11 - Stirring and Dispersing - HiTec Zang GmbH
11 - Stirring and Dispersing - HiTec Zang GmbH
11 - Stirring and Dispersing - HiTec Zang GmbH
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Here you will find:<br />
� ViscoPakt ® Torque Measuring Stirrer Drive<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
� ViscoTrol Control Module for Three Phase Stirrer Drive<br />
� <strong>Stirring</strong> Accessories (<strong>Stirring</strong> Blades, Lead-Throughs, Magnetic Couplings....)<br />
� Drives <strong>and</strong> Tools for <strong>Dispersing</strong> <strong>and</strong> Homogenisation<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/910 100 · info@hitec-zang.de · http://www.hitec-zang.com 1
2<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
Measuring Stirrer ViscoPakt ®<br />
The Visco-Pakt measuring stirrer is a strong stirring<br />
an torque measuring system with speed regulation<br />
<strong>and</strong> state-of-the-art torque measurement sensitivity.<br />
Fields of Application<br />
� System stirrer for automatic laboratory reactor<br />
� Identification of reaction phases<br />
� Detection of stirrer dissipation in the reaction<br />
calorimeter<br />
� Measurement of rheological material properties<br />
� Scale-up experiments<br />
� Process monitoring<br />
The drive unit requires only a fraction of the space<br />
needed by usual measuring stirrers, allowing more<br />
valuable space for the reactor head. Due to its<br />
compact construction, it also fits into a small<br />
apparatus, e.g. a 250 mL reactor system. The small<br />
dimensions of the drive were achieved by separating<br />
the stirrer from its control unit. The separate<br />
controller has a keypad <strong>and</strong> an LC display, which<br />
shows the torque <strong>and</strong> rotational speed.<br />
The measured torque is automatically corrected<br />
using the speed dependent “zero torque”.<br />
In many applications, ViscoPakt delivers important<br />
additional information. For polymerization <strong>and</strong> polycondensation,<br />
the initiation or completion of a<br />
reaction, which cause a change in the viscosity, can<br />
be read off <strong>and</strong> identified via the torque.<br />
The power dissipated from stirring, which is of<br />
interest for reaction calorimetry, can be determined<br />
from the torque <strong>and</strong> speed of rotation.<br />
As the design has no gearing, an extraordinarily<br />
large range of torque can be continuously achieved<br />
with no switching.<br />
Glass stirrers are protected from breaking by softstart<br />
<strong>and</strong> torque limiters.<br />
Characteristics <strong>and</strong> Functions<br />
� Powerful <strong>and</strong> compact<br />
� High measuring precision<br />
� High measuring sensitivity<br />
� Robust measurement technique<br />
� Measurement of rotational speed <strong>and</strong> torque<br />
� Wide <strong>and</strong> continuous range of rotational<br />
speeds<br />
� Smooth start-up, adjustable gradient<br />
� Automatic correction of the zero torque<br />
� Adjustable soft-start ramp<br />
� Adjustable rotational speed <strong>and</strong> torque<br />
limitation<br />
� Quick catch chuck<br />
� Low noise operation<br />
ViscoPakt rheo was developed for applications for<br />
which the exact torque, viscosity, or the dissipated<br />
energy <strong>and</strong> a precise keeping of the rotational speed<br />
are needed.<br />
The measurement sensitivity is impressive.<br />
Viscosity variations in the order of the viscosity of<br />
water are still resolved.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
ViscoPakt ®<br />
The st<strong>and</strong>ard design is equipped with a simple<br />
torque output which reflects the viscosity's trends.<br />
Variations of the rotational speeds due to load<br />
fluctuations are electronically compensated.<br />
Technical data<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
ViscoPakt model - 27 - 57 - <strong>11</strong>0 Unit<br />
Maximum torque 27 57 <strong>11</strong>0 Ncm<br />
Resolution 0,07 0,1 0,2 Ncm<br />
Reproducibility 1,5 3 5 Ncm<br />
Minimum speed 150 150 150 rpm<br />
Maximum speed 2200 2000 2000 rpm<br />
Speed uncertainty 2 1,5 1,5 %<br />
Chuck size 1 - 10 1 - 10 1 - 10 mm<br />
Type of protection<br />
controlling device<br />
20 20 20 IP<br />
Type of protection<br />
drive<br />
51 51 51 IP<br />
Approx. Weight 2 3 4 kg<br />
Motor Diameter 55 70 83 mm<br />
Length across axis<br />
(approx.)<br />
210 230 270 mm<br />
Extension<br />
diameter/length<br />
16 / 220 16 / 220 16 / 220 mm<br />
Max. viscosity 10.000 40.000 70.000 mPas<br />
Max. Mixing quantity<br />
(H2O)**<br />
15 30 50 Liter<br />
* Control Unit /Drive<br />
** Reference values for propeller stirrer in H2O<br />
Interfaces<br />
Analogue:<br />
Required rotational speed 0 - 10 V, 0/4-20mA<br />
Actual rotational speed (= required value or 0) 0 - 10 V, 0/4-20mA<br />
Actual torque value 0 - 10 V, 0/4-20mA<br />
The setpoint rotational speed can be pre-set via an<br />
analogue input or the serial interface. The torque<br />
<strong>and</strong> the setpoint rotational speed are issued via the<br />
analogue outputs <strong>and</strong> the serial interface.<br />
RS232:<br />
Send: Setpoint rotational speed<br />
Received: Setpoint rotational speed, actual torque value<br />
Delivery Scope Measuring-stirrer drive <strong>and</strong> control unit with 2.3 m cable<br />
Order Code Description Specifications<br />
IR-VIPA27 ViscoPakt-27 27 Ncm<br />
IR-VIPA57 ViscoPakt-57 57 Ncm<br />
IR-VIPA<strong>11</strong>0 ViscoPakt-<strong>11</strong>0 <strong>11</strong>0 Ncm<br />
IR-VIPARS Optional RS232 Interface Setpoint rotational speed <strong>and</strong> actual torque<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/910 100 · info@hitec-zang.de · http://www.hitec-zang.com 3
4<br />
ViscoPakt ® -rheo<br />
The ViscoPakt-Rheo model series is equipped with<br />
precision-torque measuring. The zero torque, which<br />
depends on the rotational speed, is registered by an<br />
automatic calibration process <strong>and</strong> is used to correct<br />
the actual torque signal. This allows the on-line<br />
determination of the viscosity (via a calibration table)<br />
as well as of other rheological parameters.<br />
Technical Data<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
ViscoPakt Model rheo - X7 - 16 - 27 - 57 -<strong>11</strong>0 Unit<br />
Maximum torque 7 16 27 57 <strong>11</strong>0 Ncm<br />
Resolution 0.003 0.01 0.02 0.04 0.08 Ncm<br />
Reproducibility 0.05 0.1 0.2 0.4 0.8 Ncm<br />
Minimum speed 40 40 40 40 40 rpm<br />
Maximum speed 3000 2200 2200 2000 2000 rpm<br />
Speed uncertainty 0.1 0.1 0.1 0.1 0.1 %<br />
Chuck size 1 - 10 1 - 10 1 - 10 1 - 10 1 - 10 mm<br />
Type of protection<br />
controlling device<br />
20 20 20 20 20 IP<br />
Type of protection<br />
drive<br />
54 54 54 54 54 IP<br />
Approx. Weight 0.9 1.7 2.6 3.9 6 kg<br />
Motor Diameter 70 45 55 70 83 mm<br />
Length above axis<br />
(approx.)<br />
250 245 250 255 295 mm<br />
Extension<br />
diameter/length<br />
16/220 16/220 16/220 16/220 16/220 mm<br />
Max. viscosity 5,000 6,000 10,000 40,000 70,000 mPas<br />
Max. Mixing quantity<br />
(H2O)**<br />
2 8 15 30 50 Litres<br />
* Control Unit /Drive<br />
** Reference values for propeller stirrer in H2O*<br />
Interfaces<br />
Analogue:<br />
Required rotational speed 0 - 10 V, 0/4-20mA<br />
Actual rotational speed (= required value or 0) 0 - 10 V, 0/4-20mA<br />
Actual torque value 0 - 10 V, 0/4-20mA<br />
Changes to the rotational speed which are caused<br />
by load fluctuations are registered by a digital<br />
revolution counter <strong>and</strong> are electronically regulated.<br />
The rotational speed can be pre-set via an analogue<br />
input or the serial interface. The actual rotational<br />
speed <strong>and</strong> the torque are issued via the analogue<br />
outputs <strong>and</strong> the serial interface.<br />
RS232:<br />
Send: Required rotational speed<br />
Received: Required rotational speed, actual rotational speed, actual torque value<br />
Delivery Scope Measuring-stirrer drive <strong>and</strong> control unit with 2.3 m cable<br />
Order Code Description Specifications<br />
IR-VIPARHX7 ViscoPakt-Rheo-X7 7 Ncm<br />
IR-VIPARH16 ViscoPakt-Rheo-16 16 Ncm<br />
IR-VIPARH27 ViscoPakt-Rheo-27 27 Ncm<br />
IR-VIPARH57 ViscoPakt-Rheo-57 57 Ncm<br />
IR-VIPARH<strong>11</strong>0 ViscoPakt-Rheo-<strong>11</strong>0 <strong>11</strong>0 Ncm<br />
IR-VIPARS Option RS232 Interface Setpoint <strong>and</strong> actual rotational speed <strong>and</strong><br />
actual torque<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
ViscoPakt ® -rheo+<br />
The model series ViscoPakt-Rheo+ is based on<br />
most modern brushless drives. Consequently, they<br />
are absolutely maintenance-free <strong>and</strong> the friction<br />
moment caused by the brush is no longer existent at<br />
precision torque measurements. The speeddependant<br />
zero torque is captured in the course of<br />
an automatic calibration procedure <strong>and</strong> utilised for<br />
the correction of the torque signal. Herewith, it is<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
Technical Data<br />
Type ViscoPakt-rheo+ -40 -75 -150 -220 Einheit<br />
Maximum torque 40 75 150 220 Ncm<br />
Resolution 0,01 0,03 0,04 0,05 Ncm<br />
Reproducibility 0,1 0,2 0,3 0,4 Ncm<br />
Minimum speed 40 40 40 40 rpm<br />
Maximum speed 2200 2000 2000 2000 rpm<br />
Speed uncertainty 0,01 0,01 0,01 0,01 %<br />
Chuck size 1 - 10 1 - 10 1 - 10 1 - 10 mm<br />
Type of protection<br />
controlling device<br />
20 20 20 20 IP<br />
Type of protection drive 54 54 54 54 IP<br />
Approx. Weight 1,5 2,5 3,5 5 kg<br />
Motor Diameter 43 87 87 87 mm<br />
Length above axis<br />
(approx.)<br />
200 180 180 210 mm<br />
Extension diameter/length 10 / 200 13 / 200 13 / 200 13 / 200 mm<br />
Max. viscosity 10.000 40.000 70.000 70.000 mPas<br />
Max. Mixing quantity** 15 40 60 80 Liter<br />
* Steuergerät/Antrieb<br />
** Richtwerte für Propellerrührer in H2O<br />
Schnittstellen<br />
RS232, RS485 interface with Modbus Protocol (opt.)<br />
Send: Rotational speed desired value<br />
Receive: Rotational desired/actual value, torque actual value<br />
Analogue:<br />
Required rotational speed 0 - 10 V, 0/4-20mA<br />
Actual rotational speed (= required value or 0) 0 - 10 V, 0/4-20mA<br />
Actual torque value 0 - 10 V, 0/4-20mA<br />
possible to establish the viscosity (per calibration<br />
table) <strong>and</strong> other rheological parameters online.<br />
Speed changes caused by load variations are<br />
captured by a digital speed sensor <strong>and</strong> electronically<br />
compensated. The speed can be predefined via an<br />
analogue input or the serial interface. The actual<br />
speed <strong>and</strong> the torque are issued via analogue<br />
outputs <strong>and</strong> the serial interface.<br />
Delivery Scope Measuring-stirrer drive <strong>and</strong> control unit with 2.3 m cable<br />
Bestellcode Beschreibung<br />
IR-VIPARHP40 ViscoPakt-Rheo+-40 precision-stirrer actuator, 40 Ncm<br />
IR-VIPARHP75 ViscoPakt-Rheo+-75 precision-stirrer actuator, 75 Ncm<br />
IR-VIPARHP150 ViscoPakt-Rheo+-150 precision-stirrer actuator, 150 Ncm<br />
IR-VIPARHP220 ViscoPakt-Rheo+-220 precision-stirrer actuator, 220 Ncm<br />
IR-VIPARHPRS485 Option RS485 ModBus Interface<br />
IR-VIPARHPUI Option Current <strong>and</strong> voltrage interface<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/910 100 · info@hitec-zang.de · http://www.hitec-zang.com 5
6<br />
ViscoPakt ® -mini-rheo-35<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
The ViscoPakt-mini is a<br />
precision measuring stirrer<br />
disposing of an especially<br />
compact design. It is<br />
deployed where torques<br />
must be generated in most<br />
limited spaces. These are<br />
mainly small reactors with a<br />
nominal volume below 500<br />
ml with many mounted<br />
sockets at the same time,<br />
as such are frequently<br />
deployed for parallel<br />
syntheses.<br />
The ViscoPakt-mini,<br />
amongst other utilisations,<br />
is deployed in our LabKit<br />
<strong>and</strong> MultiLab parallel<br />
reactor systems.<br />
Interfaces<br />
Analogue:<br />
Order Code Description<br />
IR-VIPA-MINI-RHEO-35 ViscoPakt-mini-rheo stirrer drive, 35 Ncm<br />
Ministirrer<br />
The MiniStirrer is the economic<br />
alternative to the ViscoPakt-mini<br />
with a lower maximum torque<br />
<strong>and</strong> simple torque measurement<br />
(current measurement).<br />
It can be deployed everywhere<br />
where a qualitative torque signal<br />
is sufficient <strong>and</strong> relatively lowviscous<br />
substances are stirred.<br />
Order Code Description<br />
IR-MINISTIRR10 Mini-stirrer-10 stirrer drive<br />
<strong>HiTec</strong>-<strong>Zang</strong> naturally also offers all necessary<br />
accessories, e.g. flexible stirrer shafts, stirrer shaft<br />
protection, special stirrer receptacles, <strong>and</strong> also a<br />
wide array of mixing elements made of glass, high-<br />
Setpoint rotational speed 0 - 10 V, 0/4-20mA<br />
Actual rotational speed (=<br />
setpoint value or 0)<br />
0 - 10 V, 0/4-20mA<br />
Actual torque value 0 - 10 V, 0/4-20mA<br />
RS232:<br />
Send: Setpoint rotational speed<br />
Received: Setpoint rotational speed, actual<br />
rotational speed, actual torque value<br />
ViscoPakt Type mini-rheo-35 Unit<br />
Maximum torque 35 Ncm<br />
Resolution 0.01 Ncm<br />
Reproducibility 0.1 Ncm<br />
Minimum speed 15 rpm<br />
Maximum speed 800 rpm<br />
Diameter 45 mm<br />
Length across axis 230 mm<br />
Interfaces<br />
Analogue:<br />
Setpoint rotational speed 0 - 10 V, 0/4-20mA<br />
Actual rotational speed (=<br />
Setpoint value or 0)<br />
0 - 10 V, 0/4-20mA<br />
Actual torque value 0 - 10 V, 0/4-20mA<br />
ViscoPakt Type Mini-strirrer-10 Unit<br />
Maximum torque 17 Ncm<br />
Resolution 0.07 Ncm<br />
Reproducibility 0.5 Ncm<br />
Minimum speed 60 rpm<br />
Maximum speed 1900 rpm<br />
Diameter 50 mm<br />
Length across axis 195<br />
*only current measurement!<br />
mm<br />
grade steel PTFE <strong>and</strong> other materials. Our experts<br />
will gladly help you to arrange the mixing elements<br />
<strong>and</strong> stirrers that exactly accord to your requirements.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
ViscoTrol Control Unit for Three-Phase Stirrer Drive<br />
The ViscoTrol control units enable an electronically<br />
controlled variation of the rotational speed of three<br />
phase stirrer drives <strong>and</strong> the electronic collection of<br />
the torque. Due to this, adjustable gear units <strong>and</strong><br />
<strong>and</strong> measuring shafts are no longer necessary.<br />
The st<strong>and</strong>ard ViscoTrol family meets simple<br />
requirements in regard to precision.<br />
Higher dem<strong>and</strong>s to precision are met by the<br />
ViscoTrol rheo family.<br />
Due to unsufficiant cooling when in low rpm mode it<br />
is recommended to adjust the motor via the set point<br />
of the control device or adding an additional cooler.<br />
ViscoTrol<br />
The control units dispose of a Start-Stop switch <strong>and</strong><br />
a setpoint potentiometer for manual operation.<br />
Interfaces:<br />
Analogue Interfaces: 4...20mA, E = setpoint<br />
rotational speed,<br />
A = Torque <strong>and</strong> actual rotational speed<br />
RS485 interface with Modbus Protocol<br />
Digital Release<br />
Notice<br />
A MODBUS interface requires the option<br />
PNKMODBUS <strong>and</strong> a free RS485 interface at the PI.<br />
The activation via 4-20 mA requires an 4-20mA<br />
analogue output for the setpoint rotational speed, as<br />
Delivery Scope Control Unit with power cable.<br />
Technical Data<br />
Performance 0.35 up to 2.2 kW<br />
Rotational Speed 1:250 (at sufficient<br />
Variation<br />
cooling of motor)<br />
Start Ramp Adjustable<br />
Torque Limiting Adjustable<br />
RPM Limiting Adjustable<br />
Resolution<br />
Torque Measurement<br />
5% (differentiated)<br />
Casing Protection<br />
Category<br />
IP54<br />
Power Supply Single phase supply 200 -<br />
240V<br />
Dimensions LxWxH 192x215x277mm<br />
well as respectively one analogue input 4-20mA for<br />
the actual rpm <strong>and</strong> torque. In addition, a digital<br />
output is required for the digital release.<br />
Order Code Description<br />
IR-VISCOTROL350 ViscoTrol350 control unit for three phase drives, 0,35 kW<br />
IR-VISCOTROL550 ViscoTrol550 control unit for three phase drives, 0,55 kW<br />
IR-VISCOTROL<strong>11</strong>00 ViscoTrol<strong>11</strong>00 control unit for three phase drives, 1,1 kW<br />
IR-VISCOTROL2200 ViscoTrol2200 control unit for three phase drives, 2,2 kW<br />
IR-VISCOTROL-MOT055 Asynchronous 0,55 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT075 Asynchronous 0,75 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT<strong>11</strong>0 Asynchronous 1,10 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT150 Asynchronous 1,5 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT300 Asynchronous 3,0 kW motor for Viscotrol<br />
IR-VISCOTROL-FAN Additional fan for ViscoTrol asynchrous motor<br />
ZK-R-HI30-BK-IX-Y-01 ViscoTrol cable for LabManager/box, 4...20mA rotational speed set point <strong>and</strong> current value,<br />
digital disengange<br />
ZK-R-HI30-BS-R4-I-01 ViscoTrol cable RS485<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/910 100 · info@hitec-zang.de · http://www.hitec-zang.com 7
8<br />
ViscoTrol rheo<br />
The activation via 4-20 mA<br />
requires an 4-20mA<br />
analogue output for the<br />
setpoint rotational speed, as<br />
well as one analogue input 4-<br />
20mA for the torque The<br />
checkback signal of the<br />
actual rotational speed via the<br />
device-internal PFM-output<br />
requires an additional digital<br />
input. In addition, a digital<br />
output is required for the digital release. Notice: The<br />
deployment of the RS485 requires an additional<br />
RS485 interface module in the PI <strong>and</strong> a device<br />
component for binary protocoling.<br />
Note: For a MODBUS-interface the option<br />
PNKMODBUS <strong>and</strong> a single free RS485 at the PI is<br />
needed.<br />
Delivery Scope Control Unit (box) with power<br />
supply line<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
Technical Data<br />
Order Code Description<br />
IR-VISCOTROL350-RHEO ViscoTrol350 control unit for three phase drives. 0,35 kW<br />
IR-VISCOTROL550-RHEO ViscoTrol550control unit for three phase drives, 0,55 kW<br />
IR-VISCOTROL750-RHEO ViscoTrol750 control unit for three phase drives, 0,75 kW<br />
IR-VISCOTROL-MOT075 Asynchronous 0,75 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT<strong>11</strong>0 Asynchronous 1,10 kW motor for Viscotrol<br />
IR-VISCOTROL-FAN Additional fan for ViscoTrol asynchrous motor<br />
Cable<br />
Performance 0.35 to 0.75 kW<br />
Rotational Speed 1:250 (if motors sufficiently<br />
Variation cooled)<br />
Start Ramp Adjustable<br />
Torque Limiting Adjustable<br />
RPM Limiting Adjustable<br />
Resolution Torque 0.5%<br />
Measurement<br />
Casing Protection<br />
Category<br />
IP 20, IP54 at connection<br />
Power Supply 400V Rotating current<br />
Interfaces:<br />
Analogue interfaces 4...20mA, I = set point rpm, O =<br />
torque<br />
RS485 interface with Modbus RTU protocol<br />
Digital disengage<br />
Bestellcode Beschreibung<br />
ZK-R-HI31-BK-IA-Y-01 Cable for LabManager/box, rotational speed setpoint value, actual value torque actual value<br />
4...20mA., release via digital output, 3m<br />
ZK-R-HI31-BK-IP-Y-01 Cable for LabManager/box, rotational speed setpoint value, actual value torque actual value<br />
4...20mA., release via digital output, 3m<br />
Accessories for the ViscoPakt®-Family<br />
Cable<br />
Order Code Description<br />
ZK-R-HI02-BA-UP-Y-03 Cable for LabManager/box, Setpoint speed <strong>and</strong> actual value,<br />
torque current value, 0...10V, 3m<br />
ZK-R-HI02-BA-IP-Y-02 Cable for LabManager/box, Setpoint speed required <strong>and</strong> actual value,<br />
torque actual value, 0/4...20mA, 3m<br />
ZK-R-HI02-BS-R2-I-01 RS232 cable, Setpoint speed <strong>and</strong> actual value,<br />
torque actual value, On/Off, 3m<br />
Mounting Elements<br />
Bilateral mounting element for LabKit square<br />
aluminum profiles.<br />
In comparison to st<strong>and</strong>ard mounting elements with<br />
round rod, this element defines all axes of the stirrer<br />
drive.<br />
Order Code Description<br />
IR-VPMONT2 Mounting element for ViscoPakt stirrer drives on to LabKit aluminum profiles<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Stirrer Couplings<br />
These stirrer shaft coulings are made of POM, a<br />
mechanically stable light-weight plastic. The power<br />
transmission is conducted via a novel internally<br />
located construction with high-grade steel ball<br />
bearings.<br />
St<strong>and</strong>ard version<br />
Version for magnetic stirrer heads<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
The individual advantages are:<br />
� low-weight but highly stable construction<br />
� extremely low centrifugal forces due to the<br />
low weight<br />
� suited for stirrer shafts jacketed with glass,<br />
metal or PTFE<br />
� Rotational direction-independent (anti- <strong>and</strong><br />
clockwise rotation equally possible)<br />
� version free of play (no vibration development<br />
or resonance)<br />
� suited for speeds up to 1200 rpm<br />
� high-power transmission up to 3 Nm<br />
� uncomplicated mounting of the stirring shaft<br />
in a Ø 8 mm <strong>and</strong> Ø 10 mm receptacle (clamp<br />
ring connection)<br />
� extra-long receptacle pin with Ø 10 mm,<br />
respectively 8 mm hexagon head, <strong>and</strong> a<br />
length of 90 mm, generates space (length can<br />
be shortened by user)<br />
� Temperature stability maximal +<strong>11</strong>0°C <strong>and</strong><br />
minimal -20°C, respectively without stress<br />
Technical Data<br />
<strong>Stirring</strong> shaft receptacle,<br />
below<br />
8 mm <strong>and</strong> 10 mm<br />
Upper receptacle Ø 10<br />
Total length 190 mm<br />
Maximum axis offset 10 mm<br />
Technical Data<br />
<strong>Stirring</strong> shaft receptacle Interior-square<br />
SW6<br />
Upper receptacle Female hexagon<br />
SW8<br />
Total Length 190 mm<br />
Maximum axis offset 10 mm<br />
Order Code Description<br />
IR-VIPARK-BF-POM Light-weight, highly stable stirring coupling made of POM, st<strong>and</strong>ard version for stirrer shafts Ø<br />
8mm or 10mm<br />
IR-VIPARK-VK-POM Light-weight, highly stable stirring coupling made of POM, for magnetic stirrer heads with interiorsquare<br />
SW5 for magnetic coupling<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/910 100 · info@hitec-zang.de · http://www.hitec-zang.com 9
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Bellows couplings<br />
In order to be able to bridge longer distances<br />
between the stirrer drive <strong>and</strong> stirring lead-through,<br />
we offer our flexible stirring shaft extensions. They<br />
consist of bellows couplings <strong>and</strong> high-grade steel<br />
shafts.<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
Order Code Description Specifications<br />
IR-VIPARWV15019 Flexible stirring shaft extension made of 19 cm, shaft Ø 6mm, 2 bellows coupling max.<br />
high-grade steel<br />
150Ncm<br />
IR-VIPARWV45020 Flexible stirring shaft extension made of 20 cm, shaft Ø 10mm, 2 bellows coupling max.<br />
high-grade steel<br />
450Ncm<br />
IR-VIPARWV45028 Flexible stirring shaft extension made of 28 cm, shaft Ø 10mm, 2 bellows coupling max.<br />
high-grade steel<br />
450Ncm<br />
IR-VIPARWV100021 Flexible stirring shaft extension made of 21 cm, shaft Ø 10mm, 2 bellows coupling max.<br />
high-grade steel<br />
1000Ncm<br />
IR-VIPARWV100029 Flexible stirring shaft extension made of 29 cm, shaft Ø 10mm, 2 bellows coupling max.<br />
high-grade steel<br />
1000Ncm<br />
Magnetic stirrer heads<br />
Technical Data<br />
For stirring shafts-Ø 8 mm 10 mm<br />
Square connection<br />
for coupling<br />
Female<br />
square<br />
adapter<br />
SW6<br />
With grinding<br />
Female<br />
square<br />
adapter<br />
SW6<br />
Guide Tube<br />
(glas)<br />
NS 29/32<br />
max. torque 50 Ncm 50 Ncm<br />
max. rpm 1500 rpm 1500 rpm<br />
max. media temp. 250°C 250°C<br />
With grinding<br />
NS 29/32<br />
Order Code Description<br />
IR-RDFMAG8 magnetic stirrer head for 8 mm stirring shafts<br />
IR-RDFMAG10 magnetic stirrer head for 10 mm stirring shafts<br />
Advantages<br />
� high performance power transmission 50<br />
Ncm<br />
� metal–free, no lubricants<br />
� easy-to-clean due to easy-to-access <strong>and</strong><br />
smooth components<br />
� compact construction, low outer dimensions<br />
-Ø 35 mm, generates space on the lid<br />
� high rotational speed up to max. 1.500 rpm<br />
� high working temperature up to +250°C<br />
� excellent chemical stability (comparable with<br />
PTFE)<br />
� Suited for dry run<br />
� Sealed rotor prevents leakages<br />
� smooth, non-porous rotor prevents memory<br />
effects<br />
� extremely durable due to exchangeable<br />
durable wear parts<br />
Miscellaneous Accessories<br />
Order Code Description Specifications<br />
IB-SIND Inductive rotation speed monitor 3...300 Impulse /min, dimensions: M30 thread x 81 mm<br />
IR-VIPASFG Chuck size for glass stirrer with shaft Diameter 8mm, 2 bellows couplings<br />
IR-VIPARWS <strong>Stirring</strong> shaft protection, half-shell Adjustable length: 19 to 30 cm<br />
Special designs <strong>and</strong> further accessories available upon request.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Stirrer Blades<br />
According to the desired application, some stirrer<br />
blades are more suited than others to perform the<br />
task. In laboratories close to production, it is often<br />
preferred to use the same stirrer type as in<br />
production in order to reach maximum comparability.<br />
Anchor Stirrer Propeller<br />
Stirrer<br />
Turbine Stirrer Cross-Arm<br />
Stirrer<br />
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
Plane Stirrer /<br />
Turbo Stirrer<br />
Slanted Blade<br />
Stirrer<br />
We are able to produce <strong>and</strong> supply stirrer blades<br />
according to your specifications made of stainless<br />
steel, glass <strong>and</strong> other materials.<br />
Stirrer blades out of metal can be provided with a<br />
thin glass coating in order to increase media<br />
compatibility.<br />
Impeller Stirrer MIG-Stirrer Toothed Disc/<br />
Dissolver<br />
Stirrer<br />
Grating Stirrer Paddle Stirrer Spiral Ribbon<br />
Stirrer<br />
Stirrer type Recommended Application Speed Range Principal Viscosity Limit Diameter Ratio<br />
approx. rpm** Current approx. mPas (cSt) D/d<br />
Anchor stirrer In case of crust<br />
development, good<br />
exchange of heat,<br />
strong shear flow,<br />
medium to high-viscous<br />
20 ... 500 tangential 50,000 1.05 ... 1.1<br />
Propeller stirrer Good mixing effect,<br />
stirring of light solid<br />
matters, thickening<br />
agents<br />
200 ... 1800 axial 4,000 3 ... 6<br />
Pane stirrer <strong>Dispersing</strong>, dispersion 300 ... 1500 radial 1,000 2 ... 4<br />
(with blades)/ of gases, strong shear<br />
Turbo stirrer flow<br />
Impeller stirrer Good mixing effect 500 ... 1500 radial 10,000 1.5 ... 2<br />
MIG-stirrer high mixing effect,<br />
strong shear flow for<br />
low to medium<br />
viscosities<br />
200 ... 1000 axial 10,000 1.05 ... 1.5<br />
Toothed disc/<br />
dissolver stirrer<br />
Particle break-up 1000 ... 3000 radial 100,000 2 ... 5<br />
Turbine stirrer Highly viscous media,<br />
lacquers, medium to<br />
high rotation speeds<br />
400 ... 2200 axial 200,000 3 ... 6<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/910 100 · info@hitec-zang.de · http://www.hitec-zang.com <strong>11</strong>
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<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
Stirrer type Recommended Application Speed Range Principal Viscosity Limit Diameter Ratio<br />
approx. rpm** Current approx. mPas (cSt) D/d<br />
Cross-arm stirrer Shea flows in several<br />
fields, medium viscous<br />
liquids, good exchange of<br />
heat<br />
400 ... 800 tangential 10,000 1.1 ... 2<br />
Slanted blade good axial mixing effect , 500 ... 2500 radial 1,000 2.5 ... 3.5<br />
stirrer<br />
shear flow, prevention of<br />
layer build-up<br />
Grating stirrer Medium viscosity, strong<br />
shear flow, good<br />
exchange of heat<br />
200 ... 700 tangential 5,000 1.4 ... 2<br />
Paddle stirrer Low rotation speed, strong 20 ... 100<br />
shear flow, very sparing at<br />
low rotation speeds<br />
tangential 100 1.5 ...3<br />
Helical ribbon Powerful shear flow, for 50 ... 200 axial 50,000 1.1 ... 1.5<br />
stirrer<br />
high-viscous liquids,<br />
suspensions, pastes<br />
**with D of approx. 20 cm<br />
The stated values do strongly vary within literature<br />
by more than one order of magnitude <strong>and</strong> are used<br />
for a first orientation. Our project department will<br />
gladly help you to find a suitable stirrer-drive.<br />
To help you, we require the following information<br />
Order Code Description<br />
IR-RBL-rt-rd-ws-wl-wd Stirrer blade<br />
rt = stirrer type:<br />
AN Anchor stirrer<br />
PR Propeller stirrer<br />
SC Plane or turbo stirrer<br />
IP Impeller stirrer<br />
MI MIG-stirrer<br />
ZA Toothed disc stirrer<br />
TU Turbine stirrer<br />
KR Cross arm stirrer<br />
ST Slant blade stirrer<br />
GI Grating stirrer<br />
BL Paddle stirrer<br />
SP Spiral stirrer<br />
rd = blade diameter in mm (d)<br />
ws = material:<br />
ES Stainless steel<br />
EG Glass coated stainless steel<br />
GL Glass<br />
wl = shaft length<br />
wd = shaft diameter<br />
Ordering example:<br />
Anchor stirrer of glass, diameter 15 cm, shaft<br />
diameter 10 mm, shaft length 30cm<br />
Order code: IR-RBL-AN-150-GL-300-10<br />
from you:<br />
Stirrer type used, rotation speed, viscosity (or<br />
comparative information like water, motor oil,<br />
honey ...), mixing pot D, used stirrer D.<br />
Projecting Aide:<br />
Estimation of Viscosity<br />
Material Viscosity in mPas<br />
approx. at 20 ° C<br />
Acetone 0.33<br />
Alcohol 0.6<br />
Benzene 0.65<br />
Water 1<br />
Liqueur 3<br />
Condensed milk 7,5% 12<br />
Condensed milk 10% 45<br />
Olive oil 80<br />
Edible oil 85<br />
Apple juice concentrate 300<br />
Egg liqueur 600<br />
Yogurt 900<br />
Glycerine 1,500<br />
Honey 2,000-10,000<br />
Mustard <strong>11</strong>,000<br />
Print colours 100,000 – 100 Mill.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
ViscoGraph – Automation of <strong>Stirring</strong> Tests<br />
ViscoGraph allows the automation of stirringtechnological<br />
tests with the ViscoPakt Torque<br />
Measurement Stirrer.<br />
The Programme enables:<br />
� Measurement of the torque in dependency of the<br />
speed<br />
� User-defined Torque Profiles<br />
� Measurement of the Viscosity<br />
� Zero Torque Calibration<br />
With the buttons on the left, it is possible to call up<br />
the various functions of ViscoGraph. The current<br />
values of the test period, rotation speed etc., are<br />
presented in the view boxes.<br />
The diagrams present the procedure of speed <strong>and</strong><br />
torque via the time.<br />
The speed profile can be defined via up to 10<br />
sampling points:<br />
it is possible to select for each speed sampling point,<br />
if the speed is approached via a jump or a ramp:<br />
The data is stored in the *.csv format <strong>and</strong> can<br />
undergo further processing with programmes such<br />
as MS-Excel.<br />
The measurement system can be extended by<br />
further measurement variables with the help of the<br />
digital measuring amplifier.<br />
The additionally captured measurement curves<br />
receive an own Y-axis in the diagram.<br />
Order Code Description<br />
SL-VISCOGRAPH ViscoGraph Control Software for automated Operation of ViscoPakt Measuring Stirrers<br />
SL-VISCOGRAPHAI ViscoGraph Control Software Upgrade for Voltage Measurement with IL-AINAMP1D<br />
SL-VISCOGRAPHPT ViscoGraph Control Software Upgrade for Temperature Measurement with I IL-PTAMP1D<br />
IL-AINAMP1D Digital Measuring Amplifier for -10...+10V, 0/4...20mA, RS232 V24 /RS485 Interface<br />
IL-PTAMP1D Digital Measuring Amplifier for Pt100 Four-Wire Technology, RS232 V24 /RS485 Interface<br />
IL-NGSAMP1D-SN Power supply for digital measuring amplifier HK-GRADOAMP1D, HK-AINAMP1D, HK-PTAMP1D<br />
HC-USB232 USB to RS232 converter<br />
Customer-specific adjustments <strong>and</strong> extensions are possible.<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/910 100 · info@hitec-zang.de · http://www.hitec-zang.com 13
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<strong>Stirring</strong> <strong>and</strong> <strong>Dispersing</strong><br />
<strong>Dispersing</strong> <strong>and</strong> Homogenising<br />
Drives<br />
These high-performance drives for laboratory<br />
applications meet all requirements to modern <strong>and</strong><br />
compact laboratory drives <strong>and</strong> represent a<br />
guarantee for safe <strong>and</strong> successful working in the<br />
laboratory.<br />
Together with the accessories, you already dispose<br />
of a wide application range:<br />
� Homogenisation<br />
� <strong>Dispersing</strong><br />
� Emulsifying<br />
� Suspending<br />
This can be utilised for the preparation of analyses<br />
as well as in reactor acceleration.<br />
The rotational speed of the drives can be adjusted<br />
continuously up to 35,000 rpm.<br />
The exchange of tools is fast <strong>and</strong> uncomplicated<br />
with the patented tool receptacle system.<br />
Tools<br />
The tools consist of rotor <strong>and</strong> stator. The rotor<br />
geometry generates a strong pumping effect. Due to<br />
this, the media is suctioned into the operational<br />
range between rotor <strong>and</strong> stator. Here, high<br />
frequency vertical <strong>and</strong> horizontal pulsations are<br />
generated. Due to the high exit speeds, ultrasonic<br />
frequencies are generated at the stator slits. This<br />
leads to cavitation.<br />
A balanced interaction between shear forces <strong>and</strong><br />
percussion effects transfers the the liquid media<br />
intended for processing into the finest state. This<br />
significantly shortens process periods <strong>and</strong> reduces<br />
the heat input.<br />
The tools are made of acid-resistant high-grade<br />
steel 316L. They can be sterilised <strong>and</strong> are<br />
autoclaveable.<br />
The special shaft geometry enables fast tool<br />
exchange. PTFE rings prevent the medium from<br />
rising into the shaft tube.<br />
Drive 350 Watt Drive 1400 Watt Tool<br />
Order Code Description<br />
IR-DISPANTR350 Drive 350Watt, up to 35,000 rpm, for dispersing tools<br />
IR-DISPANTR750 Drive 750Watt, up to 35,000 rpm, for dispersing tools<br />
IR-DISPANTR850 Drive 850Watt, up to 35,000 rpm, for dispersing tools<br />
IR-DISPANTR1400 Drive 1400Watt, up to 35,000 rpm, for dispersing tools<br />
IR-DISPWZ040 <strong>Dispersing</strong> tool with quick coupling, diameter 4 mm<br />
IR-DISPWZ063 <strong>Dispersing</strong> tool with quick coupling, diameter 6.3 mm<br />
IR-DISPWZ140 <strong>Dispersing</strong> tool with quick coupling, diameter 14 mm<br />
IR-DISPWZ200-G <strong>Dispersing</strong> tool with quick coupling, coarse, diameter 20 mm<br />
IR-DISPWZ40-F <strong>Dispersing</strong> tool with quick coupling, fine, diameter 20 mm<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor