpCB #185 �� SHIMADZU TECHNO RESEARCH, Inc.
MDL & MDL of air sample by HRMS sam p le volum e 1000m 3 � � � � � � pg/m 3 pg/m 3 o,p '-DDT 0.031 0.093 p ,p '-DDT 0.074 0.22 o,p '-DDE 0.012 0.037 p ,p '-DDE 0.039 0.12 o,p '-DDD 0.048 0.14 p ,p '-DDD 0.018 0.053 trans-Chlordane 0.23 0.69 cis-Chlordane 0.19 0.57 trans-Nonachlor 0.16 0.48 cis-Nonachlor 0.024 0.072 Oxy chlordane 0.042 0.13 Dieldrin 0.11 0.33 A ld rin 0 .0 5 0.15 Endrin 0.048 0.14 Hep tachlor 0.078 0.23 cis-Hep tach lo r e p oxide 0.017 0.052 trans-Hep ta c h lo r e p oxide 0.2 0.6 HCB 0.37 1.1 Mirex 0.017 0.05 �-HCH 0.11 0.33 � -HCH 0.041 0.12 � -HCH 0.076 0.23 �-HCH 0.05 0.15 Toxap hene Parlar #26 0.066 0.2 Toxap hene Parlar #50 0.4 1.2 Toxap hene Parlar #62 0.81 2.4 SHIMADZU TECHNO RESEARCH, Inc. MDL & Blank of biological sample in HRMS & LRMS HRGC/HRMS� �� (MDL) HRGC/HRMS� �� (�� ) HRGC/LRMS �� SHIMADZU TECHNO RESEARCH, Inc. � MDL Method Blank (pg/g) (pg/g) (ng/g) o,p'-DDT �� p,p'-DDT �� o,p'-DDE �� p,p'-DDE �� o,p'-DDD �� p,p'-DDD �� trans-Chlordane �� cis-Chlordane �� trans-Nonachlor �� cis-Nonachlor �� Oxychlordane �� Dieldrin � �� Aldrin �� Endrin �� Heptachlor �� cis-Heptachlor epoxide �� trans-Heptachlor epoxide � � � HCB �� Mirex �� -HCH �� -HCH � � � �-HCH �� -HCH ��
Page 1 and 2: Waters TOF Meeting at Dioxin2008, T
Page 3 and 4: Summary of our capability �� 11
Page 5 and 6: New New POPs POPs proposed POPs �
Page 7 and 8: Control by Database system �� A
Page 9 and 10: median, NIQR, CV% rob, min., max.,
Page 11 and 12: pg-TEQ 900 850 800 750 700 650 600
Page 13 and 14: Typical Interferences in Dioxin ana
Page 15 and 16: 100% 90% 80% 70% 60% 50% 40% 30% 20
Page 17 and 18: PCB fragment ion and PCDD ion P(n)
Page 19 and 20: Usage in Japan (ton) 1946-1972 1,00
Page 21 and 22: POPs concentrations in air sample
Page 23 and 24: HRGC/HRMS Micromass Autospec Ultima
Page 25 and 26: Native Standard Internal Standard o
Page 27 and 28: 1.20 1.10 1.00 0.90 0.80 0.70 0.60
Page 29 and 30: pg 100 10 1 0.1 0.01 0.02 0.02 TCDD
Page 31 and 32: Internal standard : different bromi
Page 33: 051019XO1001 19-Oct-2005 14:39:45 V
Page 37 and 38: �� DMSO/Hex. partioning��ef
Page 39: pg/g lipid Major POPs in Human Bloo

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