Application Compendium - Agilent Technologies

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AGILENT TECHNOLOGIES APPLICATIONS FOR POLYMERS AND RUBBERS SPECTROSCOPY Fourier Transform Infrared (FTIR) Spectroscopy Quantitative Analysis of Copolymers Using the Cary 630 FTIR Spectrometer Determination of Percent Polyethylene in Polyethylene/Polypropylene Blends Using Cast Film FTIR Techniques Rapid Identification of O-rings, Seals and Gaskets Using the Handheld Agilent 4100 ExoScan FTIR A New Approach to Sample Preparation Free Micro ATR FTIR Chemical Imaging of Polymer Laminates Identification of Contaminants in Vehicle Fuel Tank Caps Using FTIR ATR-Microscopy Component Failure Analysis of Vehicle Spark Plugs Using FTIR Spectroscopy With a Micro-ATR Large Sample Objective Material Analysis by Infrared Mapping: A Case Study Using a Multilayer Paint Sample Analytical Methods for the Agilent Cary 630 FTIR Determination of Irganox 3114 in polypropylene by infrared spectroscopy Determination of percent ethylene in ethylene-propylene statistical copolymers Determination of Irganox 1010 in polyethylene by infrared spectroscopy Determination of Irganox 1010 in polyproplene by infrared spectroscopy Determination of the vinyl content of polyethylene resins Determination of percent glycerol monostearate in polypropylene by infrared spectroscopy Atomic Force Microscopy (AFM) and Field-Emission Scanning Electron Microscopy (FE-SEM) Advanced Atomic Force Microscopy: Exploring Measurements of Local Electric Properties Agilent 5600LS AFM High-resolution Imaging Molecular-level Understanding of n-Alkanes Self-Assembly onto Graphite Several Aspects of High Resolution Imaging in Atomic Force Microscopy Compositional Mapping of Materials with Single-Pass Kelvin Force Microscopy Atomic Force Microscopy Studies in Various Environments Young’s Modulus of Dielectric ‘Low-k’ Materials Nanoindentation Nanoindentation, Scratch, and Elevated Temperature Testing of Cellulose and PMMA Films Measuring the Complex Modulus of Polyethylene Using Instrumented Indentation Complex Shear Modulus of Commercial Gelatin by Instrumented Indentation
AGILENT TECHNOLOGIES APPLICATIONS FOR POLYMERS AND RUBBERS CHROMATOGRAPHY Liquid Chromatography (LC) Sensitive Polymer Analysis using Critical Point Chromatography and ELSD Fast Analysis of Phenolic Antioxidants and Erucamide Slip Additives in Polypropylene Homopolymer Formulations Using 1200 Rapid Resolution Liquid Chromatography (RRLC) with Rapid Resolution High Throughput (RRHT) Columns and Method Translator Analysis of Phenolic Antioxidant and Erucamide Slip Additives in Polymer by Rapid-Resolution LC Developing a UHPLC Method forUV-based Detection and Quantification of Primary Aromatic Amines in Low Concentrations Determination of Polymer Additives and Migration Products Prevalent in Food Packaging Material Determination of Phthalate Migration From Toys Analysis of Bisphenol A Leaching from Baby Feeding Bottles High Sensitivity Analysis of Phthalates Using HPLC with Low Temperature Evaporative Light Scattering Detection Agilent 1290 Infinity LC with AgilentPoroshell Columns for Simultaneous Determination of Eight Organic UV Filters Gel Permeation Chromatography (GPC) Stable Baselines in the Analysis of Poly(lactide-co-glycolide) Polymers by GPC with ELSD Analyze Injection-Molding Polymers on Agilent PLgel 5 µm MIXED-C by GPC Artifact Free Analysis of Lignins by GPC using Agilent PolarGel-M GPC and Agilent PolarGel-M Columns for the True Representation of Novolac Resins Analysis of Polysaccharides by GPC Viscometry using the Agilent 390-MDS Multi Detector Suite Characterization of Block Copolymers Synthesized via Transition Metal Mediated Living Radical Polymerization Analysis of Biodegradable Polymers by GPC Analysis of Poly(styrene/butadiene) Copolymers by Conventional Gel Permeation Chromatography on the Agilent PL-GPC 50 Plus Size Exclusion Chromatography (SEC) Size Exclusion Chromatography for the Analysis of Dental Polymers SEC Analysis of a Water Soluble Copolymer SEC Analysis of a Acrylamide Copolymer GPC/SEC Analysis of biodegradable polymers by GPC/SEC Analysis of polyolefins by GPC/SEC Analysis of engineering polymers by GPC/SEC Analysis of elastomers by GPC/SEC Low molecular weight resins and prepolymers
Page 1 and 2: MATERIALS TESTING AND RESEARCH SOLU
Page 3: When accuracy and reliability in me
Page 7 and 8: Figure 1. Agilent Cary 630 FTIR spe
Page 9 and 10: The calibration samples were measur
Page 11 and 12: Author Frank Higgins Agilent Techno
Page 13 and 14: Figure 1. The overlaid aliphatic be
Page 15 and 16: Author John Seelenbinder Agilent Te
Page 17 and 18: Figure 3. Sample is lightly pressed
Page 19 and 20: Author Dr. Mustafa Kansiz Agilent T
Page 21 and 22: microscopy provides for a factor of
Page 23 and 24: Standard ATR IR Image No Pressure (
Page 25 and 26: A visual inspection of the sample u
Page 27 and 28: Experimental Instrumentation To per
Page 29 and 30: Authors Jonah Kirkwood † and Must
Page 31 and 32: Spectra were collected from each lo
Page 33 and 34: Infrared mapping allows for multipl
Page 35 and 36: The spectra in Figure 2 are visuall
Page 37 and 38: Conclusion Agilent‟s Cary 610 FTI
Page 39 and 40: Authors Dr. Wayne Collins*, John Se
Page 41 and 42: The calibration curve obtained for
Page 43 and 44: Conclusion Select ‘Peak Ratio’
Page 45 and 46: Summary This method describes a pro
Page 47 and 48: Method configuration To determine t
Page 49 and 50: Authors Dr. Wayne Collins*, John Se
Page 51 and 52: The calibration curve for the deter
Page 53 and 54: Figure 6. The MicroLab PC FTIR soft
Page 55 and 56:
Summary An analytically representat
Page 57 and 58:
Figure 3. The Irganox 1010 peak are
Page 59 and 60:
Authors Dr. Wayne Collins*, John Se
Page 61 and 62:
The calibration curve and equation
Page 63 and 64:
Select ‘Peak Ratio’ - from the
Page 65 and 66:
Summary An analytically representat
Page 67 and 68:
Figure 3. The GMS peak height absor
Page 69 and 70:
Advanced Atomic Force Microscopy: E
Page 71 and 72:
signal) image indicating the overwh
Page 73 and 74:
A dependence of surface potential o
Page 75 and 76:
A B C Figure 6A-C. The topography (
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A B Figure 10A-C. The topography (A
Page 79 and 80:
KFM with AM-FM operation in the int
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ibbons is only slightly different f
Page 83 and 84:
References 1. G. Binnig, C.F. Quate
Page 85 and 86:
Figure 1. AFM topographic image of
Page 87 and 88:
100nm 100nm 350nm 100nm Figure 3. A
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to perfect hexagonal patterns, whic
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Single-pass KFM studies have been k
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images due to the difference of the
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0.5 V) of the nanowires. Additional
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appeared in the topography image. T
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of PSS component. TEM studies of mo
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Atomic Force Microscopy Studies in
Page 103 and 104:
on graphite and MoS2 are shown in F
Page 105 and 106:
A B C D Scan size: 5 µm. Scan size
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images of PEDOT:PSS blend, (PEDOT -
Page 109 and 110:
Young’s Modulus of Dielectric ‘
Page 111 and 112:
Figure 3. Young’s modulus as a fu
Page 113 and 114:
Nanoindentation, Scratch, and Eleva
Page 115 and 116:
The samples listed as “D” sampl
Page 117 and 118:
Figure 6. Elastic modulus results f
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Figure 11. Elastic modulus results
Page 121 and 122:
Sample B Figure 16. Scratch curves
Page 123 and 124:
Conclusions Nanoindentation and scr
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measurement technique has been expl
Page 127 and 128:
References 1. J.L. Hay, “Using In
Page 129 and 130:
Theory The complex shear modulus (G
Page 131 and 132:
References 1. Jain, S.K., Bhattacha
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LCCC relies on carrying out isocrat
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log Mp 5 4.6 4.2 3.8 0.5 15% Water
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Authors Wei Luan and Chunxiao Wang
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Table 1. Chemical Information of An
Page 141 and 142:
Injection Volume Influence of Real
Page 143 and 144:
translator into three modes on diff
Page 145 and 146:
To identify the matrix influence on
Page 147 and 148:
Authors Chun-Xiao Wang and Wei Luan
Page 149 and 150:
Table 1. Polymer Additives in ASTM
Page 151 and 152:
1 2 3 4 5 1 Tinuvin P 2 BHT 3 BHEB
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1 Tinuvin P 2 BHT 3 BHEB 4 Isonox 1
Page 155 and 156:
Authors Edgar Naegele Agilent Techn
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Results and discussion To meet the
Page 159 and 160:
Authors Melissa Dunkle, Gerd Vanhoe
Page 161 and 162:
Experimental The analyses were perf
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Repeatability of the SFC/MS analysi
Page 165 and 166:
Conclusion The combination of the A
Page 167 and 168:
Introduction Phthalates form a grou
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The analytical method was applied t
Page 171 and 172:
Introduction Bisphenol A (BPA) is a
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Preparation of standards BPA and BP
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Limit of Detection (LOD) and Limit
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Sample analysis The content of BPA
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The calibration for BPA and BPF, wh
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Author Stephen Ball Agilent Technol
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Results and discussion By operating
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Introduction The wavelength of UV r
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LC parameters Premixed solutions of
Page 189 and 190:
Linearity A linearity study was per
Page 191 and 192:
References 1. Dr. James H. Gibson,
Page 193 and 194:
Instrumentation Columns: 2 x PLgel
Page 195 and 196:
Authors Greg Saunders and Ben MacCr
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Authors Greg Saunders, Ben MacCreat
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Page 201 and 202:
Page 203 and 204:
Page 205 and 206:
Author Greg Saunders Agilent Techno
Page 207 and 208:
Figure 5. Universal calibration cur
Page 209 and 210:
Methods and Materials Conditions Co
Page 211 and 212:
Materials and Methods A column set
Page 213 and 214:
Page 215 and 216:
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