HiTec Zang GmbH -- Main Catalogue 2009/10
HiTec Zang GmbH -- Main Catalogue 2009/10
HiTec Zang GmbH -- Main Catalogue 2009/10
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<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> • Ebertstrasse 30-32 • 52134 Herzogenrath • Germany<br />
General Office: +49 (0) 24 07 / 9<strong>10</strong> <strong>10</strong>0 • Fax: +49 (0) 2407 / 9<strong>10</strong> <strong>10</strong>99 • Internet: www.hitec-zang.com
Usage notes<br />
The informations within this catalog kann be reached via these indexes:<br />
Table of content 348<br />
Order codes 339<br />
To make the selection and combination of needed components easy, we assembled a couple of turnkey<br />
solutions and packages which are suitable for default applications:<br />
Basic automation systems 72<br />
Software packages 176<br />
Turnkey laboratory/minplant system 6<br />
Turnkey reaction calorimetery 28<br />
Parallel Reactor Systems 14<br />
Reactor Systems for Education 20<br />
Furthermore you will find overviews as charts for the following areas:<br />
Which signal type accords to which device? 83<br />
Which Modules for which Signal Type? 86<br />
Cables for Instrumentation <strong>10</strong>7<br />
Driver Programs for Laboratory Device Interfaces 1<strong>10</strong><br />
Which Proportional Valve for which Application? 220<br />
Which Pump for which Application? 269<br />
Which Stirrer Blade for which Application? 329<br />
If you notify us of your project details we will be happy to prepare the required components for you.<br />
To reach us directly:<br />
Department Phone +49(0)2407/9<strong>10</strong> - E-Mail<br />
Information -<strong>10</strong>12 info@hitec-zang.de<br />
Sales -<strong>10</strong><strong>10</strong> sales@hitec-zang.de<br />
Service -<strong>10</strong>26 service@hitec-zang.de<br />
Software -<strong>10</strong>17 software@hitec-zang.de<br />
Hardware -<strong>10</strong>14 hardware@hitec-zang.de<br />
Subject to technical changes, errors and misprints<br />
Windows 2000, Windows XP, Windows Vista and Teflon are registred trademarks.<br />
© <strong>2009</strong> <strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong><br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 3
4<br />
New in this Edition<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Here you will find:<br />
Automatic Laboratory Reator Systems<br />
� Standard LabKit Laboratory Reactor Systems<br />
� HiClave high-pressure autoclaves<br />
� MulitLab Parallel Reactor Systems<br />
� LabKit-ed Small Reactor Systems for Training Purposes<br />
� Laboratory Clarification Unit<br />
� Microreaction Technology<br />
Note:<br />
Custom made plants can be found in the chapter „Plant Construction and Miniplant Technology“.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 5<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
6<br />
Automatic Laboratory Reactor Systems<br />
Standard Laboratory Reactor Systems<br />
Automated laboratory reaction systems are an<br />
absolute necessity for today's product and process<br />
development and optimisation. Due to the much<br />
more intensive utilisation of the laboratory resources<br />
and the relief of the laboratory staff from routine<br />
activities, they pay off very quickly. They are a save<br />
way to achieve maximum reproducibility as well as<br />
an increase in quality and to gain new knowledge.<br />
Conventional laboratory reactor automation<br />
systems are limited to simple syntheses and are<br />
therefore no longer able to meet today's<br />
requirements.<br />
The fully-automateded <strong>HiTec</strong> <strong>Zang</strong> laboratory<br />
reactor systems are available as single and parallel<br />
reactor plants. Apart from the standard<br />
configurations, you can choose the set-up of the<br />
plant which accords to your demands from our<br />
LabKit program.<br />
Advantages:<br />
� easy to handle open system<br />
� NAMUR-conform automation with LABmanager/LabVision/HiBatch/HiLIMS<br />
� continuously expandable<br />
� space saving installation<br />
� electrically sinkable reactor vessel<br />
� optimal usage of the laboratory‘s capacity by<br />
operating 24 hours<br />
� best reproducibility<br />
� increase in quality<br />
� relief from routine jobs<br />
� reduction of the risk of accidents<br />
� GLP-compliant documentation<br />
� accessible via network, e.g. from the office<br />
� remote maintenance (dial-up by customer)<br />
Last fine-tuning before delivery<br />
<strong>HiTec</strong> <strong>Zang</strong> ALR-Systems are suited for the<br />
� Development of products and procedures<br />
� Optimisation of procedures<br />
� Safety-related tests<br />
� Scale-Up tests<br />
� Reaction calorimetry etc.<br />
The assembly of a laboratory reactor system out of<br />
individual components, e.g. out of a pH-controller, a<br />
dosing control, a vacuum controller, data collection,<br />
a control element, etc. used to be considered the<br />
best possible assembly. The capacity limits of such a<br />
conventional assembly are clearly demonstrated by<br />
LabKit due to its NAMUR-conform automation<br />
based on the LAB Manager System.<br />
Sophisticated details, such as the lowerable reactor<br />
tank, facilitate work.<br />
Options, Extensions<br />
Sensors for filling level, opacity, flow, pH, redox etc.,<br />
coupling of analysers etc., out of the chapter<br />
“Process Analytics and Sensors”, in-situ analytics,<br />
coupled multiple reactor systems, customer-specific<br />
machines out of the chapter “Customised Equipment<br />
and Miniplants” – the offered possibilities are<br />
virtually limitless.<br />
Standard systems<br />
The following depicted standard systems LabKitalr1,<br />
LabKit-alr2, LabKit-rcf, LabKit-rcb, LabKit-ed,<br />
and HiClave are complete, ready-to-use Automatic<br />
Laboratory Reactor Systems (ALR). They are suited<br />
for deployment in laboratories, pilot plants and miniplants.<br />
They can be aligned according to spacial<br />
conditions and upgraded by auxiliary modules.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Automatic Laboratory Reactor Systems<br />
LabKit-alr1 Standard-ALR-System<br />
Automatic lab reactor system in the basis version.<br />
Suitable for syntheses in a temperature range<br />
reaching from -<strong>10</strong> to +130 °C with reflux distillation.<br />
The system can be expanded with components from<br />
the LabKit-Construction Systems.<br />
Specification<br />
LabKit-alr1 ALR-standard system<br />
Rack Square section anodised aluminium profile.<br />
Reactor 1 litre plane ground container DN<strong>10</strong>0, cylindrical with heating jacket and manual PTFE<br />
base drain.<br />
Plane ground cover with centre neck NS29 for stirrer, side necks 2xNS29 slanted and<br />
1xNS29 straight, Seal DN120 Silicon/FEP, plane ground connector.<br />
Stirrer ViscoPakt-35 torque measuring stirrer, rotational speed 60..800 rpm, maximum torsion<br />
35 Ncm, including the optional RS232 interface.<br />
Accessories: light and high-strength stirrer coupling made of POM, standard agitator<br />
Heating/Cooling<br />
System<br />
closure, glass propeller stirrer.<br />
Heating/ cooling thermostat, working temperature range -25..150 °C in jacket, heating<br />
output 1 kW, refrigerating capacity 0.21 kW at 0 °C.<br />
Accessories: isolated heating tubes, heating connection adaptors, wide range<br />
tempering oil -40..165 °C.<br />
Dosing System A GraviDos Dosing System for liquids (regulated dropping funnel), 500 ml receiver<br />
tank, dosing valve (ETFE/Kalrez) controlled gravimetrically.<br />
Reflux cooling Intensive reflux cooler made of borosilicate glass, 250 mm long, NS29/32,<br />
Shutting valve for cooling water.<br />
Ventilation Air valve PVDF/Kalrez).<br />
Sensors Temperature sensor: Reactor internal temperature, thermostat bath temperature.<br />
Automation LabBox 1 with the following interfaces: 4 Pt<strong>10</strong>0 temperature measurement inputs, 4<br />
analogue inputs (current and voltage), 8 digital outputs, Sensor-/Actor power supply<br />
24 V 2.5 A, 2 RS232 interfaces.<br />
User PC : 1 CG-ABK1 <strong>HiTec</strong> display and control elements with premium 20“ TFT<br />
monitor.<br />
Materials <strong>Main</strong>ly borosilicate glass, PFA, PTFE, ETFE, PVDF. Seals in contact with media made<br />
of Kalrez, high-grade steel material 1.4571 (modifications possible).<br />
Order Code Description<br />
VL-LABKITALR1 Automatic Laboratory Reactor System, Basic Design<br />
Recommended software package<br />
Order Code Description<br />
SL-LABVIPBATL Software Package for LabBox1 and 2 to control small Batch Processes<br />
SF-PID4 Controller module with 4 PID- and application oriented controllers<br />
Recommended datapoint amount: <strong>10</strong>0<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 7<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
8<br />
Automatic Laboratory Reactor Systems<br />
LabKit-alr2 Standard-ALR-System<br />
Automatic Lab Reactor System in extended<br />
configuration. Suitable for syntheses in the<br />
temperature range from -20 to +180 °C with reflux<br />
distillation via programmable reflux separators.<br />
The system can be expanded with components from<br />
the LabKit-Construction Systems.<br />
Specification<br />
LabKit-alr2 ALR-Standard System with optional Modules<br />
Rack Square anodised aluminium profile, electrical fixture for lowering the reactor vessel,<br />
catch pan made of high-grade steel.<br />
Reactor 2 litre reactor with double jacket DN150, Duran glass, PTFE base drain with<br />
integrated PT<strong>10</strong>0 sensor, plane ground cover, seals Silicon/FEP, plane ground<br />
connector<br />
Stirrer Torque measuring stirrer ViscoPakt-rheo-57, rotational speed 50..2000 rpm,<br />
maximum torsion 57 Ncm, including the optional RS232 interface<br />
Accessories: light and high-strength stirrer coupling made of POM, standard agitator<br />
closure, glass propeller stirrer<br />
Heating/Cooling<br />
System<br />
Heating/cooling thermostat especially for tempering of external systems, working<br />
temperature range -40..200 °C in the jacket, heating output 1.5/3 kW, cooling<br />
capacity 0.7 kW at 0 °C<br />
Accessories: isolated heating tubes, heating connection adaptors, wide range<br />
tempering oil -90..200 °C<br />
Vacuum Laboratory vacuum system with chemical resistant vacuum pump < 8 mbar abs.,<br />
volume flow rate 1 m³/h, suction side separator, pressure side intensive cooler, safety<br />
valve<br />
Reflux Cooling Intensive reflux cooler out of borosilicate glass, 250 mm long, NS29/32<br />
Shutting valve for the cooling<br />
Monitoring of cooling water with floating-element meter<br />
Distillation distillate collecting scales, instrument read-out 0.01 g, weighing range 15<strong>10</strong> g<br />
2/2- way stop cock to shut off distillate collecting container and the pressure<br />
compensation.<br />
Optional: Glass reflux separator with vacuum jacket, silver-plated with viewing<br />
window, NSH+K 29/32 with PT<strong>10</strong>0 connector GL14, discharge GL14<br />
Ventilation Air escape valve (ETFE/Kalrez)<br />
Inerting Inerting valve (ETFE/Kalrez), pressure regulator from maximum 16bar to 0..1bar<br />
Dosing System A GraviDos Dosing System for liquids (regulated dropping funnel), 500 ml receiver<br />
tank, dosing valve (ETFE/Kalrez) controlled gravimetrically<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Automatic Laboratory Reactor Systems<br />
Sensors Temperatures: reactor interior space, thermostat, flow, return flow, steam dosing<br />
medium Reactor interior pressure, pH-value<br />
Automation LABbox2 with the following interfaces: 8 Pt<strong>10</strong>0 temperature measurement inputs, 8<br />
analogue inputs (Current & Voltage) of which 1 pH, 3 RS232, 4 GraviDos (DMS)<br />
Interfaces, 4 digital inputs, 8 digital outputs, 2 of which for 230 V connected sockets.<br />
Sensor power supply 24 V 1,5 A, actor power supply 24 V 3 A.<br />
User pc, 1 CG-ABK2 <strong>HiTec</strong> display and control element with premium 22“ TFT<br />
monitor, uninterrupted power supply and UPS management system<br />
Materials <strong>Main</strong>ly borosilicate glass, PFA, PTFE, ETFE, seals in contact with media made of<br />
Kalrez, high grade steel material 1.4571 (modifications possible)<br />
Dimensions D x W x H: 56 x 80 x 150 cm<br />
Order Code Description<br />
VL-LABKITALR2 Automatic Laboratory Reactor System, 2 Dosing Circuits, Reflux Boiling, Vacuum Distillation,<br />
Vacuum Control, Inerting, Stirrer Torque Measurement<br />
VL-LABKITALR2-AWE Collection plate made of high-grade steel<br />
VL-LABKITALR2-RFT Column and magnetc glas-reflux seperator with vaccuum jacket<br />
Recommended Software Package<br />
Order Code Description<br />
SL-LABVIPBATE Economy software package for LabBox2 and LabManager1 for batch operation<br />
SF-PID8 Controller module with 8 PID- and application oriented controllers<br />
Recommended datapoint amount: <strong>10</strong>0<br />
For high pressure reaction, in particular at multiphase<br />
systems, the HiClave laboratory pressure<br />
reactor systems have proven themselves to be a<br />
suited solution.<br />
They cover the volume range from <strong>10</strong> to 250 ml at a<br />
maximum pressure up to 300 bar and a maximum<br />
temperature of up to 300°C. Due to the pure metal<br />
cover gasket, the system is able to reach a tightness<br />
which enables highly precise gas consumption<br />
measurements. Up to 7 reactor connections are<br />
possible. At the reactors as of <strong>10</strong>0 ml content, the<br />
<strong>HiTec</strong> <strong>Zang</strong> Pressure Reaction Systems are suited<br />
for<br />
� Hydrogenation<br />
� Oxidations<br />
� Carbonylation<br />
� Polymerisation<br />
and further processes.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 9<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
<strong>10</strong><br />
Standard Systems<br />
Automatic Laboratory Reactor Systems<br />
HiClave plants dispose of a modular construction.<br />
The standard systems depicted in the following<br />
represent the basis for pressure reaction systems<br />
suited for a multitude of applications. They are<br />
adjustable to the respective requirements and can<br />
be equipped with the offered additional modules and<br />
components.<br />
Pressure Reactor System with Gassing and Balancing<br />
<strong>10</strong> ml and 20 ml Reactors<br />
Equipment<br />
The <strong>10</strong> ml and 20 ml reactors have<br />
a cover with cap nut and a central<br />
media connection with four-way<br />
connector. The middle connection<br />
of the four-way connector is<br />
allocated with the interior<br />
temperature sensor, the lateral<br />
ones usually with media connection<br />
and the manometer.<br />
The reactors tempered with a<br />
magnetic heating stirrer with<br />
heating block and agitated by a<br />
kinetic stirring rod.<br />
� Simple heating and stirring via a magnetic<br />
heating stirrer and a heating block attachment<br />
� Temperature Sensor (Pt<strong>10</strong>0)<br />
Pressure Reactor 20 ml, heated and agitated with Magnetic<br />
Stirrer; on the right: Reactor with fibre-optic ATR Sensor<br />
Connection Options<br />
� 1 x Temperature Sensor<br />
� 1 x Pressure Gauge<br />
� 1 x Media Connection<br />
Options<br />
� Other Connection Assignments<br />
50 ml Reaktor<br />
The 50 ml reactor a<br />
cover with cap nut<br />
and 3 connections.<br />
One of these can be<br />
equipped with a<br />
magnetic stirrer drive.<br />
The stirrer is passed<br />
through eccentrically.<br />
The other two<br />
connections are for<br />
the thermal sensor<br />
and and the media<br />
feed. If the stirrer<br />
drive is omitted in<br />
favour of magnetic<br />
stirrer, the now free<br />
connection can now<br />
be freely assigned.<br />
The reactors are<br />
heated via a heating<br />
sleeve and stirred<br />
overhead. In this<br />
case, the cooling can<br />
be conducted via a<br />
plate cooler.<br />
Alternatively, it is<br />
possible to heat and<br />
stir with a magnetic heating stirrer and heating block.<br />
Equipment:<br />
� Heating via Heating Sleeve<br />
� Stirring via Magnetic Stirring Head<br />
� Temperature Sensor (Pt<strong>10</strong>0)<br />
Connection Options<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
<strong>10</strong>0...250 ml Reactor<br />
Automatic Laboratory Reactor Systems<br />
The <strong>10</strong>0...250 ml rector<br />
have a flange cover with 7<br />
connections bolted by<br />
extension bolts. For better<br />
access, three of these<br />
connections have been<br />
placed on the outer side of<br />
the cover. The central<br />
nozzle is assigned with the<br />
magnetic stirrer head. The<br />
reactor is available in a<br />
high grade steel or<br />
Hastelloy version.<br />
The reactors are heated<br />
via a heating sleeve and<br />
can optionally be cooled<br />
by either a plate heater or<br />
an internal cooling circuit.<br />
The stirring is conducted<br />
with a magnetic stirring<br />
head, optionally either with<br />
a maximum torque of 20<br />
Ncm or 50 Ncm. The<br />
according fitting kits are available in high grade steel<br />
1.4571 (SS 316Tl) or in Hastelloy C4.<br />
Connection Options<br />
� 1 x Immersion Pipe for Temperature Sensor<br />
� 1 x Stirrer<br />
� 1 x Burst Disc made of metal for the safe<br />
limitation of the maximum pressure<br />
� 1 x Pressure Gauge<br />
� 1 x Valve for Pressure Release<br />
� 2 x freely assignable, e.g. for gas or liquid<br />
sampling<br />
Options<br />
� Hydrogenation/Gassing Module<br />
� Liquid and/or Gas Sampling<br />
� Cooling via Plate Cooler or Cooling Circuit<br />
� Hastelloy Version<br />
Hydrogenation Module<br />
The Hydrogenation Module VL-HICLAVE-HYDR<br />
enables the realisation of the complete<br />
hydrogenation process, including the inert gas<br />
rinsing and leak test of the reactor, without manual<br />
intervention. For this reason, there is no need for<br />
anyone to be in the risk area of the reactor while the<br />
same is under pressure. For this purpose, the<br />
reactor is charged with up to regulable pressure with<br />
inert gas an subsequently vented. This rinsing<br />
process can be repeated as often as required.<br />
Subsequently, a pressure test with inert gas will be<br />
conducted. The testing period and tolerance for<br />
passing the test must be entered.<br />
Only if the pressure test has been passed, will the<br />
reaction gas – in the upper example hydrogen – be<br />
released. Otherwise, the reactor is vented. In the<br />
next step, a rinsing with reaction gas is conducted,<br />
the setpoint pressure is established, and the<br />
reaction is started.<br />
A gas consumption measurement for the capture of<br />
kinetic data is integrated. The gas consumption can<br />
also be utilised as an abort criteria, i.e. the reaction<br />
is interrupted if the consumption has decreased<br />
below a predefined rate.<br />
a.) Parameter Template for Pressure Reactions b.) Protocol of a<br />
Pressure Reaction. Evaluation after a Pseudo First Order Kinetic.<br />
Automation<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 11<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
12<br />
Automatic Laboratory Reactor Systems<br />
The plant is monitored and operated via a selfexplanatory<br />
user interface. The measurement data<br />
are automatically captured and recorded in a<br />
Versions<br />
protocol. If a gas consumption measurement has<br />
been conducted, it is also possible to realise a<br />
kinetic evaluation of the consumption curve.<br />
Frame Square aluminum profile, anodised. High Grade Steel Platform.<br />
Reactor <strong>10</strong>...250 ml- High Grade Steel Reactor (opt. Hastelloy), 300 bar, 300°C. Optional<br />
450°C<br />
Stirrer Stirrer with magnetic coupling, Speed: 200..1500 rpm, Maximum Torque:20/50 Ncm,<br />
including analogue interface (Reactors ≥ 50ml).<br />
Or: Magnetic Heating Stirrer with Heating Block and Magnetic Stir Bar (Reactors ≤ 50<br />
Heating /Cooling<br />
System<br />
ml)<br />
Heating Sleeve/ Plate Cooler (alternatively Cooling Circuit), Operating Temperature<br />
Range:40..350°C in Jacket, Heating Output 700W. Or: Magnetic Heating Stirrer with<br />
Heating Block<br />
Sampling Manual with Sampling Valve<br />
Gassing Reaction gas pressure-controlled via MFC, including gas consumption measurement,<br />
by-pass valve.<br />
Inertisation Inert gas pressure-controlled. Exhaust via high pressure magnetic valve, burst disc.<br />
Dosing System, GraviDos High Pressure Dosing System. Optional High Pressure Pump and Scales.<br />
gravimetrically<br />
controlled<br />
Sensorics Temperatures: Reactor Interior Temperature, Jacket Temperature, Reactor Interior<br />
Pressure, Speed, ATR-FTIR.<br />
Automation For Example for two Autoclaves:<br />
LabBox2 with the following Equipment:<br />
Interfaces: 4 Pt<strong>10</strong>0 Temperature Measurement Inputs, 4 analogue Inputs (current and<br />
voltage), 4 RS232 Interfaces (Stirrer, Hydrogation Module), 4 GraviDos Connections, 8<br />
digital Outputs, of these 2 for Power Sockets switched to 230 V.<br />
Sensor Power Supply24V 1,5 A, Actor Power Supply 24V 3A.<br />
2 Safety Temperature Monitors.<br />
Workstation: 1 CG-ABK1 <strong>HiTec</strong> Display and Operating Component with high quality<br />
20“ TFT Monitor, Uninterrupted Power Supply and UPS Management System.<br />
This automation system is able to control 2 reactors.<br />
The extension to 4 reactors is possible.<br />
Materials <strong>Main</strong>ly High Grade Steel1.4571, other High Grade Steels, Hastelloy.<br />
Order Code Description<br />
VL-HICLAVE-SC-n Frame for HiClave Pressure Reactors, Piping, Sensorics, gravimetr. Dosing Unit 150ml<br />
VL-HICLAVE-ws-vol HiClave Pressure Reactor according to Specification ws-vol<br />
VL-HICLAVE-HEABAN-vol Heating Sleeve, 230V AC, 500 Watt, Duplex Temperature Sensor<br />
VL-HICLAVE-COOLP Plate Cooler for <strong>Main</strong>s Water or Thermostat Connection<br />
VL-HICLAVE-STIRR-20 Magnet-coupled Overhead Stirrer, 20Ncm<br />
VL-HICLAVE-STIRR-50 Magnet-coupled Overhead Stirrer, 50Ncm<br />
VL-HICLAVE-MAGHEAT Magnetic Stirrer with Plate Heating<br />
VL-HICLAVE-HYDR Hydrogenation and Gassing Module for HiClave Pressure Reactors with Mass Flow<br />
Controller<br />
VL-HICLAVE-GRAVI150 Additional gravimetr. Dosing Unit 150ml for HiClave Pressure Reactors<br />
VL-HICLAVE-ABKPNK1 Automation Unit with 20´´ Monitor and Workstation and SL-LABVIPEASY Software Package<br />
30 DP, for one HiClave Unit with gravimetric Dosing, Dosing, Tempering, Hydrogenation<br />
VL-HICLAVE-ABKPNK2 Automation Unit with 20´´ Monitor and Workstation and SL-LABVIPEASY Software Package<br />
<strong>10</strong>0 DP, for two HiClave Units with gravimetric Dosing, Dosing, Tempering, Hydrogenation<br />
VL-HICLAVE-ABKPNK4 Automation Unit with 20´´ Monitor and Workstation and SL-LABVIPEASY Software Package,<br />
300 DP for four HiClave Units with gravimetric Dosing, Dosing, Tempering, Hydrogenation<br />
n ( = Number of Reactors): 1 to 8<br />
ws ( = Material): High Grade Steel 1.4571 (SS 316Tl): e, Hastelloy C4: h, Special Material s<br />
vol ( =Operating Volume): <strong>10</strong>, 20, 50, <strong>10</strong>0, 150, 250 accordingly <strong>10</strong>, 20, 50, <strong>10</strong>0, 150 or 250 ml<br />
Special Designs, e.g. other volumes, connections, materials etc. are available upon request. Alternative<br />
dosing units can be found under the Section „Dosing Systems and Pumps“.<br />
Do you have Questions? Do not hesitate too ask!. Our project engineers will gladly help!<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Automatic Laboratory Reactor Systems<br />
Parallel Reactor Systems<br />
Reaching Objectives faster with the automated Parallel Synthesis<br />
The pressure to maximise productivity in the<br />
laboratory is consistently growing. At the same time,<br />
however, the demands on quality are also<br />
increasing.<br />
Standardised and client-specifically customised<br />
<strong>HiTec</strong> <strong>Zang</strong> parallel reactor systems are the answer<br />
to the increasing demands:<br />
� Shortened „Time to Market“<br />
� Improved Quality<br />
� Increased Reproducibility<br />
� Lower Costs<br />
You can ensure these advantages by:<br />
� Eliminating shortages through parallel<br />
operation<br />
� 24-hour, 7 day operation<br />
� Relief from routine activities<br />
� Optimal documentation and protocoling<br />
The <strong>HiTec</strong> <strong>Zang</strong> parallel reactor systems MultiLab<br />
and MiniLab significantly support and expedite<br />
research and development processes in the<br />
chemical and pharmaceutical industry. The flexibility<br />
of the parallel reactor systems overcomes the<br />
throughput restrictions of today's research and<br />
development processes.<br />
They help in shortening the “time-to-market” by<br />
expediting the optimisation processes for synthesis<br />
and alignment via the parallelisation of experiments<br />
and sophisticated automation and software<br />
solutions. Due to the possibility of unattended<br />
operation, the efficiency and the instrument<br />
utilisation is raised. All devices support batch, semibatch,<br />
continuous and multistage processes.<br />
With the parallel reactor systems, you are able to<br />
repeatedly and in parallel conduct experiments in<br />
great numbers and, consequently, decisively<br />
expedite the work process. By this, you save time,<br />
increase the efficiency and the capacity of your<br />
laboratory.<br />
The test conditions, such as temperature, pressure<br />
and pH-value may differ for every reactor.<br />
In case of the innovative tempering systems of the<br />
MultiLab and MiniLab, the otherwise usual tempering<br />
block for multi-reactor systems was intentionally<br />
omitted. Both systems allow a clear view into the<br />
reactor.<br />
The systems are suited for<br />
� Synthesis<br />
� Polymerisation<br />
� Distillation<br />
� Extraction<br />
� Crystallisation etc.<br />
Automation<br />
They neither restrict the creativity, nor do they<br />
require a specialist to operate. The user has full<br />
control over all system parameters all the time.<br />
All labour-intensive steps, from the planning of the<br />
experiment to the evaluation and documentation of<br />
the experimental data, are supported or completely<br />
automated. Even complex recipes can be<br />
established in a few minutes by combining the basis<br />
operations with the graphic HiBatch Recipe Editor.<br />
A recipe can be allocated to several reactors and<br />
individually parameterised. Due to this, the time and<br />
work expenditure even remains minimal when<br />
extensive parallel experiments are conducted.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 13<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
14<br />
Automatic Laboratory Reactor Systems<br />
MultiLab Multi-Reactor System<br />
MultiLab is a miniaturised fully automated laboratory<br />
reactor system. Therefore, any reaction that is<br />
usually conducted on the litre scale can now be<br />
carried out in the 250 or 400 ml MultiLab reactor<br />
under realistic plant conditions, fully automated and<br />
controlled independently by a <strong>HiTec</strong> <strong>Zang</strong><br />
LabManager with the leading LabVision laboratory<br />
automation software.<br />
MultiLab is a modular system and still flexible. It is<br />
available in a great variety ranging from the<br />
manually operated basis version to the individually<br />
configurable fully automated multi-reactor system.<br />
Even complex processes with educt pre-treatment,<br />
synthesis, reaction monitoring, and product postprocessing,<br />
as well as automatic sample drawing is<br />
possible.<br />
The special characteristic of the MultiLab parallel<br />
reactor system is its innovative tempering system. A<br />
high-grade steel spiral/coil holds the reactor<br />
temperature and cools, respectively heats the same,<br />
if necessary.<br />
MultiLab is suitable for all common processes:<br />
� Synthesis<br />
� Polymerisation<br />
� Distillation<br />
� Extraction<br />
� Crystallisation etc.<br />
Features<br />
� Modular compact design<br />
� Convenient and fast handling (exchange of a<br />
reactor in less than one minute)<br />
� Independent control of each reactor<br />
� Proprietary groundbreaking tempering<br />
system enables unhindered sight into the<br />
reactor<br />
� Only one chiller for multiple individually<br />
tempered reactors<br />
� Multiple dosing options (liquid, solid and<br />
gaseous, gravimetric and volumetric)<br />
� Automated sampling options<br />
� Fully automated control of reactor conditions<br />
like feed rates, temperature, pressure, pH and<br />
agitation<br />
� Multiple systems controlled by a single PC<br />
with a LAB Manager, LabVision and HiBatch<br />
recipe control software<br />
� 24 hour unattended operation<br />
� Inert construction materials: glass, PTFE<br />
� Individually expandable and upgradeable<br />
Easy Handling<br />
The exchangeable reactors of the MultiLab enable<br />
fast reaction to changing requirements. The unique<br />
and innovative heating/cooling system offers<br />
essential benefits. The glass vessel is electrically<br />
heated or cooled by a flow of cooling liquid out of a<br />
reservoir.<br />
Exchange of a reactor<br />
The reactor is released by actuating the release<br />
lever and can be removed after lifting the complete<br />
head construction.<br />
The temperature of the coil is registered and<br />
controlled and, in addition, can be limited, if<br />
necessary. For reactor volumes ranging from 75 to<br />
250 ml, the MiniLab System is alternatively<br />
available.<br />
Options<br />
� Distillation<br />
� Controlled reflux<br />
� Solid and gaseous dosing<br />
� Electric bottom outlet valve<br />
� Phase detection and separate bottling of<br />
organic/inorganic phase<br />
� ATR-FTIR online Monitoring<br />
� Automatic sampling and many more options<br />
� further options available upon request<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Module Description<br />
Automatic Laboratory Reactor Systems<br />
Module Basic Unit Equipment<br />
(common components of all<br />
reactors)<br />
Components per Reactor<br />
(one unit required for each reactor)<br />
Basic Module Tempering unit, rack with reactor lift,<br />
glas cover, 1 x NS29, 4 x NS19,<br />
high-grade steel quick release<br />
fastener, GL25 connection, anker or<br />
tilted blade stirrer, cardan shaft,<br />
sealing, vacuum-sealed, max.<br />
temperature 250 °C (monitor cooling<br />
media!), min. temperature<br />
dependant of thermostat. inside<br />
temperature sensor PT<strong>10</strong>0 PTFE<br />
coated, cables for stirrer and<br />
thermostat<br />
Vessel Reactor 250 ml, DN60, borosilicate<br />
glass, sealing silicone/FEP-coated<br />
Standard Cooling Unit Cooling thermostat -20 °C (flow<br />
temperature)<br />
Alternatives<br />
(other or extended features<br />
without specification)<br />
Reactor 400 ml<br />
base drain, manual base drain,<br />
electrical sensor sockets,<br />
electrical reactor lift,<br />
ViscoPakt -mini-rheo-35<br />
precision measurement stirrer,<br />
magnetic stirrer closure,<br />
propeller or impeller stirrer<br />
made of high-grade steel,<br />
glass thermometer, etc.<br />
Reactor 400 ml<br />
Cooling thermostat -40 °C.<br />
low temperature equipment :<br />
Cooling thermostat -60 °C,<br />
removable isolation jacket (per<br />
reactor)<br />
Reflux cooling Cooling water valve<br />
Cooling water monitor<br />
Dimroth cooler<br />
Distillation Distilling bridge<br />
Distillate weighing<br />
Pt<strong>10</strong>0 for steam temperature Additional cooler for reflux<br />
Collecting container for distillate cooling<br />
Rectification Hempel column 200 mm<br />
Vacuum jacket<br />
Micro column head according to Dr. Distillate weighing<br />
Kaminski, magnetically actuated Pt<strong>10</strong>0 in column<br />
Pt<strong>10</strong>0 column head<br />
Dimroth cooler<br />
Collecting container for distillate<br />
Filling material/Packages<br />
Vacuum Chemical-resistant vacuum pump Vacuum regulating valve<br />
Pressure sensor 0-1,6 bar<br />
Pressure relief valve<br />
Stronger vacuum pump<br />
Inerting Pressure regulator 16 bar to 0-1 Inerting valve, pressure relief valve<br />
bar<br />
1,3 bar<br />
Dosing Hanging scales Grado<strong>10</strong>00 Automatic refill<br />
Weighing container 500 ml<br />
Mounting panel for LabManager<br />
lateral refilling feed pipe<br />
(useful in case of more than 3<br />
Regulating valve<br />
modules)<br />
Other container sizes<br />
Volumetric Dosing Peristaltic pump Diaphragm, piston pumps,<br />
etc.<br />
Solid Dosing Solid doser SoliDos<br />
Inerting connection<br />
connection socket on to NS19 Inert gas heating<br />
pH-Measurement PH gel electrode pH 0-14<br />
lead-through 12 mm<br />
measuring amplifier pH<br />
Cover with sensor socket<br />
Redox-Potential Redox-electrode<br />
Cover with special sensor<br />
reference electrode<br />
socket (necessary at anchor<br />
lead-through 12 mm<br />
measuring amplifier mV<br />
stirrer!)<br />
Phase Limit Detection automatic base drain valve with Temperature measurement with<br />
Pt<strong>10</strong>0<br />
PhaDec phase limit detector<br />
regulating valve<br />
same Pt<strong>10</strong>0<br />
Gas Dosing Pressure regulator 16 bar to 0-1 Mass flow regulator<br />
bar<br />
Pressure relief valve 1,3 bar<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 15<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
16<br />
Automatic Laboratory Reactor Systems<br />
Order Code Description<br />
VL-MULTILAB-BU MultiLab multi reactor base module with tempering and stirrer unit and cover<br />
IR-VIPA-MINI-RHEO-35 ViscoPakt-rheo stirrer drive, 35 Ncm<br />
VL-MULTILAB-GRV250 MultiLab reaction vessel 250 ml, DN60, borosilcate glass, sealin silicon/FEP covered<br />
VL-MULTILAB-GRV400 MultiLab reaction vessel 400 ml, DN60, borosilcate glass, sealin silicon/FEP covered<br />
IR-RDFMAG8 Magnetic stirrer closing for 8 mm agitator<br />
VL-MULTILAB-CHILL-20 MultiLab cooling thermostat flow temperature -20 °C<br />
VL-MULTILAB-CHILL-40 MultiLab cooling thermostat flow temperature -40 °C<br />
VL-MULTILAB-CHILL-60 MultiLab cooling thermostat flow temperature -60 °C<br />
VL-MULTILAB-RFC MultiLab intensive reflux cooler<br />
VL-MULTILAB-DEST MultiLab destillation bridge, Pt<strong>10</strong>0 for fume temperature, catchment tank for destillate<br />
VL-MULTILAB-REKT MultiLab rectification attachment, Hempel-column 200 mm, micro column head magnetically<br />
activated, Pt<strong>10</strong>0 column head, Dimroth-cooler<br />
VL-MULTILAB-VAKU MultiLab vacuum control unit with vacuum control valve, pressure sensor 0-1,6 bar, pressure<br />
relief valve<br />
IP-B-V1-1200L-PTFE/FPM Chemical vacuum pump with alternating current motor 120W, 230V AC, 1200 l/h, end vacuum<br />
8 mbar, material PTFE/FFKM<br />
VL-MULTILAB-INERT MultiLab inerting unit with inerting valve and pressure control valve 1,3 bar<br />
IV-DRUMIN16/1 Pressure reducer 16 bar to 0-1 bar<br />
VL-MULTILAB-GRAVI500ml Gravimetric dosing module with hanging balance <strong>10</strong>00g, weighing vessel 500 ml, lateral refill<br />
nozle, control valve, cable<br />
VL-MULTILAB-ABKPNK1 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />
<strong>10</strong>0 data points for 1 MultiLab unit with 2 gravimetric dosing circuits, vacuum control,<br />
inerting, destillation/rectification<br />
VL-MULTILAB-ABKPNK2 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />
<strong>10</strong>0 data points for 2 MultiLab units with 2 gravimetric dosing circuits each, vacuum control,<br />
inerting, destillation/rectification<br />
VL-MULTILAB-ABKPNK4 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />
180 data points for 4 MultiLab units with 2 gravimetric dosing circuits each, vacuum control,<br />
inerting, destillation/rectification<br />
VL-MULTILAB-ABKPNK6 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />
300 data points for 6 MultiLab units with 2 gravimetric dosing circuits each, vacuum control,<br />
inerting, destillation/rectification<br />
VL-MULTILAB-ABKPNK8 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />
560 data points for 8 MultiLab units with 2 gravimetric dosing circuits each, vacuum control,<br />
inerting, destillation/rectification<br />
The VL-MULTILAB-ABKPNK automation unit is a<br />
complete set of Windows XP or Vista operating<br />
system, installed LabVision software package an d<br />
uninterruptable power supply.<br />
The automation unit can be buildt individually from<br />
our LabManager-, UI- and LabVision program.<br />
Recommended software package at individual selection:<br />
Order Code Description<br />
SL-LABVIPBAT Standard package "Batch" for LabManager1<br />
SL-MULTIBATCH HiBatch extension for parallel synthesis<br />
Recommended datapoint modules: 50 per MultiLab unit.<br />
Recommended PI-modules<br />
Recommended controller amount: 4 per MultiLab unit<br />
Further extensions:<br />
Solid dosing (SoliDos), gas dosing, volumetrik<br />
dosing (LabDos) pH- a. redox measurement<br />
(pHAmp) and controlling, clouding measurement,<br />
phase seperation (PhaSep), autosampling device<br />
(AutoSam) and other hard- and software options<br />
from our LabKit and LabVision program.<br />
Order Code Description<br />
SF-PID4 Controller module with 4 PID- and application oriented controllers<br />
Should you have any queries, our sales experts will gladly help you!<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Automatic Laboratory Reactor Systems<br />
MiniLab mini reactor system<br />
The <strong>HiTec</strong> <strong>Zang</strong> MiniLab parallel reactor system<br />
distinguishes itself by its particularly small „footprint“.<br />
It offers high-performance at minimal required<br />
space and best reproducibility due to automatic<br />
operation mode.<br />
MiniLab-Module with GraviDos Liquid Doser and ViskoPakt-MINI<br />
stirring drives.<br />
The downsizing of reactor mixtures offers the<br />
opportunity to accelerate development processes by<br />
parallel operation of experiments. At the same time,<br />
precious reactants and expensive laboratory space<br />
are saved. Very small mixtures can however be a<br />
problem in regard to reproducibility. For this reason,<br />
volumes of 75-250 ml are ideal for initial<br />
optimisations.<br />
MiniLab is based on a compact heating/cooling<br />
system. Unlike conventional hot plates, the<br />
tempering plate is also able to cool. The low thermal<br />
mass makes quick temperature changes possible. In<br />
the course of this, several stations can be supplied<br />
with cooling agent by one common cryostat.<br />
Reactors with different reaction volumes can be<br />
used in any combination.<br />
MiniLab is suitable for all common processes:<br />
� Synthesis<br />
� Polymerisation<br />
� Distillation<br />
� Extraction<br />
� Solidification etc.<br />
Features<br />
� Particularly favourable geometry for dipping<br />
sensors<br />
� Individual temperature control for each<br />
individual reactor with only one cryostat<br />
� Reactor size optional 75, 125, or 250 ml<br />
� Low expenditure of reactants<br />
� Multiple upgrading possibilities<br />
� Can also be used as Single Reactor System<br />
� High-capacity and easy to handle automation<br />
� Mini reactor systems controlled by a single<br />
PC with a LabManager, LabVision, and<br />
HiBatch multi recipe control<br />
� Fully-automated control of reactor conditions<br />
like feed rates, temperature, pressure, pH,<br />
and agitation<br />
� Multiple dosing options (liquid, solid and<br />
gaseous, gravimetric and volumetric)<br />
� Automated sampling options<br />
� Easy and fast handling<br />
� Inert construction materials: Glass, PTFE<br />
� Proprietary groundbreaking tempering<br />
system enables unhindered sight into the<br />
reactor<br />
� Modular compact design<br />
� Individually expandable and upgradeable<br />
The exchangeable reactor of the MiniLab enables<br />
fast reaction to changing requirements. The unique<br />
and innovative heating/cooling system offers<br />
essential benefits. The glass is situated on a<br />
heating/cooling plate. The same is electrically<br />
heated or cooled by a flow of cooling liquid out of a<br />
reservoir.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 17<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
18<br />
Automatic Laboratory Reactor Systems<br />
Modular and flexible<br />
MiniLab is a miniaturised fully-automated laboratory<br />
reactor system. Every process which is normally<br />
conducted in a reactor with greater volume can also<br />
run in the 75 to 250 ml reactors of the MiniLab under<br />
realistic conditions; fully automated and individually<br />
controlled for each reactor by the leading laboratory<br />
automation software LabVision and HiBatch.<br />
125 ml Reaktor 250 ml Reaktor<br />
MiniLab is available in a great variety reaching from<br />
the manually operated basis version to the<br />
individually configurable fully-automated multireactor<br />
system.<br />
Even complex operating sequences with reactant<br />
pre-treatment, synthesis, reaction monitoring, and<br />
product finishing treatment, as well as sample<br />
drawing, are possible.<br />
With the MiniLab parallel reactor system you can<br />
conduct experiments in parallel repeatedly in great<br />
numbers and therefore accelerate the work process<br />
significantly. This will save you time, increase the<br />
efficiency and the capacity of your laboratory.<br />
The test conditions such as temperature, pressure,<br />
pH etc., may differ for every reactor and are<br />
simultaneously controlled in all reactors.<br />
The vessel can be easily removed or installed after<br />
lifting up the complete top construction. Hereby, all<br />
reactor sizes can be deployed. Up to six sockets<br />
situated on the reactor cover permit flexible<br />
equipping with additional devices.<br />
The temperature of the plate is registered and<br />
controlled. It is possible to set a limit for the<br />
temperature.<br />
Options<br />
� Distillation<br />
� Rectification with Reflux Separation<br />
� Solid Dosing<br />
� Gaseous Dosing<br />
� ATR-FTIR online Monitoring<br />
� Magnet Stirrer Drive<br />
� Automatic Sampling<br />
� more options available upon request<br />
Module Description<br />
Module Basic Unit Equipment Components per Reactor<br />
(common components of all<br />
reactors, only one necessary<br />
per Parallel Reactor System)<br />
(if necessary, one unit required for<br />
each unit)<br />
Basic Module Tempering unit, rack, reactor<br />
75...250 ml, seal ring<br />
Silicon/FEP cladded, high-grade<br />
steel quick release fastener,<br />
high-grade steel cover, 1 x<br />
NS29, 5 x NS19 stirrer drive of<br />
Mini-Stirrer, flexible shaft, GL25<br />
connection, stirrer sealing,<br />
vacuum-sealed, anchor or tilted<br />
blade stirrer, max. temperature<br />
250 °C (monitor cooling<br />
media !), min. temperature<br />
dependent of thermostat. Inside<br />
temperature sensor PT<strong>10</strong>0<br />
PTFE coated with stirrer and<br />
wiring for stirrer and thermostat.<br />
Vessel Reactor 250 ml, DN60,<br />
borosilicate glass, sealing<br />
silicone/FEP-coated<br />
Standard Cooling Unit Cooling thermostat -20 °C (flow<br />
temperature)<br />
Reflux Cooling Cooling water valve<br />
Cooling water monitor<br />
Dimroth cooler<br />
Distillation Distilling bridge<br />
Pt<strong>10</strong>0 for steam temperature<br />
Collecting container for distillate<br />
Alternatives<br />
(other or expanded properties<br />
or specifications)<br />
ViscoPakt-mini-rheo35<br />
precision measurement<br />
stirrer, magnetic stirrer<br />
closure, propeller or<br />
impeller stirrer made of<br />
high-grade steel,<br />
glass thermometer etc.<br />
Reactor vessels 75 ml and<br />
125 ml with vacuum jacket<br />
for deep temerature<br />
applications<br />
Cooling thermostat -45 °C.<br />
low temperature equipment:<br />
Cooling thermostat -83 °C,<br />
removable isolation jacket<br />
(per reactor)<br />
Distillate weighing<br />
Additional cooler for reflux<br />
cooling<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Automatic Laboratory Reactor Systems<br />
Continued: MiniPlant Module Description<br />
Module Basic Unit Equipment<br />
(common components of all<br />
reactors, only one necessary<br />
per Parallel Reactor System)<br />
Components per Reactor<br />
(if necessary, one unit required for<br />
each unit) )<br />
Rectification Hempel column 200 mm<br />
Micro column head according to<br />
Dr. Kaminski, magnetically<br />
actuated<br />
Pt<strong>10</strong>0 column head<br />
Dimroth cooler<br />
Collecting container for distillate<br />
Vacuum Chemical-resistant vacuum<br />
pump<br />
Vacuum regulating valve<br />
Pressure sensor 0-1,6 bar<br />
Pressure relief valve<br />
Inerting valve, pressure relief<br />
valve 1,3 bar<br />
Inerting Pressure regulator 16 bar to 0-<br />
1 bar<br />
Gravimetric Dosing Hanging scales Grado<strong>10</strong>00<br />
Weighing container 250 ml,<br />
lateral refilling feed pipe<br />
Regulating valve<br />
Alternatives<br />
(other or expanded properties<br />
or specifications)<br />
Vacuum jacket<br />
Distillate weighing<br />
Pt<strong>10</strong>0 in column<br />
Vigreux column<br />
Filling material/Packages<br />
Stronger vacuum pump<br />
Automatic refill<br />
Mounting panel for<br />
LabManager (useful in case<br />
of more than 3 modules)<br />
Other container sizes<br />
Volumetric Dosing Peristaltic pump Diaphragm, piston pumps,<br />
etc.<br />
Solid Dosing Solid doser SoliDos<br />
Inerting connection<br />
connection socket on to NS19 Inert gas heating<br />
pH Measurement PH gel electrode pH 0-14 Cover with special sensor<br />
lead-through 12 mm<br />
measuring amplifier pH<br />
socket<br />
Redox Potential Redox-electrode<br />
Cover with special sensor<br />
reference electrode<br />
socket (necessary at anchor<br />
lead-through 12 mm<br />
measuring amplifier MA<br />
stirrer!)<br />
Reaction Calorimetry Reactor with vacuum jacket<br />
Calorimetry evaluation module<br />
Gas Dosing Pressure regulator 16 bar to 0- Mass flow regulator<br />
1 bar<br />
Pressure relief valve 1,3 bar<br />
Order Code Description<br />
VL-MINILAB-BU MiniLab multi reactor base module with tempering and stirrer unit and cover<br />
IR-VIPA-MINI-RHEO-35 ViscoPakt-rheo stirrer drive, 35 Ncm<br />
VL-MINILAB-GRV75 MiniLab reactor vessel 75 ml, DN60, borosilicate glass, gasket silicone/FEP covered<br />
VL-MINILAB-GRV125 MiniLab reactor vessel 125 ml, DN60, borosilicate glass, gasket silicone/FEP covered<br />
VL-MINILAB-GRV250 MiniLab reactor vessel 250 ml, DN60, borosilicate glass, gasket silicone/FEP covered<br />
Further extensions:<br />
MiniLab can be extended with MultiLab system<br />
modules. There you will find suitable dosing<br />
systems, automation hard- and software, user<br />
interfaces and thermostats.<br />
Should you have any queries, our sales experts will gladly help you!<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 19<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
20<br />
Automatic Laboratory Reactor Systems<br />
LabKit- Small Reactor Systems for Education<br />
Since 2002, laboratory automation, process control<br />
technology, and the basis operations of chemicalprocess<br />
engineering are included in the<br />
examination-relevant curriculum of chemical<br />
technicians and laboratory assistants. These topics<br />
should also not be omitted in the vocational training<br />
for chemists and process technicians. <strong>HiTec</strong> <strong>Zang</strong><br />
systems are already being used by numerous<br />
institutions for training, because they can be<br />
comprehended quickly.<br />
With LabKit-ed the substantial topics of modern<br />
laboratory practice can be conveyed, e.g.:<br />
� Chemical Process Engineering, Basis Operations<br />
� Control (monitoring, regulation)<br />
� Process Measuring and Control<br />
� Automation, Basic Functions<br />
� Batch, Semi-Batch and continuous Processes<br />
� Reaction Calorimetry<br />
� Recipe Control<br />
The system already becomes active at the planning<br />
stage. The P&ID editor supports the standardconform<br />
establishment of P&ID flow diagrams in<br />
accordance with EN ISO <strong>10</strong>628 (DIN28004) which<br />
are initially marked with the process and measuring<br />
control identifications according to DIN/EN19227.<br />
Specification<br />
A free version of RI-CAD, restricted to training<br />
purposes, can be requested on our website under:<br />
http://www.hitec-zang.de/de/downloads/ri-cad.html<br />
The P&ID flow sheet can be used later as the<br />
background picture for the displaying of control<br />
pictures (process pictures).<br />
In addition, the measurement and control system<br />
plan (MSR) and the circuit diagrams can be<br />
established with the same editor. It must be<br />
emphasised that the system is easy to comprehend<br />
and the handling can be comprehended in a very<br />
short period of time.<br />
The system is structured on a modular basis and<br />
can be adapted according to your special requests.<br />
With the optional Simulation Module, applications<br />
can be developed and pre-tested offline.<br />
We also train teachers in these fields of expertise.<br />
We will gladly forward you our proven teaching<br />
material (introduction manuals, exercises with<br />
solutions)!<br />
In case of interest, please ask us for further<br />
information on LabKit-ed.<br />
Rack anodised aluminium rack<br />
Reactor - 1 glass Reactor DN<strong>10</strong>0 with heating jacket and base discharge valve with<br />
integrated Pt <strong>10</strong>0 sensor manual<br />
- Glass cover with FEP-O-Ring silicone core<br />
- Stirrer shaft lead-through vacuum for <strong>10</strong> mm shaft, NS29<br />
- 2 tube connections for thermostats DN15 on to M16*1 with integratedPt<strong>10</strong>0-sensor<br />
GraviDos<br />
(Gravimetrical<br />
Dosing System)<br />
- 1 glass propeller stirrer<br />
1 GraviDos dosing System: the system consists of a glass storage container, which is<br />
suspended on a weighing system. The weight difference is registered and then the<br />
discharge regulated via valve. The system disposes of an integrated <strong>10</strong>00 g load cell,<br />
a 500 ml receiver tank, and a 2/2-way valve.<br />
Stirrer - 1 ViskoPakt torque stirrer, max. torque: 27 Ncm<br />
Dissolution: 0.07 Ncm, reproducibility: 1.5 Ncm, min. rotational speed: 150 rpm, max.<br />
rotational speed: 2000 rpm, standard stirrer lead-through (max 800 rpm).<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Automatic Laboratory Reactor Systems<br />
Tempering System - 1 circulation thermostat: with water pipes cooling coil, temperature range:<br />
35..200 °C, heating output: 2000 W, bath content: 3 litres, control via RS232,<br />
- 2 isolated metal tubes for thermostats, 150 cm<br />
- 1 2/2- way valve for cooling water supply to the thermostat<br />
Inerting - 1 binary valve for inert gas pipe<br />
- 1 pressure regulator from max. 16 bar suction pressure to 0.1..1 bar<br />
Venting/Deairing - 1 dead open binary valve<br />
- 1 Relief valve 0.1 bar made of glass for NS 29/32<br />
Instruments All sensors/actors including necessary fixtures and cables for connection to the <strong>HiTec</strong><br />
PI.<br />
Automation LabBox2-complete unit with integrated 24 V 1 A power supply sensors and and 24 V 3<br />
A power supply for actors.<br />
<strong>HiTec</strong> display and operation component including uninterrupted power supply and<br />
Power-Management-System for <strong>HiTec</strong> <strong>Zang</strong> PIs CG-ABK1.<br />
20" TFT Monitor.<br />
LabVision software package for training purposes with the following equipment: basic<br />
package with 300 data points, HiText – multitasking control and online evaluation,<br />
HiBatch Recipe Control, dialogue and protocol templates, online graphics, analogue<br />
chart recorder, event plotter, phase plotter, monitoring and messaging, Designer,<br />
P&ID-Editor, graphics library, data export, access monitoring and user administration,<br />
controller module with 4 P-, PI-, PID-, PD- or pH controller, NAMUR driver for serial<br />
interfaces, basic operations, charging, tempering, stirring, dosing, inerting,<br />
maintenance.<br />
Simulation LabVision-ed simulation version for training (VL-EDSIM) enables learning and training<br />
of automation technology and the process control by merely using a PC without PI<br />
and plant. It contains all essential LabVision modules, such as recipe control<br />
according to IEC and NAMUR, process visualisation, monitoring and messaging,<br />
online evaluation, etc.<br />
Basic operations such as dosing, temperature ramping, pressure and vacuum control,<br />
pH control, etc., can be established and tested. In order to avoid unnecessary waiting<br />
periods, the process simulation can be conducted in fast motion. The established<br />
applications can be transmitted to a LabKit-ed and tested under real conditions.<br />
Executable without PI under Windows 2000, XP and Vista.<br />
Optional equipment is available.<br />
Order Code Description<br />
VL-LABKITED Automatic Laboratory Reactor System for training, hard and software configuration according to<br />
table<br />
VL-EDDEST Expansion by distillation, reflux cooler, electronically controllable reflux separator, head<br />
temperature measurement and distillate scales, HiBatch basis operation distilling.<br />
VL-EDDOSFL LabKit-ed expansion by a volumetric dosing, a suspended receiver tank with a flowmeter and a<br />
pulse frequency controlled binary valve, HiBatch basis operation, volumetric dosing<br />
VL-EDVAK - vacuum control with the following components:<br />
-1 vacuum pump, flow rate: 20l/min, vacuum <strong>10</strong>0...<strong>10</strong>00 mbar absolute<br />
- activation via the power socket switched by the <strong>HiTec</strong> PI<br />
- 1 pressure sensor 0..1,6 bar absolute<br />
- HiBatch basis operation vacuum, 1 vacuum control valve , material: ETFE / Kalrez<br />
VL-EDDOSPU Expansion of a LabKit-ed by a volumetric and gravimetric dosing with pump and scales consisting<br />
of:<br />
- 1 scales, weighing range 3000 g, reproducibility 0.1 g, RS232 interface,<br />
- 1 magnetic diaphragm dosing pump 0.74 l/h (alternatively 1,1 or 2,1 l/h)<br />
- parts in contact with medium: PTFE<br />
- 1 dosing valve, material: ETFE,<br />
- HiBatch basis operation gravimetric dosing<br />
VL-EDSIM PI and process simulation package for one work station. Enables project establishment,<br />
parameterisation, programming, and simulation of the LabKit-ed without PI and plant.<br />
VL-EDUQUIP Case with training equipment such as Current and voltage transmitter, controlled loop simulator<br />
etc.<br />
Further information about training systems and didactic material can be found in the chapter Services &<br />
Didactics.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 21<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
22<br />
Automatic Laboratory Reactor Systems<br />
Automated Laboratory Clarification Unit<br />
The Laboratory Clarification Unit LabKit-sp<br />
enables the systematic investigation of the biological<br />
degradability of various liquid waste content<br />
substances. It consequently provides the basis<br />
information for the establishment of strategies for<br />
liquid waste purification. The unit enables the<br />
reproduction of clarification processes of large plants<br />
on a laboratory scale. It is also possible to conduct<br />
tests regarding the determination of the biological<br />
degradability according to OECD301A.<br />
The Unit comprises four levels:<br />
1.) Neutralisation with automated ph-Control, with<br />
ViscoPakt Stirrer, LabDos- Pump for the Feed,<br />
Overflow to the Denitrification.<br />
2.) Denitrification with O2-Measurement, pH-<br />
Measurement, ViscoPakt Stirrer, Interior<br />
Temperature Control (through electrical Heating with<br />
Heating Jacket), Overflow to the Nitrification.<br />
3.) Nitrification with O2-Control (through regulated<br />
Air Supply via a Base Frit), pH-Measurement,<br />
ViscoPakt-Stirrer, Interior Temperature Control<br />
(through electrical Heating with Heating Jacket),<br />
Foam Identification with automated Defoamer<br />
Addition, LabDos Pump for the transporting back the<br />
sludge into the Denitrification, Outlet into the Settling<br />
Tank.<br />
4.) Settling Tank with Overflow, Discharge Valve,<br />
LabDos Pump for the transporting back the sludge<br />
into the Denitrification.<br />
The Laboratory Clarification Unit is fully automated<br />
with a LabBox System and LabVision. It can<br />
naturally also be run manually.<br />
pH-Value, Temperature and Oxygen Concentration<br />
and further Measurement Variables are collected.,<br />
stored in the data base and graphically presented.<br />
The automation enables unattended operation and<br />
reproducibility at any given time.<br />
The permanent data recording leads to a consistent<br />
documentation of all process sequences.<br />
Neutralisation, Denitrification, Activation and Final Clarification<br />
Pilot Clarification Units deviant from this standard<br />
laboratory clarification unit, according to your<br />
specifications, are also offered by <strong>HiTec</strong> <strong>Zang</strong>.<br />
Order Code Description<br />
VL-LABKIT-SP Automated Laboratory Clarification Unit with LabBox PI and ABK1<br />
VL-LABKIT-SP-PHCON Automatic pH-Control<br />
VL-LABKIT-SP-FOCON Automatic Defoaming Control<br />
The plant is supplied in turnkey condition together with a LabBox2 Automation System and a ABK1<br />
Workstation with 20“ Monitor.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Automatic Laboratory Reactor Systems<br />
Modular Micro-Reaction Technology<br />
Micro-reaction technology opens up new ways to<br />
develop novel reaction processes and to construct<br />
advanced economic chemical plants. The<br />
advantages of the continuous operation mode in<br />
micro-structures are: ultra-fast mixing, highly<br />
effective heat transfer, short and controllable<br />
residence times, low system inertia for ideal process<br />
control and high safety due to extremely low holdup.<br />
The basic features of the micro-reaction technology<br />
for the development of new chemical processes and<br />
the production, both in the fine and mass chemical<br />
sector, offer significant potential for innovation and<br />
amortisation. Micro-modules can also be integrated<br />
into conventional plants without any problem.<br />
The micro-reaction technology enable to exactly<br />
control complex or critical reactions of fine chemistry<br />
(special products, agricultural and pharmaceutical<br />
chemicals), which considerably increases the<br />
operational safety of the chemical production.<br />
Economically attractive application possibilities have<br />
also been detected for bulk chemicals and polymers.<br />
The future technology of customised materials is not<br />
imaginable without micro-technology, as well. Microreactors<br />
allow the selective generation of nanoparticles<br />
for micro-electronics, the development of<br />
drug delivery systems for human medicine, and the<br />
realisation of new concepts within diagnostics.<br />
Micro-reaction modules enable basis process<br />
operations such as:<br />
� Mixing<br />
� Dispersing<br />
� Gassing<br />
� Precipitation<br />
� Heat Exchange, etc.<br />
<strong>HiTec</strong> <strong>Zang</strong>, in cooperation with the company<br />
Ehrfeld Mikrotechnik BTS, offers a complete<br />
package offer, which reaches from the individual<br />
module to process development and training, and as<br />
far as to engineering and the construction of ready<br />
to use fully automatic plants.<br />
The modules can flexibly be interconnected to<br />
precisely controllable reaction plants, with which a<br />
wide range of chemical syntheses can be conducted<br />
easily, quickly and cost-effective.<br />
The modular micro-reaction System represents an<br />
unique research and development platform for the<br />
development of new processes, both in laboratory<br />
scale and small-scale production.<br />
In addition, high flow modules are available, which<br />
also enable the mass production of chemicals.<br />
Dependent on the reaction conditions, these<br />
modules cover a flow rate ranging from 0.1 to <strong>10</strong>0<br />
ml/min with the modular micro-reaction system, and<br />
up to <strong>10</strong>00 litres/hour with the high flow modules.<br />
The modular micro-reaction system represents a<br />
unique tool for researchers out of the chemical and<br />
pharmaceutical sectors, to both develop new<br />
synthesis methods for the production of new<br />
chemical compounds and to improve existing<br />
methods.<br />
Hereby, one significant advantage is that the step<br />
from the development into production is conducted<br />
by simple „Numbering-Up“, e.g. the parallel<br />
connection of several identical sequences, instead<br />
of the expedient „Scale-Up“ procedure.<br />
Modular Micro-reaction System: Example for a single stage<br />
synthesis for heterogeneous conversions at solid catalysts<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 23<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
24<br />
Special Features<br />
Automatic Laboratory Reactor Systems<br />
� Ideal ultra-fast mixing effect<br />
� Extremely short holding times<br />
� Avoidance of by-products<br />
� Robust against strong exothermal reaction<br />
� Increased operational safety<br />
� Minimal requirements to ambient conditions<br />
� Without scale-up in the production scale<br />
The Micro-reaction Technology enables to conduct<br />
single-stage and multi-stage syntheses throughout<br />
the whole range of research and development right<br />
to the production of chemical substances. Hereby, it<br />
is both possible to conduct reactions in the liquid<br />
and gas phases, as well as multi-phase in<br />
heterogeneous systems in the micro-reaction<br />
modules. In addition, there are special modules for<br />
the continuous precipitation of solids into microstructures<br />
so that it is also possible to process<br />
liquids carrying particles.<br />
The modular micro-reaction system developed by<br />
the company BTS/Ehrfeld Micro-Technology enables<br />
the user to change the plant configuration himself.<br />
Depending on the modules, it is possible to realise<br />
pressures up to <strong>10</strong>0 bar and temperatures in the<br />
range of -20 to 200 °C. Additional modules extend<br />
this working range. The CryoReactor, for instance,<br />
enables low temperature reactions down to -<strong>10</strong>0 °C.<br />
All materials in contact with media are mainly made<br />
of stainless steels like DIN 1.4571 or 1.4401. Seals<br />
are either made of PTFE or perfluorinated<br />
elastomers, such as FFKM. Other materials like<br />
Hastelloy are available on request.<br />
In order to run the Modular Microreaction System for<br />
laboratory-scale experiments, only some standard<br />
peripheral devices are necessary in addition. <strong>HiTec</strong><br />
<strong>Zang</strong> will gladly assist you with advice in selecting<br />
suited devices and is able to supply individual<br />
components as well as complete ready-to-use fullyautomated<br />
plants.<br />
There are approximately 30 different modules<br />
available, e.g.:<br />
� Mixer<br />
� Reactors<br />
� Heat Exchanger<br />
� Filter<br />
� Heating Modules<br />
� Sensors<br />
� Valves<br />
� Pumps etc<br />
All components of the modular micro-reaction<br />
system are mounted on a base plate with a square<br />
grid. One grid cell has the a length of 25 mm.<br />
Accordingly, the smallest lateral length of a module<br />
is 25 mm, including a 1 mm strong seal disc. The<br />
height of a module depends on its specific function.<br />
Base plates are available in the formats A3 (16x12<br />
grid cells), A4 (12x8 grid cells) and A5 (8x6 grid<br />
cells).<br />
Stand-alone-Module<br />
The direct connection concept of the Modular Microreaction<br />
System offers unique advantages. The<br />
plants can be assembled quickly and easily, and can<br />
be easily adjusted to the respective synthesis<br />
problem. Due to the consistent waiving of tube<br />
connections and screwings between the individual<br />
modules, dead storage is reduced to a minimum.<br />
In spite of this, reactors or heat exchangers can be<br />
connected to an already existing periphery as standalone<br />
modules with 1/8” Swagelok fittings. The high<br />
flow modules with 1/8” Swagelok fittings are also<br />
available in such a version.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Automatic Laboratory Reactor Systems<br />
The Automation Technology The LabManager/LabVision-System, with a special<br />
operating interface module (Ehrfeld BTS or Syntics),<br />
is very well-suited for micro-reaction plants. You can<br />
find further details on this topic in the chapter<br />
„Laboratory Automation Software“.<br />
In combination with our Liquid-Handling-Systems, it<br />
is possible to establish fully-automated screening<br />
equipment. Samples are provided programcontrolled.<br />
Test parameters are set according to plan<br />
and test samples are filled.<br />
Would you like to know more about the possibilities<br />
of this fascinating technology?<br />
Just give us a phone call. We will gladly advise you!<br />
Note<br />
Suitable pumps can be found in the chapter Dosing Systems and Pumps.<br />
Suitable sensors, eg. low dead space pressure receivers can be found in the chapter Process Analytics and<br />
Sensors.<br />
� Formulating Stations<br />
� Customer specific plant<br />
� Component for reaction calorimeters<br />
can be found in the chapter Construction and Miniplant Technology<br />
Reactant mixing pumps can be found in the chapter Dosing Systems and Pumps.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 25<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
26<br />
Here you will find:<br />
� LabKit TM -rcf Heat Flow Calorimetry (HFC)<br />
� LabKit TM -rcb Thermal Balance Calorimeter<br />
� KalDas TM Calorimetry Evaluation<br />
� Reaction calorimetry components<br />
Reaction Calorimetry<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Reaction Calorimeters<br />
Until now, reaction calorimeters and automatic<br />
laboratory reactors, which were able to handle more<br />
than only simple syntheses, had to be regarded<br />
separately. The <strong>HiTec</strong> <strong>Zang</strong> LabKit-rc reaction<br />
calorimeters combine both devices, whereby a<br />
flexible system is generated in every respect. As a<br />
calorimeter, LabKit-rc offers different operation<br />
modes and measuring methods, and as a lab<br />
reactor system, the whole flexibility of the LabKit<br />
laboratory reactor technology and the LAB<br />
manager’s research process control system.<br />
Up to now, reaction calorimeters were very costintensive.<br />
Nevertheless, they are necessary. The<br />
knowledge of the heat tone of a process is required<br />
for the safety-related and energetic evaluation.<br />
Many users are therefore on the lookout for a costeffective<br />
possibility to conduct calorimetric<br />
measurements already during process development.<br />
In addition, according to the opinion of leading<br />
scientists, the significance of reaction calorimetry<br />
for process analytics is underestimated by far. In the<br />
event of all exothermal and endothermal processes,<br />
the signal of the current heat output delivers<br />
additional information on the reaction progression,<br />
which is currently only rarely utilised.<br />
The Advantages:<br />
� Heat Flow and Thermal Balance are possible<br />
� Isothermal, Isoperibole and Adiabate Mode of<br />
Operation<br />
� Full ALR Functionality<br />
� Uncomplicated Evaluation<br />
� Easy-to-handle Open System<br />
� Upgradeable at all Times<br />
� Electrically lowerable Reactor Head<br />
� Best possible Reproducibility<br />
� GLP-conform Documentation<br />
� Access via Network, e.g. from the Office<br />
� Remote <strong>Main</strong>tenance (Tele-Service)<br />
Reaction Calorimetry<br />
The range of possible applications is very versatile<br />
and goes far beyond the classical measurement of<br />
heat tone and thermal conversion.<br />
LabKit-rc supports adiabate, isoperibole, and<br />
isothermal operation mode.<br />
LabKit-rc Systems are ready-to-use reaction<br />
calorimeters.<br />
To allow upgrading or modernising of existing<br />
laboratory reactors or existing reaction calorimeters,<br />
all necessary components are also individually<br />
available.<br />
The standard systems LabKit-rcf and LabKit-rcb<br />
depicted in the following, are complete, ready-forcommissioning,<br />
automatic reaction calorimeters,<br />
which can also be utilised as full-fledged Automatic<br />
Labor Reactor Systems (ALRS). They can be<br />
upgraded with the available additional modules and<br />
components of the LabKit program.<br />
Next to the standard calorimeters depicted in the<br />
following, we also manufacture client-specific<br />
plants and also offer the renovation, repair, and<br />
expansion of existing reaction calorimeters of<br />
various manufacturers.<br />
Information in regard to the individually<br />
manufactured reaction calorimeters can be<br />
found in the chapters Plant Construction, Miniplant<br />
Technology, and Customised Reaction<br />
Calorimeters.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 27<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
28<br />
Reaction Calorimetry<br />
LabKit-rcf Heat Flow Reaction Calorimeter<br />
LabKit-rcf, heat flow calorimeter with extension options<br />
Reaction calorimeter in a sophisticated<br />
configuration for heat flow calorimetry. The<br />
automatic laboratory reactor system is suitable e.g.<br />
for syntheses in the temperature range from -40 to<br />
+200 °C. The system is expandable with<br />
additional modules and components offered.<br />
System Construction<br />
As standard container, a double-walled 2 litre<br />
reaction vessel is used. Other containers are<br />
available.<br />
The reaction vessel is kept at a moderate<br />
temperature by high performance heating/cooling<br />
thermostats, which enables fast temperature<br />
control for isothermic use.<br />
Measurement Method<br />
The heat flow method is based on the<br />
measurement of the temperature difference<br />
between the reactor contents and temperature<br />
medium in the container jacket. For the heat flow<br />
over the reactor wall the relationship applies:<br />
Q& = k A⋅ΔT<br />
kond<br />
w<br />
The heat transition coefficient cannot generally be<br />
theoretically calculated. Since it can vary<br />
significantly during reaction (e.g. by modification<br />
of the viscosity, the specific heat of the reaction<br />
mixture, or by boundary layer formation), it is<br />
determined by calibration with defined heat output<br />
before and after the reaction.<br />
k<br />
w<br />
Q<br />
A =<br />
ΔT<br />
&<br />
kond<br />
RJ<br />
RJ<br />
The reaction calorimeter is extendable for heat<br />
balance calorimetry and can be optionally<br />
upgraded by<br />
� Online Evaluation<br />
� Inerting<br />
� Vacuum<br />
� Distillation<br />
� Reflux<br />
For reflux distillation, the reflux separator ratio is<br />
adjustable over a programmable reflux separator.<br />
For further information see "Components for<br />
reaction calorimetry"<br />
Example Version:<br />
LabKit-rcf with electrically lowerable <strong>10</strong>00 ml reactor with<br />
vacuum jacket, two gravimetric and one volumetric dosing<br />
circuits, vacuum control, reflux distillation and inerting.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Specification<br />
Reaction Calorimetry<br />
Rack Square anodised aluminum profile, electrical fixture for lowering the reactor<br />
vessel, catch pan made of high-grade steel.<br />
Reactor 2-Liter Double-walled glass container, tempering jacket, PTFE-bottom drain valve,<br />
Lid with Center neck and 6 Supports, safety-valve 200 mbar, ventilation valve<br />
Stirrer ViskoPakt rheo57 Precision stirrer drive with Speed control and Torque<br />
measurement, Anchor Stirrer<br />
Heating/Cooling System Heat-Cool-Thermostat -40 to +200 °C, Air-/ Compressor Cooling, Heating power 3<br />
kW, Cooling power to 3 kW at 200 °C, 0,7 kW at 0°C<br />
Dosing System One GraviDos Dose circuit for Liquids (Regulated drop funnel), 500 ml feed tank,<br />
gravimetric regulated<br />
Automation LabManager. Interfaces: 8 Pt<strong>10</strong>0 Precision-Temperature measurement inputs, 8<br />
analogue inputs (Current & Voltage) of which 1 pH, 4 RS232, 4 GraviDos (DMS)<br />
Interfaces, 4 digital inputs, 8 digital Outputs (current & voltage), controllable<br />
calibration heating 50 W glass (optionally stainless steel). Sensor power supply<br />
24 V 1,5 A, actor power supply 24 V 3 A.<br />
CA-ABK2, 22“ Monitor, Uninterrupted Power Supply with UPS-Management<br />
Software<br />
Sensors Calibrated temperature sensor for: reactor, thermostat, flow line, reflux, head and<br />
environment temperature, flowmeter in the heat carrier, preasure measurement<br />
0...1600 mbar abs., stirrer: rotational speed, torque<br />
Materials <strong>Main</strong>ly borosilicate glass, PTFE, PVDF, Viton, Stainless steel 1.4571 (changes<br />
possible)<br />
Evaluation see KalDas<br />
Order Code Description<br />
VL-LABKITRCF1 Reaction calorimeter for heat flow calorimetry<br />
VL-LABKITRCONLF Online-heat flow-Evaluation<br />
Special equipment is available e.g. for inerting,<br />
vacuum, reflux boiling and reflux distillation using<br />
the programmable reflux separator and intensive<br />
cooler in a mirrored glass vacuum jacket,<br />
Recommended software packages:<br />
as well as balancing of the cooling water and<br />
distillate. See lab kit structure system.<br />
Order Code Description<br />
SL-LABVIPBATE Software Package for LabManager1 for Operation of medium-sized Batch-Processes<br />
SF-PID8 Controller Module with 8 PID- and application oriented controllers<br />
SA-KALDAS3 Evaluation Program for Heat Flow and Thermal Balance Calorimetry on KabKit-rcb<br />
Recommended upgrades<br />
� MoleculeEye with fibre optic probe for differentiated, cinetic analysis<br />
Further information can be find in the chapter Process Analytics and Sensorics.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
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Software<br />
Plant<br />
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Technology<br />
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Reaction Calorimetry<br />
LabKit-rcb-Heat balance - Reaction Calorimeter<br />
LabKit-rcb, heat balance calorimeter with expansion.<br />
Reaction calorimeter in a sophisticated<br />
configuration for heat flow and heat balance<br />
calorimetry. The automatic lab reactor system is<br />
suitable e.g. for syntheses in the temperature<br />
range from -40 to +200 °C. The system is<br />
expandable with the offered additional modules<br />
and components.<br />
System Construction<br />
As standard container for heat balance calorimetry,<br />
a triple wall, 2 litre reaction container with<br />
evacuated outer jacket is used. Other containers<br />
are available.<br />
The reaction container is kept at a moderate<br />
temperature by high performance heating/cooling<br />
thermostats, which enables a fast temperature<br />
control for isothermic operation mode.<br />
It is upgradeable with options, e.g.:<br />
� Online-Evaluation<br />
� Vacuum<br />
� Distilling<br />
� Reflux<br />
� Inerting<br />
When distilling with reflux separators, the reflux<br />
component ratio can be regulated via an<br />
electrically controllable reflux separator.<br />
For further information, see „Components for<br />
Reaction Calorimetry“.<br />
LabKit-rcf with electrically lowerable 1 litre reactor with vacuum<br />
jacket, 3 gravimetric dosing circuits, vacuum control, reflux<br />
distillation and inerting.<br />
Measurement Method<br />
The heat balance method is based on the<br />
balancing of the tempering medium at the feed and<br />
discharge opening of the container jacket. The<br />
temperatures and the flow of the heat carrier are<br />
measured.<br />
Q& = m&<br />
⋅cp<br />
⋅ ΔT<br />
Kond<br />
öl<br />
öl<br />
RJVR<br />
The heat transition coefficient (KwA) is not required<br />
for the evaluation. This is particularly important in<br />
case of reactions where a coating develops at the<br />
vessel walls, as for example, during<br />
polymerisations and dispersions.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Specifications<br />
Reaction Calorimetry<br />
Rack Square anodised aluminum profile, electrical fixture for lowering the reactor<br />
vessel, catch pan made of high-grade steel.<br />
Reactor 2Liter Double jacket glass container with vacuum jacket, temper jacket, PTFEbottom<br />
drain valve, lid with centre neck and 6 supports, safety valve 200 mbar,<br />
ventilation valve<br />
Stirrer ViskoPakt rheo57 Precision-stirrer drive with speed control and torque<br />
measurement, Anchor Stirrer<br />
Heating/Cooling System Heat-cool-Thermostat, -40 to +200 °C, Air/ Compressor cooling, heating power 3<br />
kW, cooling power up to 3 kW (200 °C), 0,7 kW (0°C)<br />
Dosing System One GraviDos Dose circuit for liquids (regulated Drop funnel), 500 ml Feed tank,<br />
gravimetric regulated<br />
Automation LabManager. Interfaces: 8 Pt<strong>10</strong>0 Precision-Temperature measurement inputs, 8<br />
analogue inputs (Current & Voltage) of which 1 pH, 4 RS232, 4 GraviDos (DMS)<br />
Interfaces, 8 digital inputs, 8 digital Outputs (current & voltage), controllable<br />
calibration heating 50 W glass (optionally stainless steel)<br />
CA-ABK2, 22“ Monitor, Uninterrupted Power Supply with UPS-Management<br />
Software<br />
Sensors Calibrated temperature sensor for: reactor, thermostat, flow line, reflux, head and<br />
environment temperature, flowmeter in the heat carrier, preasure measurement<br />
0...1600 mbar abs., stirrer: rotational speed, torque<br />
Materials <strong>Main</strong>ly glass, PTFE, PVDF, Viton compound, stainless steel material 1.4571<br />
(subject to changes)<br />
Evaluation see KalDas<br />
Order Code Description<br />
VL-LABKITRCB1 Reaction calorimeter for Heat balance calorimetry<br />
VL-LABKITRCMDM Mass flow meter for the heat carrier<br />
VL-LABKITRCONLB Online heat balance evaluation<br />
Optional equipment is available, e.g. inerting,<br />
vacuum, reflux boiling and distilling via a<br />
electrically controlled reflux separator and intensive<br />
cooler made of metallised glass, with vacuum<br />
jacket as well as balancing of the cooling water<br />
and the distillate.<br />
For further information see LabKit system<br />
construction.<br />
Recommended software packages:<br />
Order code Description<br />
SL-LABVIPBATE Software Package for LabManager1 for Operation of medium-sized Batch-Processes<br />
SF-PID8 Controller module with 8 PID and application oriented controller<br />
SA-KALDAS3 Evaluation Program for Heat Flow and Thermal Balance Calorimetry on KabKit-rcb<br />
Recommended upgrades<br />
� MoleculeEye with fibre optic probe for differentiated, cinetic analysis<br />
Further information can be find in the chapter Process Analytics and Sensorics.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Reaction Calorimetry<br />
Calorimetry Evaluation Program KalDas<br />
Uncomplicated Evaluation!<br />
►<br />
KalDas is a new development in the field of reaction<br />
calorimetry. KalDas provides you with data that you<br />
need for model evaluations (e.g. scale up) and for<br />
energy and safety considerations.<br />
KalDas is based on the flexible control and data<br />
analysis software platform HiText and can therefore<br />
be easily customised to your special requirements.<br />
The acquired data can be evaluated at the push of a<br />
button and the results are displayed in a free<br />
configurable and a clearly arranged protocol.<br />
KalDas was primarily developed for the <strong>HiTec</strong><br />
reaction calorimeter. However, there is no<br />
constriction to any specific calorimeter, i.e. the<br />
program may be adapted to any other device.<br />
It is also possible to adjust the programming for<br />
special evaluations or data transfer, e.g. to programs<br />
for reaction kinetics.<br />
Heat inflow and dissipation of the stirrer, condenser,<br />
dosage flow as well as accumulated heat is<br />
considered in the calculation. If needed, the<br />
calculations may be expanded to heat balance<br />
calorimetry or other methods.<br />
KalDas is deployed for:<br />
� Product Development<br />
� Process Optimisation<br />
� Quality Assurance<br />
� Scale Up Tests<br />
� Plant Safety<br />
KalDas3 was completely newly designed based on<br />
the proven KalDas2. The programming in HiText<br />
warrants for optimal cooperation with LabVision and<br />
enables online calorimetry.<br />
KalDas ideally operates combined with the HiBatch<br />
Recipe Control. The steps related to reaction<br />
calorimetry are integrated like normal basis<br />
operations in the recipe.<br />
The delays of the measurement signals which lead<br />
to distortions in the course of the power output<br />
evaluation are corrected by special algorithms. This<br />
allows realistic presentation of the output power<br />
progression.<br />
Advantages:<br />
� Simple Handling<br />
� Online and Offline Evaluation in one Program<br />
� Flow and Balance Evaluation simultaneously<br />
possible<br />
� Dosing, Reflux, and Dissipation are<br />
considered<br />
� Intermediate Values (Outputs) are made<br />
transparent<br />
� Fully integrated in LabVision, optional Standalone<br />
Version<br />
� First Analyses are already possible during the<br />
running Test<br />
� Alignment to your possibly already existing<br />
Equipment is possible<br />
� Application-specific Expansions are possible<br />
due to HiText Programming<br />
� Full Functionality of an Automatic Laboratory<br />
Reactor is supported<br />
� Multi-stage Recipe-controlled syntheses are<br />
possible<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Reaction Calorimetry<br />
Product Description Menu-controlled evaluation program for calorimetry data, compilation of<br />
measurement data, characteristics determination, graphic presentation, inter alia<br />
of output and heat curves, etc.<br />
Delivery Scope CD-ROM, manual<br />
Order Code Description<br />
SA-KALDAS3 Evaluation Program for the Reaction Calorimetry on LabKit-rcf and -rcb<br />
For control operations, see LabVision Basis Operations.<br />
KalDas can also be aligned to your equipment!<br />
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Reaction Calorimetry<br />
Components for Reaction Calorimetry<br />
Calibration Heating<br />
The calibration heating is required when conducting<br />
calorimetric measurements in reaction calorimeters<br />
or laboratory reactors. In particular for the<br />
establishment of the thermal capacity of a material<br />
within the scope of a heat flow calorimetry, a highprecision<br />
calibration heating is required which<br />
compensates the thermal resistance, e.g. as a result<br />
of aging and temperature influences. The heating<br />
output of the following devices can be steplessly<br />
Technical Data<br />
Power consumption 230 V, <strong>10</strong>0 W / 150 W<br />
Delivery of power 0 ... 50 W , 0 ... <strong>10</strong>0 W, <strong>10</strong>0 % duty cycle<br />
Uncertainty
Turbine Flowmeter for Heat Carrier Oil<br />
Thermal balance calorimetry requires the exact<br />
measurement of the flow rate of the heat carrier oil.<br />
The flow sensors are especially suited for this<br />
purpose and are frequently used as an alternative to<br />
the significantly more expensive Coriolis mass flow<br />
meters.<br />
In the sector of reaction calorimetry, they are<br />
particularly suited for the flow measurement of the<br />
heat carrier oil at temperatures of up to 350 °C.<br />
They are deployed as standard in our thermal<br />
balance calorimeters.<br />
Technical Data<br />
Reaction Calorimetry<br />
They function according to the principles of a<br />
turbine-type meter:<br />
Type Measuring Range<br />
in l/min<br />
Impulse/Litre Connection G<br />
TDM06 1 to <strong>10</strong> 2000 ½ inch<br />
TDM09 3 to 30 980 ½ inch<br />
The Advantages:<br />
Linearity +/-2 % v.M.<br />
Reproducibility +/-0.5 %<br />
Media Temperature -20 to 120, 180 or 350 °C<br />
Max. Working Pressure 20 bar<br />
Viscosity 0,1 to 6 mm²/s<br />
Materials High-grade steel 1.4305 and 1.4122, ceramic<br />
Seal Viton or Graphite<br />
Content of delivery: Sensor with mounted impulse amplifier<br />
Order code Description<br />
IS-F-TDMtc-tb-sa Turbine Flowmeter<br />
IS-F-TDMMV-AK-I LAB-PI Connection Cable for Turbine Flow Sensor , 4..20 mA<br />
IS-F-TDMMV-AK-F LAB-PI Connection Cable for Turbine Flow Sensor, NPN-OC<br />
tc = up to <strong>10</strong> litres/min: 06 / up to 30 litres/min: 09<br />
tb = Temperature Range 120,180, or 350 °C<br />
sa = Output Signal 4..20 mA: I / or frequencyanalogue<br />
NPN-OC: F<br />
� Compact<br />
� <strong>Main</strong>tenance-Free<br />
� Resistant against high Temperatures<br />
� Low Pressure Loss<br />
� High Working Pressure Range<br />
� Small Time Constant due to low-mass Rotor<br />
Example for an order:<br />
Flow sensor for 0-<strong>10</strong> litres/min, max. temperature<br />
180 °C, frequency-analogue output, open collector:<br />
IS-F-TDM06-180-F<br />
Information in regard to the individually<br />
manufactured reaction calorimeters can be<br />
found in the chapters Plant Construction,<br />
Miniplant Technology, and Customised Reaction<br />
Calorimeters.<br />
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Here you will find:<br />
Fermentation Technology<br />
� RAMOS® Bioprocess Optimisation in Shaking Flasks<br />
� FluidTrain Fed-batch and Sample Drawing in Shaking Flask<br />
� OmniFerm® - Mini-Fermenter System<br />
� HiFerm-FCU Client-specific Fermenter Control Systems<br />
� Gmix Precision Gas Mixing Device<br />
� AlcoTect sterilisable alcohol probe<br />
� HiSense Precision Exhaust Gas Analytics<br />
� RQFeed Feeding Algorithm for optimal Productivity<br />
� Packed Bed Reactor<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Fermentation Technology<br />
RAMOS ® Bioprocess Optimisation in Shaking Flasks<br />
RAMOS (Respiration Activity MOnitoring System) is<br />
the standard measurement system online<br />
determination of respiration activities of prokaryotic<br />
and eukaryotic cultures in shaking flasks.<br />
The respiration rate is usually directly proportional to<br />
the number of cells and therefore enables<br />
continuous monitoring of the growth progression.<br />
Clear Advantages<br />
� More information about your microbiological<br />
processes<br />
� Distinction of process-related and biological<br />
effects.<br />
� Replaces expensive experiments in the<br />
fermenter.<br />
� Identical cultivation conditions as in your<br />
reference shaking flask.<br />
� Easy handling<br />
� Reduction of development time for<br />
bioprocess and cultivation conditions<br />
� Provides ideal screening conditions.<br />
� Enables rapid characterisation and targeted<br />
optimisation of media.<br />
� Reduction of test period to the actually<br />
required time.<br />
� Shortens the „time-to-market“.<br />
RAMOS was developed in cooperation with the<br />
department of biochemical engineering (Aachen<br />
University of Technology - UAS).<br />
RAMOS supplies the required information for:<br />
� Process Development<br />
� Process Optimisation<br />
� Media Optimisation<br />
� Fermentation Validation<br />
� Scale-Up<br />
Until now, in numerous processes evaluated so far,<br />
RAMOS has contributed to reveal key insights and<br />
Fields of Application<br />
� Continuous growth monitoring of prokaryotic and<br />
eukaryotic cultures including mammalian cells in<br />
shaking flasks<br />
� 8-fold parallel online measurement of the<br />
respiration activity under sterile conditions<br />
� Easy determination of characteristic values<br />
(OTR, CTR, RQ, µmax, kLa ...)<br />
� Bioprocess optimisation through early<br />
identification of oxygen and substrate limitation or<br />
product inhibition<br />
� Bioassays (toxicity assay, proliferation assay)<br />
� Development of suitable conditions in the primary<br />
and secondary screening (culture duration,<br />
media, operating conditions)<br />
� Reduction of the development times for ideal<br />
culture media and media conditions<br />
� Mass balance of fermentation processes<br />
� Quality control<br />
Potential<br />
Many experiments which previously could only be<br />
carried out laboriously in a fermenter with gas<br />
analytics, can now be conducted much cheaper and<br />
moreover in a fraction of the time with RAMOS.<br />
RAMOS pays off within short time due to the<br />
reduction of laboratory hours and development<br />
periods. In addition, production costs can be<br />
consistently and significantly reduced due to more<br />
efficient strains and culture procedures which can be<br />
discovered with the help of RAMOS.<br />
Up To now the development of suitable media has<br />
always been neglected due to the large connected<br />
expenditures. Exemplary for this fact is that LBmedia<br />
were used for decades as standard media for<br />
Escherichia coli bacteria.<br />
Already the initial investigation with RAMOS led to<br />
the insight that this medium does not allow an<br />
optimum growth due to its insufficient buffer effect.<br />
One can securely analyse the behaviour of microbial<br />
cultures with the help of measuring curves delivered<br />
by RAMOS, e.g.:<br />
� substrate limitation<br />
� oxygen limitation<br />
� product inhibition<br />
� diauxic growth<br />
the decisive impulses for research that has been<br />
worked on for years.<br />
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The demand for equal cultivation conditions for<br />
micro-organisms in normal shaking flasks and in<br />
RAMOS-Measuring flasks was given priority in the<br />
development of the plant. For this reason, the design<br />
of the flask was devised, in regard to the gas and<br />
hydrodynamics, so that it accords to a normal<br />
shaking flask in the bottom part containing liquid.<br />
In addition, a method was developed which enables<br />
to determine the oxygen transfer merely out of the<br />
variation of the oxygen partial pressure in the head<br />
space of the measuring flasks (no invasive<br />
electrodes). The system is patented.<br />
To ensure equivalent cultivation conditions, the gas<br />
composition above the culture liquid in the flasks of<br />
the measuring plant is adjusted identically to the<br />
composition in a normal flask. For this purpose, the<br />
gas flow is set client-specifically (depending on the<br />
type of sterile seals used).<br />
The system handling can be learned very easily and<br />
quickly. Within a short period of time, you will not be<br />
able to imagine to work without RAMOS<br />
The RAMOS System<br />
Fermentation Technology<br />
The RAMOS system fits on a normal benchtop. It is<br />
delivered completely installed with flasks, sensors,<br />
shaker, incubator, and control PC including an<br />
uninterrupted power supply system.<br />
For the familiarisation with the new methods, we<br />
offer one to two-day seminars and training<br />
programmes.<br />
Measurement of the Oxygen Transfer Rate<br />
The oxygen transfer rate is the most suitable and<br />
most universal variable to characterise and quantify<br />
the physiological condition and the activity of an<br />
aerobe culture because almost every metabolic<br />
activity is combined with oxygen consumption.<br />
The online measurement of the oxygen transfer rate<br />
in shaken bioreactors is state-of-the-art, however it<br />
is technically very laborious. The determination of<br />
the oxygen transfer rate in shaken bioreactors<br />
(shaking flasks) under sterile conditions has yet not<br />
been possible. RAMOS closes this gap and<br />
therefore combines the advantages of shaking flasks<br />
(little space required, cost-efficient, the possibility of<br />
parallel operation) with those of a stirred bioreactor<br />
(online-measurement).<br />
OTR- Phenomena<br />
The figure gives a schematic selection of biological<br />
phenomena and their effect upon the oxygen<br />
transfer rate (OTR). The diagrams show how the<br />
behaviour of a microbial culture can be<br />
systematically analysed with the help of the<br />
measuring curves delivered by RAMOS.<br />
Measuring of the Carbon Dioxide Transfer Rate<br />
Next to the oxygen transfer rate, the carbon dioxide<br />
transfer rate (CTR) and the respiratory quotient (RQ)<br />
are important sources of information for<br />
microbiologists.<br />
The temporal development of OTR, CTR and RQ<br />
can be clearly monitored online.<br />
In addition, further process parameters are<br />
calculated hereof. The evaluation can be extended<br />
according to user specifications.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
The development of OTR, CTR and RQ can be<br />
viewed online at your screen. The user interface<br />
presents also further computed parameters. This<br />
analysis can be adapted and extended to customer<br />
needs.<br />
From the general overview, showing all of the 8<br />
flask, each flasks diagram can be selected<br />
individually.<br />
Fermentation Technology<br />
The diagramm show charts of the OTR, CTR and<br />
RQ of an yeast fermenetation with crabtree effect.<br />
Technical Data (RAMOS installation for 8+6 shaking flasks including shaker and incubator.)<br />
Dimensions width: 690 mm, height: 750 mm, depth: 490 mm<br />
Weight approx. 66 kg (device without cooling)<br />
Size of Shaking Tray 420 x 420 mm<br />
Measuring Flasks 8 graduated flasks (250 ml) plus 6 auxiliary perpendicular shaking flasks (250 ml)<br />
for sampling or 8 graduated flasks (500 ml). Other sizes on request<br />
Electrical Connections 230 V AC, 3 A, other voltages upon request<br />
Gas Connections none, intake of ambient air<br />
Resolution Oxygen transfer rate
40<br />
Fermentation Technology<br />
Feeding and Sample Drawing in Shaking Flasks<br />
Fluid-Train ® -Technology<br />
Pharmaceutically relevant products, such as insulin,<br />
antibodies, and many more, are synthesised by<br />
microorganisms and cell cultures in bioreactors.<br />
With the Fed-batch regulation, the pro- or eukaryotic<br />
cells are fed on a defined and regulated basis. Up to<br />
now, the use of this procedure was restricted to<br />
large-scale production to achieve optimal biomass,<br />
respectively product yield.<br />
RAMOS-Fed-batch provides fully automatic Fedbatch<br />
fermentation in shaking flasks. The parallel<br />
technology and the approved measurement<br />
procedure of the RAMOS were expanded by an<br />
automated dosing system.<br />
RAMOS-Fed-batch makes controlled feeding<br />
possible and regulates the dosing rates based on<br />
the oxygen transfer rate (OTR) or respiration<br />
quotient (RQ). The cell number-independant key<br />
parameter RQ gives information on the physiological<br />
condition and is evaluated from the oxygen and<br />
carbon dioxide transfer rate (CTR) and thus allows a<br />
metabolism-dependant regulated dosing. The<br />
targeted regulation of the ideal RQ value can<br />
therefore be utilised to achieve maximum product<br />
yield. Based on these results, a feeding algorithm<br />
was developed, which enables to to keep a<br />
physiological condition constant without drawing any<br />
samples and analytics. The dosing amount is<br />
precisely recorded by the software.<br />
Technical Data<br />
The innovative Fluid-Train Dosing and Sample<br />
Drawing Technology (FTT) ensures a comminglingfree<br />
dosing and sample drawing conducted through<br />
merely one tube. Consequently, it is possible to<br />
seperatly and sterilely dose two or optionally more<br />
different media into each individual shaking flask.<br />
The combination with the RAMOS measuring data<br />
enables the feeding of the cultures with exactly the<br />
required amount of substrate, which leads to ideal<br />
culture growth and ideal production, respectively.<br />
The diagram show a dosing control upon the OTR<br />
value. The starting set point of 0,004 mol/l*h is being<br />
reduced after 45 hrs. to 0,002 mol/l*h. After approx.<br />
ca. 60, 90 and <strong>10</strong>0 std. the feeding of media will be<br />
temporarily interrupted.<br />
Parallel, up to 24 samples are, either event or<br />
schedule-controlled, are drawn from the culture<br />
containers and deposited (AutoSam-s). This makes<br />
unattended operation over night or weekend<br />
possible.<br />
Rinsing and cleaning cycles warrant a<br />
contamination-free operation. The Fluid-Train<br />
Technology is applied for the fermentation of proand<br />
eukaryotic organisms.<br />
Receiver Bottle 2 Feed-Media Bottles, 1 Bottle NaOH, 1 Bottle ultra-pure Water<br />
Dosing Rate 1-2 ml per flask and dosing cycle, cycle period<br />
Order Code Description<br />
VA-RAMOSFTT8 Program-controlled dosing and sample drawing , 8 channels including 4 receivers<br />
VA-RAMOSCON8 RAMOS Dosing regulation for control variable = OTR, CTR or RQ, 8 channels<br />
RAMOSFTT8 requires an AutoSam sampling device IL-AUTOSAM-xx and if necessary a cooling<br />
incubatro IL-AUTOSAM-KL.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Fermentation Technology<br />
OmniFerm ® - Mini Fermentation System<br />
The OmniFerm-Mini bioreactor system is suited for<br />
the controlled cultivation of bacteria and yeasts, as<br />
well as plant, insect and mammalian cell cultures. It<br />
features an especially small footprint so that several<br />
fermenters can be placed on a laboratory bench.<br />
This small-scale fermentation system closes the gap<br />
between shaking flasks and laboratory fermenters.<br />
Results which were achieved in shaking flask<br />
cultures can be validated parallelly with minimal<br />
substrate use and time expenditure.<br />
The modular design and the multiple equipping<br />
options allow maximum flexibility compared to<br />
conventional systems.<br />
The basic unit consists of a glass vessel with a<br />
stainless steel lid individually including the required<br />
sockets (bore holes: 2 x Pg 13.5, 7 x UNF 1/4-32, 1<br />
x UNF 1/2-20 for exhaust cooler). The pH-value is<br />
measured with an invasive electrode and can<br />
optionally be controlled by CO2/base or acid/base.<br />
The reactor is aerated via the head space, a gassing<br />
tube or a gassing ring.<br />
The optionally integrated off-gas analytics system<br />
unit records the progression of the OTR, CTR, RQ,<br />
OT, CT, and µmax online. These values allow drawing<br />
conclusions in regard to the proliferation rate and the<br />
metabolic activity of the biological culture. Due to the<br />
integrated pO2-electrode, conclusions can be drawn<br />
out of comparison between dissolved oxygen and<br />
oxygen transfer rate.<br />
The fermentation control and regulation is based on<br />
a <strong>HiTec</strong> <strong>Zang</strong> MSRmanager system with a special<br />
interface module. Amongst others, it is possible to<br />
connect laboratory apparatuses like balances,<br />
special sensor systems, analysers, dosing systems,<br />
etc. Due to the proven PMC technology,<br />
simultaneous parallel operation of up to 8 reactors is<br />
possible in bus or star-shaped alignment. Highprecision<br />
dosing controllers ensure controlled<br />
feeding in semi-continuous and continuous<br />
operation mode.<br />
Characteristics<br />
� full laboratory fermenter functionality<br />
� high degree of automation<br />
� various types of sensors<br />
� control based on online analysis is possible<br />
� tempering without heat carriers<br />
Options<br />
� Client specific equipment<br />
� Free programmable recipe control<br />
� Freely configurable test report<br />
� OTR- and RQ-based feed regulation for optimal<br />
product yield, e.g. within pharmaceutical protein<br />
production<br />
� Gravimetric dosing<br />
You have the choice between containers with<br />
operating volumes of 150 to 2000 ml. The reactor<br />
can be removed quickly and easily for sterilisation or<br />
preparation.<br />
The stirrer is powered by a rpm-regulated DC motor.<br />
High-class shaft seals ensure maximum sterility.<br />
Alternatively or complementary, a magnet stirrer is<br />
available for shear-tolerant micro-organisms.<br />
The gas supply of the reactor can be optionally<br />
controlled by a rotary flow meter manually, or<br />
automated with high-quality mass flow controllers. It<br />
is likewise possible to control the gas mixture for the<br />
fermenter with a Gmix gas mixing station. For<br />
distinct off-gas analytics, the precise compliance of<br />
gas flow rates must be ensured. The Gmix gas<br />
mixing device meets the highest demands in this<br />
respect.<br />
The trend-setting automation software LabVision® in<br />
combination with the required extension modules,<br />
like EasyBatch and HiBatch-recipe control, allows<br />
the solution of complex and automation-technically<br />
demanding problems, like individual fed-batch<br />
operation in up to 8 reactors.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
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Hardware<br />
Automation<br />
Software<br />
Plant<br />
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Equipment and<br />
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Process Analytics<br />
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42<br />
Technical Data<br />
Fermentation Technology<br />
A basic project including all functionalities necessary<br />
for standard batch operation, operating displays and<br />
parameterisations is expandable almost without<br />
limit. The detectable parameters are: pH, pO2, gas<br />
supply, gas mix, fed-batch control and chemostat<br />
operation mode.<br />
There are no limits of realisation to the model driven<br />
control based upon the established self describing<br />
programming language HiText.<br />
Dimensions width: 195 mm, depth: 300 mm, height: 500 mm<br />
Reactor Capacity 250 ml 600 ml <strong>10</strong>00 ml 2000 ml<br />
Working Capacity 150– 250 ml 300 – 600 ml 500 – <strong>10</strong>00 ml 500 – 2000 ml<br />
Bottle height (outer beand) 135mm 150mm 150mm 300mm<br />
Length of electrode 120 mm 120 mm 120 mm 225 mm<br />
Electrical Connection 230 V AC, 3 A<br />
Materials Glass, polished stainless steel 1.4573<br />
Sterilisation Auto-clavable<br />
Interfaces 2 x Pg 13.5, 7 x UNF 1/4-32, 1 x UNF 1/2-20<br />
Sensors temperature, optional pH, dissolved O2, Redox, level, foam, alcohol<br />
Pumps 4 rpm-regulated peristaltic pumps<br />
Temperature RT to 50 °C (optional, cooling with water or cooling agent)<br />
Gassing Dip tube, sparger or head space<br />
Shaft Sealing mechanical<br />
Order Code Description<br />
CG-OMNIFERM-ABK Control and Operating Unit for up to 8 OmniFerm Fermentation Units<br />
VA-OMNIFERM-FE-250 OmniFerm Fermentation Unit, reactor Capacity 150 to 250 ml, with four dosing pumps<br />
VA-OMNIFERM-FE-600 OmniFerm Fermentation Unit, reactor Capacity 300 to 600 ml, with four dosing pumps<br />
VA-OMNIFERM-FE-<strong>10</strong>00 OmniFerm Fermentation Unit, reactor Capacity 500 to <strong>10</strong>00 ml, with four dosing pumps<br />
VA-OMNIFERM-FE-2000 OmniFerm Fermentation Unit, reactor Capacity 500 to 2000 ml, with four dosing pumps<br />
VA-OMNIFERM-COOL Cooling functionality, integrate cooling coil for tapped water or thermostat, contol valve<br />
IL-OXYTECT-l Dissolved oxygen, autoclavable, PG 13.5 thread<br />
IL-PHFERM-l pH probe pH 0..14, 0 to 130°C, 0..<strong>10</strong> bar, autoclavable, PG 13.5 thread<br />
IL-ODFERM-l Cell count probe (optical density), autoclavable, PG 13.5 thread<br />
VA-OMNIFERM-CHILL Cooling thermostat 300 W at 15°C (provides up to 8 fermenters)<br />
VA-OMNIFERM-BGR Gassing Stirrer<br />
VA-OMNIFERM-AIRPUM Electronic controlled gasing pump for up to 4 fermenters, max. 550 l/h<br />
VA-OMNIFERM-GAS1 Gassing Control with pulsed Valve<br />
VA-OMNIFERM-GASMF Gassing Control with Massflow Controller<br />
VA-OMNIFERM-GASMF2 Gassingsregelung with two Massflow Controllers, e.g. Air and CO2<br />
VA-OMNIFERM-GASMF4MUX Gasing controll with massflow controller, tetra multiplexing, 4 gasses<br />
VA-OMNIFERM-REDOX Redox Sensor, auto-clavable, PG13.5 thread<br />
VA-OMNIFERM-LEV Level Sensor, auto-clavable<br />
VA-OMNIFERM-FOAM Foam Sensor, auto-clavable<br />
VA-OMNIFERM-FOLE Combination Sensor Level and Foam, auto-clavable<br />
VA-OMNIFERM-ETOH Alcohol Sensor, carrier gas supply, auto-clavable<br />
IL-HISENSE-m-x Exhaust Gas Analysis System for O2, OTR, CTR and CO2 for micro biology<br />
IL-HISENSE-c-x Exhaust Gas Analysis System for O2, OTR, CTR and CO2 for cell tissue cultures<br />
VA-OMNIFERM-RQFEED RQ-based Feeding<br />
X: amount of Channels, see HiSense, further volumes upon request<br />
Complementary products LabDos Precision Dosing Pump, AutoSam Sample Drawing System, Sterile Tube<br />
Pressure Sensor, Laboratory Scales can be found in other chapters.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Fermentation Technology<br />
HiFerm-FCU Customer-specific Fermenter Control Systems<br />
The level of automation of common bioreactors in<br />
microbiology and cell culture technology has a time<br />
lag of twenty years in relation to the automated<br />
laboratory reactor systems for chemical laboratories.<br />
<strong>HiTec</strong> <strong>Zang</strong> makes its experience of over 25 years in<br />
laboratory automation henceforth available for the<br />
customer-specific automated bioreactor.<br />
Example for a customised manufactured system with dosing<br />
pumps and touchscreen monitor.<br />
The advanced fermentation control unit HiFerm FCU<br />
allows the automated operation of a fermenter with<br />
an unprecedented level of automation.<br />
It is based on the MSRmanager automation system<br />
with a special interface module for sensors,<br />
actuators, and instruments.<br />
Sensors and actuators are connected with splash<br />
waterproof IP65 plugs and bushes, so that the<br />
connection is easy to install and, if necessary,<br />
disconnected quickly.<br />
The evaluation circuitry for oxygen, pH, temperature<br />
sensors etc. is integrated and can be expanded in<br />
various ways.<br />
For control of valves and pumps, analogue and<br />
digital outputs with short-circuit-proof semiconductor<br />
switches are provided.<br />
Analogue inputs for the connection of temperature<br />
sensors, electrodes, and miscellaneous sensors are<br />
digitalised with 24 bit and yield accordingly excellent<br />
measurement accuracy. Digital inputs allow<br />
connection of limit switches or malfunction<br />
annunciators of additionally connected devices.<br />
Via serial interfaces, laboratory devices like<br />
balances, special sensor systems, analysers, dosing<br />
systems, gas mixer, etc. can be connected.<br />
Dosing controllers for pump guided or gravimetric<br />
dosing are integrated. Thus, dosing systems can be<br />
driven by online measurement and analytic values.<br />
Interfaces<br />
� dissolved oxygen sensor (pO2),<br />
� direct connection for pH and redox sensors,<br />
(expandable to 2),<br />
� alcohol sensor,<br />
� 2 special inputs with current/voltage sources e.g.<br />
for a foam sensor,<br />
� 8 analogue inputs for flow rate controllers,<br />
temperature and pressure sensors etc.,<br />
� 8 analogue outputs for dosing pumps and stirrer<br />
control,<br />
� 16 digital outputs with short-circuit-proof<br />
semiconductor switch for magnetic valves,<br />
pumps, heater, etc.,<br />
� 14 digital inputs for fill level, pressure monitor,<br />
etc.,<br />
� 8 RS232 interfaces for balances, analysers,<br />
laboratory devices, etc.<br />
� 4 USB-Interfaces for keyboard, mouse, printer,<br />
memory stick, webcam, etc.<br />
With the automation software LabVision and the<br />
expansion modules, e.g. the EasyBatch or HiBatch<br />
Recipe Control, it is possible to realise complex and<br />
challenging automation tasks in an uncomplicated<br />
manner.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
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Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
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Process Analytics<br />
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44<br />
An user-friendly interface and an easy handling of<br />
the system assure a short preparation time.<br />
A basic project with the essential functions, views<br />
and parameterisations can be expanded nearly<br />
arbitrarily by the user.<br />
All analogue values are displayed as curves in a<br />
chart. Limit violations will be alerted and the whole<br />
event history is saved in all details. All values,<br />
parameters, and events are stored in an adaptive<br />
database.<br />
Features<br />
� expandable with analysers and special sensors<br />
� freely-programmable control software LabVision<br />
with numerous extension options<br />
� Complex Process Control is possible<br />
� touch screen for keyboard- and mouseless<br />
operation<br />
� automatic managed laboratory journal<br />
� optionally as complete system with pumps,<br />
sensors, etc.<br />
� Integration of other manufacturers' components is<br />
possible<br />
Order Code Description<br />
VA-HIFERM-FCU Fermenter Control Unit<br />
Fermentation Technology<br />
Fully automatic Research Fermenter (. Frings Bonn)<br />
Via the optional off-gas analysing module, the<br />
metabolic activity of biological cultures can be<br />
detected online via the respiration activity (OTR,<br />
CTR, RQ, OT, CT, µmax). With this knowledge you<br />
can easily draw conclusions in regard to substrate<br />
consumption and changes in metabolism or<br />
biomass.<br />
For dosing with fed-batch or continuous operation<br />
mode, up to five precision peristaltic pumps can be<br />
connected. They assure a secure and constant<br />
substrate supply for semi-continuous and continuous<br />
processes and a very accurate dosing of anti-foam,<br />
base or acid for pH control.<br />
Cell fermentater control unit<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Fermentation Technology<br />
Gmix – Gas Mixing Device<br />
The Gmix precision gas mixing device was<br />
especially developed for applications which require<br />
highest accuracy and reproducibility of gas mixtures.<br />
The gas mixing device is available in various<br />
configurations with one to four outlets. The gas<br />
mixture, consisting of up to four (opt. Six) gases, can<br />
be adjusted individually for every outlet.<br />
All inlets will be calibrated ex works upon customer<br />
request. Up to six gases for eache inlet can be<br />
calibrated. Default gases are air, N2, O2 and CO2.<br />
Units can be selected as ml/min (default: cm²/min)<br />
und g/min.<br />
The Gas Mixing Device Gmix is available both as a<br />
RAMOS expansion and as independant system.<br />
Application<br />
The application areas of the precision gas mixing<br />
device are, amongst others, all biological<br />
fermentations the require a gas composition. Due to<br />
the extremely precise gas mixture, the gas mixing<br />
device can also be deployed in physical technology<br />
and trace gas analytics. One further application area<br />
is the calibration of gas sensors.<br />
Advantages<br />
Flows and percentagae will be entered into and<br />
shown in self describing dialogue mass. The actual<br />
concentrations are kept constant with high class<br />
mass flow controllers (NO time multiplexing!).<br />
Thereby, an eminently consistent and precise dosing<br />
is assured. Due to the very compact design, the<br />
device requires little space.<br />
Control / Protective Devices<br />
Outlet pressures are measured and controlled for<br />
safety reasons.<br />
In case of exceedance of the adjusted outlet<br />
pressure, the gas supply will be automatically locked<br />
and an alarm signal will be activated.<br />
Operation with RAMOS<br />
During operation with RAMOS, the UI/work station of<br />
the gas mixing device is directly integrated in the<br />
RAMOS-software. The setpoint values are predetermined<br />
by the operator.<br />
The measured flow and fractions are indicated<br />
numerically and the temporal progression is<br />
displayed graphically.<br />
Customer specific solutions e.g. for aggressive<br />
gases can be buildt upon request.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Dispersing<br />
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46<br />
Technical Data (Gas Mixing Device)<br />
Fermentation Technology<br />
Dimensions Width: 240 mm, Depth: 320 mm, Height: 150 mm with up to 4 inputs<br />
Width: 340 mm with 5 or 6 inputs<br />
Weight approx. 6 kg with up to 4 inputs, 8 kg with 5 or 6 inputs<br />
Inputs<br />
Amount 2 – 6 gases, pneumatic connection 6/4<br />
Gases Air, N2, Oxygen (O2), Carbon Dioxide(CO2) by default, non-condensing, other<br />
gases upon request. Up to 6 gases posisble. Distribution is freely selectable by<br />
the user.<br />
Inlet pressure according to specifications, up to 11 bar abs, from approx. <strong>10</strong> slm/Input, higher<br />
pressure upon request<br />
Outlets<br />
Amount 1, pneumatic connection<br />
Outlet pressure according to specification, up to <strong>10</strong> bar abs.<br />
Min. pressure difference Approx. 1 bar, according to specifications<br />
Control principle Thermal massflow controller. Each component is controlled on each outlet,<br />
NO multiplexing!<br />
Prefilter Inlet filter 20 µm<br />
Flows<br />
Operating range Default: 0,05 slm – 50 slm set value, Dynamic 1:30<br />
optionally smaller or greater, dynamics 1:<strong>10</strong>0<br />
Uncertainty Default: < 1,5 % of set value, opt. +/- 0,3% of set value, +0,5% of measured value<br />
Reproducibility
Fermentation Technology<br />
Order Code Description<br />
IL-GMIX21 Gas mixing device (2 Inlets, 1 Outlets) for non-condensing gases (Air, O2, N2, CO2)<br />
Inlet 0,05 to 5 slm, uncertainty ±1,5 % of span, Dynamic 1:30<br />
IL-GMIX31 Gas mixing device (3 Inlets, 1 Outlets) for non-condensing gases (Air, O2, N2, CO2)<br />
Inlet 0,05 to 5 slm, uncertainty ±1,5 % of span, Dynamic 1:30<br />
IL-GMIX41 Gas mixing device (4 Inlets, 1 Outlets) for non-condensing gases (Air, O2, N2, CO2)<br />
Inlet 0,05 to 5 slm, uncertainty ±1,5 % of span, Dynamic 1:30<br />
IL-GMIX21-X Gas mixing device with increased accuracy (2 Inlets, 1 Outlets) for non-condensing/corrosive gases<br />
(Air, O2, N2, CO2). Inlet 0,05 to 5 sLM, uncertainty ±(0,3 % of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />
IL-GMIX31-X Gas mixing device with increased accuracy (3 Inlets, 1 Outlets) for non-condensing/corrosive gases<br />
(Air, O2, N2, CO2). Inlet 0,05 to 5 sLM, uncertainty ±(0,3 % of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />
IL-GMIX41-X Gas mixing device with increased accuracy (4 Inlets, 1 Outlets) for non-condensing/ corrosive gases<br />
(Air, O2, N2, CO2). Inlet 0,05 to 5 sLM, uncertainty ±(0,3 % of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />
IL-GMIX21-XET Gas mixing device with increased accuracy , stainless steel model, dead volume optimised (2 Inlets, 1<br />
Outlets) for non-condensing/ corrosive gases (Air, O2, N2, CO2). Inlet 0,025 to 0,5 sLM, uncertainty ±(0,3<br />
% of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />
IL-GMIX31-XET Gas mixing device with increased accuracy , stainless steel model, dead volume optimised (3 Inlets, 1<br />
Outlets) for non-condensing/ corrosive gases (Air, O2, N2, CO2). Inlet 0,025 to 0,5 sLM, uncertainty ±(0,3<br />
% of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />
IL-GMIX41-XET Gas mixing device with increased accuracy , stainless steel model, dead volume optimised (4 Inlets, 1<br />
Outlets) for non-condensing/ corrosive gases (Air, O2, N2, CO2). Inlet 0,025 to 0,5 sLM, uncertainty ±(0,3<br />
% of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />
IL-Gmix-S-RAMP Program Control for User-defined Profiles<br />
Systems with more outlets can be accomplished by<br />
cascading multiple devices or can be manufactured<br />
upon request.<br />
Upon request we can equip all devices with further<br />
options such as:<br />
System adjustments to special gases, aggressive<br />
gases, multiple gas datasets per inlet, analogue<br />
inputs 4...20 mA and controller for dissolved O2 and<br />
pH, digital input for externally control (standby, ramp<br />
start and stop).<br />
We are also able to construct a gas mixing device exactly according to your individual requirements and<br />
specifications!<br />
Order Code Description<br />
IL-ALCOTECT-d-l Alcohol Probe with Evaluation Unit for ethanol and methanol<br />
IL-ALCOTECT-AIRS Gas Supply synthetic air 20ml/min for alcohol probe, without gas bottle<br />
d: 19, 25 = Diameter 19 or 25 mm, l: <strong>10</strong>5, 120, 220, 320 = <strong>10</strong>5, 120, 220 or 320mm<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Calorimetry<br />
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Plant<br />
Construction and<br />
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Equipment and<br />
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Process Analytics<br />
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Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
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48<br />
Fermentation Technology<br />
OxyTect Optical Dissolved Oxygen Probe<br />
The OxyTect Alcohol Probe, amongst other<br />
application options, is suited for the monitoring of<br />
fermentation processes. The disadvantages<br />
connected with the conventional Clark probes are no<br />
longer existent.<br />
Product Features:<br />
� Exact online determination of the dissolved<br />
oxygen concentration<br />
� Compatible with the connections and signals of<br />
the conventional Clark probe<br />
� Sterilisable in-situ (SIP and CIP)<br />
� Auto-diagnosis<br />
� Immediately ready for measurement<br />
� High Durability<br />
� High Precision<br />
� Short Response Time<br />
� Exchangeable Sensor Cap<br />
Technical Data<br />
Probe Diameter 12mm<br />
Probe Length 120, 160, 225, 325 o. 425mm<br />
Process Connection PG-13,5 Thread<br />
Measuring Range 4 ppb/0,05%...300% O2 Air<br />
Saturation<br />
Detection Limit 0,01 Vol%<br />
Temperature Range -<strong>10</strong> °C bis 80 (130) °C<br />
Pressure Range -1...12bar<br />
Response Time < 30s<br />
98%<br />
Materials High Grade Steel, Silicone<br />
Output Signal 4..20mA, Clark-Signal,<br />
RS485 ( MODBus RTU<br />
Fieldbus), VP 8.0 Jack<br />
Power Supply 7..30V DC, 0,6W<br />
Order Code Description<br />
IL-OXYTECT-l Dissolved Oxygen Probe with Evaluation Electronics 4..20mA, Clark Signal, RS485 ( MODBus<br />
RTU Fieldbus), VP 8.0 Jack, autoclavable, PG 13.5 Thread<br />
L: 120, 160, 225, 325, 425mm = 120, 160, 225, 325 or 425mm<br />
Autoclavable pH-Probe<br />
This autoclavable ph-probe is in particular suited for<br />
the monitoring and controlling of fermentation<br />
processes.<br />
It is distinguished by especialially high durability and<br />
robustness.<br />
Product Features:<br />
� Low-<strong>Main</strong>tenance<br />
� 2 Pinhole Diaphragms<br />
� Duralid Electrolyte with high KCl-Content<br />
� High Durability<br />
� Fast and consistent Measurement Values<br />
� Proven H-Membrane<br />
� Low Alkaline Error<br />
� Extended application area in medias with<br />
extreme ion concentration, strongly oxidising<br />
characteristics, high alkali or acid concentrations<br />
or solvents<br />
� Integrated Pt<strong>10</strong>0<br />
Technical Data<br />
Probe Diameter 12mm<br />
Probe Length 120, 225, 325, 360 and<br />
425mm<br />
Process Connection PG-13,5 Thread<br />
Measurement Range 0 … 14 pH<br />
Measurement +- 0,1%<br />
Uncertainty<br />
Temperature Range 0 to 130 °C<br />
Pressure Range 0...<strong>10</strong>bar<br />
Connection SMEK- or VP- Plug-In Head<br />
Protection Class IP 68<br />
Order Code Description<br />
IL-PHFERM-l pH Probe pH 0..14, 0 to 130°C, 0..<strong>10</strong>bar, autoclavable PG 13.5 Thread<br />
l: 20, 225, 325, 360, 425 = 120, 225, 325, 360 and 425mm<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Fermentation Technology<br />
HiSense Emission Analysis System<br />
Precision Gas Analysis System for<br />
Biotechnology<br />
The HiSense Gas Analysis systems produced by<br />
<strong>HiTec</strong>, in contrary to conventional waste gas<br />
analysis technology, are also able to deliver the<br />
biological variables OTR, CTR and RQ. The devices<br />
are suited for R&D and laboratory applications within<br />
production and quality assurance.<br />
Measurement Technology:<br />
For the oxygen analysis, sensor are deployed which<br />
distinguish themselves by low interference, lownoise<br />
measurement results and long term stability.<br />
For the CO2- measurement, NDIR photometers and<br />
flow sensors with minimal zero point and inclination<br />
faults are deployed. Due to a novel special<br />
measurement method, the precise measurement of<br />
very minute activities both at small differences and<br />
minute measurement gas flows is possible.<br />
At the cell culture version, the deployment of<br />
additional measurement technology and the<br />
offsetting of unavoidable influences, e.g. total<br />
pressure, humidity etc., enables highly precise<br />
compensation. At conventional waste gas analysis<br />
methods and the low metabolic rates and long<br />
culture periods of cell cultures, the influence can be<br />
very significant and impede or even prevent a<br />
comparison of cultivations and make the deployment<br />
of a waste gas analysis system for quality assurance<br />
impossible. Usually, without the compensation of<br />
these factors, it is not possible to gain any useful<br />
measurement values at all.<br />
As the HiSense-c Precision Waste Gas Analysis<br />
System for cell culture and fermentation applications<br />
in addition, in most cases, is also able to perform the<br />
online determination of the true CO2 production<br />
(CER) at the usual carbonate buffer systems<br />
(optional pH input is required) usual in cell cultures.<br />
For this purpose, the faults are compensated which,<br />
due to the displacement of the of the HCO3-/-CO2<br />
balance by metabolites (e.g. lactate, NH3), make a<br />
useable measurement impossible. This is the only<br />
method that enables the determination of the actual<br />
RQ.<br />
The high measurement resolution enables reliable<br />
measurements under the usual conditions also at<br />
the low respiratory rates of animal cell cultures and<br />
within a very broad flow range (1.8 to <strong>10</strong>0.000 Ln/h,<br />
depending on version).<br />
For these measurements, hardly any expenditure for<br />
calibration is required.<br />
The software conducts all calculations, including all<br />
corrections/compensations, online. All measurement<br />
values are stored in a data base and can be<br />
displayed as current values or in the x-t-recorder.<br />
The export is conducted as data file (csv, txt and<br />
other formats) or via RS232/Windows-Pipe.<br />
Extension Options:<br />
The provision of further inputs/outputs, e.g. for<br />
pumps, valves and the arrangement of regulator<br />
circuits is possible on an optional basis.<br />
Additional inputs, e.g. for pH, temperature etc., are<br />
optionally provided for.<br />
Due to the free programmability in HiText Syntax<br />
(optional), additional algorithms, such as control and<br />
regulatory functions, can be integrated into the<br />
HiSenseTM Waste Gas Analysis Station. This also<br />
includes the RQFeed process for the optimisation of<br />
the productivity of cell cultures (if required, please<br />
request the respective special documentation). .<br />
A coupling with other systems, e.g. for<br />
control/regulation purposes is possible via network,<br />
RS232, RS485 and analogue interfaces (optional).<br />
Advantages:<br />
� 1 to 8(5) Measurement Channels for 1 to 4<br />
Fermenters, optional<br />
� High Resolution Measurement<br />
� Humidity Compensation (-c Version)<br />
� "True" OUR, CER and RQ Measurements (-c<br />
Version)<br />
� Low Interference<br />
� Possible Overpressure<br />
� Wear-resistant Sensor System<br />
� Compact Design<br />
� Additional Functions can be integrated<br />
� Optionally free Programmability<br />
� Numerous Coupling Options<br />
� Data Export is possible<br />
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Technical Data (HiSense-m for microbiology)<br />
Fermentation Technology<br />
General<br />
Dimensions Width: 458 mm, Depth: 370 mm, Height: 140 mm at small flows<br />
Operating Voltage 1<strong>10</strong> – 230 V, 50 – 60 Hz<br />
Current Consumption 3 A<br />
Temperature Range 0 °C up to 30 °C<br />
Protection Category<br />
Measurement Channels<br />
IP 20<br />
Supply air/ Exhaust gas 1 … 5 (optionally) channels for measurment in supply or exhaust gas<br />
Operating Range of Flow 18 - 180 Ln/h (l/h at 0 °C / <strong>10</strong>13 mbar), optionally from 6 to 300 Ln/h<br />
Pressure Loss < <strong>10</strong>00 Pa<br />
Input Pressure<br />
O2 Measurement<br />
atmospheric, 3 bar absolute<br />
Principle Solid Electrolyte System<br />
Measurement Range 0 – 60 Vol. %<br />
Measurement Uncertainty +/- 1 % v. Measurement Range<br />
Resolution 0.02 Vol. % at 20 % O2, better upon request<br />
Long-term Drift < 0.2 Vol. %<br />
Relevant Resolution<br />
CO2-Measurement<br />
Difference, humidity, and pressure-corrected, resolution approx. 0.02 %<br />
Principle NDIR<br />
Measurement Range 0 – 20 Vol.%, others upon request<br />
Measurement Uncertainty +/- 1 % v. measurement range<br />
Resolution 0.02 Vol.% at 5 % CO2<br />
Zeropoint Drift < +/- 0.2 %<br />
Automatic Compensation Humidity, Absolute Pressure<br />
Relevant Resolution<br />
Mass Flow Measurement<br />
Difference, humidity, and pressure-corrected, resolution
Technical Data (HiSense-c for cell cultures)<br />
Fermentation Technology<br />
General<br />
Dimensions Width: 458 mm, Depth: 320 mm, Height: 280 mm at small flows<br />
Operating Voltage 1<strong>10</strong> – 230 V, 50 – 60 Hz<br />
Current Consumption 3 A<br />
Temperature Range 0 °C up to 30 °C<br />
Protection Category<br />
Measurement Channels<br />
IP 20<br />
Supply air/ Exhaust gas 2..8 (optionally) ch. for measurment in supply or exhaust gas of 1..4 fermenters<br />
Operating Range of Flow 1,8 - 20 Ln/h (l/h at 0 °C / <strong>10</strong>13 mbar), optionally higher<br />
Pressure Loss < <strong>10</strong>00 Pa<br />
Input Pressure<br />
O2 Measurement<br />
atmospheric, 3 bar absolute<br />
Principle solid electrolyte system, optionally paramagnetic<br />
Measurement Range 0..25 vol. %, paramagnetic 0..60 vol. %<br />
Measurement Uncertainty +/- 1 % v. Measurement Range<br />
Resolution 0.02 Vol. % at 20 % O2, better upon request<br />
Long-term Drift < 0.2 Vol. %<br />
Relevant Resolution<br />
CO2-Measurement<br />
Difference, humidity, and pressure-corrected, resolution approx. 0.02 %<br />
Principle NDIR<br />
Measurement Range 0..20 Vol.%, others upon request<br />
Measurement Uncertainty +/- 0.5 % v. measurement range<br />
Resolution 0.01 vol.% at 5 % CO2<br />
Zeropoint Drift < +/- 0.05 %<br />
Automatic Compensation humidity, absolute pressure<br />
Relevant Resolution<br />
Mass flow measurement<br />
difference, humidity, and pressure-corrected, resolution approx. 0.005 %<br />
Principle thermal mass flow measurement, CO2-corrected<br />
Standard all channels<br />
Measurement uncertainty better than 2 % of measurement range<br />
Reproducibility 0,2 % of measurement range<br />
Prefilter Measurement None, sterile filtration at the fermenter<br />
Sample Gases<br />
OTR-CTR<br />
At non-condensing ambient temperature, exhaust gas cooling required<br />
Measurement Values approx. <strong>10</strong> min, with 2 fermenters approx. 15 min<br />
Sensitivity OTR** approx. 1 x <strong>10</strong>-5 Mol/l<br />
at 1 l culture volume, 5 vvh (V gas / V liquid / h ) gassing rate<br />
Sensitivity CTR** approx. 1 x <strong>10</strong>-5 Mol/l<br />
at 1 l culture volume, 5 vvh gassing rate<br />
Heating Period 120 min<br />
Further Measurement pH, OTR, CTR, OT, CT, TQ, CER, CE, RQ (corrected TQ), growth rate and<br />
Variables<br />
Operation<br />
many peripheral values like solvant O2, CO2...<br />
PC Operation via software included in scope of delivery with graphic user<br />
interface. Data export to Excel or as text data file.<br />
Order Code Description<br />
IL-HISENSE-c-2 Gas Analysis System for the Determination of O2 and CO2, OTR, CER and RQ, 2 channels<br />
IL-HISENSE-c-4 Gas Analysis System for the Determination of O2 and CO2, OTR, CER and RQ, 4 channels<br />
IL-HISENSE-c-8 Gas Analysis System for the Determination of O2 and CO2, OTR, CER and RQ, 8 channels<br />
Additional in- and outlets and data interfaces are realised with the components contained in the chapter<br />
„Laboratory Automation, Hardware“.<br />
For free programmability, the software module HiText contained in the chapter „ Laboratory Automation,<br />
Software“ is required.<br />
Automatic<br />
Laboratory<br />
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Fermentation Technology<br />
RQFeed Feeding Algorithm<br />
The development of highly productive scalable<br />
processes has significantly gained significance for<br />
industrial production of recombinant proteins. Since<br />
Fed-batch fermentations are comparatively reliable<br />
in operation and relatively easy to handle, they are<br />
widely distributed.<br />
Exactly tuned feeding of substrates can significantly<br />
increase the productivity. However, the control or<br />
even the regulation of the substrate feeding in a<br />
bioreactor is a great challenge. The compliance with<br />
ideal, as constant as possible culture parameters is<br />
of particular importance for cell cultures.<br />
Inappropriate culture conditions do not only lower<br />
the productivity of the cells, but also affect the<br />
chemical structure (e.g. of side chains) of the<br />
secreting protein (in particular the glycosylation)<br />
which causes an undesired heterogeneity of the<br />
active substance often combined with a significant<br />
influence upon the pharmacological effectiveness.<br />
Traditional feeding models are based on the<br />
parameters oxygen uptake rate (OUR) as well as<br />
offline measured cell density substrate<br />
concentration. Samples must be drawn during the<br />
process at regular intervals and subsequently<br />
analysed using external devices and rapid tests,<br />
respectively. Based on the result of these, the<br />
feeding rate is re-evaluated and adjusted. The<br />
regulation of the feeding rate based merely on these<br />
offline parameters often leads to suboptimal results.<br />
The <strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> has developed the novel<br />
regulation method “RQFeed” for cell cultures which<br />
is based on the respiration activity of the cells. The<br />
aerobic degradation of the substrate is accompanied<br />
by oxygen consumption (respiratory chain) which in<br />
ultimately influences the oxygen uptake OUR. This<br />
parameter thus allows to draw conclusions about the<br />
actual condition of the culture. Essential for the new<br />
Fed-batch technology is the RQFeed algorithm for<br />
the specific cultivation and production process. This<br />
algorithm is the result of intensive research into the<br />
cultivation progression as well as the deduction of<br />
according procedures and operational instructions.<br />
Organisms in aerobic fermentation consume oxygen<br />
and produce carbon dioxide. The cell-specific uptake<br />
rate of the essential substrates, e.g. glutamine and<br />
glucose, is closely connected with the oxygen<br />
uptake rate (OUR) and the carbon dioxide emission<br />
rate (CER). These two values enable the<br />
Order code Description<br />
SP-RQFEED-AC Feed Regulator based on RQ for Animal Cell Cultures<br />
Information to feed regulators for other cultures is available upon request.<br />
determination of the respiratory quotient (RQ), a key<br />
parameter that is independent of the number of<br />
cells. It reveals the different physiological states of<br />
the cell during batch cultivation and changes<br />
dependant on concentration of substrates and<br />
products so that alterations in the physiological<br />
condition can be detected and examined on a<br />
differentiated basis.<br />
Based on these findings, a feeding algorithm was<br />
developed which is able to maintain a desired<br />
physiological condition without the necessity of<br />
having to conduct offline measurements. This leads<br />
to a significant shortening of the fermentation<br />
periods, respectively to a significant increase in<br />
production rates.<br />
The diagram shows fermentation at two different RQ<br />
levels. At the RQ level 2, the productivity is not<br />
satisfactory, while Level 2 displays an ideal<br />
productivity.<br />
The RQFeed regulation algorithm is both suited for<br />
laboratory reactors as well as fermenters in pilot<br />
plants and in production. An exact determination of<br />
the RQ requires a controlled gas feed and an<br />
exhaust analysis system for the measurement of the<br />
CER and OUR.<br />
<strong>HiTec</strong> <strong>Zang</strong> offers the RQFeed regulation algorithm<br />
together with its OmniFerm laboratory fermenters in<br />
connection with a gas supply and analysis plant as<br />
an upgrading module for existing fermenters, but<br />
also on license basis for own use. In addition,<br />
training courses and instructions for the deployment<br />
of the algorithm in R&D applications and within<br />
large-scale production are also offered.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Packed Bed Reactor<br />
One alternative to stirred tank reactors are packed<br />
bed reactors with macroporous carriers for the<br />
cultivation of adherent animal cells which facilitates<br />
a continuous cultivation at high volume-oriented cell<br />
density and low shear stress. One significant<br />
advantage of this system is the opportunity to<br />
specially adjust the retention times of viruses and<br />
monoclonal antibodies under process conditions.<br />
When scaling up packed bed reactors, in particular<br />
the oxygen supply is problematic, as the height of<br />
the bed is restricted due to the oxygen depletion. A<br />
packed bed can, at minor overall lengths, be aerated<br />
up to <strong>10</strong> cm axially without occurring oxygen<br />
limitations in the upper sector of the packed bed. A<br />
further scale-up requires a radial aeration. By<br />
selecting a suited carrier, it is also possible to<br />
cultivate challenging cell types. In comparison to a<br />
stirred tank reactor, packed bed reactors possess a<br />
higher performance capacity in regard to the<br />
reachable volume-specific cell density and<br />
productivity. Due to the cell retention in the packed<br />
bed, integrated separation procedures using ceramic<br />
membranes are easy to realise. Additionally, the<br />
operation of a packed bed is very uncomplicated<br />
and cost-effective. The packed bed system has been<br />
used in the biochemical laboratory for the largescale<br />
production within the scope of the following<br />
projects:<br />
� Production of retroviral particles for genetherapeutic<br />
applications with the Paul-Ehrlich<br />
Institute and the Technical University Hamburg<br />
Harburg.<br />
� Production of monoclonal antibodies for in vitro<br />
diagnostics on novel ceramic carriers in<br />
cooperation with the company Therapharm<br />
Deutschland <strong>GmbH</strong>.<br />
Fermentation Technology<br />
Order Code Description<br />
VA-FESTBETT Packed Bed Reactor with microporous Carriers for the Cultivation of adherent Cell Cultures<br />
One of our main strengths is the construction of Special Custom Designs! Do not hesitate to contact<br />
us with any problem, we will help you to find a solution.<br />
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Here you will find:<br />
Laboratory Automation Hardware<br />
� LabManager®-Laboratory Automation Systems<br />
� MSRmanagerAutomation Systems<br />
� Interface Cards<br />
� PI Additional Equipment external<br />
� Power Supplies<br />
� Simulation and Test Apparatuses<br />
� Display and Operating Components<br />
� Peripheral Devices<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LabManager ® -System<br />
Laboratory Automation Hardware<br />
The LabManager system is an automation and/or<br />
process control system which isspecially suited for<br />
laboratory-, mini- and bench plants as well as for<br />
pilot plant stations. It is suitable for the automation of<br />
virtually all chemical-procedures reaching from<br />
batch, semi-batch and continuous processes.<br />
The LabManager system was developed in close<br />
cooperation with specialists from laboratories and<br />
pilot plant stations of major chemical companies. It<br />
has proved its worth in a great number of areas as a<br />
standard tool.<br />
In accordance with the requirements of the NAMUR<br />
Working Party for research process control computer<br />
systems (RPCCS), particular care has been directed<br />
to develop a user-friendly man-machine interface, a<br />
compact design, and a high application flexibility.<br />
The LabManager RPCCS especially distinguishes<br />
by the fact that it is also transparent and easy to<br />
handle for personnel inexperienced in automation<br />
technique even if they want to go into detail.<br />
LabManager, the Interface Genius!<br />
With help from the graphically programmable recipe<br />
control system HiBatch and a unit operation library, a<br />
customer without automation-technical knowledge<br />
can program the control program for a complex<br />
synthesis in a few minutes.<br />
The LabManager systems usually have a pay-back<br />
period below one year!<br />
� more intense use of your human and capitalresources<br />
� GLP/GMP raked working method without<br />
additional outlay<br />
� optimal reproducibility of your recipes, also<br />
after years<br />
� complete documentation of the entire process<br />
� savings during the instrumentation thanks to<br />
virtual devices<br />
� release of the lab personnel from routine<br />
activities<br />
� shorter "Time to Market" period for your<br />
products<br />
The most significant Results:<br />
� Increase of Quality<br />
� Lowering of danger potentials<br />
� Lowering of Costs<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Technology<br />
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Areas of Application<br />
Laboratory Automation Hardware<br />
The LabManager is particularly useful in the fields:<br />
� Chemistry<br />
� Pharmacology<br />
� Biotechnology<br />
� Food Technology<br />
� Environmental Technology<br />
� Quality Assurance<br />
� Experimental plants and test beds<br />
Applications<br />
Due to its unique flexibility, the possible applications<br />
in chemistry laboratories, in pilot plant stations, for<br />
Mini-Plants and in companies are virtually unlimited.<br />
Typical applications of the system in the fields of<br />
chemistry and pharmacology are:<br />
� Process Development<br />
� Process Optimization<br />
� One and multi boiler plants<br />
� Parallel reactor systems<br />
� High-Throughput-Experimentation<br />
� Bench Plant installations<br />
� Mini-Plant Installations<br />
� Continuous processes<br />
� Batch tasks<br />
� Semi batch tasks<br />
� Syntheses<br />
� Reaction calorimetry<br />
� Exothermic early warning system<br />
� Screening<br />
� Scale-Up<br />
� Polymerization<br />
� Distillation<br />
� Extraction<br />
� Crystallization<br />
� Production oriented Labs<br />
(Verification)<br />
� Raw material Control<br />
� Quality Assurance<br />
� Analysis Laboratories<br />
The system offers all the functionalities of the<br />
automation systems and process control<br />
engineering such as:<br />
� Measuring<br />
� Process control<br />
� Recipe control system<br />
� Automatic control<br />
� Process monitoring<br />
� Process visualization<br />
� Alarming<br />
� Online intervention<br />
� Logging<br />
� Filing<br />
All basic unit operations reaching from dosing up to<br />
sample drawing are automated (see Automation with<br />
the LabManager), all measured values are collected<br />
(see LabManager and Instrumentation), visualized<br />
(see LabVision), and automatically evaluated (see<br />
HiText and KalDas).<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Economic Feasibility Analysis<br />
Laboratory Automation Hardware<br />
The economic feasibility analysis is conducted<br />
using the example of a polymerisation process in the<br />
laboratory reactor.<br />
I. Manual Operation Mode<br />
Test:<br />
Operation Hours<br />
Weighing out 1<br />
Heating 1<br />
Dosing 4<br />
Secondary Polymerisation 4<br />
Emptying and Cleaning 1<br />
Total 11<br />
Start of test,e.g. at 7:30a.m., test completed at<br />
6:00p.m.<br />
According to this, only one test per day is possible!<br />
II. Automated Test Control with the<br />
LabManager<br />
Unattended procedure with:<br />
� Temperature Control<br />
� Dosing<br />
� Torque Monitoring<br />
� Recording of Test Data<br />
� Online Evaluation<br />
� Cleartext Protocol<br />
� Remote Alarming etc., if required<br />
Day Routine:<br />
First test start, e.g. at 8:00a.m., test completed at<br />
7:00p.m. In the meantime, the laboratory technician<br />
is free for the evaluation of last night's automatic run<br />
and the preparations for the next tests.<br />
Second test start, e.g. at 7:30p.m.<br />
Test completed at 6:30a.m. (unattended).<br />
According to this, two tests per day are now possible<br />
instead of one as before!<br />
The laboratory utilisation is improved by <strong>10</strong>0%.<br />
Cost Factors EUR<br />
Direct costs of the laboratory<br />
automation<br />
25,000.00<br />
Planning, familiarisation, plant<br />
upgrade<br />
<strong>10</strong>,000.00<br />
User Schooling 3,000.00<br />
Total Cost 38,000.00<br />
The amortisation period is evaluated out of the cost<br />
of one laboratory day (e.g. 750 Euro) and the total<br />
cost:<br />
Amortisation Period = 50 days!<br />
Even in the worst case scenario, assuming an<br />
improvement laboratory utilisation of merely 15%,<br />
which accords to a saving of 21,000 Euro annually,<br />
the amortisation period is still below one year!<br />
Additional beneficial Effects:<br />
GLP-conform mode of operation by a significant<br />
improvement of the documentation, the quality and<br />
reproducibility.<br />
A further Pay-Off Calculation for Chemistry<br />
Laboratories<br />
Catalyst Research Laboratory<br />
Test series (savings due to unattended night<br />
operation):<br />
Amortisation Period = 3 months!<br />
Colour R&D Laboratory<br />
Frequently changing recipes (savings due to<br />
simplified parameterisation via HiBatch recipe<br />
control and unattended night operation).<br />
Amortisation Period = 6 months!<br />
Naturally, similar results are achieved in continuous<br />
operation, if, instead of having personnel directly at<br />
the location, it is only necessary to have an on-call<br />
duty and remote alarming.<br />
It is a known fact that one day a product is launched<br />
on to the market earlier can result in six to sevendigit<br />
additional revenue.<br />
This clearly indicates how much laboratory<br />
automation is nowadays a must!!<br />
Using project moduls shortens the process of<br />
creating projects significantly.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 57<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
58<br />
Laboratory Automation Hardware<br />
Conventional Automation compared to LabManager ®<br />
With the application-oriented device components,<br />
typical automation basic functions, such as dosing,<br />
vacuum control, and the control of the reactor<br />
interior temperature, are realised in an<br />
uncomplicated manner.<br />
The application-oriented device components contain<br />
all required functionalities.<br />
The dosing device components additionally offer the<br />
possibility to automatically or manually refill the feed<br />
tank without dosing interruption. The<br />
parameterisation of controllers is no longer<br />
Example 1: A Dosing Circuit for Liquids<br />
necessary and thus, one of the greatest and most<br />
time-consuming problems in practice is eliminated.<br />
In contrary to conventional automation systems,<br />
almost all modifications, which may become<br />
necessary in the course of a running test, can now<br />
be realised without having to shut down the plant.<br />
In order to clearly demonstrate the cost-saving<br />
potential of the LabManager-System, several cost<br />
calculations for the conventional realisation of a few<br />
process and control tasks are compared with the<br />
according realisation by the LabManager-System.<br />
Realisation Method a.) Conventional b.) with the LabManager-System<br />
Costs:<br />
Operation Conventional realisation<br />
with EMSR/PLT +<br />
individual components<br />
EUR Realisation with LabManager +<br />
GraviDos from <strong>HiTec</strong>-<strong>Zang</strong><br />
Clarification of the Task 4 hours.* 320.00 2 hours 160.00<br />
Engineering 6 hours* 480.00 1 hours. 80.00<br />
Supply 4 hours* 320.00 1 hours 80.00<br />
Instrumentation of Components Pump, scales, valves, 2500.00 GraviDos complete, with feed tank and 1700.00<br />
Fittings<br />
fixtures for connection to reactor<br />
Additional Devices Interface for scales 500.00 none 0.00<br />
Additional Material Control cabinet, according<br />
cables and accessories<br />
etc.<br />
500.00 Included in deliver scope of GraviDos 0.00<br />
Realisation, Test 12 hours* 960.00 2 hours 160.00<br />
Documentation 4 hours* 320.00 No longer necessary as selfdocumenting<br />
0.00<br />
Costs<br />
* 80 EUR/hour<br />
Conventional 5900.00 <strong>HiTec</strong>-<strong>Zang</strong> 2180.00<br />
The savings due to the LabManager, according to<br />
the above calculation, already add up to 3720.00<br />
EUR! This is more than 60 %!<br />
Or, to express it differently, a conventional solution<br />
is 2.6 times more expensive!<br />
EUR<br />
Further savings are generated by the significantly<br />
reduced required space of the LabManagers and the<br />
significantly lower costs in case of later upgrading.<br />
Here, the typical saving can be up to<br />
70– 80 % !<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
Example 2: Dosing Control of Gases with Mass-Flow-Controller<br />
Costs:<br />
Operation Conventional realisation<br />
with EMSR/PLT +<br />
individual components<br />
EUR Realisation with<br />
LabManager<br />
Clarification 80 EUR/hour. 4 hours 320.00 1 hour 80.00<br />
Engineering 80 EUR/hour. 12 hours 960.00 1 hour 80.00<br />
Supply 80 EUR/hour. 4 hours 320.00 1 hour 80.00<br />
Instrumentation Mass-Flow-Controller 1500.00 Mass-Flow-Controller ready to<br />
connect<br />
1580.00<br />
Additional Devices Interface/Control Device/<br />
Regulator<br />
2000.00 Integrated in LabManager 0.00<br />
Additional Material Control cabinet , according<br />
cables and accessories<br />
500.00 Not necessary 0.00<br />
Realisation 80 EUR/Std. <strong>10</strong> hours 800.00 1 hour 80.00<br />
Documentation 80 EUR/Std. 4 hours 320.00 Not necessary 0.00<br />
Costs Conventional 6720.00 <strong>HiTec</strong>-<strong>Zang</strong> 1900.00<br />
The savings for this individual task already add up<br />
to far more than 4820.00 EUR, which is<br />
approximately 70 %!<br />
Or, to express it differently, a conventional solution<br />
is 3.5 times more expensive!<br />
The primal saving potential is however<br />
represented by its daily use, in particular in cases of<br />
frequently changing processes and frequently<br />
changing recipes. A new recipe control can be<br />
establishment by the laboratory technician with the<br />
help of LabVision's basis operations library within a<br />
timeframe which, if conventional methods were<br />
applied, would already be needed for the technical<br />
clarification alone.<br />
Additional significant savings are generated by the<br />
smaller footprint of the LabManagers and the lower<br />
costs in case of later upgrading.<br />
EUR<br />
Further substantial advantages in regard to costs,<br />
time, and result from the fact that the PLT system<br />
LabManager is easy to upgrade and expand in case<br />
the plant should require this at a later stage.<br />
The devices can expanded at any time by refitting<br />
of modules, panels and cards.<br />
The modification of the application software can be<br />
conducted by company-own personnel.<br />
Software modifications, new connection or exchange<br />
of sensors and actors can usually be realised while<br />
the plant is in operation without shutting it down.<br />
It is only possible to estimate the savings on a<br />
rudimentary basis, but according to the evaluation of<br />
long term users, they are considerable. These<br />
advantages are mainly demonstrated by the<br />
LabManager System in every day operation in<br />
laboratories and pilot plants.<br />
You want us to provide you with further arguments?<br />
We will gladly introduce you to experienced users of<br />
the LabManager System.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 59<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
60<br />
System Assembly<br />
Laboratory Automation Hardware<br />
An automation system is composed of a "Process-<br />
Interface (PI), in this case the LabManager and a<br />
User Interface (UI) which is a Personal Coumputer<br />
with Windos OS and LabVision Software.<br />
Functionality of the Process Interface<br />
The PI includes interfaces for the connection of the<br />
sensors, actuators, and devices. It is used for<br />
� Collecting<br />
� Converting and<br />
� Linking of Signals<br />
� Monitoring<br />
� Controlling<br />
� Automatic controlling etc.<br />
The LabManager and LabBox PIs are equipped for<br />
the special ambient conditions in the laboratory or<br />
pilot plant stations. The required space is kept to a<br />
minimum.<br />
Functionality of the User-Interface<br />
The UI, also referred to as work station, represents<br />
the interface between user and process. It is used<br />
for<br />
� parameterising<br />
� operating<br />
� monitoring<br />
� reporting<br />
� logging<br />
� saving<br />
� evaluation<br />
It is comprised of a special PC running under<br />
Windows XP or Windows Vista operating systems<br />
and the required LabVision-UI software modules.<br />
Service features<br />
The high functional level of the <strong>HiTec</strong> <strong>Zang</strong><br />
automation system, compared to a traditional<br />
automation system is particularly evident in regard to<br />
the following aspects.<br />
Interfaces<br />
The extensive choice of interfaces includes all<br />
currently available interfaces for sensors, actuators<br />
and devices.<br />
Interface panels with standardised connection<br />
sockets are available for the different types of<br />
interfaces.<br />
The construction and electric wiring of the<br />
connections comply with the recommendations and<br />
guidelines for laboratory devices of the chemical<br />
industry (NAMUR NE28 recommendation). Mistakes<br />
in the course of connecting are therefore excluded.<br />
Suitable connecting cables for the usual laboratory<br />
devices are available. For this reason, customers<br />
without special EMSR technical and electro<br />
technical knowledge are also able to connect<br />
sensors, actuators and laboratory devices<br />
independently.<br />
EMC robust interfaces guarantee a problem-free<br />
application also in case of deployment under rough<br />
conditions.<br />
Beyond the measurement value collection and<br />
control function units, the devices also include the<br />
most frequent process measurement and control<br />
(PMC) components for:<br />
� Signal input/output<br />
� Potential Separation<br />
� Amplifying<br />
� Filtering<br />
� Linearisation<br />
� Control<br />
� Automatic Control<br />
� Monitoring and Reporting (Alarming)<br />
� Supply of sensors and actuators with power<br />
External transducer, buffer amplifier etc. are not<br />
necessary anymore. Due to the consequently<br />
compact design of the devices, the required space is<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
reduced to a minimum so that they will fit in any rack<br />
or on any lab table. If conventionally constructed, a<br />
comparable technology would fill one or even<br />
several control cabinets.<br />
The possibility to mount the device directly on to the<br />
plant represents a significant help to save costs for<br />
project planning and cabling and allows an easy<br />
remounting of the instrumentation.<br />
LabManager mounted directly on the plant<br />
PMC Technical Functions<br />
� PID automatic controller (optional)<br />
� Adaptive automatic controller (optional)<br />
� Comparator<br />
� Ramp<br />
� Setpoint Value Generator (profiles)<br />
� Timer impulse<br />
� Timer Start Delay<br />
� Timer Falling Delay<br />
� Scales, Thermostat, Stirrer Communication<br />
� LabCom Communication<br />
� Temperature Compensation<br />
� Sample & Hold (scan and hold element)<br />
Mathematical Functions<br />
� Differentiator<br />
� Integrator<br />
� Adder<br />
� Subtractor<br />
� Multiplier<br />
� Divider<br />
� Averaging<br />
� Algebraic Polynomial<br />
Logical functions<br />
� AND-Element<br />
� OR-Element<br />
� XOR-Element<br />
� NOT-Element<br />
� Counter<br />
Switching Functions<br />
� Switch 1 to n<br />
� Switch n to 1<br />
� Monitored Output with/without Feedback Signal<br />
� Storage element (latch)<br />
Device components belong to the standard<br />
equipment of a PI and do not have to be ordered<br />
separately. (with exception of application-oriented<br />
device components, regulators, interface drivers)<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 61<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
62<br />
Laboratory Automation Hardware<br />
Modularity<br />
The PI devices can be adapted to modified or<br />
growing requirements at any time. It is therefore<br />
possible to upgrade a device, which was initially only<br />
used for measuring and monitoring, to a regulation<br />
and control system. In addition, a system can be<br />
extended almost infinitely by parallel connection of<br />
additional PIs.<br />
LabManager PIs are available in different casing<br />
sizes ranging from 6 to 20 free panel places. The<br />
LabBox1 and LabBox2 systems with 2 or 4 panel<br />
places are suited for smaller applications.<br />
The power supply for the sensor and the actuator<br />
can also be integrated into the devices.<br />
All devices are available as individually equipped<br />
basic devices or as devices with standard<br />
equipment.<br />
Connecting technology of the LabManager:<br />
standardised plug-and-socket connectors<br />
Safety<br />
Due to their integrated 32 bit processor, the PI<br />
devices are also able to run on an autonomous<br />
basis, i.e. without PC, and therefore comply with the<br />
requirements of the NAMUR safety standard<br />
category three. The CPU is monitored by a hardware<br />
watchdog device and boots automatically in case of<br />
troubles.<br />
To increase safety, an independent external<br />
watchdog device (HP-WDOGEXT1) is available.<br />
The UI (work station) is equipped with an<br />
uninterrupted power supply (UPS) and a UPS<br />
Management System. In case of a longer-lasting<br />
power failure, the UI will be shut down in a controlled<br />
manner.<br />
Alternative Connection Technology<br />
For plants with fixed wiring, the application of the<br />
MSRmanager System (process measurement and<br />
control - PMC) is intended, which uses terminal<br />
blocks with screw terminals instead of interface<br />
panels. The other functional features of the<br />
-manager are identical to those of the LabManager.<br />
A MSRmanager system can be extended with the<br />
same software and hardware options as a<br />
LabManager. You will find further information in the<br />
chapter „MSRmanager“.<br />
Connecting technology of the MSR-manager: terminal blocks with screw terminals<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
System Configurations<br />
Laboratory Automation Hardware<br />
LabVision supports different basic topologies and<br />
media for the coupling of PI and UI (user interface,<br />
respectively work station) in order to reach a suitable<br />
projecting of the system hardware.<br />
As standard, a PI is coupled with a UI through a<br />
RS232 serial interface. Light guides, RS485 twowire<br />
technology, or modems for 2 and 4 wire leased<br />
lines, or switched connection are available for the<br />
bridging of greater distances. The PIs can also be<br />
directly connected to a network via the Ethernet<br />
COM server. The UI can then be connected to every<br />
network socket.<br />
Several PIs can be connected to a UI via multiple<br />
interface cards.<br />
In order to run several independent applications,<br />
several LabVision licenses can work in parallel on a<br />
UI. All applications on UI use the same on-line data<br />
base so that every application can access the data<br />
points of other applications, if needed.<br />
With HiNet it is possible to cross-link several PIs to a<br />
UI. HiNet uses a RS485 twin wire as transmission<br />
medium and can cover distances up to approx. <strong>10</strong>00<br />
m on a normal telephone cable. HiNet is easy to<br />
project.<br />
An evaluation computer in the office can be linked to<br />
a LAN in order to retrieve data for the evaluation.<br />
Distributed systems can be realised with the<br />
platform-overlapping standard CORBA (Common<br />
Object Request Broker Architecture). The standard<br />
Ethernet <strong>10</strong>/<strong>10</strong>0/<strong>10</strong>00 MHz, RJ45 Twisted Pair is<br />
used as transport medium.<br />
Devices of other manufacturers and field buses,<br />
such as the PROFIBUS DP, or the HART protocol<br />
canbe integrated as well. For more information, see<br />
"Remote Access"<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 63<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
64<br />
Laboratory Automation Hardware<br />
Automation with the LabManager System<br />
The LabManager system is suitable for the<br />
automation of virtually all basic unit operations and<br />
functions such as:<br />
Temperature Regulation and Control<br />
Regulated temperature control by heat/cool<br />
thermostats, heating elements or steam for<br />
� heating and chilling reactions defined by random<br />
curves and/or profiles<br />
� distillation and reflux distillation<br />
� crystallization<br />
� determination of calorific key data<br />
� temperature-controlled dosing of exothermic<br />
mixtures<br />
The special device component for the temperature<br />
regulation cascade, in connection with the autoparameterisation<br />
module HiTune, cuts the timeconsuming<br />
parameterisation procedure down to a<br />
few minutes.<br />
For the reactions calorimetry, the LabKit-rc, as well<br />
as individual hardware and software modules are<br />
available for the refitting of existing plants.<br />
Dosing<br />
Controlled dosing of solid matters, liquids and gases<br />
via<br />
� Scales<br />
� Flow Rate Sensors<br />
� Clocked and proportional Valves<br />
� LabDos Peristaltic Pumps<br />
� SyrDos Syringe Dosers<br />
� AlfaDos -controlled Dropping Funnel<br />
� GraviDos-controlled Dropping Funnel<br />
� SolidDos Solid Matter Doser<br />
� Massflow Controller<br />
The self-parameterising dosing device components<br />
also enable an inexperienced user to configure a<br />
precisely working gravimetric dosing within a few<br />
minutes.<br />
Pressure and Vacuum<br />
Flexible strategies for the pressure regulation from<br />
vacuum up to high pressures also under difficult<br />
conditions.<br />
� Simple and dual sensor<br />
� Automatic changeover rough / detailed sensor<br />
� Vacuum and aeration program control<br />
� Inerting<br />
The self-parameterising device component vacuum<br />
regulation supports systems with and without<br />
ventilation/inerting.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
pH value / RedOx potential<br />
pH value and RedOx potentials can be monitored<br />
and controlled.<br />
� One-sided automatic control (acid or base)<br />
� Bilateral automatic control (acid and base)<br />
� Titration<br />
Stirring with Torque and Viscosity Recording<br />
The recording and control of the stirrer torque can<br />
supply important additional information about the<br />
process:<br />
� Viscosity<br />
� Dissipation<br />
� Reaction Progression<br />
Sampling<br />
Sampling and storage of liquids controlled with<br />
� Single valves<br />
� Multi-way valves<br />
� Pipetting Robot (AutoSam)<br />
In addition, many further, even more complex<br />
operations, such as phase separation,<br />
fractionated distillation or crystallisation, are<br />
available.<br />
Recipe Control<br />
Due to the extraordinarily powerful graphically<br />
programmable NAMUR and IEC compliant HiBatch<br />
recipe control module, users without automation<br />
technical experience can also establish complex<br />
recipe processes, e.g. multi-stage syntheses, within<br />
shortest time and have them conducted<br />
automatically (see HiBatch).<br />
For users who want to become operational as fast<br />
as possible, an extensive basis operation library<br />
(see SLGOPBIB) is available.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 65<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
66<br />
Instrumentation<br />
Laboratory Automation Hardware<br />
Principally all sensors, actuators and laboratory<br />
devices that have an interface or are supplied<br />
electrically can be linked in the automation, for<br />
example:<br />
Sensors<br />
� Temperature<br />
� Pressure<br />
� Flow<br />
� Level<br />
� Mass<br />
� pH/RedOx<br />
� Conductivity<br />
� Turbidity<br />
� Density<br />
� Gas concentration<br />
� Rotational speed<br />
� Phase bounderies<br />
Actuators<br />
� Actuators<br />
� Electrical and pneumatic bottom outlet valves<br />
� Pumps<br />
� Heating<br />
� Reflux Separators<br />
� Drives<br />
Laboratory Devices and Instrumenting<br />
Components<br />
� Scales (→ GraviDos)<br />
� Heating/cooling Thermostats<br />
� Stirrers (→ ViscoPakt)<br />
� Dosers (→ LabDos)<br />
� Phase Detection/Separation (→ PhaSep)<br />
� Analysers<br />
� Spectrometers (→ MoleculeEye)<br />
� Particle Sensor (→ ParticleEye)<br />
The LabManager Product Family<br />
The LabManager product family contains automation<br />
devices of different sizes that are built up in a<br />
modular way: The LabManager and the LabBoxes.<br />
This ensures that you always obtain a device which<br />
optimally meets your requirements. The connecting<br />
technology is uniformly based on connection boards<br />
with standardized plugs and sockets.<br />
Auxiliary Modules<br />
Further high-performance auxiliary modules and<br />
libraries extend the possibilities and facilitate work:<br />
� Adaptive automatic controllers for difficult control<br />
processes (SF-HICON)<br />
� LabCam for event controlled online picture<br />
documentation (SL-LABCAM)<br />
� IEC 61131 I control module in the PI, comparable<br />
to a SPS (SF AWL), SF-AWLPLUS<br />
� NAMUR RS232 interface driver for device<br />
couplings on UI and PI (SF-NAMSER)<br />
� On site mini terminal (HP-LABCOM1)<br />
� Remote <strong>Main</strong>tenance and Telecontrol<br />
� Remote Alarming<br />
� Auto-Tuning for Temperature Cascade Controller<br />
Libraries<br />
� Project module Library (SL-MODBIBALR)<br />
� Basis Operation Library (SL-GOPBIB)<br />
� Laboratory and Glass Apparatuses Library (SL-<br />
BIBRILK)<br />
☞<br />
You can find ready-to-use laboratory<br />
reactor systems in the chapter " Automated<br />
Laboratory Reactor Systems"<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LabManager1 and 2<br />
Laboratory Automation Hardware<br />
The LabManager1 is the standard device for lab<br />
and pilot plant stations with up to 50 interfaces.<br />
The LabManager2 can be equipped with more than<br />
a hundred interfaces. The devices are equipped<br />
with a 32 bit CPU card with a real time operating<br />
system, a battery backed-up clock, battery backedup<br />
(UPS) and specially interference-resistant<br />
CMOS RAM for the saving of parameterisation,<br />
FLASH-ROM for the operating system, PCM<br />
control programs and a watchdog switching for the<br />
hardware and software monitoring as well as a<br />
serial interface for the operator console (UI). The<br />
devices are connected to a serial interface of the<br />
UI through a file transfer cable or a fibre-optic light<br />
guide. Up to eight devices can be operated from an<br />
UI.<br />
The power saving CMOS technology hardly<br />
produces lost heat so that the devices can be run<br />
without forced ventilation. Hence, high reliability<br />
and service life are guaranteed.<br />
Assembly Options<br />
In the standard assembly of the LabManager, the<br />
interface panels form the rear panel of the device.<br />
In case the LabManager is built into a control<br />
cabinet, the interface panels can be mounted on<br />
the door, on the back or on the sides. A specific<br />
panel frame is available for this purpose (see panel<br />
frame).<br />
The robust metal case of the LabManager is<br />
suitable for free-standing arrangement and for the<br />
mounting on 19-inch control cabinets.<br />
The user interfaces for the basic device functions<br />
are placed on the front panel of the LabManager.<br />
Properties:<br />
� 32 bit CPU<br />
� 1 MB CMOS-RAM<br />
� 6 MB FLASH store<br />
� PC<strong>10</strong>4 bus enlargement plug<br />
� battery buffered real-time clock<br />
� Watchdog (monitor switching)<br />
All devices are available with standard equipment<br />
or as basic devices for individual mounting.<br />
If one needs two outlets to be supplied with a<br />
LabManager device or if little place is available on<br />
site for the connecting technique, the interface<br />
panels can be distributed on a maximum of two<br />
outstations (see outstations). In any case though,<br />
the maximum cable length should not be more<br />
than 5 m.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 67<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
68<br />
LabBox1 and 2<br />
Laboratory Automation Hardware<br />
LabBox devices basically offer all characteristics of<br />
the LabManager devices but are designed for fewer<br />
interfaces and can only be equipped with internal<br />
sensor and actuator power supplies on a limited scale.<br />
These devices are preferably used for data logging or<br />
automation of small laboratory plants.<br />
They are respectively available with standard<br />
equipment or as a basic device for individual<br />
mounting.<br />
LabBox1 completely equipped LabBox2 completely equipped<br />
Complete Systems<br />
These ready-for-use complete systems possess<br />
proven equipment.<br />
The UI software must be individually selected since<br />
different LabVision software packages are required<br />
for different applications.<br />
LabBox1<br />
(LK-LABBOX1K)<br />
LabBox2<br />
(LK-LABBOX2K)<br />
LabManager1<br />
(LK-LABMAN1K)<br />
At any time, you can adapt a standard system to<br />
your increasing requirements by retrofitting<br />
modules.<br />
You will find a detailed description of these complete systems on the following pages.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
LabBox1 Complete System (LK-LABBOX1K)<br />
This complete system is suitable as a monitoring<br />
and data logging system.<br />
Equipment of the PI:<br />
� 4 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />
� 4 analogue inputs (0/4...20 mA or<br />
� -<strong>10</strong> V ... +<strong>10</strong> V) for the connection of analogue<br />
sensors for pressure, flow etc. and devices with<br />
analogue output such as pH meters, thermostats<br />
etc.<br />
Equipment of the UI:<br />
� State-of-the-art processor *<br />
� 1 GB RAM<br />
� Uninterrupted power supply (UPS)<br />
� UPS Management System<br />
� Pre-installed Windows XP or Windows Vista<br />
* The equipment is regularly adapted to the current standard.<br />
The UI can optionally be delivered in a desktop,<br />
tower or mini tower case and with modified<br />
equipment (see chapter Display and operating<br />
Components). The software is installed ready to use.<br />
The LabVision software update service is available<br />
for one year free of charge.<br />
The system consists of the following components:<br />
Amount Order Code Description<br />
1 LG-LABBOX1 LabBox1 standard device, for equipment see LG-LABBox1<br />
1 CG-ABK1 <strong>HiTec</strong> UI with UPS power supply and UPS management system,<br />
for equipment see CG-ABK1<br />
1 CP-M20TFTWS 20 Inch Widescreen TFT Monitor<br />
The LabBox1 can be upgraded with an additional<br />
panel with eight inputs or outputs. Up to four serial<br />
interface modules (HD-RS2329(P)L) can be<br />
equipped on the basis panel.<br />
The system can be upgraded with additional<br />
modules, e.g. internal power supply for sensors,<br />
data logger function (HS-NGS242), data logger<br />
function (SF-DATLOG), IEC 61131 I control module<br />
(SF-AWL, SF-AWLPLUS) etc.<br />
Delivery Scope Ready-to-use system (excl. LabVision software), LabBox1, UI with monitor and<br />
UPS, UI / PI cable, 230 V cable, manual<br />
Order Code Description<br />
LK-LABBOX1K LabBox1 standard system<br />
HS-NGS242 Optional 24 V internal power supply for actuators and sensors supply<br />
Recommended software package:<br />
Order Code Description<br />
SL-LABVIS LabVision basic package<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 69<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
70<br />
Laboratory Automation Hardware<br />
LabBox2 Complete System (LK-LABBOX2K)<br />
This complete system is for example suitable for the<br />
automation of lab reactor plants of medium<br />
complexity.<br />
Equipment of the PI:<br />
� 8 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />
� 8 analogue inputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V) for<br />
the connection of analogue sensors for pressure,<br />
flow etc. and devices with analogue output as pH<br />
meters, thermostats etc.<br />
� 8 analogue outputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V)<br />
For connecting devices with analogue input such<br />
as stirrer, thermostat, dosing pump etc.<br />
� 8 digital outputs (24 V, binary, PWM and PFM)<br />
For connecting binary actuators such as<br />
magnetic valves, heating, pumps, etc.<br />
� 2 serial RS232 interface modules for the<br />
connection of scales, devices and analysers with<br />
serial interface<br />
� Integrated sensor and actuator power supply<br />
Equipment of the UI:<br />
� State-of-the-art processor *<br />
� 1 GB RAM<br />
� Uninterruptible power supply (UPS)and UPS<br />
management system<br />
� Pre-installed Windows XP or Windows Vista<br />
* The equipment is regularly adapted to the current standard.<br />
The UI can optionally be delivered in a desktop,<br />
tower or mini tower case and with modified<br />
equipment (see chapter Display and operating<br />
Components). The software is installed and readyto-use.<br />
The LabVision software update service is<br />
available for one year free of charge.<br />
The system consists of the following components:<br />
Amount Order Code Description<br />
1 LG-LABBOX2-2 LabBox2 standard device with DAP8A, for equipment see LG-LABBOX2-2<br />
1 CG-ABK1 <strong>HiTec</strong> display and server components with UPS and UPS power supply<br />
management system, for equipment see CG-ABK1<br />
1 CP-M20TFTWS 20 Inch Widescreen TFT Monitor<br />
The system can be updated with additional modules,<br />
2 additional serial interfaces (HD-RS2329(P)L), IEC<br />
61131 I control module (SF-AWL, SF-AWLPLUS),<br />
adaptive controllers (SF-HICON), NAMUR interface<br />
driver for serial interfaces (SF-NAMSERxx) etc.<br />
Delivery Scope Ready to use system (excl. LabVision software), LabBox2, ABK1 with monitor and<br />
UPS, UI / PI cable, 230 V cable, manual<br />
Order Code Description<br />
LK-LABBOX2K-2 LabBox2 basic kit with LP-DAP8A<br />
Instead of the LP-DAP8A panel, a multi-purpose panel with 4 digital inputs and 4 digital outputs can be<br />
equipped.<br />
Order Code Description<br />
LK-LABBOX2K-1 LabBox2 standard system with LP-DE4DA4PA<br />
Recommended software packages (alternative):<br />
Order Code Description<br />
SL-LABVIPKONL Software package for LabBox2 For connecting small continuous-processes<br />
SL-LABVIPBATL Software package for LabBox2 For connecting small batch processes<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
LabManager Complete System (LK-LABMAN1K)<br />
This complete system is particularly suited for the<br />
automation of lab reactor plants of medium<br />
complexity.<br />
Equipment of the PI:<br />
� 8 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />
� 8 analogue inputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V) for<br />
the connection of analogue sensors for pressure,<br />
flow etc. and devices with analogue output as pH<br />
meters, thermostats etc.<br />
� 8 analogue outputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V)<br />
For connecting devices with analogue input as<br />
stirrer, thermostat, dosing pump etc.<br />
� 8 digital inputs (binary and frequency) for the<br />
connection of binary sensors such as filling level<br />
monitor, pressure regulators or status or alarm<br />
outputs of devices<br />
� 8 active digital outputs (24V, binary, PWM and<br />
PFM) For connecting binary actuators such as<br />
magnetic valves, heating, pumps, etc.<br />
� 2 RS232 serial interfaces for the connection of<br />
scales, devices and analysers with serial<br />
interface<br />
� Integrated sensor and actuator power supply<br />
� A free panel place for retrofitting<br />
Equipment of the UI:<br />
� State-of-the-art processor *<br />
� 1 GB RAM<br />
� Uninterrupted power supply (UPS)<br />
� UPS management system<br />
� Pre-installed Windows XP or Windows Vista<br />
* The equipment is regularly adapted to the current standard.<br />
The system consists of the following components:<br />
The UI can optionally be supplied in a desktop,<br />
tower or mini tower case and with modified<br />
equipment (see chapter Display and operating<br />
Components). The software is installed and readyto-use.<br />
The LabVision software update service is<br />
available for one year free of charge.<br />
The system can be updated with additional modules<br />
such as IEC 61131 I control module (SF-AWL, SF-<br />
AWLPLUS), adaptive automatic controllers (SF-<br />
HICON), NAMUR interface driver for serial<br />
interfaces (SF-NAMSERxx) etc..<br />
The free panel place can be equipped according to<br />
your requirements, for example with a thermocouple<br />
panel (LP-THP8 + interface card), a measurement<br />
module for load cells (HK-GRADOMS...) or a high<br />
precision temperature measurement module (HK-<br />
AD24PX8).<br />
Amount Order Code Description<br />
1 LG-LABMAN1 LabManager1 standard device, for equipment see LG-Labman1<br />
1 CG-ABK1 <strong>HiTec</strong> display and operating components with uninterrupted power supply and<br />
USV management, for equipment see UI1<br />
1 CP-M20TFTWS 20 Inch Widescreen TFT Monitor<br />
Delivery Scope Ready to use system (excl. LabVision software), LabManager1, UI with monitor<br />
and UPS, UI / PI cable, 230 V cable, manual<br />
Order Code Description<br />
LK-LABMAN1K Complete system with LabManager1<br />
Suitable software packages (alternative):<br />
Order Code Description<br />
SL-LABVIPBAT Software package for LabManager1 for running medium sized batch processes<br />
SL-LABVIPKON Software package for LabManager1 for running medium sized continuous-processes<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 71<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
72<br />
Standard Devices<br />
Laboratory Automation Hardware<br />
The standard devices possess proven equipment. At<br />
any time, you can adapt a standard system to your<br />
increasing requirements by retrofitting.<br />
These standard devices are included in the offered<br />
complete systems or are used for the extension of<br />
existing systems.<br />
LabBox1 Standard Device (LG-LABBOX1)<br />
This device is suited as measurement value collection and monitoring system<br />
For technical data, see LB-LABBOX1B.<br />
Equipment:<br />
� 4 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />
� 4 analogue inputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V) for<br />
the connection of analogue sensors for pressure,<br />
flow etc. and devices with analogue output such<br />
as pH meters, thermostats etc.<br />
Amount Order Code Description<br />
1 LB-LABBOX1B LabBox1 basic device<br />
1 HK-AD20NMUX8 analogue/digital 20 bit converter card solution, 8-channel multiplexer<br />
1 LP-AE4PT4PA NAMUR compliant plug-in panel with 4 0/4..20 mA current or <strong>10</strong> V..+<strong>10</strong> V<br />
voltage inputs, and 4 Pt<strong>10</strong>0 in two to four conductor technology<br />
1 HS-NGS242S 24 V DC, stabilised, 2,5 A<br />
The LabBox1 can be upgraded with an additional<br />
panel with eight inputs or outputs.<br />
Up to four serial interface modules (HD-<br />
RS2329(P)L) can be equipped. If more serial<br />
interfaced are intended to be equipped an additional<br />
card (HK-SER8ECB) is recommended.<br />
Delivery Scope LabBox1, UI/PI cable, power supply cable, manual<br />
Order Code Description<br />
LG-LABBOX1 LabBox1 standard device<br />
HK-SER8ECB Serial I/O card , 8 channels<br />
The system can be upgraded with additional<br />
modules, such as an integrated power supply for<br />
sensors and actuators (HS-NGS242), data logger<br />
function (SF-DATLOG), IEC 61131 I control module<br />
(SF-AWL, SF-AWLPLUS) etc.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
LabBox2 standard device (LG-LABBOX2)<br />
This standard device, amongst other applications, is<br />
particularly suited for the automation of lab reactor<br />
plants of medium complexity<br />
Equipment:<br />
� 8 Pt<strong>10</strong>0 inputs (-200 °C ... +600° C)<br />
� 8 analogue inputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V) for<br />
the connection of analogue sensors for pressure,<br />
flow etc. and devices with analogue output such<br />
as pH meters, thermostats etc.<br />
� 8 analogue outputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V)<br />
For connecting devices with analogue input such<br />
as stirrer, thermostat, dosing pump etc.<br />
� 8 digital outputs (24 V, binary, PWM and PFM)<br />
For connecting binary actuators such as<br />
magnetic valves, heating, pumps, etc.<br />
� Integrated sensor and actuator power supply<br />
� 2 serial RS232 interface modules for the<br />
connection of balances, devices and analysers<br />
with serial interface<br />
The standard device consists of the following components:<br />
All panel places of the device are assigned.<br />
The device can be upgraded with additional modules<br />
such as an IEC 61131 I control module (SF-AWL,<br />
SF-AWLPLUS), adaptive automatic controller (SF-<br />
HICON), NAMUR interface driver for serial<br />
interfaces (SF-NAMSERxx) as well as two more<br />
serial interfaces.<br />
For technical data, see LB-LABBOX2B.<br />
Amount Order Code Description<br />
1 LB-LABBOX2B LabBox basic device<br />
1 HK-AD20NMUX16 Analogue/digital 20 bit converter card resolution, 16 channel multiplexer<br />
1 LP-AEP8A Connection panel/board with 8 0/4..20 mA current or <strong>10</strong> V..+<strong>10</strong> V voltage<br />
inputs, integrated sensor<br />
1 LP-PTP8 NAMUR compliant interface panel for 8 Pt<strong>10</strong>0 in two to four conductor<br />
technology<br />
1 HK-DA812UI D/A 8 x 12 bit converter card, for analogue output -<strong>10</strong> ... <strong>10</strong> V or 0/4...20 mA<br />
1 LP-AAP8UI Interface panel for eightfold analogue output with current outputs (0/4...20<br />
mA) and voltage outputs (-<strong>10</strong>..+<strong>10</strong> V)<br />
1 HK-DEA16N digital input/output card with 2 x 8 inputs and 2 x 8 outputs.<br />
1 LP-DAP8A Interface panel with 8 digital outputs, 24V relays change-over contact, max. 3<br />
A resilient, 3 A power supply (short-circuit -proof)<br />
1 HK-SER8ECB additional serial card SER8ECB for the serial interface<br />
1 HS-NGS243 DC supply 24 V / 3 A calendared for actuators.<br />
1 HS-NGS241A DC supply 24 V / 1.5 A calendared for sensors.<br />
2 HD-RS2329L 9-pin RS232 interface<br />
Delivery Scope LabBox2, UI / PI cable, power supply cable, manual<br />
Order Code Description<br />
LG-LABBOX2-1 LabBox2 standard device 1 with DE4DA4PA<br />
Instead of the LP-DE4DA4PA panel, a panel<br />
LP-DAP8A with 8 digital outputs can be equipped.<br />
Order Code Description<br />
LG-LABBOX2-2 LabBox2 standard device 2 with LP-DAP8A<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 73<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
74<br />
Laboratory Automation Hardware<br />
LabManager Standard Device (LG-LABMAN1)<br />
This standard device is particularly suited for the<br />
automation of lab reactor plants of medium<br />
complexity.<br />
Equipment:<br />
� 8 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />
� 8 analogue inputs (0/4...20 mA or -<strong>10</strong> ... +<strong>10</strong> V)<br />
for the connection of analogue sensors for<br />
pressure, flow etc. and devices with analogue<br />
output such as pH meters, thermostats etc.<br />
� 8 analogue outputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V)<br />
For connecting devices with analogue input<br />
such as stirrer, thermostat, dosing pump etc.<br />
� 8 digital inputs (binary and frequency) for the<br />
connection of binary sensors such as filling<br />
level monitor, pressure monitors or status or<br />
alarm outputs of devices<br />
� 8 active digital outputs (24 V, binary, PWM and<br />
PFM) for connecting binary actuators such as<br />
magnetic valves, heating, pumps, etc.<br />
� 2 RS232 serial interfaces for the connection of<br />
balances, devices and analysers with serial<br />
interface<br />
� Integrated sensor and actuator power supply<br />
� A free panel place for retrofitting<br />
� Serial add-on card SER16ECB for serial<br />
interfaces<br />
The standard device consists of the following components:<br />
The device can be upgraded with additional<br />
modules such as an IEC 61131 I control module<br />
(SF-AWL, SF-AWLPLUS), adaptive automatic<br />
controller (SF-HICON) or NAMUR interface driver<br />
for serial interfaces (SF-NAMSERxx) etc.<br />
The free panel place can be randomly equipped,<br />
for example with a thermocouple panel (LP-THP8<br />
+ interface card), a measurement module for load<br />
cells (LP-DMS4DA4PT + HK-AD24DMS4) or a<br />
high precision temperature measurement module<br />
(LP-PTPRP8 + HK-AD24PX8).<br />
For technical data, see LB-LABMAN1B.<br />
Amount Order Code Description<br />
1 LB-LABMAN1B LabManager basic device<br />
1 HK-AD20N Analogue/digital 20 bit converter card solution, floating secondary bus for the<br />
connection of multiplexer cards<br />
1 HK-HMUX Semiconductor 16 channel multiplexer card<br />
1 LP-AEP8A Plug-in panel with 8 0/4..20 mA current or -<strong>10</strong> V..+<strong>10</strong> V voltage inputs, integrated<br />
sensor feeding<br />
1 LP-PTP8 NAMUR compliant Interface panel for 8 Pt<strong>10</strong>0 in two to four conductor<br />
technology<br />
1 HK-DA812UI D/A 8 x 12 bit converter card, for analogue output -<strong>10</strong> ... <strong>10</strong> V, or 0/4...20 mA<br />
1 LP-AAP8UI Interface panel for fourfold analogue output with current (0/4...20 mA) and<br />
voltage outputs (-<strong>10</strong>..+<strong>10</strong> V)<br />
1 HK-DEA16N Digital input/output card with 2 x 8 inputs and 2 x 8 outputs, binary inputs,<br />
frequency and event count, binary outputs, pulse-width and pulse frequency<br />
modulations<br />
1 LP-DAP8A Interface panel with 8 digital outputs, 24 V relay change-over switch, capable of<br />
bearing maximum of 1 A, LED display,<br />
1 LP-DEP8 Interface panel with 8 active digital inputs<br />
1 HS-NGS241A DC supply 24 V / 1,5 A calendared for sensors<br />
1 HS-NGS243 DC supply 24 V, 3 A calendared for actuators<br />
1 HK-SER8ECB Additional channel serial interface card SER8ECB<br />
2 HD-RS2329PL 9-pin RS232 interface<br />
Delivery Scope LabManager1, UI/PI cable, power supply cable, manual<br />
Order Code Description<br />
LG-LABMAN1 LabManager1 standard device<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
Basis devices for individual supply<br />
A basic device for individual mounting will be<br />
equipped with interface cards and interface panels<br />
according to your requirements.<br />
LabBox1<br />
basis device<br />
(LB-LABBOX1B)<br />
2 free panel places<br />
LabBox2<br />
basis device<br />
(LB-LABBOX2B)<br />
4 free panel places<br />
LabManager1<br />
basis device<br />
(LB-LABMAN1B)<br />
6 free panel places<br />
LabManager2<br />
basis device<br />
(LB-LABMAN2B)<br />
13 free panel places<br />
Example of special<br />
building:<br />
LabManager3 basis<br />
device (LABMAN3B)<br />
20 free panel places<br />
A LabManager PI is for exampleassembled as<br />
follows:<br />
� a basic device (LB-LABMAN1B),<br />
� an analogue/digital converter card (HK-AD20N),<br />
� a multiplexer card (HK-HMUX)<br />
� two interface panels (for example LP-AEP8 & LP-<br />
PTP8) as well as<br />
� a UI, e.g. a CG-ABK1 with<br />
� LabVision software.<br />
This configuration includes eight universal potentialfree<br />
analogue inputs and eight inputs for Pt<strong>10</strong>0<br />
temperature sensors and is suitable for monitoring<br />
and data logging.<br />
If the system is not supposed to be updated later, a<br />
LabBox would be the more cost-efficient alternative.<br />
If more than seven interface panels, including the<br />
basis panel, are needed, it is necessary to use a<br />
double height LabManager2. Seven more panel<br />
places are available due to the additional height unit.<br />
In case of even greater interface requirement,<br />
several more devices can be run by one UI.<br />
Common Features<br />
All devices are equipped with a CPU32 card, a basis<br />
panel and a power supply.<br />
A power supply for sensors and actuators can<br />
optionally be integrated into the devices in order to<br />
obtain a compact and comprehensive automation<br />
solution.<br />
The corresponding UI LabVision software will also<br />
be individually customised to your precise<br />
requirements.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
76<br />
LabBox Basis Device<br />
Laboratory Automation Hardware<br />
As an intelligent central processing unit, a LabBox<br />
basis device contains a 32 bit controller card<br />
(CPU32), a basis panel and a power supply for the<br />
cards.<br />
Next to a low heat device socket for the power<br />
supply and the main switch, the basis panel has a<br />
RS232 interface (opt. RS485 or Ethernet) for the<br />
connection of the UI. Up to four more serial<br />
interfaces can be mounted on the basis panel.<br />
A minimum system can be arranged for example as<br />
follows:<br />
� a basic device (e.g. LB-LABBOX1B)<br />
� an analogue/digital converter card with 8-channel<br />
multiplexers (HK-AD20NMUX8) with<br />
� an interface panel (e.g. LP-AE4PT4P) and<br />
� a user interface UI (CG-ABK1).<br />
With this setup, a LabBox is suitable for monitoring<br />
and data logging with four universal potential-free<br />
analogue inputs (-<strong>10</strong>..+<strong>10</strong> V, 0/4-20 mA) for the<br />
connection of any analogue sensors and/or signals<br />
and four inputs for the connection of Pt<strong>10</strong>0<br />
temperature sensors. The device is integrated to the<br />
LK-LABBOX1K standard system package in this<br />
configuration.<br />
If the system is supposed to be upgraded later with<br />
a total of more than eight interfaces, a LabBox2,<br />
LabManager1 or LabManager2 is the more costefficient<br />
alternative.<br />
LabBox1, example configuration LabBox2, example configuration<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
LabBox1 Basis Device (LB-LABBOX1B)<br />
Extension Reserve<br />
Reserve equipped with<br />
(1) panel 1 all available panels*<br />
(2) panel 2 all available panels*<br />
(3) SER 1 HD-RS2329L, HD-RS485P<br />
(4) SER 2 HD-RS2329L, HD-RS485P<br />
(5) SER 3 HD-RS2329L, HD-RS485P<br />
(6) SER 4 HD-RS2329L, HD-RS485P<br />
(7) internal<br />
2 interface cards plus HK-SER8ECB, sensor / actuator power supply with HS-<br />
NGS243<br />
* With the exception of PSER99 due to the installation depth of the interface modules RS2329L, RS2329PL and RS4859P<br />
Technical Data<br />
Case 3 HE desktop case<br />
Basis Panel UI interface (PC), 230 V~ connection and function LEDs<br />
CPU CPU32 card, 32 bit Embedded Controller with watchdog<br />
Extension Reserve See table<br />
Dimensions Depth: 3<strong>10</strong> mm<br />
Width: 236 mm<br />
Height: 145 mm (3 HE)<br />
Working Temperature 0 to 50 °C, non-condensing<br />
Storing Temperature 0 to 50 °C<br />
IP Protection Category IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory devices<br />
Power Consumption From 30 W to 140 W, depending on the configuration<br />
Operating Voltage 230 V +<strong>10</strong>, -20 %<br />
Delivery Scope LabBox1 basis device, cable for the connection to the 9-pin RS232 interface of<br />
the UI, 9-pin, 230 V cable, manual<br />
Order Code Description<br />
LB-LABBOX1B LabBox1 basis device for individual equipping<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
78<br />
Laboratory Automation Hardware<br />
LabBox2 Basis Device (LB-LABBOX2B)<br />
Extension Reserve<br />
Reserve supplied with<br />
(1) panel 1 all available panels*<br />
(2) panel 2 all available panels*<br />
(3) panel 3 all available panels*<br />
(4) panel 4 all available panels*<br />
(5) SER 1 HD-RS2329L, HD-RS485P<br />
(6) SER 2 HD-RS2329L, HD-RS485P<br />
(7) SER 3 HD-RS2329L, HD-RS485P<br />
(8) SER 4 HD-RS2329L, HD-RS485P<br />
(9) internal 4 interface cards, sensor / actuator power supply<br />
HS-NGS243, HS-NGS241A,<br />
HS-NGS153SN, HS-NGS245SN<br />
* With the exception of PSER99 due to the installation depth of the interface modules RS2329L, RS2329PL and RS4859P<br />
Technical Data<br />
Case 3 HE desktop units<br />
Basis panel UI interface (PC), 230 V~ connection and indication LEDs<br />
CPU CPU32 card, 32 bit Embedded Controller with watchdog<br />
Extension Reserve See table<br />
Dimensions Depth: 3<strong>10</strong> mm<br />
Width: 342mm<br />
Height: 145 mm (3 HE)<br />
Working Temperature 0 to 50 °C, non-condensing<br />
Storing Temperature 0 to 50 °C<br />
IP protection class IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory device<br />
Power Consumption From 30 W to 240 W, depending on the configuration<br />
Operating Voltage 230 V +<strong>10</strong>, -20 %<br />
Delivery Scope LabBox2 basis device, cable for the connection to the 9-pin RS232 interface of<br />
the UI, 9-pin, 230 V cable, manual<br />
Order Code Description<br />
LB-LABBOX2B LabBox2 basis device for individual equipping<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LabManager Basis Devices<br />
As an intelligent central processing unit, a<br />
LabManager basic device contains:<br />
Laboratory Automation Hardware<br />
� one 32 bit controller card (HK-CPU32),<br />
� one HK-SER8ECB card to connect up to 6(8)<br />
HD-RS2329(p) RS232 interface modules<br />
� a LP-BASIS1 or 2 basis panel and<br />
� a power supply for the cards.<br />
The basis panel is part of the standard equipment of<br />
a basic device and does not have to be ordered<br />
separately.<br />
Next to a low heat device socket for the power<br />
supply, the basis panel (LP-BASIS2) has a potentialfree<br />
RS232 interface for the connection of the UI. Up<br />
to six additional serial interfaces can be connected<br />
to the basis panel.<br />
LabManager1, front view<br />
LabManager2, front view<br />
Basis panel: LP-BASIS2<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 79<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
80<br />
Laboratory Automation Hardware<br />
LabManager1 Basis Device (LB-LABMAN1B)<br />
The device is assembled with the offered interface cards and panel models and is equipped with the<br />
available extra modules.<br />
Extension Reserve<br />
Reserve can be equipped with<br />
(1) Panel 1 all available panels<br />
(2) Panel 2 all available panels<br />
(3) Panel 3 all available panels<br />
(4) Panel 4 all available panels<br />
(5) Panel 5 all available panels<br />
(6) Panel 6 all available panels<br />
(7) SER 1 HD-RS2329L, HD-RS2329PL, HD-RS485P<br />
(8) SER 2 HD-RS2329L, HD-RS2329PL, HD-RS485P<br />
(11) internal 7 interface cards, sensor-/ actuator power supply, HS-NGS243, HS-NGS241A,<br />
HS-NGS153SN, HS-NGS245SN<br />
Technical Data<br />
Case 3 HE desktop units<br />
Basis Panel Floating UI interface (PC), 230 V~ connection and indication LEDs<br />
CPU HK-CPU32 card, 32 bit Embedded Controller with watchdog, HK-SER8ECB card<br />
Extension Reserve Depth: 370 mm<br />
Width: 450 mm (19“)<br />
Height: 145 mm (3 HE)<br />
Dimensions See table<br />
Working Temperature 0 to 50 °C, non-condensing<br />
Storing Temperature 0 to 50 °C<br />
IP Protection Category IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory devices<br />
Power consumption 30 W to 240 W, depending on the configuration (without 230 V switching outputs)<br />
Operating Voltage 230 V +<strong>10</strong>, -20 %<br />
Delivery Scope LabManager, cable for the connection to the 9-pin RS232 interface of the UI,<br />
power supply cable, manual<br />
Order Code Description<br />
LB-LABMAN1B LabManager1 basis device for individual equipping<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
LabManager2 Basis Device (LB-LABMAN2B)<br />
The device is assembled with the offered interface cards and panel models and is equipped with the<br />
available extra modules.<br />
Extension Reserve<br />
Reserve Can be equipped with<br />
(1) Panel 1 all available panels<br />
(2) Panel 2 all available panels<br />
(3) Panel 3 all available panels<br />
(4) Panel 4 all available panels<br />
(5) Panel 5 all available panels<br />
(6) Panel 6 all available panels<br />
(7) Panel 7 all available panels<br />
(8) Panel 8 all available panels<br />
(9) Panel 9 all available panels<br />
(<strong>10</strong>) Panel <strong>10</strong> all available panels<br />
(11) Panel 11 all available panels<br />
(12) Panel 12 all available panels<br />
(13) Panel 13 all available panels<br />
(14) SER1 HD-RS2329L, HD-<br />
RS2329PL, HD-RS485P<br />
(15) SER2 HD-RS2329L, HD-<br />
RS2329PL, HD-RS485P<br />
(18) internal 12 interface cards, sensor<br />
/ actuator power supply<br />
HS-NGS241A<br />
HS-NGS248<br />
Technical Data<br />
Case 6 HE desktop units<br />
Basis Panel Potential-free UI interface (PC), power supply and indication LEDs<br />
CPU HK-CPU32 card, 32 bit Embedded Controller with watchdog, HK-SER8ECB card<br />
Dimensions Depth: 370mm<br />
Width: 450mm (19“)<br />
Height: 280mm / 6HE<br />
Extension Reserve See table<br />
Working Temperature 0 to 50 °C, non-condensing<br />
Storing Temperature 0 to 50 °C<br />
IP Protection Category IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory device<br />
Power Consumption 30 W to 1500 W, depending on the configuration (without 230 V switching outputs)<br />
Operating Voltage 230 V +<strong>10</strong>, -20 %<br />
Delivery Scope LabManager, cable for the connection to the 9-pin RS232 interface of the UI, 230<br />
V cable, manual<br />
Order Code Description<br />
LB-LABMAN2B LabManager basis device for individual equipping<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 81<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
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Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
82<br />
Outstations (LZ-USTAT)<br />
Laboratory Automation Hardware<br />
The use of a space-saving outstation is<br />
recommended as a ideal solution in case of limited<br />
space. Up to two outstations can be connected to a<br />
LabManager. The case is made of anodized<br />
aluminum. A 24 V DC power supply primarily used<br />
by the binary outputs is integrated into every<br />
outstation.<br />
Dimensions Depth: 80 mm<br />
Width: 605 mm (LZ-USTAT6), 666 mm (LZ-USTAT7)<br />
Example Assembly<br />
for LZ-USTAT6<br />
Height: 141 mm<br />
Consequently, actuators (for example valves) can be<br />
connected directly, i.e. without the need of external<br />
power supply.<br />
Of course, the outstation can be equipped according<br />
to the specific application.<br />
It is connected to the LabManager via a 3 m<br />
(maximum 5 m) cable.<br />
a) LP-PHRED24B, LP-AEP2x4, LP-AEP8, LP-AAP8UI, LP-DE4DA4P, LP-DAP8A<br />
b) LP-PHRED24B, LP-AEP2x4, LP-AEP8, LP-AAP8UI, LP-DEP8, LP-DAP8<br />
c) LP-PHRED24B, LP-AEP2x4, LP-AEP8, LP-AAP8UI, LP-DEP8, LP-DAP8A<br />
Order Code Description<br />
LZ-USTAT6 Outstation for LabManager with 6 panel places<br />
including 3 m connecting cable for the LabManager<br />
LZ-USTAT7 Outstation for LabManager with 7 panel places<br />
including 3 m connecting cable for the LabManager<br />
LZ-USTAT5M Extension of the connecting cable to 5 m<br />
The feasibility of other interface combinations must<br />
be coordinated with our design department on an<br />
individual basis.<br />
Panel Frame (LZ-PR..)<br />
If the LabManager is built into a control cabinet, the<br />
interface panels can be mounted on the door, on the<br />
rear or on the sides, or into 19” slide-in modules<br />
(e.g. Located above or beneath the LabManager).<br />
One or several panel frames are screwed to a<br />
suitable section for this purpose.<br />
Order Code Description<br />
LZ-PR7 Panel frame for the installation of 7 panels into control cabinet<br />
LZ-PRx Panel frame for control cabinet installation. Panel number according to customer<br />
specifications<br />
LZ-PR19Z3HE Panel frame for 19“ rack installation of 7 Panels<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Case Accessories<br />
Mounting Bracket (LZ-BEFW19)<br />
Laboratory Automation Hardware<br />
The mounting brackets allow the installation into<br />
19 inch cabinets.<br />
Order Code Description<br />
LZ-BEFW19 Mounting bracket for 19 inch cabinets<br />
Handle Bars (LZ-GRIFFxx)<br />
The various handle bars improve the handling, or, if<br />
used as stands, guarantee the stable upright stand<br />
of the devices.<br />
Order Code Description<br />
LZ-GRIFFLU Wing handle bars for LAB PIs<br />
LZ-GRIFFRO Front handle bars for LAB PIs<br />
LAB PI interfaces<br />
The interfaces for the process are usually found on<br />
the PI (LabManager and LabBox). Serial interfaces<br />
and bus interfaces are an exception. These can be<br />
provided on the PI and on the UI (See UI interfaces).<br />
Which signal type accords to which sensor, actuator, or device?<br />
The following table displays via which signal type the<br />
different instrumentation components such as<br />
sensors, actuators and laboratory devices<br />
communicate and how they can be connected to the<br />
LAB PIs.<br />
.<br />
The PI is equipped with interface panels with<br />
standardized NAMUR compliant connections. There<br />
are suitable panels for the connection of virtually all<br />
actuators, sensors and devices present in the lab.<br />
Many laboratory devices have several connections<br />
for selection, for example analogue I/O or RS232.<br />
As far as practical applications are concerned, the<br />
analogue interfaces are more uncomplicated since<br />
less modifications have to be carried out and a multimeter<br />
suffices as a test apparatus, if one is required.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 83<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
84<br />
Task, sensor intended for<br />
connection<br />
/actuator/device<br />
Laboratory Automation Hardware<br />
Panel/interface<br />
module<br />
Signal type, connection, driver Reference source for<br />
sensor/actuator/device<br />
Sensors<br />
Temperature (Absolute, difference)<br />
Pt<strong>10</strong>0 LP-PTP8 Connected directly See sensors/Pt<strong>10</strong>0<br />
Pt<strong>10</strong>0, accuracy LP-PTPRP8 Connected directly See sensors/Pt<strong>10</strong>0<br />
Thermocouples LP-THP8 Connected directly See sensors/Thermocouples<br />
Four wire Transmitter LP-AEP8A 0-20 mA, Connected directly upon request<br />
Two wire Transmitter LP-AEP8A 4-20 mA, Connected directly upon request<br />
Temperature controller LP-DEP8 Binary See temperature controller/ watchdog device<br />
Pressure (absolute, relative, difference)<br />
2 conductor transmitters (pressure and<br />
rough vacuum)<br />
LP-AEP8A 4-20 mA, Connected directly See sensors / pressure sensors<br />
Pirani vacuum measuring instrument Various with Serial, NAMUR-Serial Driver<br />
(precise vacuum) with RS232 interface HD-RS232(P)L .<br />
(possible analogue connector) upon request<br />
Pressure controller<br />
Flow gas<br />
LP-DEP8 Binary See pressure controller/watchdog device<br />
Mass flow rate Mass Flow Meter LP-AEP8A voltage or current signal, sensor<br />
feeding<br />
See sensors/pressure sensors<br />
Mass flow rate Mass Flow Controller LP-AEAP8IA, Input and output: voltage or current upon request<br />
LP-AEAP8UA signal, sensor feeding<br />
Mass flow rate Mass Flow Meter and Various with Serial, NAMUR-Serial Driver upon request<br />
Controller<br />
HD-RS232(P)L<br />
Volumetric with gas meter LP-AEP8 Frequency Signal, HK-DEA16F upon request<br />
Gravimetric with gas bottle on balance Various with Driver for scales by Scaltec, Kern, See laboratory devices/scales<br />
Liquid flow<br />
HD-RS232(P)L Sartorius, and Mettler available<br />
Mass flow rate of Coriolis LP-AEP8 0/4...20 mA On request<br />
Volumetric with turbine wheel sensor LP-DEP8 Frequency signal on HK-DEA16N See sensors / Teflon flow<br />
Gravimetric with balance Various with HD- Drivers for scales from SCATLTEC, See laboratory device / balance<br />
RS232(P)L Kern, Sartorius, and Mettler in every<br />
<strong>HiTec</strong> <strong>Zang</strong> PI.<br />
Gravimetric with GraviDos (separately) LP-AEP8A DMS load cell with GRADOMV1 See laboratory device/dosage systems<br />
Gravimetric with GraviDos (System) LP-AEP8DMS DMS load cell with HK-AD24DMS See laboratory device/dosage systems<br />
Flow controller<br />
Level<br />
LP-DEP8 Binary signal on HK-DEA16N, See flow controller and watchdog device<br />
Gravimetric with GraviDos (separately) LP-AEP8A DMS load cell with GRADOMV1 See Laboratory Devices /Dosing Systems<br />
Gravimetric with GraviDos (System) LP-AEP8DMS DMS load cell onHK-AD24DMS See Laboratory Devices /Dosing Systems<br />
Conductive, capacitive LP-AEP8(A) 0...<strong>10</strong> V, 0/4...20 mA Upon request<br />
Trickling method, hydrostatic pressure LP-AEP8(A) 0...<strong>10</strong> V, 0/4...20 mA Upon request<br />
Gravimetric with balance Various with HD- Drivers for balances of SCATLTEC, See laboratory device/balance<br />
RS232(P)L Kern, Sartorius, and Mettler in every<br />
<strong>HiTec</strong> <strong>Zang</strong> PI.<br />
Level controller<br />
Mass<br />
LP-DEP8(A) Binary signal on HK-DEA16N See level controller<br />
with lab balance Various with HD- Drivers for balances of SCATLTEC, See laboratory device/scale<br />
RS232(P)L Kern, Sartorius, and Mettler in every<br />
<strong>HiTec</strong> <strong>Zang</strong> PI.<br />
Gravimetric with GraviDos (separately) LP-AEP8A DMS load cell on GRADOMV1 See laboratory device/dosage systems<br />
Gravimetric with GraviDos (System)<br />
pH/Rhedox<br />
LP-AEP8DMS DMS load cell on HK-AD24DMS See laboratory device/dosage systems<br />
Glass-probe, short distance LP-PHRED24 Directly connected electrode signal upon request<br />
Glass-probe, long distance LP-AEP8(A) Electrode signal directly connected via<br />
cable booster IL-PHAMP1<br />
upon request<br />
Ext. pH measuring instrument<br />
Distance<br />
LP-AEP8(A) 0...<strong>10</strong> V, 0/4...20 mA upon request<br />
Inductive, optical proximity sensor<br />
Rotation speed<br />
LP-DEP8A Binary signal and feeding on HK-<br />
DEA16N<br />
Sensors/distance<br />
Inductive, optical proximity sensor<br />
Electrical heating<br />
LP-DEP8A Binary signal and feeding on HK-<br />
DEA16N<br />
Actuators<br />
Sensors/rotation speed<br />
Heating dome, calorific, immersion HP-B230VxxA Binary and PWM, 230 V~, Connected upon request<br />
heater<br />
directly<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
Continued: Which signal type on which sensor, actuator or device?<br />
Task, connected Panel/interface Signal type, connection, driver Reference source for<br />
Sensor/actuator/device module<br />
sensor/actuator/device<br />
Valve on/off and 3/2 paths, reflux divisor<br />
Magnetic valve LP-DAP8A Binary, direct connection See Laboratory Devices/Valves<br />
Engine valve digital driving LP-DAP8x 2 x binary outputs for on and off upon request<br />
Final position acknowledgement<br />
Proportionally to valve<br />
LP-DEP8(A) 2 x binary inputs for on and off upon request<br />
Magnetic valve LP-DAP8T HK-DEA16N, PWM See laboratory device/ proportional<br />
valve<br />
Engine valve analogue driving LP-AAP8UI 0...<strong>10</strong> V, 0/4...20 mA upon request<br />
Engine valve digital driving LP-DAP8x 2 x binary outputs for on and off upon request<br />
Final position acknowledgement LP-DEP8(A) 2 x binary inputs for on and off upon request<br />
Position acknowledgement<br />
Multipath Valve<br />
LP-AEP8 1 x analogue input for position upon request<br />
With stepping motor drive<br />
Scales<br />
HD-RS232(P)L,<br />
HD-RS485P<br />
Serial, NAMUR-Serial Driver<br />
Laboratory device<br />
upon request<br />
Lab Scales from Scaltec, Sartorius, Various with HD- Drivers for scales from SCATLTEC, Kern, Sartorius, See laboratory devices/Scales<br />
Kern, and Mettler<br />
Analysers, Spectrometers<br />
RS232(P)L and Mettler in every <strong>HiTec</strong> <strong>Zang</strong> PI.<br />
GC, HPLC, NIR, ... HD-RS232(P)L, Serial connection to the PI through a NAMUR serial upon request<br />
Torque measuring stirrer<br />
HD-RS485P driver or serial connection to the UI through a PI<br />
driver<br />
ViscoPakt analogue IO LP-AEP8(A),<br />
LP-AAP8UI,<br />
LP-AEAP8U(A),<br />
LP-AEAP8I(A)<br />
See laboratory devices<br />
ViscoPakt Serial<br />
Dosing pump<br />
HD-RS232(P)L NAMUR-Serial Driver See laboratory devices/measuring<br />
stirrer<br />
Diaphragm pump LP-DAP8 Pulse frequency, HK-DEA16N See laboratory devices / dosing<br />
pumps<br />
Tube pump, reciprocating pump LP-DAP8 HK-DA816UI 0-<strong>10</strong> V or 0/4..20 mA See laboratory devices / dosing<br />
pumps<br />
Serial dosing pumps HD-RS232(P)L, Serial, NAMUR-Serial Driver See laboratory devices / dosing<br />
Solid Doser<br />
HD-RS485P<br />
pumps<br />
SOLIDOS<br />
Heating/cooling thermostat<br />
LP-DAP8 Pulse Frequency See laboratory devices/ solid<br />
matter dosing apparatus<br />
Analogue EA LP-AEP8(A), Inputs and outputs: 0...<strong>10</strong> V, 0/4...20 mA See laboratory devices/<br />
LP-AAP8UI,<br />
LP-AEAP8<br />
moderating device<br />
Serial Interface Various with Serial, NAMUR-Serial Driver<br />
See laboratory devices/<br />
HD-RS232(P)L, (Drivers for common thermostats of Haake, Huber, moderating device<br />
Calibrating-heating<br />
HD-RS485P Julabo, Laude already integrated)<br />
HD-RS232(P)L<br />
Abbreviation:<br />
Serial,<br />
NAMUR-driver<br />
See laboratory devices/ calibrating heating<br />
PWM: Pulse Width Modulated<br />
PFM: Pulse Frequency Modulated<br />
x: arbitrary alphabetic character<br />
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Which Modules for which Signal Type?<br />
The following table gives an overview of which card/<br />
panel combinations are suitable for frequently used<br />
signal and/or connection types.<br />
For each case, you can find a more detailed<br />
description of the possibilities in the description of<br />
the modules, cards, and panels.<br />
You can find suitable connecting cables for the<br />
laboratory devices of different manufacturers under<br />
"Cables for Instrumentation“.<br />
Signal Connection possibility for possible cards possible panels<br />
Analogue Output<br />
voltage and current Heating/cooling thermostats<br />
setpoint and actual value, stirrer<br />
torque, pressure feeder, flow meter<br />
HK-AD20NMUX8,<br />
HK-AD20NMUX16, HK-AD20N +<br />
HK-HMUX<br />
4-conductor Pt<strong>10</strong>0 Pt<strong>10</strong>0 direct temperature sensor HK-AD20NMUX8,<br />
HK-AD20NMUX16, HK-AD20N +<br />
HK-HMUX<br />
LP-AEP8, LP-AEP8A,<br />
LP-AE4PT4P, LP-AEAP8U(A), LP-<br />
AEAP8I(A)<br />
LP-PTP8, LP-AE4PT4P<br />
4-conductor accuracy Pt<strong>10</strong>0 Pt<strong>10</strong>0 direct temperature sensor HK-AD24PX8 LP-PTPRP8<br />
Thermocouples direct thermocouples HK-AD20NMUX8,<br />
HK-AD20NMUX16, HK-AD20N +<br />
HK-HMUX<br />
LP-THP8<br />
pH/RedOx directly connected pH and RedOx HK-AD20NMUX8,<br />
IL-PHAMP1 external to LP-AEP8,<br />
electrodes<br />
HK-AD20NMUX16, HK-AD20N + LP-AEP8A, LP-AE4PT4P,<br />
Load Cells<br />
HK-HMUX<br />
LP-AEAP8U(A), LP-AEAP8I(A),<br />
LP-PHRED24 with HK-PHAMP<br />
(just for LZ-USTAT)<br />
GraviDos load cell<br />
Analogue output<br />
HK-AD24DMS4 LP-DMS4DA4PT,<br />
2xHK-AD24DMS4, LP-DMS8<br />
voltage and current Heating/cooling thermostats set HK-DA812UI LP-AAP8UI, LP-AEAP8U(A), LPpoint,<br />
stirrer rotation speed setpoint<br />
value, proportional valves...<br />
AEAP8I(A)<br />
Combined analogue input and output<br />
voltage or current Heating/cooling thermostats set HK-DA812UI + HK-AD20NMUX8, LP-AEAP8U(A), LP-AEAP8I(A)<br />
point and actual value, stirrer HK-AD20NMUX16, HK-AD20N +<br />
Digital output<br />
rotation speed setpoint value and<br />
actual value, massflow controller<br />
setpoint value and actual value ...<br />
HK-HMUX<br />
Digital Magnetic valves, drive valves, HK-DEA16N LP-DAP8, LP-DAP8A,<br />
pumps, monitors, switching boxes<br />
LP-DE4DA4P, LP-DA230V8<br />
Pulse Width Modulated<br />
Magnetic valves, engine valves, HK-DEA16N LP-DAP8, LP-DAP8A,<br />
(PWM)<br />
pumps, floodgates, switching<br />
boxes<br />
LP-DE4DA4P, LP-DAP8T<br />
Pulse Frequency Modulated Dosing pumps with pulse HK-DEA16N LP-DAP8, LP-DAP8A,<br />
(PFM)<br />
Digital input<br />
activation, reflux divisors, solid<br />
matter dosing apparatus SOLIDOS<br />
LP-DE4DA4P<br />
Binary Boundary value senders,<br />
controllers, proximity sensors,<br />
status signals of devices<br />
HK-DEA16N LP-DEP8(A), LP-DE4DA4P<br />
Events < 50Hz Belt weigher, gas volume counter HK-DEA16N LP-DEP8(A), LP-DE4DA4P<br />
Frequency < 50Hz<br />
Serial interfaces<br />
Turbine wheel flow meter, energy<br />
counter, proximity sensors<br />
HK-DEA16N LP-DEP8(A), LP-DE4DA4P<br />
RS232, RS485 Balance, stirrers, Heating/cooling HD-RS2329L, HD-RS2329PL, HD- Basis panel, LP-SER99, LPthermostats,<br />
analysers, robots RS485P<br />
PHRED24 (only for LZ-USTAT)<br />
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Interface Panels for Analogue Input<br />
Laboratory Automation Hardware<br />
Different systems are available for analogue input,<br />
which differ in respect to accuracy and electric<br />
robustness. The combined HK-AD20NMUX8 and<br />
HK-AD20NMUX16 AD converter multiplexer cards<br />
can be used for smaller systems.<br />
8 Voltage and Current Inputs (LP-AEP8)<br />
The panel for analogue input is<br />
designed for collecting voltages<br />
of -<strong>10</strong>...+<strong>10</strong> V and current<br />
signals of 0/4 ... 20 mA.<br />
Laboratory devices such as<br />
heat/cool thermostats or mixers<br />
and measuring sensors can be<br />
connected to the eight potentialfree<br />
and EMC robust inputs.<br />
� 8 analogue inputs for voltage and current of<br />
0/4 ... 20 mA (6-pin tuchel socket DIN45322)<br />
� Combinable with other analogue input panels<br />
An example out of many possible applications is the<br />
recording of a pressure with a pressure sensor due<br />
to 4...20 mA two wire technology. This gives out 4<br />
mA at 0 mbar and 20 mA at <strong>10</strong>00 mbar.<br />
The measured electric value is converted to a mbar<br />
value in the PI by appropriate scaling of the data<br />
point. For this purpose, the parameters in LabVision<br />
must be set to the following values:<br />
Minimum process value 0<br />
Maximum process value <strong>10</strong>00<br />
Minimum interface value 4<br />
Maximum interface value 20<br />
EMC robust HK-HMUX multiplexer cards together<br />
with a HK-AD20N AD converter card are<br />
recommended for bigger systems.<br />
For each of the different signal and sensor types,<br />
suitable NAMUR standard compliant interface<br />
panels are available.<br />
Each interface panel for analogue input has 8 inputs<br />
while HK-HMUX multiplexer cards and the HK-<br />
AD20NMUX16 have 16 channels.2 panels can be<br />
connected to each card. Here it is possible to<br />
combine different panels, for example a panel for<br />
thermocouples with a panel for Pt<strong>10</strong>0 feelers.<br />
To protect unused inputs against corrosion and dust,<br />
you can cover them with plastic caps.<br />
Connection examples for the LP-AEP8 and LP-AEP8A analogue<br />
input interface panels<br />
Note: When using a LP-AEP8A panel, you can<br />
connect sensors with a twin or quadruple wire<br />
connection directly to a socket, i.e. without external<br />
power supply.<br />
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Technical Data<br />
Laboratory Automation Hardware<br />
Signal 0/4 ... 20 mA and -<strong>10</strong> ... +<strong>10</strong> V<br />
Connection type 6-pin socket, DIN 45322<br />
Usable with HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />
For the evaluation of Analogue signals such as stirrer rotation speed, torque, pressure, fill level,<br />
temperature output of a thermostat, pH-value on IL-PHAMP1 (external), etc<br />
Product description Interface panel with 8 inputs of 0/4..20 mA current or -<strong>10</strong> V..+<strong>10</strong> V voltage<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-AEP8 Interface panel with 8 current and voltage inputs<br />
LZ-AKTUB Caps for tuchel Sockets<br />
Suitable connecting cables for laboratory devices and sensors<br />
Order Code Description<br />
ZK-LAB-HI01-IA-UP-O-01 Analogue input cable with open ends for voltage<br />
ZK-LAB-HI01-IA-IP-O-01 Analogue input cable with open ends for 0/4..20 mA twin conductor<br />
For other cables, see "Cables for Instrumentation“.<br />
8 Voltage and Current Inputs with Power Supply (LP-AEP8A)<br />
The panel for analogue input is<br />
designed for collecting voltages<br />
of -<strong>10</strong>...+<strong>10</strong> V and current<br />
signals of 0/4 ... 20 mA.<br />
Laboratory devices such as<br />
heating/cooling thermostats or<br />
stirrers and measuring sensors<br />
can be connected to the eight<br />
potential-free and EMC robust<br />
inputs.<br />
� 8 analogue inputs for voltage and current of<br />
0/4 ... 20 mA (6-pin tuchel socket)<br />
� sensor feeding<br />
� combinable with other analogue input panels<br />
You can connect sensors with a twin or quadruple<br />
wire connection directly to a socket of the LP-AEP8A<br />
panel, i.e. without external power supply. Therefore,<br />
Technical Data<br />
connecting requires only few seconds since the<br />
connection to a power supply is not necessary.<br />
Connection examples for sensors as voltage and<br />
current transmitters in two and four wire technology<br />
Signal 0/4 ... 20 mA and -<strong>10</strong> ... +<strong>10</strong> V<br />
Connection type 6-pin socket, DIN 45322<br />
Usable with HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />
For the collecting of Analogue signals such as stirrer rotation speed, torque, pressure, fill level,<br />
temperature output of a thermostat,<br />
pH-value on IL-PHAMP1 (external), etc.<br />
Product Description Interface panel with 8 current or voltage inputs of 0/4..20 mA, or <strong>10</strong> V..+ <strong>10</strong> V, 24<br />
V sensor feeding through free contacts or in the 4 ... 20 mA low potential circuit<br />
(additional power unit necessary, for example HS-NGS241A, other voltages<br />
available upon request)<br />
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Laboratory Automation Hardware<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-AEP8A Interface panel with 8 current and voltage inputs, sensor power supply 24 V<br />
LZ-AKTUB Caps for tuchel Sockets<br />
Suitable connecting cables for laboratory devices and sensors:<br />
Order Code Description<br />
ZK-LAB-HI01-IA-UP-O-01 Analogue input cable with open ends for voltage<br />
ZK-LAB-HI01-IA-UA-O-01 Analogue input cable with open ends for voltage with feeding<br />
ZK-LAB-HI01-IA-IP-O-01 Analogue input cable with open ends for 0/4..20 mA twin conductor<br />
ZK-LAB-HI01-IA-IA-O-01 Analogue input cable with open ends for 0/4..20 mA twin conductor with feeding<br />
ZK-LAB-HI01-IA-IA-O-02 Analogue input cable with open ends for 0/4..20 mA four conductor with feeding<br />
For other cables, see "Cables for Instrumentation“.<br />
8 Pt<strong>10</strong>0 Temperature Sensor Inputs (LP-PTP8)<br />
Up to 8 Pt<strong>10</strong>0 or other<br />
resistance feelers can be<br />
connected directly to this panel.<br />
� 8 inputs for Pt<strong>10</strong>0 and<br />
resistance feelers (4-pin<br />
LEMO socket model S1)<br />
� Combination with other<br />
analogue input panels<br />
possible<br />
The wire length does not have any influence on the<br />
measuring accuracy in the quadruple wire<br />
technique. The resolution is better than 0.01 °C<br />
The measured value delivered by the resistance<br />
feeler is linearised and converted to °C. The<br />
resolution depends on the interface cards used. The<br />
signals of the measuring sensor can be calibrated<br />
via the software.<br />
Technical Data<br />
Connection example for a PT <strong>10</strong>0 connection panel<br />
Signal Pt<strong>10</strong>0 signal twin, triple and quadruple wiring connection<br />
Connection type 4-pin socket, model LEMO S1<br />
Usable with HK-AD20NMUX8, HK-AD20NMUX16, HK-HMUX<br />
For the evaluation of Temperatures through Pt<strong>10</strong>0 sensors<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-PTP8 NAMUR compliant interface panel for Pt<strong>10</strong>0 with twin to quadruple wire technology<br />
LZ-AKLES1 Caps for LEMO S1<br />
You can find customise temperature sensors ready for connection in "Process Analytics/Sensors"<br />
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8 High Precision Pt<strong>10</strong>0 Inputs (LP-PTPRP8)<br />
This panel is designed<br />
especially for AD24PX8<br />
precision measurement cards.<br />
For further information, see<br />
under precision temperature<br />
measurement module and HK-<br />
AD24PX8.<br />
Connection example for a PT <strong>10</strong>0-P connection panel<br />
Order Code Description<br />
LP-PTPRP8 Interface panel for Pt<strong>10</strong>0 on HK-AD24PX8 with two and four wire system<br />
LZ-AKLES1 Caps for LEMO S1<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Suited Precision Temperature Sensors<br />
Order Code Description<br />
IS-T-PT<strong>10</strong>015G Pt<strong>10</strong>0 Temperature Sensor, Measurement Uncertainty ±(0,15 °C + 0,002·|ϑ |) absolute<br />
IS-T-PT<strong>10</strong>003B Pt<strong>10</strong>0 Temperature sensor, Measurement Uncertainty: ±(0,03 °C + 0,0005·|ϑ |) absolute<br />
IS-T-PTKAL Calibration Certificate for Pt<strong>10</strong>0<br />
You can find customised temperature sensors ready for connection in "Process Analytics/Sensors"<br />
Delivery Scope PT<strong>10</strong>0 temperature sensor<br />
cable and connector (for LP-PTPRP8)<br />
calibration certificate upon request<br />
Further sensors can be found in the chapter "Process analytics and Sensors"<br />
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Laboratory Automation Hardware<br />
4 Analogue Inputs and 4 Pt<strong>10</strong>0 Inputs (LP-AE4PT4P(A))<br />
Technical Data<br />
This panel respectively<br />
combines four channels of the<br />
panels LP-AEP8(A) and LP-<br />
PTP8.<br />
For connection information, see<br />
LP-AEP8 and LP-PTP8.<br />
For connection diagram, see<br />
LP-AEP8(A) and LP-PTP8.<br />
Signal 0/4 ... 20 mA, -<strong>10</strong> ... +<strong>10</strong> V and Pt<strong>10</strong>0 resistance feeler<br />
Connection type see LP-AEP8(A) and LP-PTP8<br />
Usable with HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />
For the evaluation of Temperatures through Pt<strong>10</strong>0 sensors,<br />
Analogue signals such as mixer rotation speed & torque,<br />
fill level, temperature output of a thermostat, pH value / RedOx on IL-PHAMP1<br />
(external) etc.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-AE4PT4P Interface panel with 4 Pt<strong>10</strong>0 and 4 voltage/current inputs<br />
LP-AE4PT4PA Interface panel with 4 Pt<strong>10</strong>0 and 4 voltage/current inputs<br />
with 24 V = sensor power supply on free contacts<br />
For further information see LP-AEP8(A) and LP-PTP8.<br />
8 Thermocouple Inputs (LP-THP8)<br />
This panel is suitable for the<br />
connection of up to 8<br />
thermocouples through a 2-pin<br />
LEMO plug model 1S. The cold<br />
junction compensation occurs<br />
electronically (turn-off enabled).<br />
� 8 inputs for thermocouples<br />
(2-pin LEMO socket)<br />
� Electronic cold junction<br />
compensation<br />
� Combination with other<br />
analogue input panels<br />
possible<br />
The measured value is linearised during the<br />
measurement and converted to °C. The integrated<br />
cold junction compensator corrects influences of the<br />
ambient temperature. The resolution is better than<br />
0,1 °C.<br />
Technical Data<br />
Signal For direct connection of thermocouples<br />
Connection type 2-pin socket, model LEMO S1<br />
Usable with HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />
For the evaluation of Temperatures through thermocouples<br />
Connection example for the thermocouple interface<br />
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Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-THP8 Interface panel for thermocouples<br />
LZ-AKLES1 Caps for LEMO S1<br />
You can find customised temperature sensors ready for connection in "Process Analytics/Sensors"<br />
2 pH/RedOx and 4 RS232 Interfaces (LP-PHRED24)<br />
The pH/RedOx interface panel allows the direct<br />
connection of pH/RedOx electrodes. The panels can<br />
be optionally equipped with 9-pin RS232 interfaces.<br />
The compensation of the temperature of the pH<br />
value can be done on the LabManager. The<br />
delivered demo programs perform interactively the<br />
calibration (HiText or HiText-light software modules<br />
are necessary for that).<br />
The panel can be supplied with one or two<br />
pH/RedOx booster modules (HK-PHAMP) and up to<br />
four 9-pin RS232 interfaces (HD-RS2329L).<br />
� up to 2 connections for pH or RedOx<br />
electrodes<br />
� up to 4 serial RS232 interfaces<br />
Note: Only for the mounting on LZ-USTAT! The<br />
external IL-PHAMP1 should be used for standard<br />
devices (see laboratory devices, external pH<br />
booster).<br />
Connection example for the pH//RedOx interface panel.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-PHRED24 Interface panel for pH/RedOx and RS232 interfaces<br />
LP-PHRED24B Interface panel for pH/RedOx with battery monitoring and RS232 interface<br />
LZ-AKPH Caps for pH sockets<br />
Can be supplied with the following modules:<br />
Order Code Description<br />
HK-PHAMP Amplifier for pH and RedOx electrodes<br />
HD-RS2329 9-pin RS232 interface<br />
Technical Data PHAMP<br />
Signal mV (is buffered with the HK-PHAMP booster),<br />
RS232 signal, 24 V<br />
Connection type > <strong>10</strong>0 MΩ<br />
Usable with -1<strong>10</strong>0....1<strong>10</strong>0 mV<br />
For the evaluation of Hf-socket, D-SUB-9<br />
Signal HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />
Connection type pH value (direct electrode connection),<br />
RedOx potential (direct electrode connection),<br />
opt. battery voltage.<br />
Power supply build in lithium cell battery<br />
You can find suitable cables for devices with serial interface in the chapter “Cables for Instrumentation”.<br />
In the chapter Measurment Amplifiers IL-PHAMP1, you can find an external measuring amplifier for<br />
connection to analogue inputs as an alternative to the internal amplifiers.<br />
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4 DMS Bridge Inputs, 4 Digital Outputs (LP-DMS4DA4PT)<br />
Technical Data<br />
This panel is suitable for the<br />
connection of up to four<br />
GraviDos dosing apparatus<br />
systems or DMS full bridges<br />
and/or load cells, torque sensors<br />
etc. based on DMS. The panel is<br />
designed to work with precision<br />
DMS modules HK-AD24DMS4.<br />
Connection example for GraviDos systems and magnetic valves.<br />
Signal direct connection of DMS bridges and dosing valves (max. 500mA per channel)<br />
Connection type 6 pin socket, Type LEMO S1; 3 pin connector, DIN 41524<br />
Usable with HK-AD24DMS4<br />
For the evaluation of weight, force, flow, torque...<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DMS4DA4PT Interface panel for 4 DMS full bridges and 4 activated digital outputs (500 mA)<br />
LZ-AKLES1 Caps for LEMO S1<br />
LZ-AKTUB Caps for tuchel sockets<br />
For suitable weighing systems, see "Sensors“, "Load cells“ and "GraviDos“.<br />
8 DMS Bridge Inputs (LP-DMS8)<br />
This panel is suitable for the<br />
connection of up to eight<br />
GraviDos dosing systems or DMS<br />
full bridges and/or load cells,<br />
torque sensors etc. based on<br />
DMS. The panel is designed to<br />
work with precision DMS modules<br />
HK-AD24DMS4.<br />
Technical Data<br />
Connection example for GraviDos systems and load cells<br />
Signal For direct connection of DMS bridges<br />
Connection type 6-pin socket, Type LEMO S1<br />
Usable with 1x or 2 x HK-AD24DMS4<br />
For the evaluation of weight, force, flow, torque...<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DMS8 Interface panel for 8 DMS full bridges<br />
LZ-AKLES1 Caps for LEMO S1<br />
For suitable weighing systems, see "Sensors“, "Load cells“ and "GraviDos“.<br />
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Laboratory Automation Hardware<br />
Interface Panels for analogue Output<br />
A panel for the current and voltage output and a<br />
combined input/output panel are available on choice<br />
for analogue output.<br />
8 Voltage and Current Outputs (LP-AAP8UI)<br />
This panel is used for<br />
connecting laboratory devices<br />
with analogue voltage or<br />
current inputs for control and<br />
regulation purposes.<br />
The LP-AAP8UI panel uses<br />
eight NAMUR compliant 6-pin<br />
tuchel sockets for the output of<br />
analogue signals.<br />
� 8 analogue outputs<br />
� Voltage of -<strong>10</strong>...+<strong>10</strong> V and current of 0/4 ... 20<br />
mA (6-pin tuchel socket) working resistance<br />
of maximum 500 Ω<br />
An example out of many possible applications is<br />
driving a stirrer. It is supposed to run at 0 rpm with 0<br />
V and at 2000 rpm with <strong>10</strong> V. The rotation speed can<br />
be directly determined by suitable scaling of the data<br />
point.<br />
This means that the stirrer rotates at 300 rpm, if the<br />
a value of 300 is allocated to the data point. For this<br />
purpose, the parameters in LabVision will be set to<br />
the following values:<br />
Minimum process value 0<br />
Maximum process value 2000<br />
Minimum interface value 0<br />
Maximum interface value <strong>10</strong><br />
Technical Data<br />
Connection example for stirrers and pumps<br />
The value of the output data point can be set by the<br />
user through a control module (SL-HiText), an<br />
automatic controller (SF-PIDxx) or by direct value<br />
assignment.<br />
Signal 0/4 ... 20 mA, -<strong>10</strong> ... +<strong>10</strong> V<br />
Connection type 6-pin socket, DIN 45322<br />
Usable with HK-DA812UI<br />
For the evaluation of Analogue actuators, for example control valves, dosing pumps, temperature<br />
theoretical value of a thermostat, stirrer rotation speed, external automatic<br />
controllers, for example mass flow rate or pressure etc.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-AAP8UI Panel for analogue output, current and voltage<br />
LZ-AKTUB Caps for LEMO S1<br />
For suitable connecting cables for laboratory devices and final control elements, see “Cables for<br />
instrumentation”.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
8 Combined analogue Inputs/Outputs (LP-AEAP8xx)<br />
Technical Data<br />
This panel has combined<br />
connections for analogue input/<br />
output. It is particularly suitable<br />
for the connection of devices<br />
which are driven by an<br />
analogue theoretical value and<br />
supply on analogue actual<br />
value.<br />
Connetion example for a mass flow controller<br />
Signal 0/4 ... 20 mA, -<strong>10</strong> ... +<strong>10</strong> V<br />
Connection type 6-pin socket, DIN 45322<br />
Usable with HK-DA812UI and on choice with HK-AD20NMUX8, HK-AD20NMUX16, HK-<br />
HMUX<br />
For the evaluation of Measure flow controllers, heat/cool thermostats, measuring stirrers<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-AEAP8I Multi-purpose panel with 8 0/4 ... 20 mA current inputs, 8 0/4 ... 20 mA current outputs<br />
LP-AEAP8IA Multi-purpose panel with 8 0/4 ... 20 mA current inputs, 8 0/4 ... 20 mA current outputs, 24 V<br />
sensor power supply<br />
LP-AEAP8U Multi-purpose LabManager panel with 8 ±<strong>10</strong> V voltage inputs, 8 ±<strong>10</strong> V voltage outputs<br />
LP-AEAP8UA Multi-purpose LabManager panel with 8 ±<strong>10</strong> V voltage inputs, 8 ±<strong>10</strong> V voltage outputs, 24 V<br />
sensor power supply<br />
LZ-AKTUB Caps for tuchel sockets<br />
For suitable connecting cables for laboratory devices and final control elements, see "Cables for<br />
instrumentation“.<br />
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Reaction<br />
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Construction and<br />
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96<br />
Interface panels for digital input<br />
Laboratory Automation Hardware<br />
Beyond the pure recording of binary states (in/out),<br />
digital inputs of <strong>HiTec</strong> <strong>Zang</strong> PIs can be used for<br />
frequency measurement.<br />
8 digital inputs (LP-DEP8)<br />
The panel for digital input is<br />
suitable for the connection of<br />
switches, limiting value<br />
transmitters and other digital<br />
transmitters with NAMUR<br />
compliant turn-off levels. For a<br />
maximally simple external<br />
wiring the inputs are placed<br />
over intern pull-up resistors and<br />
pulled up to 24 V.<br />
� 8 digital inputs, active (Pull-up against 24 V),<br />
opto-electronically isolated.<br />
� for limit switches and digital status signals<br />
� 3-pin tuchel socket 180 °<br />
� one or two LP-DEP8 connectable to a HK-<br />
DEA16N card<br />
� Inputs with NAMUR compliant turn-off levels<br />
Technical Data<br />
� With optional sensor power supply (WP-DEP8A)<br />
� Also suitable for frequency measurement<br />
Connection example for fill limit switches<br />
Signal NAMUR NE28 compliant input level and pin assignment<br />
Connection type 3-pin socket, DIN 41524<br />
Usable with HK-DEA16N<br />
For the evaluation of Switch contacts, fill level switches, press switches, digital status signals of devices<br />
etc.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DEP8 Digital input interface panel with active 24 V inputs<br />
LZ-AKTUB Caps for tuchel sockets<br />
For suitable connecting cables for sensors and monitors, see “Cables for instrumentation”.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
8 Digital Inputs with Sensor Power Supply (LP-DEP8A)<br />
This panel has no pull-up<br />
resistor like the LP-DEP8,<br />
however it delivers extra 24 V<br />
on every socket (-pin3) for the<br />
supply of on available<br />
connected sensor. Optional a<br />
pull-up resistor can be<br />
provided in the connector or<br />
in the sensor.<br />
� for limiting value modulators with<br />
electronics and digital status signals<br />
� one or two LP-DEP8A suitable for<br />
connection to a HK-DEA16N/F card<br />
� Inputs with NAMUR compliant turn-off levels<br />
Technical Data<br />
Connection example for proximity and fill level sensors<br />
Signal NAMUR NE28 compliant input level and pin assignment<br />
Connection type 3-pin socket 180 °, DIN 41524<br />
Usable with HK-DEA16N<br />
For the evaluation of Proximity sensors, switch contacts, fill level switches, push switches, digital status<br />
signals of devices etc., Sensor feeding on pin 3<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DEP8A Digital input interface panel with active 24 V supply and sensor power supply<br />
LZ-AKTUB Caps for tuchel sockets<br />
For suitable connecting cables for sensors and monitors, see “Cables for instrumentation”.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
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Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Components<br />
Process Analytics<br />
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Stirring and<br />
Dispersing<br />
Services
98<br />
Interface Panels for Digital Output<br />
Laboratory Automation Hardware<br />
Not only binary switching actions (in/out, on/off) but<br />
also pulse width and pulse frequency modulated<br />
output are included in the digital output. The<br />
switching voltage is 24 V.<br />
8 passive digital outputs (LP-DAP8)<br />
This panel offers for every<br />
connection a relay switching<br />
contact which can be freely<br />
connected by the customer.<br />
� 8 digital outputs, relay contacts, a<br />
changeover switch per output, a maximum of<br />
1 A, 30 V on a 3-pin tuchel plug<br />
� Control LED for every channel<br />
� For the connection of magnetic valves,<br />
drives, heating, dosing pumps, etc...<br />
� up to two LP-DAP8 connectable to a HK-<br />
DEA16N card<br />
Technical Data<br />
For digital output, the following types of connection<br />
are available<br />
� passive changeover switch (LP-DAP8)<br />
� Active 24V changeover switch for the direct<br />
connection of valves, smaller motors...(LP-<br />
DAP8A)<br />
� Active 24V transistor outputs for proportional<br />
magnetic valves...(LP-DAP8T)<br />
Signal Contacts of a passive one pin change-over switch<br />
Connection type 3-pin plug, DIN 41524<br />
Usable with HK-DEA16N<br />
For connecting Valves, reflux divisors, motors, digital control inputs on devices etc.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DAP8 Digital output interface panel, passive change-over contacts<br />
LZ-AKTUS Caps for tuchel plugs, passive change-over contacts<br />
For suitable connecting cables for valves, actuators etc. see "Cable for Instrumentation“.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
8 active digital outputs (LP-DAP8A)<br />
Laboratory Automation Hardware<br />
This panel offers at each<br />
connection a normally open and<br />
normally closed contact with an<br />
active switch voltage of 24 V for<br />
direct activation of actuators. For<br />
power supply, depending on the<br />
power required, a HS-NGS241A<br />
to HS-NGS248 can be installed.<br />
Up to two LP-DAP8A can be<br />
connected to a HK-DEA16N or<br />
HK-DEA16n card.<br />
� 8 active digital outputs, changeover switch,<br />
24 V, a maximum of 1 A, on a 3 pin tuchel<br />
plug, max 3 A<br />
� Short-circuit proof<br />
� Control LED for every channel<br />
� For the direct connection of magnetic valves,<br />
drives, heating, dosing pumps, etc..<br />
Technical Data<br />
Connection example for magnetic valves<br />
Signal Active change-over switch (normally open contact +24 V, normally closed contact<br />
+24 V), capable of bearing 1 A<br />
Connection type 3 pin plugs, DIN41524<br />
Usable with HK-DEA16N, HS-NGS241A to HS-NGS248<br />
For connecting 24 V consumers as magnetic valves, engine valves, reflux divisors, motors, digital<br />
control inputs on devices etc.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DAP8A Digital output interface panel, active outputs<br />
LZ-AKTUS Caps for tuchel plugs<br />
For suitable connecting cables for valves, actuators etc., see "Cable for Instrumentation“.<br />
8 Active Outputs for high Switching Frequencies (LP-DAP8T)<br />
This panel allows the direct<br />
connection of proportional<br />
magnetic valves. Because of the<br />
high switching frequency of up to<br />
1 kHz, MOSFET switches are<br />
integrated. For power supply,<br />
depending on the required<br />
power, a HS-NGS241A to HS-<br />
NGS248 can be installed.<br />
� 8 active controlled current outputs<br />
� for the direct connection of proportional<br />
magnetic valves<br />
� LED control display<br />
� up to two LP-DAP8T connectible to a HK-<br />
DEA16N card<br />
� combinable with other LP-DAPxx panels<br />
� Short-circuit proof<br />
Connection example of a proportional magnetic valve<br />
Automatic<br />
Laboratory<br />
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<strong>10</strong>0<br />
Technical Data<br />
Laboratory Automation Hardware<br />
Signal active digital output 0 ...<strong>10</strong>00 Hz, 500 mA, max. 3A total<br />
Connection type 3 pin plugs, DIN41524<br />
Usable with HK-DEA16N, HS-NGS241A to HS-NGS248<br />
For connecting Proportional magnetic valves etc.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DAP8T Digital output interface panel, active outputs<br />
LZ-AKTUS Caps for tuchel plugs<br />
For suitable connecting cables for valves, actuators etc., see "Cable for Instrumentation“.<br />
4 Digital Inputs and 4 Digital Outputs (LP-DE4DA4P)<br />
This panel combines four<br />
channels of the LP-DEP8 and<br />
LP-DAP8 panels. See in the<br />
according section for detailed<br />
information.<br />
Technical Data<br />
Connection example for fill level switches<br />
Signal NAMUR compliant input level, passive one pin change-over contact<br />
Connection type see LP-DEP8, LP-DAP8<br />
Usable with HK-DEA16N<br />
For connecting Switch contacts, fill level switches, push switches, valves, reflux divisors,<br />
motors, digital control inputs on devices etc.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DE4DA4P Multi-purpose panel with 4 digital inputs and 4 digital outputs<br />
LZ-AKTUB Caps for tuchel sockets<br />
LZ-AKTUS Caps for tuchel plugs<br />
For suitable connecting cables for valves, actuators etc., see "Cable for Instrumentation“.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
4 Digital Inputs and 4 Digital Outputs and Feeding (LP-DE4DA4PA)<br />
This panel respectively combines<br />
four channels of the LP-DEP8<br />
and LP-DAP8A panels. See in the<br />
according section for detailed<br />
information.<br />
Technical Data<br />
Connection example for magnetic valves and fill level switches.<br />
Signal NAMUR compliant input level, active change-over contact (normally open contact<br />
+24 V, normally close contact +24 V), capable of bearing 1 A<br />
Connection type See LP-DEP8, LP-DAP8A<br />
Usable with HK-DEA16N, HS-NGS241A to HS-NGS245<br />
For connecting Switch contacts, fill level switches, push switches, valves, reflux divisors, motors,<br />
digital control inputs on devices etc.<br />
Delivery Scope Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-DE4DA4PA Combination panel 4 digital inputs DEP8, 4 active digital outputs DAP8A<br />
LZ-AKTUB Caps for tuchel sockets<br />
LZ-AKTUS Caps for tuchel plugs<br />
For suitable connecting cables for valves, actuators etc. see "Cable for Instrumentation“.<br />
4 Digital Outputs, 4 Heating Elements and Feeding (LP-DA4HZ4PA)<br />
This panel combines four<br />
channels for low-voltage<br />
heatings with four channels of<br />
the panel.<br />
For details, see LP-DAP8(A).<br />
Technical Data<br />
Signal 44 V AC, max. 2,5 A per output, active change-over contact (normally open<br />
contact +24 V, normally close contact +24 V), capable of bearing 1 A<br />
Applicable with HK-DEA16N, HS-NGS44AC<br />
For the Connection of Switch Contacts, Liquid Level Switch , Pressure switches, Low Voltage Heatings<br />
Scope of Delivery Panel with fastening Screws, Cable for internal cabling<br />
Order Code Description<br />
LP-LP-DA4HZ4PA Combination Panel 4 digital Outputs 24 V 1 A, 4 Low Voltage Heatings<br />
LZ-AKTUB Covers for Tuchel-socket<br />
For suited connection cables for valves, actuators etc., see chapter "Cables for Instrumenting“.<br />
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Components<br />
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Stirring and<br />
Dispersing<br />
Services
<strong>10</strong>2<br />
Serial Interfaces<br />
Laboratory Automation Hardware<br />
Serial interfaces can be provided on the PI and on<br />
the UI, (see also PC cards). Simpler laboratory<br />
devices as dosing pumps and balance will usually<br />
be connected directly to the PI so that they can<br />
simply be included in control loops. Laboratory<br />
devices with complex functionality such as analysers<br />
or titrating apparatuses are rather connected directly<br />
to the UI (see PC plug-in cards).<br />
Panel for 9x RS232 (LP-SER99)<br />
The ninefold RS232 panel can<br />
carry up to nine 9 pin serial<br />
interface modules. It can be<br />
used on the LAB and PMC PI<br />
devices.<br />
Additionally, HD-RS2329L, HD-<br />
RS2329PL or HD-RS485P<br />
interface modules are required<br />
on the panel depending on the<br />
number of interfaces. For<br />
increased performance, an<br />
additional HK-SER8ECB or HK-<br />
SER16ECB card is<br />
recommended.<br />
Order Code Description<br />
LP-SER99 Panel for 9 serial HD-RS2329 interface modules<br />
LZ-AKRS9 Caps<br />
For suitable connecting cables, see "Cables for Instrumentation".<br />
In the PI two different techniques are used: A serial<br />
interface, which is multiplexed to eight channels, is<br />
implemented on the CPU. Due to this, the connected<br />
devices can only communicate one after another<br />
and slow devices slow down the whole<br />
communication.<br />
The eightfold RS232 HK-SER8ECB module is<br />
suitable for universal use and achieves higher<br />
performance. Every channel has a 64 byte FIFO<br />
storage, so that the connected devices can<br />
communicate parallel.<br />
For communication, there are different technologies.<br />
You can find further information in the chapter<br />
"Driver Programs for Laboratory Device Interfaces“.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
RS232 Interface Module (HD-RS2329(P)L)<br />
The serial interface modules are optionally available<br />
with or without separation of the potential.<br />
HD-RS2329L<br />
Technical Data<br />
Potential separation improves the interference<br />
resistance.<br />
HD-RS2329PL<br />
Signal RS232, V24<br />
Connection type 9 pin plugs, D-SUB<br />
Usable with Basis panel, LP-SER99<br />
For connecting Balances, analysers, control systems, devices with RS232 interface<br />
Product Description RS232 interface module to mount on the LabManager or LabBox<br />
Delivery Scope Interface module with cable for internal connection<br />
Order Code Description<br />
HD-RS2329L RS232 interface module with power supply for LabCom<br />
HD-RS2329PL RS232 9 pin interface module with potential separation and power supply for LabCom (max. 4<br />
units in one LabBox)<br />
RS485 Interface Module (HD-RS485P)<br />
HD-RS485P<br />
Technical Data<br />
Signal RS485<br />
Connection type 9-pin plugs, D-SUB<br />
Usable with Basis panel, LP-SER99<br />
For connecting Analysers, control systems, devices with RS485 interfaces<br />
Product description RS485 interface module with potential separation to mount on the<br />
LabManager or LabBox, Cable, standard driver for HK-CPU32, HK-SER16ECB or<br />
HK-SER8ECB<br />
Delivery Scope Interface module with cable for internal connection<br />
Order Code Description<br />
HD-RS485P RS485 9-pin Interface Module with Potential Separation<br />
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Plant<br />
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Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
<strong>10</strong>4<br />
Laboratory Automation Hardware<br />
16 Channel Serial Interface Card (HK-SER16ECB)<br />
The HK-SER16ECB card has sixteen independent<br />
SIO channels with FIFO storing and supports<br />
RTS/CTS hardware handshake.<br />
Order Code Description<br />
HK-SER16ECB 16 channel serial interface card for the PI<br />
HK-SER8ECB 8 channel serial interface card for the PI<br />
Panel for Instrumentation Power Supply (LP-PEAP)<br />
If the power supply for the activation of inputs and<br />
outputs is not integrated in the device, the external<br />
power supply is possible via the LP-PEAP panel.<br />
If required, external components can be energised<br />
via the panel if a HS-NGSxxxx is integrated.<br />
For every channel, an additional serial interface<br />
module, like HD-RS2329PL, is required.<br />
The card can also be delivered with 8 channels (HK-<br />
SER8ECB).<br />
LP-PEAP Panel for supplying external power to feed sensors/actuators through<br />
inputs/outputs or feeding external components through on integrated power<br />
supply.<br />
LP-PEAPSK15 Plug and cable loom of cables for ± 15 V supply<br />
LPPEAPSK24 Plug and cable loom of cables, safeguard for +24 V supply<br />
Order Code Description<br />
LP-PEAP Panel for connection of external power supply<br />
LP-PEAPSK15 ±15 V= supply for LP-PEAP, including plug and cable<br />
LP-PEAPSK24 +24 V= supply for LP-PEAP, including plug and cable<br />
☞<br />
For LP-PEAPSK15 and LP-PEAPSK24, a suitable power<br />
supply HS-NGSxxxx is necessary!<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Measuring Amplifiers<br />
Laboratory Automation Hardware<br />
External Measuring Amplifier for pH/Redox<br />
The external buffer amplifier for pH and Redox<br />
electrode is integrated in a plug.<br />
The electrodes can be directly connected without pH<br />
measuring device. The cable with integrated<br />
amplifier is connected to a common analogue input.<br />
Temperature compensation and calibration are<br />
realised in a special device component in the PI.<br />
As the sensitive electrode signal is buffered directly<br />
in the plug, the cable can be extended without<br />
increasing the sensitivity.<br />
The voltage of the integrated Lithium cell can be<br />
tested at the plug.<br />
Advantages:<br />
� Space-Saving<br />
� Cable can be extended<br />
Product Description Buffer Amplifier for pH/Redox integrated in cable plug type HFS 13/4, input<br />
voltage -1<strong>10</strong>0....1<strong>10</strong>0 mV, input resistance > <strong>10</strong>0 MΩ, integrated lithium cell<br />
Delivery Scope Cable with integrated amplifier<br />
Manual with example for temperature compensation and calibration<br />
Order Code Description<br />
IL-PHAMP1 Cable with integrated amplifier pH/Redox electrodes<br />
Digital Measuring Amplifier for pH/Redox<br />
The external digital buffer amplifier for pH- and<br />
Redox electrodes does not require an own power<br />
supply when connected to a LAB-PNC.<br />
The electrodes can be directly connected without<br />
ph-measuring device.<br />
The temperature compensation is integrated. The<br />
calibration is conducted with a special module in the<br />
PNC.<br />
The sensitive electrode signal is directly digitalised<br />
and can be transmitted over long distances without<br />
any errors to the PNC.<br />
The voltage of the integrated Lithium battery can be<br />
read off via the serial interface.<br />
The amplifier can be connected to any RS232 V24<br />
interface.<br />
Advantages:<br />
� Integrated Temperature Compensation<br />
� Space-Saving Design<br />
� Extendable Cable<br />
Product Description Digital Buffer Amplifier for pH/RedOx with temperature compensation, input<br />
voltage-1<strong>10</strong>0....1<strong>10</strong>0mV, input resistance > <strong>10</strong>0 MΩ, integrated Lithium battery<br />
Delivery Scope Measuring Amplifier, Cable, Manual<br />
Order Code Description<br />
IL-PHAMP1D Digital Amplifier for pH- and Redox-Electrodes, RS232 V24 interface, incl. cable<br />
IL-PHAMP1D-SN Plug-In Power Supply for digital amplifier for pH- and Redox electrodes<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com <strong>10</strong>5<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
<strong>10</strong>6<br />
Laboratory Automation Hardware<br />
Measuring Amplifier for Load Cells and GraviDos<br />
The external is integrated into a plug housing.<br />
Load measuring cells or GraviDos weighing cells<br />
can be directly connected. The cable with the<br />
integrated amplifier is connected to a standard<br />
analogue input.<br />
The power supply of the amplifier is conducted via<br />
the interface and no additional power supply is<br />
required.<br />
In case a higher measuring precision is required, the<br />
digital measuring amplifier IL-GRADOMV1D, or the<br />
internal quadruple measuring system LP-<br />
DMS4DA4PT should be given preference.<br />
Advantages:<br />
� Space-Saving Design<br />
� Extendable Cable<br />
Product Description DMS Amplifier for DMS Full and Half-Bridge, Output Signal 4..20mA<br />
Delivery Scope Cable with integrated Amplifier<br />
Manual with Calibration Example<br />
Order Code Description<br />
IL-GRADOMV1 Cable with integrated Measuring Amplifier for DMS Load Cells<br />
You will find suited load cells in the according chapters Load Cells and under GraviDos.<br />
Digital Measuring Amplifier for Load Cells and GraviDos<br />
The digital measuring amplifier is suited for all <strong>HiTec</strong><br />
<strong>Zang</strong> load cells ( with the exception of the types with<br />
integrated measuring amplifier) as well as all other<br />
voltage-supplied DMS cells.<br />
� Integrated Calibration Function<br />
� Integrated Taring Function<br />
Technical Data:<br />
Input LEMO Jack Type S1<br />
Interface RS232 V24, Sub-D 9 pole, Power<br />
Supply on Pin 9<br />
If operated on an interface without<br />
power supply, a plug-in power<br />
Connection<br />
Measuring<br />
Bridge<br />
Bridge Supply<br />
Voltage<br />
supply is required.<br />
6 pole LEMO-Plug, Type<br />
FFA.1S.306.CLACxx<br />
5V<br />
Power Supply Via DataPlug, Sub-D 9, 5 V, 50 mA<br />
Dimensions L approx. 142 mm, W approx. 52<br />
mm, H approx. 23 mm, with Plug<br />
Product Description Digital DMS Amplifier for DMS Full and Half-Bridge, RS232 V24 Interface<br />
Delivery Scope Amplifier, RS232 Cable, Manual<br />
Order Code Description<br />
IL-GRADOAMP1D Digital Measuring Amplifier for DMS Load Cells, RS232 V24 Interface, incl. Cable<br />
IL-GRADOAMP1D-SN Plug-In Power Supply for digital amplifier for DMS load cells<br />
You will find suited load cells in the according chapters Load Cells and under GraviDos.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Cables for Instrumentation<br />
Laboratory Automation Hardware<br />
The following table presents ready to connect<br />
manufactured cables for various standard laboratory<br />
devices and instrumentation components. The offer<br />
is expanded continuously.<br />
If your device is not listed here, we can produce<br />
cables according to your specifications.<br />
Manufacturer, Device, Model,<br />
Interface<br />
kind<br />
Signal, Interface Panel / Module Cable Order Code<br />
LabManager and LabBox Cables<br />
Analogue Input, free cable ends<br />
voltage analogue LP-AEP8(A), LP-AEAP8U(A) ZK-LAB-HI01-IA-UP-O-01<br />
voltage, with 24 V sensor feed analogue LP-AEP8A, LP-AEAP8UA ZK-LAB-HI01-IA-UA-O-01<br />
0/4..20 mA twin wire analogue LP-AEP8(A) ZK-LAB-HI01-IA-IP-O-01<br />
0/4..20 mA twin wire with feed analogue LP-AEP8A ZK-LAB-HI01-IA-IA-O-01<br />
0/4..20 mA quadruple wire, opt. 24 V sensor feed<br />
Analogue Output, free cable ends<br />
analogue LP-AEP8A ZK-LAB-HI01-IA-IA-O-02<br />
Voltage analogue LP-AAP8UI ZK-LAB-HI01-OA-UP-O-01<br />
0/4..20 mA<br />
Digital Input, free cable ends<br />
analogue LP-AAP8UI ZK-LAB-HI01-OA-IP-O-01<br />
For switches, controllers<br />
Digital Output, free cable ends<br />
digital PDEP8 ZK-LAB-HI01-ID-XX-O-01<br />
For valves etc., 3 weirs: normally open and<br />
normally closed contact<br />
Pressure Transmitter<br />
digital LP-DAP8(A) ZK-LAB-HI01-OD-XX-O-01<br />
Pressure transmitter Kellar model series 21 analogue 4-20 mA current, twin wire on LP-AEP8A ZK-SP-KL21-IA-IA-I-01<br />
Pressure transmitter Kellar model series 23<br />
Heating/cooling Thermostats<br />
analogue 4-20 mA current, twin wire on LP-AEP8A ZK-SP-KL23-IA-IA-I-01<br />
Lauda thermostat model<br />
analogue temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A) ZK-T-LD01-BA-UP-Y-01<br />
C6CS/C12CS/C20CS/K6KS/K12KS/K20KS<br />
temperature set point, 0..<strong>10</strong> V on LP-AAP8UI<br />
Lauda thermostat model<br />
analogue temperature actual value, 0..<strong>10</strong>V on LP-AEP8(A) ZK-T-LD01-BA-KP-Y-01<br />
C6CS/C12CS/C20CS/K6KS/K12KS/K20KS<br />
temperature actual value channel 1 & set point, 4-20<br />
mA on LP-AEAP8I(A)<br />
Lauda thermostat model<br />
serial temperature actual value<br />
ZK-T-LD01-BS-R2-I-02<br />
C6CS/C12CS/C20CS/K6KS/K12KS/K20KS<br />
temperature actual value, set point<br />
Lauda thermostat model USH400 analogue temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A)<br />
temperature set point, 0..<strong>10</strong> V on LP-AAP8UI<br />
ZK-T-LD03-BA-UP-Y-01<br />
Jucheim thermostat model 80-4 / 90-4 analogue temperature actual value, 0..20 mA on LP-AEP8(A)<br />
temperature set point, 0..20 mA on LP-AAP8UI<br />
ZK-T-JH01-BA-IP-Y-01<br />
Julabo thermostat model FM50MH analogue temperature set point, 0..20 mA on LP-AAP8UI<br />
temperature working sensor 0-<strong>10</strong> V on LP-AEP8(A)<br />
Ext. temperature sensor, 0-<strong>10</strong> V on LP-AEP8(A)<br />
set point feedback, 0-<strong>10</strong> V on LP-AEP8(A)<br />
ZK-T-JU01-BA-KP-Y-01<br />
Julabo thermostat model FM50MH analogue temperature set point, 0..20 mA on LP-AAP8UI<br />
temperature working sensor 0-<strong>10</strong> V on LP-AEP8(A)<br />
ext. temperature sensor, 0-<strong>10</strong> V on LP-AEP8(A)<br />
ZK-T-JU01-BA-KP-Y-02<br />
Julabo thermostat model HP / SP / TP analogue temperature set point, 0..20 mA on LP-AAP8UI<br />
ext. temperature sensor, 0-<strong>10</strong> V on LP-AEP8(A)<br />
int. temperature sensor, 0-<strong>10</strong> V on PAEP8<br />
set point feedback, 0-20 mA on LP-AEP8(A)<br />
ZK-T-JU02-BA-KP-Y-01<br />
Julabo thermostat model ATS3 / ATS2 analogue temperature set point, 0..20 mA on LP-AAP8UI<br />
temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A)<br />
2 x 4-pin tuchel on thermostat<br />
ZK-T-JU04-BA-KP-Y01<br />
Julabo thermostat RS232 temperature set point, ext. temperature sensor,<br />
int. temperature sensor, set point feedback<br />
ZK-T-JU00-BS-R2-I-01<br />
Eurotherm thermostat type RD4455 model 99 analogue temperature set point, 0..<strong>10</strong> V on LP-AAP8UI<br />
temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A)<br />
ZK-T-ET99-BA-UP-Y01<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com <strong>10</strong>7<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
<strong>10</strong>8<br />
Laboratory Automation Hardware<br />
Huber thermostat model Tango analogue temperature set point, 0..<strong>10</strong> V on LP-AAP8UI<br />
Bath temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A)<br />
Open cable end<br />
ZK-T-HU04-BA-UP-O-01<br />
Huber thermostat model Tango analogue temperature set point, 4..20 mA on LP-AAP8UI<br />
temperature actual value, 4..20 mA on LP-AEP8(A)<br />
Open cable end<br />
ZK-T-HU04-BA-IP-O-01<br />
Huber thermostat model Tango(unistat<br />
control)<br />
RS232 temperature set point, actual value via RS232 ZK-T-HU01-BS-R2-I-01<br />
Huber thermostat model Tango (unistat<br />
control)<br />
RS485 temperature set point, actual value via RS485 ZK-T-HU01-BS-R4-I-01<br />
Thermostat Huber compatible control RS232 temperature set point, actual value via RS232 ZK-T-HU02-BS-R2-I-01<br />
Thermostat Huber compatible control RS485 temperature set point, actual value via RS485 ZK-T-HU02-BS-R4-I-01<br />
Haake thermostat analogue temperature set point, 4..20 mA on LP-AAP8UI<br />
ZK-T-HA01-BA-IP-Y-01<br />
temperature actual value, 4..20 mA on LP-AEP8(A)<br />
Haake thermostat RS232 temperature set point, temperature actual value ZK-T-HA01-BS-R2-I-01<br />
<strong>HiTec</strong> Laboratory Devices (see also stirrer and solid doser)<br />
Hitec model Kaloheiz, control input analogue voltage, 6 pin tuchel on LP-AAP8UI ZK-KAL-HI04-OA-UP-I-01<br />
Hitec model Kaloheiz, voltage monitor analogue voltage, 6 pin tuchel on LP-AEP8(A) ZK-KAL-HI04-IA-UP-I-01<br />
Hitec model Kaloheiz, current monitor<br />
Lab Balances/Scales<br />
analogue voltage, 6 pin tuchel on LP-AEP8(A) ZK-KAL-HI04-IA-UP-I-02<br />
Kern balance model EW 3000-2M RS232 RS232, 5pol. Hoshiden plug / D-Sub9 socket on<br />
ZK-W-KE01-BS-R2-I-01<br />
RS2329(P)L<br />
Kern balance model GS RS232 RS232, 25pin-plug - 9pin-socket ZK-W-KE02-BS-R2-I-01<br />
Kern balance model PB 4002-2 RS232 RS232, 9pin-plug - 9pin-socket ZK-W-KE03-BS-R2-I-01<br />
Sartorius / Scaltec balance model SBC RS232 RS232, 25pin-plug - 25pin-socket ZK-W-SA01-BS-R2-I-01<br />
Sartorius / Scaltec balance model SBC RS232 RS232, 9pin-plug - 9pin-socket ZK-W-SA01-BS-R2-I-03<br />
Sartorius / Scaltec balance model SBC mixed RS232, D-Sub9 socket on RS2329,<br />
tare on LP-DAP8 (passive panel)<br />
ZK-W-SA01-BK-R2P-Y-02<br />
Sartorius / Scaltec balance model SBC mixed RS232, D-Sub9 socket on RS2329,<br />
ZK-W-SA01-BK-R2A-Y-02<br />
tare on LP-DAP8A (active panel)<br />
Mettler balance model PM/AM 25 pin RS232 25 pin, 15 pin Mettler plug ZK-W-ME01-BS-R2-I-01<br />
Mettler balance model PM/AM 9 pin RS232 9 pin, 15 pin Mettler plug ZK-W-ME01-BS-R2-I-02<br />
Mettler balance model PG<br />
Magnetic Valves<br />
RS232 9 pin, 9 pin ZK-W-ME02-BS-R2-I-01<br />
Magnetic valves (on/off), plug models 2508, digital 24 V, 4 pol. ISO4400 socket / tuchel socket<br />
ZK-VMB-HI41-OD-XA-I-01<br />
DIN 43650 form A<br />
on LP-DAP8A<br />
Magnetic valves (on/off), plug models 2508, digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />
ZK-VMB-HI42-OD-XA-I-01<br />
DIN 43650 form B<br />
LP-DAP8A<br />
Magnetic valves (on/off), plug models 2508, digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />
ZK-VMB-HI43-OD-XA-I-01<br />
DIN 43650 form C<br />
LP-DAP8A<br />
Magnetic valves (proportional), plug models digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />
ZK-VMP-HI41-OD-XA-I-01<br />
2506, DIN 43650 form A<br />
LP-DAP8T, PWM<br />
Magnetic valves (proportional), plug models digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />
ZK-VMP-HI42-OD-XA-I-01<br />
2506, DIN 43650 form B<br />
LP-DAP8T, PWM<br />
Magnetic valves (proportional), plug models digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />
ZK-VMP-HI42-OD-XA-I-01<br />
2506, DIN 43650 form C<br />
Magnetic valves type Buerkert<br />
(proportional)<br />
cable head <strong>10</strong>54/<strong>10</strong>57 (Valve 0127)<br />
LP-DAP8T, PWM<br />
digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />
LP-DAP8T, PWM<br />
ZK-VMP-BU04-OD-XA-I-<br />
01<br />
Magnetic valves type Buerkert<br />
(proportional)<br />
cabel head <strong>10</strong>94<br />
analogue 4..20 mA on LP-AAP8UI ZK-VMP-BU03-OA-IA-I-01<br />
Knauer multi-path valve model HPLC7 RS232 ZK-VMO-KN07-BS-R2-I-01<br />
VICI AG Valco-Multi directional control RS232 ZK-VMO-VI01-BS-R2-I-01<br />
valve<br />
Dosing Pumps<br />
<strong>HiTec</strong> <strong>Zang</strong> pump, LabDos mixed set point 4-20 mA on LP-AAP8UI<br />
Start/Stop on LP-DAP8A<br />
ZK-HI36-OK-IP-Y-01<br />
<strong>HiTec</strong> <strong>Zang</strong> pump, LabDos RS232 set point and status information, 9pin/9pin ZK-P-HI36-BS-R2-I-01<br />
ISMATEC pump model ISM736 mixed set point 4-20 mA on LP-AAP8UI<br />
ZK-P-IS01-OK-IP-Y-02<br />
Start/Stop on LP-DAP8A<br />
ISMATEC pump model MC-Z / MS-Z analogue set point 0-5,7/0-<strong>10</strong> V voltage passive LP-AAP8UI ZK-P-IS03-OA-UP-I-01<br />
ISMATEC pump Reglo Digital hose pump RS232 ZK-P-IS04-BS-R2-I-01<br />
Knauer pump RS232 ZK-P-KN00-BS-R2-I-01<br />
Prominent Pump model Gamma analogue stroke amount set point 4..20 mA on LP-AAP8UI ZK-P-PR01-OA-IP-I-01<br />
Telab pump model BF414 RS232 stroke frequency, stroke volume ZK-P-TL02-BS-R2-I-01<br />
Telab pump model BF414, before 2000 analogue stroke frequency set point, 4...20 mA LP-AAP8UI<br />
stroke volume set point, 4...20 mA LP-AAP8UI<br />
9 pin Sub-D plug<br />
ZK-P-TL02-OA-IP-Y-01<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
Telab pump model BF414, after 2000 analogue stroke frequency set point, 4...20 mA on LP-AAP8UI<br />
stroke volume set point, 4...20 mA on LP-AAP8UI<br />
15 pin HD-plug<br />
Telab pump model BF414, before 2000 analogue stroke frequency set point, 0...<strong>10</strong> V on LP-AAP8UI<br />
stroke volume set point, 0...<strong>10</strong> V on LP-AAP8UI<br />
9 pin Sub-D plug<br />
Telab pump model BF414, after 2000 analogue stroke frequency set point, 0...<strong>10</strong> V on LP-AAP8UI<br />
stroke volume set point, 0...<strong>10</strong> V on LP-AAP8UI<br />
15 pin Sub-D plug<br />
Telab pump model BF414, before 2000 analogue stroke frequency set point, 4...20 mA LP-AAP8UI<br />
stroke volume set point, 4...20 mA LP-AAP8UI<br />
release on LP-DAP8<br />
9 pin Sub-D plug<br />
Telab pump model BF414, after 2000 analogue stroke frequency set point, 4...20 mA on LP-AAP8UI<br />
stroke volume set point, 4...20 mA on LP-AAP8UI<br />
release on LP-DAP8<br />
15 pin HD-plug<br />
Telab pump model BF414, before 2000 analogue stroke frequency set point, 0...<strong>10</strong> V on LP-AAP8UI<br />
stroke volume set point, 0...<strong>10</strong> V on LP-AAP8UI<br />
release on LP-DAP8<br />
9 pin Sub-D plug<br />
Telab pump model BF414, after 2000 analogue stroke frequency set point, 0...<strong>10</strong> V on LP-AAP8UI<br />
stroke volume set point, 0...<strong>10</strong> V on LP-AAP8UI<br />
release on LP-DAP8<br />
15 pin Sub-D plug<br />
Telab pump model BF414, before 2000 digital Pulse on LP-DAP8, release on LP-DAP8<br />
9 pin Sub-D plug<br />
Telab pump model BF414, after 2000 digital Pulse on LP-DAP8, release on LP-DAP8<br />
15 pin Sub-D plug<br />
ZK-P-TL02-OA-IP-Y-02<br />
ZK-P-TL02-OA-UP-Y-01<br />
ZK-P-TL02-OA-UP-Y-02<br />
ZK-P-TL02-OK-IP-Y-01<br />
ZK-P-TL02-OK-IP-Y-02<br />
ZK-P-TL02-OK-UP-Y-01<br />
ZK-P-TL02-OK-UP-Y-02<br />
ZK-P-TL02-OD-XP-Y-01<br />
ZK-P-TL02-OD-XP-Y-02<br />
Dosing Apparatus<br />
Metrohm Dosimat 665 RS232 set point, actual value ZK-DL-MO01-BS-R2-I-01<br />
Metrohm Titrino 718 RS232 complete Titrino command tree ZK-DL-MO02-BS-R2-I-01<br />
Solid Dosing Apparatus<br />
Solidos controller Hitec ViscoPact and<br />
ViscoPact.rheo<br />
(from firmware 2.<strong>10</strong>, March 2001)<br />
Solidos controller Hitec ViscoPact and<br />
ViscoPact.rheo<br />
(from firmware 2.<strong>10</strong>, March 2001)<br />
Solidos controller Hitec ViscoPact and<br />
ViscoPact.rheo<br />
analogue rotational speed set point voltage 0..<strong>10</strong> V<br />
on LP-AAP8UI<br />
rotational speed actual value voltage 0..<strong>10</strong> V<br />
on LP-AEP8(A)<br />
rotational speed actual value voltage 0..<strong>10</strong> V<br />
on LP-AEP8(A)<br />
analogue rotational speed set point current 0/4..20 mA<br />
on LP-AAP8UI<br />
rotational speed actual value current 0/4..20 mA on LP-<br />
AEP8(A)<br />
torque actual value current 0/4..20 mA<br />
on LP-AEP8(A)<br />
RS232 rotational speed set point,<br />
rotational speed actual value,<br />
torque actual value, on/off<br />
Stirrer drives<br />
Heidolph stirrer model RZR 2<strong>10</strong>2 analogue torque actual value 4-20 mA on LP-AEP8(A)<br />
rotational speed actual value 4-20 mA<br />
on LP-AEP8(A)<br />
<strong>HiTec</strong> stirrer model ViscoPact and<br />
ViscoPact-rheo<br />
(from firmware 2.<strong>10</strong>, March 2001)<br />
<strong>HiTec</strong> stirrer model ViscoPact and<br />
ViscoPact-rheo<br />
(from firmware 2.<strong>10</strong>, March 2001)<br />
<strong>HiTec</strong> stirrer model ViscoPact and<br />
ViscoPact-rheo<br />
rotational speed set point 4-20 mA on LP-AAP8UI<br />
analogue rotational speed set point voltage 0..<strong>10</strong> V<br />
on LP-AAP8UI<br />
rotational speed actual value voltage 0..<strong>10</strong> V<br />
on LP-AEP8(A)<br />
rotational speed actual value voltage 0..<strong>10</strong> V<br />
on LP-AEP8(A)<br />
analogue rotational speed set point current 0/4..20 mA<br />
on LP-AAP8UI<br />
rotational speed actual value current 0/4..20 mA<br />
on LP-AEP8(A)<br />
torque actual value current 0/4..20 mA on LP-AEP8(A)<br />
RS232 rotational speed set point, actual value,<br />
torque actual value,<br />
on/off<br />
IKA stirrer model Eurostar analogue rotational speed actual value voltage on LP-AEP8(A)<br />
torque actual value voltage on LP-AEP8(A)<br />
ZK-R-HI02-BA-UP-Y-03<br />
ZK-R-HI02-BA-IP-Y-02<br />
ZK-R-HI02-BS-R2-I-01<br />
ZK-R-HD02-BA-IP-Y-01<br />
ZK-R-HI02-BA-UP-Y-03<br />
ZK-R-HI02-BA-IP-Y-02<br />
ZK-R-HI02-BS-R2-I-01<br />
ZK-R-IK01-BA-UP-Y-01<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
1<strong>10</strong><br />
Laboratory Automation Hardware<br />
IKA stirrer model Eurostar mixed rotational speed actual value voltage on LP-AEP8(A)<br />
torque actual value voltage on LP-AEP8(A)<br />
set point on RS232, serial measured on HD-plug<br />
ZK-R-IK01-BK-R2-Y-01<br />
IKA stirrer model Eurostar RS232 RS232 serial interface 9-pin DSub ZK-R-IK01-BS-R2-I-01<br />
IKA stirrer model Eurostar<br />
Sensors<br />
RS232 RS232 serial interface 15-pin HD ZK-R-IK01-BS-R2-I-02<br />
Brooks flow rate sensor model 5850TR analogue Flow rate sensor 15-pin D-Sub<br />
ZK-SFM-BR01-BA-UA-Yactual<br />
value on LP-AEP8A, set point on LP-AAP8UI 01<br />
Brooks flow rate sensor model 5850TR RS232 Flow rate sensor 15-pin D-Sub<br />
actual value, set point<br />
ZK-SFM-BR01-BS-R2-I-01<br />
Bronkhorst flow rate controller model analogue LP-AEAP8UA + 24V feeding ZK-CFM-BK21-BA-UA-I-01<br />
F-xxxaa-FAB/FBB/GAB/GBB-xx-a<br />
Bronkhorst flow rate controller model MFC<br />
F-xxxx-FA/FB/GA/GB-xx and F-xxxaa-FAC/<br />
FBC/GAC/GBC-xx-a<br />
Bronkhorst flow rate controller model<br />
F-xxxaa-FCB/FDB/GCB/GDB-xx-a<br />
Bronkhorst flow rate controller model MFC<br />
F-xxxx-FC/FD/GC/GD-xx and<br />
F-xxxaa-FCC/FDC/GCC/GDC-xx-a<br />
Laboratory gas meter type TG, impulse<br />
output<br />
analogue LP-AEAP8UA +/- 15 V feeding ZK-CFM-BK22-BA-UA-I-01<br />
analogue LP-AEAP8IA + 24 V feeding<br />
First choice type<br />
ZK-CFM-BK23-BA-IA-I-01<br />
analogue LP-AEAP8IA +/- 15 V feeding ZK-CFM-BK24-BA-IA-I-01<br />
binary 5-pin plug DIN51524 device-side to 3-pin plug DIN51524<br />
for connection to DEP8A<br />
ZK-SFV-RI01-ID-XX-I-01<br />
Watchdog<br />
0/4..20mA twin wire<br />
PC Cables<br />
analogue Watchdog -plug ZK-X-HI05-IA-IA-O-01<br />
<strong>HiTec</strong> Null modem cable RS232 RS232, 2x 9-pin-SubD ZK-IT-HI<strong>10</strong>-BS-R2-I-01<br />
<strong>HiTec</strong> RS232 extension RS232 RS232 9-pin ZK-IT-HI11-BS-R2-I-01<br />
<strong>HiTec</strong> UI Com1 RS232 25-pin to 25- pin RS232 ZK-IT-HI01-BS-R2-I-01<br />
<strong>HiTec</strong> UI Com1 RS232 9- pin to 9-pin, RS232 ZK-IT-HI01-BS-R2-I-02<br />
<strong>HiTec</strong> UI Com1<br />
Miscellaneous, periphery<br />
RS232 25-pin to 9-pin, RS232 ZK-IT-HI01-BS-R2-I-03<br />
Labcom cable ZK-LAB-HI07-BS-R2A-I-01<br />
<strong>HiTec</strong> type B230V16H, B230V16R digital LP-DAP8A, LP-DAP8T ZK-LAB-HI06-OD-XX-I-01<br />
Jeti spectrometer RS232 RS232 9-pin ZK-X-JE01-BS-R2-I-01<br />
Pt<strong>10</strong>0 extension analogue LEMO socket/plug 4-pin ZK-XX-HI11-BA-PX-I-01<br />
Edwards Typ Active-Gauge-Display (AGD)<br />
for Active-Pirani-Gauge (APG)<br />
analogue analogue voltage on LPAEP8 ZK-X-EW01-IA-UP-I-01<br />
Driver Programs for Laboratory Device Interfaces<br />
Laboratory devices with serial interfaces can be<br />
integrated into the system via serial interface of the<br />
PI or the UI.<br />
Devices connected to the PI can be linked without<br />
problems to control loops such as sensor or final<br />
control elements.<br />
Devices connected to the UI can also be integrated<br />
as sensors or final control elements in control loops;<br />
however, values needed for automated control must<br />
be permanently replaced through the UI PI interface.<br />
Driver<br />
According to the complexity of the protocol, different<br />
kinds of drivers maybe useful. Drivers can partially<br />
be parameterised by the user, for the other part, they<br />
must be parameterised by a programmer.<br />
Integrated Drivers<br />
For most lab balances from Scaltec, Kern, Sartorius<br />
and Mettler, as well as heating/cooling thermostats<br />
by Huber, Julabo, Lauda or Thermo-Haake, interface<br />
drivers are already integrated.<br />
NAMUR Driver<br />
Laboratory devices with an ASCII log according to<br />
NAMUR- NE28 recommendation can simply be<br />
connected to the PI via the NAMUR driver (see<br />
NAMUR driver).<br />
PI Driver<br />
Laboratory devices with more complicated logs, in<br />
particular binary logs, can be connected to a serial<br />
interface of the UI via specific PI drivers (see PI<br />
driver).<br />
Specific Drivers<br />
For laboratory devices with more complicated logs,<br />
in particular binary logs, which are supposed to be<br />
connected directly to the PI, a driver must be<br />
programmed by our programming department.<br />
Where appropriate, a communication processor<br />
maybe necessary.<br />
HiText Driver<br />
Laboratory devices with more complicated logs can<br />
be connected to a serial interface of the UI via a<br />
driver written in HiText. The HiText driver can be<br />
programmed by the customer himself or by our<br />
programming department.<br />
The following table presents the available driver programs for various standard laboratory devices<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
and instrumentation components. The offer is<br />
continuously expanded.<br />
If your device is not listed here, do not hesitate to<br />
ask for it.<br />
Manufacturer, device, model<br />
Heating/cooling Thermostats<br />
Signal type, connection, card,<br />
driver<br />
Required interface panel / module, cable Driver Order Code<br />
Huber unistat set point output -O and<br />
actual value-I*<br />
RS232, NAMUR-driver HD-RS2329(P)L, ZK-T-HU01-BS-R2-I-01 SF-NAMTHHU1<br />
Julabo set point output -O and actual<br />
value-I*<br />
RS232, NAMUR-driver HD-RS2329(P)L, ZK-T-JU00-BS-R2-I-01 SF-NAMTHJUL1<br />
Haake thermostat F6-C35 * RS232, NAMUR-driver HD-RS2329(P)L, ZK-T-HA01-BS-R2-Y-01 SF-NAMTHHAK1<br />
Lauda set point output -O and actual<br />
value-I*<br />
Stirrer<br />
RS232, NAMUR-driver HD-RS2329(P)L, ZK-T-LD01-BS-R2-I-01 SF-NAMTHLAU1<br />
ViscoPakt * RS232, NAMUR-driver HD-RS2329(P)L, ZK-R-HI02-BS-R2-I-01 SF-NAMRUVIPA1<br />
Heidolph RS232, NAMUR-driver HD-RS2329(P)L, ZK-R-IK01-BS-R2-I-01 SF-NAMIRUPV<br />
IKA Powervisc<br />
Dosing Pumps<br />
RS232, NAMUR-driver HD-RS2329(P)L,<br />
ZK-R-IK01-BS-R2-I-01 (9 pin),<br />
ZK-R-IK01-BS-R2-I-02 (15 pin)<br />
SF-NAMIRUPV<br />
TELAB BF414, 9-pin SUB-D RS232, NAMUR-driver HD-RS2329(P)L, ZK-P-TL02-BS-R2-I-01 SF-NAMDPTEL1<br />
Knauer K1800 RS232, NAMUR-driver HD-RS2329(P)L, ZK-P-KN00-BS-R2-I-01 SF-NAMDPKNA1<br />
Knauer K501 RS232, NAMUR-driver HD-RS2329(P)L, ZK-P-KN00-BS-R2-I-01 SF-NAMDPKNA2<br />
Metrohm Dosino Titrator 718 PI-driver PC-COM-Port ZK-DL-MO02-BS-R2-I-01 SF-PNKMTRx<br />
x = 1,2,4,8<br />
Metrohm Dosino Dosimat 665 PI-driver PC-COM-Port ZK-DL-MO01-BS-R2-I-01 LV-PNKMTRx<br />
x = 1,2,4,8<br />
Ismatec hose pump Reglo Digital PI-driver HD-RS2329(P)L, ZK-P-IS04-BS-R2-I-01 LV-PNKDPISM1<br />
Ismatec wobbling piston Relgo FMI<br />
Multipath Valves<br />
PI-driver HD-RS2329(P)L, ZK-P-IS04-BS-R2-I-01 LV-PNKDPISM1g<br />
Knauer HPLC7 RS232, NAMUR-driver HD-RS2329(P)L, ZK-VMO-KN07-BS-R2-I-01 SF-NAMMVKNA1<br />
Besta MW1 / MW2 multi-path valves<br />
Massflow-Meter and Controller<br />
RS232, NAMUR-driver HD-RS2329(P)L SF-NAMMWVAL1<br />
Bronkhorst set point output and actual<br />
value-E<br />
RS232, NAMUR-driver HD-RS2329(P)L, ZK-CFM-BK00-BS-R2-T-01 SF-NAMMFBRON1<br />
Brooks set point output and actual<br />
value-E<br />
Massflow meter & Controller<br />
RS232, NAMUR-driver HD-RS2329(P)L, ZK-CFM-BR01-BS-R2-I-02 SF-NAMMFBROO1<br />
ModBus-devices PI-driver PC-COM-Port,<br />
SF-PNKMBUSx<br />
PC-RS485<br />
x = 1,2,4,8<br />
* Most of the devices of this manufacturer are already implemented as device components, so that additional<br />
drivers are only required in special cases.<br />
PI-driver: additional module for LabVision<br />
NAMUR driver: parameterisation of the module NAMSER-X (additionally required)<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Hardware<br />
Automation<br />
Software<br />
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Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
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Dosing Systems,<br />
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Autosampler<br />
Stirring and<br />
Dispersing<br />
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112<br />
Laboratory Automation Hardware<br />
MSRmanager-System<br />
MSRmanager front view with mounted fastening angles<br />
The MSRmanager is mainly used in installations of<br />
the process and chemical engineering industry,<br />
research, environmental and process engineering,<br />
test facility automation and the manufacturing<br />
industry.<br />
It is deployed instead of the LAB-PI’s if the<br />
installation is to be hardwired.<br />
The main emphasis was put on compact<br />
construction and flexibility. One of many advantages<br />
in comparison to usual PLC or process computer<br />
based solutions derives from the possibility to<br />
change the parameters during the runtime without<br />
having to stop the installation. Especially during<br />
challenging projects of automation, the<br />
MSRmanager shows its unique features.<br />
Universal, free from potential and flexible interfaces<br />
save many transducers, interface and driver circuits.<br />
Using minimal space, the MSRmanager enables to<br />
even fulfil the most complex tasks which could either<br />
not be accomplished at all or only at great expense<br />
using conventional equipment.<br />
Because of its wide field of possible applications and<br />
its universal connection technology, the<br />
MSRmanager is an economical alternative to many<br />
other systems.<br />
The broad spectrum of available inputs and outputs<br />
even includes serial interfaces. To connect balances,<br />
analysers, dosing units etc., up to 15 serial<br />
interfaces can be installed.<br />
The MSRmanager system can be easily expanded<br />
and used for diverse applications. It is possible to<br />
realize networked systems and to include controllers<br />
from other manufacturers.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
MSRmanager Organisation<br />
Laboratory Automation Hardware<br />
In order to realize installations for applications with<br />
up to 240 inputs/outputs, an MSRmanager can be<br />
equipped with the required interface cards and<br />
terminal blocks.<br />
The suitable modules can be found in the chapter<br />
MSRmanager Interfaces. A serial interface with<br />
potential isolation for connection to the Operator-<br />
Console (control computer) is provided.<br />
The Connection Technology<br />
Sensors and positioners are connected to the PI unit<br />
via terminal blocks. They are connected to the input/<br />
output cards by ribbon cable. Therefore, there is a<br />
plug on every terminal module to connect the ribbon<br />
cable. The signalling lines are applied with screwing<br />
terminals at the terminal block<br />
CG-ABK1x or CG-ABK2x are used as the control<br />
computer.<br />
The PI-UI coupling is accomplished via RS232 and<br />
up to <strong>10</strong> m long data cables (as standard, a 3 m<br />
cable will be delivered, other lengths upon request).<br />
The cabling can optionally be done by RS485 or<br />
optical fibres with up to 2000 m length.<br />
(HAV24LINK...).<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
114<br />
Free standing mounting installation<br />
Laboratory Automation Hardware<br />
The terminal blocks can either be mounted on the<br />
backside of the MSRmanager or on the top-hat rail<br />
or in a cabinet.<br />
Basic Devices<br />
MSRmanager-Basic Device<br />
The basic device contains the interface cards and<br />
the subsystems. The electronic frame is a solid 19inch<br />
chassis made of metal, which is suitable for<br />
freestanding mounting as well as for integrating into<br />
19-inch cabinets.<br />
The minimum configuration includes the circuit<br />
board with the bus, a 32-bit CPU, a watchdog circuit<br />
and a serial Operator-Console interface which is<br />
potential-isolated.<br />
The power saving CMOS-technology does not<br />
create much heat so that the device does not have<br />
to be ventilated. Therefore, there are no specific<br />
conditions as to where to install it.<br />
The minimal configuration consists of the basic<br />
device, a <strong>HiTec</strong> UI (e.g. CG-ABK1), a HK-AD20N<br />
analogue/digital conversion card and a HK-HMUXmultiplexor<br />
card with terminal block (e.g. MB-<br />
MSRmanager rear view Clamping yoke for ribon cable and Cable outlet<br />
The ribbon cables to the MSRmanager can be<br />
tailored accordingly. For each input/output card there<br />
are various terminal blocks available. The example<br />
shown here is the terminal block MB-AEB16V.<br />
We look forward to supporting your project planning!<br />
A terminal block mounted on a system rail<br />
AEB16VP). This system is well suited for e.g. data<br />
logging with 16 zero potential universal analogue<br />
inputs.<br />
Onto this device, thermal elements, Pt<strong>10</strong>0, voltage<br />
and current emitting sensors, etc. can be coupled in<br />
arbitrary combinations.<br />
The device can be upgraded to up to 240 analogue<br />
and 128 binary interfaces (with PLC subsystem) so<br />
that it is adaptable to every task.<br />
The indicators and control elements for basic<br />
operations are located on the front panel of the<br />
MSRmanager. The “DC“ display indicates the status<br />
of the power supply. The “Busy“ display signalizes<br />
the operational status. The “COM“ display indicates<br />
the traffic to and from the Operator Console.<br />
Upon request, the terminal block can be mounted on<br />
the device rear panel.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
Configuration of the MSRmanager Basic Device:<br />
� 19 inch, 3HE slide-in module or desktop chassis<br />
� 14 slots (optional 19), one of which is occupied<br />
by the CPU card<br />
� Battery backed real time clock<br />
� Watchdog (monitoring circuit)<br />
� Zero potential serial port for the UI (control<br />
computer)<br />
Reserves for extensions<br />
On the back of the MSRmanager there are ports for<br />
the control computer and an optional 6 serial<br />
interfaces.<br />
Up to a maximum of four DIN system rails (top-hat<br />
rails) can be attached to the back of the terminal<br />
blocks to save additional space. For strain relief of<br />
the ribbon cables there is a clamping mechanism.<br />
Optionally the MSRmanager can be delivered with a<br />
24 V or 48 V power supply instead of a 230 V~ one.<br />
Reserve supplied with<br />
13 slots HK-AD20N, HK-HMUX, HK-DEA16N, HK-DA812UI, HK-SER8ECB, HK-<br />
SER16ECB<br />
6 serial interfaces on<br />
basis panel<br />
HD-RS2329(P)L, HD-RS485P<br />
1 panel slot for<br />
LP-SER99<br />
HD-RS2329(P)L, HD-RS485P<br />
Internal Power supply, control voltage, digital terminal blocks HS-NGS242, HS-NGS241S<br />
Technical Data<br />
Casing 3 HE desktop case<br />
Basis panel UI-Interface, 230 V~ power supply and indicator LEDs<br />
CPU CPU 32 card, 32 bit embedded controller with watchdog<br />
Development reserve See table<br />
Dimensions Depth: 370 mm<br />
Width: 450 mm (19“)<br />
Height: 145 mm (3 HE)<br />
Working temperature 0 - 50 °C, non-condensing<br />
Storing temperature 0 - 50 °C<br />
IP protection class IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory device<br />
Power consumption From 30 W to 140 W, depending on the configuration<br />
Operating voltage 230 V +<strong>10</strong>/-20 %, opt. widerange <strong>10</strong>0 to 240 V.<br />
Delivery Scope MSRmanager<br />
power supply cable<br />
manual<br />
cable to connect to the 9-pin RS232 interface of UI<br />
Order Code Description<br />
MG-MSRMAN MSRmanager basic device<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
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Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Components<br />
Process Analytics<br />
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Dosing Systems,<br />
Pumps<br />
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Stirring and<br />
Dispersing<br />
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MSRbox Basic Device<br />
Laboratory Automation Hardware<br />
The MSRbox-basis devices are, with exception of<br />
the reduced mounting possibilities, to a large extent<br />
identical with the MSRmanager basis device. They<br />
carry the required interface cards, sub systems, and<br />
hardware options. The electronics chassis is a<br />
robust metal casing, which is both suited for free<br />
mounting and for the assembly in control cabinets.<br />
The minimum configuration includes the circuit<br />
board with the bus, a CPU and multifunction card,<br />
the CMOS-RAM and a watchdog circuit as well as<br />
serial interface to the control computer, which is<br />
potential-isolated.<br />
The power saving CMOS-technology minimises lost<br />
heat so that the device does not have to be<br />
ventilated. Therefore there are no specific conditions<br />
as to where to install it.<br />
The basic device, in connection with a <strong>HiTec</strong> UI (e.<br />
g. CG-ABK1), a HK-AD20NMUX8 card with terminal<br />
block (e. g. MB-AEB16VP) already represents the<br />
hardware of a data logging system with 8 potentialfree,<br />
universal analogue input channels.<br />
Configuration of the MSRbox Basic Device:<br />
� 3HE slide-in module or desktop chassis<br />
� Battery backed real time clock<br />
� Watchdog (monitoring circuit)<br />
� serial port for the control computer (UI)<br />
Extension Reserve:<br />
To this device, thermal elements, Pt<strong>10</strong>0, voltage and<br />
current emitting sensors, etc. can be coupled in<br />
arbitrary combination<br />
The devices can be upgraded with the available<br />
interfaces and consequently adjusted to any<br />
application purpose.<br />
The indicators and control elements for basic<br />
operations are located on the front panel of the<br />
MSRmanager. The “DC“ display indicates the status<br />
of the power supply. The “Busy“ display signals the<br />
operational status. The “COM“ display indicates the<br />
traffic to and from the Operator-Console.<br />
For strain relief of the ribbon cables there is a<br />
clamping mechanism.<br />
Upon request, the terminal blocks can be mounted<br />
on the device rear panel.<br />
At the MG-MSRBOX2 up to HS-NGS243 can be<br />
integrated for activated sensors and actuators. If the<br />
peripheral power supply can be the MG-MSRBOX2<br />
is a space safing alternative in the MG-MSRBOX1<br />
and MG-MSRBOX2.<br />
On the rear of the MSRbox, there are connections<br />
for UI/workstations and up to four serial ports for<br />
connection of suitable devices.<br />
MSRbox1 MSRbox2S (1/2 19“) MSRbox2<br />
slots 2 (+ 1 CPU) 5 (+1 CPU) 5 (+1 CPU)<br />
supplied with HK-AD20NMUX8, HK- HK-AD20NMUX8, HK- HK-AD20NMUX8, HK-<br />
AD20NMUX16, HK- AD20NMUX16, HK- AD20NMUX16, HK-<br />
DEA16N, HK-DA812UI, HK- DEA16N, HK-DA812UI, HK- DEA16N, HK-DA812UI, HK-<br />
AD24DMS4, HK-SER8ECB, AD24DMS4, HK-SER8ECB, AD24DMS4, HK-SER8ECB,<br />
HK-SER16ECB<br />
HK-SER16ECB<br />
HK-SER16ECB<br />
serial interfaces Max. 4 HD-RS2329L, HD- Max. 4 HD-RS2329L, HD- Max. 4 HD-RS2329L, HD-<br />
RS2329PL, HD-RS485P RS2329PL, HD-RS485P RS2329PL, HD-RS485P<br />
internal Power supply for digital Power supply for digital Power supply digital terminal<br />
terminal blocks (control terminal blocks (control blocks (control voltage) ma.<br />
voltage)<br />
current) by main power<br />
supply<br />
2xNGS243<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Technical Data<br />
Laboratory Automation Hardware<br />
Case 3 HE desktop units<br />
Basis panel UI interface (PC), power supply and indication LEDs 230V<br />
CPU HK-CPU32 card, 32 bit Embedded Controller with watchdog<br />
Extension Reserve See table<br />
Working temperature 0 to 50 °C, non-condensing<br />
Storing temperature 0 to 50 °C<br />
IP Protection Category IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory device<br />
Power consumption 30 W to 140 W<br />
Operating voltage 230 V +<strong>10</strong>/-20 %, opt. widerange <strong>10</strong>0 to 240 V.<br />
MSRbox1 MSRbox2S MSRbox2<br />
Dimensions Depth: 318 mm<br />
Width: 236 mm (1/2 19“)<br />
Height: 145 mm (3 HE)<br />
Depth: 318 mm<br />
Width: 236 mm (1/2 19“)<br />
Height: 145 mm (3 HE)<br />
Delivery Scope MSRbox device<br />
power supply cable<br />
manual<br />
cable to connect to the 9-pin RS232 interface of UI<br />
Order Code Description<br />
MG-MSRBOX1 MSRbox1 basis device to equip individually<br />
MG-MSRBOX2 MSRbox2 basis device to equip individually<br />
MG-MSRBOX2s MSRbox2s basis device to equip individually<br />
Terminal Blocks for PMC PIs<br />
For the connection of practically all existent sensors,<br />
actors, and devices to the MSRmanager and<br />
MSRboxes used in practice, you will find the suited<br />
terminal blocks in the following.<br />
Terminal blocks (universal-) analogue Input<br />
This terminal block is an<br />
extended version of the MB-<br />
AEB16V. It features an<br />
additional terminal strip for<br />
the reference voltage in<br />
order to connect the Pt<strong>10</strong>0 in<br />
four wire circuit.<br />
Thus, it is suitable for all<br />
kinds of sensors and signals.<br />
� Screw-type terminals for 16 test ports<br />
� Voltage -<strong>10</strong>...+<strong>10</strong> V, Pt<strong>10</strong>0, resistance sensor,<br />
current 0/4...20 mA,<br />
� Thermocouples<br />
� Integrated electronic compensation of cold<br />
junctions for thermocouples<br />
� Precision current source 1 mA for Pt<strong>10</strong>0<br />
� Additional terminal strip for the connection of<br />
a current source<br />
� Mounted on DIN-system rails<br />
Technical Data<br />
Depth: 318 mm<br />
Width: 342mm (3/4 19“)<br />
Height: 145 mm (3 HE)<br />
The blocks are connected to the interface card by a<br />
ribbon cable.<br />
Please indicate the desired length in your order. The<br />
default length is 180 cm. (max. 3 m).<br />
Automatic<br />
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Laboratory Automation Hardware<br />
Product description Terminal block for HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16 with 16<br />
analogue inputs and comparator for thermocouples, additional terminal strip for<br />
conductors 3 and 4 of Pt<strong>10</strong>0 in four wire circuit<br />
Dimensions Width: 112 mm<br />
Depth: 77 mm<br />
Height: 72 mm<br />
Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />
Order Code Description<br />
MB-AEB16VP Terminal block for voltage, current, Pt<strong>10</strong>0 and thermocouples<br />
Terminal Block for Voltage and Current Output<br />
This terminal block is used to<br />
control devices with analogue<br />
inputs via current or voltage.<br />
� Screw-type terminals for 8 current and<br />
voltage outputs<br />
� For 8 channels either 0/4...20 mA or -<strong>10</strong>...+<strong>10</strong><br />
V<br />
� For the connection of thermostats, stirrers,<br />
analogue actuators etc.<br />
� Integrated protection from noise voltages<br />
� Mounted on DIN-system rail<br />
Technical data<br />
Product description Terminal block for D/A-converter-card-HK-DA812UI,<br />
8 x -<strong>10</strong>..+<strong>10</strong> V voltage outputs and parallel 8 x 0/4..20 mA current outputs<br />
Dimensions Width: 67 mm<br />
Depth: 77 mm<br />
Height: 72 mm<br />
Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />
Order Code Description<br />
MB-AAB8UI Terminal block for voltage and current output<br />
Terminal Block with 8 digital Inputs<br />
This terminal block<br />
enables the connection of<br />
switches, alarm units,<br />
binary detectors, etc. to<br />
the MSRmanager. Up to 2<br />
MB-DEB8-blocks can be<br />
connected to a HK-<br />
DEA16N card by ribbon<br />
cable. The range of the<br />
input voltage is NAMUR-compliant or optional from 5<br />
to 24 V.<br />
� Eight NAMUR-consistent inputs<br />
(or optionally 5 – 24V)<br />
� Screw-type terminals<br />
� Mounted on DIN-system rails<br />
� Integrated protection from noise voltages<br />
Technical Data<br />
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Laboratory Automation Hardware<br />
Product description Terminal block for HK-DEA16x, 8 digital inputs, NAMUR compliant<br />
Dimensions Width: 67 mm<br />
Depth: 77 mm<br />
Height: 50 mm<br />
Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />
Order Code Description<br />
MB-DEB8 Terminal Block for digital Entry<br />
Terminal block with 8 Relay outputs<br />
This terminal block is the default<br />
one, since it is universally<br />
applicable and electrically most<br />
robust. The outputs are passive,<br />
i.e. they can connect external<br />
current sources.<br />
� Screw-type terminals<br />
� Switching voltage up to 40 V AC or DC<br />
� Switching current up to 2 A<br />
� 1 NO contact and 1 NC contact (passive)<br />
� For the connection of magnetic valves,<br />
drives, heaters, etc.<br />
� Mounted on DIN-system rails<br />
Technical Data<br />
Product description Terminal block for HK-DEA16x, 8 relay outputs, 1 break contact element, 1 shutter<br />
(passive), LED control (requires HS-NGS241S in addition)<br />
Dimensions Width: 112 mm<br />
Depth: 77 mm<br />
Height: 50 mm<br />
Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />
Order Code Description<br />
MB-DAB8R Terminal block digital output, 8 relay outputs<br />
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Laboratory Automation Hardware<br />
Terminal Block with 8 Transistor Outputs<br />
The transistor terminal block<br />
is equipped with transistors<br />
as emitter followers. It is<br />
operated only to control<br />
electronic devices or small<br />
consumer loads. The<br />
outputs are active. If the<br />
outputs are to be operated<br />
in active mode a 24 V power<br />
supply (HS-NGS24xx) is required.<br />
� Screw-type terminals<br />
� Switching voltage up to 24 V<br />
� Active outputs, switching current up to 0,5 A<br />
(other values are optional)<br />
� Mounted on DIN-system rails<br />
In the standard version, all 8 output channels are<br />
secured via separate (self-resetting) multifuses,<br />
max. 0,5 A.<br />
Technical Data<br />
Product description Terminal block for HK-DEA16x, 8 active emitter follower outputs,<br />
up to 24 V, 0,5 A<br />
Dimensions Width: 67 mm, Depth: 77 mm, Height: 50 mm<br />
Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />
Order Code Description<br />
MB-DAB8T_0.5A Terminal block digital output, with 8 transistor outputs<br />
Serial Interfaces<br />
For the PMC devices the same modules for serial<br />
interfaces are available as for the LabManager (see<br />
Special Terminal Blocks<br />
LabManager, serial ports).<br />
For special applications, e.g. extreme environmental<br />
conditions like splash water etc., we build special<br />
customized solutions for the terminal blocks like the<br />
shown stainless steel IP65.<br />
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Laboratory Automation Hardware<br />
Intrinsically safe inputs/ outputs (Ex-equipment)<br />
For applications, which have a high explosive risk, in<br />
zone 1 the inputs and outputs of the MSRmanager<br />
can be equipped with IS power supply and loop<br />
powered supplies. The inherently safe circuits are<br />
[EEx ib] certified. The MSRmanager can be<br />
installed outside the hazardous area if it is not<br />
encapsulated or inside the hazardous area if<br />
encapsulated with overpressure type "p" following<br />
DIN EE50016 / VDE 0170/0171 Part 3. The<br />
configuration is user-specific, if desired including<br />
certification by the TÜV. The protective chassis of<br />
the MSRmanager and the control PC is also userspecific.<br />
Product Description Upgrade for applications in hazardous areas<br />
[Eex-ib](zone 1), per I/O - interface, Eex-ia (zone 0) on application<br />
Order Code Description<br />
HE-EEXIU Intrinsic safety for voltage inputs and outputs 0..<strong>10</strong> V<br />
HE-EEXII Intrinsic safety for current inputs and outputs 0..20 mA<br />
HE-EEXID Intrinsic safety for digital inputs and outputs 20 V<br />
HE-EEXIRS232 Intrinsic safety for serial ports TxD, RxD<br />
HE-EEXIPT<strong>10</strong>0 Intrinsic safety for Pt<strong>10</strong>0 inputs<br />
HE-EEXITH Intrinsic safety for thermocouples<br />
Interface Cards<br />
Analogue/Digital-Converter Card<br />
This card contains a 24-bit analogue /digital<br />
converter with a programmable amplifier. A<br />
potential free secondary bus is provided for the<br />
connection of multiplexer cards (HK-HMUX). To an<br />
A/D card up to 15 relays or semiconductor<br />
multiplexer cards can be connected, with a total of<br />
240 analogue measuring channels.<br />
� High precision with 24 bit resolution<br />
� up to 15 multiplexers (HK-HMUX) on one A/Dconverter<br />
card (= 240 Channels)<br />
� potential free secondary bus for connecting<br />
multiplexer-cards<br />
� Potential isolation secondary bus /bus 1500 V<br />
Technical Data<br />
HK-AD20N Analogue/Digital-Converter Card<br />
Resolution 24 Bit guaranteed Resolution<br />
Measurement Range Voltage –0,125 V...+0,125 V, -1...+1 V, -<strong>10</strong>...+<strong>10</strong> V, current 0/4..20 mA,<br />
Absolute Measurement<br />
Uncertainty of one<br />
(during maintenance<br />
interval)<br />
Pt<strong>10</strong>0 -200..+600 °C, Thermocouples (NiCr-Ni) -200...+1373 °C<br />
-<strong>10</strong>...+<strong>10</strong> V: 0,05 %<br />
-1...+1 V: 0,05 %<br />
-125 mV..+125 mV: 0,05 %<br />
0/4...20 mA: 0,15 %<br />
Pt<strong>10</strong>0 -50...+300 °C: 2 °C, Resolution 0,01 °C<br />
Thermocouples (NiCr-Ni) -50...+300 °C: 2 °C, Resolution 0,1 °C<br />
Delivery Scope Analogue/Digital-Converter card<br />
Order Code Product Description<br />
HK-AD20N Analogue/Digital-Converter card with 20 bit resolution<br />
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Multiplexer Cards<br />
Laboratory Automation Hardware<br />
The <strong>HiTec</strong> multiplexer cards enable the direct<br />
connection of analogue sensors and signal sources<br />
such as thermocouples, resistive sensors, voltage or<br />
current-supplying devices, etc.. Transducers are not<br />
needed and can be saved in the budget.<br />
As alternative connection methods, different<br />
Semiconductor-Multiplexer Cards<br />
The semiconductor multiplexer card offers all<br />
properties for process operation under rough<br />
conditions. The electric strength of the used<br />
semiconductor switches is 350 V.<br />
interface panels and terminal blocks are available,<br />
which are connected via ribbon cables with the<br />
multiplexer card<br />
☞ A multiplexer card requires at least one<br />
connection module for operation.<br />
The semiconductor multiplexer cards are<br />
characterized by the following properties:<br />
� 16 potential free differential inputs for mixed<br />
connection of different analogue signals and<br />
sensors<br />
� suitable for electrically rough process operation<br />
� Potential isolation between bus and input (1500<br />
V)<br />
� Total sampling rate approx. 40 channels per<br />
second<br />
� Electronic cold junction compensation for<br />
thermocouples<br />
� Up to 15 HK-HMUX on one A/D-Converter card<br />
240 channels (please note: Limited to number of<br />
free slots!)<br />
To a semiconductor multiplexer card, a MB-AEB16xx terminal block or up to two of the following panels can<br />
be connected:<br />
Suited Connection Panels Order Code<br />
Connection panel with 4 current/voltage inputs and 4 Pt<strong>10</strong>0 inputs LP-AE4PT4P<br />
Combi-panel with 4 voltage-/current inputs with power supply and 4 Pt<strong>10</strong>0 inputs LP-AE4PT4PA<br />
Combi-panel 8 current inputs 0/4...20 mA, 8 current outputs 0/4...20 mA LP-AEAP8I<br />
Combi-panel 8 current inputs 0/4...20 mA with sensor feed,<br />
8 current Outputs 0/4...20 mA<br />
LP-AEAP8IA<br />
Combi-panel 8 voltage inputs ±<strong>10</strong> V, 8 voltage outputs ±<strong>10</strong> V LP-AEAP8U<br />
Combi-panel 8 voltage inputs ±<strong>10</strong> V with sensor feed,<br />
8 voltage outputs ±<strong>10</strong> V<br />
LP-AEAP8UA<br />
Connection panel with 8 current and voltage inputs LP-AEP8<br />
Connection panel with 8 current and voltage inputs with sensor feed LP-AEP8A<br />
Connection panel with 8 PT<strong>10</strong>0 sensors LP-PTP8<br />
Connection panel with 8 thermocouples LP-THP8<br />
Description Semiconductor-multiplexer-card, with 16 universal, potential free analogue-inputchannels<br />
and 1 mA reference current source for resistive sensors.<br />
Order Code Article Description<br />
HK-HMUX semiconductor Multiplexer Card with 16 channels<br />
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Laboratory Automation Hardware<br />
Analogue Measurement Card, 8/16 Channels<br />
This card is designed for LAB and MSRbox systems<br />
and contains a 24-Bit-analogue/digital converter with<br />
programmable amplifier. The card posses an<br />
integrated 8 or 16 channel multiplexer.<br />
Technical data<br />
Resolution: 20 Bit<br />
Measurement Range: Voltage -0.125 V...+0.125 V, -1...+1 V, -<strong>10</strong>...+<strong>10</strong> V, current 0/4...20 mA,<br />
Absolute measurement<br />
uncertainty of one<br />
(within maintenance<br />
interval):<br />
To a HK-AD20NMUX16 analogue measurement<br />
card a MB-AEB16xx or up to two of the following<br />
panels can be connected:<br />
Pt<strong>10</strong>0 -200...+ 600 °C, Thermocouples (NiCr-Ni) -200...+1373 °C<br />
-<strong>10</strong>...+<strong>10</strong> V: 0.05 %<br />
-1...+1 V: 0.05 %<br />
-125 mV..+ 125 mV: 0.05 %<br />
0/4..20 mA: 0.15 %<br />
Pt<strong>10</strong>0 -50...+300 °C: 0.2 °C, Resolution 0.01 °C<br />
Thermocouples (NiCr-Ni) -50...+3 00 °C: 2 °C, Resolution 0.1 °C<br />
To a HK-AD20NMUX8 analogue measurement card<br />
one of the following panels can be attached:<br />
Description Order Code<br />
Connection panel with 4 current/voltage inputs and 4 Pt<strong>10</strong>0 inputs LP-AE4PT4P<br />
Combi-panel with 4 voltage-/current inputs with power supply and 4 Pt<strong>10</strong>0 inputs LP-AE4PT4PA<br />
Combi-panel 8 voltage inputs -<strong>10</strong>V ... +<strong>10</strong> V, 8 voltage outputs -<strong>10</strong>V...+<strong>10</strong>V LP-AEAP8U<br />
Combi-panel 8 voltage inputs -<strong>10</strong>V ... +<strong>10</strong> V, 8 voltage outputs -<strong>10</strong>V...+<strong>10</strong>V with sensor feed LP-AEAP8UA<br />
Combi-panel 8 current inputs 0/4...20 mA, 8 current outputs 0/4...20 mA LP-AEAP8I<br />
Combi-panel 8 current inputs 0/4...20 mA with sensor feed,<br />
8 current Outputs 0/4...20 mA<br />
LP-AEAP8IA<br />
Connection panel with 8 current and voltage inputs LP-AEP8<br />
Connection panel with 8 current and voltage inputs with sensor feed LP-AEP8A<br />
Connection panel with 8 PT<strong>10</strong>0 sensors LP-PTP8<br />
Connection panel with 8 thermocouples LP-THP8<br />
Product Description Semiconductor-multiplexer card, with 16 universal, potential free analogue input<br />
channels and 1 mA reference current source for resistance feeler.<br />
Order Code Description<br />
HK-AD20NMUX8 Analogue measurement card, 8 channels, 20 Bit AD-converter<br />
HK-AD20NMUX16 Analogue measurement card, 16 channels, 20 Bit AD-converter<br />
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Laboratory Automation Hardware<br />
Precision Acquisition Card, 8 Channels Pt<strong>10</strong>0<br />
The precision measuring card HK-AD24Pxx was<br />
developed for applications with the highest demands<br />
in resolution and measuring accuracy. Due to its<br />
eight-channel specification the cost-use relation of<br />
this card is particularly favourable in applications<br />
which need several channels, e.g. reaction<br />
calorimetry.<br />
Special Properties<br />
� Highest accuracy: 24 Bit Resolution<br />
� Relative differential measurement uncertainty<br />
� ≤ ±0,001 °C in range -180 to 266 °<br />
� 8 channels are virtually simultaneously<br />
captured in < 1 s<br />
� Self calibrating<br />
� 8 channels for Pt<strong>10</strong>0<br />
Applications<br />
� High precision temperature measurement, e.g. in<br />
calorimetry<br />
� Calibration measurements with sensors<br />
� Precision voltage measurements in quality<br />
control applications<br />
Technical Data<br />
The HK-AD24Pxx-cards have a very exact converter<br />
and a precision current source for resistive sensors.<br />
On eight inputs temperatures can be monitored with<br />
highest resolution over a very large temperature<br />
range.<br />
The modern circuit design makes compensation<br />
elements unnecessary. By self calibration,<br />
temperature- and aging influences are reduced to<br />
the extremely low long-time drift value of the highprecision<br />
reference elements.<br />
The temperature sensors are connected via a<br />
connection panel with connectors according to<br />
NAMUR standard. Suitable temperature sensors in<br />
different precision classes are available upon<br />
request with calibration certificate.<br />
Sensor/signal: Pt<strong>10</strong>0 / voltage<br />
Range: -180 to +266 °C<br />
Number of channels: 8<br />
Absolute measurement ≤ ±0,01 °C (≤ ±0,03 °C) after calibration<br />
uncertainty v.E.<br />
(within maintenance<br />
period):<br />
Relative measurement ≤ ±0,001 °C (≤ ±0,003 °C)<br />
uncertainty for<br />
differential<br />
measurement:<br />
Added measuring < 1 mW with sampling / 1 s (minimal self heating of the Pt<strong>10</strong>0)<br />
power:<br />
To use this card the connection panel LP-PTPRP8 is necessary.<br />
Delivery Scope: Card with 8 Analogue-inputs for voltage and resistive sensors, manual<br />
Order Code Description<br />
HK-AD24PX8 Precision measurement card with 8 channels for Pt<strong>10</strong>0, Abs. Differential measurement<br />
uncertainty 0,01 °C<br />
HK-AD24PKAL Industry calibration certificate for HK-AD24PX8<br />
Panel<br />
Delivery Scope: Panel with holding bolts, cable for internal connection<br />
Order Code Description<br />
LP-PTPRP8 Panel for HK-AD24PX<br />
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Laboratory Automation Hardware<br />
Precision Measuring Card analogue for GraviDos Load Cell<br />
This card for strain gauges (DMS) – full bridge is<br />
suited for the connection of up to four GraviDos<br />
dosing systems, load cells, torque pickups, etc.<br />
� high precision 24 bit analogue/digital<br />
converter<br />
� integrative measurement due to the<br />
deployment of individual converters per<br />
channel<br />
� Minimisation of temperature drift due to Chop<br />
Operation<br />
Technical data<br />
Sensor/signal: DMS (strain gauge) full bridge<br />
Measurement Range:: Dependent on the measurement cell<br />
Number of Channels: 4<br />
Resolution: 24 Bit<br />
Absolute measurement<br />
uncertainty v.E.:<br />
(within maintenance period)<br />
≤ ±0,1 %<br />
Measurement Resolution: ≤ ± 0,01 %<br />
Delivery Scope: Card with manual<br />
Order Code Description<br />
HK-AD24DMS4 Plug-in card with 4 channels for strain gauge (DMS) bridges and 4 digital outputs<br />
(semiconductor)<br />
You can find suited load cells in the chapter "Process Analytics and Sensors“.<br />
To operate this card, one of the following connector panels is required:<br />
Order Code Suitable Panels<br />
LP-DMS4DA4PT Combination Panel with 4 DMS (strain gauge) inputs and 4 digital outputs (semiconductor)<br />
LP-DMSP8 Connector Panel with 8 DMS (strain gauge) inputs (at 2 cards)<br />
Remark: For MSR (process measurement and control) systems, the terminal block (AEB4DMS) is available.<br />
Analogue-Output Card, 8 Channels<br />
The digital/analogue converter card enables the<br />
output of voltages or currents for control and<br />
regulation purposes.<br />
� Potential isolation between output and bus<br />
(<strong>10</strong>00 V Isolation)<br />
� current- and voltage Outputs<br />
Technical Data<br />
Resolution 12 Bit<br />
Number of channels: 8<br />
voltage outputs -<strong>10</strong>..+<strong>10</strong> V max. 2 mA<br />
current outputs 0/4..20 mA<br />
Absolute uncertainty:<br />
(within maintenance period)<br />
≤ ±0.2 %<br />
Product Description D/A-Converter card 8 x 12 Bit, for analogue-output voltage and current.<br />
Order Code Description<br />
HK-DA812UI 8 x analogue output card 0...20 mA and –<strong>10</strong>...+<strong>10</strong> V, 12 Bit<br />
Automatic<br />
Laboratory<br />
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Reaction<br />
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Automation<br />
Software<br />
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Laboratory Automation Hardware<br />
To the HK-DA812UI analogue output card the following connection modules can be attached:<br />
Order Code Description<br />
LP-AAP8UI Panel for analogue-output, current and voltage<br />
LP-AEAP8U LabManager combi-panel 8 voltage inputs ±<strong>10</strong> V, 8 voltage outputs ±<strong>10</strong> V<br />
LP-AEAP8UA LabManager combi-panel 8 voltage inputs ±<strong>10</strong> V, 8 voltage outputs ±<strong>10</strong> V, sensor feed 24 V<br />
LP-AEAP8I LabManager combi-panel 8 current inputs 0/4...20 mA with sensor feed,<br />
8 current outputs 0/4...20 mA<br />
LP-AEAP8IA LabManager combi-panel 8 current inputs 0/4...20 mA with sensor feed,<br />
8 current outputs 0/4...20 mA<br />
MB-AAB8UI MSRmanager connection block for voltage and current output ±<strong>10</strong> V and 0/4...20 mA<br />
Digital-In/Output Card<br />
The digital-input/output card is needed, if valves,<br />
monitors etc. are to be directly switched over the<br />
MSRmanager or binary senders such as switches<br />
and limit value transmitters are to be queried. The<br />
card is inserted into the internal MSRmanager bus.<br />
The pulse-width modulated output allows quasicontinuous<br />
control of heaters, motorized control<br />
valves, etc.. Thus, there is no necessity for<br />
expensive thyristor actuators or additional control<br />
electronics.<br />
The pulse area modulation is an extended form of<br />
pulse frequency modulation (PFM), which minimises<br />
the pulse amount and consequently prevents<br />
damage to the actuator (e.g. a magnet valve).<br />
� 16 Optio-coupler outputs for Bit-, Byte-, pulse<br />
width and frequency modulated output (max. 1<br />
kHz)<br />
� Defined selectable reset status<br />
� 16 isolated digital inputs 24 V NAMURconforming<br />
� Frequency and event counting (max. 4kHz)<br />
� Inputs optionally recording/non-recording for bitand<br />
byte input (edge detection)<br />
Product Description Digital-Input/Output card with 2 x 8 inputs and 2 x 8 outputs, inputs selectable<br />
recording/non-recording, frequency and event counting, outputs selectable pulse<br />
width modulated, pulse frequency modulated, defined reset status.<br />
Order Code Description<br />
HK-DEA16N Digital-Input/Output card Standard, 16 DE, 16 DA<br />
The following connection modules can be attached:<br />
Order Code Description<br />
LP-DEP8 Digital input connection panel with 8 active 24 V input<br />
LP-DEP8A Digital input connection panel with 8 passive 24 V input and sensor feeding<br />
LP-DAP8 Digital output connection panel with 8 passive output<br />
LP-DAP8A Digital output connection panel with 8 active 24 V output<br />
LP-DAP8T Digital output connection panel with 8 active transistor outputs<br />
LP-DE4DA4P Combi-panel with 4 active digital inputs, 4 passive digital outputs<br />
LP-DE4DA4PA Combi-panel with 4 active digital inputs, 4 active digital outputs<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Serial Input/Output Card<br />
Laboratory Automation Hardware<br />
The SER8 and SER16 interface cards with 8 or 16<br />
SIO channels each, ensure optimal performance of<br />
the serial interfaces. As every channel possesses an<br />
own SIO component with character buffer, optimal<br />
performance is achieved. Up to 2 cards, therefore a<br />
maximum of 32 channels, are possible.<br />
� Independent SIO channels with FIFO memory,<br />
supports RTS/CTS-Hardware-Handshake.<br />
Requires a interface module (HD-RS2329(P)L or<br />
HD-RS485P) per used channel.<br />
� Parallel processing of all channels, which leads<br />
to reduction of delay.<br />
� Maximum transmission rate 19200 baud (per<br />
channel)<br />
� 8/16 Channels<br />
� Faster processing in comparison to serial<br />
interfaces of the CPU32<br />
Order Code Description<br />
HK-SER8ECB Serial Input/Output Card, 8 Channels<br />
HK-SER16ECB Serial Input/Output Card, 16 Channels<br />
To these cards, the following interface modules can be connected:<br />
Order Code Description<br />
HD-RS2329L RS232 Interface Module, 9-pin, with LabCom feeding<br />
HD-RS2329PL RS232 Interface Module, 9-pin, electrically insulated, with LabCom feeding<br />
HD-RS485P RS485 Interface Module , 9-pin , electrically insulated<br />
All serial interfaces can communicate with the automation unit in different manners:<br />
� default device driver für known laboratory devices<br />
� NAMUR device driver for "unknown" laboratory devices<br />
� HiText control programm<br />
Further informations can be found in the chaptor Laboratory Automation Software.<br />
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PI Additional Devices<br />
Laboratory Automation Hardware<br />
The PI-additional devices conduce to expand the<br />
functionality of the PI.<br />
Switch Box 2x230V<br />
External connection box with two single pole<br />
switched (edition -H) or two double pole (edition -R)<br />
mains sockets. Control inputs for connection to LP-<br />
DAP8T or LP-DAP8A. When controlled by a LP-<br />
DAP8 or MB-DAB8x an external power suppply is<br />
needed.<br />
The control can happen with a control voltage of up<br />
to a maximum of 24 V DC. The outputs can also be<br />
controlled pulse width or pulse frequency modulated<br />
HP-B230V16R is not suitable for switching<br />
frequencies above 1 Hertz.<br />
Technical Data<br />
Operating<br />
voltage/current<br />
2x230 V AC, sum load 16 A / 3680 VA, Edition HP-B230V16H: unipolar wiring,leak<br />
current 5 mA minimum load <strong>10</strong>0 mA; Edition HP-B230V16R: double pole<br />
switching<br />
Connection type <strong>Main</strong>s plug<br />
Control signal Max. 24 V DC<br />
Usable with Panel LP-DAP8T, LP-DAP8A, Cable, ZK-LAB-HI06-0D-XX-I-01<br />
For switching Pumps, Heater Jackets, Heater Domes...<br />
Delivery Scope Switch box with fixed mains cable 2.5 m<br />
Order Code Description<br />
HP-B230V16H Socket switch box 2 x 230 V, sums load 16 A, single-pole switched, semi-conductor switcher<br />
HP-B230V16R Socket switch box 2 x 230 V, sums load 16 A, dual-pole switched, capacity relais<br />
ZK-LAB-HI06-OD-XX-I-01 Cable for connection to LAB-PI (2 necessary)<br />
Special Construction:<br />
HP-B400V16A electrical socket switchboard three-phase switched, rated voltage 400 V, 16 A per<br />
phase. Connection type: 16A CEE connector.<br />
If used with the panel DAP8T, the panel must be Please state in the order, if this is the case.<br />
modified.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LabCom Mini Terminal<br />
Laboratory Automation Hardware<br />
LabCom is a local mini terminal for LabManager,<br />
LabBox, and MSRmanager systems. It provides<br />
access to the most important process variables right<br />
at the plant. LabCom is predominantly used, if the<br />
control PC is not in direct proximity of the plant or if it<br />
must be ensured that with a disturbance or a total<br />
failure of the control PC, most important functions for<br />
operating and monitoring remain ensured.<br />
Particularly if several LAB/PMC devices are<br />
attached to a control PC, it is recommended to equip<br />
each device with a LabCom.<br />
Properties and Functions<br />
� Local display of important process values<br />
� Free definable dialogue for operation<br />
guidance<br />
� Local input possibility for values and<br />
parameter<br />
� Local alarming by flashing LEDs and acoustic<br />
signals<br />
� Shutdown button starts shutdown program in<br />
critical situations<br />
� Watchdog circuit monitors the PI and alarms<br />
on errors<br />
LabCom is connected to a specially equipped serial<br />
interface of the Lab/PMC device and supplied with<br />
power from the same.<br />
The following structure is an example for several<br />
LAB/PMC devices (up to eight possible) mounted on<br />
an operating panel:<br />
The LCD display presents 4 x 20 characters and can<br />
be allocated with display and input fields in random<br />
order. Identifiers and number formats can be<br />
selected individually. The layout is easy and<br />
uncomplicated to create with a mask editor.<br />
The following Display Elements are designated:<br />
� Alphanumeric Text<br />
� Numeric Data Point Values<br />
� Date<br />
� Time<br />
Up to 16 different masks can be defined. A mask can<br />
be selected by using the Page-Up/ Down keys on<br />
the LabCom terminal or by assigning the mask<br />
number per program.<br />
LabCom is set up as a device component within the<br />
Lab /MSRmanager systems. This provides various<br />
logical inputs/outputs as data points which are<br />
assigned to the individual functionalities.<br />
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Technical Data<br />
Laboratory Automation Hardware<br />
Dimensions: 222 mm x <strong>10</strong>5 mm x 40 mm<br />
Housing: ABS<br />
Protection: IP64<br />
Screen: Plexiglas<br />
Control codes: ANSI<br />
Product Description LCD-Terminal for LabManager system, with 4 x 20 character display, Stop-button,<br />
Alarming function, Input keyboard, Hand held terminal (additionally HD-RS2329L<br />
needed, optional: Connection cable ZK-LAB-HI07-BS-R2-I-01)<br />
Order Code Description<br />
HP-LABCOM1 Local Hand Terminal<br />
HD-RS2329(P)L PI-RS232 Interface module with power supply for LabCom<br />
Delivery scope: Mini-Terminal with connection cable 3 m<br />
Other possibilities, e.g. Light-up display, large display or device without keyboard, on request.<br />
Watchdog Device<br />
The external watchdog device is a systemmonitoring<br />
device which is used if increased safety<br />
is necessary. It monitors a temperature, a further<br />
arbitrary sensor with a 4..20 mA signal as well as<br />
hard and software components of the automation<br />
system.<br />
If one of the adjustable limit values is exceeded, or<br />
in case of a failure of the automation system, the<br />
cut-off circuit of the system is interrupted via a<br />
potential-free switching contact and an alarm is<br />
sounded.<br />
A short circuit proof voltage for the supply of a<br />
sensor (e.g. pressure sensor) is available (12 V,<br />
max. 35 mA).<br />
The following conditions can be monitored:<br />
� Pt-<strong>10</strong>0-Element for monitoring an adjustable<br />
safety temperature within the range 0..300 °C;<br />
connection via 4-pin Lemosa socket with feeler<br />
break recognition.<br />
� 4 – 20 mA input with cable-break recognition,<br />
monitoring of an adjustable limit value in the<br />
range 4-20 mA. Connection via 6-pin Tuchel<br />
(DIN45327) plug. To this input, any sensor can be<br />
attached for monitoring any physical variable,<br />
e.g. a pressure sensor for monitoring of an<br />
adjustable maximum pressure.<br />
� Monitoring of the automation system,<br />
transmission of a binary toggle signal in 1 to 9 s<br />
intervals via the binary output to the automation<br />
system, monitoring of the response from the<br />
automation system via a binary input. Connection<br />
via 5-pin 180 ° Tuchel-plug (DIN41524).<br />
Each monitoring condition can be activated<br />
individually.<br />
If one of these events occurs, an early warning is<br />
released and a built-in piezo buzzer is sounded.<br />
Therefore, a potential-free contact is provided for the<br />
control of an external signal generator. If this early<br />
warning is not acknowledged within an adjustable<br />
time (5 s – 500 s) using the “suppress”-key, the cutoff<br />
circuit is interrupted over an open potential-free<br />
contact. With the “acknowledge”-key, the alarm can<br />
be acknowledged.<br />
Safety can be further increased by building a<br />
switched output of the PI into the cut-off circuit and<br />
the PI redundantly monitors the watchdog device as<br />
well as the same physical parameters.<br />
With the help of a key, an individual alarm condition<br />
can be simulated in order to check the electronics.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Technical Data<br />
Laboratory Automation Hardware<br />
Connections 4-pol. LEMO socket for PT-<strong>10</strong>0<br />
6-pol. DIN-socket DIN 45327 for 4-20 mA signal<br />
Switched output for signal generator<br />
Switched output for triggering the cut-off function via 4-pol. DIN-socket DIN41524<br />
Dimensions Depth: 41 mm, Width: 165 mm, Height: <strong>10</strong>3 mm<br />
Power supply 9V..12 V / 200 mA<br />
Environmental 0..45 °C, max.95 % humidity, no bedewing<br />
conditions<br />
Delivery Scope Y-connection cable for connection to a digital input and a digital output of a LAB or<br />
PMC-PI<br />
Order Code Description<br />
HP-WDOGEXT1-pa External System monitoring device<br />
ZK-X-HI05-IA-IA-O-01 Cable for 4 – 20 mA sensors with Tuchel-plug and one open end<br />
pa = PI connection: L: LAB PIs, M: PMC PIs<br />
UI-PI-Coupling<br />
The <strong>HiTec</strong> <strong>Zang</strong> PI’s can be coupled in various ways<br />
with the UI.<br />
Depending on distance or surrounding field<br />
conditions, a suitable medium can be selected.<br />
Media Specials Max. distance<br />
RS232 default 7m<br />
RS485 <strong>10</strong>0m accross simple telefon line,<br />
<strong>10</strong>00m accross rdt-cable<br />
Fibre optics shortened live expectance mit Kunststoff-LL bis ca. 20m<br />
mit Glaslichtleiter 2000m<br />
T1 accross given telephon line approx. <strong>10</strong>km<br />
COM-Server over networkk (own network segment necessary) random<br />
UI-PI Coupling via Optic Cables<br />
With unfavourable electrical conditions like strong<br />
magnetic interference fields or placing of the<br />
transmission cable outside a data communication is<br />
recommended between the PI (LAB/PMC<br />
managers or box) and the UI (system controller) via<br />
fibre-optics. For distances to 50 m a less expensive<br />
plastic light conductor can be used. For larger<br />
distances up to 2000 m an optical glass-fibre cable<br />
is necessary.<br />
The module HA-V24LINK2 is attached to the<br />
normal RS232-UI-interface of the PI.<br />
Order Code Description<br />
HA-V24LINK2 Optical modem (PC-side) for synthetic fibre with separate power supply<br />
HA-V24LINKKLI Synthetic fibre for indoors<br />
HA-V24LINKKLA Synthetic fibre for outdoors<br />
UI-PI Coupling via RS485<br />
If the distance between MSR manager and system<br />
controller is more than 7 m data communication<br />
according to the RS485 standard is recommended.<br />
With the help of the option RS485, distances up to<br />
2000 m can be bridged.<br />
Order Code Description<br />
HA-RS485 Level-converter RS485<br />
The level converter is attached to a normal RS232<br />
interface and can be used on both the UI and on the<br />
PI side.<br />
Alternatively, a RS485 interface can be built into the<br />
PI in place of the RS232-UI-interface. Likewise, a<br />
RS485 interface card can be built into the UI. In this<br />
case the level converters are omitted.<br />
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Laboratory Automation Hardware<br />
UI-PI Coupling via LAN<br />
With the help of a COM-Server, <strong>HiTec</strong> PIs<br />
(LAB/PMC manager or box) can be connected via<br />
Ethernet LAN with the UI (system controller).<br />
Order Code Description<br />
HA-COMSERV<strong>10</strong>01 Com-Server Twisted-Pair or Coax <strong>10</strong>0 Mbit on RS232<br />
UI-PI Coupling via Leased Line<br />
With the help of a special leased-line modem <strong>HiTec</strong><br />
PIs (LAB/MSRmanager or Box) can be connected<br />
Order Code Description<br />
HA-MODEM4 Leased line modem pair for 4 wire connection<br />
DC power supply<br />
A 24 V DC power supply is needed for running the<br />
connection block and interface panels or for feeding<br />
other devices, e.g. sensors and actuators.<br />
Power units are needed for the connection blocks<br />
MB-DAB8R, MB-DAB8T DAB8T and for activating<br />
the panels LP-AEP8A, LP-DAP8A, LP-AEAP8IA,<br />
LP-AEAP8UA, LP-DE4DA4PA.<br />
Some of the devices have smoothed, and some<br />
stabilised outputs.<br />
It should be clarified with the responsible network<br />
administrators, whether the network can handle the<br />
additional load, or whether an own net segment<br />
must be established.<br />
using a 4-core telecom line. The maximum distance<br />
amounts to <strong>10</strong>,000 m.<br />
Power supply 24 V, 0,7 A regulated<br />
Technical Data<br />
Product description 24 V DC Power supply on connection block, stabilised,<br />
0.7 A continuous load, 1A 70 % ED duty cycle for DIN-System rail mounting,<br />
For usage with MSRmanager or switchboard mounting<br />
Environmental 0..45 °C, max. 95 % humidity, non condensing<br />
conditions<br />
Dimensions Depth: 112 mm, Width: 77 mm, Height: 64 mm<br />
Order Code Description<br />
HS-NGS241S Power supply 24 V, 0.7 A regulated, top-hat rail fitting<br />
Power supply 24 V, 7,5 A regulated<br />
Technical Data<br />
Product Description 24 V power supply on, stabilized, 7.5 A.<br />
Possible fitting into LabManager2<br />
Dimensions Depth: 220 mm, Width: 170 mm, Height: 120 mm<br />
Order Code Description<br />
HS-NGS248S Power supply 24 V, 7.5 A, regulated<br />
Power supply 24 V, 1.5 A<br />
Technical Data<br />
Product description 24 V power supply on, stabilized, 1.5 A for DIN system rail fitting.<br />
Possible fitting into LabManager1/2, LabBox2, MSRbox 2, MSRmanager.<br />
Dimensions Depth: 1<strong>10</strong> mm, Width: 55 mm, Height: 75 mm<br />
Order Code Description<br />
HS-NGS241A Power supply 24 V, 1.5 A, smoothed, system rail fitting<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
Power supply 24 V, 2.5 A<br />
Technical Data<br />
Product Description 24 V power supply, smoothed, 2.5 A, for DIN-system rail fitting. Possible fitting into<br />
LabBox1, MSRbox 1.<br />
Dimensions Depth: 1<strong>10</strong> mm, Width: 55 mm, Height: 75 mm<br />
Order Code Description<br />
HS-NGS242 Power supply 24 V, 2.5 A, smoothed, system rail fitting<br />
Power supply 24 V, 3 A<br />
Technical Data<br />
Product description 24 V power supply, smoothed, 3 A, DIN-system rail fitting.<br />
Possible fitting into LabManager1 a. 2, LabBox2, MSRbox 2, MSRmanager.<br />
Dimensions Depth: 1<strong>10</strong> mm, Width:<strong>10</strong>0 mm, Height: 75 mm<br />
Order Code Description<br />
HS-NGS243 Power supply 24 V, 3 A, smoothed, system rail fitting<br />
Power supply 24 V, 8 A<br />
Technical Data<br />
Product Description 24 V power supply, smoothed, 8 A.<br />
Possible fitting into LabManager2<br />
Dimensions Depth: 200 mm, Width: 170 mm, Height: <strong>10</strong>5 mm<br />
Order Code Description<br />
HS-NGS248 Power supply 24 V, 8 A, smoothed<br />
Power supply 24 V, 8 A extern<br />
Technical Data<br />
Product description 24 V power supply, smoothed, 8 A, for external use<br />
Connection cable for external use<br />
Suitable to active LabManager interfaces or USTAT.<br />
Dimensions Depth: 200 mm<br />
Width: 170 mm<br />
Height: <strong>10</strong>5 mm<br />
Order Code Description<br />
HS-NGS248E Power supply 24V , 8 A, smoothed, external use<br />
Power supply 15 V, 2.8 A<br />
Technical Data<br />
Product description 15 V power supply, controlled, 2.8 A.<br />
switching power supply for DIN-system rail fitting.<br />
Possible fitting into LabManager1/2, LabBox2, MSRbox 2, MSRmanager.<br />
Dimensions Depth: 1<strong>10</strong> mm, Width: 55 mm, Height: 75 mm<br />
Order Code Description<br />
HS-NGS153SN Power supply 15 V, 2.8 A, controlled, switching power supply, System Rail Fitting<br />
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Simulation Devices<br />
Pt<strong>10</strong>0 Simulator<br />
Laboratory Automation Hardware<br />
With this simulator, the user can check the<br />
measuring accuracy and function of the Pt<strong>10</strong>0 and<br />
voltage measuring inputs. Temperatures of 0, 30,<br />
<strong>10</strong>0, and 300 °C can be simulated. Additionally there<br />
is a variable adjustment possibility. The tolerance of<br />
the reference resistances is 0,02 %.<br />
Order Code Description<br />
HX-SIMPT1 Pt<strong>10</strong>0 Simulator<br />
Further simulation and test control units can be found in „Training and Education Modules“.<br />
Digital Signal Converter<br />
The <strong>HiTec</strong> <strong>Zang</strong> digital signal converters convert<br />
analogue and digital signals into RS232 or RS485<br />
ModBus protocols. They can be deployed, if the<br />
number of measuring channels is so low that the<br />
deployment of a Lab-PNC is not cost-effective.<br />
They are also suited as interfaces for small<br />
HiBuilder projects, e.g. as a supplement to LabDos<br />
or AutoSam in case additional signals need to be<br />
collected or additional actors require to be activated.<br />
Module Overview<br />
In LabManager/LabVision projects, they can be<br />
deployed on a supplementary basis, if the sampling<br />
rate of the internal interfaces is not sufficient to, e.g.,<br />
register a rapid pressure rise.<br />
� Power Supply via Interface Cable or Plug-In<br />
Power Supply 24V<br />
� RS232 and RS485 ModBus Interface<br />
� Compact Metal Casing<br />
Technical Data:<br />
Interface RS232 V24 and RS485, ModBus<br />
Protocol, Power Supply 24V via<br />
RJ48.<br />
If operated on an interface without<br />
power supply, a plug-in power<br />
supply is required.<br />
Dimensions L approx. 142 mm, W approx. 52<br />
mm, H approx. 23 mm, with Plug<br />
Connection Description Plug Order Code<br />
Current and -<strong>10</strong>...<strong>10</strong>V, 0/4..20mA, 24bit ADU, Measuring 6-pole Jack, DIN 45322 IL-AINAMP1D<br />
Voltage ON Uncertainty 0,1%<br />
Pt<strong>10</strong>0<br />
Measuring Range -200..+600 °C, Four Wire Lemo Type 1S, 4-pole IL-PTAMP1D<br />
Temperature<br />
Sensor<br />
Technology<br />
DMS-Bridge Digital DMS Amplifier for DMS Half and Full-<br />
Bridges<br />
Lemo Type 1S, 6-pole IL-GRADOAMP1D<br />
Current and<br />
Voltage OFF<br />
0...<strong>10</strong>V, 0/4..20mA, Uncertainty 0,1% 6 pole Jack, DIN 45322 IL-PHAMP1D<br />
pH-Probe, pH 0...14, Temperature with Pt<strong>10</strong>0, VarioPin -Device Socket IL-CLARKAMP1D<br />
Temperature integrated Temperature Compensation<br />
O2, Clark Probe O2-Messverstärker VarioPin -Device Socket IL-AOUT1D<br />
Digital ON Binary, Frequency and Event Counting, 24V 3-pole Jack, DIN 41524 IL-DIN1D<br />
Digital OF Binary, pulse width modulated, pulse<br />
frequency modulated, active (24V) or<br />
passive<br />
3-pole Plug, DIN 41524 IL-DOUT1D<br />
Delivery Scope Amplifier, Manual, (Please order cable separately)<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Hardware<br />
Order Code Description<br />
IL-AINAMP1D Digital Measuring Amplifier for -<strong>10</strong>...+<strong>10</strong>V, 0/4...20mA, RS232 V24 /RS485 Interface<br />
IL-PTAMP1D Digital Measuring Amplifier for Pt<strong>10</strong>0 Four Wire Technology, RS232 V24 /RS485 Interface<br />
IL-GRADOAMP1D Digital Measuring Amplifier for DMS Load Cells, RS232 V24 /RS485 Interface<br />
IL-PHAMP1D Digital Measuring Amplifier for pH- und Redox-Electrodes, RS232 V24 /RS485 Interface<br />
IL-CLARKAMP1D Digital Measuring Amplifier for Clark O2-Electrodes, RS232 V24 /RS485 Interface<br />
IL-AOUT1D Analogue Output for -<strong>10</strong>...+<strong>10</strong>V, 0/4...20mA, RS232 V24 /RS485 Interface<br />
IL-DIN1D Digital Converter for 24V Binary, Frequency and Event Counting. RS232 V24 /RS485 Interface<br />
IL-DOUT1D Digital Output passive and active 24V, RS232 V24 /RS485 Interface<br />
ZK-MV-BS-R4-I-01 RS485 Cable for Digital Measuring Amplifier with 24V Power Supply via Pin 1<br />
IL-MV1D-SN Plug-In Power Supply for Digital Measuring Amplifier<br />
Display and Operating Elements<br />
A display and operation component (OC) for a <strong>HiTec</strong><br />
<strong>Zang</strong> System consists of a special PC with Windows<br />
XP or Windows Vista operating system and<br />
LabVision-UI software.<br />
The OC, as a component of an automation system,<br />
must meet special requirements:<br />
� Uninterupted Power Supply (UPS) with Shut<br />
Down Interface<br />
� LabVision compatible UPS Management<br />
� EMV-robust<br />
� Run-In System Test<br />
These requirements are not met by normal office<br />
PCs. <strong>HiTec</strong> OCs are devices with adjusted and<br />
proven hardware. The devices are tested with ready<br />
to use, already installed software in the complete<br />
system before dispatch.<br />
The OC software LabVision is based on a database<br />
system, which increases the hardware requirements.<br />
As the database and the operating system could be<br />
damaged in case of a current failure, a <strong>HiTec</strong> OC is<br />
principally equipped with an uninterrupted power<br />
supply system and a UPS Management System.<br />
During a current failure, the system runs buffered by<br />
storage batteries. Before the storage battery<br />
capacity is used up, the system is shut down in a<br />
defined manner.<br />
The normal equipment version comprises a<br />
Standard UPS. This must not be deeply discharged,<br />
as may happen if the whole plant is switched off via<br />
a main switch. Should the UPS be separated from<br />
the net, this must be done in charged condition at<br />
the operator panel. If this can not be ensured, the<br />
Online UPS CP-USV7O should be used, which is<br />
equipped with a deep discharge protection.<br />
PC-Hardware is subject to extremely fast innovation.<br />
According to this fact, <strong>HiTec</strong> <strong>Zang</strong> occasionally<br />
adapts the models to the state of technology. For<br />
this reason, it does not really make sense to present<br />
the current devices, which will soon be out of date.<br />
We rather offer a selection of two devices: The<br />
standard version with standard equipment and<br />
performance according to the current state of the<br />
technology and a device with upscale equipment<br />
and performance. Details in regard to the current<br />
equipment are gladly forwarded upon request.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 135<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
136<br />
Casing Design<br />
Laboratory Automation Hardware<br />
Our display and operation components are available<br />
in four differently designed casings.<br />
For useunder rough conditions, it is advisable to use<br />
the industrial PC with protected drives and the<br />
option to be installed in 19 inch system cabinets.<br />
The standard casing is the midi tower.<br />
Desktop Microcube Midi tower 19 Inch Industrial PC<br />
Depth: 375 mm<br />
Width: 415 mm<br />
Height: 165 mm<br />
Products similar to photos!<br />
<strong>HiTec</strong>-ABK1<br />
Depth: 335 mm<br />
Width: 2<strong>10</strong> mm<br />
Height: 269 mm<br />
The <strong>HiTec</strong> ABK1 is used for applications of small<br />
and medium size, e.g. in connection with a LabBoxor<br />
LabManager1 PI.<br />
The basic configuration can be upgraded with the<br />
offered options such as the DVD burner etc..<br />
You have the choice between four different casing<br />
designs. By default, the device is delivered as midi<br />
tower.<br />
Depth: 500 mm<br />
Width: 2<strong>10</strong> mm<br />
Height: 380 mm<br />
Basic Equipment*:<br />
Depth: 500 mm<br />
Width: 482,6 mm (19“)<br />
Height: 177 mm (4 HE)<br />
� Single-Core processor<br />
� at least 2 GB RAM<br />
� fast SATA hard disk (> 250GB)<br />
� DVD/CD Drive<br />
� Sound card<br />
� UPS and UPS Management Software<br />
� Windows-Keyboard and Wheel-Mouse<br />
� Windows XP© or Windows Vista© preinstalled<br />
*As of 3/<strong>2009</strong>. The equipment is consistently aligned to the<br />
proven state of the technology.<br />
Order Code Description<br />
CG-ABK1C <strong>HiTec</strong> Display and Operating Component in Micro Cube Casing, with UPS System<br />
CG-ABK1M <strong>HiTec</strong> Display and Operating Component in Midi Tower Casing, with UPS System<br />
CG-ABK1D <strong>HiTec</strong> Display and Operating Component in Desktop Casing,with UPS System<br />
CG-ABK1I <strong>HiTec</strong> Display and Operating Component in 19inch industrial Casing, with UPS System<br />
CP-USV7O Upgrading: Online UPS System 700 VA, secured against deep discharge, incl. software<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
<strong>HiTec</strong>-ABK2<br />
Laboratory Automation Hardware<br />
The <strong>HiTec</strong> ABK2 is used for medium and greater<br />
applications, e.g. in connection with a LabManager2<br />
PI or several PIs with a multitude of LabVision<br />
entities.<br />
You have the choice between four different casing<br />
designs. By default, the device is delivered as midi<br />
tower.<br />
For increased data protection, the ABK2 can be<br />
equipped with a RAID System.<br />
Basic Equipment*:<br />
� Dual-Core processor<br />
� at least 4096 MB RAM<br />
� fast SATA hard disk (> 500GB)<br />
� DVD/CD Recorder<br />
� Sound card<br />
� UPS and UPS Management Software<br />
� Windows-Keyboard and Wheel-Mouse<br />
� Windows XP© or Windows Vista© preinstalled<br />
*As of 3/<strong>2009</strong>. The equipment is consistently aligned to the<br />
proven state of the technology.<br />
The ABK2 enables the connection of a second<br />
monitor. With this, it is for example possible to<br />
assign the manual operation level and the recipe<br />
control each to an own monitor.<br />
Order Code Description<br />
CG-ABK2C <strong>HiTec</strong> Display and Operating Component in Micro Cube Casing, with UPS System<br />
CG-ABK2M <strong>HiTec</strong> Display and Operating Component in Midi Tower Casing, with UPS System<br />
CG-ABK2D <strong>HiTec</strong> Display and Operating Component in Desktop Casing,with UPS System<br />
CG-ABK2I <strong>HiTec</strong> Display and Operating Component in 19 inch industrial Casing, with UPS System<br />
CK-RAID1 Mirrored Disc RAID 1 (with intelligent Controller Card)<br />
For supplementary components, see "UI Additional Components“, for suited monitors, see "Monitors“.<br />
Expansions<br />
Order Code Description<br />
CK-RAM2x512 Memory Expansion by 1 Gigabyte DDR2-RAM for <strong>HiTec</strong> AKB<br />
(additional 2 x 512 MB Brand-RAM for Dual-Channel Technology)<br />
CK-RAM2x<strong>10</strong>24 Memory Expansion by 2 Gigabyte DDR2-RAM for <strong>HiTec</strong> AKB<br />
(additional 2 x 1 Gigabyte Brand-RAM for Dual-Channel Technology)<br />
CK-RAM2x2048 Memory Expansion by 4 Gigabyte DDR2-RAM für <strong>HiTec</strong> AKB<br />
(additional 2 x 2 Gigabyte Brand-RAM for Dual-Channel Technology )<br />
P-USV7O Upgrading: Online UPS System 700 VA, secured against deep discharge, incl. Software<br />
Ex Industrial PC<br />
This computer is suited for direct use in areas with a<br />
risk of explosions. Equipped with stainless steel<br />
casing for PC and monitor with plastic foil keyboard.<br />
Further information upon request.<br />
Order Code Description<br />
CG-ABKEX <strong>HiTec</strong> Display and Operating Component in Explosion Protective Casing, with UPS System<br />
CZ-EXMAUS Wireless mouse for operation in explosive areas<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 137<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
138<br />
Fileserver<br />
Laboratory Automation Hardware<br />
We offer fileservers with Windows and Linux<br />
operating systems. Please request for our current<br />
models and specifications.<br />
UPS Power Supply Standard<br />
If the control system is intended to keep running in<br />
case of a power failure, an uninterrupted power<br />
supply (UPS) must be provided for the fileserver,<br />
ABKs, PIs, and, where required, for the most<br />
important devices of the primary instrumenting.<br />
To ensure controlled shutdown of the computer in<br />
case of electrical power outage, a UPS management<br />
system is required in addition.<br />
The Standard UPS may not be deeply discharged as<br />
this may occur if the plant is completely shut down<br />
via a main switch. If the UPS is intended to be<br />
disconnected from the net for a longer period, it<br />
must be shut down at the operator panel. If this can<br />
not be ensured, it is advisable to use the online<br />
UPS CP-USV7O.<br />
� Monitoring Output for UI<br />
� Power Output 700 VA<br />
� Maximum Bridging Period approx. 15 min.<br />
Upon request, we are also able to deliver online<br />
UPS with greater performance, e.g. with <strong>10</strong>00 or<br />
2000 VA.<br />
Order Code Description<br />
CP-USV7 UPS System supply 700 VA for <strong>HiTec</strong> display and operating components including software<br />
Note: CP-USV7 is already included in the delivery scope of all <strong>HiTec</strong> <strong>Zang</strong> work stations.<br />
UPS Power Supply Online<br />
Online UPS constantly provides equal voltage<br />
quality and is secured against deep discharge.<br />
It is intended for usage in cases where, after a<br />
power failure longer than the maximum bridging<br />
operation period, the shutdown of the UPS cannot<br />
be ensured.<br />
� Secured against deep discharge<br />
� Sinus voltage<br />
� Controlled voltage<br />
� Monitoring Output for UI<br />
� Power Output 700 VA<br />
� Maximum Bridging Period approx. 15 min.<br />
Upon request, we are also able to deliver online<br />
UPS with greater performance, e.g. with <strong>10</strong>00 or<br />
2000 VA.<br />
Order Code Description<br />
CP-USV7O Online UPS System 700VA, secured against deep discharge, including software<br />
Monitors<br />
Our monitors all meet the requirements of the current ergonomics regulations.<br />
Industrial Monitor<br />
The metal casing contains a 19 inch TFT Monitor<br />
and protects the same under rough conditions. It is<br />
prepared for the installation into a 19 inch control<br />
cabinet. If intended to install it free-standing or as<br />
part of a transportable system, it is recommended to<br />
install it in a plastic casing with handles (CZ-<br />
KTRAG).<br />
Technical Data<br />
Dimensions Depth: 116 mm, Width: 483 mm, Height: 399 mm<br />
Order Code Description<br />
CP-INMON Industrial monitor for mounting in control cabinet<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Standard Monitors<br />
17 Inch TFT Monitor<br />
� Resolution 1280 x <strong>10</strong>24 pixels<br />
� Low Radiation according to TCO03<br />
� 36 months warranty by manufacturer<br />
Laboratory Automation Hardware<br />
Order Code Description<br />
CP-M17TFT 17 Inch TFT Colour Monitor<br />
19 Inch TFT Monitor<br />
� Resolution up to 1280 x <strong>10</strong>24 pixels<br />
� Low Radiation according to TCO03<br />
� 36 months warranty by manufacturer<br />
Order Code Description<br />
CP-M190TFT 19 Inch TFT Colour-Monitor<br />
20 Inch Widescreen TFT Monitor<br />
� Resolution up to 1680 x <strong>10</strong>50 pixels<br />
� Low Radiation according to TCO03<br />
� 36 months warranty by manufacturer<br />
� Refresh Rate: 60 Hz<br />
� Adjustable height<br />
� with Swivel Base<br />
� Refresh Rate: 60 Hz<br />
� Adjustable height<br />
� with Swivel Base<br />
� Refresh Rate: 60 Hz<br />
� Adjustable height<br />
� with Swivel Base<br />
This monitor is as high as a normal 17 inch monitor but has a greater width. It is therefore easier to arrange<br />
windows, e.g. the recipe control and the analogue pen recorder, next to each other. This is also beneficial for<br />
operator ergonomics. In many cases, this is a real alternative to a second monitor.<br />
Order Code Description<br />
CP-M20TFTWS 20 Inch Widescreen TFT Monitor<br />
22 Inch Widescreen TFT Color Monitor<br />
� Resolution up to 1680 x <strong>10</strong>50 pixels<br />
� Low Radiation according to TCO03<br />
� 36 months warranty by manufacturer<br />
� Refresh Rate: 60 Hz<br />
� Adjustable height<br />
� with Swivel Base<br />
This monitor is as high as a normal 19 inch monitor but has a greater width. It is therefore easier to arrange<br />
windows, e.g. the recipe control and the analogue pen recorder, next to each other. This is also beneficial for<br />
operator ergonomics. In many cases, this is a real alternative to a second monitor.<br />
Order Code Description<br />
CP-M22TFTWS 22 Inch Widescreen TFT Monitor<br />
(Other models upon request!)<br />
Serial Interfaces for the Operating Components (OC)<br />
The following serial interfaces serve both for the<br />
connection of several PIs to one UI and for the<br />
connection of devices.<br />
The interfaces can be addressed via a HiText<br />
Program or with <strong>HiTec</strong> UI device drivers.<br />
Order Code Description<br />
CS-RS2322-PCI PCI Plug-in card for <strong>HiTec</strong> <strong>Zang</strong> Ocs (operating components) with 2 RS 232 interfaces<br />
Plug&Play, only 1 IRQ per card (interrupt sharing). Max. 921 kbps<br />
CS-RS2324-PCI PCI Plug-in card for <strong>HiTec</strong> <strong>Zang</strong> Ocs (operating components) with 4 RS 232 interfaces<br />
Plug&Play, only 1 IRQ per card (interrupt sharing) Max. 921 kbps<br />
CS-RS4852-PCI PCI Plug-in card for <strong>HiTec</strong> <strong>Zang</strong> Ocs (operating components) with 2 RS-422/485 interfaces<br />
Optically isolated isolated, Plug&Play, only 1 IRQ per card (interrupt sharing). Max. 921 kbps<br />
CS-RS4854-PCI PCI Plug-in card for <strong>HiTec</strong> <strong>Zang</strong> Ocs (operating components) with 4 RS-422/485 interfaces<br />
Optically isolated, Plug&Play, only 1 IRQ per card (interrupt sharing).<br />
Max. 921 kbps<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 139<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
140<br />
Periphery<br />
Laboratory Automation Hardware<br />
The following peripheral devices have been tested<br />
on <strong>HiTec</strong>h operating components (OC) and are<br />
supported by LabVision.<br />
Barcode Scanner<br />
The extremely high-performance, compact, handheld<br />
scanner is ideal for utilisation in the laboratory<br />
sector. The device offers quick and precise scanning<br />
with or without contact and can be easily configured<br />
for application in the <strong>HiTec</strong>-<strong>Zang</strong> OCs.<br />
The device is compatible with LabVision.<br />
Order Code Description<br />
CP-BCS232 Hand-held Barcode Scanner, RS232 connection to OC with driver and manual<br />
Printer<br />
The following printers are suited as standard PC-,<br />
protocol-, document- and pen recorder printers. Only<br />
robust and proven devices by acclaimed<br />
manufacturers are offered. The scope of delivery<br />
includes cables and manuals.<br />
Order Code Description<br />
CP-DRUHPDJC Hewlett Packard Colour Ink Jet Printer A4, Colour, with single feed feeder, with single sheet<br />
feeder, for printing of flow charts, screenshots, etc.<br />
CP-DRUHPLJ Hewlett Packard Black/White Laser Printer A4<br />
CP-DRUHPLJC Hewlett Packard Colour Laser Printer A4<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Here you will find:<br />
Laboratory Automation Software<br />
Laboratory Automation Software<br />
� LabVision® Software for Laboratory Automation<br />
� LabVision® Project Module<br />
� EasyBatch TM Table based Recipe Control<br />
� HiBatch TM Basis Operation based Recipe Control and Administration<br />
� Basis Operation Library for HiBatch TM<br />
� HiLIMS TM Laboratory Information Management System<br />
� PI-Firmware Modules, Regulator Modules, programmable logic controller (PLC)<br />
� HiBuilder TM Data Evaluation and Presentation<br />
� RI-CAD TM Uncomplicated Drawing of piping and instrumentation diagram (P&ID)<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 141<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
142<br />
LabVision®<br />
Advantages<br />
Laboratory Automation Software<br />
Maximum Automation, with Minimum Engineering<br />
LabVision is a modular visualisation and automation<br />
software system for automation devices from <strong>HiTec</strong><br />
<strong>Zang</strong> as well as other providers. Your system is<br />
presented on the display for monitoring and<br />
operating. Your process is monitored, controlled, and<br />
regulated, all processes are logged and archived.<br />
The process plant is presented on the monitor as a<br />
dynamic flow diagram for monitoring and operating.<br />
The online evaluation already delivers important<br />
information regarding the process during runtime.<br />
The process data chain reaches from the definition<br />
of the experiment right to the Laboratory Information<br />
Management System.<br />
Various advantages<br />
� Complete documentation of all process<br />
events<br />
� Intensive use of your resources<br />
� Consistent presentation of values, events and<br />
phases<br />
� Relief from routine tasks<br />
� Savings on Instrumentation thanks to virtual<br />
devices<br />
� Realisation of a consistent data process<br />
chain from the work order to the Laboratory<br />
Information Management System<br />
LabVision is one of the most efficient and<br />
outstanding modern process visualisation tools.<br />
Within the area of research process control systems<br />
(RPCS) it has an outstanding position. The System<br />
is particularly suited for visualising and automating<br />
continuous and batch processes in laboratories, pilot<br />
plants, mini-plants, and production in chemistry,<br />
pharmacy, bio and food technology. Due to its<br />
flexibility it can be used also in other areas such as<br />
waste management, solar and environmental<br />
technology.<br />
Its special strength is its flexible application<br />
range. LabVision fulfills the requirements of the<br />
NAMUR working group - AK 2,4 for research<br />
process control systems and is hereby ready for<br />
frequently changing or modified tasks.<br />
LabVision can be used on different complexity<br />
levels. If you want to use LabVision merely as a<br />
user, one day of instruction is usually sufficient to get<br />
acquainted with the handling.<br />
Even if you wish to establish automation projects for<br />
changing assemblies yourself, you can learn this<br />
within one day.<br />
This is enabled by the Project Module Library, which<br />
contains predefined project modules for all important<br />
basic functions such as tempering, dosing, pH or<br />
vacuum regulation, distilling etc..<br />
Specialists who wish to learn the complete range of<br />
possibilities of parameterisation and programming,<br />
merely require one week for familiarisation instead<br />
of the several months of schooling usually required<br />
for conventional process control systems.<br />
Features that convince:<br />
� Easy to use, minimum learning effort<br />
� As RPCS according to NAMUR standards online<br />
configurable and parameterised.<br />
� Project modules for fast and easy application<br />
development<br />
� Histo-Database for consistent storage of values,<br />
text, and events.<br />
� Support of the basic operations concept for batch<br />
processes (NAMUR NE 33)<br />
� Support of GLP and TQM by resource<br />
administration and automatic documentation<br />
� Scalable from small measurement acquisition<br />
systems up to networked process control<br />
systems with shared online-databases<br />
� English language version available, other<br />
languages upon request<br />
� Personalised user interface<br />
LabVision increases your efficiency, by relieving you<br />
from routine activities. Processes driven once can<br />
be repeated at any time, even after years, with<br />
optimum reproducibility, because all steps are made<br />
at the correct point in time, all materials are added<br />
and adjusted automatically and correctly. Parameters<br />
are set automatically to the correct value.<br />
The securing of the reproducibility and the optimal<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
documentation of all parameters, values and events<br />
contribute to an improvement in quality.<br />
The user interface has the following properties:<br />
� Operation to XP- and Vista-Standard<br />
� Logically object orientated and context sensitive<br />
� Self explanatory operating symbols with dynamic<br />
hint windows<br />
� Personalised (desktop can be stored and reloaded)<br />
� Protection from unauthorised access (own user<br />
administration)<br />
� Remotely controllable via network & modem<br />
User Requirements<br />
LabVision can be used on different levels of<br />
complexity and detail and requires appropriate levels<br />
of knowledge from the user (see also training course<br />
offer).<br />
1. Operation by shift personnel<br />
Operating and monitoring the current system by<br />
shift changing personnel requires a briefing of<br />
approx. half a day.<br />
2. Operation by personnel with minimum<br />
training<br />
With a training course of approx. two days, the<br />
service personnel is in the position to<br />
parameterise pre-fabricated applications for<br />
starting and operation. With the help of the basic<br />
operations library for batch running, also the<br />
minimum trained user is in a position to create,<br />
parameterise, and operate a complex recipe<br />
operational sequences with smallest time<br />
expenditure.<br />
3. Project engineering and operation by well<br />
trained personnel<br />
Well trained users (approx. one week) can<br />
address and use substantial details of the<br />
system according to his/her request with this<br />
easy to handle system. The user is able to<br />
independently create display and control<br />
screens, as well as control programs and online<br />
analyses of any complexity.<br />
4. Projects using well trained automation<br />
specialists<br />
The well trained automation engineering<br />
specialist (at least one week) can use functions<br />
of this completely open system in detail. Display<br />
and control screens can be created as well as<br />
control programs and online analyses of any<br />
complexity. Also the possibilities of the process<br />
interface (PI) for increased safety standards e.g.<br />
by use of the PLC Functionality of the LAB/MSR<br />
manager can be used.<br />
Libraries<br />
Libraries prearranged to the usual application cases<br />
support the user to save time and costs when<br />
establishing the project (see Laboratory Automation<br />
Software, SL-GOPBIB, SL-MODBIBALR, SL-<br />
BIBRILK and EN/ISO <strong>10</strong>628).<br />
Data Objects<br />
The following types of data points ( = data objects)<br />
are supported:<br />
� Input<br />
� Output<br />
� Variable<br />
� Text<br />
� Monitoring<br />
� Device Components<br />
Data points can be used for values and for parameters.<br />
Thus it is for example simply possible to<br />
change controller parameters dynamically with the<br />
program.<br />
Data points can be defined and administered on the<br />
different automation units (LAB/MSR Manager and<br />
display and control units (UI)).<br />
For each data point defaults for the diagram scaling<br />
and the format of numeric displays can be made.<br />
These defaults are taken over by the visualisation<br />
objects.<br />
Device components provide higher functionalities in<br />
the PI, e.g.:<br />
� application oriented controller<br />
� Integrators<br />
� Differentiators<br />
� Programmers<br />
� Device Communication etc.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 143<br />
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Laboratory Automation Software<br />
All data objects are administrated in the onlinedatabase.<br />
Particular features of the online-database<br />
are:<br />
� Fastest known access mechanism at present<br />
� High throughput<br />
� Multi - Client / multi - server principle,<br />
expandable by further clients and servers<br />
Values, events, and text objects are stored in the<br />
history data base. For data reduction, only values<br />
which changed significantly are stored. This delta-x,<br />
delta-t procedure reduces the stored quantity of data<br />
to a minimum.<br />
Safety<br />
LabVision puts a special emphasis on safety. The<br />
Application Manager constantly checks all modules<br />
and alarms in case of a module failure, whereby the<br />
remaining general system remains stable.<br />
Numeric and other non-critical errors cause only<br />
error messages and can be treated by programming<br />
and do not obstruct the further operational sequence.<br />
HiText programs with formula errors cannot<br />
be started at all.<br />
LabVision protects, to a large extent, your parameterisation<br />
from errors when configuring and from<br />
faulty operation and incorrect input during the runtime.<br />
This is guaranteed, amongst others, by the<br />
bottom-up technique during the application establishment,<br />
the extensive use of prefabricated objects,<br />
as well as the examination of the input values.<br />
The access control with user administration prevents<br />
unintentional and unauthorised interventions.<br />
During a power failure, the system is shut down after<br />
completion of an emergency operation phase.<br />
The resource administration guarantees that during<br />
the definition of new data points, only available, i.e.<br />
existing, not already assigned interfaces are used.<br />
Deleting of a process becomes effective only after<br />
acknowledgement of at least one safety query.<br />
PI control programs are stored safely from<br />
interferences in the non volatile FLASH-memory.<br />
Even the value history can be buffered in the PI, in<br />
order to bridge brief failures of the UI (e.g. during<br />
maintenance and servicing), and to ensure a<br />
continuous documentation of the experiment/test<br />
data. The data is entered automatically with the reavailability<br />
of the UI.<br />
Special Features<br />
LabVision varies from conventional PLS in essential<br />
points. Especially significant in this regard are the<br />
relation to the capacity of the system, simple<br />
handling and transparency.<br />
Online Changeability<br />
One important feature is the capability of LabVision<br />
for online-configuration and online-parameterisation.<br />
It does not differentiate between construction phase<br />
and runtime. This means for you that, for example in<br />
case of an unplanned necessary intervention into<br />
the process or in the event of a malfunction, you do<br />
not need to shut down and reactivate your plant.<br />
This is the reason for the special suitability as FPLS<br />
for F & E applications in the laboratory or pilot plant<br />
stations. Conventional systems do not dispose of<br />
this ability. It is however indispensable for flexible<br />
and efficient operation in the laboratory or pilot plant<br />
stations.<br />
Visual Configuration Ability<br />
The visual configuration of interfaces of a LAB-<br />
Manager PNC is especially simple and comfortable.<br />
You are able to select the interface type, e.g. Pt <strong>10</strong>0,<br />
in a display of the available connection panel of your<br />
individually equipped LAB-Manager with the list<br />
selection field. The respectively suited free plug-in<br />
connections are marked. The programme proposes<br />
the first free plug-in connection via a blinking<br />
marking. You must now simply select the same or<br />
any other free connection by clicking on to it.<br />
The current and the historic values of the connected<br />
sensor are immediately available for visualisation<br />
and further processing.<br />
Even the connection of any random laboratory or<br />
analysis devices via serial interfaces can be realised<br />
in a simple way with the freely parameterisable<br />
NAMUR device component.<br />
The only data required to be entered into the entry<br />
mask are the interface parameters contained in the<br />
respective device manual.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Module Overview<br />
Laboratory Automation Software<br />
LabLision is modularly structured. The LabVision<br />
basis module SL-CLABVIS can be equipped with the<br />
depicted modules.<br />
The basis module is equipped with 30 data points.<br />
The number of data points can be adjusted to the<br />
project size accordingly. The progression is 30, <strong>10</strong>0,<br />
180, 300, 560, <strong>10</strong>00, 3000 and <strong>10</strong>000 data points.<br />
Modules and data points can be upgraded at any<br />
time. This is conducted after clearance via the<br />
download from our website server or by forwarding a<br />
data carrier.<br />
Modules as Full Versions<br />
A LabVision license contains the free update<br />
authorisation for one year. Software versions<br />
adjusted to the respective client system can be<br />
requested via download from our website server. As<br />
soon as you are entered in our E-mail list, you will<br />
automatically be informed of available new software<br />
updates for your system.<br />
The base module can be extended using the<br />
following modules in full and light-Versions:<br />
Order Code Option / Function<br />
SL-HITEXT HiText- Multi-tasking Control and Online-Evaluation<br />
SL-EASYBATCH Table based Recipe control module<br />
SL-HIBATCH Recipe control module with graphical recipe process-editor<br />
SL-ACTIONTRACK ActinnTracker to record user activaties as EasyBatch program<br />
SL-REZGEN Recipe series generator<br />
SL-DIAPROT Dialog and Protocol forms with tables incl. graphics<br />
SL-ONLGRA Full version online charts with reference curve presentation, MDI-capable<br />
SL-SCHANA Full version analogue plotter, MDI-capable<br />
SL-SCHERE Event plotter<br />
SL-SCHPHA Phase plotter<br />
SL-BERICHT Full version process report, batch orientated<br />
SL-UEBMEL Full version monitoring and reporting<br />
SL-LABCAM LabCam, Digital Camera module, event controlled digital-photo documentation<br />
SL-DESIGN Worksheet designer<br />
SL-RIEDIT P&ID-Editor according to EN/ISO <strong>10</strong>628<br />
SL-EXPORT Full version automatic data export and externally controlled<br />
SL-SELFIL Selectors and Filters<br />
SL-BENRECH Access monitoring with user administration<br />
SL-JOURNAL Parameterisable electronic laboratory notebook<br />
SL-MULTIBATCH HiBatch extension for parallel synthesis<br />
SL-MULTIPROJ Multiple starting of LabVision on one computer<br />
SL-LABVOICE Voice output for messages, alarms and HiText modules<br />
SL-EMLRUF Alarm call via e-mail (also suitable for text messages)<br />
SL-ALRRUF Alarm call via telephone call with voice message<br />
SL-PROJMOD Project modules generator and editor for LabVision<br />
SL-KALDAS3 KalDas 3.0<br />
SL-ANWINT Programmable interface for Visual-Basic, C++ or DELPHI<br />
SL-CLONLV Cloning tools for LabVision (parallel reactor system)<br />
SL-SWITCHER Administration of different versions of LabVision on one PC<br />
SL-HILIMS Laboratory information management system with local SQL Database<br />
SL-HILIMSSQL HiLIMS multi user server software without SQL server licence<br />
SL-PNKSIM Emulator for <strong>HiTec</strong> Pis (incl. HiSim)<br />
SL-WEBVIS Remote maintenance of active LabVision projects via TCP/IP<br />
Automatic<br />
Laboratory<br />
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Reaction<br />
Calorimetry<br />
Fermentation<br />
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Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 145<br />
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Module as Light-Version<br />
Laboratory Automation Software<br />
Different modules are also available as a lightversion.Different<br />
modules are also available as a<br />
light-version. The Light versions are dimensioned so<br />
that they are sufficient in most cases. Modules in the<br />
full version and light version can be combined.<br />
Order Code Option / Function<br />
SL-HITEXTL HiText light, 4 Programs each <strong>10</strong>0 lines<br />
SL-HIBATCHL Recipe Control-Module light with max. 20 steps<br />
SL-ONLGRAL Online charts light, 2 diagram pages each 8 curves<br />
SL-SCHANAL Analogue Plotter light with 2 plot pages each 8 curves<br />
SL-SCHEREL Event Plotter light (without hints)<br />
SL-SCHPHAL Phase Plotter light (max. 3 phases)<br />
SL-DESIGNL Designer light, one worksheet with max. 400 Visualisation-Objects<br />
SL-RIEDITL P&ID-Editor light, one worksheet with max. 120 Visualisation-Objects<br />
SL-WEBVISL WebVision light, only multi plotter visualisation<br />
SL-HILIMSL Single-User HiLIMS licence with local SQL database (max. 4 GB)<br />
LAB/MSRmanager PI-Module<br />
Order Code Option / Function<br />
SF-PIDxx xx = 4, 8, 16, 24, 32, or 64 PID controller or application oriented device components<br />
SF-HICONx x = 1, 2 ,4 or 8 fully adaptive controller<br />
SF-NAMSERxx NAMUR driver for xx = 4, 8, 16, 32, 64 or 128 serial interfaces<br />
SF-AWL Instruction List EN 61131 PLC Module , including Programming Desktop<br />
SF-AWLPLUS Extended Instruction List Module with structured Text in HiText-orinted Syntax<br />
SF-HITUNE Automatic parameterisation for PID controllers<br />
SF-ANWTAB User defined linearisation table<br />
SF-DATLOG Data Logger Function, Data Buffering in the PI in case of UI Failure<br />
SF-PNKMSR Serveral PI’s at one computer<br />
External PI Drivers<br />
Order Code Option / Function<br />
SL-PNKPERF PI-Driver for Braun Perfusor<br />
SL-PNKSPS PI-Driver for Siemens S5/S7, 3964(R) protocol and AEG Modicon<br />
SL-PNKLASENTEC PI-Driver for Lasentec FBRM - particle systems<br />
SL-PNKMTRx PI-Driver for Metrohm titrators (x = 1, 2, 4, 8 Devices)<br />
SL-FREMDPNK LabVision access module for solely foreign-PI systems (with Dongle)<br />
SL-PNKOPC PI-Diver for OPC-DA (Version 1+2), OPC-Client<br />
SL-PNKDDE PI-Driver for DDE data exchange<br />
SL-PNKMBUSSER PI-Driver for ModBus devices over serial PC interface<br />
Further PI drivers e.g. ProfiBUS- and CANBUS-systems are available upon request.<br />
Miscellaneous<br />
Order Code Option / Function<br />
SL-TELES Remote maintenance<br />
Libraries<br />
Order Code Option / Function<br />
SL-GOPBIB Basis Operation Library<br />
SL-MICROBIB Base for Ehrfeld Library (Microbib Content)<br />
SL-MODBIBALR Project Module Library for Designer, Full Version<br />
SL-BIBRILK Glass and Laboratory Devices Library for P&ID-Editor<br />
Notice: Software which is allocated to products, like KalDas is to Reaction Calorimetry, can be found in the<br />
according chapters of the respective products.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
The LabVision Base Module<br />
Laboratory Automation Software<br />
The LabVision base module is the minimum software<br />
configuration of the LabVision program system.<br />
It is sufficient for systems with small application statistics<br />
and a small degree of automation. It can be<br />
equipped with the upgrade modules in full or light<br />
versions. The number of data points can be extended.<br />
This is conducted after clearance via the download<br />
from our website server or by forwarding a data<br />
carrier. A LabVision license has a one year's free<br />
update authorisation.<br />
A minimum or demo version of some of the modules<br />
can be found in the base module. The base module<br />
is equipped with 30 data points and contains the<br />
functions:<br />
Order Code Option / Function<br />
SL-LABVIS LabVision base module with 30 data points<br />
System Requirements<br />
LabVision demands the following minimum<br />
requirements from the UI:<br />
� Single-Core CPU<br />
� 1 GB RAM (Vista),<br />
� 1 GB free hard drive space<br />
� Windows-Vista or Windows-XP<br />
� 2 button mouse<br />
� 1 x serial port or USB2Serial connector<br />
� Configuring and Parameterising<br />
� Monitoring and reporting of alarms, without<br />
reactions and long text messages 3 predefined<br />
message classes<br />
� Designer limited to one worksheet and 30<br />
visualisation objects<br />
� P&ID-Editor limited to 50 graphic objects<br />
� Online charts limited to 8 curves, one page<br />
� Analogue plotter limited to 8 curves and one<br />
axis<br />
� Progress report basic features<br />
� HiText limited to one program and 30 lines<br />
� Device components for <strong>HiTec</strong> PIs<br />
� Demo project module samples<br />
� Data export in text or table files, limited to<br />
manual start<br />
� System in German and/or English<br />
LabVision is tested exclusively on <strong>HiTec</strong> <strong>Zang</strong> UI.<br />
Perfect function is not guaranteed on other machines.<br />
Absolute necessary safe shutting down of the<br />
data base in the case of power failure can only be<br />
guaranteed with <strong>HiTec</strong> <strong>Zang</strong> UIs and UPSs.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
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Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 147<br />
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Stirring and<br />
Dispersing<br />
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The Multi-Plotter System<br />
Laboratory Automation Software<br />
The multi-plotter is an innovative, integrated plotting<br />
system. It displays, clarity and consistency not seen<br />
until now, current and historical process conditions in<br />
the form of values (analogue plotters), events (event<br />
plotters) and process phases (phase plotters).<br />
The diagram can be printed out directly, or can be<br />
inserted into documents using the clipboard.<br />
The presented period can be changed manually,<br />
over a worksheet or a HiText program.<br />
The presented values can be directly exported to<br />
spreadsheet programs.<br />
The Analogue Plotter<br />
The analogue plotter presents the analogue values<br />
as curves. It can plot up to forty pages with 8 curves<br />
on up to 8 axes each. The representation can be<br />
randomly spread and zoomed.<br />
When reading off values, you are supported by<br />
the read-off cursor in the form of a vertical line.<br />
With a mouse-click you set the position which will be<br />
read off. The values can be read directly at the<br />
cursor or in the allocated table column below the<br />
diagram window.<br />
With the delta-t trend cursor, you set the trend<br />
display interval. In the column Value Table Trend<br />
you can directly read off the trend for each curve.<br />
The analysis cursor supports you during graphic<br />
analysis with min, max, average and gradient etc..<br />
Significant curve sections can be highlighted with a<br />
text comment after clicking on to them.<br />
The plotter can be configured online, i.e. you can<br />
create new curves and modify all settings at any<br />
time. The curves can optionally also be displayed,<br />
either linear or logarithmically, un-smoothed or<br />
smoothed.<br />
Time domains of interest can be retrieved in many<br />
ways. In connection with the export module, the<br />
presented pen recorder page can be passed for<br />
numeric value export to the export module (e.g. via<br />
Excel) with a mouse click.<br />
Order Code Description<br />
SL-SCHANA Analogue plotter (MDI), 40 pages with each 8 curves<br />
SL-SCHANAL Analogue plotter light, 1 window limited to 2 plotting pages with each 8 curves<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
The Event Plotter<br />
Laboratory Automation Software<br />
The event plotter provides a symbolic explanation of<br />
monitored events, messages, comments etc. Each<br />
occurring event is displayed with its own symbol.<br />
If the mouse cursor is moved over an event symbol, a<br />
popup will appear that will display all important<br />
information to the event.<br />
If you click on an event symbol, the progress report is<br />
opened and the appropriate plain text message with<br />
source note is displayed.<br />
Order Code Description<br />
SL-SCHERE Event plotter with clear text indication window and additional option<br />
SL-SCHEREL Event plotter light, no hint-function (no clear text indication window)<br />
The Phase Plotter<br />
The phase plotter provides a visualisation of the<br />
temporal operational sequence, e.g. the process<br />
phases or the sequence of recipe steps.<br />
It enables the direct allocation of the value curves<br />
and events to the phases (defined in plain text).<br />
Order Code Description<br />
SL-SCHPHA Phase Plotter<br />
SL-SCHPHAL Phase Plotter light, limited to 3 parallel phases<br />
The Progress Report<br />
If the mouse cursor is directed at a phase bar, a<br />
popup will appear that contains information to the<br />
event. Per mouseclick on to a phase bar, the<br />
according period in the process record will be<br />
opened.<br />
Order Code Description<br />
SL-BERICHT Progress Report, batch orientated extended search possibility<br />
In the progress report all events, values or parameters<br />
are recorded, the presentation of which as a<br />
curve would not be useful or not possible. These<br />
include comments from the operator, process messages<br />
and monitoring reports including their respective<br />
text information, pictures, and LabCam Videos.<br />
With the help of the many filter possibilities, you can<br />
also select the respective interesting information fast<br />
and safely even out of many thousands of entries.<br />
Where required, the progress report also delivers<br />
the batch protocol.<br />
The report can also be printed or exported to<br />
EXCEL.<br />
Note: The basic program only contains a progress<br />
report with simple search, export and filter<br />
possibilities.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
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Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 149<br />
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The Online Chart<br />
Laboratory Automation Software<br />
The online charts represent xt-diagrams. In contrast<br />
to the analogue plotters, the curves are drawn<br />
in the diagram on the left-hand side. The time axis<br />
can be marked alternatively with absolute time or<br />
relative to the start time, i.e. beginning with zero.<br />
An insertable read-off cursor supports easy<br />
reading off of the values.<br />
For online or offline comparisons, historical values<br />
or calculated values can be inserted as curves.<br />
For online and offline comparison, it is possible to<br />
blend in the historic values or calculated setpoints<br />
as curves. These reference curves can be preset<br />
out of recorded LabVision data values or Excel<br />
data files.<br />
Current Value<br />
Set Points<br />
The graphics can be printed out directly or be<br />
pasted into documents from the clip board.<br />
Additionally, the event and phase plotters can be<br />
viewed. The diagrams can be marked with a title.<br />
A memo can also be inserted for additional<br />
information.<br />
The starting time, representation period, heading<br />
and additional text as well as phase texts can be<br />
set manually or by a HiText program.<br />
The online charts module offers 40 pages with<br />
respectively up to eight curves.<br />
Respectively one axis can be placed on the right or<br />
left side of the diagram.<br />
Order Code Description<br />
SL-ONLGRA Full version Online charts with reference curve presentation, MDI-capable<br />
SL-ONLGRAL Online charts light, limited to 2 diagrams each of 8 curves, no reference curves<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Display and Control Graphics<br />
Laboratory Automation Software<br />
Your system can be driven completely from the<br />
display and control pictures in manual operation.<br />
Therefore external display and control elements<br />
are unnecessary.<br />
Even operators not educated in detail with the<br />
system are immediately able to find the significant<br />
elements and can arrange the displayed values<br />
directly.<br />
Due to the clear presentation, the operation is to a<br />
large extent self-explanatory. The operating<br />
possibilities can be limited user specifically.<br />
Therefore, also lesser qualified shift personnel can<br />
be made familiar with the operation with little time<br />
expenditure.<br />
The design scope is virtually limitless. The functionality<br />
is extraordinarily versatile: e.g. each of the<br />
display and control objects explains itself with a<br />
freely generateable text message, if the mouse<br />
cursor moves over the object.<br />
Even the control philosophy can be set. You have<br />
the choice between control objects, which can be<br />
operated directly, e.g. by clicking on to them with<br />
the mouse, or control objects, which must first be<br />
opened by clicking a (hand) symbol, to exclude<br />
inadvertent operation.<br />
Critical values can additionally be provided with an<br />
acknowledgement window. By depositing user<br />
definable RTF-formatted text and diagrams via<br />
popups, complex operating instructions or maintenance<br />
instructions can be blended in as an<br />
additional help next to the operating and display<br />
elements.<br />
The Designer<br />
The designer is your tool for setting display and<br />
control views (process pictures), protocol forms,<br />
operating panels for devices etc..<br />
In addition you do not need any special know-how<br />
or programming knowledge. Larger plant pictures<br />
can be distributed on several sides.<br />
In order to make your plant flow sheet "dynamic"<br />
you only need to draw the desired display and<br />
control objects on the worksheet and link with the<br />
appropriate data points. In the library provided you<br />
find everything from the trip switch to the pointer<br />
instrument. The visualisation objects indicate not<br />
only the value of the connected data point, but<br />
visualise also limiting and warning value violations<br />
by flashing symbols.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 151<br />
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Stirring and<br />
Dispersing<br />
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Laboratory Automation Software<br />
Data point names and physical units are<br />
automatically blended in and the settings of the<br />
display range etc. are automatically assigned from<br />
the associated data points.<br />
Also, complex dialogue elements like e.g. forms for<br />
inputting experimental parameters with save and<br />
load functions or with a symbol, minimizable<br />
control panels can be simply created without any<br />
programming.<br />
A freely expandable library of pre-defined display<br />
and control panels is included in the delivery.<br />
In connection with prefabricated project modules<br />
(see project modules), you gain immediately<br />
deployable visualisation objects which are already<br />
linked with the according inputs/outputs and<br />
component devices. Complete sub-projects,<br />
respectively plant basis operations can be set up<br />
and visualised in this manner with one mouse click.<br />
The used control and display components are<br />
constantly advanced and are updated to the<br />
current windows technology.<br />
In addition to the standard display and control<br />
objects, the Designer offers complex elements, like<br />
e.g.<br />
� registers for organising and grouping of<br />
extensive visualisations<br />
� panels for saving and loading of all values in a<br />
group of elements<br />
� dynamic assignment of screen position<br />
� dynamic blending in/out of visualisation objects<br />
You can create your own reusable combined<br />
visualisation objects and add them to the library.<br />
With application oriented device components<br />
typical automation specific basic functions and<br />
basic unit operatoins will be realises. The are e.g<br />
� Dosing<br />
� Vacuuum control and<br />
� reactor inside temperature control<br />
Thus a dosing circuit will be realised with a dosing<br />
device component, a balance and a pump<br />
connected to a LabManager. Instead of a balance<br />
a GraviDos weighing cell and instead of a pump a<br />
valve can be used.<br />
Up to now this functionality could only be<br />
established using a PID-controller with a programm<br />
or a ramping device component. This demanded<br />
instrumental and control knowledge to realise and<br />
parameterise the controller.<br />
The application oriented dosing device<br />
components on the other hand contain the<br />
complete controlling functionality including an<br />
option to refill receiver tank without interrupting the<br />
dosing. The parameterisation of the controller and<br />
therefore the biggest and most time consuming<br />
problem in general is completely omitted. The<br />
project modules are based on these application<br />
oriented device components.<br />
Further information can be found under PI-<br />
Firmware-Modules.<br />
Order Code Description<br />
SL-DESIGN Designer<br />
SL-DESIGNL Designer light, limited to 1 worksheet with 400 visualisation objects<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LabVision ® Project Modules<br />
Laboratory Automation Software<br />
Establishment of Automation Projects in Record Time!<br />
The LabVision Project Module Technology marks a<br />
new generation of automation software of yet unknown<br />
user-friendliness and functionality.<br />
Project modules enable the visual establishment of<br />
projects with preconditioned, ready to function modules<br />
per Drag and Drop Technology. This means<br />
that a project is established by moving the required<br />
modules of the needed functionalities out of a<br />
browser window on to the work sheet.<br />
Project modules are combined out of different<br />
LabVision objects, e.g.:<br />
� Data Points<br />
� Device Components<br />
� Operating Objects<br />
� Visualisation Objects<br />
� Monitoring Objects<br />
� HiText Programmes<br />
� Pen Recorders etc.<br />
Completed project modules of the most common<br />
configurations are available as a library. These<br />
merely require to be adjusted to the hardware<br />
equipment in the course of importing. This significantly<br />
shortens the development period for<br />
projects.<br />
Examples:<br />
Reactor Rectification Column<br />
Dosing Module Tempering Unit<br />
Stirring Drive Stirrer Blade<br />
Distillate Weighing Vacuum Control<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 153<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
154<br />
Laboratory Automation Software<br />
Due to a library administration of the generated<br />
project modules, it is possible to easily secure and<br />
transmit various work statuses of a module in a<br />
compressed data file analogue to LabVision Project<br />
Administration.<br />
A gravimetric dosing module, for example, consists<br />
of a dosing regulator, the data points for the scales,<br />
pump and cut-off valve, the respective monitoring<br />
and the graphic display and operating objects. In<br />
comparison to conventional work procedures, the<br />
project establishment time shrinks from a few days<br />
to a few, which is especially effective in case of<br />
frequently changing assemblies to a point where the<br />
expenditure in time and effort can be neglected.<br />
Even users with limited automation experience can<br />
securely establish a demanding automation project.<br />
The project modules bring along the required<br />
process measurement and control functions and<br />
visualisation elements. This means that the data<br />
points, for the inputs and outputs, the control<br />
components, the user interface etc, are<br />
automatically applied and can be immediately<br />
deployed.<br />
An Example:<br />
A 1 litre plant with a stirred reactor, a gravimetric<br />
dosing, vacuum control, rectification and distillate<br />
weighing is intended for automation.<br />
The required modules are merely pulled over from<br />
the browser window on to the work sheet.<br />
A display for operating and monitoring combined out<br />
of the project modules then looks as follows:<br />
After the parameters of the regulator modules, for<br />
temperature, dosing and vacuum have been set with<br />
the help of the automatic parameterisation function,<br />
the plant can already be run via the operating display<br />
in flow chart presentation.<br />
The performance of the project module is illustrated<br />
in the following example. The projected screen has<br />
been created in under <strong>10</strong> minutes.<br />
The ALR (Automatic Laboratory Reactor) Project<br />
Module Library contains all required modules for the<br />
automation project establishment of a flexible<br />
laboratory reactor system:<br />
� Temperature Regulation cascade with<br />
Thermostat<br />
� Gravimetric or volumetric Dosing<br />
� Solid Dosing<br />
� Vacuum Regulation<br />
� pH Regulation<br />
� Distillation<br />
� Rectification<br />
� Crystallisation<br />
� Hydration<br />
� Phase Separation<br />
� Sample collector<br />
� Stirring etc.<br />
A project established on the basis of a project<br />
module library is HiBatch compatible. This means<br />
that it can be used as a basis for the recipe control<br />
system and the basis operation library.<br />
Already deployed modules are marked in colour in<br />
the project module browser of the library.<br />
The modules can be shared, so that e.g. an<br />
expansion by further dosing circuits can be easily<br />
realised.<br />
The data points for the connection of the required<br />
scales, pumps, and valves are applied automatically.<br />
The technical documentation can be established<br />
automatically by the push of a button.<br />
The context menus of the individual modules, which<br />
can be reached by pressing the mouse on the right<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
side, contain a graphic display of the connection<br />
panels of the LabManager, which then displays on to<br />
which plug-in positions the required instrumenting<br />
components, such as scales, stirrer drive,<br />
thermostat, valves etc. need to be connected.<br />
The user interface is extremely functional. By<br />
clicking on to the hand symbols of the operating<br />
objects the parameterising dialogues are opened.<br />
This prevents that unintended operation actions are<br />
triggered unintentional mouse clicks.<br />
As the project modules are based on the standard<br />
design objects, they can be randomly arranged or<br />
Projectmodule Libraries:<br />
extended/upgraded by the user. The module library<br />
is aligned to <strong>HiTec</strong> <strong>Zang</strong> instruments and laboratory<br />
devices, but can also easily be adapted to other<br />
components.<br />
►<br />
Projecting could not be easier!<br />
Order Code Description<br />
SL-MODBIBALR ALR-Project Module Library for Designer, Full Version.<br />
All project modules of the light library and additionally<br />
- Stirring misc. actuators (Output of a setpoint rm to a stirrer and torque display)<br />
- volumetric dosing with analogue controlled pump<br />
- gravimetric surge dosing with GraviDos (Demands: amount)<br />
- gravimetric amount dosing with GraviDos (Demands: amount, time)<br />
- gravimetric flow rate dosing with GraviDos (Demands: dosing rate, time)<br />
- gravimetric conti dosing with GraviDos (Vorgabe: dosing rate)<br />
- Destillation (Destillation with jacket temperature control)<br />
- Rectification (multilevel destillative seperation)<br />
- Christalisation<br />
- Gasing with MFC<br />
- Flow rate counter/Integrator for gas meter and flow through sensor<br />
- Calotrend (simple online Flow-calorimetry)<br />
- Titration<br />
- Filling<br />
SL-MODBIBALRL ALR-Project Module Library light for Designer<br />
- pumping with LabDos and SyrDos<br />
- pH_control (pH-value-control for base and/or acid dosing)<br />
- Inerting (establish inerte atmosphere by continued vacuumation / inerting)<br />
- volumetric dosing with LabDos a. SyrDos<br />
- gravimetric surge dosing with GraviDos (Demands: amount)<br />
- gravimetric amount dosing with GraviDos (Demands: amount, time)<br />
- gravimetric flow rate dosing with GraviDos (Demands: dosing rate, time)<br />
- gravimetric conti dosing with GraviDos (Vorgabe: dosing rate)<br />
- temperature control with thermostat and temperature cascade controller<br />
- SoliDos (Solid dosing with SoliDos)<br />
- Stirring with ViscoPakt (Output of a setpoint to a stirrer and torque display)<br />
- Inerting (Inlet of intergas)<br />
- Vacuum control<br />
- Reflux destillation<br />
- Automatic phase seperation with PhaSep<br />
- Automatic sample taking and filling with AutoSam and LabDos or SyrDos<br />
Order Code Description<br />
SL-PROJMOD Project Module Generator (Generation of Project Modules)<br />
SL-MODBIBALR ALR-Project Module Library for Designer, Full Version.<br />
SL-MODBIBALRL ALR-Project Module Library light for Designer with Dosing, Tempering, Stirring, Vacuum<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 155<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
156<br />
P&ID-Editor<br />
Laboratory Automation Software<br />
The P&ID-Editor Software Module for LabVision<br />
(modulename RI-Editor) is mainly identical with the<br />
stand-alone Version RiCAD. In LabVision, it is possible<br />
to dynamise the piping and instrumentation<br />
diagram (P&ID) with the Designer, this means provide<br />
the same with display and operating elements,<br />
and use them as user interfaces.<br />
The P&ID-Editor (linked in to the Designer) was<br />
specially developed for drawing control flow sheets<br />
according to the EN ISO <strong>10</strong>628 standard. It serves<br />
for the creation of the static background images of<br />
display and control diagrams.<br />
In the tool palette you will find all the necessary<br />
drawing tools.<br />
This tool can also be expediently put to use during<br />
the planning stage for „standard conforming“<br />
drawing of the plant.<br />
The library elements contain additional information,<br />
which can be freely expanded by e.g. suppliers or<br />
with maintenance information.<br />
Universities and other educational institutions may<br />
request a free RI-CAD version including library!<br />
Order Code Description<br />
SL-RIEDIT Piping and instrumentation diagram (P&ID) Editor<br />
SL-RIEDITL Piping and instrumentation diagram (P&ID) Editor Iight, limited to one worksheet with max.<br />
120 graphic objects<br />
Laboratory Components Library<br />
The library SL-BIBRILK for the P&ID-Editor contains<br />
presentations of the components in a laboratory<br />
reactor system which are more detailed and more<br />
realistic than in the EN ISO <strong>10</strong>628 library for the<br />
P&ID-Editor.<br />
Here you will find the glass reactors in varying<br />
constructions and sizes and glass devices like reflux<br />
separators, coolers, containers etc. also other lab<br />
devices in a descriptive form.<br />
Order Code Description<br />
SL-BIBRILK Glass and lab devices library for P&ID-Editor<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Monitoring and Reporting<br />
Laboratory Automation Software<br />
In the register monitoring/reporting you are able to<br />
define your monitoring conditions and different<br />
reporting options.<br />
If one of the specified monitoring conditions is<br />
fulfilled, this is entered in the monitoring report<br />
(extended alarm journal) and in the progress report,<br />
as is the going and the acknowledging of the<br />
monitored event.<br />
Extended Monitoring and Reporting Module<br />
Complex plants require sophisticated, flexible alarm<br />
strategies. For this reason the extended alarm<br />
module was developed. In this way, various reactions<br />
to limit and warning value violations can be<br />
established by the user.<br />
As monitoring conditions, beyond the usual static<br />
comparisons of limit and warning values, dynamic<br />
comparisons between data points or fault conditions,<br />
e.g. conductor breakage, can be set.<br />
Both the message and the confirmation are recorded.<br />
In case of important alarms a horn, for example,<br />
can be switched on or a control program can be<br />
started for the selective processing of the incident.<br />
Certain notifications of emergency can alternatively<br />
be shown delayed.<br />
Order Code Description<br />
SL-UEBMEL Extended monitoring and reporting module<br />
In the message report, the danger and warning<br />
messages are listed and acknowledged, if necessary.<br />
In the lower table window, the current messages are<br />
always indicated. The upper table is for acknowledging.<br />
As needed, it can be filtered and scrolled,<br />
in order to show previous messages outside of the<br />
represented range.<br />
Projectable message categories make it possible to<br />
establish the message behaviour of the categories<br />
centrally<br />
� Danger report<br />
� Warning report<br />
� Operation report<br />
and optionally user-defined message categories.<br />
The standard version is part of the LabVision Basic<br />
Module.<br />
For a better overview, the user can have the notifications<br />
of emergencies sorted, e.g. according to the<br />
message time.<br />
Alarms and messages, as well as acknowledgement<br />
requiring and non-acknowledgement requiring<br />
messages are differentiated.<br />
� User defined report categories<br />
� Long text reports<br />
� Complex alarm handling by control program<br />
As an addition for this module, telephone, fax, and<br />
E-mail are available.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 157<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
158<br />
Multi-LabCam System<br />
Laboratory Automation Software<br />
Certain process conditions and events can be best<br />
documented photographically. Examples are collections<br />
of turbidity, colour change, precipitation, etc..<br />
The modern server system architecture permits the<br />
integration of several different image sources<br />
(LabCams, Videostreams etc.) which can be<br />
provided by the own PC or by completely different<br />
computers.<br />
The LabCam module offers the possibility to document<br />
visual procedures automatically event-controlled<br />
or in programmed intervals and by manual triggering<br />
as digital pictures or videos. The digital pictures<br />
are inserted reduced in size into the progress<br />
report.<br />
A photo in full size or the recorded video is displayed<br />
by clicking with the mouse. The current live images<br />
can be integrated in work sheets and are also available<br />
in WebVision Modules for remote diagnostics<br />
without restriction.<br />
The image files are freely available for further use.<br />
� Documentation of visual statuses and events<br />
� Monitoring of the system from the office<br />
� Visual remote monitoring<br />
Cameras with a higher resolution are available upon<br />
request. Individual cameras (only photo function,<br />
without video recording function, as well as without<br />
programmable image trigger or WebVision support)<br />
can also be connected directly to the LabVision<br />
computer without the auxiliary module depicted<br />
above.<br />
A Multi-LabCam generates completely new<br />
possibilities!<br />
Order Code Description<br />
SL-LABCAM LabCam, Digital-Camera Module, event controlled digital-photo and video documentation<br />
CP-DIGICAM1 Digital-Camera, resolution 640 x 480 points, color<br />
CP-DIGICAM2 Digital-Camera, resolution <strong>10</strong>24 x 768 points, color<br />
Telephone-Alarm Call<br />
With the help of the telephone alarm call module,<br />
telephone calls can be triggered automatically with<br />
defined events. Event-dependent, one or several<br />
texts can be announced. In addition, the announcement<br />
of current measured values is possible.<br />
A library of letters, numbers and standard words are<br />
included. Optionally, further words and complete<br />
sentences can be added customer-specifically.<br />
In a control program, one or more telephone<br />
numbers can be called as a reaction to a certain<br />
event e.g. staff on call during plant disturbance or<br />
the service personnel after completion of batch can<br />
be called and the appropriate message announced<br />
in plain language.<br />
Order Code Description<br />
SL-ALRRUF Telephone alarm call with speech output<br />
Furthermore, it is possible, depending on date and<br />
time, to activate different call numbers, so that an<br />
on-call service can be arranged in advance even<br />
over several days. If unexpected deviations arise,<br />
e.g. as a result of illness, the settings can also be<br />
changed by remote maintenance.<br />
The confirmation of the received call is entered in to<br />
the progress report by key code.<br />
☞ Required is the option SL-HITEXT(L)<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
E-mail Alarm<br />
Laboratory Automation Software<br />
E-mail messages, as prepared event-dependent<br />
texts, can be sent to different e-mail addresses and<br />
forwarded to you mobile phone as text message<br />
Order Code Description<br />
SL-EMLRUF Alarm Call by E-mail<br />
Control and Online-Evaluation<br />
In the field of control and online evaluation,<br />
LabVision is a class of its own. Available are the<br />
graphical recipe procedure control EasyBatch and<br />
HiBatch, the plain text language HiText, Instruction<br />
List according to EN 61131, and AWLplus with<br />
structured text in HiText-oriented syntax (see PI-<br />
Firmware Modules) and the device components (see<br />
LabManager-System, System Construction). This<br />
offer considers the realisation, that depending upon<br />
your problem definition, each programming type<br />
disposes of its special specific suitability.<br />
HiText The Universal Text Language<br />
HiText is a plain text language for control, onlineevaluation<br />
and communication. HiText was developed<br />
in cooperation with users from the chemical<br />
industry with the aim to achieve a self explanatory<br />
and self-documenting language, useful for everyone.<br />
As also users with no programming experience are<br />
able to learn HiText in a short time, the language<br />
enjoys highest acceptance, in particular for the<br />
applications in laboratories and pilot stations.<br />
The module contains a comfortable editor with many<br />
helpful functions, a multitasking capable interpreter<br />
and a process visualisation tool with debugging<br />
assistant.<br />
The syntax check takes place direct during the input.<br />
by the control program as a reaction to certain<br />
incidents.<br />
☞<br />
Required is the option SL-HITEXT(L) and an<br />
internet access.<br />
Programming of Algorithms<br />
Algorithms are best programmed in HiText with<br />
English key words. Example: Calculations,<br />
programmed relationships (If..., then...).<br />
In the German version, German language elements<br />
are used instead.<br />
Programming Processes/Recipes<br />
Processes/Recipes can be programmed in text form<br />
in HiText, table based in EasyBatch or graphically as<br />
HiBatch sequences to NAMUR and EN/IEC<br />
standards.<br />
Errors are underlined and are clearly marked. Only<br />
formal error free programs can be started.<br />
For the calculation of mathematical expressions<br />
there are, apart from the basic functions, all<br />
important mathematical functions available. Setpoint<br />
value specifications for controllers can be created<br />
with random progression (Profile).<br />
The common control types<br />
� Logic control<br />
� Process control<br />
� Timing control<br />
can be implemented also in mixed form.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 159<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
160<br />
Laboratory Automation Software<br />
HiText is multitasking capable, i.e. several programs<br />
can run at the same time. Therefore you can clearly<br />
separate different tasks such as process control,<br />
monitoring, executing necessary reactions, online<br />
analysis etc. and retain the overview even in complex<br />
projects.<br />
For example, specifications of temperature ramps do<br />
not have to laboriously be interwoven in a single<br />
sequential program during simultaneous monitoring<br />
of a pH and a temperature window. Rather, each<br />
individual function is formulated as its own program,<br />
whereby in particular the re-usability of modules and<br />
the long-term maintainability are ensured.<br />
A HiText program is self-explanatory and self-documenting,<br />
so that you can attach it directly as documentation<br />
of the process cycle to your GMP or GLP<br />
documents.<br />
You can follow, interrupt, start and end the program<br />
progression online in the editor window. The values<br />
can even be changed during the run-time. In addition,<br />
you can also use variables instead of numbers,<br />
the values of which are allocated using the<br />
dialog forms or files.<br />
If necessary, a HiText program can co-operate with a<br />
subordinate PLC, an IEC 61131 IL-PI control program<br />
or device components and take over the<br />
function of a superordinate group control level.<br />
Common data points (variables) enable an uncomplicated<br />
data exchange with the PI.<br />
Beyond that, the modules of the HiBatch basic<br />
operations library are written in HiText. The user can<br />
Order Code Description<br />
SL-HITEXT HiText Full version<br />
SL-HITEXTL HiText light, max. 4 Programs each <strong>10</strong>0 lines<br />
therefore program new unit operations themselves<br />
and extend the library.<br />
HiText Language Elements<br />
The tab card language elements contain the<br />
available commands.<br />
You create a HiText program, by dragging the language<br />
elements or instructions simply with the<br />
mouse into the word processor window or by entering<br />
them directly using the keyboard.<br />
In the tab card functions you will find functions of the<br />
areas: arithmetics, trigonometry, text, and time/date.<br />
These functions support the implementation of<br />
online analysis programs and timing control etc.<br />
The following program example shows you how<br />
easily HiText is to understand and to apply:<br />
The command lines Output "...." to Report create the<br />
following entries in the progress report, which are<br />
automatically provided with a time stamp.<br />
This short example can only offer a first impression<br />
of the user-friendliness and only a small section of<br />
the capabilities of HiText and LabVision.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Dialogue and Protocol forms<br />
Laboratory Automation Software<br />
Protocol forms with display and input objects,<br />
diagrams, graphics, switches etc. can be created<br />
with the graphical editor, without even having to<br />
program a single line. These forms can not only be<br />
used for online-presentation of the data, but also as<br />
an extension to printed documents.<br />
Together with HiText you can automatically evaluate<br />
your experiment and present it directly in a suitable<br />
form.<br />
To every diagram there is a value table, which<br />
contains all the presented values and using the<br />
HiText program or manually this can be edited for<br />
further use.<br />
The form of the diagrams can be adjusted and fitted<br />
in many ways:<br />
� Multi axis, x-t, x-y<br />
� Multi-curves<br />
� Multi-diagram<br />
� Curve attribute lines, plot symbols<br />
� Fill areas<br />
� Subsidiary Lines<br />
� Linear or logarithmic scaling<br />
� Auto scaling<br />
Order Code Description<br />
SL-DIAPROT HiText Dialog and Protocol forms with diagram and tables<br />
The dialog and protocol masks are also being used<br />
within the electronic laboratory journal.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 161<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
162<br />
Laboratory Automation Software<br />
EasyBatch and ActionTracker- Table-based Recipe Control<br />
Recipe Control – The easy Way!<br />
EasyBatch<br />
Reproducibility and clear documentation of a test<br />
procedure are the requirements to assure quality<br />
and to reduce development times. This can only<br />
be reached in the scope of reasonable expenditure<br />
through automation of the procedure already in the<br />
research laboratory. Up to now, only the text-based<br />
language HiText or the graphical sequential function<br />
chart Hibatch were available for programming.<br />
As a new option of unmatched simplicity, EasyBatch<br />
is now available. EasyBatch enables uncomplicated<br />
table-based and and self-documenting<br />
programming. The operation can be conducted on<br />
an intuitive basis. EasyBatch can also be used in<br />
combination with the manual operation mode and<br />
ensures reproducibility in an easy manner.<br />
EasyBatch is even simpler to handle as HiText and<br />
HiBatch and is in particular suited for the<br />
programming of processes of simple to medium<br />
complexity.<br />
EasyBatch is also ideally suited for the control of<br />
fermenters, microreaction technology plants, and<br />
robots.<br />
An own table column is provided for all parameters<br />
and values, such as times and amounts, intended<br />
for regulation. The first column contains the order to<br />
be performed. In the simplest case, a programme<br />
only consists of set and wait orders. It represents<br />
recipe establishment without the necessity of<br />
programming knowledge and a minimum<br />
expenditure of time.<br />
� More time for Core Tasks due to a more<br />
efficient Mode of Operation<br />
� Automatic Test Control , also during the Night<br />
and Weekends<br />
� Modification of the Programme Parameters<br />
and the Procedure also during the actual Run<br />
Time is possible<br />
� Ideal Documentation due to consistent and<br />
complete Recording of Measurement Values,<br />
Sequences, Events and manual Interventions<br />
� Supports the GLP and GMP-conform<br />
Operation Mode<br />
Command Description<br />
Wait Programme waits until the time set in the parameter column hh:mm:ss has expired before executing next line<br />
Wait for Programme waits for the fulfillment of the condition in the the parameter column before executing next line<br />
Wait until Programme waits until /for the stated date or time before executing next line<br />
Set Allocates the respective values stated in the current line to the data points stated in the column head<br />
Ramp Establishes ramps for all setpoint values in the time stated in the parameter column to the end values stated in the<br />
current line<br />
Start Starts the HiText programme stated in the parameter column<br />
Stop Stops the HiText programme stated in the parameter column<br />
Pause Interrupts the HiText programme stated in the parameter column<br />
If Branches out to the stated programme line, if the condition in the parameter column is fulfilled<br />
Continue if Branches out without condition to the programme line stated in the column „line“<br />
Acknowledge Opens a window containing the message stated in the parameter column and interrupts the programme until the<br />
operator acknowledges (click on to OK)<br />
Full flexibility is reached through further commands<br />
such as „Wait until“, „Ramp“, If , The<br />
table listed below, depicts the commands in detail.<br />
As a special solution, HiText programmes can be<br />
integrated into the procedure, which are controlled<br />
with the programme Start/Stop/Pause.<br />
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Laboratory Automation Software<br />
The command parameters, such as time intervals,<br />
conditions, e.g. "pH > 6,5" or a HiText programme<br />
name are entered into the parameter column. The<br />
last column, if necessary, serves for the entry of<br />
comments by the operator for relevant information<br />
which can not be automatically captured.<br />
In the MultiWriter, occurring events, values and<br />
sequence phases are consistently presented.<br />
A batch protocol containing all events, operation<br />
interventions, value modifications etc., can be<br />
established and archived automatically in HiLIMS.<br />
This warrants for the ideal backup of test results and<br />
reproducibility at any time.<br />
The LabVision Project Modules represent the ideal<br />
basis for EasyBatch. The deployed modules<br />
automatically allocate the EasyBatch programme<br />
table so that the laboratory work can be immediately<br />
commenced after a project has been established.<br />
The EasyBatch Module is therefore the ideal tool to<br />
automate frequently changing applications with<br />
minimum expenditure.<br />
ActionTracker Action Recorder<br />
The operator operates the plant manually with the<br />
help of the operating screen. All setpoint value<br />
modifications are automatically recorded in the table.<br />
All value modifications are added as a line of the<br />
table by the ActionRecorder. Consequently, there is<br />
a clear and reproducible description of the actual<br />
procedure in table form available at the end of each<br />
process. In other words: A workable programme is<br />
automatically established by the operating activities<br />
of the operator without the necessity of any further<br />
action.<br />
The chain of activities recorded in table form can<br />
now be automatically repeated without any further<br />
effort. It is possible, during the run time or before the<br />
repeated start of the table, to enter intervals,<br />
setpoints, comments, conditions etc.<br />
Usually, before repeated execution, the table is<br />
edited to consolidate the same. Setpoints which<br />
were modified shortly after another can be<br />
summarised in one line and certain operatorsupported<br />
tasks such as the reaching of a certain<br />
value (in this case: Wait pH > 7) can be integrated<br />
into the programme.<br />
If values are modified by the operator during<br />
realisation, the table is automatically accordingly<br />
adjusted. This ensures that the procedure is<br />
documented and reproducable <strong>10</strong>0% at any given<br />
time.<br />
Order Code Description<br />
SL-EASYBATCH Table-based Recipe Control<br />
SL-ACTIONTRACK ActionTracker for the Recording of Operation Activities as EasyBatch Programme<br />
Remark: EasyBatch and ActionTracker require SL-HITEXT(L) and SL-DIAPROT.<br />
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Laboratory Automation Software<br />
HiBatch Recipe Control and Administration<br />
Reproducibility and clear documentation of an<br />
experimental process are the conditions for<br />
increased quality and shortening of development<br />
times. The basis for this is the automation of the<br />
procedure even in the development laboratory.<br />
The recipe module HiBatch, available as extension<br />
to HiText, enables the creation of recipe flow<br />
diagrams by linking unit operations with the help of a<br />
graphical recipe editor. HiBatch is even simpler to<br />
handle than HiText. Even complex recipe flow diagrams<br />
can be created to IEC and NAMUR norms in<br />
clear form with minimum time expenditure. By<br />
clicking an operation in the flow diagram you open<br />
the appropriate dialog form, in order to input parameters<br />
and values such as quantities and times.<br />
A unit operation can be used several times, also<br />
parallel or at the same time. The process plan is<br />
checked and executed automatically. The active<br />
steps are colour indicated and freely selectable<br />
control values are displayed directly in the flow<br />
diagram.<br />
Whole experiment series can be run automatically in<br />
series on one reactor or parallel on multiple reactors.<br />
With a unit operation library to the NAMUR standard,<br />
application of the recipe control program HiBatch<br />
gives you a number of further advantages:<br />
� Recipe creation without programming<br />
knowledge in minimum time<br />
� More time for qualified base activities from<br />
more efficient work methods<br />
� Automatic experiment control, also over night<br />
and at the weekend<br />
� Changing of program parameters and the<br />
procedure even possible during runtime<br />
� Optimal documentation by complete<br />
recording of measurement data, procedures,<br />
events and manual intrusion<br />
� Simplified and safe transfer of the EMSR-<br />
Know-How from the lab to pilot plant and the<br />
production stage<br />
� Supports the GLP and GMP suited methods<br />
The input parameters are checked with freely<br />
definable plausibility criteria and if necessary,<br />
corrected. The parameter sets can be saved for<br />
further future use.<br />
Also for running recipe process control, you can still<br />
change the parameters and temporarily interrupt the<br />
process at any time, e.g. for manual actions.<br />
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Laboratory Automation Software<br />
Thanks to the open programming in HiText the<br />
system can be added to without problems using<br />
preloaded and saved functionalities, e.g. a scaling<br />
function for the basis recipe, automatic<br />
parameterisation of whole series of experiments,<br />
automated evaluation, or administration of the<br />
parameters and results.<br />
You can write your own basic operations with HiText<br />
or make use of the basic operations library (SL-<br />
GOPBIB). For the establishment of special basic<br />
operations you may call upon our respective<br />
services offered.<br />
In the multi-plotter, events, values, and process<br />
phases are consistently presented.<br />
A batch protocol with all events, operator<br />
interventions, value changes etc. is automatically<br />
established. This guarantees an optimal<br />
reproducibility of the process even after manual<br />
interventions.<br />
The electronic laboratory journal eJournal and the<br />
laboratory information management system HiLIMS<br />
complete HiBatch. They create a consitent process<br />
chain from the contract to the control of the complete<br />
R&D process to the final report.<br />
For simpler applications EasyBatch might be of<br />
choice.<br />
Note: HiBatch requires HiText.<br />
Order Code Description<br />
SL-HIBATCH Recipe control module with graphical editor<br />
SL-HIBATCHL Recipe control module with graphical editor, Light-Version, limited to 20 steps<br />
SL-HIBATCHAP Recipe control module with graphical editor for closed basic operations library<br />
SL-HIBATCHRT Recipe control runtime module, limited to running and parameterisation of recipe process<br />
plans<br />
Additionally recommende modules:<br />
Order Code Description<br />
SL-GOPBIB <strong>HiTec</strong> Basic Operations Library for HiBatch<br />
SL-GOPBIBL <strong>HiTec</strong> Basic Operations Library Light for HiBatch<br />
SL-SCHERE Event plotter<br />
SL-SCHPHA Phase Plotter<br />
SL-BERICHT Extenderter Ablaufbericht mit Batch/Rezeptur-Filter<br />
SL-JOURNAL Parametrierbares elektronisches eLabor-Journal<br />
SL-HILIMSL Single-User HiLIMS licence with local SQL database (max. 4 GB)<br />
SL-HILIMS Laboratory information management system with external SQL-database<br />
Please note our discounted<br />
Software packages with their proven module collection.<br />
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Basic Operations Library<br />
Laboratory Automation Software<br />
With the <strong>HiTec</strong> <strong>Zang</strong> basic operations library you<br />
have a tool at hand, with which you can respond<br />
quickly and flexibly to continuous new demands.<br />
The progress program is arranged out of standard<br />
components. Therefore, even a synthesis of high<br />
complexity can be programmed with minimum time<br />
expenditure.<br />
The elements of the basic operations library are<br />
written in the self-documenting language HiText.<br />
Therefore you can make randomly many individual<br />
adjustments by changing the control program.<br />
Likewise, you can also edit the dialogue forms with a<br />
comfortable Designer where necessary.<br />
If required, our application developers can create<br />
further basic operations according to your<br />
requirements.<br />
The basic operations are available individually or as<br />
a library.<br />
Basic Unit Operations:<br />
Order Code Description<br />
SL-GOPBIB <strong>HiTec</strong> Basic Operations Library for HiBatch<br />
- Pressure (the program controls a pressure regulation with setpoint ramp)<br />
- Pressure_Hold (simple pressure regulation)<br />
- Vacuum_Hold (vacuum control)<br />
- Control Program (types or versions of a control program)<br />
- SoliDos (solid dosing with SoliDos)<br />
- PH_Regulation (pH-value-regulation for base and/or acid metered addition)<br />
- Inert_Establish (establishment of inert atmosphere by repeated drawing of vacuum/inerting)<br />
- Fill (metered addition without regulator)<br />
- Distilling (distillation with jacket -temperature regulation)<br />
- Weighing-in (weighing in by hand with reporting)<br />
- Inerting (addition of inert gas )<br />
- Reflux Distillation (waiting for setpoint temperature and initialised time )<br />
- Boiling Point Recognition of boiling points for subsequent distilling)<br />
- Rectifying (control of a rectification column)<br />
- Vacuum (program to run vacuum ramps)<br />
- Repeat (determines the number of passes of a recipe cycle)<br />
- Wait_Condition (waiting until freely-definable condition is fulfilled)<br />
- Wait_Operator (waits for acknowledgement by operator)<br />
- as well as all basic operations of the options SL-GOPBIBL<br />
SL-GOPBIBL <strong>HiTec</strong> Basic Operations Library Light for HiBatch<br />
- Surge_Doser (fastest possible gravimetric dosing of the stated amount)<br />
- Batch Amount_Doser (gravimetric dosing of the stated amount within the stated time)<br />
- Batch Rate_Doser (gravimetric dosing at the stated rate during the stated time )<br />
- Conti (-nuous) Doser (continuous dosing with consistent dosing rate)<br />
- Temperature_Hold (temperature control)<br />
- Dosing (gravimetric dosing)<br />
- Dosing_Gravi (gravimetric dosing from load cell, without refilling)<br />
- Final Operation (end step of recipes with export possibilities)<br />
- Stirring (input of a setpoint temperature to stirrer)<br />
- Initial Operation (start/initial step for a recipe)<br />
- Taring_Gravi (taring of a load cell)<br />
- Taring_Scales (taring of a scales)<br />
- Tempering (program to run heating and cooling ramps)<br />
- Value Output (output of a new value to a data point)<br />
- Wait (taking of adjustable idle time)<br />
- Wait_Until (waiting for the set point of time)<br />
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Individual Basic Operations:<br />
Laboratory Automation Software<br />
Order Code Basis Operations Description<br />
SL-GOPBEFUEL Fill Charge dose without controller. The pump power is reduced towards the<br />
end of the dose automatically to come as accurate as possible to the desired<br />
amount.<br />
SL-GOPDEST Distil Distillation with jacket temperature regulation.<br />
The setpoint value for the jacket temperature results from the current reactor<br />
inner temperature plus the setpoint difference between inner and jacket<br />
temperature. The setpoint difference between inner and jacket temperature<br />
is given by the user. Small setpoint differences mean sparing distillation!<br />
The reflux fraction ratio can be controlled dependent of the head<br />
temperature.<br />
SL-GOPDOSI Dose Gravimetric dosing of one balance with setpoint value ramp and controller.<br />
SL-GOPDOSIGRAVI1 Dose_Gravi1 Gravimetric dosing from one load cell (e.g. Hitec <strong>Zang</strong> GraviDos) with set<br />
value ramp and controller. Without refilling of the feed tank.<br />
SL-GOPDPWERT Value Output Output of a new value to a data point<br />
SL-GOPDRUCK Pressure The program controls a pressure regulation.<br />
The setpoint is controlled via ramp to the final value.<br />
SL-GOPDRUCKHALTEN Pressure Hold The program controls a pressure regulation.<br />
The predetermined setpoint is directly issued to the regulator.<br />
Transition is possible according to time or through structural transition (e.g. if<br />
a parallel path is completed).<br />
SL-GOPEINWIEG Weighing Weighing of a substance "manually". The weighed quantity is recorded to<br />
the progress report.<br />
SL-GOPEND Final Operation This operation serves as final step for recipes.<br />
There is the possibility to automatically start an arranged export out of this<br />
recipe step. As time period for the export, the period from the start of the<br />
recipe and the start of the export is applied. Prerequisite for the function of<br />
the export is the utilisation of the initial operation out of the basic operation<br />
library, as well as the full version of the data export module.<br />
SL-GOPGRAVITARI Taring_GraviDos Program for resetting a load cell (e.g. Hitec <strong>Zang</strong> GraviDos)<br />
SL-GOPINERT Inerting The program serves to open a binary and proportional inerting valve. It can<br />
optionally be opened for a certain period or as long as a parallel path is<br />
running.<br />
SL-GOPINERTHERST Inert_Provision To provide an inert atmosphere by n-fold turning vacuum pulling /inerting to<br />
pressure with vacuum control<br />
SL-GOPKALOHEIZ CaloHeater The program is used to control a calorimetric heater (e.g. <strong>HiTec</strong> <strong>Zang</strong><br />
KaloHeiz). Thereby, a defined heat load can be switched on to the reactor for<br />
a certain time period.<br />
SL-GOPKALOONL OnlineCalo The program offers simple online reaction calorimetry evaluation.<br />
SL-GOPKONTIDOS Continuous_ Doser Continuous gravimetric dosing with consistent dosing rate.<br />
SL-GOPMENGENDOS Batch amount Doser Gravimetric dosing of the stated amount in the stated period of time.<br />
SL-GOPPHREGELUNG pH Control PH Value Control for base and/or acid metered addition via pH value<br />
regulator. Transition is possible after reaching a pH tolerance limit or through<br />
structural transition (e.g. if a parallel path is completed).<br />
SL-GOPPROGRAMM Control Program Starting or execution of a HiText program<br />
SL-GOPRATENDOS Batch Rate Doser Gravimetric dosing with the stated rate during the stated period of time<br />
SL-GOPREKTIF Rectification Fractionated distillation, discharge of several fractions, control according to<br />
temperature or pressure difference. Consistent linear or exponential column<br />
head control.<br />
SL-GOPRUECKDEST Reflux destillation The programm will wait until the next initialised setpoint temperature during<br />
the destillation is reached and then waits for a certain amount of time.<br />
SL-GOPRUEHR Stirring The program gives as an output the setpoint rotational speed of a stirrer.<br />
Stirring can either take place for a certain time or until a parallel step is<br />
complete.<br />
SL-GOPSIEDEP Boiling Point This program offers the detection of boiling points (e.g. for following<br />
distillation).<br />
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Individual Basic Operations (continued):<br />
Laboratory Automation Software<br />
Order Code Basis Operations Description<br />
SL-GOPSTART Initial Operation Start step for a recipe with the possibility to carry out initialisations and<br />
settings.<br />
SL-GOPSTOSSDOS Surge_Doser Fastest possible dosing of the stated amount.<br />
SL-GOPTEMP Tempering Program for driving heating/cooling ramps<br />
SL-GOPTEMPHALTEN Temp_Hold The program controls a temperature regulation. The predetermined setpoint<br />
is issued directly to the regulator when controlling interior temperature, and<br />
directly to the thermostat when controlling the jacket temperature. Transition<br />
is possible according to time or through structural transition (e.g. if a parallel<br />
path is completed).<br />
SL-GOPVAKHALTEN Vacuum_Hold The program controls a vacuum regulation. The predetermined setpoint is<br />
issued directly to the regulator. Transition is possible according to time or<br />
through structural transition (e.g. if a parallel path is completed).<br />
SL-GOPVAKU Vacuum The program controls vacuum regulation. The setpoint value is run to a<br />
desired end value using a ramp.<br />
SL-GOPWAAGETARI Tare_Scales Program for resetting a balance<br />
SL-GOPWARTET Wait_Until Program for holding for an arbitrary waiting time.<br />
SL-GOPWARTEZ Wait Program for holding until an arbitrary time.<br />
SL-GOPWBEDIENER Wait_Operator Waits until the operator presses OK.<br />
SL-GOPWBEDINGUNG Wait_Condition Waits until the condition is fulfilled.<br />
SL-GOPWIEDERH Repeat Determines the number of passes of a recipe cycle.<br />
As long as the counter is smaller than the number of repetitions, the right<br />
output of the of the element is used, otherwise, the lower output.<br />
Recipe Series Generator<br />
The recipe series generator, in connection with<br />
HiBatch, allows automatic parameterisation and<br />
execution of experiment series. RezGen generates a<br />
whole experiment series automatically out of a few<br />
specifications. The desired parameters are varied<br />
within defined ranges from experiment to<br />
experiment. This results in:<br />
� Great time savings when conducting serial or<br />
parallel experiments<br />
� Increase of the Laboratory Performance<br />
� Shortened „Time to Market"<br />
For the parameters intended to be varied, the<br />
operator merely needs to predefine the initial value,<br />
the final value, and the increase from experiment to<br />
experiment.<br />
RezGen will then produce an experiment plan, which<br />
contains all variations. Unnecessary variations can<br />
be excluded.<br />
If, for example, experiments are to be conducted at<br />
four different temperatures, and one reactant is to be<br />
added metered at each temperature in three<br />
different quantities, this will result in 12 variations.<br />
The control recipes automatically generated out of<br />
one basic recipe, can, in a suitable assembly,<br />
Order Code Description<br />
SL-REZGEN Recipe Series Generator<br />
conducted in automatic mode in succession or<br />
simultaneously in a parallel reactor system.<br />
The variable parameters are entered into the basic<br />
recipe form.<br />
The intended variations of individual parameters are<br />
specified in the factor plan.<br />
The individual work recipes are generated out of the<br />
entered data. In the Release form, the work recipes<br />
can be released or disabled.<br />
Informations about StatGen for compiling multi factorial test planing for the statistic experiment planing<br />
upon request.<br />
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MultiBatch<br />
Laboratory Automation Software<br />
The definition of parallel experiments is made<br />
possible as simple as can be by the HiBatch<br />
extension MultiBatch. A recipe established as a<br />
sample can be applied to a random number of<br />
reactors with MultiBatch. The recipes can be<br />
individually parameterised and the progression<br />
individually modified.<br />
You define all parallel experiments by allocating the<br />
sample recipe to the reactors intended for use with<br />
the help of the reactor allocation chart.<br />
Allocation of the reactors for the sample recipe.<br />
MultiBatch will then generate an entity for each<br />
reactor. In order to be able to differentiate, the<br />
names of the recipes are indexed with the attached<br />
reactor identification number.<br />
Order Code Description<br />
SL-MULTIBATCH MultiBatch Option for HiBatch<br />
The entities can be started, held, and completed<br />
independent of each other and have separate data<br />
records.<br />
The recipe procedures are initially the same at the<br />
respective parallel experiments. Individual<br />
procedures can however be individually modified.<br />
Cloner<br />
Display of the allocated reactors.<br />
The cloner is a benefical tools too multiplicate<br />
control structures. Creating a parallel reactor project<br />
will be a lot easier with the cloner. After the project<br />
has been created for one reactor it can be cloned to<br />
all further reactors. The user decides which objects<br />
will be cloned.<br />
The cloned objects will signed by indices attached to<br />
the data point name eg. Valve[2] .<br />
The channel number will be assigned automatically,<br />
but can be changed later.<br />
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Laboratory Automation Software<br />
eJournal, the electronic Laboratory Notebook (ELN)<br />
Test Documentation as it should be!<br />
The electronic laboratory notebook eJournal<br />
represents more than an adequate substitute for the<br />
paper-bound laboratory notebook. The eJounal<br />
automatically protocols all information gained in the<br />
course of the test progression. In addition, it is also<br />
possible to consistently present and archive test<br />
regulations, material properties of the educts and<br />
products, laboratory analyses and further<br />
information. This significantly increases productivity<br />
and prevents the loss of knowledge through<br />
employee turnover.<br />
The trend towards the electronic document is<br />
becoming more and more evident. The American<br />
FDA (Food and Drug Administration) is pushing the<br />
deployment of electronic media within<br />
documentation. Due to the Electronic Signature Act,<br />
digitally signed electronic documents are legally<br />
equivalent to hand-signed paper documents. The<br />
increase of productivity in the research industry due<br />
to the change to an electronic system is estimated to<br />
be 50%.<br />
A computer-supported laboratory notebook offers<br />
significant advantages: reading and writing mistakes<br />
are eliminated, a retrieval function enables the fast<br />
search for experiments and results. The<br />
manipulation-secure filing with electronic signature<br />
is made possible. Test parameters, measurement<br />
data, and evaluated results are presented clearly on<br />
protocol pages.<br />
The laboratory personnel is supported with<br />
additional functionalities (e.g. automated evaluation)<br />
and, in particular, relieved of bothersome routine<br />
activities such as the noting of measurement values.<br />
An electronic laboratory notebook is particularly a<br />
„must-have“, if the laboratory process (synthesis<br />
laboratory, fermentation laboratory) must run GLPconform<br />
(Good Laboratory Practice) or a validated<br />
mode of operation is required.<br />
Advantages:<br />
� Standardised Mode of Operation<br />
� Relief of Laboratory Personnel from Routine<br />
Activities<br />
� Elimination of Reading and Writing Mistakes<br />
� Manipulation-secure Filing<br />
� Easier Retrieval of Experiments<br />
� A Contribution towards the paperless<br />
Laboratory<br />
� Individually configurable<br />
� Online Evaluation and Spreadsheet<br />
� Full Text Retrieval in individual or all pdf-<br />
Documents<br />
� Export of the Test Report as pdf or rtf Data<br />
File<br />
The following diagram illustrates the information flow<br />
between the individual modules of the LabVision<br />
System.<br />
Recording<br />
In the electronic laboratory notebook all relevant<br />
values, parameters, and results, as well as eventual<br />
defining text and comments, of a test are recorded<br />
and stored. It is also possible to automatically<br />
integrate digital photographs made event-driven or<br />
according to schedule with the LabCam Module<br />
during the test.<br />
The recorded data is presented in freely<br />
configurable report pages with tables and graphic<br />
value and text fields. This warrants for an optimal<br />
documentation of the test progression at all times.<br />
Manual processing of the data is no longer required,<br />
which eliminates one major source for mistakes.<br />
Unattended operation is now possible – night time<br />
and weekends are now available for experimenting.<br />
A multitude of tests can now be processed in a<br />
minimum of time.<br />
Protocoling<br />
The batch protocol containing all values, events,<br />
operating interventions, value changes, etc. is<br />
established automatically. Digital photographs,<br />
chemical formulas, laboratory analysis data, links to<br />
data files or websites, comments etc. can just be<br />
integrated. eJournal therefore represents a major<br />
step in the direction of a paperless laboratory.<br />
Authenticity and integrity of the information are<br />
secured.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
The protocol can be aligned to the special<br />
requirements of your laboratory. It contains, amongst<br />
others, a first page with general information, one<br />
page with information to the educts and products<br />
and plant properties, one page with analysis values,<br />
as well as protocol pages with the recorded<br />
measurement values, events, and comments. The<br />
layout of the protocol pages can be designed freely<br />
with the form generator.<br />
To enable a better overview and clarity, the recorded<br />
values are also graphically presented. The<br />
laboratory notebook can be exported as pdf or rtf<br />
data file for further processing. The manipulationsecure<br />
pdf data file can be transmitted e.g. per Email.<br />
The rtf data file can be reworked with a word<br />
processing program.<br />
Evaluation<br />
Evaluation and documentation of the experimental<br />
data are supported or completely automated. The<br />
recorded data can be evaluated automated with<br />
HiText and presented in tables or various<br />
presentation forms, e.g. as a set of curves, average<br />
values with minimum and maximum bars or<br />
standard deviations. Self-calculating tables are also<br />
possible.<br />
Data import/export<br />
For data exchange to third party software multiple<br />
options are available<br />
� scv-file<br />
� text file<br />
� Windows Pipe<br />
� apis<br />
Order Code Description<br />
SL-JOURNAL eJournal, parameterisable, electronic laboratory notebook<br />
eJournal requires SL-HITEXT and SL-DIAPROT.<br />
Comprehensive Documentation<br />
A comprehensive synthesis regulation is elementary<br />
for the explicit performance of a reaction. It contains,<br />
respectively interconnects all information required to<br />
make the reaction reproducible. These include<br />
statements to the test assembly, the recipe<br />
workflow, the data of the reactants and solvents and<br />
test parameters such as periods, quantities, and<br />
pressures. The storage of the synthesis regulation<br />
ensures the availability of all information required for<br />
a later repetition of a test.<br />
Savin of the sythesis directive ensures an availability<br />
of all information within the systems to reproduce the<br />
the experiments.<br />
Organisational, procedural, and chemical<br />
information are also registered in the eJounal to<br />
enable the precise allocation of the other data.<br />
The eJournal structures the data in such a manner<br />
that it can easily be retrieved with the help of the<br />
HiLIMS Laboratory-Information-Management-System<br />
and are available for further use. This ensures<br />
that new and proven synthesis regulations, including<br />
the knowledge of the synthesised substances, are<br />
not lost and available at all times.<br />
Informations about LIMS can be found under<br />
HiLIMS Laboratory-Information-Management-<br />
System.<br />
We will create your own laboratory journal according<br />
to your specifications.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 171<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
172<br />
Data Export<br />
Laboratory Automation Software<br />
The data export server supports the manual and<br />
automatic exporting of values and protocol files in<br />
the file formats<br />
� Excel SYLK (slk)<br />
� Text format (csv)<br />
� Excel direct export (xls)<br />
� HTML format (.html)<br />
For predetermined times, several export jobs can be<br />
defined and implemented manually or automatically.<br />
In addition, there is also the possibility to control the<br />
export via HiText program, e.g. in order to export the<br />
data automatically at the end of an experiment.<br />
A data export can also be started directly from the<br />
analogue pen recorder.<br />
The data points intended for export can be selected<br />
individually. The number of places before and after<br />
the decimal point can be determined.<br />
Numeric data exported are subject to a data<br />
reduction. The reduction is optionally conducted by<br />
forming the:<br />
� average value<br />
� max value<br />
� min value<br />
� unaveraged<br />
� interpolate<br />
The reduction interval is freely definable.<br />
One data point can be entered several times e.g. to<br />
export average, min and max values. The time can<br />
be issued optionally either absolute or relative to a<br />
freely selectable start time.<br />
An export that can be started manually is already<br />
contained in the Basic Version.<br />
Order Code Description<br />
SL-EXPORT LabVision export module, Option for automatic or <strong>HiTec</strong>-controlled Exports<br />
Selectors and Display Filters<br />
The display filters help to handle larger arising data<br />
floods at plants, e.g. by limiting the time domains.<br />
Selectors serve as user-specific classification<br />
criterion, e.g. when looking for or sorting the data<br />
points and in the protocols. Selectors can be defined<br />
by the user in a separate form freely.<br />
Example:<br />
System1, System2, to wait, to be calibrated, no<br />
operation.<br />
The selectors offer the possibility to select a group of<br />
data points during selection, in reports etc.<br />
The selectors can be linked by the operators<br />
� plus<br />
� without<br />
� )thereof(<br />
Order Code Description<br />
SL-SELFIL Selectors and filters for LabVision<br />
Example: (Reactor1 plus cooling unit) thereof (all<br />
without required values)<br />
All data points are selected by this selection except<br />
the setpoint value data points of Reactor1 and the<br />
cooling unit.<br />
This option also extends the filter possibilities<br />
� Project Modules<br />
� Progress Report<br />
� Message Report<br />
� Data Point Selection<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
Access Control and User Administration<br />
The access supervision is active in:<br />
� Modules e.g. project administration, control<br />
program editor...<br />
� Windows with critical data point parameterisation<br />
possibilities<br />
� Objects established by the user such as<br />
programs, flow sheets and recipes and individual<br />
operating objects.<br />
For every user, authorisations can be assigned<br />
individually. A user must first register with name and<br />
password before he can operate the system.<br />
The user administration can, according to an<br />
adjustable inactivity period, automatically lock the<br />
system to prevent operation.<br />
Order Code Description<br />
SL-BENRECH Access and user administration for LabVision<br />
Multiple Projects<br />
Several plants each with its own PI can be driven<br />
with an UI.<br />
The option "multiple projects" makes it, in each case,<br />
possible to start on one UI several projects with its<br />
own LabVision.<br />
Order Code Description<br />
SL-MULTIPROJ Multiple Projects with LabVision<br />
WebVision<br />
WebVision enables to operate and monitor<br />
LabVision from an external computer (Client) via a<br />
network connection (TCP/IP).<br />
Running LabVision projects can be accessed from<br />
one or several computers connected via network<br />
without the necessity of having to install a Labvision<br />
system at these locations.<br />
The WebVision user interface is mainly identical with<br />
the same of LabVision.<br />
For WebVision integrations, the access control is<br />
obligatory.<br />
Each project has then an independent control<br />
interface.<br />
For licensing the data points of all simultaneously<br />
active applications are added together.<br />
WebVision supports the same modules (work<br />
sheets, multichart recorders, process reports,<br />
message reports, and LabCam) according to the<br />
optional equipment of the currently assembled<br />
LabVision-System.<br />
The LabVision User Administration is supported.<br />
Work sheet operator operations can be permitted or<br />
prohibited by the Labvision computer depending on<br />
the user setting. WebVision operating activities are<br />
protocolled in the process report.<br />
Several WebVision installations can respectively<br />
access (simultaneously) on to one or more<br />
LabVision Systems in the net. The LabVision or<br />
HiText uer interface must not be active for this<br />
purpose. Worksheets can both be displayed and<br />
operated in WebVision.<br />
A "Chat Function" enables the communication<br />
between the user of the LabVision System and the<br />
WebVision users. The „light“ version is limited to the<br />
display of the multichart recorder.<br />
Order Code Description<br />
SL-WEBVIS Access to active LabVision projects via TCP/IP LAN connection<br />
SL-WEBVISL Only MultiChart recorder visualisation of active LabVision-Projects<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 173<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
174<br />
Laboratory Automation Software<br />
Activation Module for PI of other Manufacturers<br />
If Labvision is intended to be exclusively run by a PI<br />
of other manufacturers, a dongle is required for the<br />
administration of the program options.<br />
Order Code Description<br />
SL-FREMDPNK LabVision Activation Module for PI of other Manufacturers ( with Dongle)<br />
PI-Drivers<br />
The PI driver makes the communication between the<br />
UI with a PI possible. The PI Driver for the <strong>HiTec</strong> PIs<br />
LabManager, LabBox, MSR manager and MSR box<br />
is supplied free of charge with the devices. A <strong>HiTec</strong><br />
PI can be simulated by the special PI driver<br />
PNKSIMMAN. Due to this, it is possible to provide<br />
an application without an attached PI.<br />
PI Driver for other PIs and Field Bus Systems<br />
The PI driver for (external) other manufacturers' PIs ,<br />
a software connection to existing automation<br />
software or data bases, as well as fieldbus systems,<br />
can be operated parallel to PI drivers.<br />
Next to the PI drivers for the <strong>HiTec</strong> PIs, drivers for<br />
various laboratory instruments and PIs of other<br />
manufacturers are available. LabVision can<br />
integrate several PI drivers and consequently<br />
communicate with different Pis simultaneously. PI<br />
drivers are available for a broad range of devices.<br />
The range is consistently extended by us. For this<br />
reason, if you require a driver for an automation unit<br />
that is not listed in this catalogue please inquire if<br />
there is a connection possibility in the mean time.<br />
If required, our programming department will<br />
establish customer-specific PI drivers for any device.<br />
Order Code Option / Function<br />
SL-PNKPERF PI-Driver for Braun Perfusor<br />
SL-PNKSPS PI-Driver for Siemens S5/S7, 3964(R) protocol and AEG Modicon<br />
SL-PNKLASENTEC PI-Driver for Lasentec FBRM - particle systems<br />
SL-PNKMTRx PI-Driver for Metrohm Dosimat 665 and 765, Titrino 718 and 702,<br />
and Liquino over Dosing Interface 846 (x = 1, 2, 4, 8 Devices)<br />
SL-PNKOPC PI-Driver for OPC-DA (version 1+2), OPC-Client<br />
SL-PNKDDE PI-Driver for DDE data exchange<br />
SL-PNKMODBUS PI-Driver for ModBus devices over serial PC interface<br />
SL-FREMDPNK LabVision access module for externally manufactured -PI systems (with Dongle)<br />
Further drivers upon request.<br />
Programming-Interface<br />
The module ANWINT makes it possible to access<br />
from other programs (Visual basic, C++, Pascal...)<br />
the current values of the data points being written<br />
and read. A briefing of one day by our programmers<br />
is mandatory.<br />
Order Code Description<br />
SL-ANWINT Programming interface for LabVision<br />
DS-LVPROG Instruction into „SL-ANWINT“ programming for LabVision<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Remote Connection<br />
LabVision offers different possibilities for the<br />
remote connection of the UI.<br />
Connection via<br />
� Internet<br />
� Network (LAN)<br />
� Modem<br />
� ISDN<br />
Applications<br />
� remote maintenance<br />
� remote support<br />
� remote diagnosis<br />
� software maintenance<br />
� remote control<br />
� data transfer<br />
Laboratory Automation Software<br />
Remote <strong>Main</strong>tenance/ Remote Support<br />
� Support and Fault remedy without delay<br />
� Short service-reaction times, particular in<br />
critical situations<br />
� Savings on service costs<br />
With the help of this „Remote Access“ software, the<br />
UI can be operated from a remote work station.<br />
This computer virtually makes a second keyboard<br />
and monitor available, so that all functions can be<br />
carried out like at the UI itself. Both monitors<br />
therefore display the same screen image.<br />
In addition, file transfer is possible in both<br />
directions.<br />
All keyboard and mouse actions, also screen<br />
settings, are communicated via the telephone or<br />
LAN network.<br />
Consequently, fault detection and remedy, network<br />
maintenance, file transfer, installation of updates,<br />
etc. can be carried out quickly and cost effectively.<br />
Other possibilities not yet mentioned here are in<br />
preparation, or can be arranged according to<br />
customer specifications.<br />
Order Code Description<br />
SL-TELES Tele-Service, remote connection to an UI for remote maintenance<br />
CP-MODEM2 External Modem for analogue telephone networks<br />
CP-MODEM4 External Modem for leased lines<br />
CP-ISDNAD ISDN-Adapter-card for digital networks<br />
Price Structure<br />
The sale price is determined from the number of<br />
data points and the selected options. This ensures<br />
that you must only purchase what you really need.<br />
All inputs and outputs are counted as data points,<br />
inputs and outputs of device components, except<br />
controllers, monitoring conditions and text data<br />
points.<br />
Local variables and/or indicators in HiText and AWL<br />
(Instruction List) do not count as data points.<br />
The necessary number of data points can be<br />
evaluated as follows:<br />
Number of data points = number of the inputs<br />
and outputs * automation factor<br />
Level of Tasks Automation<br />
Automation<br />
Factor<br />
Minimum Only recording of measurement 1<br />
Low Recording of measurement, limit-value monitoring, simple regulation 2<br />
Medium Recording of measurement, limit-value monitoring, control, regulation 4<br />
High Recording of measurement, limit-value monitoring, control, regulation,<br />
complex prompting<br />
8<br />
In regard to the number of data points, there is the Our application advisors will gladly discuss with you<br />
choice between 30, <strong>10</strong>0, 180, 300, 560, and <strong>10</strong>00. your automation project and arrange a suitable<br />
package. The packages can be upgraded by<br />
program options and data points at any time.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 175<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
176<br />
LabVision ® standard packets<br />
Laboratory Automation Software<br />
For the most frequent applications, the following<br />
LabVision standard packages were arranged. They<br />
save you laborious arranging of the individual<br />
modules and are, in addition, lower-priced than the<br />
sum of the single modules.<br />
Overview of all LabVision Software packets<br />
LabVision module<br />
Order code packet<br />
SL-LABVIS<br />
(LabVision base module with 30 data points)<br />
SL-HITEXT<br />
(HiText- Multi-tasking Control and Online-Evaluation)<br />
SL-HIBATCH<br />
(Recipe control module w. graphic recipe editor)<br />
SL-EASYBATCH<br />
(Table based recipe control module)<br />
SL-ACTIONTRACK<br />
(Recording of activities as EasyBatch program)<br />
SL-GOPBIB<br />
(<strong>HiTec</strong> basic unit operations library f. HiBatch)<br />
SL-DIAPROT<br />
(Dialog and Protocol forms with tables incl. graphics)<br />
SL-ONLGRA<br />
(Online charts with reference curve presentation)<br />
SL-SCHANA<br />
(Analogue plotter, MDI-capable)<br />
SL-SCHERE<br />
(Event plotter)<br />
SL-SCHPHA<br />
(Phase plotter)<br />
SL-UEBMEL<br />
(Monitoring and Reporting)<br />
SL-DESIGN<br />
(Designer)<br />
SL-MODBIBALR<br />
(Project Module Library for Designer)<br />
SL-PROJMOD<br />
(Project modules generator and editor for LabVision)<br />
SL-RIEDIT<br />
(RI-Editor according to EN ISO <strong>10</strong>628)<br />
SL-BIBRILK<br />
(Glass a. Laboratory Devices Library for P&ID-Editor)<br />
SL-EXPORT<br />
(LabVision export module, automatic or exports)<br />
SL-SELFIL<br />
(Selectors and filter functionality)<br />
SL-BENRECH<br />
(Access and user administration for LabVision)<br />
SF-AWLPLUS<br />
(Instruction List Module with structured Text )<br />
SL-BERICHT<br />
(Progress Report, batch orientated extended search)<br />
SL-JOURNAL<br />
(Parameterisable electronic laboratory notebook)<br />
SL-WEBVIS<br />
(Remote maintenance of projects via TCP/IP)<br />
1 Light-Version: one worksheet, max. 200 objects<br />
2 Light-Version: 4 programms with <strong>10</strong>0 code lines each<br />
3 Light-Version: consisting of dosing, tempering and vacuum<br />
4 Light-Version: max. 120 objects<br />
5 Light-Version: 2 plotter pages with 8 curves each<br />
SL-LABVIPKONL<br />
For continuous and batch processes, individual<br />
packages are intended. The packages can also be<br />
individually extended later.<br />
The packages already contain the minimum data<br />
point amount of 30 and must be extended to the<br />
number required for the application.<br />
SL-LABVIPKON<br />
SL-LABVIPKONP<br />
SL-LABVIPEASY<br />
x x x x x x x x<br />
x 2 x x x x x x x<br />
x<br />
SL-LABVIPBATL<br />
SL-LABVIPBATE<br />
SL-LABVIPBAT<br />
SL-LABVIPBATP<br />
x 8 x x x<br />
x 9 x x x<br />
x x x x x x<br />
x x<br />
x 5 x x x 5 x 5 x 5 x x<br />
x 6 x x x 6 x 6 x 6 x x<br />
x 7 x 7 x x x<br />
x x x<br />
x 1 x x x 1 x 1 x x x<br />
x 3 x x x 3 x 3 x x x<br />
x<br />
x 4 x x x 4 x 4 x x x<br />
x x<br />
x x x<br />
x x x<br />
x x<br />
x x<br />
x x<br />
x x<br />
6 Light-Version: Events will only shown as shortened hints<br />
7 Light-Version: max. 3 phases<br />
8 Light-Version: max. 20 steps<br />
9 Light-Version: limited library see "Basic unit operations library"<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
Conti-light Software packet for LabBox 1 and 2<br />
This software package is made for LabBox1 and 2<br />
PIs and is suited for the automation of small<br />
continuous processes. (Description, see chart<br />
above)<br />
Order Code Description<br />
SL-LABVIPKONL Software packet for LabBox1 & 2 for running small continuous-processes<br />
Recommended PI-Modules<br />
Order Code Description<br />
SF-PID4 Controller module with 4 PID and application oriented controllers<br />
SF-NAMSER4 NAMUR-Driver for serial interfaces<br />
SF-ANWTAB User defined linearisation table<br />
SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />
Conti-standard Software packet for LabManager1<br />
This software package is designed for the<br />
LabManager1 for the automation of medium<br />
continuous processes. (Description, see chart<br />
above)<br />
Order Code Description<br />
SL-LABVIPKON Software packet for LabManager1 for running medium sized continuous processes<br />
Recommended PI-Modules<br />
Order Code Description (PI modules)<br />
SF-PID8 Controller module with 8 PID and application oriented controllers<br />
SF-NAMSER4 NAMUR-Driver for serial interfaces<br />
SF-ANWTAB User defined linearisation table<br />
SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />
Conti-plus Software packets for LabManager1 and 2<br />
This software package is designed for automation<br />
with the LabManager1 or 2 for large continuous<br />
processes. (Description, see chart above)<br />
Order Code Description<br />
SL-LABVIPKONP Software packet for LabManager1 or 2 for running large continuous processes<br />
Recommended PI-Modules<br />
Order Code Description (PI modules)<br />
SF-PID16 Controller module with 16 PID and application oriented controllers<br />
SF-NAMSER4 NAMUR-Driver for serial interfaces<br />
SF-ANWTAB User defined linearisation table<br />
SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 177<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
178<br />
Laboratory Automation Software<br />
EasyBatch Software packets for LabBox1 and 2 and LabManager<br />
This software package is designed for automation of<br />
small batch and continuous processes with any<br />
automation unit.<br />
(Description, see chart above)<br />
Bestellcode Beschreibung<br />
SL-LABVIPEASY Software packet EasyBatch for LabBox1 & 2 for running small batch-processes<br />
Recommended PI-Modules<br />
Order Code Description (PI modules)<br />
SF-PID4 Controller module with 4 PID and application oriented controllers<br />
SF-NAMSER4 NAMUR-Driver for serial interfaces<br />
SF-ANWTAB User defined linearisation table<br />
SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />
Batch-light Software packets for LabBox1 and 2<br />
This software package is designed for automation<br />
of small batch processes with the LabBox1 and 2.<br />
(Description, see chart above)<br />
Order Code Description<br />
SL-LABVIPBATL Software packet for LabBox1 & 2 for running small batch-processes<br />
Recommended PI-Modules<br />
Order Code Description (PI modules)<br />
SF-PID4 Controller module with 4 PID and application oriented controllers<br />
SF-NAMSER4 NAMUR-Driver for serial interfaces<br />
SF-ANWTAB User defined linearisation table<br />
SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />
Batch-economy software packets for LabBox2 and LabManager1<br />
This software package contains equipment<br />
components which are sufficient to run a laboratory<br />
reactor system in batch operation mode. An<br />
according plant, for example, is the LabKit2.<br />
(Description, see chart above)<br />
Order Code Description<br />
SL-LABVIPBATE Economy software package for LabBox2 and LabManager1 designed for batch processes<br />
Recommended PI-Modules<br />
Order Code Description (PI modules)<br />
SF-PID8 Controller module with 8 PID and application-oriented controllers<br />
SF-NAMSER4 NAMUR-Driver for serial interfaces<br />
SF-ANWTAB User defined linearisation table<br />
SF-HITUNE Auto parameterisation for temperatur controll SF-PIDxx<br />
SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
Batch-standard software packets for LabManager1<br />
This software package is designed for the<br />
automation of medium-sized batch processes with<br />
the LabManager1.<br />
(Description, see chart above)<br />
Order Code Description<br />
SL-LABVIPBAT Software packet for LabManager1 for medium sized batch-processes<br />
Recommended PI-Modules<br />
Order Code Description (PI modules)<br />
SF-PID8 Controller module with 8 PID and application oriented controllers<br />
SF-NAMSER4 NAMUR-Driver for serial interfaces<br />
SF-HITUNE Automatic parameterisation for temperature cascade controller SF-PIDxx<br />
SF-ANWTAB User defined linearisation table<br />
SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />
Batch-plus Software packets for LabManager1 or 2<br />
This software package is designed for automation of<br />
giant sized batch processes with the LabManager1<br />
and 2.<br />
(Description, see chart above)<br />
It consists of the following modules:<br />
Order Code Description (Number of Data Points)<br />
SL-LABVIPBATP Software packet for LabManager1 and 2 for giant sized batch-processes<br />
Recommended PI-Modules<br />
Order Code Description (PI modules)<br />
SF-PID16 Controller module with 16 PID and application oriented controllers<br />
SF-ANWTAB User defined linearisation table<br />
SF-NAMSER4 NAMUR-Driver for serial interfaces<br />
SF-HITUNE Automatic parameterisation for temperature cascade controller SF-PIDxx<br />
SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />
All software packages are discounted.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 179<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
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Stirring and<br />
Dispersing<br />
Services
180<br />
Laboratory Automation Software<br />
HiLIMS Laboratory Information Management-System<br />
Finally, the sure way to Retrieval!<br />
The general development towards the electronic<br />
document is becoming more and more evident. Due<br />
to the Electronic Signature Act, digitally signed<br />
electronic documents are legally equivalent to handsigned<br />
paper documents. The American FDA (Food<br />
and Drug Administration) is pushing the deployment<br />
of electronic media within documentation. Laboratory<br />
Information Management Systems (LIMS) are<br />
entering the laboratories, where they are replacing<br />
laboratory notebooks or books on paper basis.<br />
Just one irretrievable test can represent more costs<br />
than the investment in a LIMS, as patent claims can<br />
not be defended, liability claims can not be repulsed<br />
or for the simple cause that tests need to be<br />
repeated.<br />
Advantages of the Electronic Information<br />
Administration:<br />
� Support of laboratory-internal procedures<br />
� Secure retrieval of test results<br />
� Increase of productivity<br />
� Prevention of mistakes<br />
� Internal availability of knowledge<br />
� Protection of knowledge from exterior access<br />
� Protection of information from manipulation<br />
� Securing of information for re-use<br />
� Secure own claims and prevent liability claims<br />
The term LIMS covers a wide range. The LIM<br />
systems are just as varied as the laboratories they<br />
are applied in, e.g. a laboratory for medical<br />
diagnostics, a laboratory for productionaccompanying<br />
tests, or a chemical development<br />
laboratory.<br />
HiLIMS is the special LIMS for the F&E laboratory.<br />
There, next to to increasing the efficiency and<br />
shortening the „time to market“, the LIMS serves the<br />
purpose of protecting intellectual property and<br />
avoiding liability claims through electronic<br />
documentation and archiving. The last mentioned<br />
also serve to enable the fast retrieval of information<br />
gained in the tests (batch and continuous operation<br />
mode) by searching the electronic laboratory<br />
notebooks.<br />
The data of test series, parallel experiments, or<br />
freely arranged tests can be visually compared in<br />
various graphics and can be compressed in freely<br />
configurable reports. In comparison to the<br />
conventional mode of operation, it is no longer<br />
required to actually „handle“ the data. This<br />
eliminates many sources of error right from the<br />
beginning and drastically reduces the reworking<br />
periods. According to a study (CENSA 2004), the<br />
increase of productivity in the research industry due<br />
to the change to an electronic system is estimated to<br />
be 50%.<br />
A LIMS should consistently cover the complete F&E<br />
process chain from the placing of the order, over the<br />
control and attendance, right to the final report.<br />
A LIMS consists at least out of the basic modules<br />
measurement value logging and measurement value<br />
evaluation. Further modules provide for the<br />
connection of the hardware in the measuring line,<br />
the connection of the ERP systems, controlling<br />
software, data protection infrastructure etc.. LIMS<br />
can also be realised as distributed systems, so that<br />
it is possible to enter and call up data from different<br />
work places. HiLIMS can image all essential parts of<br />
a laboratory and supports both the administration of<br />
static (e.g. material data) and dynamic data (e.g.<br />
temperature progressions).<br />
Modern laboratory automation and analysis devices<br />
produce huge amounts of raw data, e.g. a recipe<br />
control system with online analytics and<br />
chemometrics, which would remain more or less<br />
useless without subsequent efficient data<br />
administration and data evaluation. For the purpose<br />
of data transfer, the EDP connection to automated<br />
laboratory reactor systems, chromatography data<br />
systems, instruments etc. is required.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Special features of the HiLIMS:<br />
Laboratory Automation Software<br />
� Fast relational SQL Database<br />
� Self-explaining User Interface<br />
� Network and Multi-User Capability<br />
� Smooth Integration in LabVision/HiBatch<br />
� R&D-oriented<br />
� Very versatile<br />
� Integrated forms and Form Designer<br />
� Integrated Data Mining, Evaluation and<br />
Reporting<br />
� Various Import and Export Possibilities<br />
The usual question whether to „Make or Buy“ does<br />
not arise any longer, as HiLIMS can be so flexibly<br />
aligned to various tasks that an individual<br />
programming is no longer cost-effective.<br />
There are virtually no limits to the integration of<br />
measurement devices, sensors and analysis devices<br />
into the measurement line. The control line can also<br />
be randomly extended by mathematical processing<br />
and evaluation of the measurement values, sample<br />
management, settlement etc..<br />
HiLIMS is the last but very important link of the<br />
processing chain consistently integrated into the<br />
LabVision/HiBatch program system. It attaches itself<br />
directly on to the data tables of the electronic<br />
laboratory notebook and the LabVision data base. I<br />
can however also be adjusted as independent<br />
program to other systems.<br />
Planning and Organising<br />
The processing chain commences with the order.<br />
The same contains the organisational data, e.g.<br />
customer, order ID, deadline, as well as the test<br />
specifications.<br />
The order form is freely configurable with the form<br />
editor. Informa tion deposited in the data base such<br />
as customer, laboratory and product, can be<br />
selected via selective lists. In addition, text fields for<br />
freely editable text, tables, and graphics can be<br />
integrated.<br />
Administration and Documentation<br />
All relevant information such as order, recipe, test<br />
parameter, measurement values, events, laboratory<br />
data or laboratory notebook are deposited in the<br />
LIMS data base in such a manner that they can be<br />
retrieved via freely configurable search queries the<br />
fastest possible way. This, beyond the better internal<br />
organisation, is useful for the securing of property<br />
rights and liability issues.<br />
The archived recipes and parameter sets can be retransferred<br />
to the HiBatch recipe control system in<br />
order to, if necessary, repeat a batch run or test<br />
program. An adjustment to special requirements,<br />
including the connection of laboratory and analysis<br />
devices, can be conducted by <strong>HiTec</strong> <strong>Zang</strong>, an<br />
external service provider or the user himself.<br />
Administration of:<br />
� Recipe data<br />
� Batch data<br />
� Educt and product data<br />
� Sample data<br />
� Documents<br />
Searching and Retrieval<br />
Due to the deployment of HiLIMS as knowledge<br />
base, the generated research knowledge is made<br />
easily accessible and the transparency is increased.<br />
A query can be established by the user either based<br />
on forms or scripts. This may contain various criteria<br />
such as organisational dates, material data,<br />
measurement values, laboratory data etc. The freely<br />
configurable search forms are self-explaining and<br />
support standard procedures. Individually configured<br />
search forms can be used as predefined search<br />
dialogues after they have been logged.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 181<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
182<br />
Elements of the Search Dialogues:<br />
Laboratory Automation Software<br />
� Organisational Data<br />
� Dates, times, time domains<br />
� Values, value ranges of measurement values,<br />
analyses data, etc.<br />
� Keywords, terms<br />
The search dialogue forms may contain search<br />
elements in random combination.<br />
The search dialogue forms can also be established<br />
by the user with the form designer. For this purpose,<br />
the required search elements are merely integrated<br />
into the form via drag and drop.<br />
As the result of a search, all data records that<br />
accord to the search query will be displayed.<br />
The user is able to remove single tests from the list<br />
and before the start of the evaluation and<br />
complement the list via the switch “Attach Single<br />
Test”, e.g. for a reference test.<br />
Alternatively a script-based (expert search) search is<br />
possible. More complex search terms can be<br />
generated via the And and Or links and by the<br />
setting of brackets.<br />
Errors in the search script will be detected and<br />
displayed.<br />
Different search scripts can be stored for later use.<br />
Evaluation<br />
The data of the tests retrieved with the search<br />
function can be evaluated in a diversity of manners.<br />
The simplest case is the direct comparison of<br />
selected variables in diagram form. For this purpose,<br />
various diagrams are available for selection, e.g.<br />
array of curves, average values with min/max bars<br />
or standard deviations.<br />
The protocol of the evaluation consists, e.g. of a<br />
cover sheet with the general information and<br />
possibly a copy of the order with the protocol pages<br />
following.<br />
The layout of the protocol pages is established with<br />
the form designer.<br />
Evaluation Possibilities:<br />
� Evaluation of test series and parallel tests<br />
� Comparative presentation<br />
� Statistical evaluation<br />
� Freely programmable evaluation<br />
The stored information such as order, recipe,<br />
laboratory notebook, report data table, raw data, can<br />
be displayed or exported as data file for further<br />
processing.<br />
Setting<br />
The master data is created with the table-based<br />
master data editor. The user is also able to create<br />
data base fields and tables himself, e.g. part<br />
numbers or materials with material data. In the<br />
course of establishing an order, in the laboratory<br />
notebook, in case of queries or when designing the<br />
report, it is now possible to immediately gain access<br />
to the created data base fields and tables via the<br />
selective list.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
User Administration<br />
In the user administration, the users are allocated to<br />
different groups such as administrator and user. The<br />
user must log in and his respectively stored data are<br />
assigned an ID.<br />
Device Coupling<br />
For the coupling of analysis devices, spectrometers,<br />
etc., there are various interfaces and protocols at<br />
disposal.<br />
� OPC<br />
� ModBus<br />
� Text data files<br />
� csv-data files<br />
� MS-Excel ® -tables<br />
� Device-DLL etc.<br />
For the coupling with other software, such as ERP<br />
and chemometrics programs, individual<br />
programming is available.<br />
Technical Data:<br />
Database<br />
System<br />
Microsoft SQL Server ® as of Version<br />
2000.<br />
Basic Version is delivered with free<br />
version of SQL-Server Express, limited<br />
to 4 GB.<br />
1 to unlimited (dependent of database<br />
server and client licenses)<br />
1 to unlimited<br />
Number of<br />
Users<br />
Client<br />
Licenses<br />
Modules - Basic Version (single-user)<br />
- Multi-user extension<br />
- SQL-Database server<br />
- User Administration<br />
- Electronic Signature<br />
- Device Driver<br />
- Client-specific adjustments to ERP<br />
Program<br />
- Client-specific adjustments to<br />
Chemometry Program<br />
HiLIMS is also available as LabVision-Module (SL-<br />
HILIMS-C) and as stand-alone software (SL-HILIMSSA-C).<br />
Order Code Description Data Point<br />
Extra<br />
Charge<br />
SL-HILIMSL Single-User License HiLIMS light Option for LabVision including local SQL-<br />
Database Volume 4 GB<br />
yes<br />
SL-HILIMSSQL-S HiLIMS Serverl License for Multi-User Version<br />
Notice: Requires additional SQL-Server License<br />
no<br />
SL-HILIMS-C HiLIMS Option LabVision<br />
Notice: Requires HiLIMS Server and also additional SQL-Client License<br />
yes<br />
SL-HILIMSSA-C Stand-alone Workplace Client (HiBuilder Version, without LabVision run<br />
capable)<br />
Notice: Requires HiLIMS Server and also additional SQL-Client License<br />
no<br />
SL-SQLSERV SQL Server License without Client Licenses no<br />
SL-SQLCLNT SQL-Client License per Workplace no<br />
HiLIMS requires eJournal.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 183<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
184<br />
PI-Firmware-Modules<br />
Laboratory Automation Software<br />
The PI firmware auxiliary modules can be used to<br />
upgrade the PI‘s for fulfilling specialist tasks, which<br />
would otherwise not be possible with the basic<br />
setup. These modules are software modules<br />
(Firmware).<br />
Controller Modules<br />
The <strong>HiTec</strong> <strong>Zang</strong> PIs can be equipped with up to 32<br />
controller modules. Next to the standard PID<br />
regulators, so-called application-oriented<br />
controllers are available for the typical procedural<br />
regulation tasks.<br />
Example for a PID Controller Parameterisation Panel<br />
for lines which are difficult to control and to achieve<br />
a special quality of control, the adaptive control<br />
module SF-HICON is available.<br />
All control parameters are passed over data points<br />
and can be dynamically re-parameterised. It is<br />
therefore possible to control non-linear lines without<br />
any problems.<br />
You can choose between Standard PID controllers<br />
and application-oriented controllers.<br />
Standard PID-Controller<br />
The smallest version of the MSRmanager controller<br />
module consists of 4 controllers.<br />
The controllers can be individually set. The type is<br />
individually selectable:<br />
� P<br />
� I<br />
� PD<br />
� PDTz (Tz = shortened D amount)<br />
� PID<br />
� PIDTz<br />
� PH (for pH-control)<br />
The controllers have the characteristics of industrial<br />
controllers such as variable regulation value<br />
limitation, auxiliary regulation value cut-in, tolerance<br />
band, jolt-free takeover, and "anti-windup"<br />
functionality.<br />
Target and actual values, auxiliary regulation values<br />
and regulation values are set via a configuration<br />
menu with the corresponding data-points<br />
(input/output). The sampling interval is adjustable<br />
with a resolution of 1/<strong>10</strong>s.<br />
The regulation value limitation works alternatively<br />
before or after the cutting in of the auxiliary<br />
regulation value and permits the specification of a<br />
maximum and a minimum for the regulation value.<br />
Starting the I-proportion in the case of longer<br />
persisting offsets is prevented (anti-windup). The<br />
specification of a tolerance band is useful when<br />
heating/cooling or regulating pH values.<br />
For the output of the regulation values digital bit and<br />
byte, pulse-width modulated and similar outputs are<br />
made use of.<br />
Since all control variables are linked with data<br />
points, cascaded or guided controller systems and<br />
special functions, e.g. dynamic limitation, mapping<br />
controller, split outputs etc., can be implemented<br />
without any problems.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Application-oriented Controllers<br />
Application-oriented controllers are controllers<br />
respectively optimised for special tasks, e.g.:<br />
Laboratory Automation Software<br />
� Batch Dosing Control<br />
� Continuous Dosing Control<br />
� Vacuum Control<br />
� pH Control<br />
� Temperature Cascade Control<br />
The application-oriented controllers are selfparameterising<br />
or are automatically adjusted by a<br />
controller optimisation program. This saves you the<br />
according time when establishing an application.<br />
The achieved control qualities can only be reached<br />
with PID controllers with a lot of effort and knowhow.<br />
With the help of application-oriented controllers, the<br />
laboratory personnel is able to solve problems which<br />
would usually require to call a control technician.<br />
Order Code Description<br />
SF-PID4 4 controller modules Type P to PIDTz and application oriented controllers<br />
SF-PID8 8 controller modules Type P to PIDTz and application oriented controllers<br />
SF-PID16 16 controller modules Type P to PIDTz and application oriented controllers<br />
SF-PID24 24 controller modules Type P to PIDTz and application oriented controllers<br />
SF-PID32 32 controller modules Type P to PIDTz and application oriented controllers<br />
Auto tuning for temperature cascade controllers<br />
With the module "HiTune", the PID controller can be<br />
automatically parameterised. This is particularly<br />
favourably for stages, whose behaviour is subject to<br />
different influences e.g. a reactor inner temperature<br />
control, which is known for instance to be<br />
dependent on the material properties, the filling level<br />
and the stirrer speed.<br />
The appropriate process applying conventional<br />
modes of operation would require at least some<br />
hours, often days.<br />
The parameterisation of the controller takes place<br />
automatically during the running up to the setpoint<br />
values. The following diagram shows the controller<br />
behaviour at different setpoint value changes.<br />
Order Code Description<br />
SF-HITUNE Automatic parameterisation for temperature cascade controller SF-PIDxx<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 185<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
186<br />
Adaptive Regulation with HiCon<br />
Laboratory Automation Software<br />
HiCon is a highly developed, fully-adaptive controller<br />
for the LAB/MSRmanager system.<br />
With HiCon you allow a first-class control<br />
engineering specialist to work for you. This also<br />
ideally regulates stages for which a PID controller<br />
cannot be parameterised satisfactorily. Also in the<br />
course of the usually demanding and timeconsuming<br />
parameterisation of the inner<br />
temperature control of reactors, HiCon proves its<br />
strength, when it comes to fast run-up with minimum<br />
overshooting.<br />
A field test, which was conducted to compare HiCon<br />
with other regulation procedures such as PID and<br />
fuzzy-controllers, showed that HiCon is superior to<br />
all other procedures.<br />
The adjusting (parameterising) of PID controllers is<br />
conducted in practice, predominantly via direct trial.<br />
This requires special experience and is, in particular<br />
with slow-acting processes such as temperature<br />
runs, extremely time-consuming and unsatisfactory.<br />
To make things worse, only a more or less<br />
acceptable regulation quality is usually obtained,<br />
which is far away from the optimum. If the process<br />
changes during the run-time, or operating pointdependently,<br />
then the controller adjustment again<br />
becomes more difficult, if not even impossible.<br />
In reagrd to all these points, the adaptive controller<br />
HiCon represents the remedy. It adapts fast and<br />
automatically to variable process properties, but it<br />
can also - as a better alternative to the PID controller<br />
- be operated with fixed parameters, by switching off<br />
adaptation after a single controller parameter<br />
optimisation.<br />
If, necessary, a later follow-up optimisation can be<br />
carried out at any time, without disturbing or<br />
interrupting the process cycle.<br />
Order Code Description<br />
SF-HICON 1 HiCon Controller module adaptive<br />
HiCon supplies an outstanding regulation quality<br />
also for processes with pure delay elements, for<br />
processes with integral components and for<br />
processes with extensive dead times, which would<br />
be difficult to control with conventional controllers, if<br />
at all. In contrast to the PID-controller, HiCon<br />
delivers an equally optimal regulation quality both in<br />
the reference (setpoint value changes) and in the<br />
interference behaviour (interference to the controlled<br />
variable).<br />
Adaptive controllers have been available for<br />
decades. They have not however become generally<br />
accepted, because their handling was complicated,<br />
their behaviour not always stable and the price too<br />
high. The results of many years of development<br />
have been put into HiCon, which was "fine-tuned" in<br />
practical tests. The result is an industry-suited<br />
adaptive controller, which is robust and easy to<br />
deploy.<br />
Outstanding advantages compared to conventional<br />
controllers:<br />
� significant time saving during controller<br />
parameterisation<br />
� principally improved regulation quality<br />
� significantly better control for processes with<br />
integral times or dead times<br />
� optimal reference and interference variable<br />
control<br />
� Online-Adaptation of variable process<br />
properties<br />
Since this controller processes substantially more<br />
information about the process than a PID controller,<br />
it is clearly superior. Its efficiency is particularly<br />
evident at stages with dead time and double<br />
integrating behaviour, which can hardly be regulated<br />
with PID controllers. After a setpoint value change<br />
or a malfunction of the process, all status deviations<br />
are reduced to zero.<br />
The regulating behaviour merely depends on one<br />
setting parameter, the controller sensitivity, which<br />
can be adjusted between 0 and <strong>10</strong>0%. The standard<br />
value for this parameter is 50% and does not have<br />
not to be adjusted for most processes. Principally,<br />
an increase of the parameter means an increase of<br />
the controller activity, i.e. the controller intervenes<br />
more often, the actuator is more agitated and uses<br />
more adjustment energy.<br />
In a PI, up to four HiCon controllers can be<br />
operated.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
IEC 61131 IL– PLC Functionality for the PI<br />
The IEC 61131 IL module and device components<br />
bring extended PLC functionality into all <strong>HiTec</strong> PIs.<br />
The IEC 61131 IL (instruction list) is a proven control<br />
language and is internationally standardised via the<br />
EN 61131. The <strong>HiTec</strong> PIs MSRmanager, MSRbox,<br />
LabManager and LabBox can independently<br />
execute control functions, i.e. without participation of<br />
the UI (work station). For this purpose, the IEC<br />
61131 IL-control language and dynamic device<br />
components are available, which can be active even<br />
with a switched off PC. Therefore, the <strong>HiTec</strong> LAB<br />
and MSR-systems fulfil the safety-relevant NAMUR<br />
category three.<br />
The Instruction List control rounds off the LAB- /<br />
MSRmanager-System and simultaneously<br />
complements the application range in the direction<br />
of larger projects.<br />
As it is implemented on the PI, it significantly<br />
increases the security and enables the programming<br />
of even the most complex security and running<br />
routines which are realised without involvement of<br />
the UI.<br />
The PI-technically oriented language statement list<br />
(IEC 61131 IL) and device components are an ideal<br />
supplement to the application technology oriented<br />
HiText control and evaluation language. Their<br />
application is recommended then, if the control<br />
functions must be executed particularly safely, thus<br />
also in case of a failure of the UI-PC, or increased<br />
requirements on the performance are demanded.<br />
It must be emphasised that IEC 61131 IL and device<br />
components are "online capable", i.e., during a<br />
running program, a modified program can be loaded<br />
into the PI, which then takes over the control at the<br />
start of the next cycle.<br />
The programs are stored permanently and safely in<br />
the FLASH memory of the PI.<br />
IEC 61131 IL has access to all PI data points.<br />
Interesting is also the possibility to implement<br />
randomly complex alarm reactions directly in the PI,<br />
which range right up to the controlled shutting down<br />
of the system, e.g. in case of UI malfunction.<br />
An IEC 61131 IL program is started automatically<br />
immediately after the switching on of the PI and can<br />
execute several thousand operations per second.<br />
By using debugging functions such as break points,<br />
single-sequence and monitored printouts, you are<br />
supported during the program development.<br />
Symbolic variables and field variables are<br />
supported.<br />
Permanent (value remains after Reset and Power-<br />
Off) and non-permanent variables are supported.<br />
Characteristics:<br />
� IEC 61131 compatible<br />
� Indirect addressing<br />
� Sub-program technology<br />
� Cyclic and continuous execution<br />
� Combinable with device components<br />
� Binary and Analogue value processing<br />
� Online download capability<br />
� Simplest data exchange with the UI<br />
� Extended Alarm processing for the PI<br />
An Instruction List program is started automatically<br />
immediately after switching on the PI and is able to<br />
realise several thousands of operations per second.<br />
The Language Elements<br />
IEC 61131 IL-control supports the following IEC<br />
61131 commands:<br />
Operator Meaning<br />
LD Load operant<br />
ST Save operant<br />
S<br />
R<br />
Set, reset, depending on operant<br />
AND<br />
OR<br />
XOR<br />
ADD<br />
SUB<br />
MUL<br />
DIV<br />
GT<br />
GE<br />
EQ<br />
NE<br />
LE<br />
LT<br />
Boolean AND<br />
Boolean OR<br />
Boolean exclusive-OR<br />
Addition<br />
Subtraction<br />
Multiplication<br />
Division<br />
Compare on „Greater than“<br />
Compare on „Greater/Equal“<br />
Compare on „Equal“<br />
Compare on „Not Equal“<br />
Compare on „Less/Equal“<br />
Compare on „Less than“<br />
JMP Jump to given code-line<br />
NOP No Operation<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 187<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
188<br />
Data Types<br />
Laboratory Automation Software<br />
Mode Type<br />
PI-Data points All types of the PI<br />
Word memory Analogue, digital 32 bit<br />
Bit memory Bool<br />
Digital-inputs direct addressed Bool<br />
Digital-outputs direct<br />
addressed<br />
Bool<br />
Constants Integer and floating points<br />
Functional Elements<br />
TP Timer Pulse<br />
TON Timer Switch-on delay<br />
TOF Timer Switch-off delay<br />
CTU Counter Counter (up)<br />
CTD Counter Counter (down)<br />
CTUD Counter Up/down Counter<br />
F_TRIG Pos. edge detecting Flip-Flop<br />
R_TRIG Pos. edge detecting Flip-Flop<br />
SR RS-Flip-Flop with priority setting<br />
RS RS-Flip-Flop with priority re-setting<br />
The number of system functional elements present<br />
amounts to:<br />
� 30 Timers<br />
� <strong>10</strong> Counters<br />
� <strong>10</strong>0 RS-Flip-Flop-Functions<br />
The optional direct addressing of the digital inputs<br />
and outputs enables accelerated access to these<br />
inputs and outputs. Additionally, this direct access is<br />
protected from faulty parameterisation or<br />
manipulation via the user interface.<br />
Used data points are easily available in all other<br />
modules of the UI and the PI; i.e. they can be<br />
connected with visualisation objects or can be used<br />
in HiText programs.<br />
The Program Editor<br />
The easy to use editor (such as the HiText-Editor)<br />
offers many debug functions such as Breakpoint,<br />
Step-Over, Trace-Into, CPU-Window, and Watch<br />
Window with value change function.<br />
Online help functions are integrated. The reserved<br />
language elements are marked and comment areas<br />
are pointed out in colour (Syntax Highlighting).<br />
Entered programs are verified for correct language<br />
application in the LabManager before being loaded<br />
and activated.<br />
Test Auxiliaries<br />
The monitoring of terms supports troubleshooting,<br />
in particular during the development phase. Here,<br />
the current values of freely selectable data points<br />
and flags are displayed and constantly updated.<br />
Instruction List - plus (structured Text)<br />
An Instruction List (IEC 61131 IL) program can be<br />
written as structured text in HiText-oriented syntax<br />
with Instruction List-Plus. The program is<br />
transformed into the Instruction List syntax before<br />
execution.<br />
An uncomplicated exchange of program parts is<br />
possible with the HiText-Editor via the clipboard.<br />
Before the actual transfer of the completed program<br />
into the LAB-/MSRmanager, a vigorous syntax and<br />
error verification is conducted.<br />
Order Code Description<br />
SF-AWL IEC 61131 IL (Instruction List)<br />
SF-AWLPLUS IEC 61131 IL (Instruction List) plus HiText oriented strucured Text<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
NAMUR - Driver<br />
Laboratory Automation Software<br />
The freely parameterisable NAMUR - driver for serial<br />
interfaces enables the linking of any laboratory<br />
devices and analysers via serial interfaces of the PI,<br />
as long as the interface protocols of these devices<br />
principally accord to the NAMUR recommendations<br />
NE28.<br />
A serial interface can be split up logically into several<br />
channels. The individual channels are respectively<br />
addressed via their own data points. Furthermore,<br />
there is the possibility to connect bus capable<br />
devices.<br />
In the configuration table, the interface parameters<br />
out of the respective equipment manual are<br />
transferred.<br />
Order Code Description<br />
SF-NAMSER4 NAMUR-driver for 4 serial interfaces on the PI<br />
SF-NAMSER8 NAMUR-driver for 8 serial interfaces on the PI<br />
SF-NAMSER16 NAMUR-driver for 16 serial interfaces on the PI<br />
SF-NAMSER32 NAMUR-driver for 32 serial interfaces on the PI<br />
SF-NAMSER64 NAMUR-driver for 64 serial interfaces on the PI<br />
SF-NAMSER128 NAMUR-driver for 128 serial interfaces on the PI<br />
SL-PNKNAMSERA NAMUR-Driver for serial interfaces of the UI<br />
Example: An interface configured for a stirrer allows:<br />
� Setting of required speed<br />
� Requesting the current speed<br />
� Monitoring of error status<br />
As template a changable "general NAMUR device"<br />
is available. Here Inputs and Outputs need to be<br />
defined. The defined device can be used as<br />
template for a device component.<br />
Certain "external devices" where generated using<br />
this technology (eg. Knauer pumps, Heidolph<br />
stirrers) and need this device driver to work properly.<br />
For predetermined parameterisations for lab devices see „Driver Programs for Lab Devices“.<br />
User Tables<br />
Next to the standard linearisation tables for<br />
thermocouples, etc., firmly implemented in the PI<br />
and LAB PIs, up to four personal linearisation tables<br />
can be defined by the user. These are called user<br />
tables.<br />
With the help of a user table, a function can be<br />
described discretely using sampling points. A<br />
function is described, by entering the 64 equidistant<br />
sampling points between the smallest and largest<br />
values of the input into a table.<br />
Order Code Description<br />
SF-ANWTAB User defined linearisation tables<br />
Data logger function for PI<br />
The data logging module for Lab/MSR Manager and<br />
the Lab/MSR Box PI stores the resulting data in<br />
case of a failure of the UI. As soon as the UI is back<br />
online, the data is automatically transferred to the<br />
UI.<br />
Order Code Description<br />
SF-DATLOG Data logger module for <strong>HiTec</strong> PIs<br />
A selection between characteristic curve,<br />
thermoelement and resistance sensor can be made.<br />
In this way, devices can be linked without any<br />
problems even if their characteristics are only<br />
available as tables.<br />
Equipped user tables can later be used as interface<br />
type when defining a new data point.<br />
Technical Data:<br />
512 kB memory, page administration up to 64 kB,<br />
roll memory.<br />
Storage of up to 32.000 events.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 189<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
190<br />
Laboratory Automation Software<br />
HiBuilder Data Evaluation and Presentation<br />
Decisive for the development of HiBuilder was the<br />
demand by many users for a program that combines<br />
the easy handling of the table-oriented programs<br />
with the practically unlimited possibilities of a high<br />
level language compiler and in addition offers a<br />
publication-suitable graphical presentation for the<br />
technical-scientific documentation.<br />
HiBuilder distinguishes itself through the following<br />
performance features:<br />
� Online Coupling for Data Collection<br />
(LabVision)<br />
� Unproblematic Handling of even greatest Data<br />
Quantities<br />
� Super fast Arithmetics<br />
HiBuilder offers an enormous functionality:<br />
� HiText Syntax for randomly complex<br />
Evaluation Programs and Work Sheets<br />
� Publication-suitable graphical Presentation<br />
� Form Generator for Dialogue forms ,<br />
Protocols and Reports<br />
� Data Editor for Data Selection and Reduction<br />
� Signal Processing<br />
� Mathematical and statistic Functions<br />
� Windows Copy Function for Tables,<br />
Diagrams, and Forms<br />
� Data Export and Import for MS-EXCEL,<br />
Databases etc.<br />
HiBuilder can be coupled online via network with the<br />
PMC computer, so that the current process data is<br />
available at the work place without delay. With<br />
HiBuilder, it is possible to establish complete<br />
evaluation programs with the comfortable Windows<br />
user interface with only a fraction of the usual time<br />
expenditure. For this purpose, dialogue elements,<br />
e.g. input fields, buttons, option buttons etc. are<br />
available. Examples are the RAMOS Software,<br />
LiquiMaster, DosiMaste, KalDas etc.<br />
�<br />
Calculating sheets in HiText-Syntax enable even the<br />
most complex calculations to be conducted in a<br />
clear manner.<br />
The graphical presentation accords to the general<br />
perception in regard to the form of diagrams<br />
contained in technical-scientific publications.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Laboratory Automation Software<br />
Preconditioned diagram layouts can be randomly<br />
adjusted according to the requirements. A freely<br />
editable value table is attached to every diagram.<br />
Diagrams can be transferred to plotters, matrix, inkjet<br />
or laser printers, imported by a word processing<br />
or a DTP-program and post-edited under Windows<br />
with graphics programs e.g. CorelDraw or Designer.<br />
The monitor display accords exactly to the print<br />
document (WYSIWYG Principle).<br />
The design possibilities of the diagrams are varied:<br />
� Free axes allocation of the values , xy- or xt-<br />
Presentation<br />
� Various line types, colours and thicknesses,<br />
error bar presentation, and various plot<br />
symbols<br />
� Freely placeable axes<br />
� Scaling linear, logarithmic and automatic<br />
� Coarse and fine raster, extra raster,<br />
subsidiary lines<br />
Order Code Description<br />
SD-HIBUILDER Program for Data Evaluation and graphical Presentation.<br />
The legend and the explanatory text can be placed<br />
freely. There is a data table to every diagram.<br />
Modifications to the table are directly assumed by<br />
the graphics.<br />
With the help of the Form Generator it is possible to<br />
establish protocols and self-calculating forms.<br />
In this manner, you can equip your evaluation<br />
programs with an appealing and easy to handle user<br />
interface.<br />
The graphic and the table values can now be<br />
assumed by a word processing program, e.g. MS-<br />
Word, via the Windows clipboard and consequently<br />
integrated into a report in an uncomplicated manner.<br />
The applications mentioned here only represent a<br />
small section of the various possibilities of HiBuilder.<br />
The calculating sheets and the statistic functions<br />
especially aligned to the measurement value<br />
evaluation open the user the opportunity to realise<br />
the automation of evaluations of virtually any<br />
complexity.<br />
With this, HiBuilder closes the currently demanded<br />
consistent data chain reaching from the sensor up to<br />
the presentation. There is no more chance for<br />
(careless) mistakes. This will save you time and<br />
money as well as trouble.<br />
For examples for the application of HiBuilder, see<br />
the chapters Reaction Calorimetry, Services, and<br />
Application Programming.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 191<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
192<br />
Laboratory Automation Software<br />
RI-CAD the CAD-Software for P&ID-flow diagrams<br />
RI-CAD is available as stand-alone Software for<br />
Windows and as LabVision module.<br />
It is used to establish control flow diagrams without<br />
the necessity of longer familiarisation periods.<br />
RI-CAD was especially developed for drawing<br />
control flow diagrams according to the EN ISO<br />
<strong>10</strong>628 standard.<br />
In the tool palette you will find all the necessary<br />
drawing tools.<br />
This tool can also be expediently put to use during<br />
the planning stage for the standard-conform drawing<br />
of the plant.<br />
The library elements contain additional information<br />
which can be freely expanded by e.g. suppliers or<br />
with maintenance information.<br />
Universities and other educational institutions<br />
can apply for a free of charge RI-CAD licence,<br />
including the EN ISO <strong>10</strong>628 library!<br />
Order Code Description<br />
SL-RICAD P&ID-Editor stand-alone Software to create control flow diagrams.<br />
Laboratory Components Library<br />
The library SL-BIBRILK for the P&ID-Editor contains<br />
presentations of the components in a laboratory<br />
reactor system which are more detailed and more<br />
realistic than in the EN ISO <strong>10</strong>628 library for the<br />
P&ID-Editor.<br />
Here you will find glass reactors in varying<br />
construction versions and sizes and glass devices<br />
like reflux separators, coolers, containers, etc. also<br />
other lab devices graphically presented.<br />
Order Code Description<br />
SL-BIBRILK Glass and lab devices library for P&ID-Editor<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Here you will find:<br />
Plant Construction and Miniplant Technology<br />
� Customised Reaction Equipment<br />
� Customised Parallel Reactor Systems<br />
� Customised Reaction Calorimeters<br />
� Customised Formulating Stations<br />
Note:<br />
Plant components can be found under<br />
• Equipment and Components,<br />
• Process Analytics and Sensors,<br />
• Dosing Systems and Pumps,<br />
• Stirring and Dispersing,<br />
• Liquid Handling and Autosampler.<br />
Individually manufactured laboratory robot system can be found under Liquid Handling and Autosampler.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 193<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
194<br />
Plant Construction and Miniplant Technology<br />
The demands in chemistry are different everywhere.<br />
For this reason, there exists no such thing as the<br />
universal plant. Wherever the properties or<br />
possibilities of our Standard Laboratory Reactor<br />
Systems are not convenient or sufficient, this calls<br />
for the deployment of our LabKit systems<br />
customised according to client specifications:<br />
� customised reactor apparatus<br />
� customised reaction calorimeters<br />
� customised formulation devices<br />
A LabKit Laboratory Reactor System is individually<br />
designed to your specific requirements and<br />
commissioned turnkey-ready by our project<br />
engineers directly in your company.<br />
We manufacture LabKit Systems like:<br />
� Laboratory Installations<br />
� Bench Plants<br />
� Mini Plants<br />
� Pilot Plants<br />
They are applied for product and process<br />
development, process optimisation, etc.<br />
Characteristics:<br />
� Client-specific Solutions<br />
� Single and Multi Reactor Systems<br />
� Batch, Semi-Bacth or continuous Operation<br />
� Fully automated<br />
� Various possibilities for Upgrades<br />
Advantages<br />
� perfectly fitted to your needs<br />
� open system with easy handling<br />
� continuously expandable<br />
� space-saving installation<br />
� electrically lifted reactor vessel<br />
� optimal usage of the laboratory‘s capacity by<br />
operating 24 hours<br />
� best reproducibility<br />
� increase in quality<br />
� relief from routine jobs<br />
� reducing the risk of accident<br />
� GLP-compliant documentation<br />
� accessible via network, e.g. from the office<br />
� remote maintenance (dial-up by customer)<br />
Possibilities<br />
� single and multi stage syntheses<br />
� distillation reflux<br />
� crystallisation<br />
� polymerisation and polycondensation<br />
� hydrogenation with consumption measurement<br />
� reaction calorimetry<br />
� temperature, pressure, and vacuum control<br />
� dosing of solids and gases<br />
� dosing liquids, gravimetric and volumetric with<br />
pumps or with gas pressure via valves<br />
� continuous weighing of distillate<br />
� titration<br />
� phase separation<br />
� stirrer RPM control and torque measurement<br />
� regulation the pH basic and/or acid<br />
� controlling the recipe compliant with the NAMUR<br />
basic operational concept<br />
� coupled multi reactor systems<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Plant Construction and Miniplant Technology<br />
Construction example: LabKit double jacket reactor system each<br />
with a three-jacket glass reactor for deep temperature handling up<br />
to -80°C reactor inside temperature, with freeze desalination and<br />
dosing unit for gases at -90°C, three volumetric and one<br />
gravimetric dosing circuits, inerting system with electronic reactor<br />
lift.<br />
LabKit Modules<br />
You have the choice between different mounting<br />
frames, vessels, gadgets, and other components for<br />
instrumentation and automation.<br />
The composition of a laboratory system with single<br />
components, like pH dosing controller, vacuum<br />
controller, data acquisition, master control (e.g. PLC)<br />
etc. was regarded the best equipment during the last<br />
years. It is the limits of these conventional systems<br />
where LAB-Kit shows its superiority due to its<br />
NAMUR-compliant automation based on the<br />
LabManagersystems.<br />
The following summary shortly depicts some of the<br />
modules. More detailed descriptions of the same<br />
can be found in other chapters.<br />
Frames<br />
The frames are made of anodised aluminum square<br />
profiles and/or round profile high-grade steel.<br />
Optionally, an electrical lifting device for the reactor<br />
can be installed.<br />
Reactors<br />
Verfügbar sind Glasgefäße, auch spezielle Anfertigungen<br />
von <strong>10</strong>0 ml bis <strong>10</strong>0 l, in unterschiedlichen<br />
Bauformen, mit Einfach- oder Doppelmantel. Deckel<br />
mit Öffnungen nach Bedarf. Für höhere Drücke sind<br />
geprüfte Glasreaktoren oder Edelstahl- und Hastelloygefäße<br />
von 20 ml bis 20 l verfügbar.<br />
Cooler, reflux seperator etc. custom-made products<br />
on demand.<br />
Stirrer<br />
The torque signal delivers substantial additional<br />
information for processes which are associated with<br />
viscosity modification. In many cases, the torque<br />
signal, which is easily traceable, can be consulted<br />
as a indicator for the product quality.<br />
The ViscoPakt torque measuring stirrer is a stirrer<br />
drive with a high torque, with speed regulation and<br />
torque monitoring. It has outstanding measuring<br />
accuracy (see ViscoPakt). Anchor, beam, or<br />
propeller stirrers can be used. In special cases, the<br />
torque can be transmitted by a magnetic clutch.<br />
Heating/Cooling System<br />
Heating-/cooling thermostats in different versions<br />
made by Huber and Julabo, as well as other<br />
manufacturers, can be used within a range of -80 to<br />
+300 °C. Alternatively, a regulated rod heater or<br />
heating mantle or a cooling coil can be deployed.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 195<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
196<br />
Dosing Systems<br />
Plant Construction and Miniplant Technology<br />
The LabDos peristaltic pump is the cost-effective<br />
solution for the volumetric dosing of liquids. For<br />
precise dosing of smallest amounts and under high<br />
pressure the SyrDos dosing system is availble.<br />
For higher demands, gravimetric dosing with<br />
GraviDos or laboratory scales with dosing pump is<br />
advisable. The innovative GraviDos dosing system is<br />
first choice for gravimetric dosing even for high<br />
pressure dosing.<br />
For special cases (exothermic reactions, risk of<br />
clumping due to crystallization...), time profiles can<br />
be programmed. The dosing process can also be<br />
linked with other variables (e.g. temperature, pH...)<br />
or integrated into control circuits.<br />
Gases can be valve-controlled, or alternatively, be<br />
proportioned via dosing pumps, balances, load cells<br />
or mass flow meters.<br />
For hydration purposes the hydration unit VL-<br />
HICLAVE-HYDR is available.<br />
<strong>HiTec</strong> <strong>Zang</strong> solids doser SoliDos is suited for dosing<br />
of free flowing solids.<br />
Pressure/Vacuum<br />
The glass reactors can generally be used in<br />
pressure ranges from vacuum to slight over<br />
pressure. Special designs, e.g. 2 L reactors made<br />
for up to 5 bar over pressure are possible. The<br />
required work protection equipment can optionally<br />
be provided.<br />
For pressure measurements, proven piezo-resistive<br />
pressure sensors with stainless steel diaphragms<br />
are used. For more precise measurement during<br />
vacuum operation, a tandem sensor system with<br />
measurement range switching can also be used.<br />
Over the entire pressure range, the internal pressure<br />
can be regulated very exactly with suitable sensor<br />
and valve configurations. The setpoints values are<br />
precisely reached and held within a short time.<br />
Control takes place with proportionally controlled<br />
solenoid valves.<br />
For the vacuum range up to approximately <strong>10</strong> mbar,<br />
we mount vacuum systems, chemical membrane<br />
pumps. For low pressures, we deploy rotary vane<br />
pumps. We principally equip vacuum systems and<br />
pumps with a cold-trap (chargeable with (dry) ice).<br />
Automatic Sample Bottling<br />
Samples can be drawn automatically or processcontrolled<br />
and subsequently bottled with an<br />
AutoSam sample collector.<br />
Aditional liquid-handling operations and downstream<br />
processing can be realised..<br />
Options, Extensions<br />
In-Situ sensors for the filling level, turbidity, flow rate,<br />
pH, Redox, etc. Connection of analysers for<br />
sophisticated control strategies, coupled multireactor<br />
systems and many client-specific plants.<br />
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Materials<br />
Plant Construction and Miniplant Technology<br />
Borosilicate glass, PTFE, PFA, Kalrez and highgrade<br />
steel are mainly used as standard materials. If<br />
required, other materials can be deployed.<br />
Automation<br />
LabManager(and LabBox) provide the necessary<br />
interfaces for connection of the laboratory devices,<br />
sensors and actors, reaching from the temperature<br />
sensor to the dosing pump, to the proven connection<br />
boards with NAMUR-conform connections.<br />
The devices are able to replace the electronics of<br />
various individual devices of the conventional<br />
laboratory automation, such as doser, controller, pen<br />
recorder, titrators, transducers, data loggers etc.<br />
Predefined project modules for basic functions, e.g.<br />
Dosing, Tempering, Vacuum Control, etc, also<br />
enable the user inexperienced in automation<br />
applications to establish a fully automated<br />
application within a short period of time.<br />
Application-oriented controllers for dosing, vacuum,<br />
pH, temperature, etc. , ideally accomplish their tasks<br />
and do not require expert knowledge for<br />
parameterisation.<br />
Visualisation<br />
With LabVision, the plant can be operated and<br />
monitored from the display; recipes can be<br />
established, values monitored etc.<br />
Recipe Control<br />
For a versatile recipe control and management<br />
either the table based EasyBatch or HiBatch with a<br />
grafical recipe editor and its extensive basic unit<br />
operation library are available.<br />
Evaluation and Presentation<br />
The LabVision module HiText enables evaluation<br />
already during the runtime of a process.<br />
The electronic laboratory journal eJournal presents<br />
all relevant test parameter and data.<br />
The laboratory journal protocols are deposited in the<br />
data base of the Laboratory Information<br />
Management System HiLIMS and can easily be<br />
retrieved and consolidated to reports.<br />
Reaction Calorimetry<br />
During almost all exothermal and endothermal<br />
processes, the signal of the current heat output<br />
provides additional information about the reaction<br />
process, the merit of which is still often<br />
underestimated.<br />
Further information can be found in the chapter<br />
Custom Reaction Calorimeter.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
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Technology<br />
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Components<br />
Process Analytics<br />
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Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
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Stirring and<br />
Dispersing<br />
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198<br />
Plant Construction and Miniplant Technology<br />
LabKit Custom Reaction Equipment<br />
The modular LabKit assembly system enables the<br />
customer-specific construction of laboratory and<br />
miniplant plants wherever the standard systems are<br />
not sufficient. A base frame made of aluminum or<br />
high-grade steel aligned to the available space is<br />
equipped with the respectively required process<br />
hardware, instrumenting and automation<br />
components.<br />
Summary LabKit Module<br />
Notice: You can find information regarding the<br />
standard laboratory systems LabKit-ALR1, LabKit-<br />
ALR2, LabKit-rcf, LabKit-rcb, and LabKit.ed in the<br />
chapter Automatic Laboratory Reaction systems.<br />
The PI and suited software packages must be<br />
arranged according to the equipment and the<br />
desired level of automation.<br />
Base Frame Anodised square aluminum profile, high-grade steel collecting tray, power<br />
distribution. Optional high-grade steel round profile with powder-coated<br />
connecting elements.<br />
Reactors Standard glass vessels from <strong>10</strong>0ml up to 50 litres with tempering jacket, optional<br />
vacuum jacket, or O-ring sprinkler, manual or automatic bottom discharge valve,<br />
cover with sockets according to requirements and feasibility, custom designs<br />
according to customer specifications, high-grade steel up to 300 bar, special<br />
materials.<br />
Lowering Device Electric lifting device for the reactor with manual switch.<br />
Stirring Drives ViskoPaktxx and ViskoPakt-rheoxx precision stirring drives with RPM control and<br />
torque measurement.<br />
Stirring Blades Propeller, turbo, blade, and anchor stirrer can be selected. Other type and special<br />
designs available upon request.<br />
Dosing, gravimetric Gravimetric dosing with GraviDos (controlled dropping funnel) or via dosing pump<br />
(e.g. <strong>HiTec</strong> <strong>Zang</strong> LabDos) and laboratory scales.<br />
Dosing, volumetric Dosing with membrane pump, dosing with peristaltic pump (see chapter<br />
Instrumenting , Pumps).<br />
Dosing Minute Dosing with syringe doser or LabDos peristaltic pump (see chapter Instrumenting,<br />
Quantities<br />
Pumps).<br />
Gas Dosing Gas dosing via Mass-Flow-Controller.<br />
Sequential Multi-Dosing 2/3 – way or multi-way valve for the selection of the feed tank.<br />
via Scales<br />
Solid Dosing, volumetric SoliDos solids doser.<br />
Solid Dosing,<br />
SoliDos solids doser combined with GraviDos.<br />
gravimetric<br />
Heating/Cooling Heating/Cooling thermostats manufactured by Huber, Julabo, Lauda etc. with<br />
Systems<br />
connection to the LAB-xxx PI.<br />
Sensors Temperature sensor for: reactor, thermostat, supply line, reflux and steam. Interior<br />
pressure, pH value, vacuum up to 2.5 bar and working temperature up to 130°C.<br />
Redundant monitoring of the jacket temperature with shut-down function.<br />
Pressure Measurement, Pressure pick-up 0-1.6 bar absolute, others available upon request.<br />
simple<br />
Pressure Measurement, Tandem pressure pick-up system for increased precision in the vacuum range 0-<br />
tandem<br />
250 mbar/1.6 bar absolute.<br />
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Plant Construction and Miniplant Technology<br />
Continuation Summary LabKit Module<br />
Vacuum Control Laboratory vacuum system with chemical-resistant vacuum pump < 8mbar<br />
absolute, suction-side separator, cold trap, relief valve, lock valve (PVDF/Kalrez).<br />
Other vacuum systems available upon request.<br />
Pressure Control Pressure control module (Standard up to 1,6 bar) combined with inerting. Venting<br />
/Inerting<br />
valve and air relief valve with control. .<br />
Pressure Relief Spring-loaded ball and socket relief valve made of glass for unpressurised<br />
systems closed against atmosphere. Bursting disc for pressure systems. Safety<br />
valves.<br />
Inerting, simple Inerting (only for unpressurised systems with venting, otherwise, pressure and<br />
safety monitoring is necessary). Vent valve with control. Optional pressure relief<br />
valve with control.<br />
Reflux Separator Vacuum-jacketed reflux separator with electrically controllable reflux separation<br />
ratio (see chapter Equipment and Components, Reflux Separator).<br />
Reflux Cooling Intensive reflux condenser made of borosilicate glass.<br />
Optional lock valve for the cooling water. Cooling water monitoring with rotary<br />
flowmeter.<br />
Distillation Glass reflux separator with electrically controllable reflux separation ratio (see<br />
chapter Equipment and Components, Reflux Separator), vacuum jacket, silvercoated<br />
with viewing window (optional), NSH+K 29/32 with PT<strong>10</strong>0 connection,<br />
distillate collecting scales, 2/2- way shut off to separate the distillate collecting<br />
tank from the distillate flow and from the venting.<br />
Phase Separation Automatic phase separation in the bottom discharge valve.<br />
pH Control, Titration Two AlfaDos dosing systems (optional GraviDos or dosing pumps) for acid and<br />
base with pH control module.<br />
Sampling Automatic sampling optionally on the basis of a valve cascade (for a small number<br />
of samples), a multi-way valve (for a medium number of samples), sample<br />
collector (see chapter Liquid Handling and Sample Drawing, AutoSam) or a<br />
pipetting robot (for large numbers of samples).<br />
Reaction Calorimetry Heat-flow calorimetry, heat balance calorimetry, online (option), calibration<br />
heating.<br />
Extended Temperature Extension of the heating/cooling system and the sealing materials to accord to<br />
Range<br />
lower or higher temperatures available upon request.<br />
Materials <strong>Main</strong>ly borosilicate glass, PFA, PTFE, ETFE, PVDF, seals in contact with media<br />
out of Kalrez, high-grade steel material 1.4571 (subject to modification)<br />
Special solutions available upon request.<br />
Multiple examples of our plant construction can be found on our website www.hitec-zang.de.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
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Autosampler<br />
Stirring and<br />
Dispersing<br />
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200<br />
Plant Construction and Miniplant Technology<br />
Custom Parallel Reactor System<br />
Custom-made Parallel Reactor System for crystallisation<br />
screening with turbidity sensor. Joint heated dosing vessel.<br />
The general development is moving towards<br />
increasingly smaller volumes and to parallel<br />
preparations. We dispose of experience in parallel<br />
reactor systems reaching from the ml to the litre<br />
scale, and from 4 to 48 reactors. Experience has<br />
taught us that these systems must also meet<br />
individual requirements. For this reason, there is no<br />
such thing as “the” reactor parallel system.<br />
Application<br />
� Parallel Syntheses<br />
� Active Ingredient Screening<br />
� Bioprocess Monitoring etc.<br />
In addition to our standardised parallel reactor<br />
systems MultiLab and MiniLab, we also construct<br />
client-specific parallel reactor systems for all<br />
possible kinds of application.<br />
Your Advantages<br />
� Individually designed<br />
� Various possibilities<br />
� Reators reaching from the ml to the litre scale<br />
� Adapted Dosing Technology<br />
� Adapted Stirring Technology<br />
� Adapted Tempering Technology<br />
Further examples for Parallel Reactor Systems:<br />
Fourfold parallel reactor system with 250ml double jacket reactors<br />
for deep temperature synthesis and sample taking.<br />
Threefold parallel reactor system with 2 l reactors, parallel,<br />
selective dosing from the receiver tanks a, b and p.<br />
Parallel reactor systsm with 2 reactors<br />
and MultiLab tempering system.<br />
Further examples for parallel reactor systems can be<br />
found on our website.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Plant Construction and Miniplant Technology<br />
Custom Reaction Calorimeters<br />
Customer specific reaction calorimeter with heated cover and<br />
front side special nozzle.<br />
Next to the standard reaction calorimeters LabKit-rcf<br />
and LabKit-rcb, <strong>HiTec</strong> <strong>Zang</strong> also offers customised<br />
calorimeters. <strong>HiTec</strong> <strong>Zang</strong> also modernises existing<br />
calorimeters.<br />
Up to now, reaction calorimeter and laboratory<br />
reactors which can perform more than simple<br />
syntheses needed to be regarded separately. <strong>HiTec</strong><br />
<strong>Zang</strong> LabKit-rc reaction calorimeters combine the<br />
two devices, which leads to a flexible system<br />
versatile in every aspect. As a calorimeter, the<br />
LabKit-rc offers various operational modes and<br />
measuring methods, as laboratory reaction system,<br />
the complete flexibility of the LabKit laboratory<br />
reaction technology and the LabManagerresearch<br />
process control system.<br />
Next to the classic deployments in the security<br />
laboratory, the reaction calorimetry is increasingly<br />
also establishing itself as an effective method within<br />
process development and process optimisation. For<br />
selective reaction control and risk analysis of<br />
chemical reactions, it is necessary to know the<br />
reaction heat output and the respective temporal<br />
progression at operational conditions.<br />
The following components are available:<br />
� Precision Temperature Measurement Module<br />
� Calibrated Temperature Sensors<br />
� Flowmeter for Heat Carriers<br />
� Controllable proportional Calibration Heating<br />
� HiCon adaptive Controller for ideal isothermal<br />
effect<br />
� Basis Operation Calorimetry with Online<br />
Evaluation<br />
� KalDas Evaluation Software for Heat Flow and<br />
Heat Balance Calorimetry<br />
You will find a detailed description in the chapter<br />
Components for Reaction Calorimetry. The<br />
application possibilities are various and go far<br />
beyond the classic measurement of the heat tone<br />
and thermal conversion.<br />
For the dimensioning of cooling systems, reliable<br />
data regarding the energy potential of a reaction<br />
mixture, as well as the heat transfer rate and the<br />
properties and/or the heat storage capability must be<br />
at hand, this often in dependency of the mixture and<br />
temperature.<br />
The reliable evaluation of complex chemical<br />
processes requires variable test equipment, which<br />
can be aligned to the conditions of the process<br />
intended for examination.<br />
For this reason, the systems can be arranged in<br />
such a manner that all functions of the laboratory or<br />
operational assembly can also be realised in the<br />
calorimeter.<br />
Examples for our customised recation calorimeters<br />
can be found on our website.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Equipment and<br />
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202<br />
Plant Construction and Miniplant Technology<br />
Components for Reaction<br />
Calorimeters<br />
These modules will enable you to upgrade your<br />
default reactor systems to a reacton calorimeter and<br />
thus making it possible to receive additional<br />
important and significant values within the an early<br />
stage of the process develeopment. Constraints to<br />
the functionality and the experiments will nearly not<br />
occur.<br />
Easy Evaluation<br />
You will find an evaluation program for heat flow and<br />
heat balance calorimetry which can be adapted to<br />
any device in the chapters Reaction Calorimetry/<br />
Calorimetry Evaluation Program KalDas.<br />
Calibration Heater<br />
A calibration heater is required for calorimetric<br />
measurements at laboratory reactors.<br />
In particular for the establishment of the heat<br />
capacity of a material within the scope of a heat flow<br />
calorimetry, a very precise calibration heating is<br />
required, which corrects changes of the heating<br />
resistor, e.g. due to deterioration and temperature<br />
influences. For further information see chapter<br />
Components for Reaction Calorimetry.<br />
Thermostats<br />
Reaction calorimeters require thermostats with high<br />
cooling capacity and low thermal mass.<br />
We will gladly advise you to help to find the device<br />
best suited to your requirements.<br />
Temperature Control<br />
For isothermal calorimeter operation, exceptionally<br />
effective cascade controllers are required. You will<br />
find suited controllers in the chapter Laboratory<br />
Automation Software in the section controller<br />
modules.<br />
Temperature Measurement with maximum<br />
Precision<br />
This high precision temperature measurement<br />
module meets the highest requirements in terms of<br />
resolution and measurement precision. You find<br />
detailed information in the chapter Laboratory<br />
Automation Hardware,under cards, HK-AD24P8.<br />
Sensors for the Reaction Calorimetry<br />
Sensors that accord to the particular high demands<br />
of reaction calorimetry can be found under LAB-PI<br />
Interfaces/Precision-Pt<strong>10</strong>0 Inputs.<br />
Turbine-Flow Sensors for Heat Carrier Oil<br />
The heat balance calorimetry requires the exact<br />
measurement of the flow rate of the heat carrier oil.<br />
These flow sensors (IS-F-TDM...) are especially<br />
suited for this purpose and are frequently used as an<br />
alternative to the significantly more expensive and<br />
more voluminous Coriolis mass flowmeters.<br />
Measurement Stirrer<br />
The heat incorporated by the stirring can be<br />
measured with the high-resolution ViskoPakt rheo<br />
stirring drives. You will find further information in the<br />
chapter “Stirring and Dispersing”.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Plant Construction and Miniplant Technology<br />
Formulation and Handling Stations<br />
The programme-controlled formulation stations are<br />
used for the automatic establishment and<br />
adjustment of formulations to certain target variables<br />
such as final volume and viscosity. The required<br />
basis operations, e.g. filling with liquids and solids,<br />
stirring, measuring, dosing etc., are executed<br />
programme-controlled. This consequently leads to<br />
varied applications in the chemical, pharmaceutical,<br />
biotechnical, cosmetics and food industry. Due to the<br />
availability of custom designs and the flexible<br />
automation system, the hardware and software<br />
application possibilities are virtually unlimited.<br />
The devices are arranged by combing the different<br />
components of our mechatronic modular system<br />
with our laboratory automation systems, laboratory<br />
devices and our sensor/actor components.<br />
The processes are programmed with the selfexplaining<br />
script language HiText or the graphic<br />
sequential function chart HiBatch. For this reason,<br />
they can be easily adapted to modified conditions by<br />
the user. The protocols can be automatically<br />
established. The protocol layout can be flexibly<br />
designed.<br />
The protocols can be automatically stored in the<br />
data base of the HiLIMS Laboratory Information<br />
Management System. HiLIMS supports the<br />
uncomplicated and efficient administration of all<br />
parameters and data.<br />
With the help of freely establishable search queries,<br />
the protocols are quickly retrieved when needed.<br />
Drehtellertyp<br />
The presented formulation station produces up to 8<br />
formulations fully automatically in exchangeable<br />
containers with a volume reaching from 1 to 5 litres.<br />
The user charges the tray before the test-start with<br />
stirring tanks that contain a random sample amount.<br />
Linear Type<br />
As an alternative to the formulating stations based<br />
on rotary plates or AutoSam sample collectors, a<br />
After the start of the test, the predefined samples are<br />
adjusted exactly to the predefined viscosity and<br />
target amount by adding doses of certain educts in<br />
consecutive order. The stirrer is cleansed<br />
automatically to ensure contamination is excluded.<br />
Due to the high-resolution torque coverage of the<br />
ViscoPakt-X7 torque measurement stirrer, it is<br />
possible to reach ideal reproducibility and therefore<br />
a consistent product quality during different tests.<br />
In comparison to the manual procedure conducted<br />
in the past, the automatic formulation usually leads<br />
to time saving in regard to the test period of 70 %,<br />
and 80 % in regard to the handling period. The payback<br />
period of the plants is accordingly short. To be<br />
stated as additional advantages are the increased<br />
reproducibility and product quality, as well as the<br />
automatically established documentation.<br />
The required sensor system can be fully integrated<br />
and enable measurement directly in the tanks. In<br />
comparison to the in situ sensor system, the<br />
measurement sensor is spared and can be easier<br />
exchanged and calibrated.<br />
Properties<br />
� Flexible Construction<br />
� Comprehensive Tank Selection<br />
� Fully automated<br />
� Freely programmable<br />
� Flexible Sensor System<br />
� Short Pay-Back Period<br />
Please note the versatile xyz-robots in the chapter<br />
Liquid Handling.<br />
pneumatically driven linear type is available for<br />
special applications.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
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Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
204<br />
Plant Construction and Miniplant Technology<br />
Special Application Cases<br />
� Ex- Zone<br />
Components<br />
Viscosity Measurement<br />
Precision measurement stirrers of the ViscoPakt-<br />
Rheo Series enable a in situ measurement of the<br />
viscosity and, with the help of the automatic fluid<br />
handling system, e.g. the automatic adjustment of<br />
the viscosity. In particular low viscous media, can be<br />
measured with the ViscoPakt-Rheo X7.<br />
Further components of our Miniplant Technology:<br />
� Laboratory Scales<br />
� Reactor Weighing<br />
� Electric Bottom Discharge Valves<br />
� Automatic Liquid Phase Separation<br />
� Valves and Shut-Offs<br />
� Multi-way Valves<br />
� Little available Construction Depth<br />
Properties<br />
� Pneumatic Drive<br />
� Bottling of sampling bottles. Bottle size 250 ml<br />
(plastic or glass, other sizes available upon<br />
request.<br />
Options<br />
� Programme-controlled handling of liquids and<br />
solids.<br />
� Automatic Sensor System (pH, RedOx,<br />
conductivity, ion-selective electrodes,<br />
turbidity, pO2, viscosity, in situ spectroscopy).<br />
� LIMS Coupling<br />
Technical Data (ViscoPakt-Rheo X7)<br />
MaximumTorque 7Ncm<br />
Resolution 0,003 Ncm<br />
Reproducibility 0,05 Ncm<br />
Minimum RPM 40U/min<br />
Maximum RPM 3000 u/min<br />
Uncertainty RPM 0,1 %<br />
Chuck 1-<strong>10</strong>mm<br />
Drive Weight ca. 900g<br />
Diameter Motor 70mm<br />
Length across axis<br />
approx.<br />
250mm<br />
For further information, see chapter Stirring and<br />
Dispersing, ViskoPakt.<br />
can be found in the chapter„Equipment and<br />
Components“. Further devices and components can<br />
be found in the chapters:<br />
� Process Analytics and Sensors<br />
� Dosing Systems and Pumps<br />
� Liquid Handling and Sample Drawing<br />
� Stirring and Dispersing<br />
� Custom Reaction Calorimeters<br />
Please note our customised robots in the chapter Liquid-Handling and Sampling.<br />
Talk to our engineerss about our special requirements!<br />
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206<br />
Laboratory Scales<br />
<strong>HiTec</strong> <strong>Zang</strong> is a competent partner for scales of a<br />
wide range of manufacturers. Your advantages are:<br />
Equipment and Components<br />
� Ideal alignment to the LabManager system<br />
� Competent consultancy in the selection of the<br />
suited scales<br />
� Competent consultancy in case of interface<br />
problems<br />
� Low-cost calibration service<br />
GraviDos ® Suspended Scales<br />
As a space-saving alternative to electronic<br />
laboratory scales, the GraviDos Suspended Scale<br />
has in many cases proven to be very useful. Using<br />
the available adaptors, it can be directly attached to<br />
the rodding of a laboratory plant.<br />
They can be queried faster than standard laboratory<br />
scales, which positively influences dosing and flow<br />
control. In addition, air movements are less<br />
disturbing to them than to platform scales.<br />
The GraviDos Suspended Scale is connected to a<br />
GraviDos Measuring Amplifier. The digital version<br />
disposes of a serial interface.<br />
The GravidosDos Dosing system is based on the<br />
GraviDos Suspended Scales. Further information<br />
can be found in the Chapter „Dosing Systems and<br />
Pumps“.<br />
In order to be able to establish an offer that meets<br />
your requirements, we need to know the weighing<br />
range and the required resolution. The serial<br />
interface is standard at most models. In spite of this,<br />
you should also state if you require one. Further<br />
requirements, such as documentation according to<br />
GLP, and other demanded special features should<br />
also be stated.<br />
Technical Data<br />
Measuring Resolution approx. 0,01% of Unit<br />
Measuring Uncertainty approx. 0,1% of Unit<br />
Dimensions Load Cell<br />
(without rodding)<br />
200x40x50mm<br />
Higher precision is available upon request.<br />
Delivery Scope Suspended Scales with signal cable for the connection to GraviDos<br />
Measuring Board or Measuring Amplifier<br />
Order Code Description<br />
IW-GRAVITS3000 GraviDos Suspended Scales 3000g, including cable<br />
IW-GRAVITS7500 GraviDos Suspended Scales 7500g, including cable<br />
IW-GRAVITS15000 GraviDos Suspended Scales 15kg, including cable<br />
IW-GRAVITS30000 GraviDos Suspended Scales 30kg, including cable<br />
IW-GRAVITS<strong>10</strong>00D GraviDos Suspended Scales 1.000g, integrated measuring amplifier , RS232, including cable<br />
IW-GRAVITS3000D GraviDos Suspended Scales 3.000g, integrated measuring amplifier, RS232, including cable<br />
IW-GRAVITS7500D GraviDos Suspended Scales 7.500g, integrated measuring amplifier, RS232, including cable<br />
IW-GRAVITS15000D GraviDos Suspended Scales 15kg, integrated measuring amplifier, RS232, including cable<br />
IW-GRAVITS30000D GraviDos Suspended Scales 30kg, integrated measuring amplifier, RS232, including cable<br />
HK-GRADOMV1 Measuring Amplifier 1 Channel, external measuring amplifier for connection to analogue input<br />
HK-GRADOMV1D Digital Measuring Amplifier external, 1 Channel, with RS232 V24 Interface<br />
HK-GRADOMV1D-SN Plug-In Power Supply for Digital Measuring Amplifier HK-GRADOMV1D<br />
HK-AD24DMS4 Measuring System 4 Channels, Board for <strong>HiTec</strong> <strong>Zang</strong> PNC Panel<br />
IL-GRADOADV Square Adaptor, adapter piece for load cell to square aluminium assembly systems<br />
IL-GRADOADR Round Adaptor, adapter piece for load cell to 12mm tube assembly systems<br />
You will find further information to the measuring amplifiers and more in the chapters „Laboratory Automation<br />
Hardware“ and „External Measuring Amplifiers“.<br />
Information to the GravDos Dosing Systems can be found in the Chapter „Dosing Systems and Pumps“.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
GraviDos ® Desktop Scales<br />
Equipment and Components<br />
The GraviDos desktop<br />
scales represent a spacesaving<br />
alternative to<br />
electronic laboratory<br />
scales. Without the foot<br />
element, they can, in<br />
addition, be directly<br />
attached to the rodding of a<br />
laboratory plant. The<br />
GraviDos desktop scales<br />
are connected to a<br />
GraviDos measurement<br />
amplifier.<br />
Order Code Description<br />
IW-GRAVITS<strong>10</strong>00 GraviDos desktop scales 1.000g<br />
IW-GRAVITS3000 GraviDos desktop scales 3.000g<br />
IW-GRAVITS7500 GraviDos desktop scales 7.500g<br />
IS-W-GRAVISTAND Desktop stand with levelling screws<br />
IS-W-GRAVIPLATE Weighing plate, diameter 140mm<br />
IS-W-GRAVICRANE Hose guide to weighing vessel<br />
GraviDos ® Platform Scales<br />
GraviDos platform scales represent a robust<br />
alternative to electronic laboratory scales for<br />
deployment under rough conditions.<br />
The GraviDos System enables shorter and more<br />
consistent measuring periods than electronic<br />
laboratory scales. This in turn enables a more<br />
consistent flow during dosing regulation. The<br />
GraviDos platform scales are connected to a<br />
GraviDos measurement amplifier.<br />
The scales dispose of adjustable foots for levelling.<br />
The Advantages:<br />
� Robust Construction for In-Process Applications<br />
� Ideal Alignment to the LabManager-System<br />
� Ideal Regulating Properties due to a high Sampling Rate<br />
Technical Data<br />
Dimensions Weighing Platform 300mm x 300mm<br />
Measurement Range 3kg, 7.5kg, 15kg, 30kg<br />
Measurement Resolution 0.01%<br />
The three-element hose guide ensures the stable<br />
guidance of the hose into the vessel.<br />
Further information can be found in the chapter<br />
“Dosing Systems and Pumps”.<br />
Technical Data<br />
Height Weighing Plate 70mm<br />
Diameter Weighing Plate 140mm<br />
Maximum Height of Holder 400mm<br />
Maximum Width 160mm<br />
Measurement Range 1kg, 3kg, 7,5kg<br />
Delivery scope Desktop scales with signal cable for<br />
connection to a GraviDos<br />
measurement card or measurement<br />
amplifier<br />
Delivery Scope Platform scales with signal cable for connection to a GraviDos measurement card<br />
or measurement amplifier<br />
Order Code Description<br />
IW- GRAVIPF3000 Platform scales for a maximum load of 3,000g<br />
IW- GRAVIPF7000 Platform scales for a maximum load of 7,500g<br />
IW- GRAVIPF15000 Platform scales for a maximum load of 15,000g<br />
W-GRAVIPF30000 Platform scales for a maximum load of 30,000g<br />
Ex-Equipment is available upon request.<br />
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208<br />
Reactor Weighing<br />
Equipment and Components<br />
An exact measurement of the filling level in the<br />
reactor is difficult to realise, as the measurement<br />
transmitters are too large and dispose of too low<br />
resolution. One alternative is the weighing of the<br />
complete reaction vessel. In order to achieve a high<br />
resolution at the lowest cost, the tare weight of the<br />
plant is compensated by balance weights. The<br />
variable weight of the tempering oil (due to thermal<br />
expansion) can be compensated by the LabManager<br />
on a calculated basis.<br />
Technical Data<br />
Weighing Range As required<br />
Measurement 1 g at 50 kg<br />
Resolution<br />
Order Code Description<br />
IW-GRAVIREAKW GraviDos reactor weighing module<br />
Kern Scales<br />
Kern scales are our low-cost alternative.<br />
� Good Quality at a low Price<br />
� 3 Years Guarantee by Manufacturer<br />
� Optional Self-Calibration<br />
� Outstanding Cost/Performance Ratio<br />
Preferential Types of System Scales:<br />
Example for reactor weighing with GraviDos load cell: 60 kg<br />
construction. Above: view of the complete plant, left: load cell,<br />
right:balance weights for tare compensation.<br />
Model Weighing Range [g] Reading Precision [g] Weighing Plate Remark<br />
572-35 1.5<strong>10</strong> 0,01 ø 150 Robust metal casing<br />
Including RS232<br />
572-49 15.<strong>10</strong>0 0,1 160x200 Robust metal casing<br />
Including RS232<br />
PLS 5<strong>10</strong>-3 5<strong>10</strong> 0,001 128x128 Back-lit Display<br />
Very robust metal casing<br />
Including RS232<br />
PLS 4000-2 4.000 0,01 165x165 Back-lit Display<br />
Very robust metal<br />
casing<br />
Including RS232<br />
QKE 36K0.5 36.<strong>10</strong>0 0,5 340x240 Self-explanatory filling<br />
level control<br />
Including RS232<br />
Order Code Description<br />
IW-572-35 Precision laboratory scales, Kern Type 572-35, Max. 1,5<strong>10</strong>g, resolution 0.01g, reproducibility<br />
0.01g, incl. RS232<br />
IW-572-49 Precision laboratory scales, Kern Type 572-35, Max. 15,<strong>10</strong>0g, resolution 0.1g, reproducibility<br />
0.1g, incl. RS232<br />
IW-PLS 5<strong>10</strong>-3 Precision laboratory scales, Kern Type PLS 5<strong>10</strong>-3, Max. 5<strong>10</strong>g, resolution 0.001g, reproducibility<br />
0.001g, incl. RS232<br />
IW-PLS 4000-2 Precision laboratory scales, Kern Type PLS 4000-2, Max. 4000g, resolution 0.01g, reproducibility<br />
0.01g, incl. RS232<br />
IW-QKE 36K0.5 Large desktop scales, Kern Type QKE 36K0.5, resolution 0.5g, reproducibility 0.5g, incl. RS232<br />
ZK-W-KE04-BS-R2-I-02 Connection cable Kern scales Type IW-572 and Typ QKE, RS232, 3m<br />
ZK-W-KE06-BS-R2-I-01 Connection cable Kern scales Type IW-PLS, RS232, 3m<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Sartorius Scales<br />
Sartorius scales represent the proven industrial<br />
standard with a particularly wide range of different<br />
types:<br />
� Proven industrial Standard<br />
� Extremely robust<br />
� Made in Germany<br />
� Calibrated Version available<br />
� Optional Self-Calibration<br />
� Ex-Version available<br />
� Good Cost/Performance Ratio<br />
Features of the Extend Series:<br />
� Internal motor-driven alignment weight<br />
element<br />
� Fully automatic calibration and alignment<br />
function isoCAL<br />
� ReproTEST for quick determination of<br />
reproducibility<br />
� ISO/GLP-conform protocoling<br />
Available in 2 Versions<br />
Depending on the application complexity, you can<br />
select between Extend precision scales models<br />
including or without an internal alignment weight<br />
element. Both scales model series are ideally suited<br />
for deployment as testing instrument in the quality<br />
assurance system. The measurement range of the<br />
scales is 0.001 to 8200 g. As an example, the<br />
following depicts the ED6202S with a weighing<br />
range of 0.01 up to 6200g.<br />
Sartorius ED6202S<br />
Equipment and Components<br />
Secured against unauthorised Modifications<br />
The access to the scales menu can be locked via a<br />
code determined by you. With this, you are able to<br />
secure your settings against manipulations and<br />
unauthorised modifications.<br />
In combination with a connected printer, the scales<br />
of the Extend series meet the demands of the<br />
ISO/GLP-conform protocoling to <strong>10</strong>0%.<br />
Quality QA:<br />
Sartorius also offers platform scales with a weighing<br />
range of 0.1g up to 65 kg.<br />
Quality QA is based on a modular concept: display<br />
unit and weighing platform can be mounted<br />
separately.<br />
Technische Daten<br />
Weighing Range 6200 g<br />
Reading Precision 0.01g<br />
Weighing Plate 180 x 180 mm<br />
Order Code Description<br />
IW-LP4200S Sartorius scales LP42000S incl. RS232<br />
ZK-W-SA01-BS-R2-I-03 Connection cable Sartorius scales to <strong>HiTec</strong>-PI, 9-pole RS232. 3 m<br />
Sartorius ME414S<br />
Technische Daten<br />
Weighing Range 4<strong>10</strong> g<br />
Reading Precision 0.0001g<br />
Weighing Plate ø 90, weighing space<br />
166 x 248<br />
Order Code Description<br />
IW-ME414S Sartorius scales ME414S incl. RS232<br />
ZK-W-SA01-BS-R2-I-03 Connection cable Sartorius scales to <strong>HiTec</strong>-PI, 9-pole RS232. 3 m<br />
Take advantage of the experience of our project engineers. We will gladly advise you!<br />
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Automation<br />
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Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
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Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
2<strong>10</strong><br />
Equipment and Components<br />
Electrical Base Discharge Valves<br />
Automatic base discharge valves enable the<br />
program-controlled discharge of the reactor content.<br />
Base discharge valves actuated by electric drive, in<br />
comparison to the pneumatically-driven ones, have<br />
the advantage that the opening degree can be<br />
adjusted continuously.<br />
The combination with the phase detector PhaDec<br />
enables conducting additionally automatic phase<br />
separation and extraction.<br />
Automatic base discharge valves, in comparison to<br />
manually operated valves, offer the following<br />
Advantages:<br />
� Minimisation of the risk of injuries<br />
� Automatic discharge at the ideal point of time<br />
� Enables automation of phase separation in<br />
combination with PhaDec<br />
The <strong>HiTec</strong> <strong>Zang</strong> electrical base discharge valves are<br />
based on proven manual base discharge valves<br />
made by different manufacturers. These are<br />
equipped with a special electrical drive and a control<br />
system.<br />
An important feature is that no extra headroom is<br />
required for this.<br />
NORMAG-valve with electrical drive<br />
Especially important and advantageous is the<br />
possibility to operate the valve manually at any time,<br />
e.g. in case of a power failure.<br />
Die Ansteuerung erfolgt über Bedientaster RS232<br />
Schnittstelle. Eine Positionsregelung sorgt für<br />
optimale Reproduzierbarkeit.<br />
Optional können 24V Binärein- und Ausgänge<br />
vorgesehen werden, jeweils für auf und zu.<br />
Technical Data<br />
Ambient temperatur 40 °C<br />
Operating voltage 24V DC<br />
Control RS232, opt. 2x Binär 24V<br />
Response RS232, opt. 2x Binär 24V<br />
Industrial Protection IP30<br />
Delivery Scope Drive and control unit with connection cable and manual<br />
GKB-valve with electrical drive<br />
HWS-Ventil <strong>10</strong> mm Type T/PT HWS-Ventil 20 mm Type H<br />
Order Code Description<br />
VL-BAVM-GKB Manual base discharge valve Type Glas Keller, for 250 and 400 ml<br />
VL-BAVA-GKB Electrical drive for base discharge valve Type Glas Keller<br />
VL-BAVA-NOR<strong>10</strong> Electrical drive for base discharge valve Type NORMAG nominal width <strong>10</strong> mm, GL25<br />
VL-BAVA-NOR15 Electrical drive for base discharge valve Type NORMAG nominal width <strong>10</strong> mm, GL32<br />
VL-BAVA-NOR25 Electrical drive for base discharge valve Type NORMAG nominal width <strong>10</strong> mm, GL45<br />
VL-BAVA-HWST Electrical drive for base discharge valve Type HWS Standard T and T/PT nominal width <strong>10</strong>mm<br />
VL-BAVA-HWS<strong>10</strong> Electrical drive for base discharge valve Type HWS Typ short version <strong>10</strong><br />
VL-BAVA-HWS20 Electrical drive for base discharge valve Type HWS Typ short version 20<br />
VL-SOLIDOS-BIN Option Binärein- und Ausgänge<br />
The drives can also be adjusted by us to fit other valves.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Equipment and Components<br />
Automatic Liquid Phase Separation<br />
The <strong>HiTec</strong> <strong>Zang</strong> PhaSep phase separation module<br />
is in particular deployed in the automatic separation<br />
and separate bottling of liquid phases out of reactors<br />
or collecting vessels, e.g. after reactions with phase<br />
transfer catalysis, after azeotropic distillations or<br />
extractions.<br />
The application of PhaSep is not limited to<br />
transparent or conductible fluids.<br />
Properties<br />
� Robust und economic<br />
� Integratable into any system<br />
� Universally deployable for all liquid phases –<br />
even for not transparent or non-conductible fluids<br />
� Resistant to pressure and chemicals<br />
� Also deployable as temperature sensor<br />
� Easy to operate<br />
� Inert materials: glass, high-grade steel, Hastelloy,<br />
PEEK, PTFE<br />
� Full integration into the HiBatch recipe control<br />
The sensor can alternatively be mounted into the<br />
base discharge valve, the discharge tubing, or from<br />
above into the reaction vessel.<br />
PhaSep requires a control valve (see electrical base<br />
discharge valves) for regulation of the discharge<br />
speed and, if necessary, a separation valve for<br />
separate bottling.<br />
<strong>Main</strong> Areas of Deployment<br />
� Extraction<br />
� Extractive Distillation<br />
� Azeotropic Distillation<br />
� Phase Transfer Catalysis<br />
PhaSep operates with most fluids, regardless<br />
whether they are liquid or gas, conductive or nonconductive,<br />
transparent or not. As long as there is a<br />
clear phase limit, the phases are securely<br />
separated.<br />
Order Code Description<br />
IL-PHASEP Liquid phase separation module<br />
PhaSep phase separation module with PhaDec Sensor at a 5-l<br />
research reactor. Detector 6 mm PTFE in automatic base<br />
discharge, on the left: control and separation valve as well as<br />
collecting vessel. Additional buttons for manual operation.<br />
Initialising mask of the basis operation PhaSep.<br />
You can find suited electrical base discharge valves in the section Electrical Base Discharge Valves<br />
PhaSep as a stand-alone system is available upon request.<br />
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Laboratory<br />
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212<br />
Glass Components<br />
Reflux Separator<br />
Reflux separators enable the adjustment of the<br />
reflux ratio, i.e. the division of the occurring<br />
condensate in reflux and discharge at rectification<br />
columns.<br />
Two differently constructed types are available:<br />
Typ 1 comprises a pivot/rotary funnel with a sealed<br />
magnet which can be turned from the outside with<br />
an electric magnet to the positions reflux and<br />
discharge.<br />
Typ 2 operates with a ball and pocket valve, which<br />
can be moved from the outside via an electric<br />
magnet to the positions reflux and discharge. The<br />
Equipment and Components<br />
advantage in this case is that the discharge nozzle is<br />
tightly sealed due to the ball and pocket valve in the<br />
reflux position.<br />
Both types can be directly connected to a digital<br />
output of a LAB-PI and be activated via pulse<br />
frequency, pulse width or pulse area modulation can<br />
be activated.<br />
An extra reflux control device is therefore no longer<br />
required.<br />
The reflux division ratio can be pre-determined,<br />
dependant of temperature, e.g. by the HiBatch basis<br />
operation „Distilling“.<br />
Reflux separator Type 1 with funnel Reflux separator Type 2 with ball and pocket valve<br />
Order Code Description<br />
IL-RFT-TR-1 Reflux separator with funnel , NS29<br />
IL-RFT-TR-MAG Electric magnet for reflux separator with funnel<br />
ZK-X-HW01-OD-XA-I-01 Cable for reflux separator with funnel, Tuchel plug for connection to LAB-PI<br />
IL-RFT-SV-1 Reflux separator with ball and pocket valve, from NS19<br />
IL-RFT-SV-MAG Electric magnet for reflux separator with ball and pocket valve<br />
ZK-HM-HI01-OD-XA-I-01 Cable for reflux separator with ball and pocket valve, Tuchel plug for connection to LAB-PI<br />
Sensor Protection Tube<br />
This sensor protection tube protects the sensitive<br />
measuring head of pH electrodes or other electrodes<br />
and serves as an extension at the same time.<br />
Order Code Description<br />
L-SONSCHR-1 Sensor Protection Tube made of glass, dimensions according to specifications<br />
Further glass parts, components and equipment for the laboratory and mini-plant technology, and special<br />
designs are available upon request.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Equipment and Components<br />
Low Pulsation Total Evaporator<br />
Low pulsation vapour dosing with quick responding<br />
behaviour to load changes is required for many<br />
technical applications.<br />
The new evaporator concept enables low pulsation<br />
total evaporation with very good dynamics. The<br />
essential features are the evaporation in very narrow<br />
channels, the strict partitioning of the apparatus into<br />
a cooled feed sector and a hot evaporation and<br />
overheating sector, as well as the fact that the<br />
construction can be disassembled for cleaning<br />
purposes.<br />
the cooling of the liquid in-feed prevents preliminary<br />
evaporation of the fed liquid, which leads the phase<br />
transition to take place with low pulsation and in a<br />
defined range on a very short section. An additional<br />
absorption volume is consequently no longer<br />
necessary.<br />
The defined evaporation in narrow channels with low<br />
liquid volume ensures controlled and low pulsation<br />
evaporation with very fast responding behaviour to<br />
load changes.<br />
Technical Data<br />
Working Range 2 - 120 g/h<br />
Pressure 0 to <strong>10</strong> bar<br />
Temperature 0 to 400 °C<br />
Heating Exchangeable, electric heating<br />
cartridge 230 V, max. 400 W<br />
Medias Amongst others, water,<br />
methanol, iso-octane, petrol,<br />
SiCl4<br />
Material High-grade steel 1,4301,<br />
1,4571 (special materials, e.g.<br />
Hastelloy available upon<br />
request)<br />
Media<br />
Pipe, Ø6 mm<br />
Connection<br />
Order Code Description<br />
IL-VERDA120 Laboratory Evaporator max. 120g/h (H2O)<br />
IL-VERDA-TREG Universal Temperature Controller<br />
IL-VERDA-THEL Thermo Element in a high-grade steel tube<br />
Suited liquid pumps can be found under LabDos Peristaltic Pumps.<br />
Versions Welded or demountable (with<br />
O-Ring seal made of Viton,<br />
Temperature: max. 200 °C;<br />
(Teflon upon request)<br />
Applications<br />
Precise evaporation of liquid dosed feed materials in<br />
laboratories and pilot plants.<br />
� Fuel Cell<br />
� Car Exhaust Catalysis<br />
� Reaction Technology<br />
� Vapour Reforming<br />
� Process Technology ...<br />
The laboratory evaporator is also available as<br />
complete device with temperature control and<br />
dosing.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
214<br />
Valves and Stop-Cocks<br />
Valves, stop-cocks, flaps, etc. are required in large<br />
numbers for the control of the material flows in<br />
laboratory reactor plants, pilot plant stations, and<br />
mini-plants.<br />
Here you will find the special valve you require for<br />
your laboratory, pilot plant, or mini-plant station. You<br />
can select between open/closed valves and<br />
proportional valves. All valves can be directly<br />
connected to our LAB- and PMC-PIs.<br />
Also in this sector, you can count on our<br />
competence in the planning stage and acquisition of<br />
the suited products by acclaimed manufacturers.<br />
Application Areas<br />
� Addition/Feed of Reactants<br />
� Extraction of Products<br />
� Discharge of Reaction Vessels<br />
� Venting and Deairing<br />
� Inerting<br />
� Vacuum Generation<br />
� Cooling and Heating Agents Control<br />
� Switching between different reservoir containers,<br />
feeds, etc.<br />
� Safety: Preliminary Locking, Pressure Relief,<br />
Emergency Cooling ...<br />
� Ex-Area Zone 1 and 2: intrinsically safe and<br />
pressure-sealed magnetic valves, pneumatic<br />
valves balanced or controlled from the non-risk<br />
area.<br />
Equipment and Components<br />
You can, in particular, expect from us competent<br />
advice and an individual concept aligned to your<br />
special requirements, respectively for your case of<br />
application.<br />
Our know-how covers many manufacturers and<br />
construction types, so that we are able to exactly<br />
correspond to your requirements. Do not hesitate to<br />
ask!<br />
For the most important tasks in the laboratory, you<br />
will find a selection of proven standards under<br />
“Preferential Types”, which will facilitate the selection<br />
for you.<br />
Advantages and Performance:<br />
� All valves can be activated via the digital<br />
outputs of our PIs<br />
� Complete delivery with cable and plug for<br />
direct connection to your LAB-xxx PI<br />
� Hydraulic design and alignment to the media<br />
of your plant, available auxiliary energy etc.,<br />
established by our engineering department<br />
� Consultancy and alignment to your<br />
automation devices completely from one<br />
single source<br />
To establish the lay out design of a valve, we require<br />
some information, which you can, if desired,<br />
coordinate together with our project engineers:<br />
Work Conditions:<br />
Flow Rate (often, estimation is sufficient)<br />
Suction Pressure (p1), Back Pressure (p2)<br />
Working Temperature (media, ambient)<br />
Special ambient conditions (explosion protection,<br />
flammable/corrosive materials...)<br />
Media:<br />
Description, Aggregate Condition, in case of<br />
mixtures, hydraulic, rheological, chemical and<br />
physical features<br />
Valve Type:<br />
Gate valve, change-over valve- (2/3-way), rest<br />
position, secure position<br />
Auxiliary Energy:<br />
Compressed air//inert gas available?, Pressure?<br />
Connections:<br />
Deployed/ required tubing, hoses and connection<br />
elements?<br />
Special Requirements:<br />
Safety-relevant aspects, final position display /<br />
monitoring, cleaning possibilities, behaviour in case<br />
of auxiliary energy failure, media separation CIPcompatible<br />
etc..<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Which Valve for which Application?<br />
The following table will help you to find the suited<br />
valve for a multitude of applications.<br />
Equipment and Components<br />
IV-MB-FK2-2-1,6..<br />
IV-MB-FK1-3-1,6..<br />
In case of any uncertainties, our project department<br />
will gladly help you.<br />
IV-MB-FK1-2-1,6..<br />
Task<br />
Locking of smaller Flows + + + o +<br />
Locking of medium Flows + + o +<br />
Locking of large Flows + + +<br />
Viscose, abrasive Media +<br />
Distributing + o +<br />
Selecting + o +<br />
Mixing + o +<br />
Control Valve for Liquid<br />
Dosing via the Force of Gravity<br />
(e.g. GraviDos)<br />
+ + o o<br />
Suction-side Valve at Pump<br />
Dosing for Vessel Switching<br />
+ + o o<br />
Additional Locking Valve at<br />
Dosing into Vacuum<br />
+ o<br />
Reactor Venting o o + o<br />
Reactor Deairing o o + o<br />
Inert Gas Feed o o + o<br />
Gas Feed + + o o<br />
Reactor Discharge Stop-Cock + +<br />
Sample Bottling o o o +<br />
High Pressure +<br />
Ex-Area + + o o o<br />
+ = well suited, o = limited suitability, upon request<br />
IV-MB-GM1-2-2...<br />
Multi-way channels can be found in the following pages.<br />
Preferential Types<br />
(A selection of standard types for typical<br />
laboratory applications)<br />
We have arranged a selection of preferential types<br />
for the most frequent laboratory applications which<br />
have proven to be especially effective.<br />
Preferred Types of Connection<br />
SN4/6 Screwing for hose with diameter interior/exterior 4.0/6.0 mm<br />
GMGx/x Thread Bushing G x/x inch e.g. G3/8 = 3/8 inch cylindrical G-thread<br />
IV-MB-UM1-2-3...<br />
IV-MB-UM1-3-3...<br />
IV-MB-UM2-2-..<br />
IV-PB-FG1-2-15..<br />
IV-PB-FG2-2-15..<br />
IV-PB-FG3-3-20..<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 215<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
216<br />
Universal Laboratory Valve<br />
This low dead storage laboratory valve is particularly<br />
suited in the low pressure and low viscosity area for:<br />
� Distributing<br />
� Mixing<br />
� Switching of small Flows<br />
� As a Control Valve for Liquid Dosing via the<br />
Force of Gravity<br />
� As a Suction-side Valve at Pump Dosing for<br />
Vessel Switching<br />
� As an additional locking Valve when Dosing<br />
� For Dosing of aggressive, highly pure and sterile<br />
Media<br />
Technical Data<br />
Equipment and Components<br />
Amongst others, it is deployed in the GraviDos-<br />
Dosing System.<br />
Flow Rate Kv-Value 3-way: 0.047 m³/h, accords to 15 l/h H2O at approx. p=<strong>10</strong>0 mbar<br />
(≈1 m height difference), 2-way: 0.06 m³/h<br />
Mode of Operation Open/Closed magnetic valve<br />
Rest Position dead, closed<br />
Nominal Width 1.6 mm / 1.5 mm<br />
Media Connection G 1/8“, UNF<br />
Media Temperature 0 to 50 °C<br />
Ambient Temperature max. 55 °C<br />
Pressure Range 0 to 2 bar<br />
Dead Storage Volume 85 μl<br />
Casing Material PVDF, ETFE<br />
Seal Material FFKM (Kalrez, similar to Simrez, Chemraz, Perlast)<br />
Media Compatibility Against almost all chemicals, except freons and highly halogenated solvents<br />
Flow Direction random<br />
Operational Voltage 24V DC<br />
Power Consumption 3.4 W warm<br />
Protection Category IP 40<br />
Ex-Version no<br />
Order Code Description<br />
IV-MB-FK1-2-1,6-GMG1/8-ea Universal 2/2-way laboratory valve nominal width 1.6 mm, Kv 0.06 m³/h, with 3 m cable for<br />
connection to LAB-PI (plug) or MSR-PI (open ends)<br />
IV-MB-FK1-3-1,6-GMG1/8-ea Universal 3/2-way laboratory valve nominal width 1.6 mm, Kv 0.047 m³/h, with 3 m for<br />
connection to LAB-PI (plug) or MSR-PI (open ends)<br />
IV-MB-FK2-2-1,5-UNF-ea Universal 2/2-way laboratory valve nominal width 1,5 mm, Kv 0,039 m³/h, with 3 m cable for<br />
connectino to LAB-PI plug or MSR-PI (open ends)<br />
IV-MB-FK2-3-1,5-UNF-ea Universal 3/2-way laboratory valve nominal width 1,5 mm, Kv 0,047 m³/h, with 3 m cable for<br />
connectino to LAB-PI plug or MSR-PI (open ends)<br />
VL-KB-MB-FK1 Valve holding element for LabKit-ALU System<br />
ea = Electrical Connection<br />
T Tuchel plug for LAB-PI<br />
O Open ends for PMC-PI<br />
Order Example:<br />
3/2 way valve, media connection, thread bushing G<br />
1/8“, cable for LabManager/box<br />
Order Code: IV-MB-FK1-1,6-3-GMG1/8-T<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Equipment and Components<br />
Universal Laboratory Valve with Manual Emergency Actuation<br />
An universal magnetic valve for application where a<br />
manual actuation is possibly necessary in<br />
emergency cases:<br />
� Reactor Venting and Deairing<br />
� Addition of Inert Gases<br />
� Distributing<br />
� Mixing<br />
� Interruption of small Flows<br />
� As a Control Valve for Liquid Dosing via the<br />
Force of Gravity<br />
Technical Data<br />
Flow Rate, Kv Value 0.25 m³/h (accords to approx. 30 l/min air at Δp=<strong>10</strong>0 mbar) to 0.40 m³/h<br />
Mode of Operation Open/Closed or 2/3-way magnetic valve<br />
Rest Position dead, closed<br />
Nominal Width 3, 4, 5 mm<br />
Media Connection G1/4“<br />
Media Temperature -30 to +80°C at EPDM, 0 to +80°C at FKM<br />
Ambient Temperature max. 55°C<br />
Pressure Range 0-8 bar at DN3, 0-3 bar at DN5<br />
Casing Material PP and PVDF<br />
Seal Material EPM, FKM, media separation via diaphragm , FFKM optional<br />
Media Compatibility bases, many solvents, many oils,<br />
acids and salt solutions should be verified in individual cases<br />
Operational Voltage 24V DC<br />
Power Consumption 8 W<br />
Protection category IP 65<br />
Order Code Description<br />
IV-MB-FK2-2-nw-ma-ea Universal 2/2-way laboratory valve with manual emergency actuation with 3 m cable for<br />
connection to LAB-PI (plug) or MSR-PI (open ends)<br />
IV-MB-FK2-3-nw-ma-ea Universal 3/2-way laboratory valve with manual emergency actuation with 3 m cable for<br />
connection to LAB-PI (plug) or MSR-PI (open ends)<br />
VL-KB-FK2-UM1 Valve holding element for LabKit-ALU-System<br />
nw = Nominal Width<br />
3 3 mm 0,25 m³/h<br />
4 4 mm 0,30 m³/h<br />
5 5 mm 0,40 m³/h<br />
ma = Media Connection:<br />
GMG1/4 Thread Bushing G 1/4“<br />
ea = Electrical Connection<br />
T Tuchel plug for LAB-PI<br />
O Open ends for MSRmanager<br />
Order Example:<br />
3/2 way valve, DN3, Kv 0.25 m³/h, media connection<br />
thread bushing G 1/4“,<br />
Cable for<br />
LabManager/box.<br />
Order Code: IV-MB-UM1-3-GMG1/4<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 217<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
218<br />
Inerting, Venting and Deairing Valve<br />
This valve is particularly suited for:<br />
� Reactor Venting<br />
� Reactor Deairing<br />
� Addition of Inert Gases<br />
Amongst other applications, this valve is deployed in<br />
reactor systems operating under high pressure.<br />
Technical Data<br />
Equipment and Components<br />
Flow Rate, Kv Value 0.12 m³/h (accords approx. 15 l/min air at Δp=<strong>10</strong>0 mbar) up to 0.55 m³/h<br />
Mode of Operation Open/Closed magnetic valve<br />
Rest Position dead, closed<br />
Nominal Width 2 bis 6mm<br />
Media Connection G1/8 bis G3/8<br />
Media Temperature -<strong>10</strong> to +<strong>10</strong>0°C at FKM, up to 180° at graphite/PTFE<br />
Ambient Temperature max. 55 °C<br />
Pressure Range 0 to 25 bar at NW 2 mm, 0 to 2,5 bar at NW 6 mm<br />
Casing Material High grade steel<br />
Seal Material FKM, PTFE/Graphite or EPDM<br />
Media Compatibility bases, many solvents, many oils,<br />
acids and salt solutions should be verified in individual cases<br />
Operational Voltage 24V DC<br />
Power Consumption 8 W<br />
Protection Category IP 65<br />
Ex-Version Optional (pressure sealed)<br />
Order Code Description<br />
IV-MB-GM1-2-nw-ma-ea Universal 2/2-way laboratory valve nominal width 2.0 mm, Kv 0.12 m³/h, with 1.5 m cable for<br />
connection to LAB-PI or MSR-PI<br />
VL-KB-MB-GM1 Valve holding element for LabKit-ALU-System<br />
nw = Nominal Width<br />
2 2 mm 0,12 m³/h<br />
2,5 2,5 mm 0,16 m³/h<br />
3 3 mm 0,23 m³/h<br />
4 4 mm 0,30 m³/h<br />
6 6 mm 0,55 m³/h<br />
ma = Media Connection:<br />
GMG1/8 Thread Bushing G 1/8“<br />
GMG1/4 Thread Bushing G 1/4“<br />
GMG3/8 Thread Bushing G 3/8“<br />
ea = Electrical Connection<br />
T Tuchel plug for LAB-PI<br />
O Open ends for PMC-PI<br />
Order Example:<br />
2 way valve, media connection thread bushing G<br />
1/8, cable for LabManager/box.<br />
Order Code: IV-MB-GM1-2-2-GMG1/8<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
High Pressure Magnetic Valve<br />
This high pressure valve features an exceptional<br />
pressure resistance of 4<strong>10</strong> bar. The directly<br />
controlled magnetic valve operates with a nipple<br />
seal.<br />
Application Areas:<br />
� Ventilation and Deairing of Reactor<br />
� Feeding of Inert Gas<br />
� Distribution<br />
� Mixing<br />
� Interruption of small Flows<br />
� Control Valve for the Dosing of Liquids via the<br />
Force of Gravity<br />
Technical Data<br />
Equipment and Components<br />
Seat Diameter 1,5mm<br />
Operation Modes Open/Closed 2/2-Way Magnetic Valve<br />
Idle Position Currentless Closed<br />
Nominal Width 1,5 mm<br />
Media Connection G1/4“<br />
Media Temperature -<strong>10</strong>...80°C<br />
Ambient Temperature max. 35°C<br />
Pressure Range 0-4<strong>10</strong>bar<br />
Casing Material High Grade Steel 1.4305/1.4<strong>10</strong>4<br />
Seal Material PTFE, PEEK<br />
Media Compatibility Bases, many solvents, many oils, acids and salt solutions. Please verify the<br />
individual cases.<br />
Operational Voltage 24V DC<br />
Power Consumption <strong>10</strong>0 W<br />
Protection Class IP 65<br />
Order Code Description<br />
IV-MB-UM2-2 2/2-Way High Pressure Valve 24V, 4 A<br />
IV-MB-UM2-PS Power Supply for 2/2-Way High Pressure Valve, 24V, 4 A, with Auxiliary Contactor<br />
VL-KB-MB-UM2 Valve Retaining Element for V-MB-UM2-2 Valve at the LabKit-ALU-System<br />
Further valves (further information available upon request).<br />
Order Code Description<br />
IV-MB-UM1-2-3-ma-ea Universal 2/2-way laboratory valve Ex nominal width 3.0 mm, Kv 0.23 m³/h<br />
IV-MB-UM1-3-3-ma-ea Universal 3/2-way laboratory valve Ex nominal width 3.0 mm, Kv 0.23 m³/h<br />
IV-PB-FG1-2-15-ma-ea 2/2-way ball valve nominal width 15 mm, Kv 11 m³/h<br />
IV-PB-FG2-2-15-ma-ea 2/2-way diaphragm valve nominal width 15 mm, Kv 7 m³/h<br />
IV-PB-FG3-3-20-ma-ea 3/2-way electric-pneumatical Open/Closed valve,nominal width 20 mm, Kv 7 m³/h<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 219<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
220<br />
Adjustment and Control Valves<br />
Equipment and Components<br />
Valves, stop-cocks, flaps, etc. are required in large<br />
numbers for the control of the material flows in<br />
laboratory reactor plants, pilot plant stations, and<br />
mini-plants.<br />
Material flows are often also integrated into control<br />
circuits. In this case, it is necessary to adjust these<br />
with continuously operating adjustment devices. For<br />
this purpose, adjustment valves are deployed.<br />
Application Areas<br />
� Pressure Control<br />
� Vacuum Control<br />
� Mass Flow Control for Heating and Cooling<br />
Media<br />
� Fast Temperature Regulation via Mixing<br />
Regulations<br />
� Mastering of exothermal Reactions through<br />
Temperature Control via:<br />
� Mass Flow of deployed Materials<br />
� Cooling/Heating agent Flow<br />
� Cascaded Temperature Control, e.g. subordinate<br />
Mass Flow Control for Heating Steam<br />
� Mass Flow Regulations<br />
� Controlled Release/Pressure Generation<br />
according to predetermined Profiles<br />
� Material Flow Regulation in continuously<br />
operating Plants<br />
� Level Control via Feed and Discharge<br />
� Ex-Area Zone 1 and 2 with intrinsically safe Valve<br />
Positioners<br />
In simple cases, it is also possible to operate with<br />
open/closed valves, if a certain generated pulsation<br />
does not matter (PWM-modulation, two-step<br />
control). Please do not hesitate to ask us. We will<br />
gladly also propose low-cost solutions to you, if this<br />
is possible.<br />
Advantages, Services<br />
Which Proportional Valve for which Application?<br />
With the help of the following table you will be able<br />
to find the suited valve for a multitude of<br />
applications.<br />
� All valves can be activated via the analogue<br />
outputs (panels AAP, AEAP..) of our PIs<br />
� Complete delivery with cable and plug for<br />
direct connection to your LAB-xxx PI<br />
� Hydraulic design and alignment to the media<br />
of your plant, available auxiliary energy etc.,<br />
established by our engineering department<br />
� Upon request, integration of your application<br />
programs by our application programmers<br />
� Upon request, design, installation and<br />
parameterisation of your control circuits by<br />
our engineering department<br />
� Ready-to-use software modules, e.g. vacuum/<br />
pressure control...<br />
� Establishment of complicated controller<br />
structures: self-adapting controllers, cascade<br />
controllers, characteristics controllers...<br />
� Consultancy and alignment to your<br />
automation devices completely from one<br />
single source<br />
In addition, we are also able to equip valve types out<br />
of the chapter “ Valves and Stop-Cocks” (e.g. ball<br />
valves, diaphragm valves) with continuously<br />
operating actuators. Also with these, to a certain<br />
extent, it is possible to conduct controlled operation.<br />
For higher quality regulations, we are also able to<br />
design characteristics regulations aligned to the<br />
respective application.<br />
For the most important tasks in the laboratory, you<br />
can find a selection of proven standards under<br />
“Preferential Types”, which will facilitate the selection<br />
for you.<br />
In case of any uncertainties, our project department<br />
will gladly assist you.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Equipment and Components<br />
IV-MP-UM...<br />
Task \ Type<br />
Pressure Control + +<br />
Vacuum Control + o +<br />
Mass Flow Control Small Flow + +<br />
Mass Flow Control Large Flow + o<br />
Mass Flow, viscose, abrasive Media o +<br />
Level Control + o o o<br />
Heating/Cooling Media, Temperature Control + + +<br />
Quick Temperature Control + + o<br />
Ex-Area +<br />
+ = well suited, o = limited suitability, upon request<br />
Electromagnetic Control Valve<br />
These electromagnetic proportional valves with<br />
outstanding features are the most cost-effective<br />
possibility to proportionally reduce material flows.<br />
Features<br />
� Low Hysteresis<br />
� Low Pressure Dependency<br />
� High Manipulating Speed<br />
� Simple Activation<br />
Applicable for:<br />
� Pressure Control<br />
� Vacuum Control<br />
� Mass Flow Control in Heating and Cooling<br />
Medias<br />
� Further Applications within Reactor Systems<br />
Technical Data<br />
IV-PP-UG1-2-13<br />
IV-PP-FG1-3-20..<br />
IV-PP-UX1-2...<br />
There are two methods to connect the<br />
valves to <strong>HiTec</strong>-<strong>Zang</strong> PIs.<br />
IV-PP-FG2-2-15...<br />
� Direct connection to a digital output<br />
(PWM 400 Hz an LP-DAP8T). The<br />
available power output of the digital<br />
output must be observed. This<br />
solution is particularly advisable in<br />
case of several valves are deployed.<br />
� 4..20mA analogue output (LP-AAP8UI or (LP-<br />
AE4AA4P...) via electronics IV-MP-ELBU...<br />
For the supply with operational voltage, a digital<br />
output (LP-DAP8A) or an external power supply<br />
source with according 24 V power output can be<br />
used.<br />
Flow Rate, Kv Value DN 0.8: approx. 0.02 m³/h, DN 2: 0.1 m³/h, DN 4: 0.33 m³/h, DN 6: 0.7 m³/h<br />
Qair (5 bar on atm.) DN 0.8: approx. 1,500 l/h, DN 2: 6,600 l/h, DN 4: 21,800 l/h, DN 6: 46,200 l/h<br />
Suited Vacuum Pump DN 2: approx. 1,000-3,000 l/h, DN 4: 3,000-8,000 l/h, DN 6: 8,000-16,000 l/h<br />
Mode of Operation 2/2-way magnetic valve with electronics 4-20 mA<br />
Rest Position dead, closed, zero point cut-off<br />
Nominal Width 0.8 + 2 + 4 + 6 mm<br />
Media Connection DN 0.8: G 1/8“, DN 2 + DN 4: G 1/4“, DN 6: G 3/8“<br />
Media Temperature -<strong>10</strong> to +90°C<br />
Ambient Temperature max. +55°C<br />
Pressure Range DN 0.8: 0-12 bar, DN 2: 0-8 bar, DN 4 u. DN 6: 0-2 bar<br />
Activation 4-20 mA with electronics or directly to LP-DAP8T<br />
Power Supply 24 V DC<br />
Power Output DN 0.8: 4 W, DN 2 + 4: 8 W, DN 6: 15 W<br />
Casing Material High-grade steel, DN 6 brass!<br />
Seal material FPM, Viton, Kalrez, PTFE<br />
Media Compatibility Almost all chemicals; acids and salt solutions need to be verified in individual<br />
cases, DN 6 only neutral gases (cold trap in case of vacuum application!)<br />
Hysteresis < 5%<br />
Reproducibility < 0.5 % of final value<br />
Response Time (90%) < 50 ms<br />
Protection Category IP 65<br />
Ex-Version No<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 221<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
222<br />
Equipment and Components<br />
Order Code Description<br />
IV-MP-UK1-2-0,8-ma-ea 2/2-way magnetic control valve, nominal width 0.8 mm, Kv 0.02 m³/h, with 1,5 m cable for<br />
connection to LAB-PI or MSR-PI<br />
IV-MP-UM1-2-2-ma-ea 2/2-way magnetic control valve, nominal width 2 mm, Kv 0.1 m³/h, with 1,5 m cable for<br />
connection to LAB-PI or MSR-PI<br />
IV-MP-UM2-2-4-ma-ea 2/2-way magnetic control valve, nominal width 4 mm, Kv 0.33 m³/h, with 1,5 m cable for<br />
connection to LAB-PI or MSR-PI<br />
IV-MP-UG1-2-6-ma-ea 2/2-way magnetic control valve, nominal width 6mm, Kv 0.7 m³/h, with 1,5 m cable for<br />
connection to LAB-PI or MSR-PI, only avaialable in brass!<br />
IV-MP-ELBU1 Separate electronics 4-20mA and 0-<strong>10</strong>V for IV-MP... proportional valves<br />
IV-MP-ELBU2 Integrated electronics 4-20mA for IV-MP proportional valves except -08<br />
ma = Media connection:<br />
GMG1-8 Thread Bushing G 1/8“, only DN 0.8<br />
GMG1-4 Thread Bushing G 1/4“, only DN 2 + 4<br />
GMG3-8 Thread Bushing G 3/8“, only DN 6<br />
SN6/SN4-6 Hose diameter=4mm, hose screwing, interior/exterior diameter 4/6mm for DN2<br />
SN<strong>10</strong>/SN8-11 Hose diameter=8mm, hose screwing, interior/exterior diameter 8/11mm for DN4<br />
SN15/SN<strong>10</strong>-15 Hose diameter=<strong>10</strong>mm, hose screwing, interior/exterior diameter <strong>10</strong>/15mm for DN6<br />
ea = Electrical Connection<br />
Order Example:<br />
T Tuchel plug for LAB-PI<br />
2/2-way magnetic control valve, nominal width 2<br />
O Open ends for PMC-PI<br />
mm, hose olive for di = 6, for LabBox<br />
Order Code: IV-MP-UM1-2-2-SN6-T<br />
Further Control Valves (Further information upon request):<br />
Order Code Description<br />
IV-PP-UG1-2-13-ma-ea 2/2-way electro-pneumatic slanted fit control valve, nominal width 13 mm, Kv 2.8 m³/h,<br />
integrated valve positioner<br />
IV-PP-FG1-3-20-ma-ea 3/2-way electro-pneumatic control valve, nominal width 20 mm, Kv 7 m³/h, with integrated<br />
valve positioner<br />
IV-PP-UX1-2-ma-ea-kv 2/2-way electro-pneumatic precision control valve with integrated valve positioner<br />
Multi-Way Valves<br />
These multi-way valves are intended for the<br />
distribution or combining of materials at low<br />
pressures. For the connection to the LAB-System, a<br />
serial interface is required at the UI/workstation.<br />
Multi-Way Valve for Small Flows<br />
Possible versions with 3/4/6/12/24-way distributor<br />
and 6-way sample feeding<br />
Typical applications are:<br />
� Bottling of Samples<br />
� Dosing out of many Preparation Drums<br />
Technical Data<br />
Nominal Width 0.75 mm, 1.5 mm<br />
Mode of Operation Rotor with step motor drive<br />
Media Connection 1/16 inch (1.58 mm), ¼ - 28<br />
Fittings<br />
Pressure Range 21 oder 68 bar at 6-way<br />
Flow Direction random<br />
Material Rotor PEEK/PCTFE<br />
Media<br />
Compatibility<br />
Operating Voltage 24V DC<br />
Activation RS232<br />
Ex-Version no<br />
Almost all chemicals, except<br />
acids containing sulphur and<br />
nitrogen and several solvents<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Equipment and Components<br />
Order Code Description<br />
IV-MW1-wa-ma-ea Multi- way valve with 1.5 m cable for connection to LAB-PI or PMC-PI<br />
IFN-IV-MW1 NAMUR driver for multi-way valve IV-MW1<br />
wa = Number of Positions 4, 6, 12 or 24.<br />
ma = Media Connection: UNF1/4“<br />
We advise to obtain feedback from our project<br />
department before placing an order for this valve.<br />
Multi-Way Valve for Medium Flows<br />
1/16 Fittings for 1/16 inch tubes, nominal<br />
width of valve: 0.75 mm.<br />
1/8 Fittings for 1/8 inch tubes, nominal<br />
width of valve 1.5 mm.<br />
Technical Data<br />
Nominal Width 4.6 mm<br />
Mode of Operation Rotor with step motor drive<br />
Media Connection Fittings for 1/4 inch tubes<br />
(6.35 mm)<br />
Media Temperature 50 °C<br />
Ambient<br />
40 °C<br />
Temperature<br />
Pressure Range 6 bar liquid<br />
Flow Direction random<br />
Material Stator PPS<br />
Material Rotor PTFE<br />
Media Compatibility Almost all chemicals<br />
Operational Voltage 24V DC<br />
Activation RS232<br />
Protection Category IP30<br />
Ex-Version optional<br />
Order Code Description<br />
IV-MW2-wa-1/4 Multi-way valve with 1.5 m cable for connection to LAB-PI or PMC-PI<br />
IFN-IV-MW2 NAMUR driver for multi-way valve IV-MW1<br />
wa = Number of Positions 4, 6.<br />
We advise to obtain feedback from our project department before placing an order for this valve.<br />
Further equipment and components can be found in<br />
the chapters:<br />
� Process Analytics and Sensors<br />
� Dosing Systems and Pumps<br />
� Liquid Handling and Sample<br />
� Stirring and Dispersing<br />
� Customised Reaction Calorimeters<br />
The present catalogue, due to the limited space, can only present an extract of all available equipment and<br />
components.<br />
<strong>HiTec</strong> <strong>Zang</strong>, amongst many other articles, also retails thermostats of the leading manufacturers, including<br />
respective accessories, e.g. hoses, heat carrier oil and pressure rising pumps.<br />
We will gladly assist you to find the ideal choice for your particular case of application.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 223<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
224<br />
Process Analytics and Sensors<br />
Here you will find a selection of instruments for<br />
process analytics, as well as sensors and monitors,<br />
which are suited for laboratory and mini-plant<br />
technology.<br />
All sensors are suited for deployment with the Laband<br />
MSR/PMC managers.<br />
Process Analytics and Sensors<br />
Notice:<br />
In case of interest, please contact us for information<br />
regarding special topics such as VIS-, NIR- or US-<br />
Spectroscopy.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
MoleculeEye ® ATR-FTIR-Spectroscopy<br />
Online-Monitoring of Reactions via<br />
ATR-FTIR Spectroscopy<br />
MoleculeEye ATR-probe in a MultiLab 250 ml reactor<br />
In order to be able to follow reactions, a great<br />
number of online-sensors are available. The majority<br />
of these however have one great disadvantage: they<br />
are not able to deliver substance-specific<br />
information. Spectroscopic methods are able to fill<br />
this gap. One of these is the Fourier Transformation-<br />
Infrared Spectroscopy (FTIR). Due too its very high<br />
absorption speed, this represents one of the most<br />
effective methods.<br />
IR-spectrometers, both in regard to quality and<br />
quantity, deliver outstandingly well evaluable<br />
spectrums, which also deliver utilisable information<br />
about unknown substances.<br />
Due to the narrow absorption band in the middle<br />
infrared band, this method is also suited for multicomponent<br />
analysis. In addition, it is also able to<br />
deliver information about transition conditions of a<br />
reaction, regardless whether this concerns an<br />
enzyme or a catalyst, via intermediates or transient<br />
aggregates. It is even possible to still gain<br />
information about individual substances out of multicomponent<br />
mixtures.<br />
All IR-active substances are detectable. As there are<br />
only a few non-IR-active substances (pure elements,<br />
a few simple compounds), this method is universally<br />
deployable.<br />
To draw samples and to transport them into the<br />
laboratory is the classic method – but it is laborious<br />
and time-consuming.<br />
With an ATR-probe, the laboratory is virtually directly<br />
brought into the reactor. ATR-FTIR-spectroscopy is<br />
therefore currently the most effective method for<br />
online-evaluation. It allows parallel determination of<br />
substances both according to type as well as<br />
amount.<br />
Advantages<br />
General:<br />
� Time saving due to online- in-situ measurement<br />
methods<br />
� Improvement of the product quality by minimising<br />
of by-products<br />
� Easy handling, mechanically robust, portable<br />
� Neither adjusting nor maintenance necessary<br />
� Minute sample amounts, no preliminary sample<br />
preparation necessary<br />
� Inert, free of reagents<br />
� No falsification of the sample due to transfer (e.g.<br />
as at HPLC)<br />
� Also deployable in small vessels<br />
� No sample wastage<br />
The MoleculeEye within Chemistry:<br />
� Fingerprint-Measurements<br />
� Recognition of intermediate products<br />
� Temperature and pressure-resistant<br />
� Chemically robust, explosion-protected<br />
The MoleculeEye within Biotechnology:<br />
� Delivers an exact image of the physiology of the<br />
bioprocess<br />
� Early problem detection<br />
� No contamination<br />
� Sterilisable sensor<br />
The MoleculeEye ATR-Diamond – Probe<br />
The novel fibre-optic MoleculeEye probe utilises the<br />
principle of the attenuated total reflection (ATR).<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 225<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
226<br />
Process Analytics and Sensors<br />
The ATR-Principle with diamond prism<br />
The ATR-crystal is made of diamond and connected<br />
to the fixture without seal elements. The<br />
MoleculeEye probe is therefore insensitive in regard<br />
to chemical and mechanical influences. A light ray<br />
which reaches an optically less dense media out of<br />
an optically dense one in a flat angle is reflected at<br />
the boundary area. But not exactly at the boundary<br />
area: the ray penetrates into the optically less dense<br />
media a few µm . Certain frequency components of<br />
the light are substance-specifically absorbed in the<br />
less dense media. This leads to the generation of<br />
absorption spectrums that are registered by the<br />
spectrometer.<br />
The MoleculeEye probe is highly inert, resistant<br />
against chemicals, pressure, and high temperatures<br />
and can therefore be installed in reactors without<br />
any problems. The 6mm probe fits into even the<br />
smallest reactors.<br />
The ATR-principle also functions in strongly coloured<br />
solutions, in emulsions and highly solid-containing<br />
suspensions, as the measurement merely takes<br />
place in a very thin layer at the crystal. Substances<br />
are partially, depending on their IR-absorption,<br />
detectable up to the trace range.<br />
MoleculeEye ATR Hand Probe<br />
The simple technical construction makes the method<br />
robust, its speed allows real-time measurement and<br />
consequently direct process guidance.<br />
The method is able to measure in the trace range<br />
and also delivers information to intermediate<br />
products and transition conditions.<br />
For this reason, it is particularly suited for<br />
examinations of reaction mechanisms. In<br />
comparison to similar effective methods, e.g. mass<br />
spectrometry, it is significantly more cost-effective<br />
and easier to handle.<br />
The <strong>HiTec</strong> <strong>Zang</strong> MoleculeEye FTIR Spectrometer<br />
System disposes of a fibre-optic ATR-Sensor with<br />
unique properties:<br />
� Diameter of only 6 mm<br />
� Simple Coupling with pin and socket<br />
connector<br />
� Outstanding long-term Stability<br />
� No Adjusting and Compensating necessary<br />
� Outstanding Measurement Accuracy and<br />
Linearity<br />
� Ideal Signal/Disturbance Ratio, consequently<br />
high Measurement Sensitivity<br />
� Fast Real Time Measurement, high Time<br />
Resolution<br />
� Several Sensors at one Spectrometer<br />
possible (Multiplexer)<br />
� Adaptation to spectrometers made by Bruker,<br />
Mettler, Nicolet, Perkin-Elmer, Jasco, and<br />
others is possible<br />
� Coupling to LabManager System is possible<br />
� Special Designs/solutions available<br />
Application Areas<br />
� Chemistry, Biotechnology, Pharmaceutics, Food,<br />
Environment ...<br />
� All IR-active substances detectable<br />
� Solid and liquid samples, non-transparent and<br />
solid-containing liquids and emulsions<br />
MoleculeEye ATR Probe mounted in a 2 litres<br />
LabKit Reaction Plant<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
Up to 6 probes can be connected to a spectrometer<br />
with a multiplexer unit. Parallel experiments are<br />
therefore possible without any problem.<br />
MoleculeEye ATR Probes in the MultiLab Parallel Reactor<br />
System<br />
MoleculeEye ATR-flow through cell for MRT plants<br />
Areas of Deployment and Examples<br />
Polymer Analysis: ATR-FTIR delivers both<br />
information regarding the chemical composition as<br />
well as the molecule size. Naturally, one can also<br />
just follow the progression of the reaction.<br />
FTIR spectrums of a polymerisation process.<br />
Catalysis: The IR-spectrums of adsorbates and<br />
transition conditions of a reaction differ from the<br />
spectrums of these substances in solution. These<br />
differences are due to the binding of the substrate to<br />
the catalyst. In this way, information about such<br />
conditions can be gained. Due to the measurement<br />
in an extremely thin layer surrounding the crystal,<br />
the solids do not interfere with the analysis.<br />
Reaction Technology: Following the reaction<br />
progress<br />
FTIR spectrums in the progression of a Grignard<br />
reaction.<br />
Protein Analysis: The normal IR analysis at<br />
proteins is strongly disturbed by the high and broadbanded<br />
adsorption of the functionally essential<br />
water. At ATR- robes, the water hardly causes<br />
disturbance, as only a thin layer is transilluminated.<br />
Diamond does not adsorb proteins, for which reason<br />
the ATR-crystal does not cause any disturbance.<br />
Monitoring of Clarification Plants: Parallel<br />
analysis of organic acids, carbonhydrates,<br />
carbonate, hydrogencarbonate, phosphate,<br />
hydrogenphosphate, carboxlate, and many further<br />
parameters in water and clearing sludge.<br />
Food: CO2 in Beer<br />
FTIR-spectrums of CO2 in beer and comparative solutions.<br />
Chemicals: Butylacetate and Toluene compared .<br />
ATR-FTIR-spectrums of Butylacetate and Toluene compared.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 227<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
228<br />
Pharmaceuticals: Caffein, Ascorbic Acid,<br />
Acetylsalicylic Acid.<br />
Process Analytics and Sensors<br />
ATR-FTIR-spectrums of Caffein, Ascorbic Acid, and Acetylsalicylic<br />
Acid compared.<br />
Technical Data<br />
The fibre optic probe with SMA connector<br />
Diamond-ATR MIR Probe head diameter: 6 mm, Length: 20 cm<br />
Standard Probe (extension possible)<br />
Materials In contact with media: Hastelloy, Gold, Diamond<br />
Length of Light Guide Standard 150 cm, optional up to 400 cm (with cooled detector )<br />
Measurement Principle ATR 45 °, double reflection<br />
Spectral Range Standard probe 3 to 18 µm (at standard length)<br />
Temperature Range -<strong>10</strong>0 to 150°C<br />
Pressure Range -1 up to <strong>10</strong>0 bar (up to 300 bar available upon request)<br />
Spectrometer FTIR-Spectrometer with light guide coupling, extendable standard software<br />
Detection Sensitivity < 1% (up to 0.02%)<br />
Detector MCT (mercury cadmium telluride), nitrogen-cooled, 3 -18 µm<br />
(3300 - 600 cm-1 ), thermo-electrical cooling 3 - 8 µm (3300 - 1250 cm-1 )<br />
Multiplexer Optional: six-fold Multiplexer, e.g. for parallel reactor systems<br />
Delivery Scope Compact, robust, FT-IR spectrometer with industry-hardened protective housing.<br />
MCT-detector (fl.N2), MIR, 12,000-600 cm-1, typical hold time: 8 h, incl. alignment optics.<br />
Diamond-ATR-Probe (MIR)<br />
Data System P4 > 3 GHz, 512 MB RAM, > 80 GB HDU, DVD-writer, LAN, 20“-<br />
TFT-flat screen monitor, colour printer, Windows XP Professional.<br />
Software package for analytics and research.<br />
Extensions Multiplexer unit for 6 probes<br />
Program for the establishment and control of process-relevant settings for cyclic<br />
measurements, communication with external process control systems (fieldbus or<br />
4-20 mA interfaces) and visualisation. The run-time component necessary for<br />
operation is included in the delivery scope. Communication with process control<br />
systems requires further hardware and, possibly, control-system specific<br />
programming.<br />
Program for the control of cyclic measurements, communication with external<br />
process control systems (fieldbus or 4-20 mA interfaces) and visualisation.<br />
Software package for quantitative analysis.<br />
Software package for chromatography-couplings<br />
Order Code Description<br />
IS-MOLECULEEYE MIR Spectrometer system with fibre-optic ATR diamond probe<br />
IS-MOLECULEEYEMUX Multiplexer unit for 6 probes<br />
Further accessories and extensions are available upon request. <strong>HiTec</strong> <strong>Zang</strong> also offers ready-to-use<br />
complete systems, individual components and special designs!<br />
If you have any special questions, our consultant engineer will gladly advise you. Test measurements can be<br />
conduced!<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
ParticleEye Particle Sizer<br />
LabKit-rc Reaction Calorimeter with ParticleEye-3D-Probe<br />
The ParticleEye In-Situ Particle Sizer enables the<br />
identification of geometrical particle characteristics<br />
and their respective changing conditions under test<br />
and production conditions already during the<br />
reaction.<br />
The unique dynamic focussing allows for an<br />
extensive measurement range of 0,5 to 4000 μm<br />
due to the continuous focus-depth variance.<br />
Multiple scatterings are not registered due to the<br />
patented opto-mechanical construction of the<br />
sensors. A laser beam is guided into the measuring<br />
probe through a single mode fibre with a diameter of<br />
merely 4 μm and dynamically focussed into the<br />
product intended for analysis by special optics.<br />
The dynamic focus represents the decisive<br />
advantage compared to conventional turbidimetry<br />
FBRM® (Registered Mettler-Toledo/Lasentec<br />
trademark).<br />
Features:<br />
� High Precision<br />
� Compact Construction<br />
� Robust<br />
� Ideal PAT-Sensor<br />
Options<br />
� In Situ stability control in the production process<br />
� Inline product monitoring in real time<br />
� Online quality control for the prevention of<br />
redundant laboratory analyses<br />
� Optimisation of the solid matter quality and purity<br />
� Improvement of productivity at the formulation of<br />
new products<br />
� Quality control 24h on 365 days throughout the<br />
year<br />
� Most simple function control of the PAT sensors<br />
due to the deployment of reticles<br />
� Improved control<br />
Applications<br />
� Crystallisation<br />
� Precipitation<br />
� Release<br />
� Fermentation<br />
� Homogenisation<br />
� Polymerisation<br />
� Agglomerations of Particle Systems<br />
� Dispersion<br />
� Granulation<br />
� Dissolution<br />
� Flocculation<br />
� Optimisation of Grinding Processes<br />
� Stability Analyses at Dispersed Phase Systems<br />
Advantages:<br />
� All particles are counted and presented as<br />
quantity distribution, length distribution,<br />
surface distribution, and volume distribution<br />
� Highest possible selectivity and sensitivity<br />
under original production conditions<br />
� Improvement of the safety at the scale up and<br />
production<br />
� Accelerated product development<br />
� High concentrations are possible<br />
� Measurement periods from 1 to 300 sec<br />
� Temperatures of -120°C to 220°C are possible<br />
� The additional option to in-situ sterilise the<br />
PAT sensors in deactivated condition up to a<br />
temperature of 165°C<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 229<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
230<br />
Sensors<br />
Available are dynamic 2D and 3D sensors with<br />
different characteristics.<br />
Process Analytics and Sensors<br />
Data Visualisation and Presentation<br />
The data evaluation can be conducted on the basis<br />
of the particle size distribution according to ISO<br />
66141.<br />
Measuring data is available in form of graphics and<br />
tables. Up to five distribution diagrams can be<br />
presented at the same time.<br />
Reference data, which may derives from previously<br />
recorded measurements or any other data which<br />
has been entered with the help of an integrated<br />
editor, can be faded into the distribution diagrams.<br />
For cumulative distributions, it is possible to<br />
additionally, or instead of the reference data, to fade<br />
in a distribution range of selectable band width.<br />
The presentation is available as cumulative curve or<br />
as trend diagram. Up to eight characteristics (of d<br />
01 to d99) can be presented as trend data, e.g. the<br />
transition variable according to DIN D0.1 to D99.9,<br />
count rate, intensity, fraction ratios, optional<br />
analogue signals 0V to <strong>10</strong>V or 4 to 20 mA. Any<br />
statistical moments from 0 to 3 can be utilised.<br />
Data Storage and Re-evaluation<br />
The distribution, statistical, respectively trend data<br />
available as measuring data can be exported to<br />
other programmes such as Word, Excel etc., and<br />
printed out or used otherwise in this form, via the<br />
clipboard.<br />
Measuring data in Excel format can be transported<br />
into a customer-related evaluation programme<br />
through a continuous data transfer.<br />
Measurable Products<br />
Over 6000 different products have already been<br />
measured. Why not take advantage from the<br />
experience of our product specialists?<br />
Measurable are all particles and drops that dispose<br />
of an optical reflection feature, reaching from<br />
aluminium oxide to sugar crystals.<br />
As the particles commence to agglomerate as of a<br />
concentration of 1Vol%, the particle collectives are<br />
usually at hand as particle systems (PSyA) under<br />
process conditions. The respectively generated<br />
particular fingerprints therefore represent<br />
reproducible characteristics for the PAT control.<br />
Due to the ascertainability of agglomerate<br />
structures, you can consequently cover broader<br />
particle distributions compared to a laser diffraction<br />
spectrometer (PSD). It is possible to present the<br />
total scope of your products as variable<br />
characteristic via the time.<br />
The measurements with PAT sensors in original<br />
concentrated products therefore present fingerprints<br />
of the actual particle system distribution under<br />
production conditions!<br />
The changes during production are collected and<br />
presented in-situ, therefore under original condition,<br />
by the PAT sensors.<br />
If the products intended for measurement are diluted<br />
online, the sensors will register the particle size<br />
distribution of the discretely existent particles<br />
continuously as under laboratory conditions.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Application Examples<br />
Process Analytics and Sensors<br />
Process Particle Change Evaluation<br />
Drop Formation Drops of various<br />
components are<br />
homogenised<br />
Intrusion of pigments in<br />
emulsions<br />
Distribution of the drop<br />
formation during the<br />
polymerisation<br />
Distribution of pigments in<br />
the emulsion<br />
Drops increase in size and<br />
stabilise<br />
Significant shifting of the distribution<br />
After the emulsion is homogeneous, the<br />
emulsion raw data are subtracted from the data<br />
pigments + emulsion = distribution of the<br />
pigments<br />
Fine fraction reduced in favour of the coarse<br />
fraction<br />
Grinding – wet or dry Reduction of particle size Change of distribution – higher fine fraction<br />
Germ formation at<br />
precipitation<br />
Particle Breakage or<br />
Cleavage<br />
Particles grow out of the<br />
nanoscale<br />
Change of distribution – cumulative higher fine<br />
fraction<br />
Reduction of particle size Change of distribution – higher fine fraction –<br />
reduced coarse fraction<br />
Growth of the Particles Increase of particle size Change of distribution – higher coarse fraction<br />
Agglomeration and<br />
Coagulation Processes<br />
Particles form particle<br />
systems<br />
Change of distribution - higher coarse fraction –<br />
reduced fine fraction<br />
Dissolution Particles dissolve Reduction of number of counts<br />
Change of form at the<br />
Crystallisation<br />
Sensor Head with Measuring Window<br />
Technical Data:<br />
Particles deform Change of distribution function<br />
Pressure 3 bar, optional to 64 bar<br />
Measuring Medium<br />
Temperature<br />
5...85°C, optional -120...20°C, 5° to 125°C, -20..165°C, 5 to 220°C<br />
Parts in contact with High Grade Steel 1.4571, sulphur-free, optional Hastelloy C276, Hastelloy C2,<br />
Measuring Medium Hastelloy C4, Sapphire Glass, Hifluor (FKM)® or Kalrez<br />
Sensor/Probe Length 260 mm, optional 350mm<br />
Sensor Diameter 8mm, 18mm or 22mm<br />
Sensor Cable Length <strong>10</strong>m<br />
Sensor Window Sapphire Glass, Quality Category MIL– PRF-1383B <strong>10</strong>-5<br />
Sensor Protection Category IP 68<br />
Scanner Speed 1 m/s, optional 2m/s<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 231<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
232<br />
Technical Data:<br />
Configuration Examples<br />
Process Analytics and Sensors<br />
Device Configuration Characteristics<br />
2D ORM (optical backreflection) passive Signal<br />
Capture System >5 µm exclusively based on the<br />
duration of the particles in the focus for consistent<br />
Reynold numbers.<br />
2D ORM active Signal Capture System >2µm based<br />
on the patented sensor technology (see above) plus<br />
runtime-levelling signal capture method.<br />
3D ORM active Signal Capture System >2µm with<br />
in-depth focus based on a controlled 3mW laser<br />
3D ORM active Signal Capture >0.8µm with in-depth<br />
focus + Selective Scanning based on a controlled<br />
5mW laser system and double screening.<br />
3D ORM IPAS active Signal Capture System >1µm<br />
with in-depth focus + Selective Scanning + controlled<br />
open signal system based on a <strong>10</strong>mW laser system,<br />
regulable between1 and <strong>10</strong>mW with multiple<br />
screening.<br />
APAS active Multi Capture Signal Capture System<br />
>500nm with 3D ORM in-depth focus + Selective<br />
Scanning (SMF)+ controlled open signal system<br />
based on a 25mW laser system, regulable between1<br />
and 25mW with multiple screening.<br />
„Multiscattering“ Signals and turbidity are not<br />
processed by the patented sensor technology.<br />
Counting of all captured particles and their size.<br />
Especially designed for rough industrial deployment<br />
– no moving parts in the sensor.<br />
Upgraded through a dynamic scanning system and a<br />
consequently higher count rate.<br />
Upgraded through in-depth scanning and better<br />
resolution.<br />
Upgraded through dynamic and controlled in-depth<br />
scanning and better resolution.<br />
Partially open system for R&D tasks based on the<br />
APAS system. Input raw signals from the sensor are<br />
trapped and are, if required, available to the<br />
researchers.<br />
Advanced Particle Analysing System. Completely<br />
open System for R & D tasks. Input raw signals from<br />
the sensor, as well as the signals of the individual<br />
processing steps, are trapped and are, if required,<br />
available to the researchers.<br />
Order Code Description<br />
IS-PARTICLEYE-S- l ParticleEye Particle Measurement System, static; comprises sensor, electronics and software<br />
module<br />
IS-PARTICLEYE- 2D-l ParticleEye Particle Measurement System, dynamic 2D; comprises sensor, electronics and<br />
software module<br />
IS-PARTICLEYE- 3D-l-t ParticleEye Particle Measurement System, dynamic 3D; comprises sensor, electronics and<br />
software module<br />
IS-PARTICLEYE-AA6 6 Analogue Outputs 4...20mA for ParticleEye Particle Measurement System<br />
IS-PARTICLEYE-EEX Ex-Equipment for ParticleEye Particle Measurement System<br />
IS-PARTICLEYE- WV <strong>Main</strong>tenance Contract for ParticleEye Particle Measurement System<br />
l: Sensor Length :<br />
t: according to table, only concerns 3D sensor.<br />
Type Measurement<br />
Range in µm<br />
Max. Concentration<br />
in %<br />
125 0,5 – 125 80<br />
250 1 – 250 60<br />
500 1 - 500 50<br />
<strong>10</strong>00 2 - <strong>10</strong>00 40<br />
2000 5 - 2000 30<br />
3000 30 - 3000 25<br />
4000 20 - 4000 20<br />
Options:<br />
� Special Materials<br />
� Other Sensor Forms and Diameters<br />
� EEX-Version<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Turbidity Probe<br />
Process Analytics and Sensors<br />
Turbidity measurement probe in a high-grade steel<br />
protective tube. Probe measures in retro-reflection<br />
(backscatter) with IR-light (880nm). The diameter is<br />
12 mm, the length between 120 and 407 mm. The<br />
optical window is made of sapphire and sealed with<br />
a Kalrez- sealing ring (FDA-conform).<br />
Applications:<br />
� Crystallisation<br />
� Precipitation<br />
� Releasing<br />
� Fermentation<br />
Characteristics:<br />
� High Accuracy<br />
� Compact Construction<br />
� Robust<br />
Technical Data:<br />
Measurement Principle Retro-reflection (backscatter)<br />
Measured Material Temperature –30...130°C<br />
Temperature<br />
Pressure 0...6 bar<br />
Parts in Contact with<br />
Measured Material<br />
High-grade steel 1,4404 or 1,4435, sapphire, Kalrez<br />
Probe Tube Dimensions of probe 12 x 120/205/297/407 mm<br />
Measurement Range <strong>10</strong>...4000 FTU (display in other measurement units possible)<br />
Output signal 0/4...20 mA<br />
Operational Voltage Transmitter <strong>10</strong>0...240 V AC<br />
Protection Category Transmitter sealed front-side, resulting protection category dependant of mounting<br />
EEX EEX probe category 1...3, Zone 0...2, T4...T6<br />
Connection to the LabManager:<br />
The probe is delivered ready to connect with a cable and a Tuchel plug for the direct connection to an<br />
analogue input panel AEP8A. Please coordinate the feed with our project department.<br />
Order Code Description<br />
IS-TRUB-O-ea Turbidity probe made of high-grade steel 1,4404, for direct connection to an analogue input panel<br />
ea=Electrical Connection:<br />
T Tuchel plug for LabManager<br />
O Open ends for MSRmanager<br />
Order Example:<br />
Turbidity probe made of high-grade steel 1,4571,<br />
probe tube <strong>10</strong> mm, with connection 1.5 m for<br />
LabManager Panel LP-AEP8A, coordinate the probe<br />
length with our project department when placing<br />
order.<br />
Order Code: IS-TRUB-O-O<br />
Available upon request:<br />
� Materials: Hastelloy C4<br />
� other probe designs and diameters<br />
� EEX Versions<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 233<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
234<br />
Process Analytics and Sensors<br />
Fibre-Optic Submersible Reflection Probes<br />
With the Superior Optical Material –<br />
Sapphire<br />
These reflection submersion probes convince with a<br />
robust design and an uncompromising choice of<br />
materials regarding all parts in contact with media.<br />
With sapphire as optical material, they are virtually<br />
absolutely resistant to abrasion and corrosion and<br />
therefore also stable when deployed with<br />
concentrated acids and bases. They are also<br />
resistant against pressure and temperature peaks.<br />
The application range reaches from the simple<br />
turbidity measurement in liquids right to the<br />
characterisation of solids. All probes are designed<br />
for the direct installation into vessels and tubings.<br />
They can be flexibly aligned to individual<br />
requirements, due to the diversity of available<br />
materials, process connections, pressure and<br />
temperature ranges.<br />
Advantages:<br />
� abrasion and corrosion-free sapphire optics<br />
� chemical stability<br />
� verifiable process suitability<br />
� application range from UV to NIR<br />
� compatible with all spectrometer types<br />
� varied versions and special designs<br />
� robust and extremely stable<br />
The application range reaches from the simple<br />
turbidity measurement with fibre-optic turbidity<br />
measurement systems right to the identification and<br />
characterisation of solids.<br />
Technical Details<br />
Typical Applications<br />
� Reaction tracing of heterogeneous reactions in<br />
the chemical synthesis in the NIR<br />
� determination of residual solvent concentration at<br />
solids directly in driers<br />
� Homogeneity of solid compounds directly in the<br />
mixer<br />
Our product portfolio is not restricted to fibre-optical<br />
probes. It includes everything you may need for the<br />
implementation of probes in processes and the<br />
coupling to practically every spectrometer type.<br />
You can rely on us to find an ideal solution!<br />
Light Spot 1 mm<br />
Dimension<br />
6 mm<br />
Diameter<br />
Alternative 12 mm<br />
Submersion Depth As of <strong>10</strong>0 mm<br />
Standard Materials High-grade steel DIN 1,4435/316L, sapphire<br />
Process Connections DIN or ANSI flanges<br />
Screwings e.g. Swagelok, PG 13.5, further connections available upon request<br />
Temperature max. 280°C (continuous operation)<br />
Pressure 0–<strong>10</strong>0 bar<br />
Order Code Description<br />
IS-TRUB-ORF-ea Fibre-optic reflection probe<br />
ea=Electrical Connection:<br />
T Tuchel plug for LabManager<br />
O Open ends for MSRmanager<br />
Options:<br />
Alternative materials: high-grade steel DIN 1.4571 /<br />
SS316Ti, Titanium, Hastelloy, PVDF, PP, PTFE, etc.<br />
Further constructions, dimensions, and<br />
specifications available upon request.<br />
Conformity Statement 97/23/EU according to EU<br />
Pressure Equipment Directive.<br />
You can find fibre-optic probes for the MIR sector<br />
under „MoleculeEye“.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
Phase boundary Detector<br />
The <strong>HiTec</strong> <strong>Zang</strong> PhaDec is a robust and costefficient<br />
detector system for the detection of phase<br />
boundaries. PhaDec is in particular used for the<br />
automatic separation and separate bottling of liquid<br />
phases out of reactors or collecting vessels, e.g.<br />
after reactions with phase transfer catalysis, after<br />
azeotropic distillations or after extractions.<br />
<strong>Main</strong> Application Areas:<br />
� Extraction<br />
� Extractive Distillation<br />
� Azeotropic Distillation<br />
� Phase Transfer Catalysis<br />
Other Application Areas:<br />
� Filling Level Monitor<br />
� Flow Monitor<br />
� Leakage Monitor<br />
PhaDec utilises the different heat conductivity of the<br />
phases to recognise the boundary areas. Therefore,<br />
the application of the PhaDec is not limited to<br />
transparent or conductive liquids. Deployed as<br />
sensor is a special resistance sensor, which can<br />
also be used as a temperature sensor.<br />
The sensor can optionally be installed into the base<br />
discharge valve, the discharge line or into the<br />
reaction vessel from above.<br />
Advantages<br />
� Robust and cost-effective<br />
� Integrateable into any system<br />
� Universally applicable for all liquid phases –<br />
even at non-transparent and non-conductive<br />
fluids<br />
� Pressure-resistant and chemically stable<br />
� Also deployable as temperature sensor<br />
� Inert materials: glass, high-grade steel,<br />
Hastelloy, PEEK, PTFE<br />
Technical Data Phadec<br />
PI-Connectors to Pt<strong>10</strong>0-Input, Analog Input, Analog Output, Digital output<br />
Cable Length 200 cm (modification possible)<br />
Ambient Temperature -20 up to +70 °C<br />
Technical Data Phadec-x<br />
PhaDec operates with virtually all fluids, regardless<br />
whether liquid or gas, conductive or not conductive,<br />
transparent or not. As long as there is a clear phase<br />
boundary, the PhaDec will generate evaluable<br />
signals.<br />
The sensor is available with all known jacket<br />
materials. A preliminary lead time for the discharge<br />
of the main part of the lower phase is considered in<br />
the basis operation.<br />
The reaction period of the PhaDec depends on the<br />
type of sensor deployed. Sensors with a metal jacket<br />
and small outer dimensions react most rapidly. For<br />
quick response, we recommend an exterior diameter<br />
236<br />
Level Sensor<br />
Robust high-quality level sensor for industrial<br />
applications.<br />
� High Accuracy<br />
� Compact Construction<br />
Conductive Liquids > 1 μScm -1<br />
� Limit Area Detection<br />
to Liquids < 1 μScm -1<br />
Technical Data:<br />
Process Analytics and Sensors<br />
Measurement Principle Conductometric via scattering potential<br />
Measurement Media<br />
Temperature<br />
Max. 180°C<br />
Parts in Contact with<br />
Measurement Media<br />
High-grade steel 1,4571, Hastelloy available upon request<br />
Probe Tube d = <strong>10</strong> mm<br />
Measurement Range According to customer specifications<br />
Output Signal 0 - <strong>10</strong> V DC<br />
Supply Voltage ± 15 V DC<br />
Protection Category IP 54<br />
EEX Upon request<br />
Connection to the LabManager:<br />
The probe is delivered ready to connect with a cable<br />
and a Tuchel plug for the direct connection to an<br />
analogue input panel AEP8A. Please coordinate the<br />
feed with our project department.<br />
Order Code Description<br />
IS-L-FA-ea Level pick-up sensor, conductometric, made of high-grade steel 1,4571, probe tube<br />
<strong>10</strong>mm, with connection cable 1.5m for LabManager Panel LP-AEP8A<br />
ea=Electrical Connection:<br />
T Tuchel plug for LabManager<br />
O Open ends for MSRmanager<br />
Please coordinate the probe length with our project<br />
department when placing order!<br />
Order Example:<br />
Level pick-up sensor, conductometric, made of highgrade<br />
steel 1,4571, probe tube <strong>10</strong>mm, with<br />
connection cable 1.5m for LabManager Panel LP-<br />
AEP8A<br />
Please coordinate the probe length with our project<br />
department when placing order!<br />
Order Code: IS-L-FA-T<br />
available upon request:<br />
� Materials: Hastelloy C4<br />
� other probe designs and diameters<br />
� Float, PTC thermistor, ultrasonic, radar,...flow<br />
sensors and monitors<br />
� EEX Versions<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Teflon ® Flow Sensors<br />
Process Analytics and Sensors<br />
Due to new manufacturing technologies, the parts in<br />
contact with media of the Teflon flow sensors are<br />
completely made of Teflon ® and ruby. The resulting<br />
special properties, in particular the excellent<br />
resistance against most chemicals, give the sensor<br />
the suitability for a wide application range. The ruby<br />
bearing minimises friction and wear and guarantees<br />
high durability.<br />
Versatile: The One-Way - Click - Sensor (open)<br />
This outstanding product received an award at the<br />
„Salon International des Innovations“ in Geneva and<br />
is internationally protected by patent.<br />
For the high-pressure range, the sensors are also<br />
available in a high-grade steel casing.<br />
The Advantages<br />
� low cost<br />
� maintenance-free<br />
� sealless<br />
� extremely compact<br />
� little pressure decline<br />
� great flow range<br />
� Ex- version available<br />
� high working pressure range<br />
� high chemical resistance<br />
� sterilisable version (up to 160 °C)<br />
� one-way version for hardening materials<br />
� optionally, threaded or hose connection<br />
� high resolution (up to 1<strong>10</strong>.000 impulses per<br />
litre)<br />
� high durability and consistency due to ruby<br />
bearings<br />
� little response time due to low-mass rotor<br />
(approx. 15 mg)<br />
Application Areas<br />
� Chemical Industry<br />
� Pharmaceutical industry<br />
� Bio-Technology<br />
� Food Technology<br />
� Flow Measurement<br />
� Dosing of Feed Tanks<br />
� Continuous Dosing<br />
� Bottling and Charging<br />
� Flow Monitoring<br />
� Consumption Counter<br />
� Heat Counter<br />
The flow generating part of the sensor can easily be<br />
exchanged in case of hardening media and sterilised<br />
with up to 120 °C.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 237<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
238<br />
The Functional Principle<br />
Process Analytics and Sensors<br />
The media is put into a rotational motion by a spiral<br />
flow former (worm) and actuates the virtually<br />
weightless rotor.<br />
The rotor is optically scanned in the course of which<br />
a frequency-analogue rectangular signal<br />
proportional to the flow speed is generated. This<br />
can, if necessary, be transformed to current, voltage<br />
or serial signals with one of the available measuring<br />
transducers.<br />
As the optical scan, at the light guide models, is<br />
conducted via a cable which is up to 40 m long, the<br />
sensors are particularly suited for the EX area.<br />
The sensor also operates with turbid media such as<br />
ink or diffuse media such as milk. Problems are only<br />
to be expected in case of strongly light scattering<br />
media such as latex or suspensions with titanium<br />
dioxide. Solid particles usually do not interfere.<br />
Merely fibres should be removed by a filter.<br />
Sensor Type Series S4.5 / 0.1 – 1.5 l / min<br />
The sensors of the type series S4.5 are available<br />
with hose and threaded connection. The connection<br />
cable of the standard version is cladded with Tefzel,<br />
a plastic material with properties similar to Teflon,<br />
but better elasticity.<br />
Technical Data<br />
Available Versions<br />
The sensors are available with the nominal widths<br />
4.5 mm, 8.5 mm and 12.5 mm, respectively with<br />
copper or light guide cable connection. The nominal<br />
widths 4.5 and 8.5 mm are only available in the<br />
standard version or as click-sensor with hose or<br />
threaded connection. The nominal width 12.5 mm, in<br />
the standard version, is available with threaded<br />
connection.<br />
The light-guide version is particularly suited for<br />
applications in explosive environments or in case of<br />
higher temperatures.<br />
The Click-sensor version enables sterilisation up to<br />
160°C, as well as the exchange of the measuring<br />
insert in case of hardened media.<br />
Measurement Range 0.06-2 litres/min<br />
Nominal Width 4.5 mm<br />
Connection for Media Hose nozzle 7mm or 1/8“ conical outer thread NPT<br />
Working Pressure 20 bar / 2MPa<br />
Pressure Decline approx. 200 mbar at 75% flow<br />
Max. Temp. Media 80 °C, with plastic light-guide 1<strong>10</strong> °C, with glass light-guide 180 °C<br />
Viscosity Range 0.8-<strong>10</strong>mm²/s, higher with calibration<br />
Signal Line TEFZEL® or light guide<br />
Output Signal 1<strong>10</strong>.000 Impulses = 1l<br />
Output Frequency <strong>10</strong>0 Hz - 3.1 kHz<br />
Reproducibility ± 0.15 %<br />
Linearity Faults ± 1%<br />
Protection Category IP 65, Click-Sensor IP 50<br />
Length 52 mm<br />
Max. Diameter 17 mm<br />
Length of Cable Intake 47 mm<br />
* The measurement range, in case of reduced demands to linearity, can be extended.<br />
Special designs for increased linearity in case of<br />
very low flows are available upon request. The<br />
stated values and measurement values are based<br />
on laboratory measurements with water at 20°C, as<br />
well as the manufacturer's statements in regard to<br />
the properties of the materials. The manufacturer<br />
reserves the right to modify/align the specifications<br />
to the state of the technology at any time.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
Measuring Transducer<br />
Standard version available with:<br />
� Transducer 6<strong>10</strong>0 with different signal outputs<br />
� Flow Calculator 6200<br />
� Dosing Calculator 6500<br />
� Plug for direct connection to <strong>HiTec</strong> <strong>Zang</strong><br />
LabManager<br />
� Connections according to customer specifications<br />
The light-guide version requires transducer 6700IR.<br />
For Order Code see the table “Order Codes“.<br />
Sensor Type Series S8.5 / 0.8 - 20 l / min<br />
The sensors of the type series S8.5 are available<br />
with hose and threaded connection. The connection<br />
cable of the standard version is cladded with Tefzel,<br />
a plastic material with properties similar to Teflon,<br />
but better elasticity.<br />
Technical Data<br />
IS-F-0045.T.H.P.01.DX disposable sensor with tubing connector<br />
The light-guide version is particularly suited for<br />
applications in explosive environments or in case of<br />
higher temperatures.<br />
The Click-sensor version enables sterilisation up to<br />
160°C, as well as the exchange of the measuring<br />
insert in case of hardened media.<br />
Measurement Range 1.0-20 litres/min<br />
Nominal Width 8.5 mm<br />
Connection for Media Hose nozzle 12mm or 1/4´´ conical outer thread NPT<br />
Working Pressure 15 bar / 1.5MPa<br />
Pressure Decline approx. 200 mbar at 75% flow<br />
Max. Temp. Media 80 °C, with plastic light guide 1<strong>10</strong> °C, with glass light guide 180 °C<br />
Viscosity Range 0.8-<strong>10</strong>mm²/s, higher calibration<br />
Signal Line TEFZEL® or light guide<br />
Output Signal 6.350 Impulses/litre = 1Impulss/157µl<br />
Output Frequency 40 Hz - 2.2 kHz<br />
Reproducibility ± 0.15 %<br />
Linearity Fault ± 1.5 %<br />
Protection Category IP 65, Click-Sensor IP 50<br />
Length 60 mm<br />
Max. Diameter 22 mm<br />
Length of Cable Intake 47 mm<br />
* The measurement range, in case of reduced demands to linearity, can be extended.<br />
Special designs for increased linearity in case of<br />
very low flows are available upon request. The<br />
stated values and measurement values are based<br />
on laboratory measurements with water at 20°C, as<br />
Measuring Transducer<br />
Standard version available with:<br />
� Transducer S6000 u. S6<strong>10</strong>0 with different signal<br />
outputs<br />
� Flow Calculator 6200<br />
� Dosing Calculator 6500<br />
� Plug for direct connection to <strong>HiTec</strong> <strong>Zang</strong><br />
LabManager<br />
� Connections according to customer specifications<br />
well as the manufacturer's statements in regard to<br />
the properties of the materials. The manufacturer<br />
reserves the right to modify/align the specifications<br />
to the state of the technology at any time.<br />
The light-guide version requires transducer 6700 IR.<br />
For Order Code see the table “Order Codes“.<br />
Type IS-F-0085.T.P.01.XX<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 239<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
240<br />
Process Analytics and Sensors<br />
Sensor- The sensors Type of the type Series series S12.5 S 12.5 / have 2.5 a-<br />
40 l / min<br />
threaded connection. The connection cable of the<br />
standard version is cladded with Tefzel, a plastic<br />
material with properties similar to Teflon, but better<br />
elasticity.<br />
Technical Data<br />
The light-guide version is particularly suited for<br />
applications in explosive environments or in case of<br />
higher temperatures.<br />
Measurement Range 2-40 litres /min<br />
Nominal Width 12.5 mm<br />
Connection for Media 1/2“´outer thread BSP<br />
Working Pressure <strong>10</strong> bar max.<br />
Working Pressure approx. 200 mbar at 75% flow<br />
Max. Temp. Media 80 °C, with plastic light guide 1<strong>10</strong> °C, with glass light guide 180 °C<br />
Viscosity Range 0.8 - <strong>10</strong> mm²/s, higher with calibration<br />
Signal Line TEFZEL® or Light Guide<br />
Output Signal 2050 Impulses/litre = 1 Impulse/488µl<br />
Output Frequency 22 - 1200 Hz<br />
Reproducibility ± 0.15 %<br />
Linearity Fault ± 3 %<br />
Protection Category IP 65<br />
Length 72 mm<br />
Max. Diameter 26 mm<br />
Length of Cable Intake 47 mm<br />
* The measurement range, in case of reduced demands to linearity, can be extended.<br />
Special designs for increased linearity in case of<br />
very low flows are available upon request. The<br />
stated values and measurement values are based<br />
on laboratory measurements with water at 20°C, as<br />
Measuring Transducer<br />
Standard version available with:<br />
� Transducers S6000 and S6<strong>10</strong>0 with different<br />
signal outputs<br />
� Flow Calculator 6200<br />
� Dosing Calculator 6500<br />
� Plug for direct connection to <strong>HiTec</strong> <strong>Zang</strong><br />
LabManager<br />
� Connections according to customer specifications<br />
The light-guide version requires transducer 6700 IR.<br />
For Order Code see the table “Order Code”.<br />
well as the manufacturer's statements in regard to<br />
the properties of the materials. The manufacturer<br />
reserves the right to modify/align the specifications<br />
to the state of the technology at any time.<br />
Type IS-F-0125.T.B.P.01.XX with screwing connection<br />
Documentation to the special version up to 200 bars is forwarded upon request!<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Signal Connection<br />
Process Analytics and Sensors<br />
For the uncomplicated integration into your<br />
automation technology, measuring transducer-power<br />
supply units are available with the usual standard<br />
signals. The sensors can be directly connected to<br />
the <strong>HiTec</strong>-PIs with HK-DEA16N cards via special<br />
cables (IS-F-LABTUC) without a separate<br />
measuring transducer. For independent operation,<br />
flow calculators and dosing controller- components<br />
are available.<br />
The sensors, in the standard version, can also be<br />
operated without measuring transducer-power<br />
supply unit. The supply voltage is 5 V at approx. 15<br />
mA, the amplitude of the output signal is approx. 3 V<br />
at min. load resistance 1 kOhm.<br />
Working Range<br />
The sensors are available for the measurement<br />
ranges 0.1 – 1.5l/min, 0.8-18l/min and 2-40l/min.<br />
The specifications apply for the viscosity range of<br />
0.8-<strong>10</strong> mm²/s (water at 20 °C = 1chour = 1mm²/s,<br />
lubricating oil SAE30 at <strong>10</strong>0°C or ISO VG<strong>10</strong> at 40 °C<br />
= approx. <strong>10</strong> mm²/s).<br />
PFA Disposable Turbine Flowmeters - 5-30 V DC power supply series<br />
The sensors can also be deployed beyond this<br />
range, if it is taken into consideration that this leads<br />
to a change of the impulse rate and the calibration.<br />
The upper limit of the viscosity then accords to the<br />
viscosity of liquids with a similar viscosity as<br />
shampoo.<br />
Any mounting position is possible.<br />
Special Designs<br />
Upon request, special designs are available. If the<br />
standard versions do not meet your demands, do<br />
not hesitate to contact us. We will do our best to help<br />
you.<br />
Examples<br />
Special designs in high-grade steel up to 200 bar,<br />
special connections, special cable materials,<br />
modified flow ranges, special dosing and flow<br />
controls.<br />
Order Code Description Connection Flowrate l/min<br />
IS-F-0045.T.H.P.01.DX PFA turbine flowsensor 4.5 disposable 7 mm hosebarb 0,06 - 2,0<br />
IS-F-0045.T.H.0.00.DX PFA tube 4.5 only 7 mm hosebarb 7 mm hosebarb 0,06 - 2,0<br />
IS-F-0045.P.X.P.01.DX Electronics 4.5 only - -<br />
IS-F-0045.T.N.P.01.DX PFA turbine flowsensor 4.5 disposable 1/8" NPT 0,06 - 2,0<br />
IS-F-0045.T.N.0.00.DX PFA tube 4.5 only 1/8" NPT 1/8" NPT 0,06 - 2,0<br />
IS-F-0045.P.X.P.01.DX Electronics 4.5 only - -<br />
IS-F-0085.T.H.P.01.DX PFA turbine flowsensor 8.5 disposable 12 mm hosebarb 0,5 - 20,0<br />
IS-F-0085.T.H.0.00.DX PFA tube 8.5 only 12 mm hosebarb 12 mm hosebarb 0,5 - 20,0<br />
IS-F-0085.P.X.P.01.DX Electronics 8.5 only - -<br />
IS-F-0085.T.N.P.01.DX PFA turbine flowsensor 8.5 disposable 1/4" NPT 0,5 - 20,0<br />
IS-F-0085.T.N.0.00.DX PFA tube 8.5 only- 1/4" Thread 1/4" NPT 0,5 - 20,0<br />
IS-F-0085.P.X.P.01.DX Electronics 8.5 only - -<br />
PFA Disposable Turbine Flowmeters; 5 V DC series Low Voltage<br />
Order Code Description Connection Flowrate l/min<br />
IS-F-0045.T.H.P.01.DL PFA disposable turbine flowsensor 4.5 - 5 Vdc 7 mm hosebarb 0,06 - 2,0<br />
IS-F-0045.T.H.0.00.DX PFA tube 4.5 only 7 mm hosebarb 7 mm hosebarb 0,06 - 2,0<br />
IS-F-0045.P.X.P.01.DL Electronics 4.5 only - 5 Vdc - -<br />
IS-F-0045.T.N.P.01.DL PFA disposable turbine flowsensor 4.5 - 5 Vdc 1/8" NPT 0,06 - 2,0<br />
IS-F-0045.T.N.0.00.DX PFA tube 4.5 only 1/8" NPT 1/8" NPT 0,06 - 2,0<br />
IS-F-0045.P.X.P.01.DL Electronics 4.5 only - 5 Vdc - -<br />
IS-F-0085.T.H.P.01.DL PFA disposable turbine flowsensor 8.5 - 5 Vdc 12 mm hosebarb 0,5 - 20,0<br />
IS-F-0085.T.H.0.00.DX PFA tube 8.5 only 12 mm hosebarb 12 mm hosebarb 0,5 - 20,0<br />
IS-F-0085.P.X.P.01.DL Electronics 8.5 only - 5 Vdc - -<br />
IS-F-0085.T.N.P.01.DL PFA disposable turbine flowsensor 8.5 - 5 Vdc 1/4" NPT 0,5 - 20,0<br />
IS-F-0085.T.N.0.00.DX PFA tube 8.5 only- 1/4" Thread 1/4" NPT 0,5 - 20,0<br />
IS-F-0085.P.X.P.01.DL Electronics 8.5 only - 5 Vdc - -<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
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technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 241<br />
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Components<br />
Process Analytics<br />
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Dispersing<br />
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PFA Turbine Flowmeters Fixed - 5-30 Vdc power supply series<br />
Order Code Description Connection Flowrate l/min<br />
IS-F-0045.T.H.P.01.XX PFA turbine flowsensor 4.5 7 mm hosebarb 0,06 - 2,0<br />
IS-F-0045.T.N.P.01.XX PFA turbine flowsensor 4.5 1/8" NPT 0,06 - 2,0<br />
IS-F-0085.T.H.P.01.XX PFA turbine flowsensor 8.5 12,5 mm hosebarb 0,5 - 20,0<br />
IS-F-0085.T.N.P.01.XX PFA turbine flowsensor 8.5 1/4" NPT 0,5 - 20,0<br />
IS-F-0125.T.B.P.01.XX PFA turbine flowsensor 12.5 1/2" BSP/NPT 2,0 - 40,0<br />
PFA Turbine Flowmeters Fixed; 5 Vdc series Low Voltage<br />
Order Code Description Connection Flowrate l/min<br />
IS-F-0045.T.H.P.01.XL PFA turbine flowsensor 4.5 - 5 Vdc 7 mm hosebarb 0,06 - 2,0<br />
IS-F-0045.T.N.P.01.XL PFA turbine flowsensor 4.5 - 5 Vdc 1/8" NPT 0,06 - 2,0<br />
IS-F-0085.T.H.P.01.XL PFA turbine flowsensor 8.5 - 5 Vdc 12 mm hosebarb 0,5 - 20,0<br />
IS-F-0085.T.N.P.01.XL PFA turbine flowsensor 8.5 - 5 Vdc 1/4" NPT 0,5 - 20,0<br />
IS-F-0125.T.N.P.01.XL PFA turbine flowsensor 12.5 - 5 Vdc 1/2" BSP/NPT 2,0 - 40,0<br />
Stainless Steel Turbine Flowmeters - 5-30 Vdc power supply series<br />
Order Code Description Connection Flowrate l/min<br />
IS-F-0045.S.N.P.01.XX SS Turbine flowsensor 4.5 NPT 1/4" NPT 0,06 - 2,0<br />
IS-F-0045.S.B.P.01.XX SS Turbine flowsensor 4.5 BSP 1/4"BSP 0,06 - 2,0<br />
IS-F-0085.S.N.P.01.XX SS Turbine flowsensor 8.5 NPT 3/8" NPT 0,5 - 20,0<br />
IS-F-0085.S.B.P.01.XX SS Turbine flowsensor 8.5 BSP 3/8" BSP 0,5 - 20,0<br />
IS-F-0125.S.N.P.01.XX SS Turbine flowsensor 12.5 NPT 1/2" NPT 2,0 - 40,0<br />
IS-F-0125.S.B.P.01.XX SS Turbine flowsensor 12.5 BSP 1/2"BSP 2,0 - 40,0<br />
PVDF Disposable Turbine Flowmeters 5-30 Vdc<br />
Order Code Description Connection Flowrate l/min<br />
IS-F-0045.P.H.0.00.CX PVDF Disposable rotor tube 4.5; Hose Barb; Clip<br />
mounting<br />
0,03 - 2,0<br />
IS-F-0085.P.H.P.01.CX PVDF Disposable Turbine Flowmeter 8.5; Hose Barb; 5-30 Vdc;<br />
Clip<br />
0,3 - 20,0<br />
IS-F-0085.P.H.0.00.CX PVDF Disposable rotor tube; Hose Barb; Clip<br />
mounting<br />
0,3 - 20,0<br />
IS-F-0000.P.X.P.01.CX Electronic pick-up; 5 - 30 Vdc; clipmounting -<br />
IS-F-0045.X.X.X.00.CX Mounting Clip in behalf of the 0045 flowmeters -<br />
IS-F-0085.X.X.X.00.CX Mounting Clip in behalf of the 0085 flowmeters - -<br />
Dosing pumps monitors<br />
In connection with a projected flow through sensor<br />
the monitor can measure and validate the flow .<br />
The dosing pump monitors can be controlled via<br />
RS232, USB, Ethernet or optionally via an analogue<br />
interface.<br />
Order Code Description<br />
IS-F-S601-P2 Dosing pumps monitors for monitoring of flow rates from 0,06 to 2 l/min<br />
IS-F-S601-P20 Dosing pumps monitors for monitoring of flow rates from 0,5 to 20 l/min<br />
IS-F-S601-P40 Dosing pumps monitors for monitoring of flow rates from 1,5 to 40 l/min<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Measuring Transducer<br />
LAB-PI-Connection Cable<br />
Process Analytics and Sensors<br />
The electronics integrated into this connection cable<br />
supplies the sensor with current and aligns the<br />
frequency-analogue sensor output signal with a<br />
digital input with frequency counting options of a<br />
Lab-PI. The cable is fixed to the sensor and can be<br />
directly connected to a digital input with a 24V DC<br />
transducer power supply unit (LP-DEP8A).<br />
Technical Data<br />
Supply Voltage 24V DC, via LAB-PI<br />
Current Consumption < 50 mA<br />
Output signal Level 23 V rectangular<br />
Output Signal 0 – 2.5 kHz (sensor frequency)<br />
Cable Length 200 cm (modification possible)<br />
Ambient Temperature -20 up to +70 °C<br />
Suited for the sensor type series: S4.5/8.5/12.5PFA-H/T/D-T<br />
Not available for sensors in light guide version!<br />
Order Code Description<br />
IS-F-LABTUC Level converter and supply for flow sensor with Tuchel plug for digital input<br />
Measuring Transducer 6<strong>10</strong>0 D/A<br />
The measuring 6<strong>10</strong>0 D/A supplies the sensor with<br />
current and converts the frequency-analogue sensor<br />
output signal into the electrical standard signals<br />
0V...<strong>10</strong>V or 0 / 4 - 20mA for further processing in the<br />
automation devices with voltage or current inputs.<br />
The current outputs are passive (without current).<br />
Technical Data<br />
Power supply 12 - 30 V DC or 115 – 240 V DC<br />
Current Consumption < 50 mA<br />
Output Signal 0 / 4 - 20 mA or 0V ... <strong>10</strong>V<br />
Width 71 mm<br />
Height 71 mm<br />
Depth 90 mm<br />
Protection Category IP30<br />
Ambient Temperature -20 to +70 °C<br />
Suited for the sensor type series: S4.5/8.5/12.5 cable types P and T<br />
Order Code Description<br />
IS-F-6300.BA.CON.DC.XX Measuring transducer 0-<strong>10</strong>V, 0/4 - 20 mA and supply for flow sensor<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Automation<br />
Hardware<br />
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Software<br />
Plant<br />
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Process Analytics and Sensors<br />
Measuring Transducer 6700 D/A for Light Guide Sensors<br />
The measuring transducer 6700 D/A supplies the<br />
sensor with current and converts the frequencyanalogue<br />
sensor output signal into the electrical<br />
standard signals 0 / 4 - 20mA for further processing<br />
in the automation devices with voltage or current<br />
inputs.<br />
Technical Data<br />
Supply Voltage 12 - 30V DC<br />
Current Consumption 230 mA<br />
Output Signal 0 / 4 - 20 mA<br />
Width 71 mm<br />
Height 71 mm<br />
Depth 90 mm<br />
Protection Type IP30<br />
Ambient Temperature -20 to +70°C<br />
Suited for the sensor type series: S4.5/8.5/12.5<br />
Cable Type F<br />
The current outputs are passive (without current).<br />
Order Code Description<br />
IS-F-6700-DA-CON-DC Measuring Transducer and supply for light guide sensors, output 0 - <strong>10</strong>V, 0/4 - 20mA<br />
Additional transducers upon request.<br />
Turbine Flow Sensor for Heat carrier Oil<br />
These flow sensors were developed for the<br />
measurement of the volume flow of water, fuel,<br />
heating oil, heat carrier oil, cooling agents,<br />
pharmaceutical, chemical and cryogenic liquids,<br />
liquid gases and solvents.<br />
Within the sector of the reaction calorimetry, they are<br />
particularly suited for the flow measurement of the<br />
heat carrier oil at temperatures of up to 350°C.<br />
They are deployed by default in our heat flow<br />
calorimeters. Due to their extremely short response<br />
time and the high resolution, they are also extremely<br />
well suited for chemical or pharmaceutical bottling<br />
and dosing plants. They operate according to the<br />
principle of the turbine-type meter.<br />
They operate according to the principle of the<br />
turbine-type meter.<br />
Type Measurement Range Impulses / l Connection<br />
in l/min<br />
G<br />
TDM06 1 to <strong>10</strong> 2000 ½ inch<br />
TDM09 3 to 30 980 ½ inch<br />
The Advantages:<br />
� compact<br />
� maintenance-free<br />
� resistant against high temperatures<br />
� low pressure decline<br />
� high working pressure range<br />
� fast response time due to low-mass rotor<br />
Application Areas<br />
� Chemical Industry<br />
� Pharmaceutical Industry<br />
� Heat Carrier Flow Measurement<br />
� Bottling and Charging<br />
� Flow Monitoring<br />
� Consumption Counter<br />
� Heat Counter<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Technical Data<br />
Process Analytics and Sensors<br />
Linearity ±2% v.M.<br />
Reproducibility ±0.5%<br />
MediaTemperature -20 to 120, 180 or 350°C<br />
Max. Operating 20 bar<br />
Pressure<br />
Viscosity 0.1 to 6 mm²/s<br />
Materials High-grade steel 1,4305 and 1,4122, ceramic<br />
Seal Viton or graphite<br />
Delivery Scope : Sensor with mounted impulse amplifier<br />
Order Code Description<br />
IS-F-TDMtc-tb-sa Turbine-type flow sensor<br />
ZK-SF-KM01-IA-IA-I-01 LAB-PI connection cable for turbine-type flow sensor, 4..20mA<br />
ZK-SF-KM01-ID-XA-I-01 LAB-PI connection cable for turbine-type flow sensor, NPN-OC<br />
tc = to <strong>10</strong>l/min: 06 alternatively up to 30l/min: 09<br />
tb = Temperature Range 120, 180 or 350 °C<br />
sa = Output Signal 4..20mA: I<br />
or frequency-analogue NPN-OC: F<br />
Order Example:<br />
Flow sensor for 0-<strong>10</strong>l/min, max. temperature 180°C, frequencyanalogue<br />
output, open collector: IS-F-TDM06-180-F<br />
Thermal Mass Flowmeters and Controllers<br />
The thermal flowmeters serve for the measurement<br />
of the mass flow of liquids. They operate on the<br />
basis of the calorimetric principle.<br />
The digital LIQUI-FLOW® Series L30 Mass-<br />
Flowmeter/controller was developed for measuring<br />
ranges between 2 and 20 kg/h (final value). It<br />
represents an ideal supplement to the larger<br />
measurement ranges of the smaller product family<br />
(up to the minute ranges of 30 mg/h). The mass<br />
flowmeter is based on a straight 316L high grade<br />
steel tube. A temperature sensor and a heating<br />
winding are mounted in thin film technology on the<br />
exterior side of the tube. The sensor signal is<br />
generated by the measurement of the current<br />
necessary for a consistent slight increase of the<br />
liquid.<br />
The Advantages:<br />
� Compact Design<br />
� Straight Measuring Tube<br />
� <strong>Main</strong>tenance-Free<br />
� Extensive Operational Range<br />
� Short Response Time<br />
Application Areas:<br />
� Chemistry<br />
� Pharmaceutics<br />
� Filling and Bottling<br />
� Flow Monitoring<br />
� Metering<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 245<br />
Equipment and<br />
Components<br />
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and Sensors<br />
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Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
246<br />
Technical Data<br />
Process Analytics and Sensors<br />
Physical Characteristics<br />
Accuracy, Standard ±1% of Final Value (at calibration under operational conditions)<br />
Span 2...<strong>10</strong>0%<br />
Reproducibility 0,2% of Final Value typical for H2O<br />
Setting Time Sensor 1...2 seconds, Controller 4...<strong>10</strong> seconds<br />
Max. Operational Pressure <strong>10</strong>0 bar<br />
Pressure Loss 35...350 mbar (based on 2...20 kg/h H2O)<br />
Operational Temperature 5...70°C<br />
Temperature Sensitivity ±0,2% of Final Value/°C<br />
Position Dependency Non-sensitive<br />
Heating Period<br />
Mechanical<br />
Characterisics<br />
30 minutes for highest accuracy; 3 minutes for an accuracy of ±2% of Final<br />
Value<br />
Material High Grade Steel 316L, electropolished (parts in contact with media). Other<br />
materials are available upon request.<br />
Process Connections 1/4” or 6 mm clamp ring connection; 1/4” vacuum connection, orbital welded.<br />
Other connections are available upon request.<br />
Gaskets towards the<br />
exterior<br />
Metallic<br />
Baffle Plate (in the Kalrez-6375. Others are available upon request.<br />
Controller Valve)<br />
Protection Class IP65<br />
Electrical<br />
Characteristics<br />
Supply Voltage +15...24 Vdc<br />
Output Measuring Device max. 18,5 Watt; Controller max. 22 Watt<br />
Output/Setpoint Value 0...5 (<strong>10</strong>) Vdc or 0 (4)...20 mA (active Output Signal)<br />
analogue<br />
Output/Setpoint Value Standard RS232, Optional Profibus-DP®, DeviceNet, Modbus-RTU, FLOWdigital<br />
BUS<br />
Electrical Connection Analogue/RS232/Supply 8-pole DIN-Connector male, Bus Systems-5-pole<br />
M12-Socket female<br />
Calibration Reference : Verifed by the NKO (National Calibration Service), is based on<br />
international standards.<br />
Liquid : Standard Calibration Liquid: H2O. For other liquids, please contact us.<br />
Models and Flow Ranges<br />
Mass Flowmeter for Liquids<br />
Model Minimum Flow Maximum Flow<br />
L30 0,0 0,04…2 kg/h 0,4…20 kg/h<br />
Mass Flow Controllers for Liquids<br />
Model Minimum Flow Maximum Flow<br />
L30C2I (Kv-max: 2,37x<strong>10</strong>-3) 0,04…2 kg/h 0,4…20 kg/h<br />
L30C5I (Kv-max: 6,93x<strong>10</strong>-2) 0,04…2 kg/h 0,4…20 kg/h<br />
Based on liquids with thermal characteristics equal to H2O.<br />
Delivery Scope: Sensor with Manual<br />
Order Code Description<br />
IS-FM-L30 0,0 Thermal Mass Flowmeter 0,04…2 kg/h to 0,4…20 kg/h<br />
IS-FM-L30C2I Thermal Mass Flowmeter(Kv-max: 2,37x<strong>10</strong>-3) 0,04…2 kg/h to 0,4…20 kg/h<br />
IS-FM-L30C5 Thermal Mass Flowmeter (Kv-max: 6,93x<strong>10</strong>-2) 0,04…2 kg/h to 0,4…20 kg/h<br />
Further flowmeters and devices in EX design are available upon request, for example, the μ-FLOW Series<br />
for the smallest possible flow amounts with measurement ranges reaching between 1,5...30 mg/h to 0,1...2<br />
g/h equivalent to water.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
Coriolis Mass Flowmeters and Controllers<br />
These mass flow sensors serve for the<br />
measurement and the control of the mass flow of<br />
liquid. They operate according to the Coriolis<br />
principle. They offer, compared to all other<br />
flowmeters, the great advantage that the mass flow<br />
is measured independent of the material<br />
characteristics. With them, multiple-phase materials<br />
can also be measured on an interference-free basis.<br />
The Advantages:<br />
� Real Mass Flow Measurement<br />
� Suited for Gasses and Liquids<br />
� Independent of Material Characteristics<br />
� Compact Design<br />
� <strong>Main</strong>tenance-Free<br />
� Extensive Operational Range<br />
� Low Response Time<br />
Application Areas<br />
� Chemistry<br />
� Pharmaceutics<br />
� Dosing<br />
� Filling and Bottling<br />
� Flow Monitoring<br />
� Metering<br />
Technical Data<br />
Physical Characteristics M12 / M13 / M14<br />
Accuracy, Standard Gases 0.5% p.M. Liquids 0.2% p.M.<br />
Span<br />
Reproducibility 0.05% v.M. ±1/2 [ZS x <strong>10</strong>0/flow]% (Digital Output) (ZS = Zero Stability)<br />
Setting Time(Regler) (
248<br />
Models and Flow Ranges<br />
Mass Flowmeters for Liquids<br />
Model Smallest Measurement<br />
Range<br />
Process Analytics and Sensors<br />
Nominal Highest Measurement<br />
Range<br />
M12 0.1…5g/h 1…<strong>10</strong>0g/h 2…200g/h<br />
M13 1…50g/h <strong>10</strong>…<strong>10</strong>00g/h 20…2000g/h<br />
M14 0.03…1kg/h 0.1…<strong>10</strong>kg/h 0.3…30kg/h<br />
Mass Flow Controllers for Liquids<br />
Model Smallest Measurement<br />
Range<br />
Nominal Highest Measurement<br />
Range<br />
M12V1NI 0.1…5g/h 2…<strong>10</strong>0g/h 4…200g/h<br />
M13V1NI 1…50g/h 20…<strong>10</strong>00g/h 40…2000g/h<br />
M14V1NI 0.03…1kg/h 0.2…<strong>10</strong>kg/h 0.6…30kg/h<br />
Delivery Scope: Sensor with Manual<br />
Order Code Description<br />
IS-FM-M12 Coriolis Mass Flowmeter 1…<strong>10</strong>0g/h<br />
IS-FM-M13 Coriolis Mass Flowmeter <strong>10</strong>…<strong>10</strong>00g/h<br />
IS-FM-M14 Coriolis Mass Flowmeter 0.1…<strong>10</strong>kg/h<br />
IS-FM-M12V1NI Coriolis Mass Flowmeter 1…<strong>10</strong>0g/h<br />
IS-FM-M13V1NI Coriolis Mass Flowmeter <strong>10</strong>…<strong>10</strong>00g/h<br />
IS-FM-M14V1NI Coriolis Mass Flowmeter 0.1…<strong>10</strong>kg/h<br />
Further flowmeters and devices in EX design are available upon request.<br />
Laboratory Gas Counter<br />
Drum-Type Gas Counter<br />
Wet Gas version<br />
Drum gas counters are universally deployable for<br />
volume measurement of flowing gases, in particular<br />
in case of minute and medium flow quantities, e.g. in<br />
the laboratory sector where utmost precision is<br />
demanded.<br />
Correction factors that consider gas type,<br />
temperature, humidity, etc. are therefore not<br />
required.<br />
Drum gas counters do not require maintenance and<br />
no power supply (as long as they are not operated<br />
with the option “pulse generator”).<br />
Advantages of the drum gas counter:<br />
� Housing and measuring drum are made of<br />
high quality plastics<br />
� Welded measuring drum – not soldered<br />
� Housing and measuring drum are resistant in<br />
regard to sealing liquid – in case an acid<br />
should generate out of the same<br />
� Epoxy coating for the measuring drum not<br />
required<br />
� Magnetic coupling instead of an O-Ring for<br />
drum shaft<br />
� PVC gas counter made of transparent PVC<br />
� 4-chamber measuring drum<br />
� Totalising roll counting mechanism (8-digit)<br />
� Large one-needle instrument dial<br />
� Magnetic coupling (between measuring drum<br />
and counting mechanism)<br />
� Filling level indicator (for adjustment of the<br />
sealing liquid level)<br />
� Recordings for manometer/thermometer<br />
� Viton seal<br />
� Circular bubble<br />
� Device foots can be levelled<br />
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Performance Data<br />
Process Analytics and Sensors<br />
� Measurement Accuracy:<br />
± 0.2% at nominal flow (exact value is stated in<br />
calibration certificate),<br />
approx. ± 0.5% above the measurement range<br />
� Maximum input pressure:<br />
50 mbar at housings made of thermoplastics,<br />
500 mbar (0.05 MPa) at housings of high-grade<br />
steel<br />
Available Types<br />
Available Versions (materials):<br />
Type Flow Display (Standard Version)<br />
Minimum Maximum Standard Lowest Resolution Highest Resolution<br />
[l/h] [l/h] [l/h] [l]<br />
[l]<br />
TG 01 0.1 30 <strong>10</strong> 0.0005 (1) 999,9999 (1)<br />
TG 05 1 60 50 0.002 9,999,999.9<br />
TG 1 2 120 <strong>10</strong>0 0.01 99,999,999<br />
TG 3 5 360 300 0.02 99,999,999<br />
TG 5 <strong>10</strong> 600 500 0.02 99,999,999<br />
TG <strong>10</strong> 20 1200 <strong>10</strong>00 0.1 99,999,999<br />
TG 20 <strong>10</strong>0 4000 3200 0.2 999,999,990<br />
TG 25 <strong>10</strong>0 7000 5000 0.1 999,999,990<br />
TG 50 200 18000 <strong>10</strong>000 0.5 999,999,990<br />
(1) Display at the EDU 32<br />
Accessories (optional):<br />
� Thermometer (Gas), Measurement Range 0-<br />
60°C<br />
� Thermometer (Sealing Liquid),<br />
Measurement Range 0-60°C<br />
� Manometer, Measurement Range <strong>10</strong>mbar<br />
Differential Pressure<br />
� Digital Display Unit, with Interface RS232 and<br />
Analogue Output, (Impulse Generator required in<br />
Gas Counter)<br />
Housing Measuring<br />
Drum<br />
Version<br />
PVC-transparent PVC-grey 5<br />
PP-grey PP-grey 6<br />
PVDF PVDF 7<br />
PE-el PE-el 8<br />
1.4571 PVC-grey 1<br />
1.4571 PE-el 2<br />
1.4571 PP-grey 3<br />
1.4571 PVDF 4<br />
In case of any questions regarding the chemical<br />
resistance, please contact us. Both plastic and highgrade<br />
steel housings are welded.<br />
Options (installed in Gas Counter):<br />
Impulse Generator (for connection to Digital Display<br />
Unit/Computer)<br />
� Standard Version<br />
� Ex Version<br />
Slanted Tube Filling Level Indicator for Sealing<br />
Liquid „HPLI“<br />
Roll Counting Mechanism, resettable, 6 -digit<br />
(instead of totalising roll counting mechanism)<br />
Order Code Description<br />
IS-FV-GAS-tc-au Laboratory gas counter, wet gas version<br />
IS-FV-GAS-IG Impulse generator for connection to digital display unit/LAB- or PMC-PI<br />
IS-FV-GAS-IGEX Impulse generator for connection to digital display unit/LAB- or PMC-PI, Ex Version<br />
IS-FV-GAS-THG Thermometer (Gas), measurement range 0-60°C<br />
ZK-SFV-RI01-ID-XX-I-01 Connection cable for connection to DEP8A<br />
IS-FV-GAS-THS Thermometer (sealing liquid), measurement range 0-60°C<br />
IS-FV-GAS-MAN Manometer, measurement range <strong>10</strong> mbar differential pressure<br />
IS-FV-GAS-DISP Digital display unit, with interface RS232 and analogue output, (impulse generator required in<br />
gas counter)<br />
tc = Type code according to table types<br />
au = Version according to table versions (materials)<br />
Order Example: Type TG5 in PVDF with impulse generator for LabManager:<br />
Order Codes: IS-FV-GAS-TG5-7 and IS-FV-GAS-IG<br />
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Temperature Sensors<br />
Pt<strong>10</strong>0 Sensors<br />
Process Analytics and Sensors<br />
Pt<strong>10</strong>0 sensors have asserted themselves as<br />
standard in laboratories and pilot plants due to their<br />
high accuracy. They are available in different<br />
versions and dimensions.<br />
Accuracy Categories<br />
DIN Class A = ½ DIN B<br />
DIN B = ±(0.3+ 0.005|ϑ|)°C<br />
1/3 DIN B = ±(0.1+ 0.0016|ϑ|)°C<br />
1/5 DIN B = ±(0.06+ 0.001|ϑ|)°C<br />
1/<strong>10</strong> DINB= ±(0.03+ 0.0005|ϑ|)°C<br />
Diameter d = 2/3/6mm, Length l = 50/<strong>10</strong>0/300/600mm<br />
Technical Data<br />
Material: High-grade steel 1,4541 (V4A) (food and<br />
chemical resistant with the exception of chlorine)<br />
Temperature Range: -200 to 500°C<br />
Four-wire Technology<br />
Cable: 3 m, individual wires Teflon-isolated<br />
Outer cladding silicone, with bend protection.<br />
Lemo Plug Size 1<br />
The Pt<strong>10</strong>0 sensors are delivered ready to connect<br />
with a cable and a Lemo plug for direct connection<br />
to a Pt<strong>10</strong>0-Panel PTP8.<br />
Order Code Description<br />
IS-T-PT<strong>10</strong>0-1/1-VA-d-l Pt<strong>10</strong>0 Sensor DIN B, high-grade steel cladding 1,4541, with cable for LAB-PI Panel PTP8<br />
IS-T-PT<strong>10</strong>0-1/3-VA-d-l Pt<strong>10</strong>0 Sensor 1/3 DIN B, high-grade steel cladding 1,4541, with cable for LAB-PI Panel PTP8<br />
IS-T-PT<strong>10</strong>0 1/5-VA-d-l Pt<strong>10</strong>0 Sensor 1/5 DIN B, high-grade steel cladding 1,4541, with cable for LAB-PI Panel PTP8<br />
IS-T-PT<strong>10</strong>0-1/<strong>10</strong>-VA-d-l Pt<strong>10</strong>0 Sensor 1/<strong>10</strong> DIN B, high-grade steel cladding 1,4541, with cable for LAB-PI Panel PTP8<br />
Diameter d = 1/1.6mm, Length l = <strong>10</strong>0/250/<strong>10</strong>00mm<br />
Order Code Description<br />
IS-T-PT<strong>10</strong>0-1/1-VA -d-l Pt<strong>10</strong>0 Sensor DIN B, high-grade steel jacket 1,4541, with cable for LAB-PI Panel PTP8<br />
Special Designs<br />
� Precision Temperature Sensor (see under<br />
Precision Measurement Card)<br />
� Temperature Range -200 to 500°C, 600°C<br />
� Other Cladding Materials (Glass, Titanium ...)<br />
Calibration Certificates<br />
Manufacturer's Certificate or DKD certificate<br />
(German Calibration Service) upon request.<br />
Thermo- Elements<br />
Thermo-elements are available in various materials<br />
and dimensions. Especially small diameters are also<br />
available. This, in connection with their extremely<br />
broad temperature range, makes them<br />
indispensable.<br />
Connection to the LabManager:<br />
The cladded thermo-elements are delivered ready to<br />
connect with a cable and a Lemo plug for direct<br />
connection to a thermo-element Panel (LP-THP8).<br />
Accessories<br />
Screwing fixtures with slide function, process<br />
connection with G ¼ inch, glass thread GL or<br />
standard grinding.<br />
Technical Data:<br />
Material Cladding Tube: High-Grade Steel<br />
(food and chemical resistant with the exception of<br />
chlorine compounds)<br />
Temperature Range: -200 to 800°C<br />
Lemo-Plug Size 1 for LAB-PI<br />
Available upon request:<br />
� Open cable ends for MSRmanager<br />
� Other Cladding Materials (Glass, Titanium ...)<br />
� Area Sensor<br />
� Special Designs<br />
Order Code Description<br />
IS-T-NICRNI-d-l Thermo-element NiCr-Ni with connection cable for LAB-PI Panel THP8<br />
Diameter d = 0.5/1/2mm, Length l = <strong>10</strong>0/250/500/<strong>10</strong>00mm<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Pressure Transmitters<br />
Standard Pressure Transmitters<br />
Process Analytics and Sensors<br />
Robust high-quality pressure transmitter for<br />
industrial deployment. These pressure transmitters<br />
can be directly connected to <strong>HiTec</strong> PIs. We offer<br />
three different types of pressure transmitters:<br />
� Relative Pressure:<br />
Atmospheric pressure as reference pressure,<br />
e.g. for filtration/vacuum filtration<br />
� Absolute Pressure:<br />
Vacuum reference, in particular for reactors,<br />
vacuum, distillation, steam pressure<br />
� Differential Pressure:<br />
2 Connections,<br />
filling level, pump monitoring...<br />
Technical Data:<br />
Properties:<br />
� High Accuracy<br />
� Compact Design<br />
� In Situ Digital<br />
Display available<br />
� High Overload<br />
Capability<br />
(5- to <strong>10</strong>-fold, dependant of Measurement<br />
Range)<br />
Connection to the LabManager<br />
The sensor is delivered ready to connect with a<br />
cable and a Tuchel plug for direct connection to an<br />
analogue input Panel LP-AEP8A. The power supply<br />
is conducted via Pin 5 = +24V and Pin 6 = GND.<br />
Measurement Principle Piezo-resistive<br />
Characteristic Line<br />
Deviation<br />
0.25% of Range<br />
Reproducibility 0.05 % of Range<br />
Hysteresis Fault 0.1 % of Range<br />
Stability/Year 0.2 % of Range<br />
Response Time (<strong>10</strong> - 90%) 1 ms<br />
Temperature Dependency Usually< 0.2% of Range/<strong>10</strong>K<br />
Measurement Media<br />
Temperature<br />
-30 to +<strong>10</strong>0°C<br />
Ambient Temperature -20 to +80°C<br />
Parts in Contact with<br />
Measurement Media<br />
High-Grade Steel 1,4571, 1,4542<br />
Pressure Connection G ¼“B (others upon request)<br />
Output Signal 4 - 20mA<br />
Supply Voltage <strong>10</strong> - 30 V DC unregulated, two-wire switching with plug-on display 13 - 30 V DC<br />
Electrical Connection Angle plug 4-pole, DIN 43 650<br />
Protection Category IP 65<br />
EEX Upon request<br />
Dimensions L approx. <strong>10</strong>0 mm, D approx. 48 mm with plug<br />
Order Code Description<br />
IS-P-R-6-ma-ea Pressure Transmitter 0- 6 bar relative with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />
IS-P-A-025-ma-ea Pressure Transmitter 0- 0.25 bar absolute with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />
IS-P-A-1,6-ma-ea Pressure Transmitter 0- 1.6 bar absolute with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />
IS-P-A-2,5-ma-ea Pressure Transmitter 0- 2.5 bar absolute with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />
IS-P-A-6-ma-ea Pressure Transmitter 0- 6 bar absolute with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />
IS-P-Z-AA Electronic plug-on display<br />
Nn<br />
ma=Media Connection:<br />
GMG1/4 Outer Thread G ¼“<br />
GMG1/2 Outer Thread G ½“<br />
ea=Electrical Connection:<br />
T Tuchel-plug for LAB-PI<br />
O Open ends for PMC-PI<br />
Order Example:<br />
Pressure Transmitter 0 – 0.25 bar absolute, G1/2“,<br />
with connection cable 1.5 m for LabManager<br />
Panel LP-AEP8A<br />
Order Code: IS-P-A-025-GMG1/2-O<br />
Available upon request:<br />
� Materials: Hastelloy C4<br />
� Other Measurement Ranges<br />
� Front-flush Diaphragm<br />
� Differential Pressure<br />
� EEX Versions<br />
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Process Analytics and Sensors<br />
Low Dead Space - pressure transducer<br />
This robust pressure transducer is suited for<br />
applications where particular low dead spaces are<br />
required, e.g. within micro-reaction technology.<br />
The measuring media does not come in contact with<br />
any metals.<br />
Features :<br />
� Metal- free Measuring Circuit<br />
� High Precision<br />
� Compact Design<br />
� Digital display available in-situ<br />
� High Overload Capability<br />
The pressure transducer can be directly connected<br />
to the <strong>HiTec</strong> PNCs.<br />
The pressure transducer is available for the<br />
measurement of relative and absolute pressure.<br />
Technical Data:<br />
Dead Volume 250µl<br />
Measuring Principle Piezo-resistive<br />
Characteristics Deviation 0,25% of Range<br />
Reproducibility 0,05 % of Range<br />
Hysteresis Fault 0,1 % of Range<br />
Stability/Year 0,2 % of Range<br />
Response Time (<strong>10</strong> - 90%) 1 ms<br />
Temperature Dependency Usually< 0,2% of Range /<strong>10</strong>K<br />
Measuring Media<br />
Temperature<br />
-0 to +<strong>10</strong>0°C<br />
Ambient Temperature -20 to +80°C<br />
Parts in Contact with PFA, PEEK, Kalrez Gaskets<br />
Measuring Media<br />
Connection to the LabManager<br />
The sensor is delivered in ready-to-connect<br />
condition with a cable and a Tuchel plug for the<br />
direct connection to an Analogue-Entry-Panel LP-<br />
AEP8A. The power supply is conducted via Pin 5 =<br />
+24V and Pin 6 = GND.<br />
For connection to a panel without sensor power<br />
supply (e.g. LP-AEP8), you additionally require a<br />
24V power supply unit.<br />
Output Signal 4 - 20mA<br />
Supply Voltage <strong>10</strong> - 30 V DC not controlled, two-wire circuit, with plug-on display 13 - 30 V DC<br />
Electrical Connection Angle Plug 4-pole, DIN 43 650<br />
Protection Category IP 65<br />
EEX Upon Request<br />
Dimensions L approx. <strong>10</strong>0 mm, D approx. 48 mm with plug<br />
Order Code Description<br />
IS-PTOT-R-16-ea Low Dead Space pressure transducer 0- 16 bar relative with connection cable 1,5m for LAB-<br />
PNC Panel LP-AEP8A<br />
IS-PTOT-A-16-ea Low Dead Space pressure transducer 0- 16 bar absolute with connection cable 1,5m for LAB-<br />
PNC Panel LP-AEP8A<br />
IS-P-Z-AA Electronic Plug-On Display<br />
Nn<br />
ea=Electrical Connection:<br />
T Tuchel-Plug for LAB-PNC<br />
O Open Ends for MSR-PNC<br />
Example Order:<br />
pressure transducer 0 - 16 bar abs., with connection<br />
cable 1,5 m for LabManager Panel LP-AEP8A,<br />
Order Code: IS-PTOT-A-16-T<br />
Other Measurement Ranges are available upon request.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
Hose Pressure Transmitter<br />
These novel pressure transmitters measure the<br />
pressure or the differential pressure at normal hoses<br />
from the exterior. For this reason, they are<br />
particularly suited for sterile applications. No<br />
mounting parts are required in the hose. The plant is<br />
completely sterilised and the hose is merely inserted<br />
into the sensor after sterilisation. The novel<br />
measurement principle is subject to legal protection.<br />
The Advantages:<br />
� Suited for sterile applications<br />
� Media compatibility determined by hose<br />
� Subsequent mounting possible<br />
� Differential and absolute pressure<br />
measurement<br />
� The sensor can be operated with all load cell<br />
amplifier types<br />
Technical Data:<br />
The sensor can, in particular, be used for pressure<br />
measurement and filter monitoring in bio-technical,<br />
sterile plants.<br />
Due to the measurement principle, the specification<br />
is strongly dependant of the hose (diameter, wall<br />
thickness, material). For this reason, the values<br />
stated below are only to be considered as guideline<br />
values. In particular in case of thin hoses and great<br />
wall thicknesses, greater deviations may occur. In<br />
practice, in case great care is directed at the<br />
calibration, significantly better specifications are<br />
usually reached at hose diameters >=<strong>10</strong> mm.<br />
Measurement Principle Measuring of the hose wall force from the exterior<br />
Resolution < 1 mbar<br />
Characteristic Line Deviation * < 50 mbar<br />
Zero Point Stability < 30 mbar<br />
Reproducibility* < 20 mbar<br />
Hysteresis Faults* < 30 mbar<br />
Stability/Year* < 50 mbar/a<br />
Response Time (<strong>10</strong> - 90%)* approx. 1 sec<br />
Temperature Dependency Calibration at operating temperature ± 5°C expedient<br />
Measurement Media Temperature * <strong>10</strong> to +50°C<br />
Ambient Temperature <strong>10</strong> to +40 °C<br />
Parts in Contact with Media Hose material<br />
Hose Diameter 3 to 22 mm<br />
Output Signal 6 conductor-resistance bridge<br />
Electrical Connection 6-pole LEMO-plug Size 1<br />
Protection Category IP 20<br />
Ex-Protection Equipment Upon request<br />
Dimensions 140x120x45mm<br />
* with silicone hose 22mm<br />
Order Code Description<br />
IS-P-TUBE-sd Pressure Transmitter 0 – 2 bar, for hose diameter of 3mm to 22mm, absolute and differential<br />
pressure with connection cable 1.5m for 6-conductor measurement amplifier<br />
HK-GRADOMV1 Measurement amplifier 1 channel, external measurement amplifier for connection to analogue input<br />
HK-AD24DMS4 Measurement system 4 channels, card for <strong>HiTec</strong> <strong>Zang</strong> PNC panel<br />
*** requires LP-DMS4DA4PTR<br />
sd = Exterior Hose Diameter in mm<br />
Special designs available upon request.<br />
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Humidity Sensors<br />
Process Analytics and Sensors<br />
The humidity sensor IS-M-FEU1 has a linear<br />
operational range of 0-<strong>10</strong>0%. Trough laser trimming<br />
down to 2 %, the sensor can be exchanged in most<br />
cases without the need of additional calibration. The<br />
sensor is delivered without housing. When installing<br />
it, care must be taken that the humidity diffusion to<br />
the sensor is not disturbed.<br />
Technical Data:<br />
Measurement Uncertainty ± 2 %, 0-<strong>10</strong>0%, not condensing<br />
Linearity Fault ± 0.5 % typical<br />
Hysteresis Fault ± 0.8 % of range<br />
Reproducibility ± 0.5 %<br />
Stability ± 1 % in 5 years<br />
Response Time 1/e 15 s in slowly agitated air<br />
Operational Range 0 - <strong>10</strong>0%, not condensing<br />
Working temperature Range -40 to 85°C<br />
Output Signal 0.8V at 0%, 4V at <strong>10</strong>0%<br />
Temperature Dependency 0.22%/°C of reading value<br />
Dimensions 6mm x 9mm x 19mm<br />
Connection to the LabManager:<br />
Scaling of the Analogue Input:<br />
The sensor is delivered ready to connect with a<br />
cable and a Tuchel plug for direct connection to an<br />
analogue input Panel LP-AEP8A. The power supply<br />
is conducted via Pin 5 = +24V and Pin 6 = GND.<br />
For the connection to a panel without sensor supply<br />
LP-AEP8, you additionally require an adapter cable<br />
with wall power supply ZK-LAB-HI99-IA-XA-Y-0.1.<br />
Interface Value Process Value<br />
0.8 V 0 %<br />
4 V <strong>10</strong>0%<br />
Under laboratory conditions, the temperature fault is<br />
situated within the scope of the measurement<br />
uncertainty and does not need to be corrected.<br />
Increased temperature range available upon<br />
request.<br />
Order Code Description<br />
IS-M-FEU1 Humidity sensor with connection cable for LabManager Panel LP-AEP8A<br />
ZK-LAB-HI99-IA-XA-Y-0.1 Adapter cable for AEP8 (not actived!) with wall power supply for the sensor 24V DC<br />
Distance and Rotational Speed Measurement<br />
Inductive Proximity Switch<br />
With the help of a proximity switch, the position of an<br />
object and the rotational speed at a rotating object<br />
can be measured and monitored.<br />
The Sensor generates an impulse at every approach<br />
to the optical, respectively magnetic marking. The PI<br />
collects the pulse frequency and calculates the<br />
rotational speed hereof.<br />
Inductive Proximity Switch as a Rotational Speed Sensor<br />
Order Code Description<br />
IS-G-REFL1 Infrared reflection sensor, max. switching frequency <strong>10</strong>0Hz, exterior diameter 12mm<br />
IS-G-IND1 Inductive proximity switch<br />
Suited cards and connection modules: HK-DEA16F with LP-DEP8A or MB-DEB8 with cable adapter.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
Weight Measuring and Load Cells<br />
KMZ<strong>10</strong>00 to KMZ30000<br />
KMZ50k to KMZ<strong>10</strong>00k<br />
The load cells can be used for:<br />
� Vessel Weighing<br />
� Reactor Content Measurement (see Reactor<br />
Weighing)<br />
� Gravimetric Dosing (see also GraviDos)<br />
A load measuring system consists of a load cell IS-<br />
W-KMZxxxx, and, optionally, an external<br />
measurement amplifier HK-GRADOMV1 or a PIinternal<br />
measurement system HK-AD24DMS4 for<br />
four channels.<br />
The digital measuring amplifier HK-GRADOMV1D<br />
enables the connection to a serial interface.<br />
Technical Data (KMZ<strong>10</strong>00 to 3000)<br />
Measurement<br />
Approx. 0.01%<br />
Resolution<br />
Measurement<br />
Approx. 0.1% p.U.<br />
Uncertainty<br />
Dimensions<br />
approx. 195x40x52 mm<br />
(without rodding)<br />
Ex-Protection optional<br />
Connection 6 pole LEMO-plug, Type<br />
FFA.11S.306.CLACxx<br />
Technical Data (KMZ50k to <strong>10</strong>00k)<br />
Accuracy Classes D1, C3, C4, C6<br />
Calibratable Up to 6000 Parts<br />
Approvals OIML, NTEP, Ex, GOS<br />
Order Code Description<br />
IS-W-KMZ<strong>10</strong>00 Load cell, 0 to <strong>10</strong>00g, including cable<br />
IS-W-KMZ3000 Load cell, 0 to 3000g, including cable<br />
IS-W-KMZ7500 Load cell, 0 to 7500g, including cable<br />
IS-W-KMZ15000 Load cell, 0 to 15 kg, including cable<br />
IS-W-KMZ30000 Load cell, 0 to 30 kg, including cable<br />
IS-W-KMZ<strong>10</strong>00D Load cell, 0 to <strong>10</strong>00 g, integrated measurement amplifier, RS232 interface, including cable<br />
IS-W-KMZ3000D Load cell, 0 to 3000 g, integrated measurement amplifier, RS232 interface, including cable<br />
IS-W-KMZ7500D Load cell, 0 to 7,5 kg, integrated measurement amplifier, RS232 interface, including cable<br />
IS-W-KMZ15000D Load cell, 0 to 15 kg, integrated measurement amplifier, RS232 interface, including cable<br />
IS-W-KMZ30000D Load cell, 0 to 50 kg, integrated measurement amplifier, RS232 interface, including cable<br />
IS-W-KMZ50k Load cell, 0 to 50 kg, including cable<br />
IS-W-KMZ<strong>10</strong>0k Load cell, 0 to <strong>10</strong>0 kg, including cable<br />
IS-W-KMZ200k Load cell, 0 to 200 kg, including cable<br />
IS-W-KMZ500k Load cell, 0 to 500 kg, including cable<br />
IS-W-KMZ<strong>10</strong>00k Load cell, 0 to <strong>10</strong>00 kg, including cable<br />
HK-GRADOMV1 Measurement amplifier 1 channel, external measurement amplifier for connection to<br />
analogue input<br />
HK-GRADOMV1D Digital measurement amplifier 1 channel, external measurement amplifier, RS232 interface<br />
HK-GRADOMV1D-SN Power supply for digital measurement amplifier HK-GRADOMV1D<br />
HK-AD24DMS4 Measuring system 4 channels, Card for <strong>HiTec</strong> <strong>Zang</strong> PNC panel<br />
IL-GRADOADV Adapter-square, manifold measuring cell to square aluminum construction system<br />
IL-GRADOADR12 Adapter-round, manifold measuring cell to 12 mm tube construction systems<br />
IL-GRADOADR14 Adapter-round, manifold measuring cell to 14 mm tube construction systems<br />
Informationen zu den Messverstärkern und weitere Informationen finden Sie in den Kapiteln Laborautomatisierung<br />
Hardware, Externe Messverstärker und Laborgeräte und Komponenten, Waagen.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 255<br />
Equipment and<br />
Components<br />
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Dosing Systems,<br />
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Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
256<br />
Monitors<br />
Process Analytics and Sensors<br />
Monitors serve for the monitoring of limit values.<br />
They usually have a (binary) switching output or a<br />
passive switching contact.<br />
Temperature Monitor and Safety Temperature Limiter<br />
If there is possibility of damage and harm to persons<br />
and expensive equipment in case of the breakdown<br />
of the automation technology or deployed devices<br />
and components, a redundant, certified temperature<br />
monitoring, which deactivates the plant, if required,<br />
is absolutely compulsory.<br />
The external certified temperature monitor,<br />
respectively safety temperature limiter, monitors a<br />
temperature which is regulable via a potentiometer.<br />
In the case the set limit value is exceeded, the<br />
switching circuit can for example be interrupted via a<br />
potential-free switching contact and an alarm could<br />
be triggered.<br />
Temperature Monitor<br />
If the set temperature limit value is not reached, or<br />
should a fault such as a sensor breakage, short<br />
circuit or power failure, occur within the permissible<br />
temperature range, the device will shut down without<br />
delay. As soon as no malfunction is pending, it is<br />
necessary to unlock, if the device is set on<br />
temperature limiter function (TL). This unlocking can<br />
be realised by a push-button on the device or via an<br />
external push-button.<br />
Technical Data<br />
For safety reasons, it is in most cases advisable to<br />
use a normally closed contact (NCC).<br />
The temperature monitors may only be deployed<br />
together with an additional control system such as<br />
the LabManager System.<br />
The temperature monitor, respectively safety<br />
temperature limiter are intended for mounting on<br />
standard rails and must be installed in a control box,<br />
respectively control cabinet.<br />
The temperature monitor, respectively safety<br />
temperature limiter is integrated into the existing<br />
Emergency Stop circuit or deployed in connection<br />
with a suited contactor.<br />
The safety temperature limiter accords to the Safety<br />
Category SK 3 of DIN/EN 954-1.<br />
Adjustable Sensor Input Resistance Thermometer (PT<strong>10</strong>0, 3-wire)<br />
Thermal Element (Types J, K, T, E, R, S, B)<br />
Measuring Circuit Sensor Breakage Identification<br />
Monitoring<br />
Short Circuit Identification (only at PT<strong>10</strong>0)<br />
Output Relay, Change-over Contact, max. 3A, 250 VAC<br />
Display LED supply voltage, fault message sensor breakage, lock ON<br />
Resetting 1 push-button on front panel or external push-button<br />
Versions Smallest Setting Step 1C°<br />
Input Measuring Range<br />
PT <strong>10</strong>0 DIN EN 60751 0... 400°C<br />
Fe-CuNi (J) DIN EN 60584 0... 400°C<br />
NiCr-Ni (K) DIN EN 60584 0... 400°C<br />
Cu-CuNi (T) DIN EN 60584 0... 400°C<br />
NiCr-CuNi (E) DIN EN 60584 0... 400°C<br />
Dimensions Depth: <strong>10</strong>0 mm<br />
Width: 22 mm<br />
Height: <strong>10</strong>2 mm<br />
Mounting Snap-on mounting on standard 35 mm rail<br />
Power Supply 115/230VAC or 24VDC<br />
Ambient Conditions <strong>10</strong>..55°C, max. 85% humidity, no bedewing<br />
Order Code Description<br />
HP-SITEMPWAE1 External Temperature Monitor for PT<strong>10</strong>0 or Thermal Elements<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Safety Temperature Limiter<br />
Process Analytics and Sensors<br />
If the permissible temperature limit is exceeded, or<br />
at the occurrence of a malfunction, the STL will,<br />
without delay, switch the plant to an operationally<br />
safe condition. The device can be deployed in<br />
connection with the resistance pick-ups of the type<br />
Pt<strong>10</strong>0.<br />
The limit temperature T can be adjusted via a<br />
frontally located scaled potentiometer. Unintended,<br />
respectively unauthorised setting of the limit value is<br />
prevented by a lead-sealable transparent cover.<br />
Technical Data<br />
Sensor Connection Resistance Thermometer PT <strong>10</strong>0, 3-wire according to EN 60751/IEC 781<br />
Measuring Circuit Monitoring Sensor Breakage Identification, Short Circuit Identification<br />
Output Relay, Change-over Contact, max. 3A, 250 VAC<br />
Display LED supply voltage, fault message sensor breakage, lock ON<br />
Resetting 1 push-button on front panel or external push-button<br />
Temperature Ranges Type A: 0...200°C, Type B: <strong>10</strong>0...300°C, Type C: 200...500°COther<br />
Measuring Ranges -200...+700 °C available upon request<br />
Dimensions Depth: 121 mm, Width: 42 mm, Height: 82 mm<br />
Power Supply 115/230VAC or 24VDC<br />
Mounting Snap-on mounting on standard 35 mm rail<br />
Ambient Conditions <strong>10</strong>..55°C, max. 85% humidity, no bedewing<br />
Order Code Description<br />
HP-SITEMPBEG1 External Safety Temperature Limiter for Pt<strong>10</strong>0<br />
Flow Monitors<br />
Low-cost flow monitors with fixed switching point.<br />
Robust mechanical flow monitor for monitoring of<br />
cooling and heating circuits.<br />
The connection to the LabManager/box is conducted<br />
via digital input. The monitor is suited for looping into<br />
a monitor chain.<br />
Technical Data:<br />
Switching Point 60 l/h, 120 l/h permanent adjustment<br />
Operational Pressure 7 bar at 20°C, 3.5 bar at 80°C<br />
Measured Media Temperature Max. +<strong>10</strong>0°C<br />
Ambient Temperature -25°C to +70°C<br />
Parts in Contact with Housing PP, seal FKM, spring made of high-grade steel<br />
measurement Media<br />
Connection R ¾“ Inner thread, corner mount version<br />
Stability Water, silicone oil, in case of chemicals, verification is necessary<br />
problematic: some solvents, materials containing chlorine, oxidants<br />
Switching Contact Normally open contact<br />
Switching Load Max. 5A AC/ 0.3A DC/ 250 V<br />
EEX in intrinsically safe electric circuits Zone 1<br />
Dimensions Length approx. <strong>10</strong>0 mm, width approx. 64 mm<br />
Order Code Description<br />
IB-FVGE-60-GMG3/4-ea Flow monitor 60 l/h, R ¾“, with connection cable 1.5 m for LAB- or PMC-PI<br />
IB-FGVE-120-GMG3/4-ea Flow monitor 120 l/h, R ¾“, with connection cable 1.5 m for LAB- or PMC-PI<br />
ea=Connection<br />
T Tuchel plug for LAB-PI<br />
O Open ends for PMC-PI<br />
Order Example:<br />
Flow monitor 120 l/h, R ¾“, with connection cable<br />
1.5 with open ends for LabManager<br />
Order Code: IB-FVGE-120-GMG3/4-O<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 257<br />
Equipment and<br />
Components<br />
Process Analytics<br />
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Dosing Systems,<br />
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Stirring and<br />
Dispersing<br />
Services
258<br />
Pressure Monitor<br />
Process Analytics and Sensors<br />
Robust mechanical pressure monitor for industrial<br />
application.<br />
� For Pressure Monitoring independent of the<br />
Pressure Measurement<br />
� High Overload Capacity<br />
The connection to a LabManager/box is conducted<br />
via a digital input. The device is suited for integration<br />
into a monitor chain.<br />
Technical Data:<br />
Setting Range 0,5 - 6 bar relative<br />
Hysteresis Fixed 0,15 bar<br />
Maximum permissible<br />
Pressure<br />
16 bar<br />
Measurement Media<br />
Temperature<br />
Max +85°C<br />
Ambient Temperature -25°C to +70°C<br />
Parts in Contact with<br />
Measurement Media<br />
High Grade Steel 1.4571 + 1.4<strong>10</strong>4<br />
Pressure Connection Outside Thread G 1/2“<br />
Resistance Many chemicals except chloric ones, HCI, oxidants<br />
Switching Contacts 1-pole changeover switch<br />
Switching Capacity Max. 5A AC, 0,3A DC, 250V AC/DC<br />
Electrical Connection Angular Connector 4-pole, DIN 43 650<br />
Protection Class IP 54<br />
EEX In intrinsically safe electrical circuits Zone 1<br />
Compression-proof enclosed version is available.<br />
Dimensions L approx. <strong>10</strong>5 mm, W approx. 112 mm with Jack<br />
Order Code Description<br />
IB-PRKO-6-ma-ea Pressure Monitor 0 - 6 bar relative, with connection cable 1,5m for LAB- or MSR-PNC<br />
ma=Media Connection<br />
AG1/2 Screw Socket G ½“<br />
ea=electrical Connection<br />
T Tuchel-Connector for LAB-PNC<br />
O Open Ends for MSR-PNC<br />
Example Order:<br />
Pressure Monitor 0 - 6 bar rel., G1/2“, with<br />
connection Cable 1,5 m with open ends for<br />
LabManager<br />
Order Code: IB-PRKO-6-AGG1/2-O<br />
Available upon request:<br />
� Other Switching Ranges<br />
� Differential Pressure<br />
� EEX Version<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Process Analytics and Sensors<br />
Flow Monitor with visual Flow Control<br />
Robust mechanical flow indicator (rotameter) with<br />
adjustable switching point for monitoring of cooling<br />
and heating circuits.<br />
The connection to the LabManager/box is conducted<br />
via an active digital input with 24V DC power supply.<br />
The monitor is suited for looping into a monitor<br />
chain.<br />
Technical Data:<br />
Adjustment Range 24 l/h to 1200 l/h<br />
Operational Pressure max. 7 bar<br />
Repeat Accuracy 2%<br />
Switching Point<br />
Accuracy<br />
± 5%<br />
Measured Media<br />
Temperature<br />
Max. +80°C<br />
Ambient Temperature max. +65°C<br />
Parts in Contact with<br />
Measured Media<br />
Housing PP, seal BUNA N<br />
Connection G 1/4“ Inner thread<br />
Stability Water, silicone oil, in case of chemicals, verification is necessary<br />
problematic: some solvents, materials containing chlorine, oxidants<br />
Supply Voltage 24 V DC<br />
Switching Contact Normally open and closed contact<br />
Switching Load max. 1 A, 24 V DC<br />
EEX no<br />
Dimensions 78 x 60 x 61 mm<br />
Order Code Description<br />
IB-FVGE-1200-GMG1/4-ea Flow monitor 1200 l/h, G ¼“, with connection cable 1.5 m for LAB- or PMC-PI<br />
ea=connection<br />
T Tuchel plug for LAB-PI<br />
O Open ends for PMC-PI<br />
Order Example:<br />
Flow monitor 1200 l/h with visual indicator, G 1/4“,<br />
with connection cable 1.5 m with Tuchel plug for<br />
LAB-PI<br />
Order Code: IB-FVGE-1200-GMG1/4-T<br />
Available upon request:<br />
� Greater Flow Rates and Connection Diameters<br />
� Materials: Brass, Cr-Ni-Steel<br />
� As Sensor 0-<strong>10</strong> V or Impulse Output<br />
� Without Electronics as visual Flow Indicator<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 259<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
260<br />
Filling Level Monitor<br />
Optically<br />
Process Analytics and Sensors<br />
Optical filling level monitor for monitoring of the filling<br />
level in reactors, feed tanks, thermostats, collecting<br />
containers.<br />
Features<br />
� No moving parts<br />
� Parts in contact with media made of DURAN-<br />
Glass<br />
� Compact design<br />
� Conductive and non-conductive liquids, which<br />
absorb IR or are penetrable by IR<br />
Technical Data:<br />
Diameter of the Glass<br />
Rod (Sensor)<br />
12mm<br />
Glass Rod Lengths <strong>10</strong>0/250/300mm<br />
Used Light IR<br />
Parts in Contact with<br />
measured Media<br />
DURAN Glass<br />
Installation Glass rod 12 mm in GL-screwing or similar<br />
Switching Contacts PNP, normally open and closed contact<br />
Switching Load Max. 0.2A, 30V DC<br />
Response Time 0.65ms<br />
Supply Voltage <strong>10</strong>- 30V DC<br />
Electrical Connection Cable 2 m<br />
Protection Category IP 65<br />
EEX Upon request<br />
Dimensions Diameter max. approx. 20 mm<br />
Order Code Description<br />
IB-LWE-<strong>10</strong>0-sk-ea Opto-electronic level monitor <strong>10</strong>0 mm,<br />
with connection cable 2 m for LAB- or PMC-PI<br />
IB-LWE-250-sk-ea Opto-electronic level monitor 250 mm,<br />
with connection cable 2 m for LAB- or PMC-PI<br />
IB-LWE-300-sk-ea Opto-electronic level monitor 300 mm,<br />
with connection cable 2 m for LAB- or PMC-PI<br />
sk=Switching Contact:<br />
NC Normally closed contact: opens with<br />
rising level<br />
NO Normally open contact: closes with<br />
rising level<br />
Thermal<br />
The phase detector PhaDec can also be used as<br />
filling level monitor. It functions with all liquids<br />
independent of optical or other properties.<br />
The functional principle of these monitors is based<br />
on total reflection. The end of the glass rod is slightly<br />
grinded at an angle of 45°. As long as the rod is<br />
suspended in air, incoming light at the conical end is<br />
totally reflected. As soon as the rod end submerges<br />
into a more dense material than air, no more<br />
reflection occurs and the reflection sensor does not<br />
receive anymore light.<br />
The glass rod d = 12 mm can be inserted with<br />
standard GL-25 screwings and with according<br />
adaptors in grindings NS 29/32.<br />
The monitor is connected at an active digital input of<br />
the LabManager/box. The monitor is not suited for<br />
looping into a monitor chain.<br />
ea=Connection<br />
T Tuchel plug for LAB-PI<br />
O Open ends for PMC-PI<br />
You will find further information under PhaDec<br />
Phase Limit Detector.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Floaters<br />
Process Analytics and Sensors<br />
Filling level monitor based on a floater mechanism<br />
are utilised to monitor the filling levels in feed tanks,<br />
thermostats and collecting containers.<br />
� No auxiliary energy necessary<br />
� No special requirements to the media<br />
� Applicable as normally open and closed contact<br />
(depending on installation)<br />
The monitor is connected at an active digital input of<br />
the LabManager/box. The monitor is not suited for<br />
looping into a monitor chain.<br />
Technical Data:<br />
Parts in Contact with<br />
measured Media<br />
PVDF<br />
Installation Vertical<br />
Switching Contact NOC<br />
Switching Load 25W, 24V<br />
Supply Voltage Not required<br />
Electrical Connection Tuchel plug of LAB-PI or open ends for PMC-PI<br />
Protection Category IP67<br />
EEX No<br />
Dimensions approx. Ø 27 mm<br />
Order Code Description<br />
IB-LWE-250-NC-ea Filling level monitor based on floater mechanism<br />
ea=Connection<br />
T Tuchel plug for LAB-PI<br />
O Open ends for PMC-PI<br />
Order Example:<br />
Level monitor (at limit exceedance), with connection<br />
cable 2 m with Tuchel-plug for LAB-PI<br />
High Pressure Float Monitor<br />
This filling level monitor based on a floater<br />
mechanism is suited for applications at very high<br />
pressures.<br />
The floater has two switching points.<br />
� No auxiliary energy necessary<br />
� No special requirements to the media<br />
� Applicable both as normally open and closed<br />
contact<br />
The monitor is connected at an active digital input of<br />
the LabManager/box.<br />
Order Code: IB-LWE-250-NC-T<br />
Available upon request:<br />
� Floater, posistor, ultra-sonic, radar...flow sensors<br />
and monitors<br />
� EEX versions<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 261<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
262<br />
Technical Data:<br />
Process Analytics and Sensors<br />
Connection Casing Aluminum<br />
Process Connection Screwing thread G 1/2'' in downward direction<br />
HD Version Slide Tube 12 mm (optionally 14 mm) total length: 200 mm<br />
Switching Points L1 = 60 mm change-over switch, L2 = 155 mm change-over switch<br />
Floater PN80 Titanium<br />
Density <strong>10</strong>00 kg/m¨<br />
Pressure <strong>10</strong>0 bar<br />
Temperature 150 °C<br />
Measurement Value High-grade steel 1,4571, with connection casing and thread<br />
Transmitter<br />
Connection Casing Aluminium positioned with 60mm clearance<br />
Process Connection Screwing thread G 1/2'' in downward direction<br />
Order Code Description<br />
IB-LWDRU-NC-ea Floater magnetic switch made of high-grade steel 1,4571 with connection casing<br />
ea=Connection<br />
T Tuchel-plug for LAB-PI<br />
O Open ends for PMC-PI<br />
Order Example:<br />
Level monitor (at limit exceedance), with connection<br />
cable 2 m with Tuchel-plug for LAB-PI<br />
Order Code: IB-LWDRU-NC-T<br />
Rotational Speed Monitor<br />
The rotational speed monitor is mainly used for the<br />
monitoring of stirring drives.<br />
Scanning is mainly conducted inductively.<br />
For this purpose, a small marking in form of an<br />
electrically conductive area is placed on the rotating<br />
object. The sensor compares the impulse frequency<br />
with the set threshold and switches in case of<br />
shortfall.<br />
Available upon request:<br />
� Floater, posistor, ultra-sonic, radar...flow sensors<br />
� EEX Version<br />
Order Code Description<br />
IB-SIND Inductive rotational speed monitor, threshold adjustable 3 - 300 impulses /min,<br />
Dimensions M30 thread x 81 mm<br />
Suited cards and connection modules: HK-DEA16N, LP-DEP8A, MB-DEB8<br />
This catalogue, due to the limited space, can only contain an excerpt of the most important products.<br />
In case you do not find what you require in the catalogue, please do not hesitate to contact us!<br />
Our experienced project engineers will gladly help you!<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Here you will find:<br />
� GraviDos® Gravimetric Dosing<br />
� AlfaDos Controlled Dropping Funnel<br />
� Pumps and Dosing Pumps<br />
� Vacuum Pumps<br />
� Reactant mixing pump<br />
� Multi-Channel Dosing Systems<br />
� SoliDos Solid Doser<br />
Dosing Systems and Pumps<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 263<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
264<br />
Dosing Systems and Pumps<br />
Controlled Dropping Funnel GraviDos ®<br />
The innovative dosing system GraviDos functions as<br />
a classical dropping funnel according to the force of<br />
gravity principle and consequently does not need<br />
any pumps. Due to this, the problems which always<br />
occur with pumps, like media incompatibility, suction<br />
problems, bubbles, etc. are eliminated. The integrated<br />
weighing system requires so little space that<br />
several dosing-units can be integrated without<br />
problems into a compact laboratory.<br />
In addition, it results in a considerable saving of cost<br />
since no expensive balances and pumps are<br />
needed.<br />
Fields of Application<br />
� Gravimetric dosing<br />
� Tank content measurement<br />
� Reactor content measurement<br />
� Mass flow rate measurement<br />
� pH-control<br />
� Titration<br />
A GraviDos system consists of a glass feed tank<br />
which is hung on the weighing system. The weight<br />
change is registered and the drain controlled by a<br />
magnetic valve. It consists of a real mass flow rate<br />
control, which does not have to be "metered" for<br />
different materials and remains unaffected by<br />
bubbling.<br />
Optionally, a pulsation-free dosing can be achieved<br />
by deploying a proportional valve. Dosing under<br />
vacuum or pressure is possible, if a pressure<br />
compensation pipe is provided.<br />
Properties and Functions<br />
� Low-cost gravimetric dosing<br />
� Compact and robust<br />
� No need for pumps<br />
� Easy to clean<br />
� Large dosing-range<br />
� Refilling without dosing interruption<br />
� Optional pulsation-free dosing<br />
� Resistant to aggressive media<br />
� Ex-suitable design available<br />
The weighing systems are available graded from 1,5<br />
kg to 15 kg, feed tanks from 500 ml to 2000 ml<br />
(above as a special production).<br />
There are GraviDos-connection boards available for<br />
the connection of four or eight weighing systems.<br />
One GraviDos dosing device occupies a channel on<br />
the GraviDos board of the LabManager. An on/off<br />
valve occupies a channel on a digital-output-board.<br />
A proportioning valve occupies a channel on an<br />
analogue-output-board.<br />
For the dosage of liquids with high viscosity, an<br />
auxiliary pressure on the feed tank can be applied, if<br />
required.<br />
A maximum of six GraviDos cards can be integrated<br />
into a PI, which corresponds to 24 channels.<br />
A HiText example application is attached. For an<br />
operation with the recipe control system HiBatch,<br />
there is the base command „Dose Gravi" (SB-<br />
DOSGRAVI). This also allows refilling during<br />
operation without interrupting the dosing process.<br />
GraviDos in a controlled circuit<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
A complete system consists of<br />
� a feed tank<br />
� a proportioning valve IV-MP-UK1 for continuous<br />
dosing or a magnetic valve IV-MB-FK1 for pulsed<br />
dosing<br />
� a suspended balance IL-GRADO-xxxx,<br />
� an external single channel measuring amplifier<br />
HK-GRADOMV1 to be connected to an analogue<br />
input socket<br />
Alternatively:<br />
� a measurement card HK-AD24DMS4<br />
� a LP- DMS4DA4PTR board for four channels<br />
(four controlled dosing circuits)<br />
Alternatively:<br />
� two measurement cards HK-AD24DMS4<br />
� a panel LP-DMS4 for four channels (eight dosage<br />
controlled circuit s)<br />
� a LP-DAP8T panel<br />
Alternatively:<br />
� a digital suspended balance to be connected to a<br />
serial interface<br />
If automatic refilling is desired, further digital outputs<br />
and valves are required.<br />
In case only one to two dosing circuits are required,<br />
it is possible to merely use the measurement<br />
amplifier HK-GRADOMV1 instead of a whole<br />
measurement system. It is connected to normal<br />
analogue input.<br />
The optional Ex-adapter enables the operation of the<br />
GraviDos load cell in explosive environments.<br />
In the standard version all parts in contact with<br />
media are only made of glass, ETFE and Kalrez .<br />
Custom designs made of other materials are<br />
available.<br />
Blast protection category inherent control [EEx ia]<br />
IIC for zone 0.1 or 2.<br />
Application Examples:<br />
Gravimetric Dosing (controlled dropping funnel)<br />
The classical dropping funnel or dosing mechanisms<br />
with pumps and balances are replaced by GraviDos.<br />
GraviDos (unpressurised system)<br />
Dosing Systems and Pumps<br />
Precise Dosing of large Amounts<br />
The medium is automatically refilled from the<br />
reservoir. During the refilling-stage, the flow is<br />
optionally kept consistent or suspended.<br />
GraviDos with feed tank<br />
Distillate Weighing<br />
During fractioned distillation, the fractions are<br />
supposed to be weighed and individually bottled.<br />
The distillate is lead into a GraviDos receiver, and<br />
after the collection of a fraction, is bottled into<br />
vessels via a distribution valve. This assembly<br />
operates under vacuum and pressure.<br />
Distillate weighing and separate bottling of the fractions:<br />
on the left: collection vessels, center: GraviDos distillate scales,<br />
right: rectification column<br />
Further information about GraviDos weighing<br />
cells can be found in the chapter balances.<br />
Technical Data<br />
Resolution Approx. 0.01% v.E.<br />
Measurement<br />
Approx. 0.1% v.E.<br />
uncertainty<br />
Dimensions load cell 200x40x50mm<br />
(without linkages)<br />
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GraviDos ® suspended balance<br />
Dosing Systems and Pumps<br />
The GraviDos dosing system is<br />
basde upon a GraviDos<br />
suspended balance. In direct<br />
comparison to a lab balance it is<br />
extremely compact an suitable for<br />
process application.<br />
GraviDos ® pressure resistant<br />
With the pressure<br />
resistant GraviDos<br />
tank the system<br />
can be operated up<br />
to 345 bar.<br />
GraviDos ® Standing Feed Tank<br />
With the GraviDos desktop scales<br />
standing containers can also be<br />
used as feed tanks.<br />
For further information see chapter<br />
Equipment and Components.<br />
GraviDos ® heating jacket<br />
GraviDos ® - Control Device for Stand-Alone Operation<br />
The GraviDos-Stand-Alone System enables a<br />
gravimetric dosing control even without automation<br />
system. The setpoint flow rate, the final weight, and<br />
the dosing period can be preset via the installed<br />
operator interface as well as via serial or analogue<br />
interface.<br />
The two-way valve necessary for flow control and<br />
the suspended scales of the GraviDos-System are<br />
connected directly.<br />
The device is both suited for batch and continuous<br />
dosing. In addition, it also supports automatic<br />
refilling.<br />
The optional Ex-adapter enables the deployment of<br />
the GraviDos load cells in explosive environments.<br />
Blast protection category inherent control [EEx ia]<br />
IIC for zone 0,1 or 2.<br />
With the GraviDos heating jacket it is<br />
possible to heat up the GraviDos<br />
receiver containers.<br />
The heating jacket is connected to a<br />
switching socket. The heating output<br />
can be adjusted from 0 to <strong>10</strong>0%.<br />
If the interior temperature is<br />
supposed to be controlled, it is<br />
necessary to install a temperature socket in the<br />
cover or an additional optional socket.<br />
Technische Daten<br />
Power Supply 230 V, 1A<br />
Weight approx. 900 g<br />
Max. Temperature 200 °C<br />
Order Code Description<br />
IL-GRAVIDOSST1 GraviDos control device for stand-alone operation<br />
IL-GRAVIRS Optional RS232 interface<br />
IL-GRADOEX Ex equipment of the GraviDos weighing module for zones 0.1 or 2<br />
The GraviDos control device for Stand-Alone Operation is compatible with all components and accessories<br />
of the GraviDos-System.<br />
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Dosing Systems and Pumps<br />
Order Code Description<br />
IL-GRADO<strong>10</strong>00D Digital suspeded balance 1.000 g for receiver tanks up to 500ml, incl. bracket, cable<br />
IL-GRADO3000D Digital suspeded balance 3.000 g for receiver tanks up to 2000ml, incl. bracket, cable<br />
IL-GRADO7000D Digital suspeded balance 7.000 g for custom made receiver tanks, incl. bracket, cable<br />
IL-GRADO<strong>10</strong>000D Digital suspeded balance <strong>10</strong>.000 g for custom made receiver tanks, incl. bracket, cable<br />
IL-GRADO15000D Digital suspeded balance 15.000 g for custom made receiver tanks, incl. bracket, cable<br />
IL-GRADO<strong>10</strong>00 Suspended balance with tank mounting <strong>10</strong>00 g, for feed tanks up to <strong>10</strong>00 ml, incl. cable<br />
IL-GRADO3000 Suspended balance with tank mounting 3000 g, for feed tanks up to 2000 ml, incl. cable<br />
IL-GRADO7000 Suspended balance 7000 g, for customized feed tank, incl. cable<br />
IL-GRADO<strong>10</strong>000 Suspended balance <strong>10</strong>000 g, for customized feed tank, incl. cable<br />
IL-GRADO15000 Suspended balance 15000 g, for customized feed tank, incl. cable<br />
HK-GRADOMV1 Measuring amplifier 1 channel external measuring amplifier to connect to an analogue input<br />
HK-GRADOMV1D External digital measuring amplifier, 1 channel to connect to RS232 V24 interface<br />
HK-GRADOMV1D-SN Power supply for digital measuring amplifier HK-GRADOMV1D<br />
HK-AD24DMS4PTR Measurement system 4 channels, card w/o connection board for GraviDos suspended scales<br />
LP-DMS4DA4PT connection board with 4 channels for GraviDos, 4 digital inputs<br />
LP-DMSP8 connection board with 8 strain-gauge channels for GraviDos (requires 2 times HK-AD24DMS4)<br />
IL-GRAVLBB250 Feed tank* 250 ml, borosilicate glass, PTFE tap, GL 14 connection, weight: 250g<br />
IL-GRAVLBB500 Feed tank* 500 ml, borosilicate glass, PTFE tap, GL 14 connection, weight: 350g<br />
IL-GRAVLBB<strong>10</strong>00 Feed tank* <strong>10</strong>00 ml, borosilicate glass, PTFE tap, GL 14 connection, weight: 550g<br />
IL-GRAVLBB2000 Feed tank* 2000 ml, borosilicate glass, PTFE tap, GL 14 connection, weight: 900g<br />
IL-GRAVLBGRAD Grading of a feed tank (ml-scale)<br />
IL-GRAVLBS150 Receiver tank 150 ml, 345 bar, high-grade steel 316L/ DOT-3A 5000 TC-3ASM<br />
IL-GRAVLBS300 Receiver tank 300 ml, 345 bar, high-grade steel 316L/ DOT-3A 5000 TC-3ASM<br />
IL-GRAVLBS500 Receiver tank 500 ml, 345 bar, high-grade steel 316L/ DOT-3A 5000 TC-3ASM<br />
IL-GRAVIHEAT250 Heating jacket for GraviDos feed tank 250 ml<br />
IL-GRAVIHEAT500 Heating jacket for GraviDos feed tank 500 ml<br />
IL-GRAVIHEAT<strong>10</strong>00 Heating jacket for GraviDos feed tank <strong>10</strong>00 ml<br />
IL-GRAVIHEAT2000 Heating jacket for GraviDos feed tank 2000 ml<br />
IL-GRAVIHEATSON Heating jacket for GraviDos custom design<br />
IV-MB-FK1-2-1,5-UNF-ea Universal 2/2 way lab valve ETFE, FFKM, nominal diameter of 1.5 mm, Kv 0,06 m³/h, 0 to approx.<br />
3 l/h media connector 1/4" UNF with cables of 3 m for the connection to LAB-PI or MSR-PI<br />
VL-KB-MB-FK1 Fixing element to connect small and medium sized HITec <strong>Zang</strong> valves to LAB-kit-ALU-system.<br />
Please state exact valve type when ordering .<br />
IV-MP-UK1-2-0,8-ma-ea 2/2 way proportional magnetic control valve, FPM, nominal diameter of 0.8 mm, Kv 0.02 m³/h,<br />
with cables of 1.5 m for the connection to LAB-PI or MSR-PI<br />
IV-MB-UM2-2 2/2-way- high-pressure-valve, 420 bar, 24V, 4 A<br />
IV-MB-UM2-PS Power supply for 2/2-way- high-pressure-valve, 24V, 4 A, with auxillary relay<br />
VL-KB-MB-UM2 Valve-connection piece to connect one V-MB-UM2-2 valve to LabKit-ALU-system<br />
IL-GRADOADV Adapter round measurement cell reducing adapter to 12 mm tube construction systems<br />
IL-GRADOADR12 Adapter-round manifold for measuring cell on to 12 mm tube construction system<br />
IL-GRADOADR14 Adapter-round manifold for measuring cell on to 14 mm tube construction system<br />
IL-GRAVI-KAL<strong>10</strong>00 Calibration weight <strong>10</strong>00g<br />
IL-GRAVI-KAL2000 Calibration weight 2000g<br />
IL-GRAVIDOSST1 GraviDos control device for stand-alone operation<br />
IL-GRAVIRS Optional RS232 interface<br />
IL-GRADOEX Ex equipment of the GraviDos weighing module for zones 0.1 or 2<br />
IS-W-GRAVISTAND Table stand with leveling screws<br />
IS-W-GRAVIPLATE Weighing plate diameter 140mm<br />
IS-W-GRAVICRANE Three element pivot lift crane for tube guidance into open weighing containers<br />
SL-GOPGRAVITARI HiBatch basis operation: Taring a load cell<br />
SL-GOPDOSIGRAVI1 HiBatch basis operation: gravimetric dosing without refilling option<br />
*with additional Gl14 connection above for venting or pressure compensation ** higher Kv values and other materials upon request<br />
ma = Medienanschluss:<br />
SN4/6 Verschraubung für Schlauch mit<br />
Durchmesser innen/außen 4,0/6,0 mm<br />
GMG1/8 Gewindemuffe G 1/8“<br />
ea = Elektrischer Anschluss<br />
T Tuchel-Stecker für LAB-PI<br />
O offene Enden für MSR-PI<br />
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Dosing Systems and Pumps<br />
Controlled Dropping Funnel AlfaDos<br />
The dosing system AlfaDos functions like the<br />
classic dropping funnel according to the force of<br />
gravity principle or supported with pressure and, like<br />
these, does not need any pumps. Due to this, the<br />
problems, which always occur with pumps, such as<br />
media incompatibility, suction problems, bubbles,<br />
etc. are eliminated.<br />
In addition, it leads to a considerable saving of<br />
expense since no expensive balances and pumps<br />
are needed. The flow is controlled via a magnetic<br />
valve. As there is no measurement or control of the<br />
flow rate, the dosing rate is not particularly accurate.<br />
In some cases, for example during the pHadjustment,<br />
the consistent compliance to a specific<br />
dosing-rate is however not so important. In this case<br />
AlfaDos is the absolute the lowest-cost solution.<br />
Application fields<br />
� Simple dosing tasks<br />
� pH-control<br />
� RedOx-adjustment<br />
� Titration<br />
� Dosing depends on process sizes<br />
An AlfaDos system consists of a supply vessel of<br />
glass, stainless steel, or synthetic material. The<br />
drain occurs due to the force of gravity or applied<br />
pressure and is controlled via a magnetic valve.<br />
Dosing under pressure or vacuum is possible if<br />
pressure compensation pipe is provided..<br />
Applications:<br />
The classical dropping funnel or dosing mechanisms<br />
with pumps and balances are replaced by AlfaDos, if<br />
the requirements regarding the stability of the dosing<br />
rate are modest, or the dosing is adjusted in<br />
dependency to another variable, for example the pH<br />
value or the RedOx potential, or if a controlled<br />
variable, such as the temperature, is deployed as a<br />
process signal.<br />
In the standard version, any material in contact with<br />
media is made glass, PTFE and PVDF. Special<br />
versions in other materials are also possible.<br />
An AlfaDos dosing device occupies a channel for the<br />
valve on a digital-output-board.<br />
Properties<br />
� Low-cost<br />
� Compact and robust<br />
� Does not need pumps<br />
� Resistant to aggressive media<br />
� Easy to clean<br />
Technical data<br />
Viscosity range 0,1...<strong>10</strong>0 mPa s<br />
Pressure range 0...1 bar abs.<br />
(for overpressure on<br />
request)<br />
H2O flow range up to <strong>10</strong>0 ml / min<br />
(di=2 m³, h=50cm, no<br />
pressure)<br />
H2O flow range up to 20 ml / min<br />
(di=1 m³, h=50cm, no<br />
pressure)<br />
H2O flow range up to 500 ml / min<br />
(di=2 m³, auxiliary<br />
pressure of 1 bar)<br />
Order Code Description<br />
IL-GRAVLBB250 Feed tank* 250 ml, Borosilicate glass, PTFE tap, GL 14 connection, 250 g<br />
IL-GRAVLBB500 Feed tank* 500 ml, Borosilicate glass, PTFE tap, GL 14 connection, 350 g<br />
IL-GRAVLBB<strong>10</strong>00 Feed tank* <strong>10</strong>00 ml, Borosilicate glass, PTFE tap, GL 14 connection, 550 g<br />
IL-GRAVLBB2000 Feed tank* 2000 ml, Borosilicate glass, PTFE tap, GL 14 connection, 900 g<br />
IV-MB-FK1-2-1,5-UNF-ea Universal 2/2 way lab valve PVDF, FFKM, nominal diameter of 1,5 mm, Kv 0,06 m³/h, 0 to<br />
approx. 3 l/h, media connector 1/4“ UNF, 3m cables for the connection to LAB-PI or MSR-PI<br />
VL-KB-MB-FK1 Valve to valve fixing element for LAB-kit-ALU-system<br />
*with additional Gl14 connection above for aeration or pressure compensation ** higher Kv values and other materials on request<br />
ea = Electrical connection T Tuchel plugs for LAB-PI<br />
O open ends for MSR-PI<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Pumps, dosing pumps<br />
Pumps, just as valves, have an important role in<br />
laboratories and pilot plant stations. Their variety is<br />
nearly unmanageable as they are needed for<br />
conveying, circulating or detailed volume dosing of<br />
the smallest to bigger material flows, across a large<br />
scale of viscosity values even with solids or for<br />
emulsions. Also the dosing of gases and the<br />
evacuating of plants belongs to the application area.<br />
Here, you can also expect our competent advice and<br />
individual lay out design especially for your<br />
application. Our know-how stretches over the most<br />
famous manufactures like: <strong>HiTec</strong> <strong>Zang</strong> Prominent,<br />
Lang, Gather, Ismatec, Speck, Lewa and many<br />
more, so that we can also help you with realising<br />
special tasks.<br />
Areas of Application<br />
� Circulation of heating and cooling media<br />
� Dosing of ingredients<br />
� Transport of ingredients, intermediate and final<br />
products<br />
� Generation of pressure, e.g. in pressure reactors,<br />
for filtering<br />
� Generation of vacuum<br />
� Ex-area zone 1 and 2 with pressure enclosed exthree-phase<br />
motor, respectively special versions.<br />
Which Pump for which Application?<br />
For the most important tasks in the laboratories and<br />
pilot plant stations, you can find approved standards<br />
under “First Choice”, which will help you to make<br />
your choice. With help of the following table, you can<br />
find the appropriate pump for various applications.<br />
In case of doubt, clarify with our project department<br />
which application you need.<br />
Here you will find:<br />
� Peristaltic pumps<br />
� Pneumatic pumps<br />
� Magnetic membrane dosing pumps<br />
Dosing Systems and Pumps<br />
Advantages, performances<br />
� All pumps are directly controllable from<br />
<strong>HiTec</strong>-PIs<br />
� Feedback from operation parameters to<br />
monitor when required<br />
� Cables and plugs for the direct connection<br />
with your LAB-xxx or MSR-xxx PI available<br />
� Hydraulic design and tuning to the media in<br />
your plant, available auxiliary power etc. by<br />
our engineering department<br />
� Special modifications to your control tasks by<br />
variable displace volumes, frequency<br />
converter…<br />
� We search and deliver also special<br />
accessories and we deliver your pump as a<br />
ready to use device<br />
� On request, bonding into your application<br />
program by our application programmer<br />
� On request, design, construction and<br />
parameterising of your control circuit by our<br />
engineering department<br />
� Advise and adjustment to your existing<br />
automation devices completely from one<br />
source<br />
� Magnetic piston dosing pumps<br />
� Positive displacement dosing pumps<br />
� Syringe dosing<br />
� High pressure double piston dosing pumps<br />
� Eccentric spiral pumps<br />
� Tooth ring pumps<br />
� Micro-tooth ring pumps<br />
� Centrifugal pumps<br />
� Membrane vacuum pumps<br />
� Rotary valve vacuum pump<br />
Automatic<br />
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Dosing Systems and Pumps<br />
IP-P-SM1..<br />
IP-P-M1..<br />
IP-P-P1..<br />
IP-P-M2..<br />
IP-P-m³..<br />
IP-P-LabDos-P..<br />
Application \ Type<br />
dosing<br />
fluids + + + + + + + + + + + + + +<br />
aggressive + + + + + + + + o + o o o +<br />
suspensions + + + o + o +<br />
viscous + o + + o + o o + +<br />
abrasive + + o o +<br />
outgassing + + o o o<br />
high pressure o o + o + +<br />
very high pressure +<br />
in vacuum + o + o + + o o o + o +<br />
volumetric + + + + + + + + + + + o + +<br />
gravimetric in control circuit + + + + + o o o + + + + +<br />
small quantities + + + + o + + o + + o<br />
multi-channel + +<br />
melting o o + +<br />
gases + o o o + o<br />
conveying / circulation<br />
fluids + + o o o o o o o + + + + + + +<br />
aggressive + + o o o o o o o + + o o + + +<br />
abrasive + o o +<br />
viscous + o + o + o o +<br />
heat carrier o + o<br />
flammable (solvent) + + o o o o o + o o + o + o o<br />
high temperatures o o + +<br />
gases + o o o +<br />
vacuum<br />
+<br />
rough + + +<br />
fine o + o<br />
aggressive vapours + + o +<br />
general characteristics<br />
self-priming + + + + + + o + o + +<br />
pulsation free o o o + + + + + + +<br />
bi-directional flow +<br />
warming up + o o +<br />
steriliseable +<br />
ex-application o + o o o o<br />
+ = well suitable, o = conditional suitable, upon request<br />
First Choice Types for Laboratories and Pilot Plants<br />
In the following you can find a suitable pump for<br />
every application.<br />
To make clear which pump you need, we need some<br />
information from you. It is also possible to consult<br />
one of our engineers and find out together the<br />
needed information.<br />
What we will ask you:<br />
Applications:<br />
� Dosing: volumetric, gravimetric in a control circuit<br />
...<br />
� Circulation, conveying: cooling- heating media,<br />
solvents...<br />
Convey media:<br />
Particular features: density, viscosity, flammable,<br />
explosive, conductibility, aggressive, emulsion,<br />
suspension, abrasive, crystallise...<br />
IP-SYRDOS..<br />
IP-P-LabDos-T..<br />
IP-P-P3..<br />
IP-P-E1..<br />
IP-P-S1..<br />
IP-P-S2..<br />
IP-P-Rx..<br />
IP-P-Z1..<br />
IP-B-K1..<br />
IP-B-K2..<br />
IP-B-V1..<br />
Convey quantity / range<br />
Media temperature / range<br />
Vapour pressure at operation temperature<br />
Self-priming / supply / primary pressure<br />
Ambient temperature<br />
IP-B-V2..<br />
IP-B-VPS..<br />
Connections:<br />
used / wished piping, tubes, and connecting parts?<br />
Bonding in a control circuit:<br />
Actual value – signal transmitter, control accuracy,<br />
control velocity, noise magnitudes, linking with other<br />
control circuits / controllers...<br />
Particular requirements:<br />
Safety aspects, cleaning possibilities, CIPcompatible<br />
etc.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LabDos Peristaltic Pump<br />
Dosing Systems and Pumps<br />
Superios dosing technology: One fits all!<br />
Selection criteria for pumps are their dosing range,<br />
precision of dosing, media compatibility, viscosity<br />
range, interface types etc. The LabDos laboratory<br />
dosing pump fulfils many different criteria at a<br />
remarkable low price. LabDos is suited for dosing<br />
into reaction systems, transferring between tanks,<br />
sampling from vessels, for automatic sample<br />
drawing and for other liquid handling processes.<br />
The path breaking SofDrive drive technology<br />
combines the advantages of a servo motor and the<br />
step motor. The drive disposes of the robustness,<br />
the extremely broad revolution range, the absolute<br />
precision and the high durability of a step motor, but<br />
does however not show the pulsating running<br />
characteristics of the same. The SofDrive builds a<br />
perfect team with Watson Marlow and Masterflex.<br />
Large pushbuttons allow changing settings even<br />
with thick gloves. The wide display is illuminated, a<br />
wide viewing angle is ensured. It is suited both for<br />
stand-alone operation, as well as within automation<br />
systems.<br />
Properties of LabDos dosing pumps:<br />
� Universal use<br />
� Extremely large dosing range<br />
� Pulsation free high-precision drive<br />
� Revolution direction reversible<br />
� May be calibrated in g/min and ml/min<br />
� Robust and compact stainless steel housing<br />
� Optional separated pump head<br />
� Fast mode for aspiration, drain, flushing<br />
� Manual and external control<br />
� Ergonomic and intuitive handling<br />
� Stackable<br />
The simple functional principle of a peristaltic pump<br />
enables its cost efficient use from pumping to<br />
complex fluid handling requirements. The pump<br />
head is mounted on a sloped front for easy handling<br />
and maintenance.<br />
The LabDos peristaltic pump is a displacement<br />
pump, where outer rolls will drive the liquid through a<br />
hose.The conveyed media will therefore not touch<br />
any metal, the hose is the only media touching<br />
material. A contamination of pump and media is<br />
impossible.<br />
The gentle functionial principle assures a safe<br />
conveying of high viscous, abrasive, aggressive,<br />
scher-sensitive, foaming, gas or solid loaded, pure<br />
and valuable as well as explosive liquids and gases.<br />
Advantages of the LabDos peristaltic pump:<br />
� Free of dead storage<br />
� Self priming<br />
� Direct displacement against pressure<br />
� Low pulsation<br />
� High viscosity range<br />
� No valves or seals<br />
� Suction from 50 mbar vacuum<br />
� High media resistance, inert, hygienic<br />
� Suitable for media with solid particles<br />
� Dosing of shear strain sensitive fluids<br />
� No problems with bubbles<br />
� Fluid path visible<br />
� Easy to clean, easy maintenance<br />
� Monitoring of hose run time<br />
� Exchangeable pump head (optional)<br />
In combination with a GraviDos system, LabDos<br />
pumps may be used for gravimetric dosing.<br />
At the LabDos-Vario, it is possible to exchange the<br />
pump head without having to use any tools.<br />
Available are single head, double head, as well as 5<br />
and <strong>10</strong>-fold cassettes.<br />
FDA and USP23 Class VI conform hoses are<br />
available. With the development of new hose<br />
material the life expectancy was highliy increased<br />
eg. HPT-Ultra hose times fifty. The HPT-Ultra hose is<br />
suitable for nearly all aggressive chemicals,<br />
including organic solvants like MEK, THF and Toluol<br />
or acetone.<br />
The following comparative matrix illustrates that the<br />
LabDos peristaltic pump posseses more advantages<br />
than any other pump and is therefore universally<br />
deployable!<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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The following comparative matrix illustrates that the<br />
LabDos peristaltic pump posseses more advantages<br />
than any other pump and is therefore universally<br />
deployable!<br />
Pump characteristics compared<br />
Dosing Systems and Pumps<br />
Peristaltic Diaphragm Gear Plunger<br />
pump pump pump pump<br />
Dosing range ++ o ++ +<br />
Exact dosing of small volumes ++ o o +<br />
Direct displacement against pressure + + - ++<br />
Bidirectional pumping ++ - - ++ o<br />
Pumping of shear strain sensitive fluids ++ ++ - o<br />
Fluids containing abrasive solids ++ - - -<br />
High viscous media ++ - - ++ -<br />
Self-priming ++ - - - - ++<br />
Dosing from/to vacuum ++ o - - ++<br />
Without dead storage ++ - - - - - -<br />
Self locking ++ - - - - - -<br />
Safe dry running ++ o - - - -<br />
Autoclavable (dependent on hose) ++ - - - - - -<br />
Chemically persistant + + o +<br />
<strong>10</strong>0% decontamination ++ - - - - - -<br />
Easy maintenance ++ o o o<br />
Price/performance ratio ++ + o - -<br />
LabDos is available with various pump heads.<br />
Technical Data<br />
Pump head P30 P<strong>10</strong>0 Easy-Load Vario4(3)<br />
Dosing range 1 μl to 30 ml/min <strong>10</strong> μl to <strong>10</strong>0 0,2ml to 1,1 l/min 0,1ml to 1(1,2)<br />
ml/min<br />
l/min<br />
Hose inner diameter 0,25 to 2,4 mm 0,5 to 4 mm 0,8 to 8 mm 0,5 to 8 mm<br />
Wall thickness 0,85 mm 1,6 mm 1,6mm 1,6mm<br />
Supply preasure 0..2 bar 0..2 bar 0..2,5 bar 0..2,5 bar<br />
Revolution speed 0,01.. 300 rpm 0,01.. 200 rpm 0,01.. 300 rpm 0,01.. 250 rpm<br />
Viscosity 0...150.000 cps, 0...150.000 cps, 0...150.000 cps, 0...150.000 cps,<br />
newt.<br />
newt.<br />
newt.<br />
newt.<br />
Communication Interfaces RS232. optionally RS485 (ModBus or CAN) and analogue (0–5V/4–20mA)<br />
RS485 Mod-bus (opt.) Up to 32 pumps using one serial interface<br />
Digital input (TTL) Start/Stop, revolution direction<br />
Drive Pulsation-free SofDriveTM precision drive<br />
Power Supply 24V DC, 600 mA , Easy-Load Vario: 24V DC, 1A<br />
Protection Class IP 20<br />
Dimensions D / W / H 250 x 165 x 1<strong>10</strong> mm<br />
Weight approx. 2 kg<br />
The projected values are maximum values. They are dependend on tubing material, pressure and viscosity. Other pump heads are<br />
available on request.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Dosing Systems and Pumps<br />
LabDos P<strong>10</strong>0, with adjustable hose fitting<br />
LabDos-vario drive with fast exchangeable<br />
and stackable pumpheads<br />
LabDos-P-Easy-Load pump<br />
Vario-4 pumphead open<br />
Stack of Vario-3 and Vario-3E pump heads LabDos-P30 pump with fast-loading mini pump head<br />
The LabDos-Easy-Load pumps allows the use of a<br />
further Easy-Load for parallel dosing.<br />
With the stackable extension pump head VARIO-4E<br />
and VARIO-3E it is possible to extend the LabDosvario<br />
to multiple traces.<br />
Hint: By parallel dosing with two stackable<br />
Vario3/Vario3-E or two Easy-Load pump heads, an<br />
outstanding pulsation free feeding over the total<br />
feeding amount can be achieved.<br />
Automatic<br />
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Order Code Description<br />
IP-P-LABDOS-P30 LabDos Pump with mini pump head max. 30 ml/min, RS232 Interface<br />
IP-P-LABDOS-P<strong>10</strong>0 LabDos Pump with single pump head max. <strong>10</strong>0 ml/min, RS232 Interface<br />
IP-P-LABDOS-P-EASYLOAD LabDos Pump with pump head Easy-Load, 3 rolls, max. revolution speed 300 rpm<br />
IP-P-LABDOS-P-EASY-E Extension pump head Easy-Load, 3 rolls, max. revolution speed 300 rpm<br />
IP-P-LABDOS-P-EASY-TC Twin chanal pump head Easy-Load, 3 rolls, max. revolution 300 rpm, max. 500ml/min<br />
IP-P-LABDOS-P-VARIO LabDos Basic unit without pump head, RS232 Interface<br />
IP-P-LABDOS-P-VARIO-3 Peristaltic pump head for vario, 3 rolls<br />
IP-P-LABDOS-P-VARIO-3E Peristaltic stackable extension pump head for LabDos vario, 3 rolls<br />
IP-P-LABDOS-P-VARIO-4 Peristaltic pump head for vario, 4 rolls<br />
IP-P-LABDOS-P-VARIO-4E Peristaltic stackable extension pump head for LabDos vario, 4 rolls<br />
IP-P-LABDOS-P-MULTI-4-5 Pump head 5-fold maximum revolution speed <strong>10</strong>0 rpm, 4 rolls<br />
IP-P-LABDOS-AE Analogue interface/input revolution control (0–5 Volt and 4–20mA)<br />
IP-P-LABDOS-SK Flexible protection caps for push buttons<br />
CZ-USB-RS232 USB/RS232 converter cable USB/Sub-D9, 3 m, connects USB and RS232 interface<br />
IP-P-LABDOS-RS232BA RS232-T-bus adapter for a pump, max. 4 pumps at a single RS232 interface possible<br />
ZK-P-HI36-BS-R2-I-01 RS232 cable Sub-D9/Sub-D9, 3 m, to connect a LAB- or MSR-PI or PC<br />
ZK-P-HI36-BS-R2-I-02 RS232-bus cable Sub-D9/Sub-D9, 0,3 m, to connect of a RS232-bus adapter<br />
IP-P-LABDOS-RS485 RS485 bus connector, control of up to 32 pump via a serial interface<br />
IP-P-LABDOS-RS485BA RS485-T-bus adapter for a pump<br />
ZK-P-HI36-BS-R4-I-01 RS485 cable Sub-D9/Sub-D9, 3 m, to connect a LAB- or MSR-PI or PC<br />
ZK-P-HI36-BS-R4-I-02 RS485-bus cable Sub-D9/Sub-D9, 0,3 m, to connect a RS485-bus adapter<br />
IP-P-LABDOS-DISPENS Optional dispenser mode for LabDos, dosage of predefined volumina and amounts<br />
IP-P-LABDOS-DISPPB Pushbutton for LabDos, to trigger dosage start<br />
IP-P-LABDOS-DOMAS DosiMaster Software for dosage profiles and graphical charts<br />
CG-LABCOMMANDER LabCommander mini-terminal for laboratory devices<br />
Order Examples:<br />
LabDos basic unit with four-wheel pump head plus<br />
extension head and analogue interface.<br />
LabDos Extensions<br />
The LabDos Bus System<br />
All LabDos pumps are bus-compatible. The user is<br />
able to choose between a RS232-based or a<br />
RS485-based bus system. With the basic RS232<br />
bus, up to four pumps can be connected to a normal<br />
RS232 or, using the converter cable CZ-USB-<br />
RS232, to a USB interface.<br />
RS232 Bus for up to four Pumps<br />
Subsequently, a LABDOS-RS232BA bus adaptor<br />
and a RS232 cable is required for each pump.<br />
IP-P-LabDos-P-VARIO<br />
IP-P-LabDos-P-VARIO4<br />
IP-P-LabDos-P-VARIO4E<br />
IP-P-LabDos-AE<br />
The optional RS485 Bus IP-P-LABDOS-RS485<br />
enables the connection of up to 32 pumps to a<br />
RS485 interface. Subsequently, a IP-P-LABDOS-<br />
RS485BA bus adaptor is required for each pump.<br />
The bus adaptors are connected to each other with<br />
a bus cable of the required length.<br />
RS485 Bus for up to 32 Pumps<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LabDos Dispenser<br />
With the Dispenser extension, a LabDos pump<br />
becomes an independent dispenser. This enables<br />
the dosing of pre-set volumes or amounts. A<br />
dispensing process can be started using an external<br />
push-button (IP-P-LABDOS-DISPPB). This means<br />
that the set amount is dosed at the set dosing rate<br />
with every actuation of the push-button.<br />
LabDos PC Software<br />
With the DosiMaster software, it is possible to<br />
establish dosing profiles in an easy manner.<br />
The dosed amount is logged and graphically<br />
presented as a cumulative curve.<br />
The software can be extended through additional<br />
functions such as protocol print-out or data export to<br />
LIMS.<br />
Dosing Systems and Pumps<br />
Multi-Component-Mixer<br />
The Component-Mixer-Function is an extension of<br />
the DosiMaster software. It enables multicomponent<br />
mixing in batch and continuous<br />
operation through simultaneous activation of up to<br />
eight LabDos pumps.<br />
In batch operation mode, a mixture of up to eight<br />
components is established upon the actuation of a<br />
button. Hereby, it is possible to pre-set the amounts<br />
of the individual components or the mixing ration<br />
and the total amount.<br />
In continuous operation mode, the flows of the<br />
components intended for mixing, as well as the<br />
ratios in percent of the individual components, are<br />
preselected.<br />
LabCommander – Mini-Bedienstation<br />
Das LabCommander mini-Notebook ermöglicht die<br />
platzsparende Realisierung von Dosier-, Dispensierund<br />
Mischstationen auf dem Labortisch.<br />
Order Code Description<br />
CZ-USB-RS232 USB/RS232 Converter Cable USB/Sub-D9, 3 m to connect USB and RS232 interface<br />
IP-P-LABDOS-RS232BA RS232-T-Bus Adaptor for one Pump, max. 4 pumps possible at a RS232 interface<br />
ZK-P-HI36-BS-R2-I-01 RS232 Cable Sub-D9/Sub-D9, 3 m for connection to LAB- or MSR-PI or PC<br />
ZK-P-HI36-BS-R2-I-02 RS232-Bus Cable Sub-D9/Sub-D9, 0,3 m, for connection of RS232 Bus Adaptors<br />
IP-P-LABDOS-RS485 RS485 Bus Connection, activation of up to 32 pumps via a serial interface<br />
IP-P-LABDOS-RS485BA RS485-T-Bus Adaptor for one pump<br />
ZK-P-HI36-BS-R4-I-01 RS485 Cable Sub-D9/Sub-D9, 3 m for connection to LAB- or MSR-PI or PC<br />
ZK-P-HI36-BS-R4-I-02 RS485-Bus CableSub-D9/Sub-D9, 0,3 m, or connection of RS485 Bus Adaptors<br />
IP-P-LABDOS-DISPPB Dispensing-Option for LabDos wih push button to trigger dispensing processes<br />
SA-P-LABDOS-DOMAS DosiMaster Software for dosing profiles and graphical presentation of the cumulative curve<br />
SA-P-LABDOS-DOMASM DosiMaster Extension: Mixer Function<br />
CG-LABCOMMANDER LabCommander Mini-Control Station for Laboratory Devices<br />
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Laboratory<br />
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Maximum delivery rates in ml/min, dependant of hose diameter and pump:<br />
Di/<br />
mm<br />
P30 (at 290<br />
rpm)<br />
P<strong>10</strong>0 (at<br />
200rpm)<br />
VARIO-3<br />
(at 250<br />
rpm)<br />
VARIO-4<br />
(at 250<br />
rpm)<br />
Easy-<br />
Load<br />
(at<br />
300rpm)<br />
P30<br />
(per rev)<br />
P<strong>10</strong>0<br />
(per rev)<br />
VARIO-3<br />
(per rev)<br />
VARIO-4<br />
(per rev)<br />
Easy-Load<br />
(per rev)<br />
0,25 0,73 -- -- -- -- 0,0025 -- -- -- --<br />
0,5 2,8 3 7,5 7,5 -- 0,0095 0,015 0,03 0,03 --<br />
0,8 5,8 7 15 15 18 0,025 0,035 0,06 0,06 0,06<br />
1,6 20 22 65 62 75 0,07 0,13 0,26 0,25 0,21<br />
2,4 35 48 125 <strong>10</strong>0 113 0,12 0,25 0,5 0,4 0,35<br />
3,2 -- 82 250 212 240 -- 0,41 1 0,85 0,8<br />
4,0 -- 118 325 275 3<strong>10</strong> -- 0,52 1,3 1,1 1,0<br />
4,8 -- -- 550 475 500 -- -- 2,2 1,9 1,7<br />
6,4 -- -- 900 750 850 -- -- 3,6 3 2,8<br />
8,0 -- -- 1250 <strong>10</strong>00 1150 -- -- 5 4 3,8<br />
All value are depended on hose material and media. All values are only for orientation pusposes.<br />
IP-P-LabDos-P-MULTI-4-5.<br />
Maximum delivery rates in ml/min:<br />
Di/ mm IP-P-LabDos-P-MULTI-4<br />
(in ml at 1<strong>10</strong>rpm) approx.<br />
0,13 0,1<br />
0,25 0,5<br />
0,59 2,5<br />
0,63 3<br />
0,89 7<br />
1,02 9<br />
1,3 16<br />
1,42 18<br />
1,52 20<br />
2,06 33<br />
2,54 47<br />
2,79 55<br />
If in doubt please get in touch with us. We will<br />
Compatibility of Hose Materials<br />
advice you which hose are best suited for you<br />
media.<br />
Samples can be sent upon request.<br />
Hose Acid Base Solvent Others Remarks<br />
Name<br />
weak<br />
Mid<br />
strong<br />
weak<br />
Mid<br />
HPT-Silicon<br />
(Platin) + o - + + + - - - o - + o<br />
HPT-PVC + + - + + + - - - - - + o<br />
HPT-FuelOil + o - + o - + - - + - + -<br />
HPT-Neopren o o - + o o - - - o - + o<br />
HPT-Chem + + + + + + - - - + o + +<br />
strong<br />
aliphatic<br />
aromatic<br />
halogenated<br />
alcohols<br />
aldehyde/ketone<br />
salt<br />
oxidants<br />
*) These first class attributes do not<br />
guarantee a resistance to all<br />
chemicals. Some solvents cause<br />
swelling of the hose (e.g. Hydrocarbon,<br />
amine, CHC and other solvents). In<br />
case of doubt please order test probes.<br />
Bio compatible, very good<br />
mechanical attributes, not solvent<br />
resistant. transparent<br />
very inexpensive, very good<br />
mechanical attributes, contains<br />
diluent. Non solvent resistant. clear<br />
Special hose for motor fuels and<br />
oils. yellowish<br />
pressure/vacuum resistant, high<br />
lifetime expectancy, inexpensive black<br />
Flexibiliser free, inexpensive.<br />
Limited resistance to ketone. clear<br />
HPT-Viton® + + + + + + + + + + - + + Highly resistant, inexpensive. black<br />
pressure/vacuum resistant, high<br />
HPT-Pharm o o - + o o - - - o - + o<br />
lifetime expectancy, FDA, USP, cell<br />
culture. light beige<br />
HPT-Ultra* + + + + + + + + + + + + +<br />
Extremely high life cycle and highly<br />
resistant, expensive. dimm white<br />
+ Resistant: None or only minimal swelling, None or only minimal restriction of life span.<br />
o Limited resistance: Moderate swelling, restriction of life span. Must be tested in individual case.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Dosing Systems and Pumps<br />
- Not resistant: Strong restriction of life span or complete destruction of the hose.<br />
Availability with 1.6 mm wall thickness<br />
For LabDos P<strong>10</strong>0, Vario and Easy-Load, not suitable for P30 and MULTI-4<br />
Di/ HPT-Silicon HPT-PVC HPT-FuelOil HPT-Neopren HPT-MHL HPT-Viton® HPT-Ultra coupling<br />
mm<br />
(2 pcs.)<br />
0,8 + + + + + + -- +<br />
1,6 + + + + + + *** +<br />
2,4 + + + + + + -- +<br />
3,2 + + + + + + *** +<br />
4,0 + + + + + + -- upon request<br />
4,8 + + + + + + *** upon request<br />
6,4 + + + + + + -- upon request<br />
8,0 + + + + + + *** upon request<br />
+ available, stock article, *** only pre configured as pieces of 15cm available<br />
Availability with 0.8 mm wall thickness<br />
For P30 and MULTI-4, not suitable for LabDos P<strong>10</strong>0, Vario and Easy-Load<br />
Di/ HPT-Silicon HPT-PHARM HPT-FuelOil Tygon® Lab HPT-Viton® HPT-Ultra coupling<br />
mm<br />
(2 pcs)<br />
0,19 + upon request<br />
0,25 + + *** upon request<br />
0,51 + + + + upon request<br />
0,63 + + upon request<br />
0,89 + + + + upon request<br />
1,3 + + + upon request<br />
1,42 + + + + + upon request<br />
2,06 + + + + + upon request<br />
2,79 + + + + + upon request<br />
+ available, stock article, *** only pre configured as pieces of 15cm available<br />
The coupling element for the transition from the pump hose to other hose material is made of PVDF.<br />
All hoses are available as products sold by meter (except HPT-Ultra) or as pre configured 15 cm pieces per<br />
dozen.<br />
Analytics hoses for P30 pump heads (stock artikles):<br />
Order Code Description<br />
IP-P-HPT-PHARM-08-005-m Hose Pharmed, inner diameter 0.51 mm, wall thickness 0.8 mm<br />
IP-P-HPT-PHARM-08-009-m Hose Pharmed, inner diameter 0.89 mm, wall thickness 0.8 mm<br />
IP-P-HPT-PHARM-08-028-m Hose Pharmed, inner diameter 2.79 mm, wall thickness 0.8 mm<br />
IP-P-HPT-SILP-08-006-m Hose Silikon (platinum), inner diameter 0.64 mm, wall thickness 0.8 mm<br />
IP-P-HPT-SILP-08-013-m Hose Silikon (platinum), inner diameter 1.3 mm, wall thickness 0.8 mm<br />
IP-P-HPT-SILP-08-028-m Hose Silikon (platinum), inner diameter 2.79 mm, wall thickness 0.8 mm<br />
IP-P-HPT-PVC-08-003-m Hose PVC, inner diameter . 0,25 mm, wall thickness 0,8 mm<br />
IP-P-HPT-PVC-08-009-m Hose PVC, inner diameter . 0,89 mm, wall thickness 0,8 mm<br />
IP-P-HPT-PVC-08-028-m Hose PVC, inner diameter . 2,75 mm, wall thickness 0,8 mm<br />
IP-P-VITON-08-009-m Hose Viton®, inner diameter 0.89 mm, wall thickness 0.8 mm<br />
IP-P-VITON-08-014-m Hose Viton®, inner diameter 1.42 mm, wall thickness 0.8 mm<br />
IP-P-VITON-08-028-m Hose Viton®, inner diameter 2.79 mm, wall thickness 0.8 mm<br />
IP-P-HPT-FUELOIL-08-005-m Hose fuels and oils, inner diameter 0.51 mm, wall thickness 0.8 mm<br />
IP-P-HPT-FUELOIL-08-014-m Hose fuels and oils, inner diameter 1.42 mm, wall thickness 0.8 mm<br />
IP-P-HPT-FUELOIL-08-028-m Hose fuels and oils, inner diameter 2.79 mm, wall thickness 0.8 mm<br />
Hoses for other pumping heads can be found on the next page.<br />
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Dosing Systems and Pumps<br />
Order Code Description<br />
IP-P-HPT-SILP-16-008-x Hose silicone (platinum), inner diameter 0.8 mm, wall thickness 1.6 mm<br />
IP-P-HPT-SILP-16-016-x Hose Silikon (platinum), inner diameter 1.6 mm, wall thickness 1.6 mm<br />
IP-P-HPT-SILP-16-032-x Hose Silikon (platinum), inner diameter 3.1 mm, wall thickness 1.6 mm<br />
IP-P-HPT-SILP-16-048-x Hose Silikon (platinum), inner diameter 4.8 mm, wall thickness 1.6 mm<br />
IP-P-HPT-SILP-16-064-x Hose Silikon (platinum), inner diameter 6.4 mm, wall thickness 1.6 mm<br />
IP-P-HPT-SILP-16-080-x Hose Silikon (platinum), inner diameter 7.9 mm, wall thickness 1.6 mm<br />
IP-P-HPT-PVC-16-008-x Hose PVC, inner diameter 0.8 mm, wall thickness 1.6 mm<br />
IP-P-HPT-PVC-16-016-x Hose PVC, inner diameter 1.6 mm, wall thickness 1.6 mm<br />
IP-P-HPT-PVC-16-032-x Hose PVC, inner diameter 3.1 mm, wall thickness 1.6 mm<br />
IP-P-HPT-PVC-16-048-x Hose PVC, inner diameter 4.8 mm, wall thickness 1.6 mm<br />
IP-P-HPT-PVC-16-064-x Hose PVC, inner diameter 6.4 mm, wall thickness 1.6 mm<br />
IP-P-HPT-PVC-16-080-x Hose PVC, inner diameter 7.9 mm, wall thickness 1.6 mm<br />
IP-P-HPT-NEOPR-16-016-x Hose Neopren, inner diameter 1.6 mm, wall thickness 1.6 mm<br />
IP-P-HPT-NEOPR-16-032-x Hose Neopren, inner diameter 3.1 mm, wall thickness 1.6 mm<br />
IP-P-HPT-NEOPR-16-048-x Hose Neopren, inner diameter 4.8 mm, wall thickness 1.6 mm<br />
IP-P-HPT-NEOPR-16-064-x Hose Neopren, inner diameter 6.4 mm, wall thickness 1.6 mm<br />
IP-P-HPT-VITON-16-016-x Hose Viton®, inner diameter 1.6 mm, wall thickness 1.6 mm<br />
IP-P-HPT-VITON-16-032-x Hose Viton®, inner diameter 3.1 mm, wall thickness 1.6 mm<br />
IP-P-HPT-VITON-16-048-x Hose Viton®, inner diameter 4.8 mm, wall thickness 1.6 mm<br />
IP-P-HPT-VITON-16-064-x Hose Viton®, inner diameter 6.4 mm, wall thickness 1.6 mm<br />
IP-P-HPT-FUELOIL-16-016-x Hose fuels and oils, inner diameter 1.6 mm, wall thickness 1.6 mm<br />
IP-P-HPT-FUELOIL-16-032-x Hose fuels and oils, inner diameter 3.1 mm, wall thickness 1.6 mm<br />
IP-P-HPT-FUELOIL-16-048-x Hose fuels and oils, inner diameter 4.8 mm, wall thickness 1.6 mm<br />
IP-P-HPT-FUELOIL-16-064-x Hose fuels and oils, inner diameter 6.4 mm, wall thickness 1.6 mm<br />
IP-P-HPT-CHEM-16-016-x Hose Chem (Tygon® chemical), inner diameter 1.6 mm, wall thickness 1.6 mm<br />
IP-P-HPT-CHEM-16-032-x Hose Chem (Tygon® chemical), inner diameter 3.1 mm, wall thickness 1.6 mm<br />
IP-P-HPT-CHEM-16-048-x Hose Chem (Tygon® chemical), inner diameter 4.8 mm, wall thickness 1.6 mm<br />
IP-P-HPT-CHEM-16-064-x Hose Chem (Tygon® chemical), inner diameter 6.4 mm, wall thickness 1.6 mm<br />
IP-P-HPT-ULTRA-16-016-x Hose High Performance, inner diameter 1.6 mm, wall thickness 1.6 mm<br />
IP-P-HPT-ULTRA-16-032-x Hose High Performance, inner diameter 3.1 mm, wall thickness 1.6 mm<br />
-x: m = product sold by meter , k = 12 pcs 15 cm segments<br />
Other hoses and couplings are available on request.<br />
Order information hose couplings (stock articles):<br />
Order Code Description<br />
IP-P-FIT-I-PV-1/8 Hose coupling 1/8", PVDF<br />
IP-P-FIT-I-PV-3/16 Hose coupling 3/16", PVDF<br />
IP-P-FIT-I-PV-1/4 Hose coupling 1/4", PVDF<br />
IP-P-FIT-I-PV-1/16 Hose coupling 1/16", PVDF<br />
IP-P-FIT-I-PV-1/8 Hose coupling 1/8", PVDF<br />
IP-P-FIT-I-PV-3/16 Hose coupling 3/16", PVDF<br />
IP-P-FIT-I-PV-1/4 Hose coupling 1/4", PVDF<br />
IP-P-FIT-R-PV-1/16-1/8 Hose coupling as reduction piece 1/16 auf 1/8", PVDF<br />
IP-P-FIT-R-PV-3/16-1/8 Hose coupling as reduction piece 3/16 auf 1/8", PVDF<br />
IP-P-FIT-R-PV-1/4-1/8 Hose coupling as reduction piece 1/4 auf 1/8", PVDF<br />
IP-P-FIT-R-PV-3/8-1/4 Hose coupling as reduction piece 3/8 auf 1/4", PVDF<br />
Other hose couplings, T- and Y-couplings are available on request.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LabDos Gear Pumps<br />
Annual gear pumps for the pulsation-free conveying<br />
and dosing within the control circuit of particle-free<br />
liquids of low to higher viscosity with medium flow.<br />
Heating is possible.<br />
Special Characteristics:<br />
� Low-Noise Run<br />
� Valveless Design<br />
� High Pressure<br />
� Accurate and reliable<br />
� Long Term Stability<br />
� Extensive Operational Range<br />
� Small Dead Volume<br />
For operation at a LAB-PI, a RS232 interface is<br />
required.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Pump Heads:<br />
Type Maximum Delivery<br />
Rate<br />
280ML80B 280 ml/min<br />
070ML30B 70 ml/min<br />
018ML<strong>10</strong>B 18 ml/min<br />
Mode of Operation Magnet-coupled Annual Gear Pump<br />
Delivery Rate 0,05...280 ml/min / 0,012..70 ml/min / 0,03...18 ml/min<br />
Max. Pump Pressure 80 bar /30 bar / <strong>10</strong> bar<br />
Media Connections Di 4mm Da 6mm / Di 1/16" Da 8"/ Di 1/16" Da 1/8"<br />
Speed 0 to 6000 Rev/min. Speed is load-independent.<br />
System Pressure <strong>10</strong>0 bar<br />
Dosing into Vacuum No<br />
Suction Height Self-priming up to a low suction height depending on media.<br />
Materials in Contact<br />
with Media<br />
High Grade Steel 316L<br />
Media Temperature -5 ..60°C . Higher temperatures are available upon request.<br />
Activation RS232, optional 4..20mA<br />
Operational Voltage/ 230V AC, 150W<br />
Power<br />
Media Compatibility Many chemicals. Please verify individual cases.<br />
Protection Class IP 30<br />
EX Version No. If required, please contact us.<br />
Delivery Scope: Annual Gear Pump with RS232 Interface<br />
Order Code Description<br />
IP-P-Z1-280ML80B-E Gear Pump with 0,05...280 ml/min, Differential Pressure 80 bar, High Grade Steel 316L<br />
IP-P-Z1-070ML30B-E Gear Pump with 0,012..70 ml/min, Differential Pressure 30 bar, High Grade Steel 316L<br />
IP-P-Z1-018ML<strong>10</strong>B-E Gear Pump with 0,03...18 ml/min, Differential Pressure <strong>10</strong> bar, High Grade Steel 316L<br />
IP-P-Z1-HEAT Heating System for Annual Gear Pump Z1, Tmax = 60 °C<br />
ZK-IT-HI01-BS-R2-I-03 RS232 Cable Sub-D9/Sub-D9, 3 m for connection to a LAB- or MSR-PI or PC<br />
IP-P-LABDOS-RS485 RS485 Bus. Activation of up to 32 pumps via serial interface.<br />
Further accessories can be found in the Chapter „ LabDos Peristaltic Pumps“.<br />
Automatic<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
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Dosing Systems,<br />
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Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
280<br />
LabDos Piston Dosing Pump<br />
Valveless positive displacement piston pumps<br />
enables the precise dosing and pumping of small<br />
quantities of aggressive, viscous and crystallising<br />
media within the medium pressure and temperature<br />
range.<br />
The piston dosing pump LabDos-T is suited for<br />
varied dosing tasks even below the microlitre range<br />
(sub-microlitre).<br />
Particular Features:<br />
� Valveless Design<br />
� Chemically inert due to use of ceramic<br />
� Precise and reliable<br />
� Long term stability<br />
� Great working range<br />
� Only one moving part<br />
� Reversible<br />
� Small dead storage<br />
The displaced volume and the stroke frequency can<br />
be independently adjusted. This leads to an enormous<br />
working range. The displaced volume can be<br />
adjusted in <strong>10</strong>00 steps at the calibrating ring. The<br />
stroke frequency can be varied from 0,01 to 500 /<br />
min.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Pump Heads:<br />
Type Max.<br />
Displaced<br />
Volume<br />
Maximum<br />
Delivery Rate<br />
T-2 0 - 5 µl 0 – 2,5 ml/min<br />
T-12 0 - 25 µl 0 – 12,5 ml/min<br />
T-25 0 - 50 µl 0 – 25 ml/min<br />
T-50 0 -<strong>10</strong>0 µl 0 – 50 ml/min<br />
Operating mode Valveless positive displacement piston pump with adjustable drive<br />
Max. flow rate up to 3000 ml/h<br />
Max. discharge pressure 6,9 bar<br />
Dosing in vacuum possible<br />
Stroke frequency up to 500/min<br />
Max. Displaced Volume 5 – <strong>10</strong>0 μl<br />
Suction Lift Self-priming, dependent of media<br />
Media affecting materials PVDF/ceramic piston and bushing<br />
Media connection Hose/plastic tube inner /outer diameter = 4/6 mm<br />
Media temperature Max. <strong>10</strong>0 °C<br />
Activation serial connector RS232<br />
Power supply 230 V AC<br />
Media compatibility Various chemicals, necessity to examine in individual cases<br />
Protection Category IP20<br />
Ex-version No<br />
Delivery Scope: Piston dosing pump with RS232 interface.<br />
Order Code Description<br />
IP-P-LABDOS-T-2 LabDos pump with piston pump head, 0 – 2,5 ml/min<br />
IP-P-LABDOS-T-12 LabDos pump with piston pump head, 0 – 12,5 ml/min<br />
IP-P-LABDOS-T-25 LabDos pump with piston pump head, 0 – 25 ml/min<br />
IP-P-LABDOS-T-50 LabDos pump with piston pump head, 0 – 50 ml/min<br />
IP-P-LABDOS-AE Analogue interface /input rpm control (0–5 Volt and 4–20mA)<br />
ZK-IT-HI01-BS-R2-I-03 RS232 Cable sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />
IP-P-LABDOS-RS485 RS485 Bus, activation of up to 32 pumps via a serial interface<br />
media connection:<br />
SN4-6 Tube fitting I.D./OD 4/6mm On request deliverable:<br />
� Other flow rates<br />
� Other materials: high grade steel, carbon<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Dosing Systems and Pumps<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 281
282<br />
SyrDos2 Syringe Doser<br />
The SyrDos2 pump offers extended application<br />
options.<br />
The integrated control panel with a LC-Display also<br />
enable the operation as independent pump.<br />
It supports, in addition to the LabDos-compatible<br />
RS232 protocol, the standardised MODBus-RTU<br />
protocol. The power supply for the two pumps is<br />
integrated.<br />
If two pumps are accordingly connected with the<br />
-CONT option, continuous conveying is also<br />
possible. Shock-free change-overs are reached with<br />
a special algorithm.<br />
Due to the robust high grade steel casing, it is also<br />
suited for deployment in rouh process conditions.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
SyrDos2 Syringe Doser with 2/3-Way Valves<br />
Mode of Operation Syringe Doser with step motor drive with up to <strong>10</strong>.000 steps/s.<br />
Max. Delivery Rate Depending on syringe, 50/<strong>10</strong>0/250/500 µl and 1/2,5/5/<strong>10</strong>/25/50 ml in<br />
2,5/4,9 s<br />
Max. Pump Pressure <strong>10</strong> bar, depending on syringe. Higher pressures (up to 28 bar) are<br />
available upon request.<br />
Dosing into Vacuum Possible up to <strong>10</strong> mbar (consider the vapour pressure)<br />
Resolution 24.000/48.000 Steps<br />
Suction Height Self-priming, media-dependent<br />
Materials in Contact with Media Glass, PTFE, Kel-F or PPF, optional Ceramic<br />
Media Connections UNF ¼“ 28G<br />
Media Temperature 15 to 40°C<br />
Activation Serial Interface RS232 or RS485 (MODBus-RTU Protocol)<br />
Operational Voltage (SYRDOS2) 230V AC, <strong>10</strong>0VA<br />
Media Compatibility Many chemicals. Please verify individual cases.<br />
Protection Class IP 20<br />
Dimensions (WxHxD) 223 x 270 x 180 mm<br />
Weight approx. <strong>10</strong> kg<br />
EX Version No<br />
Order Code Description<br />
IP-SYRDOS2-ss-V2/3 SyrDos2 Syringe Doser for 50µl to 50ml Syringes, RS232, RS485, 2/3-Way Valve<br />
IP-SYRDOS2-ss-VDxx SyrDos2 Syringe Doser for 50µl to 50ml Syringes, RS232, RS485, mutliway-valve (distr)<br />
IP-SYRDOS2-ss-VNDyy Syringe Doser for 50µl to 50ml Syringes, RS232, RS485, mutliway-valve (non distribution)<br />
IP-SYRDOS-VCER Extra Charge for Ceramic Version for 2/3-Way or Multi-Way Valve (1 required per valve)<br />
IP-SYRDOS-VHPR Extra Charge for max. Pressure 28 bar for 2/3-Way or Multi-Way Valve (1 required per valve)<br />
IP-SYRDOS-SYRG-vol Syringe for Syringe Doser, Glass<br />
IP-SYRDOS-CONT SyrDos Extension for continuous conveying with two pumps<br />
IP-SYRDOS-CHCKVAL 1 Pair of nonreturn valves for SyrDos, moisted material: PEEK, Spring: Gold-plated High Grade<br />
Steel<br />
ZK-IT-HI01-BS-R2-I-03 RS232 Cable Sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />
ss = Resolution, Steps 24 = 24.000, 48 = 48.000<br />
xx = Number of Positions, 2 to12<br />
yy = Number of Ways, 3 or 4<br />
vol = 50U, <strong>10</strong>0U, 250U, 500U, <strong>10</strong>00U, 2500U, 5M,1M, 25M, 50M<br />
accordingly 50/<strong>10</strong>0/250/500 μL and 1/2/2,5/5/<strong>10</strong>/25/50 ml<br />
Example Order:<br />
Duplex-Syringe Doser, Resolution: 48.000 Steps,<br />
12-Way-Distribution Valve, Media Connection UNF<br />
1/4-28, Activation RS232, 3 m RS232 Cable for<br />
connection to LAB- or MSR-PI, 1 ml Syringe.<br />
Special Design for higher pressure. Special materials<br />
etc. are available upon request..<br />
Please do not hesitate to request more detailed<br />
information, if required.<br />
Order Codes: IP-SYRDOS-48-VD12 and IP-SYRDOS-SYRG-<br />
<strong>10</strong>00U<br />
Other delivery rates are available upon request.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Dosing Systems and Pumps<br />
Diaphragm Doser with Step Motor Control<br />
MembraneDoser and PTFE-Pump Head<br />
This pump is particularly suited for the low-pulsation<br />
conveyance of aggressive fluids within the range<br />
0‚002 L/h - 48L/h at up to 18 bar<br />
the membrane pump doser combines all features<br />
and functions of conventional dosing pumps and<br />
makes dosing so uncomplicated that you can take<br />
Dosing Heads<br />
PP Type DME PP<br />
VA (high grade steel) Type DME VA<br />
VA (electrically heated) Optional<br />
PTFE Type DME PTFE<br />
PTFE / externally cooled Optional<br />
PTFE / externally heated Optional<br />
PTFE /electrically heated<br />
Accessories<br />
Optional, with/without<br />
control for heating<br />
jackets<br />
Pulsation Absorber PTFE Optional<br />
Pulsation AbsorberVA Optional<br />
Pressurised Valve PTFE Optional<br />
(Prel.) Filter PTFE Optional<br />
Connections PTFE Optional in GL14B or<br />
GL18B<br />
Connections high grade Optional in Swagelok or<br />
steel<br />
Gyrolok<br />
Heating/cooling f. pump<br />
head/feeding<br />
Optional<br />
Vaccuum application Optional<br />
high precision for granted.<br />
The main functional principle of the pump is based<br />
on the direct connection of motor and diaphragm<br />
over a slide crank gear transmission with a tooth belt<br />
transmission. With this method, in contrary to to<br />
conventional dosing pumps, the position and the<br />
speed of the diaphragm are controlled via an<br />
electronic system with a microprocessor throughout<br />
the whole pressure/suction cycle.<br />
The stroke frequency and the duration of the<br />
pressure stroke are controlled via a microprocessorcontrolled<br />
step motor according to the required<br />
dosing quantity. This drive is unique in this category<br />
and can only found here.<br />
Alternatively, the diaphragm doser is available with<br />
PP / VA or PTFE dosing heads and / or heatable or<br />
cooled dosing units.<br />
Interfaces<br />
4-20mA yes<br />
RS232 Optional with digitalanalogue<br />
converter<br />
External Pulse yes<br />
Internal Timer yes<br />
Fieldbus-Interface yes<br />
NAMUR-Interface<br />
Technical Data<br />
Optional<br />
Operating Mode step motor- diaphragm<br />
dosing pump<br />
Flow Rate 0,002 l/h bis 48 l/h<br />
Adjustable Range Flow<br />
Rate<br />
1:<strong>10</strong>00<br />
Maximum Output 18 bar<br />
Pressure<br />
Dosing in Vacuum no<br />
Suction Lift 5 m<br />
Dosing Faults ± 1% of the set value<br />
Max. Viscosity 500 mPas<br />
In contact with Media VA or PP orPTFE<br />
Activation serial connector RS232,<br />
4-20 mA, 2-<strong>10</strong> V, single<br />
stroke control<br />
Power supply <strong>10</strong>0-230 V AC<br />
Order Code Description<br />
IP-P-SM1-VA -mc Precision step motor dosing pump, VA pump head, RS232<br />
IP-P-SM1-PP -mc Precision step motor dosing pump, PP pump head, RS232<br />
IP-P-SM1-PTFE -mc Precision step motor dosing pump, PTFE pump head, RS232<br />
ZK-IT-HI01-BS-R2-I-03 RS232 Cable sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />
mc=Model Code:<br />
Model Code Dosing Rate Max. Pressure<br />
2-18 2,5 l/h 18 bar<br />
8-<strong>10</strong> 7,5 l/h <strong>10</strong> bar<br />
12-6 12 l/h 6 bar<br />
48-3 48 l/h 2,6 bar<br />
Order example:<br />
Precision step motor dosing pump, 2,5 L/h, 18 bar,<br />
pump head PTFE,<br />
Order code: IP-P-SM1-PTFE-2-18<br />
Automatic<br />
Laboratory<br />
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Plant<br />
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Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 283<br />
Equipment and<br />
Components<br />
Process Analytics<br />
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Stirring and<br />
Dispersing<br />
Services
284<br />
Pneumatic Dosing Pumps<br />
Modotec ® Dosing system; pneumatic dosing of<br />
liquids and gases.<br />
Modular constructed dosing system consisting of a<br />
control unit and diaphragm dosing head with<br />
positively controlled diaphragm valves.<br />
The pneumatic activation ensures that the pump<br />
heads are especially suited for the Ex-range.<br />
Module Control<br />
� Autonomous Control Unit<br />
� Externally controllable<br />
� Direct control through PLS via<br />
Type C<br />
� Power Supply220V / 24 V<br />
� Compressed Air 3 – 6 bar<br />
Autonomous Control with integrated pneumatic Valve Terminal<br />
Valve Terminal for Activation via LabBox/manager or SPS<br />
Dosing Systems and Pumps<br />
Module Dosing Head<br />
� Compact Dosing Head<br />
� Small Dimensions<br />
� Version with low dead storage<br />
� No mechanically moved parts<br />
� Low wear, low-maintenance<br />
� Corrosion-resistant materials<br />
� Simple assembly and cleaning<br />
� Option: Ex-version<br />
Special Features Dosing Head Type T<br />
� Controllable Diaphragm Valves<br />
� Position-independent installation<br />
� Dosing directly into the vacuum<br />
� Optional Ex-version<br />
Special Features Dosing Head Type S<br />
� Ball Valves<br />
� Twin Dosing Heads<br />
� Optional Ex-version<br />
Special Features Dosing Head Type P<br />
� Dosing Head with additional controllable multifunction<br />
valves for automated sample drawing<br />
� Multi-Component Dosing<br />
� Multi-way Dosing Head<br />
� Optional Ex-version<br />
Special Features Dosing Head Type V<br />
� Conveyance out of the vacuum into the normal<br />
pressure range<br />
� Controlled valves combined with ball valves<br />
Pump Heads Dimensions<br />
A<br />
mm<br />
B<br />
mm<br />
C<br />
Depth<br />
mm<br />
Process<br />
Connection<br />
mm<br />
Pneumatic<br />
Connection<br />
mm<br />
Type 1T 78 38 45 1,6/3,2 4<br />
Type 2T 88 48 55 3,2 4<br />
Type 4T <strong>10</strong>9 69 55 3,2 4<br />
Type 6T 160 120 75 6 4<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Pump Heads<br />
Pneumatic Pressure<br />
Supply<br />
Process Pressure<br />
Suction Lift(mWs)<br />
Delivery Height<br />
(mWs)<br />
Process Temperature<br />
(if necessary, heating<br />
module **)<br />
Max. Displaced<br />
Volume<br />
Head Size 1<br />
Head Size 2<br />
Head Size 4<br />
Head Size 6<br />
Max. Delivery Volume<br />
Head Size 1<br />
Head Size 2<br />
Head Size 4<br />
Head Size 6<br />
*) in flooded con<br />
**) Heating with Thermostat<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Type T Type S<br />
Type P Type V<br />
3 – 6 bar 3 – 6 bar 3 – 6 bar 3 – 6 bar<br />
4<br />
50<br />
4<br />
50<br />
4<br />
50<br />
< <strong>10</strong>0 °C < <strong>10</strong>0 °C < <strong>10</strong>0 °C<br />
40 µl<br />
500 µl<br />
1800 µl<br />
8000 µl<br />
<strong>10</strong>0 ml/h<br />
1800 ml/h<br />
4000 ml/h<br />
8000 ml/h<br />
upon request<br />
500 µl<br />
1800 µl<br />
upon request<br />
upon request<br />
2000 ml/h<br />
8000 ml/h<br />
upon request<br />
upon request<br />
250 µl<br />
900 µl<br />
upon request<br />
upon request<br />
250 µl<br />
900 µl<br />
upon request<br />
Operating mode Piston dosing pump with pneumatic gear<br />
Max. flow rate see table<br />
Dosing in vacuum Models with pressure-keeping and closing valve<br />
Stroke Frequency 0 - 180/min<br />
Stroke length variable 0 - <strong>10</strong>0%<br />
Suction Lift 5 m Ws<br />
Materials in contact with media PTFE/carbon/ceramic<br />
Media connection Tube/Pipe ID/OD = 4/6 mm<br />
Ambient temperature -<strong>10</strong> ... 45°C<br />
Control Voltage 4 ... 20 mA<br />
Power supply 230 V AC<br />
Display Strokes/min, after calibration l/h either<br />
Media compatibility Almost all chemicals<br />
Protection Category IP 65<br />
Ex-version No<br />
Order Code Description<br />
IP-P-N1-PK-mc Pump head pneumatic diaphragm dosing pump<br />
IP-P-N1-PK-STRG-E Autonomous control, pneumatic diaphragm dosing pump<br />
IP-P-N1-PK-STRG-VI Valve terminaldiaphragm dosing pump for binary activation<br />
mc = Model Code: T,S,P,V<br />
ec=electrical connection:<br />
T Tuchel connector LAB-PI<br />
O Open ends for MSR-PI<br />
<strong>10</strong> *)<br />
50<br />
upon request<br />
upon request<br />
upon request<br />
900 µl<br />
1500 µl<br />
upon request<br />
upon request<br />
2000 ml/h<br />
6000 ml/h<br />
Order example:<br />
Pneumatic diaphragm dosing pump Type P,<br />
autonomous control:<br />
Order Code: IP-P-N1-PK-mc und IP-P-N1-PK-STRG-E<br />
Automatic<br />
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Magnetic dosing pump<br />
Magnetic dosing pumps are driven by an electric<br />
magnet. These generate a short and forceful dosing<br />
stroke. The dosing rate is controlled via the stroke<br />
frequency. The dosing stroke can additionally be<br />
adjusted manually.<br />
Magnetic membrane dosing pump<br />
Robust, calibratable membrane dosing pump with a<br />
magnetic drive for volumetric dosage or gravimetric<br />
dosage with a receiver on the balance in the control<br />
circuit.<br />
Technical data<br />
Operating mode Membrane dosing pump<br />
with magnetic gears<br />
Max. flow rate 1,1 l/h<br />
Max. discharge pressure 16 bar<br />
Dosing in vacuum Only with pressurised<br />
blocking valve<br />
Stroke frequency 0 - 180/min<br />
Stroke length variable 0 - <strong>10</strong>0%<br />
Suction height 5 m Ws<br />
Material in contact with PTFE/carbon/ceramic<br />
media<br />
Media connection Tube/pipe ID/OD = 4/6<br />
mm<br />
Ambient temperature -<strong>10</strong> to 45°C<br />
Activation 4 to 20 mA<br />
Power supply 230 V AC<br />
Display Strokes/min, after<br />
calibration also l/h<br />
Media compatibility Almost all chemicals<br />
Protection class IP 65<br />
Ex-version ---<br />
Order Code Description<br />
IP-P-M1-1<strong>10</strong>0M-<br />
PTFE/C/KER-SN4/6-ea<br />
ea=electrical connection:<br />
T Tuchel connector LAB-PI<br />
O Open ends for MSR-PI<br />
Order example:<br />
Magnetic membrane dosing pump, 1,1 l/h, 16 bar<br />
self-priming, Materials PTFE/Carbon/Ceramic, 180<br />
strokes/min, Activation 4 - 20mA, with 1 x 1,5m<br />
Cable for connection with a LAB-PI.<br />
Dosing Systems and Pumps<br />
Magnetic membrane dosing pump, 1.1 l/h, 16 bar self-priming, materials<br />
PTFE/carbon/ceramic, 180 strokes/min, Activation 4 - 20mA, with 1 x 1,5m cable for<br />
connection at a LAB- or MSR-PI (please indicate which one)<br />
Order Code: IP-P-M1-1<strong>10</strong>0-PTFE/C/KER-SN4/6-T<br />
On request deliverable:<br />
� PP,acrylic glass, stainless steel 1.4571<br />
� Dosing monitoring, self bleeding head for<br />
outgassing media<br />
� Other flowrate<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Magnetic piston dosing pump<br />
Robust, accurate piston dosing pump for liquids with<br />
a magnetic drive for precise, pressure-independent<br />
volumetric dosage. This pump is primarily suitable<br />
for precisely dosing small quantities.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Operating mode Piston dosing pump with magnetic gears<br />
Flow rate 0,06 ... 150 ml/h<br />
Max. discharge<br />
pressure<br />
40 bar<br />
Pressurised valve 2,5 bar<br />
Dosing in vacuum yes<br />
Stroke frequency 0 - 50/min<br />
Displace volume 1 - 50 μl, by micrometer button<br />
Stroke length variable 0 - <strong>10</strong>0%<br />
Suction Lift 6 m Ws<br />
Materials in contact with<br />
media<br />
PTFE/ceramic or stainless steel 1.4571/ceramic<br />
Media connection Capillaries da =1,75 mm or 1/16“ accords to 1,58 mm<br />
Ambient temperature 5 to 45°C<br />
Reproducibility better ± 0,5%<br />
Activation 4 - 20 mA<br />
Power supply 230 V AC<br />
Media compatibility Almost all chemicals<br />
Protection Category IP 65<br />
Ex-version Possible, on request<br />
Order Code Description<br />
IP-P-P1-0150M-PTFE/KER-SN17-ea Magnetic piston dosing pump, 0,06 - 150 ml/h, 40 bar self-priming, materials<br />
PTFE/Ceramic, 0 - 50 strokes/min, activation 4 - 20mA, with 1 x 1,5m cable for<br />
connection at a LAB- or MSR-PI (please indicate which one)<br />
IP-P-P1-0150M-VA/KER-SN16-ea Magnetic piston dosing pump, 0,06 - 150 ml/h, 40 bar self-priming, materials<br />
1.4571/ceramic, 0 - 50 strokes/min, activation 4 - 20mA, with 1 x 1,5m cable for<br />
connection at a LAB- or MSR-PI (please indicate which one)<br />
ma=media connection:<br />
SN17 Capillary screw connection OD =<br />
1,75mm, only in PTFE<br />
SN16 Capillary screw connection OD =<br />
1/16“ according 1,58mm, only in<br />
stainless steel<br />
ea=electrical connection:<br />
T Tuchel connector LAB-PI<br />
O Open ends for MSR-PI<br />
Order example:<br />
Magnetic piston dosing pump, 150 ml/h, 40 bar<br />
self-priming, materials stainless steel/ceramic, 0 -<br />
50 strokes/min, activation 4 - 20mA, with 1 x 1,5m<br />
cable for connection with a LAB-PI.<br />
Order Code: IP-P-K1-0150M-VA/KER-SN16-T<br />
available on request:<br />
� Ex-version<br />
� Greater discharge flows<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Calorimetry<br />
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Ex-Magnetic Membrane Dosing Pump<br />
Explosion-proof, robust membrane dosing pumps<br />
with a magnetic drive for volumetric dosage,<br />
gravimetric dosage with a receiver on a balance in a<br />
control circuit .<br />
The standard type, made of PTFE/carbon/ ceramic<br />
materials are particularly suitable for aqueous media<br />
with a certain electrical conductivity.<br />
When using flammable media we recommend the<br />
stainless steel model.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Operating mode Membrane dosing pump with magnetic gears<br />
Max. flow rate 1,0 l/h<br />
Max. discharge<br />
pressure<br />
16 bar<br />
Dosing in vacuum Only with pressurised blocking valve<br />
Stroke frequency 0 - 120/min<br />
Stroke length variable 0 - <strong>10</strong>0%<br />
Suction height 6 m Ws<br />
Materials in contact with<br />
media<br />
PTFE/carbon/ceramic<br />
Media connection Tube/Pipe6 x 4 mm<br />
Ambient temperature -<strong>10</strong> ... 45°C<br />
Activation 4 - 20 mA, input inherently safe „ia“<br />
Power supply 230 V AC<br />
Media compatibility Almost all chemicals<br />
Protection Category IP 65<br />
Ex-version EEx ia d IIC T6<br />
Order Code Description<br />
IP-P-M2-<strong>10</strong>00M-<br />
PTFE/C/KER-SN4/6-ea<br />
ma=media connection:<br />
SN4-6 Tube fitting I.D./OD 4/6mm<br />
ea=electrical connection:<br />
T Tuchel connector LAB-PI<br />
O Open ends for MSR-PI<br />
Ex-magnetic diaphragm dosing pump, 1,0 l/h, 16 bar self-priming, materials<br />
PTFE/carbon/ceramic, 120 strokes/min, activation 4 - 20mA, with 1 x 1,5m cable for<br />
connection at a LAB- or MSR-PI (please indicate which one)<br />
Order example:<br />
Ex-Magnetic membrane dosing pump, 1,0 l/h, 16 bar<br />
self-priming, materials PTFE/carbon/ceramic, 120<br />
strokes/min, activation 4 - 20mA, with 1 x 1,5m cable<br />
for connection at a LabManager.<br />
Order Code: IP-P-M2-<strong>10</strong>00M-PTFE/C/KER-SN4/6-T<br />
available on request:<br />
Materials:<br />
� PP,acrylic glass, stainless steel 1.4571<br />
� self-venting head for outgassing media<br />
� Model for higher viscosity<br />
� further discharge flows<br />
Notice: When using flammable media, use electrical<br />
grounding at stainless steel models and metal<br />
conductors, because of electrostatic discharge.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Dosing Systems and Pumps<br />
Precision Motor Membrane Dosing Pump<br />
Accurate membrane dosing pumps with positively<br />
controlled valves are used for precise dosing of<br />
gases and liquids. They can also dose small<br />
quantities of aggressive, abrasive, and viscous<br />
media. The inlets can be thermostatically heated and<br />
cooled. Stroke frequency and displaced volumes<br />
can be controlled separately.<br />
Due to the special construction (controlled cam<br />
valves, valve closing and opening during diaphragm<br />
standstill, through overlapping of the closing<br />
conditions no uncontrolled flow) this doser has an<br />
extremely high precision and repeat accuracy. It can<br />
convey into vacuum and convey out of vacuum.<br />
Through the forced drive of the valves, a secure<br />
valve function and a high impermeability is also<br />
achieved. This makes the reliable dosing of gases<br />
possible.<br />
Technical Data<br />
The dosing of gases should take place without<br />
pressure. Principally, the dosing with other pressure<br />
ratios is also possible. But the pressure difference<br />
range is limited due to the densification ratio. The<br />
flow rates must be calculated by calibration runs.<br />
Operating mode Motor diaphragm dosing pump with cam-controlled valves<br />
Flow rate 0 - 1800 ml/h<br />
Max. input compression 5 bar<br />
Max. pressure<br />
1 bar<br />
difference<br />
Dosing in vacuum Yes, till 0,001 mbar abs.<br />
Stroke frequency 0 - 60/min<br />
Displace volume <strong>10</strong> - 500 μl<br />
Suction Lift Self-priming, till 30 mbar abs. primary pressure<br />
Materials in contact with Post-compressed PTFE<br />
media<br />
Media connection PTFE, tube/plastic pipe I.D./OD = 4/6mm<br />
Media temperature up to <strong>10</strong>0 °C<br />
Activation serial connector RS232, 4-20 mA, 2-<strong>10</strong> V, single stroke control<br />
Power supply 230 V AC<br />
Power consumption 70 W<br />
Media compatibility Almost all chemicals<br />
Ex-version upon request<br />
Order Code Description<br />
IP-P-M3-1800M-PTFE-SN4/6 Precision motor diaphragm dosing pump, 36 - 1800 ml/h, 1 bar, materials PTFE, 0 - 60<br />
strokes/min, activation RS232<br />
ZK-P-TL02-BS-R2-I-01 RS232 Cable Sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />
ma=media connection:<br />
SN4-6 Tube fitting I.D./OD 4/6mm<br />
Order example:<br />
Precision motor diaphragm dosing pump, 36 - 1800<br />
ml/h, 1 bar, materials PTFE, 0 - 60 strokes/min,<br />
activation RS232, with 3m serial cable for<br />
connection at a LabBox or LabManager.<br />
Order Code: IP-P-M2-1800M-PTFE-SN4/6 and ZK-P-HZ01-<br />
BS-R2-I-01<br />
available on request:<br />
� Other flowrates<br />
� Heating and cooling of the pump head and feed<br />
lines<br />
� Vacuum applications<br />
Automatic<br />
Laboratory<br />
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Dosing Systems and Pumps<br />
High Pressure Double Piston Dosing Pump<br />
The high pressure double piston pump is made out<br />
of resistant materials and has a pulsations free flow.<br />
It is suited for dosing under high pressure in high<br />
pressure reactor systems and micro-reactor<br />
systems.<br />
Technical Data<br />
Operating mode Motor double piston pump for high pressure<br />
Max. flow rate 6 - 599,4 ml/h<br />
Max. discharge<br />
pressure<br />
500 bar<br />
Dosing in vacuum possible<br />
Materials in contact with<br />
media<br />
Stainless steel 1.4571, Aluminum oxide ceramic, carbon reinforced PTFE<br />
Media connection Capillary OD = 1/16“ equivalent 1,58mm<br />
Activation 0-<strong>10</strong> V DC, 2 x digital, RS232<br />
Power supply 230 V AC<br />
Media compatibility Almost all chemicals, besides chlorine-containing materials, hydrochloric acids<br />
Ex-version --<br />
Order Code Description<br />
IP-P-P3-0600M-VA/KER-<br />
SN16-ea<br />
ma=media connection:<br />
SN16 Screw connection for capillary 1/16“<br />
(1,58mm)<br />
ea=electrical connection:<br />
T Tuchel connector LAB-PI<br />
O Open ends for MSR-PI<br />
High pressure double piston dosing pump, 6 - 599,4 ml/h, 500 bar, materials 1.4571/ceramic,<br />
activation 0 - <strong>10</strong>V DC, 2 digital outputs with 3 x 1,5m cable for connection at a LAB- or MSR-<br />
PI, RS232<br />
Order example:<br />
High pressure double piston dosing pump, 6 - 599, 4<br />
ml/h, 500 bar, materials 1.4571/ceramic, activation 0<br />
- <strong>10</strong>V DC, 2 digital outputs with 3 x 1,5m cable with<br />
Tuchel plugs for connection to a LabManager<br />
Order Code : IP-P-K3-0600M-VA/KER-SN16-T<br />
available on request:<br />
� Increased discharge pressure up to 800 bar<br />
� Flow rates from <strong>10</strong> to <strong>10</strong>00ml/min<br />
� Other packing materials<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Eccentric screw pump<br />
Self-priming, pulsation free motor dosing pump for<br />
dosing and conveying for:<br />
� Media with different viscosities up to the pasty<br />
range<br />
� Suspensions, for instance sauces<br />
� abrasive suspensions, for instance soldering<br />
paste, polishing paste<br />
� Polymer, high viscous and crystal-containing preproducts,<br />
for example: lacquer, glue and melts<br />
� Viscous materials and granulated suspensions of<br />
the foods and pharmaceutical industry<br />
The pump is easy to disassemble and to clean.<br />
It is well suitable for speed regulated operations at a<br />
frequency converter.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Normally for connection at a LAB-PI an analogue<br />
output (LP-AAP8 or LP-AEAP), an passive digital<br />
output (LP-DAP8) for releasing and a digital input<br />
(LP-DEP8x) for the fault report are needed.<br />
Operating mode Eccentric screw pump with rotary current motor<br />
Flow rate 0 ... 24 l/h, depending on viscosity<br />
Max. discharge<br />
pressure<br />
12 bar<br />
Dosing in vacuum upon request<br />
Speed 0 ... <strong>10</strong>00 rpm, depending on viscosity<br />
Metered volume per rev. 0,40 ml<br />
Suction height Self-priming, media dependent<br />
Materials in contact with<br />
media<br />
Stainless steel 1.4571 hard chrome plated /perfluor rubber/PTFE<br />
Viscosity 1 ... 2.000.000 mPas<br />
Media connection Suction sided G ½“, pressure sided Rp ¼“, equivalent transitions available on<br />
request<br />
Media temperature up to 200 °C<br />
Metered accuracy Normally < ± 1%<br />
Control Frequency converter<br />
Power Input 0,25 kW<br />
Power supply 230 V AC<br />
Media compatibility Most chemicals beside chlorine-containing materials, hydrochloric acids<br />
Protection class IP 54<br />
Ex-version possible<br />
Order Code Description<br />
IP-P-E1-2700M-VA/FKM-ea Eccentric spiral pump with rotary current – asynchronous motor 0,25KW and frequency<br />
converter, 0-14 l/h, 12 bar, materials 1.4571 hard-chromium plated/fluorine rubber/PTFE, 0-<br />
<strong>10</strong>00 rpm, with cables to connect to a PI<br />
ea=electrical connection:<br />
T Tuchel connector LAB-PI<br />
O Open ends for MSR-PI<br />
Order example:<br />
Eccentric spiral pump with rotary current<br />
asynchronous motor 0,25KW und frequency<br />
converter, 0 - 24 l/h, 12 bar, materials 1.4571 hard<br />
chrome plated/fluorine rubber/PTFE, 0-<strong>10</strong>00 rpm,<br />
with cable for connection at a LabManager<br />
Order Code: IP-P-E1-2700M-VA/FKM-T<br />
available on request:<br />
� Other flowrate<br />
� Adjustable revolution gear<br />
Other materials:<br />
� Hastelloy<br />
� Pump head heating<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Calorimetry<br />
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Automation<br />
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Toothed Ring Pumps<br />
Toothed ring pumps are suitable for pulsation poor<br />
conveyance and dosing of particle-free and not<br />
lubricating fluids of lower to high viscosity at low flow<br />
rates. They distinguish themselves by small dead<br />
storage and high dynamics.<br />
Low pressure pump<br />
Low pressure pumps distinguish themselves by a<br />
small construction volume and a favorable price. It<br />
makes pulsation free and highly precise conveying<br />
of small quantities, also not lubricating media<br />
possible.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Applications:<br />
� Small quantity dosage<br />
� Analysis technology<br />
� Biotechnology<br />
� Medical technology<br />
Operating mode Directly coupled toothed ring pump<br />
Flow rate 0,15 - 9 ml/min and 0,3 - 18 ml/min continuous<br />
Pulsation 1.5% and 6%<br />
Revolution <strong>10</strong>0 to 6000 rpm, DC motor, revolution load independent<br />
Max. discharge 0 ... 3 bar<br />
pressure<br />
Viscosity 0.5 ... 20mPas<br />
Dosing in vacuum conditional<br />
Suction Lift Self-priming up to low lift, media dependent<br />
Materials in contact with Hard metal (tungsten carbide), nickel bronze, PTFE<br />
media<br />
Media connection Tube nipple OD = 2 mm<br />
Media temperature 5 ... 50°C<br />
Activation 0-<strong>10</strong>V, (4-20mA, RS232 opt.)<br />
Revolution feedback 0-<strong>10</strong>V, (4-20mA, RS232 opt.)<br />
Power supply / 230 V AC, 50 W<br />
Performance<br />
Media compatibility Watery solutions, solvents, low viscous oil and lubricants<br />
Ex-version ---<br />
Order Code Description<br />
IP-P-R1-9M-HM-SN2-ea Micro toothed ring pump with controllable DC motor, 0.15 - 9 ml/min, max. pressure<br />
difference 3 bar, materials: hard metal/nickel bronze/PTFE, with cable for connection at a<br />
<strong>HiTec</strong> <strong>Zang</strong>-PI<br />
IP-P-R1-18M-HM-SN2-ea Micro tooth ring pumps with controllable DC motor, 0.3 - 18 ml/min, max. pressure<br />
difference 3 bar, materials hard metal/nickel bronze/PTFE, with cable for connection at a<br />
<strong>HiTec</strong> <strong>Zang</strong>-PI<br />
ea=electrical connection:<br />
T Tuchel connector LAB-PI<br />
O Open ends for MSR-PI<br />
Order example:<br />
Toothed ring pumps with controllable DC motor, 0.15<br />
- 9 ml/min, Max. pressure difference 3 bar, materials<br />
hard metal/nickel bronze/PTFE, cable with Tuchel<br />
connectors for connection at a LabManager.<br />
Order Code: IP-P-R1-9M-HM-SN2-T<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
High Performance Pump<br />
This high performance toothed ring pump<br />
distinguishes itself by good suction behaviour, less<br />
dead volumes, less pulsation and a very large<br />
viscosity range, and high dynamics.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Operating mode Direct coupled toothed ring pump<br />
Pulsation 6%<br />
Revolution <strong>10</strong>0 up to 6000 R/min, DC motor, Revolution load independent<br />
Viscosity 0.5 ... 50.000 mPas<br />
Dosing in vacuum conditional<br />
Suction Lift Self-priming, media dependent<br />
Material in contact with hard metal (tungsten-carbide), stainless steel 316L, PTFE<br />
media<br />
Media connection Screw fitting for 6/4mm plastic tube<br />
Media temperature 0 bis 50 °C (-126 bis –140°C upon request)<br />
Activation 0-<strong>10</strong>V, (4-20mA, RS232 opt.)<br />
Revolution feedback 0-<strong>10</strong>V, (4-20mA, RS232 opt.)<br />
Power supply / Leistung 230V AC, 50W<br />
Media compatibility Media compatibility Watery solutions, solvent, low viscous oil and lubricants<br />
Ex-version --<br />
For a safe operation a particle filter is required.<br />
Order Code Description<br />
IP-P-R2-18M-HM-SF1/8-ea High performance pump 0,003 - 18 ml/min, Delta-p max. 30 bar, max. 50.000 mPas<br />
IP-P-R2-72M-HM-SF1/8-ea High performance pump 0,012 – 72 ml/min, Delta-p max. 50 bar, max. 50.000 mPas<br />
IP-P-R2-288M-HM-SF1/8-ea High performance pump 0,048 – 288 ml/min, Delta-p max. 40 bar, max. 1.000.000 mPas<br />
IP-P-R2-<strong>10</strong>152M-HM-SF1/8-ea High performance pump 0,192 – 1.152 ml/min, Delta-p max. 00 bar, max. 150.000 mPas<br />
ea=electrical connection:<br />
T Tuchel connector LAB-PI<br />
O Open ends for MSR-PI<br />
Order example:<br />
Toothed ring pump with controllable DC motor, 0,3 -<br />
18 ml/min, max. pressure difference 30 bar,<br />
materials hard metal/stainless steel/PTFE, cable<br />
with Tuchel connectors for connection at a<br />
LabManager.<br />
Order Code: IP-P-R2-18M-HM-SF1/8-T<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
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Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Components<br />
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Dosing Systems,<br />
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Centrifugal Pumps<br />
Centrifugal Pump for High Pressure<br />
This magnet coupled centrifugal pump without shaft<br />
seal is particularly suitable for recirculation of heat<br />
carriers up to 350°C. The conveying of chemicals<br />
with higher temperature is also possible within the<br />
range of stability. It is also possible to provide<br />
systems and control vales with high flow<br />
resistances. Due to the complete separation of the<br />
media and drive, this pump is also very robust at<br />
extreme application conditions.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Operating mode Small magnet coupled centrifugal pump<br />
Delivery Rate water 840 l/h at 3 bar<br />
Max. flow rate 1800 l/h<br />
Max. pressure difference 5 bar<br />
Revolution 2800 rpm<br />
max. System pressure 25 bar<br />
Suction Lift No, influent<br />
Materials in contact with Stainless steel 1.4408, 1.4571, 1.4581<br />
media<br />
Particularly in multi reactor and parallel reactor<br />
systems with a joint thermostat control in mixing<br />
operations (large temperature changing rates,<br />
emergency cooling at exothermically reactions) the<br />
thermostat installed in the pump is often not<br />
sufficient. In this case, our pump is an appropriate<br />
solution.<br />
Media connection Internal thread G ½“<br />
Media temperature Up to 350 °C heat transfer oil, aqueous media up to 200°C possible<br />
Activation Over switching sockets (LP-DA230V2) or (HP-B230V8A)<br />
Power supply 230V AC 1 Ph, 0,5 kW. 400V AC 3 Ph possible<br />
Media compatibility Many chemicals, no chlorine-containing materials and hydrochloric acids.<br />
Protection Category IP 54<br />
Ex-version Possible, upon request<br />
Order Code Description<br />
IP-B-K1-1800L-VA-GMG1/2-ep Centrifugal pump, 0,5 kW, 2800 rpm at 50 Hz, up to 1800 l/h max. pressure difference 5<br />
bar, system pressure max. 25 bar, material stainless steel<br />
ep=<strong>Main</strong>s Power connection:<br />
230V 230V AC 1 Ph<br />
400V 400V AC 3 Ph<br />
Accessories for electrical connection of the pump<br />
like switching sockets (HP-B230V8A), protection etc.<br />
upon request.<br />
Order example:<br />
Centrifugal pump with three-phase asynchronous<br />
motor 0,5 kW,230V AC, 2800 rpm at 50 Hz, up to<br />
1800 l/h Max. pressure difference 5 bar, system<br />
pressure max. 25 bar, material: stainless steel.<br />
Order Code: IP-B-K1-1800L-VA-GMG1/2-400V<br />
We can offer you a complete spectrum of similar<br />
pumps for similar applications. Please contact us!<br />
available on request:<br />
� Other rotor material: PEEK<br />
� Controllable model with frequency converter<br />
� Model complete with frequency converter and<br />
difference pressure measuring for difference<br />
pressure control<br />
� Model with IDM measuring orifice plate for mass<br />
flow control<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Centrifugal Pump for Chemicals<br />
Magnet coupled chemical centrifugal pump without<br />
shaft seal for conveying and recirculation of pure<br />
and aggressive chemicals like acids, bases and<br />
solvents....<br />
Typical applications:<br />
� Extraction<br />
� Distillation in pilot plant, mini plant<br />
� Recirculation of baths: galvanic industry, photo<br />
industry...<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Usually, a digital output (LP-DAP8...) is required for<br />
start and stop at a LAB-PI. In individual cases a<br />
revolution controller (e.g. pressure difference<br />
controller) can be useful. In this case, an analogue<br />
output (LP-AAP8UI or LP-AEAP8I) for activation of a<br />
frequency converter will be needed.<br />
If needed, please additionally order the frequency<br />
converter.<br />
Operating mode Small magnet coupled centrifugal pump for chemical engineering<br />
Delivery Rate Water: 3000 l/h at 0,4 bar<br />
Max. flow rate 3900 l/h<br />
Max. pressure<br />
0,78 bar (7,8m discharge height, water)<br />
difference<br />
Revolution 2800 rpm<br />
max. Density 1300 kg/m³<br />
Suction Lift No, influent<br />
Material in contact with CFRETFE (Carbon fiber PE/PTFE-compound), silica carbide, FKM<br />
media<br />
Media connection External screw thread 1“<br />
Media temperature Up to 80°C<br />
Activation Over switching sockets (LP-DA230V2) or (HP-B230V8A)<br />
Power supply / 230V AC 1 Ph, 170W. three-phase current possible.<br />
Performance<br />
Media compatibility Media compatibility. Most chemicals, acids and bases.<br />
Ex-version Possible, upon request. Please inquire when using not conductive, flammable<br />
liquids because of the static charge.<br />
Order Code Description<br />
IP-B-K2-3900L-ETFE/SIC Chemical centrifugal pump with alternating current motor 170W, 230V AC, up to 3900 l/h Max.<br />
pressure difference max. 0,78 bar, materials CFRETFE/SiC/FKM<br />
We can offer you a complete spectrum of similar<br />
pumps for further applications. Please inquire.<br />
available on request:<br />
� Other flowrates and pressure difference<br />
� Other materials: PP...<br />
Automatic<br />
Laboratory<br />
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296<br />
Reaction Proportioning Pumps<br />
Reaction proportioning pumps are especially suited<br />
for the production of nanoparticles and to test the<br />
reaction conditions for mixing or mass transfer tasks.<br />
The pumps dispose of peripheral wheel- typical<br />
pressure cells. In these, the liquid educt is<br />
compressed and flushed over the mixing rotor due to<br />
the generated turbulences. The subsequently<br />
generated circulation flows lead to especially<br />
homogenous and stable mixtures.<br />
Depending on the material, the mixers are<br />
chemically highly resistant and are able to handle<br />
system pressures up to 350 bar and temperatures of<br />
up to 450 °C.<br />
Reaction proportioning pumps are basically<br />
peripheral wheel pumps with several inlet nozzles<br />
for the fluid and gas feed.<br />
There is a separate inlet opening for each<br />
component in the diameter wall of the mixing<br />
chamber, the flow section of which is especially<br />
constructed according to the viscosity of the fluid,<br />
the projected mixing ratio or the expected reaction. A<br />
gaseous component can be fed into the mixing<br />
chamber between the inlet opening of the liquid<br />
component and the outlet/discharge opening of the<br />
mixture.<br />
Dosing Systems and Pumps<br />
Characteristics:<br />
� Robust and Safe<br />
� Simple Test Equipment<br />
� Safe test conditions, e.g. for phosgene<br />
transformation<br />
� Total volume is continuously regulable<br />
� Represents an alternative to stirred reactors or<br />
micro-mixers<br />
� Especially homogenous and stable mixtures due<br />
to intensive mixing<br />
In order to ensure a high chemical stability, the<br />
reaction mixers are constructed in Hasteloy, Tantal<br />
or silicon carbide for the part in contact with the<br />
products as well as with PTFE or Perfluorelastomer<br />
gaskets. Plastic linings with antistatic PTFE or PFA<br />
are also deployed. The drive of the mixer is magnetcoupled.<br />
In case of toxic or corrosive substances, it<br />
is possible to deploy double separating cans.<br />
The wear due to solid material content in the fluid,<br />
e.g. due to precipitation during a reaction, is<br />
countered with a suited selection of materials and<br />
design of the wheel, separating can and the shaft<br />
bearing. The separating can and the bearing, if<br />
necessary, can be flushed with a suited liquid.<br />
Depending on the respective reaction conditions, the<br />
chemical objectives, or the process-related basic<br />
conditions, special equipment is available for the<br />
reaction mixers.<br />
If exothermal o endothermal reactions are to be<br />
expected, the pumps can be equipped with heated<br />
or cooled pump heads. It is, for instance,<br />
subsequently possible to run a reaction isothermally<br />
or to prevent a melt from sulphuring. For this<br />
purpose, pump heads with a heating chamber or<br />
with a heatable separating can are available.<br />
When producing nanoparticles, the peripheral<br />
conveying system ensures fast mixing and a short<br />
holding time. As the nanoparticles are specifically<br />
produced in the reaction chamber, there is no<br />
increased risk of blockage or wear for the bearing or<br />
separating can.<br />
Due to the dosing pumps and the speed regulation,<br />
there is a high variance of possible test parameters.<br />
Order Code Description<br />
IP-B-REAKT1-4P Reaction Proportioning Pump, three inlets, one outlet, three phase motor<br />
IP-B-REAKT1-FU Frequency Converter for Reaction Proportioning Pump<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Dosing Systems and Pumps<br />
Multi-Channel Dosing Systems<br />
Flexible gravimetric dosing systems can be realised<br />
by combining the accordingly suited components.<br />
Here are just a few of the possible combinations:<br />
� Four-fold Dosing System with GraviDos<br />
LabBox1with GraviDos weighing card and 4<br />
magnetic valves or PFM-controlled pumps ,<br />
HiBuilder custom software for dosing profiles and<br />
simple records and protocoling.<br />
Options:<br />
Special cable for the connection of the dosing<br />
pumps to 4..20mA digital outputs (PWM), further<br />
RS232 interfaces for connection of dosing<br />
pumps.<br />
� Four-fold Dosing System with Laboratory<br />
Scales:<br />
LabBox1 with 4 RS232 interfaces for laboratory<br />
scales and 8 digital outputs for connection of the<br />
magnetic valves or PFM-controlled pumps,<br />
HiBuilder custom software for dosing profiles and<br />
simple records and protocoling.<br />
� Four-fold Dosing System with Notebook<br />
acting as Control Unit:<br />
Notebook, USB to RS232 Converter, four-fold<br />
DMS-Card RS232, 4 GraviDos modules, 4<br />
LabDos with RS232-Bus, HiBuilder custom<br />
software for dosing profiles and simple records<br />
and protocoling.<br />
� Mehrfachdosiersystem mit SyrDos<br />
Spritzendosierer<br />
Notebook, USB an RS232 Converter, LabBox1,<br />
2 SyrDos Systeme, DosiMaster Spezialsoftware<br />
für Dosierprofile und einfache Aufzeichnung u.<br />
Protokollierung.<br />
Options:<br />
Special cable for the connection of the dosing<br />
pumps to 4..20mA digital output (PWM), further<br />
RS232 interfaces for connection of LabDos and<br />
other dosing pumps.<br />
Custom Design, mobile 4-fold Dosing Station<br />
Kundenspezifisch gefertigte SyrDos-Dosierstationen<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
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298<br />
Vacuum pumps<br />
Membrane vacuum pump<br />
Dry running vacuum pump for neutral, highly<br />
aggressive and corrosives gases and vapours.<br />
Applications:<br />
� Evacuate in a raw vacuum range with or without<br />
cryo trap<br />
� Rotary evaporator<br />
� Evacuation of dehydrator<br />
� Substitute of water jet pumps<br />
� Discharge of process gases<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Operating mode Two phase membrane vacuum pump for the chemistry<br />
Suction capacity 1200 l/h<br />
Final vacuum 8 mbar abs.<br />
Media affecting PTFE/FFKM<br />
materials<br />
For the connection at a LAB-PI a digital output (LP-<br />
DAP8) and a switching sockets (HP-B230V8A) or a<br />
digital output 230V (LP-DA230V2) are needed.<br />
Media connection Tube nipple for vacuum tube I.D. = 6mm, OD = <strong>10</strong>mm<br />
Activation Over switching sockets (LP-DA230V2) or (HP-B230V8A)<br />
Power supply / Leistung 230V AC 1 Ph, 120W<br />
Current consumption 0,7A<br />
Media compatibility Almost all chemicals, gases and vapours<br />
Ex-version ---<br />
Order Code Description<br />
IP-B-V1-1200L-PTFE/FPM Chemical vacuum pump with alternating current motor 120W, 230V AC, 1200 l/h, final vacuum<br />
8 mbar, materials PTFE/FFKM<br />
On request deliverable:<br />
� Other flowrate<br />
� Final vacuum 2 ... <strong>10</strong>0 mbar<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Two phase rotary valve vacuum<br />
pump<br />
Two phase oil sealed rotary valve membrane pump<br />
for generating fine vacuum.<br />
Applications:<br />
� Evacuating of small up to middle reactor systems<br />
up to the higher fine vacuum range<br />
� Lyophilization / freeze drying<br />
� Vacuum distillation<br />
By condensing aggressive media a cryo trap shall<br />
be provided.<br />
For the connection at a LAB-PI a digital output (LP-<br />
DAP8) and a switching sockets (HP-B230V8A) or a<br />
digital output 230V (LP-DA230V2) are needed.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
Operating mode Two phase oil sealed rotary valve vacuum pump<br />
Suction capacity 5600 l/h<br />
End partial pressure or<br />
gas ballast<br />
4 x <strong>10</strong>-4 mbar abs.<br />
End total pressure or.<br />
Gas ballast<br />
2 x <strong>10</strong>-3 mbar abs.<br />
End partial pressure<br />
with gas ballast<br />
6 x <strong>10</strong>-3 mbar abs.<br />
Media connection Tube nipple for vacuum tube I.D. = 6mm or clamped flange DN <strong>10</strong><br />
Activation Over switching sockets (LP-DA230V2) or (HP-B230V8A)<br />
Power supply /<br />
Performance<br />
230V AC 1 Ph, 0,30kW<br />
Media compatibility Neutral gases, low quantities condensing and corroding vapors, apply cryo trap<br />
Ex-version ---<br />
Order Code Description<br />
IP-B-V2-5600L-SN6 Two phase rotary vacuum pump with alternating current motor 0,30kW, 230V AC, 5600 l/h,<br />
final vacuum 2 x <strong>10</strong>-3 mbar abs.<br />
On request deliverable:<br />
� Other flowrate<br />
� One-level version<br />
� Hybrid pump with better compatibility for<br />
aggressive vapors<br />
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Vacuum Pump Stand<br />
These laboratory vacuum systems are equipped<br />
with a controller. The control of the pressure is<br />
distinguished by a connection, respectively<br />
disconnection of the diaphragm pump. It is possible<br />
to suppress the connection of the pump motor a<br />
selective setting of the pressure rise rate or through<br />
an active Teach-Function. This means, that the<br />
system will only activate if a potential load is<br />
connected.<br />
Advantages<br />
� equipped with a vacuum controller, chemical<br />
resistant diaphragm pump with control<br />
� Vacuum control through revolution control<br />
� Consistent operational readiness<br />
� reduced operational costs<br />
� increased service life and longer maintenance<br />
intervals of the diaphragm pump<br />
� simple programming of the controller, directly<br />
or via PC<br />
� Storage of all program and measurement<br />
values possible<br />
Laboratory vacuum systems offer you an automatic<br />
cost-effective operation without additional charge.<br />
You do not need to supervise the operation of the<br />
pump. The integrated intelligent vacuum controller<br />
economically controls the revolutions of the pump. A<br />
suction-side separator ensures the protection of the<br />
vacuum pump by retaining particles and liquid<br />
droplets.<br />
Technical Data<br />
Dosing Systems and Pumps<br />
The pressure-side emission condenser ensures nonpolluting<br />
operation by regaining and collecting<br />
solvent remains.<br />
All components in contact with gas are made of top<br />
quality, chemically resistant materials. This even<br />
enables the evacuation of acids and solvent<br />
vapours. All glass parts are coated with a<br />
transparent shatter protection coating which<br />
preserves visibility of the processes. The coolers are<br />
insulated.<br />
Operating mode Chemical-resistant diaphragm pump, separator<br />
Suction capacity 2,2 / 4,9 / 9,1 m³/h<br />
Final Pressure or gas<br />
ballast<br />
< 2 mbar<br />
Media connection DN16KF-1/4 inch / DN16KF-1/4 inch / DN25KF-1/4 Zoll<br />
Activation RS232<br />
Power supply 230V AC<br />
Media compatibility Neutral gases, small quantities of condensing and corroding vapors<br />
Ex-version No<br />
For the connection to a LAB-PI, a RS232 cable is required.<br />
Order Code Description<br />
IP-B-VPS-mc Vacuum pump stand with chemical-resistant diaphragm pump and separator<br />
ZK-P-VB01-BS-R2-I-01 Rs232 cable for IP-B-VPS-mc<br />
mc=Model Code:<br />
Model Final Suction<br />
Code vacuum capacity<br />
2-2.2 < 2 mbar 2,2 m³/h<br />
2-4.0 < 2 mbar 4,9 m³/h<br />
2-9.1 < 2 mbar 9,1 m³/h<br />
Other delivery rates and final pressures are available on request.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Solid Matter Dosing System<br />
Dosing Systems and Pumps<br />
Load Lock Conveying System for Powders, Granulates, Crystalls....<br />
Fields of application<br />
The SoliDos solid matter<br />
dosing system is suitable<br />
for the dosing of powdery<br />
and granular solid matters.<br />
For the laboratory<br />
technician, the manual<br />
adding of solid educts at<br />
specific times, or the adjustment<br />
of the pH-value<br />
through solid matter addition<br />
are a time-consuming<br />
matter.<br />
With SoliDos You can<br />
now automate these operation<br />
steps. SoliDos is<br />
also suitable at best for<br />
the automatic seeding<br />
procedure of crystallization<br />
processes.<br />
Thanks to its especially<br />
slim design, SoliDos ideally<br />
fits into the reactor<br />
installation.<br />
� Dosing of solid matter<br />
� pH-adjustment with solid matter<br />
� Seeding of crystallization processes<br />
SoliDos can be run through a specific control device<br />
or directly through a PFM (pulse frequency module)<br />
modulated digital output of the LabManager.<br />
SoliDos can also be run through an optionally<br />
available, separate control device.<br />
The dosing rate can be adjusted via the rotation<br />
speed and the volume of the lock chamber.<br />
Optionally, a nitrogen flushing connection and a side<br />
refilling nozzle can be provided.<br />
SoliDos is built out of resistant materials. The<br />
standard model is made of borosilicate glass,<br />
stainless steel, and POM. Alternatively the material<br />
PTFE is available.<br />
Technical Data<br />
Diameter: approx. 70 mm<br />
Length: approx. 330 mm<br />
Connection: NS29/32<br />
Weight approx. 1300 g<br />
Dosage amount max. 200 ccm<br />
For assembly, the SoliDos is directly mounted on to<br />
a NS 29/32 standard grinding socket. The dosing<br />
matter, also during the running operation, can be<br />
refilled manually or automatically through the lateral<br />
refill-socket by a mounted storage container. A<br />
rinsing/flushing connection for inert gas is provided<br />
between the lock chamber and the socket.<br />
Advantages<br />
� Resistant to most chemicals<br />
� Suitable for powder and granular materialdosing<br />
� Large range for the dosing rate<br />
� Novel mechanics prevents fusing and dome<br />
formation<br />
� Minimum floor space required, very simple<br />
installation<br />
� Can be completely dismounted for cleaning<br />
� Combination with GraviDos gravimetric<br />
dosing is possible<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
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Versions<br />
Dosing Systems and Pumps<br />
Version (SoliDos2 - x ) -12 -25 -50 -<strong>10</strong>0 -200 -400<br />
Dosing rate approx. [ccm/min] 12 25 50 <strong>10</strong>0 200 400<br />
Dosed amount (per pulse) approx. [ccm] 0,12 0,25 0,50 1 2 4<br />
Max. dosing amount: 200 ccm, unlimited by refilling through the side nozzle<br />
Delivery Scope Doser with 1,5 m connection cable for active digital output of a LabManager<br />
or-box-PI, respectively Stand-Alone-control unit<br />
Order Code Description<br />
IL-SOLIDOS2-x Solid dosing basis device for LAB-PI<br />
IL-SOLIDOS2-x-ST Solid dosing basis device for stand-alone device<br />
IL-SOLIDOS2-SK-x SoliDos dosage valve<br />
IL-SOLIDOS2-HEIZ Electrical heating element for heating of the socket to prevent condensation<br />
IL-SOLIDOS2-KF Cold trap to prevent condensation in socket, NS29/32<br />
x=version according to table-12 to -400<br />
SoliDos Options<br />
An inert gas is pressed through the drive casing via<br />
the inerting connection on the drive casing in order<br />
to protect the drive from aggressive gases and to<br />
keep the dosing matter dry.<br />
Order Code Description<br />
IL-SOLIDOS1IN Inerting Connection for SoliDos solid doser on the drive<br />
Adapter for GraviDos for gravimetric dosing.<br />
Order Code Description<br />
IL-SOLIDOSADGD SoliDos/GraviDos adapter for gravimetric dosing<br />
Special designs and adapters for reactor nozzles are available on request.<br />
Screw Conveyor<br />
The SoliDos-s conveys powdery and granulate-like<br />
solids out of a storage container. A knocking mechanism<br />
prevents possible stowage in the screw.<br />
The SoliDos is available as vacuum and pressureresistant<br />
(-<strong>10</strong>00 up to 300 mbar) version.<br />
Special designs are available on request.<br />
The devices are available as client-specific custom<br />
designs in various sizes. The length of the screw, in<br />
Size 1, can be up to 500 mm.<br />
Technical Data<br />
Volumen 500 ml<br />
Dimensions without 300x300x400 mm<br />
Screw<br />
max. Length of Screw 500 mm<br />
Diameter of Screw <strong>10</strong> mm<br />
Weight approx. 2000 g<br />
Max. Dosing Rate 1 ccm/min<br />
Other dosing rates available on request.<br />
Required as PI-interfaces are:<br />
2 digital outputs<br />
Content of<br />
delivery<br />
Order Code Description<br />
IL-SOLIDOS-SF-V-1 SoliDos screw conveyor 500ml, volumetric<br />
Doser with 1,5 m connection<br />
cable for active digital outputs of a<br />
LabManager or -box-PI.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Gravimetric Solid Doser<br />
The SoliDos-s screw conveyor can be completed as<br />
gravimetric dosing unit. In the course of this, the<br />
weight reduction is registered by a precision<br />
scales.<br />
Dosing Systems and Pumps<br />
Technical Data<br />
Volume 500 ml<br />
Dimensions 300x300x400 mm<br />
max. Length of Screw: 500 mm<br />
Diameter of Screw: <strong>10</strong> mm<br />
Weight approx. 3500 g<br />
Max. Dosing Rate 1 ccm/min<br />
approx.<br />
Order Code Description<br />
IL-SoliDos-SF-G-1 Gravimetric solid doser with SoliDos screw conveyor Size 1<br />
Gravimetric frictional filler<br />
Max. Dosing Fault ±<strong>10</strong> mg<br />
Required as PI-interfaces are:<br />
2 digital outputs and one RS232 interface for the<br />
scales.<br />
Other dosing rates available on request.<br />
Delivery Scope Doser with 1,5 m connection<br />
cable for active digital outputs of a<br />
LabManager or -box-PI.<br />
The SoliDos-td frictional filler is suitable for precise<br />
dosing of solid matters.<br />
Technical data<br />
Volume 1500 ml<br />
Dimension Höhe: 600mm<br />
Durchmesser: 180 mm<br />
Materials metallfreie Ausführung in PP,<br />
optional Edelstahlausführung<br />
Weight (approx.) 4500 g<br />
Max. dosing rate 220 ccm/min<br />
Max. dosing rate 5 ccm/min<br />
As PI-interfaces are needed:<br />
Digital output (DAP8T) at the Lab/MSR-PI or<br />
GraviDos dosing control.<br />
Other dosing rates upon request.<br />
We also construct custom made systems.<br />
Delivery Scope Doser with 1,5 m connection<br />
cable for active digital outputs of a<br />
LabManager or -box-PI.<br />
Order Code Description<br />
IL-SOLIDOS-TD-V-1 frictional filler 1, volumetric<br />
IL-SOLIDOS-TD-G-1 frictional filler 1, gravimetric<br />
IL-SOLIDOS-TD-G SoliDos control device for standalone operation (combinable with IL-SOLIDOS-TD-G-1)<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
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Plant<br />
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Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 303<br />
Equipment and<br />
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304<br />
Dosing Systems and Pumps<br />
SoliDos - Control Device for Stand-Alone Operation<br />
The SoliDos control device offers the best<br />
functionality for the operation of the SoliDos solid<br />
doser.<br />
The device can both be controlled via the keypad<br />
and the serial (optional) or analogue interface. As it<br />
disposes of 5 dosing modes, this compact device<br />
can also be deployed everywhere without automation<br />
system.<br />
Dosing mode<br />
The SoliDos supports five Dosing modes, that can<br />
be selected from the parameter menu. The setpoint<br />
values can either be entered manually via the<br />
keypad or analogue determined via the analogue<br />
interface or serially via the RS232 interface.<br />
Delivery Scope Control device and manual.<br />
rp : pulse rate<br />
In the mode rp, a pulserate is predetermined. As<br />
soon as the SoliDos is started, it doses with the set<br />
pulse rate.e.g. 1 dosing stroke.<br />
rw: weight rate<br />
In the mode rw, a weight rate in g is predetermined.<br />
The weight rate operation mode requires a<br />
calibration run.<br />
sp: pulse sum<br />
In the mode sp, a pulse sum is predetermined. As<br />
soon as the SoliDos is started, it doses with the<br />
adjusted pulse rate until the adjusted pulse number<br />
is reached.<br />
sw: weight sum<br />
In the mode sw, a weight sum in g is predetermined.<br />
Exactly like in the mode rw, a calibration run of<br />
the appliance is necessary. As soon as the SoliDos<br />
is started, it commences dosing with the preset<br />
weight rate until the set weight sum is reached.<br />
p: single pulse<br />
In the mode p, the SoliDos can be driven in single<br />
step operation. If the UP button is actuated, a single<br />
dosing stroke will be triggered.<br />
Order Code Description<br />
IL-SOLIDOSST1 SoliDos control device for standalone operation (combinable with IL-SOLIDOS2-X-ST)<br />
IL-SOLIDOS-RS Option RS232 interface<br />
ZK-IT-HI01-BS-R2-I-03 RS232 Cable sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Here you will find:<br />
Liquid Handling and Autosampler<br />
� Sampling Systems and Pipetting Robots<br />
� AutoSam Sample Collector and Sample Dispensers<br />
� LiquiDos Peristaltic Pump<br />
� SyrDos Syringe Doser<br />
� LiquidMaster Control Software<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 305<br />
Equipment and<br />
Components<br />
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Dosing Systems,<br />
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Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
306<br />
Liquid Handling and Autosampler<br />
Sample Drawing Systems and Pipetting Robots<br />
24 Hour Reactor Sampling<br />
AutoSam is a fully automatic sample handling<br />
system with varied application possibilities. The<br />
robust construction enables deployment in rough<br />
plant environment.<br />
Applications<br />
� Bottling of Samples<br />
� Provision of reactants<br />
� Quenching, Mixing, Diluting<br />
� Derivatising with several Reactants<br />
� Liquid/Liquid Extraction<br />
� Creation of Backup samples<br />
In connection with an automation device or a control<br />
PC with the LiquiMaster control software, it is<br />
possible to realise any procedures time or processcontrolled<br />
according to specification of test period,<br />
time etc.<br />
Flexibility:<br />
� For Batch and Continuous Processes<br />
� For Upstream and Downstream Processes<br />
� Fully adequate Liquid Handling System<br />
� Optional interfaces for magnetic valves,<br />
pumps and switches for automation devices<br />
� Optional Stirring and Tempering Function<br />
� Interfaces for process automation<br />
Occurring sample waste and rinsing solutions are<br />
collected in a separate waste container. Due to the<br />
utilisation of inert materials and freely programmable<br />
rinsing cycles is eliminated and sterility ensured in<br />
bioprocesses.<br />
The AutoSam can be deployed as sample dispenser,<br />
respectively as a multicomponent collector, as the<br />
needle can be lowered right down to the bottle base.<br />
The precise control allows selective liquid/liquid<br />
phase separation through siphoning off to phase<br />
limit level.<br />
Optionally, it is possible to assemble digital inputs<br />
and outputs to switch external valves or pumps or to<br />
query monitors for filling level, pressure, etc. This<br />
enables easy realisation of liquid handling systems.<br />
Bottles with septa can be used as sample vessels.<br />
Vessels (e.g. 1.5 and 2ml-E-Caps) sealed with<br />
plastic covers or thin membranes are suited. By<br />
exchanging the sample tray, it is possible to switch<br />
to different vessel sizes.<br />
AutoSam300 as a fully integrated Process Component<br />
The AutoSam is connected to the <strong>HiTec</strong> <strong>Zang</strong><br />
LabManager or any other control system via serial<br />
interface. The control is easily conducted via HiText-<br />
Program or HiBatch basis operations. This ensures<br />
uncomplicated integration into the <strong>HiTec</strong> <strong>Zang</strong> LUIit<br />
and MultiLab systems.<br />
The module IL-AUTOSAM-SA enables an optional<br />
connection of an internal 2/3 way valve or an<br />
external pump a stand-alone sampling without<br />
external control device.<br />
The parameters sample amount, intervall and filling<br />
time can be set via the AutoSam control panel.<br />
For stand-alone application, the „LiquiMaster“<br />
Software is available, which enables table or scriptbased<br />
schedule control for AutoSam with two/threeway<br />
valve in combination with our peristaltic and<br />
syringe pumps.<br />
The sample tray can be exchanged by merely lifting<br />
the old one and fitting the new one.<br />
The devices are automatically able to identify an<br />
exchange of the sample tray and the number of<br />
sample positions of the sample tray.<br />
We advise to order the devices with at least two<br />
sample trays in order to prevent the necessity to<br />
individually change the sample bottles.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Liquid Handling and Autosampler<br />
As a component of the LabVision/LabManager<br />
laboratory automation, the control and protocoling<br />
can be arranged flexibly:<br />
� Process and time controlled methods<br />
� Control of the sample tray position and the<br />
injection needle<br />
� Simple integration into the plant and recipe<br />
control<br />
� Free programmable handling methods<br />
� Free programmable rinsing cycles and needle<br />
rinsing programs<br />
� Data exchange with existing LIMS-systems is<br />
possible<br />
� Protocoling in the laboratory journal and LIMS, as<br />
sample ticket etc.<br />
We also manufacture customer-specific sample tray<br />
for any sample vessels.<br />
Properties and Functions:<br />
� Materials in contact with media are made of<br />
PTFE or PVDF and glass<br />
� Vessel with septum seal are also reliably<br />
processed<br />
� Bottling under inert gas is possible<br />
� Exchangeable sample tray<br />
� Separate, big waste container<br />
� Control via serial RS232 interface, optional<br />
RS485 with ModBus or CanBus protocol, USB,<br />
Ethernet or SPS I/O<br />
� sample collector, fraction collector,<br />
multicomponent dispenser<br />
� Multicomponent mixer, phase separator<br />
� Fully automated sample handling<br />
� Options: magnetic stirrer, tempering system,<br />
tandem needle system<br />
Tandem Assembly Double Needle with Fixture<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
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Stirring and<br />
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308<br />
AutoSam300<br />
Liquid Handling and Autosampler<br />
The AutoSam 300 is the basic device of the<br />
AutoSam type series. It is chargeable with sample<br />
tray for sample bottles reaching from 2 ml to <strong>10</strong>0 ml<br />
and, if necessary, fits well into a cooling incubator.<br />
At the zero position of the sample tray, the needle is<br />
able to deliver into the waste. At the rear panel of the<br />
device, there is a tube connection used for<br />
connection to the waste container (waste).<br />
With the control panel, it is possible to<br />
� move to zero position<br />
� move to next position<br />
� move needle downwards<br />
� move needle upwards<br />
� open/close valve<br />
� control stirrer rpm<br />
� exchange sample tray manually.<br />
The LC-Display presents<br />
� position of the sample tray<br />
� position of the needle<br />
� etc.<br />
Technical Data<br />
Sample tray Speed Max. 5 Rev/min.<br />
Reproducibility x-pos. ±1 mm<br />
Traverse Path Needle Drive 80 mm<br />
Power Needle Drive <strong>10</strong> N<br />
Reproducibility y-pos. ±0,1 mm<br />
Dimensions WxDxH 31x41x46 cm<br />
Diameter Sample tray 30 cm<br />
Protection Category IP20<br />
Bottle Size ml Diameter mm Number of Septum Type<br />
Bottles possible<br />
2 12,0 49 (+1) yes AutoSam300-T-12-50<br />
5 a. 8 17,2 31 (+1) yes AutoSam300-T-17-32<br />
<strong>10</strong> a. 20 23,0 24 (+1) yes AutoSam300-T-23-25<br />
50 46,0 14 (+1) yes AutoSam300-T-46-15<br />
50 30,2 22 (+1) yes AutoSam300-T-30-23<br />
<strong>10</strong>0 56,0 <strong>10</strong> (+1) yes AutoSam300-T-56-11<br />
Note: (+1) means the usually assigned waste position.<br />
Order Code Description<br />
IL-AUTOSAM300 Automatic sampler for 300mm sample tray with sample bottles reaching from 2 to <strong>10</strong>0 ml<br />
IL-AUTOSAM300-T-12-50 AutoSam300 sample tray for 50 pieces 2ml, D = 12mm sample bottles<br />
IL-AUTOSAM300-T-17-32 AutoSam300 sample tray for 32 pieces 5 and 8 ml, D = 17,2mm sample bottles<br />
IL-AUTOSAM300-T-23-25 AutoSam300 sample tray for 25 pieces <strong>10</strong> and 20ml, D = 23 mm sample bottles<br />
IL-AUTOSAM300-T-46-15 AutoSam300 sample tray for 15 pieces 50ml, D = 46mm sample bottles<br />
IL-AUTOSAM300-T-30-23 AutoSam300 sample tray for 23 pieces 50ml, D = 30,2mm sample bottles<br />
IL-AUTOSAM300-T-56-11 AutoSam300 sample tray for 11 pieces <strong>10</strong>0ml, D = 56mm sample bottles<br />
You will find further auxiliary modules at the end of the chapter.<br />
Other bottle sizes are available upon request.<br />
The casings can be made of satin or polished high-grade steel.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
AutoSam360<br />
Liquid Handling and Autosampler<br />
The AutoSam 360 is chargeable with sample trays<br />
for sample bottles reaching from 2 ml to <strong>10</strong>0 ml.<br />
At the zero position of the sample tray, the needle is<br />
able to deliver into the waste. At the rear panel of the<br />
device, there is a tube connection leading for<br />
connection to the waste container..<br />
With the operator buttons, it is also possible to<br />
� move to zero position<br />
� move to next position<br />
� move needle downwards<br />
� move needle upwards<br />
� open/close valve<br />
� control stirrer rpm<br />
� exchange sample tray manually.<br />
The LC-Display presents<br />
� position of the sample tray<br />
� position of the needle<br />
� etc.<br />
Technical Data<br />
Sample tray Speed Max. 5 Rev/min.<br />
Reproducibility x-pos. ±1 mm<br />
Traverse Path Needle Drive 80 mm<br />
Power Needle Drive <strong>10</strong> N<br />
Reproducibility y-pos. ±0,1 mm<br />
Dimensions WxDxH 31x47x46 cm<br />
Diameter Sample tray 36 cm<br />
Protection Category IP20<br />
Bottle Size ml Diameter mm Number of Septum Type<br />
Bottles possible<br />
2 12,0 79 (+1) yes AutoSam360-T-12-80<br />
5 a. 8 17,2 48 (+1) yes AutoSam360-T-17-49<br />
<strong>10</strong> a. 20 23,0 40 (+1) yes AutoSam360-T-23-41<br />
50 46,0 17 (+1) yes AutoSam360-T-46-18<br />
<strong>10</strong>0 56,0 14 (+1) yes AutoSam360-T-56-15<br />
Note: (+1) means the usually assigned waste position.<br />
Order Code Description<br />
IL-AUTOSAM360 Automatic sampler for 360mm sample tray with sample bottles reaching from 2 to <strong>10</strong>0 ml<br />
IL-AUTOSAM360-T-12-80 AutoSam360 sample tray for 80 pieces 2ml, D = 12mm sample bottles<br />
IL-AUTOSAM360-T-17-49 AutoSam360 sample tray for 49 pieces 5 and 8 ml, D = 17.2mm sample bottles<br />
IL-AUTOSAM360-T-23-41 AutoSam360 sample tray for 41 pieces <strong>10</strong> and 20ml, D = 23mm sample bottles<br />
IL-AUTOSAM360-T-46-18 AutoSam360 sample tray for 18 pieces 50ml, D = 46mm sample bottles<br />
IL-AUTOSAM360-T-56-15 AutoSam360 sample tray for 15 pieces <strong>10</strong>0ml, D = 56mm sample bottles<br />
You will find further auxiliary modules at the end of the chapter.<br />
Other bottle sizes are available upon request.<br />
The casings can be made of satin or polished high-grade steel.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 309<br />
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Stirring and<br />
Dispersing<br />
Services
3<strong>10</strong><br />
AutoSam495<br />
Liquid Handling and Autosampler<br />
The device is chargeable with 495 mm sample trays<br />
for sample bottles reaching from 2 ml to <strong>10</strong>0 ml.<br />
At the zero position of the sample tray, the needle is<br />
able to deliver into the waste. At the rear panel of the<br />
device, there is a tube connection leading for<br />
connection to the waste container (waste).<br />
With the operator buttons, it is also possible to<br />
� move to zero position<br />
� move to next position<br />
� move needle downwards<br />
� move needle upwards<br />
� open/close valve<br />
� control stirrer rpm<br />
� exchange sample tray manually.<br />
The LC-Display presents<br />
� Position of the Sample tray<br />
� Position of the Needle<br />
� etc.<br />
Technical Data<br />
Sample tray Speed Max. 5 Rev/min.<br />
Reproducibility x-pos. ±1 mm<br />
Traverse Path Needle Drive 80 mm<br />
Power Needle Drive <strong>10</strong> N<br />
Reproducibility y-pos. ±0,1 mm<br />
Dimensions WxDxH 31x57x40 cm<br />
Diameter Sample tray 49,5 cm<br />
Protection Category IP20<br />
Bottle Size ml Diameter mm Number of Septum Type<br />
Bottles possible<br />
5 and 8 17,2 59 (+1) yes AutoSam495-T-17-60<br />
12 and 15 19,0 59 (+1) yes AutoSam495-T-19-60<br />
<strong>10</strong> 23,0 49 (+1) yes AutoSam495-T-23-50<br />
25 28,0 39 (+1) yes AutoSam495-T-28-40<br />
2 12,0 2x 49 (+1) yes AutoSam495-T-12-<strong>10</strong>0<br />
5 15,2 2x 49 (+1) yes AutoSam495-T-15-<strong>10</strong>0<br />
Order Code Description<br />
IL-AUTOSAM495 Automatic sampler for 495mm sample tray with sample bottles reaching from 2 to <strong>10</strong>0 ml<br />
IL-AUTOSAM495-T-17-60 AutoSam495 sample tray for 60 pieces 5 and 8 ml, D = 17.2mm sample bottles<br />
IL-AUTOSAM495-T-19-60 AutoSam495 sample tray for 60 pieces 12 and 15ml, D = 19mm sample bottles<br />
IL-AUTOSAM495-T-23-50 AutoSam495 sample tray for 50 pieces <strong>10</strong>ml, D = 23mm sample bottles<br />
IL-AUTOSAM495-T-28-40 AutoSam495 sample tray for 40 pieces 25ml, D = 28mm sample bottles<br />
IL-AUTOSAM495-T-12-<strong>10</strong>0 AutoSam495 Tandem sample tray for 2x50 pieces 2ml, D = 12mm sample bottles<br />
IL-AUTOSAM495-T-15-<strong>10</strong>0 AutoSam495 Tandem sample tray for 2x50 pieces 5ml, D = 15.2 mm sample bottles<br />
Other bottle sizes are available upon request.<br />
You will find accessories and further options under Auxiliary Components for Liquid Handling<br />
The casings can be made of satin or polished high-grade steel.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
AutoSam200<br />
Liquid Handling and Autosampler<br />
The AutoSam 200 is constructed very compact and<br />
is particularly suited for application within<br />
biotechnology. The sample tray can accommodate<br />
up to 24 standard 1.5 ml or 2.0 ml sample vessels.<br />
With the control panel, it is possible to<br />
� move to zero position<br />
� move to next position<br />
� move needle downwards<br />
� move needle upwards<br />
� open/close valve<br />
� control stirrer rpm<br />
� exchange sample tray manually.<br />
The LC-Display presents<br />
� Position of the Sample tray<br />
� Position of the Needle<br />
� etc.<br />
Technical Data<br />
Sample tray Speed Max. 5 Rev/min.<br />
Reproducibility x-pos. ±1 mm<br />
Traverse Path Needle Drive 80 mm<br />
Power Needle Drive <strong>10</strong> N<br />
Reproducibility y-pos. ±0.1 mm<br />
Dimensions WxDxH 20x25x46 cm<br />
Diameter Sample tray 16 cm<br />
Protection Category IP20<br />
Bottle Size<br />
ml<br />
Number of<br />
Samples<br />
Septum possible<br />
1.5 (E-caps) 24 yes<br />
2 (E-caps) 24 yes<br />
Order Code Description<br />
IL-AUTOSAM200 Automatic Sampler for 200mm sample tray<br />
IL-AUTOSAM200-T-11-32 Automatic Sampler for 32 pieces 1.5 or 2 ml D = 11mm sample bottles and E-caps<br />
Other bottle sizes are available upon request.<br />
You will find accessories and further options under Auxiliary Components for Liquid Handling<br />
The casings can be made of satin or polished high-grade steel.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 311<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
312<br />
Accessories, Options<br />
2/3-Way Valve<br />
Liquid Handling and Autosampler<br />
This 2/3 way valve for AutoSam sample collectors is<br />
mounted on the needle sliding carriage.<br />
The needle is directly attached at the valve fitting so<br />
that there is no tube between needle and valve. This<br />
leads to minimum dead volume and accordingly<br />
minimal flushing losses.<br />
For activation, the valve requires one of the three<br />
possible digital switching outputs.<br />
Material in contact with media: PTFE. Other<br />
materials are available upon request.<br />
Tube diameter 3 to 3.2 mm.<br />
Order Code Description<br />
IL-AUTOSAM-MB-2-3-P 2/3- way valve with needle holder wetted parts made of PTFE, steam-sterilisable<br />
IL-AUTOSAM-MB-2-3-K 2/3- way valve with needle holder wetted parts made of KEL-F steam-sterilisable<br />
IL-AUTOSAM-DA24 Digital switching output, 24V, 0.5 A<br />
Other bottle materials are available upon request.<br />
Multi-way valves can be found under Equipment and Components, Multi-way valves.<br />
Magnetic Stirrer Drive<br />
Beneath the needle position, a magnetic stirrer drive can be integrated in order to be able to drive magnetic<br />
stir bars in the sample bottles without contact.<br />
Order Code Description<br />
IL-AUTOSAM-R Magnetic stirrer drive for AutoSam<br />
IL-AUTOSAM-RF-d-l Magnetic stir bars for sample bottles, Teflon outer cover, 1VPE=<strong>10</strong> pieces<br />
d-l = Dimensions of the magnetic stir bar<br />
d-l: 3-6 6-<strong>10</strong> 6-15<br />
Diameter/mm 3 6 6<br />
Length/mm 6 <strong>10</strong> 15<br />
Tandem Equipment<br />
At devices and trays with tandem equipment there<br />
are always two sample bottles at every position<br />
which can be separately filled, respectively emptied.<br />
Out of the first vessel, e.g. an reactant can be<br />
provided whilst a product sample is filled into the<br />
second vessel.<br />
The needles always move in parallel.<br />
Order Code Description<br />
IL-AUTOSAM-TAN Tandem Equipment, Double Bottle Line<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Contact Guard<br />
Liquid Handling and Autosampler<br />
The contact guard prevents unintentional contact<br />
with the needle point.<br />
It is made of transparent Plexiglas and does not<br />
influence vision.<br />
Order Code Description<br />
IL-AUTOSAM-BSCHU Contact guard for needle<br />
Cooling Incubator<br />
The devices of the type series AutoSam200, 300,<br />
and 360 fit into the cooling incubator. The required<br />
electrical and fluidic connections are passed<br />
outwards through the rear panel. The cooling<br />
incubator is assembled ready for connection for<br />
AutoSam sample collector.<br />
� Glass Door<br />
� High-Grade Steel Casing<br />
� Interior Lighting<br />
� Ready to install connections for AutoSam devices<br />
Please note: Not all devices fit into the cooling<br />
incubator. In case of the AutoSam360, the plugs on<br />
the side panels and the waste connection must be<br />
relocated into the base tray.<br />
Technical Data<br />
Temperature Range 0 to +15 °C<br />
Interior Dimensions W x H x D 52 x 70 x 44 cm<br />
Exterior Dimensions W x H x D 60 x 85 x 60 cm<br />
Interior Material Plastic (silver), grids are zinc-trayd<br />
Order Code Description<br />
IL-AUTOSAM-KL Cooling Incubator for AutoSam Sample Collector<br />
Consumable Material<br />
Order Code Description<br />
IL-AUTOSAM-EN-6-x Needles for AutoSam, inside diam.= 0.6mm, outside diam.= 1.0mm 1VPE = 6 pieces<br />
IL-AUTOSAM-DN-6-x-x AutoSam double needle for venting and gassing function 1VPE = 6 pieces<br />
x = Needle length. The standard length for single needles is 50mm (x = 50). In case of double needles, the<br />
transport needle is 50mm, the venting needle is 25mm long (x-x = 50-25). Please request for other lengths.<br />
Custom designs are possible. Other inside and outside diameters on request.<br />
Automatic<br />
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Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
314<br />
Stand-alone use<br />
Liquid Handling and Autosampler<br />
The module IL-AUTOSAM-SA enables an optional<br />
connection of an internal 2/3 way valve or an<br />
external pump a stand-alone sampling without<br />
external control device.<br />
Order Code Description<br />
IL-AutoSam-SA AutoSam module for stand-alone sample taking<br />
Miscellaneous Options<br />
The parameters sample amount, intervall and filling<br />
time can be set via the AutoSam control panel.<br />
Order Code Description<br />
IL-AUTOSAM-SA AutoSam module for stand-alone sample taking<br />
IL-AUTOSAM-SPPS SPS Interface for AutoSam, control via 4 binary signals<br />
IL-AUTOSAM-DA24 Digital switching output, 24V, 0.5 A (maximum number 3 pieces)<br />
IL-AUTOSAM-FEACON Feature Connector 2 inputs 5-24V, 2 inputs 5V with internal Pull-up resistor , 5V<strong>10</strong>0mA<br />
IL-AUTOSAM-RS485 Bus-compatible RS485-Interface for AutoSam<br />
IL-AUTOSAM-TVERL Extension of the tower, e.g. in case bottles are higher than 70mm<br />
IL-AUTOSAM-B-DN Connecting element for double needle<br />
IL-AUTOSAM-WASBO Passing of the waste connection into the base tray<br />
IL-AUTOSAM-STLI Relocation of the plugs to the left casing side<br />
IL-AUTOSAM-STRE Relocation of the plugs to the right casing side<br />
IL-AUTOSAM-POLI Casing made of polished high-grade steel<br />
Further Options are available upon request. The devices are also available in the OEM version.<br />
Additional Components for Liquid Handling<br />
Liquid Handling applications are laborious and timeconsuming,<br />
if conducted manually. With the<br />
AutoSam liquid handlers, it is possible to realise<br />
liquid handling processes efficiently and precisely<br />
and consequently significantly reduce the amount of<br />
work.<br />
AutoSam Liquid handlers are flexibly deployable<br />
and, next to the precise and fast bottling of samples,<br />
enable applications such as:<br />
� Dispensing<br />
� Multiple Dispensing<br />
� Diluting and<br />
� Pipetting.<br />
Due to the possibility to control the processes with<br />
HiText, it is also possible to realise complex systems<br />
with integrated sensor systems and integration into<br />
plant automation etc. A liquid handling system<br />
consists of an AutoSam, an electrical pump unit, a<br />
LabBox/manager system, and further optional<br />
peripheral equipment. As pumps, the LiquiDos and<br />
LabDos peristaltic pumps or the SyrDos syringe<br />
pump with 2/3 way valve are particularly suited.<br />
Single and double needles with inerting and venting<br />
connections are available as feeding needles.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
LiquiDos Peristaltic Pump<br />
Liquid Handling and Autosampler<br />
Pump/valve unit for liquid handling applications, in<br />
particular within the biotechnological sector.<br />
The LiquiDos pump can be applied to realise sterile<br />
systems (tubes are auto clavable).<br />
Technical Data<br />
Tube Diameter interior 0.25 to 2.06 mm<br />
Wall Thickness 0.85 mm<br />
Maximum Delivery Rate 20 ml/min<br />
Maximum Delivery Pressure 2 (1.5 at Di = 2mm) bar<br />
Control RS232 Interface V24<br />
LiquiDos Precision Dosing Pump with integrated 2/3-way Valve<br />
(tube squeeze valve)<br />
Order Code Description<br />
IL-LIQUIDOS1 Pump unit with 2/3 way valve for Liquid-Handling with AutoSam, Control: RS232, with 3 m<br />
serial cable for connection to LAB- or MSR-PI<br />
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Stirring and<br />
Dispersing<br />
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316<br />
Liquid Handling and Autosampler<br />
LiquiMaster Control Software<br />
The LiquiMaster Software is intended for the<br />
realisation of stand-alone liquid handling<br />
applications with AutoSam devices.<br />
With the LiquidMaster, it is possible to realise<br />
spreadsheet or script-based schedule control for<br />
AutoSam with 2/3 -way valve in combination with<br />
our LabDos and LiquiDos peristaltic pumps and the<br />
SyrDos syringe pumps.<br />
LiquiMaster can control the sampling optionally by<br />
the integrated 2/3 way valve or/and with a LabDos<br />
peristaltic pump.<br />
Timings for valves and pumps, the pumpheads<br />
rotational speed and delivery volume as well as the<br />
cleaing time/volume can be parameterised.<br />
Sampling times will be managed be the timetable<br />
element.<br />
The programm creates a protocol of all executed<br />
sampling.<br />
With the ight version (SL-LIQUIML) an AutoSam can<br />
be used for standard samplings.<br />
The LiquiMaster full version uses the additional<br />
freely programmable HiText syntax, with which<br />
additional valves and pumps can be controlled and<br />
sensors can be integrated.<br />
The optional AutoSam feature.connector (IL-<br />
AUTOSAM-FEACON) enables the connection of two<br />
additional valves and two binary sensors at the<br />
AutoSam. With the RS232 interface additional<br />
sensors and devices can be integrated.<br />
The possibilities<br />
� Control of the position of the sample tray and the<br />
injection needle<br />
� Control of the 2/3-way valve and one pump<br />
� Free programmable rinsing cycles and needle<br />
rinsing programs<br />
� Protocoling as sample tickets etc.<br />
� Data exchange with existing LIMS systems<br />
The software is based on HiBuilder and can be<br />
extended with much ease for instance to<br />
send/receive data to/from a LIMS.<br />
It is a Microsoft Windows based software that runs<br />
on a LabCommander - Mini-Terminal.<br />
LabCommander - Mini-Terminal<br />
The LabCommander mini-terminal enables to space<br />
saving realisation of dosing-, dispering and mixing<br />
stations on the laboratory bench.<br />
Order Code Description<br />
SL-LIQUIM LiquidMaster Software for spreadsheet supported and freely programmable liquid handling<br />
SL-LIQUIML LiquiMaster Software light, for spreadsheet supported liquid handling<br />
CG-LABCOMMANDER LabCommander Mini-terminal for laboratory devices<br />
<strong>HiTec</strong> <strong>Zang</strong> also establishes ready-to-use sampling and liquid handling systems according to your<br />
specifications!<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Type Series AutoSam xl<br />
Liquid Handling and Autosampler<br />
The type series AutoSam xl is suited for the bottling<br />
of the total reactor content into containers up to 2<br />
litres. The permanently mounted high-grade steel<br />
nozzle moves to a waste position when in wait state,<br />
so that dripping rests can be directly disposed and<br />
can not cause spoilage.<br />
Bottle Size ml Number Septum Type<br />
of Bottles possible<br />
2000 8 yes AutoSam2000-8<br />
<strong>10</strong>00 12 yes AutoSam<strong>10</strong>00-12<br />
500 14 yes AutoSam500-14<br />
Technical Data<br />
Sample tray Speed max. 6 Rev/min<br />
Reproducibility x-pos. ±3 mm<br />
Traverse path needle drive approx. 80 mm<br />
Power Needle Drive approx. <strong>10</strong>0 N<br />
Reproducibility y-pos. ±3 mm<br />
Dimensions WxDxH 70x90x80 cm<br />
Order Code Description<br />
IL-AUTOSAM-XL-2000-8 Automatic Sampler for 8 x 2000ml sample bottles<br />
IL-AUTOSAM-XL-<strong>10</strong>00-12 Automatic Sampler for 12 x <strong>10</strong>00ml sample bottles<br />
IL-AUTOSAM-XL-500-14 Automatic Sampler for 14 x 500ml sample bottles<br />
Other bottles are available upon request.<br />
You can find accessories under Additional Components for Liquid Handling.<br />
XY-Pipetting Robots<br />
This pipetting robot is suited for „Liquid Handling“ of<br />
a greater number of samples. The control is easily<br />
conducted via HiText.<br />
Samples can be filled in containers, substances can<br />
be dosed out of containers, and substances can be<br />
filled from one container into another container.<br />
Optionally, sensors, e.g. pH sensors, can be moved<br />
from container to container and submerged for<br />
measuring.<br />
� For filling, sampling and pipetting<br />
� Container height up to 200 mm<br />
� RS232 Interface for <strong>HiTec</strong> UI<br />
Product Description Pipetting robot with serial interface for connection to the UI (workstation). Is<br />
assigned to one serial interface of the UI.<br />
Delivery Scope Pipetting robot with PI driver, cable, and manual.<br />
Order-Code Description<br />
IL-PIPET1 Pipetting Robot with serial interface, with cable and PI driver<br />
As pumps, the LiquiDos and SyrDos pumps are particularly suited.<br />
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318<br />
Liquid Handling and Autosampler<br />
SciLab Laboratory Robot<br />
<strong>HiTec</strong> <strong>Zang</strong> manufactures the SciLab Laboratory<br />
Robot exactly to the specifications of your special<br />
application. As the devices are smoothly integrated<br />
into the <strong>HiTec</strong> <strong>Zang</strong> Automation Environment, the<br />
coupling with online analytics is possible. Therefore,<br />
the prerequisite for the realisation of automated<br />
intelligent experiments is established.<br />
Features and Functions<br />
� Flexible Liquid Handling Platform<br />
� Optional sterilisable (24h at 90°C)<br />
� Integratable additional Sensor 'Technology<br />
� Integratable additional Actuators<br />
� Simple Integration in Up and Downstream<br />
Applications<br />
Typical Applications<br />
� Up Stream Processing<br />
� Down Stream Processing<br />
� Screening<br />
� Liquid Handling<br />
� Formulations<br />
� Cell Cultures in Microtitration Plates<br />
Example 1: Robot for Cell Culture<br />
Features and Functions<br />
� Sterilisable(24h at 90°C)<br />
� Compact Construction, Incubator Operation<br />
� Detection of Liquid Surfaces<br />
� Simultaneous Handling also of Microtitration<br />
Plates of different Formats<br />
Example 2: Robot for Formulation<br />
Special Features<br />
Product Description XYZ-Pipetting Robot with serial Interface<br />
Delivery Scope Robot with Cable and Manual<br />
� Blending out of up to 12 Components<br />
� Individual Stirring Functions for all Positions<br />
� Integrated gravimetric liquefied Material Dosing<br />
Order Code Description<br />
IL-SCIBOT-x Customer-specific XYZ-Robot<br />
IL-SCIBOTBIB Software Library for HiText and HiBuilder for Liquid Handling and Pipetting Tasks<br />
x: Specification according to functional requirements.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Here you will find:<br />
� ViscoPakt ® Torque Measuring Stirrer Drive<br />
Stirring and Dispersing<br />
� ViscoTrol Control Module for Three Phase Stirrer Drive<br />
� Stirring Accessories (Stirring Blades, Lead-Throughs, Magnetic Couplings....)<br />
� Drives and Tools for Dispersing and Homogenisation<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
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Automation<br />
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Stirring and<br />
Dispersing<br />
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320<br />
Stirring and Dispersing<br />
Measuring Stirrer ViscoPakt ®<br />
The Visco-Pakt measuring stirrer is a strong stirring<br />
an torque measuring system with speed regulation<br />
and state-of-the-art torque measurement sensitivity.<br />
Fields of Application<br />
� System stirrer for automatic laboratory reactor<br />
� Identification of reaction phases<br />
� Detection of stirrer dissipation in the reaction<br />
calorimeter<br />
� Measurement of rheological material properties<br />
� Scale-up experiments<br />
� Process monitoring<br />
The drive unit requires only a fraction of the space<br />
needed by usual measuring stirrers, allowing more<br />
valuable space for the reactor head. Due to its<br />
compact construction, it also fits into a small<br />
apparatus, e.g. a 250 mL reactor system. The small<br />
dimensions of the drive were achieved by separating<br />
the stirrer from its control unit. The separate<br />
controller has a keypad and an LC display, which<br />
shows the torque and rotational speed.<br />
The measured torque is automatically corrected<br />
using the speed dependent “zero torque”.<br />
In many applications, ViscoPakt delivers important<br />
additional information. For polymerization and polycondensation,<br />
the initiation or completion of a<br />
reaction, which cause a change in the viscosity, can<br />
be read off and identified via the torque.<br />
The power dissipated from stirring, which is of<br />
interest for reaction calorimetry, can be determined<br />
from the torque and speed of rotation.<br />
As the design has no gearing, an extraordinarily<br />
large range of torque can be continuously achieved<br />
with no switching.<br />
Glass stirrers are protected from breaking by softstart<br />
and torque limiters.<br />
Characteristics and Functions<br />
� Powerful and compact<br />
� High measuring precision<br />
� High measuring sensitivity<br />
� Robust measurement technique<br />
� Measurement of rotational speed and torque<br />
� Wide and continuous range of rotational<br />
speeds<br />
� Smooth start-up, adjustable gradient<br />
� Automatic correction of the zero torque<br />
� Adjustable soft-start ramp<br />
� Adjustable rotational speed and torque<br />
limitation<br />
� Quick catch chuck<br />
� Low noise operation<br />
ViscoPakt rheo was developed for applications for<br />
which the exact torque, viscosity, or the dissipated<br />
energy and a precise keeping of the rotational speed<br />
are needed.<br />
The measurement sensitivity is impressive.<br />
Viscosity variations in the order of the viscosity of<br />
water are still resolved.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
ViscoPakt ®<br />
The standard design is equipped with a simple<br />
torque output which reflects the viscosity's trends.<br />
Variations of the rotational speeds due to load<br />
fluctuations are electronically compensated.<br />
Technical data<br />
Stirring and Dispersing<br />
ViscoPakt model - 27 - 57 - 1<strong>10</strong> Unit<br />
Maximum torque 27 57 1<strong>10</strong> Ncm<br />
Resolution 0,07 0,1 0,2 Ncm<br />
Reproducibility 1,5 3 5 Ncm<br />
Minimum speed 150 150 150 rpm<br />
Maximum speed 2200 2000 2000 rpm<br />
Speed uncertainty 2 1,5 1,5 %<br />
Chuck size 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> mm<br />
Type of protection<br />
controlling device<br />
20 20 20 IP<br />
Type of protection<br />
drive<br />
51 51 51 IP<br />
Approx. Weight 2 3 4 kg<br />
Motor Diameter 55 70 83 mm<br />
Length across axis<br />
(approx.)<br />
2<strong>10</strong> 230 270 mm<br />
Extension<br />
diameter/length<br />
16 / 220 16 / 220 16 / 220 mm<br />
Max. viscosity <strong>10</strong>.000 40.000 70.000 mPas<br />
Max. Mixing quantity<br />
(H2O)**<br />
15 30 50 Liter<br />
* Control Unit /Drive<br />
** Reference values for propeller stirrer in H2O<br />
Interfaces<br />
Analogue:<br />
Required rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />
Actual rotational speed (= required value or 0) 0 - <strong>10</strong> V, 0/4-20mA<br />
Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />
The setpoint rotational speed can be pre-set via an<br />
analogue input or the serial interface. The torque<br />
and the setpoint rotational speed are issued via the<br />
analogue outputs and the serial interface.<br />
RS232:<br />
Send: Setpoint rotational speed<br />
Received: Setpoint rotational speed, actual torque value<br />
Delivery Scope Measuring-stirrer drive and control unit with 2.3 m cable<br />
Order Code Description Specifications<br />
IR-VIPA27 ViscoPakt-27 27 Ncm<br />
IR-VIPA57 ViscoPakt-57 57 Ncm<br />
IR-VIPA1<strong>10</strong> ViscoPakt-1<strong>10</strong> 1<strong>10</strong> Ncm<br />
IR-VIPARS Optional RS232 Interface Setpoint rotational speed and actual torque<br />
Automatic<br />
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Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
322<br />
ViscoPakt ® -rheo<br />
The ViscoPakt-Rheo model series is equipped with<br />
precision-torque measuring. The zero torque, which<br />
depends on the rotational speed, is registered by an<br />
automatic calibration process and is used to correct<br />
the actual torque signal. This allows the on-line<br />
determination of the viscosity (via a calibration table)<br />
as well as of other rheological parameters.<br />
Technical Data<br />
Stirring and Dispersing<br />
ViscoPakt Model rheo - X7 - 16 - 27 - 57 -1<strong>10</strong> Unit<br />
Maximum torque 7 16 27 57 1<strong>10</strong> Ncm<br />
Resolution 0.003 0.01 0.02 0.04 0.08 Ncm<br />
Reproducibility 0.05 0.1 0.2 0.4 0.8 Ncm<br />
Minimum speed 40 40 40 40 40 rpm<br />
Maximum speed 3000 2200 2200 2000 2000 rpm<br />
Speed uncertainty 0.1 0.1 0.1 0.1 0.1 %<br />
Chuck size 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> mm<br />
Type of protection<br />
controlling device<br />
20 20 20 20 20 IP<br />
Type of protection<br />
drive<br />
54 54 54 54 54 IP<br />
Approx. Weight 0.9 1.7 2.6 3.9 6 kg<br />
Motor Diameter 70 45 55 70 83 mm<br />
Length above axis<br />
(approx.)<br />
250 245 250 255 295 mm<br />
Extension<br />
diameter/length<br />
16/220 16/220 16/220 16/220 16/220 mm<br />
Max. viscosity 5,000 6,000 <strong>10</strong>,000 40,000 70,000 mPas<br />
Max. Mixing quantity<br />
(H2O)**<br />
2 8 15 30 50 Litres<br />
* Control Unit /Drive<br />
** Reference values for propeller stirrer in H2O*<br />
Interfaces<br />
Analogue:<br />
Required rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />
Actual rotational speed (= required value or 0) 0 - <strong>10</strong> V, 0/4-20mA<br />
Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />
Changes to the rotational speed which are caused<br />
by load fluctuations are registered by a digital<br />
revolution counter and are electronically regulated.<br />
The rotational speed can be pre-set via an analogue<br />
input or the serial interface. The actual rotational<br />
speed and the torque are issued via the analogue<br />
outputs and the serial interface.<br />
RS232:<br />
Send: Required rotational speed<br />
Received: Required rotational speed, actual rotational speed, actual torque value<br />
Delivery Scope Measuring-stirrer drive and control unit with 2.3 m cable<br />
Order Code Description Specifications<br />
IR-VIPARHX7 ViscoPakt-Rheo-X7 7 Ncm<br />
IR-VIPARH16 ViscoPakt-Rheo-16 16 Ncm<br />
IR-VIPARH27 ViscoPakt-Rheo-27 27 Ncm<br />
IR-VIPARH57 ViscoPakt-Rheo-57 57 Ncm<br />
IR-VIPARH1<strong>10</strong> ViscoPakt-Rheo-1<strong>10</strong> 1<strong>10</strong> Ncm<br />
IR-VIPARS Option RS232 Interface Setpoint and actual rotational speed and<br />
actual torque<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
ViscoPakt ® -rheo+<br />
The model series ViscoPakt-Rheo+ is based on<br />
most modern brushless drives. Consequently, they<br />
are absolutely maintenance-free and the friction<br />
moment caused by the brush is no longer existent at<br />
precision torque measurements. The speeddependant<br />
zero torque is captured in the course of<br />
an automatic calibration procedure and utilised for<br />
the correction of the torque signal. Herewith, it is<br />
Technical Data<br />
Stirring and Dispersing<br />
Type ViscoPakt-rheo+ -40 -75 -150 -220 Einheit<br />
Maximum torque 40 75 150 220 Ncm<br />
Resolution 0,01 0,03 0,04 0,05 Ncm<br />
Reproducibility 0,1 0,2 0,3 0,4 Ncm<br />
Minimum speed 40 40 40 40 rpm<br />
Maximum speed 2200 2000 2000 2000 rpm<br />
Speed uncertainty 0,01 0,01 0,01 0,01 %<br />
Chuck size 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> mm<br />
Type of protection 20 20 20 20 IP<br />
controlling device<br />
Type of protection drive 54 54 54 54 IP<br />
Approx. Weight 1,5 2,5 3,5 5 kg<br />
Motor Diameter 43 87 87 87 mm<br />
Length above axis 200 180 180 2<strong>10</strong> mm<br />
(approx.)<br />
Extension diameter/length <strong>10</strong> / 200 13 / 200 13 / 200 13 / 200 mm<br />
Max. viscosity <strong>10</strong>.000 40.000 70.000 70.000 mPas<br />
Max. Mixing quantity** 15 40 60 80 Liter<br />
* Steuergerät/Antrieb<br />
** Richtwerte für Propellerrührer in H2O<br />
Schnittstellen<br />
RS232, RS485 interface with Modbus Protocol (opt.)<br />
Send: Rotational speed desired value<br />
Receive: Rotational desired/actual value, torque actual value<br />
Analogue:<br />
Required rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />
Actual rotational speed (= required value or 0) 0 - <strong>10</strong> V, 0/4-20mA<br />
Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />
possible to establish the viscosity (per calibration<br />
table) and other rheological parameters online.<br />
Speed changes caused by load variations are<br />
captured by a digital speed sensor and electronically<br />
compensated. The speed can be predefined via an<br />
analogue input or the serial interface. The actual<br />
speed and the torque are issued via analogue<br />
outputs and the serial interface.<br />
Delivery Scope Measuring-stirrer drive and control unit with 2.3 m cable<br />
Bestellcode Beschreibung<br />
IR-VIPARHP40 ViscoPakt-Rheo+-40 precision-stirrer actuator, 40 Ncm<br />
IR-VIPARHP75 ViscoPakt-Rheo+-75 precision-stirrer actuator, 75 Ncm<br />
IR-VIPARHP150 ViscoPakt-Rheo+-150 precision-stirrer actuator, 150 Ncm<br />
IR-VIPARHP220 ViscoPakt-Rheo+-220 precision-stirrer actuator, 220 Ncm<br />
IR-VIPARHPRS485 Option RS485 ModBus Interface<br />
IR-VIPARHPUI Option Current and voltrage interface<br />
Automatic<br />
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ViscoPakt ® -mini-rheo-35<br />
Stirring and Dispersing<br />
The ViscoPakt-mini is a<br />
precision measuring stirrer<br />
disposing of an especially<br />
compact design. It is<br />
deployed where torques<br />
must be generated in most<br />
limited spaces. These are<br />
mainly small reactors with a<br />
nominal volume below 500<br />
ml with many mounted<br />
sockets at the same time,<br />
as such are frequently<br />
deployed for parallel<br />
syntheses.<br />
The ViscoPakt-mini,<br />
amongst other utilisations,<br />
is deployed in our LabKit<br />
and MultiLab parallel<br />
reactor systems.<br />
Interfaces<br />
Analogue:<br />
Order Code Description<br />
IR-VIPA-MINI-RHEO-35 ViscoPakt-mini-rheo stirrer drive, 35 Ncm<br />
Ministirrer<br />
The MiniStirrer is the economic<br />
alternative to the ViscoPakt-mini<br />
with a lower maximum torque<br />
and simple torque measurement<br />
(current measurement).<br />
It can be deployed everywhere<br />
where a qualitative torque signal<br />
is sufficient and relatively lowviscous<br />
substances are stirred.<br />
Order Code Description<br />
IR-MINISTIRR<strong>10</strong> Mini-stirrer-<strong>10</strong> stirrer drive<br />
<strong>HiTec</strong>-<strong>Zang</strong> naturally also offers all necessary<br />
accessories, e.g. flexible stirrer shafts, stirrer shaft<br />
protection, special stirrer receptacles, and also a<br />
wide array of mixing elements made of glass, high-<br />
Setpoint rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />
Actual rotational speed (=<br />
setpoint value or 0)<br />
0 - <strong>10</strong> V, 0/4-20mA<br />
Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />
RS232:<br />
Send: Setpoint rotational speed<br />
Received: Setpoint rotational speed, actual<br />
rotational speed, actual torque value<br />
ViscoPakt Type mini-rheo-35 Unit<br />
Maximum torque 35 Ncm<br />
Resolution 0.01 Ncm<br />
Reproducibility 0.1 Ncm<br />
Minimum speed 15 rpm<br />
Maximum speed 800 rpm<br />
Diameter 45 mm<br />
Length across axis 230 mm<br />
Interfaces<br />
Analogue:<br />
Setpoint rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />
Actual rotational speed (=<br />
Setpoint value or 0)<br />
0 - <strong>10</strong> V, 0/4-20mA<br />
Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />
ViscoPakt Type Mini-strirrer-<strong>10</strong> Unit<br />
Maximum torque 17 Ncm<br />
Resolution 0.07 Ncm<br />
Reproducibility 0.5 Ncm<br />
Minimum speed 60 rpm<br />
Maximum speed 1900 rpm<br />
Diameter 50 mm<br />
Length across axis 195<br />
*only current measurement!<br />
mm<br />
grade steel PTFE and other materials. Our experts<br />
will gladly help you to arrange the mixing elements<br />
and stirrers that exactly accord to your requirements.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Stirring and Dispersing<br />
ViscoTrol Control Unit for Three-Phase Stirrer Drive<br />
The ViscoTrol control units enable an electronically<br />
controlled variation of the rotational speed of three<br />
phase stirrer drives and the electronic collection of<br />
the torque. Due to this, adjustable gear units and<br />
and measuring shafts are no longer necessary.<br />
The standard ViscoTrol family meets simple<br />
requirements in regard to precision.<br />
Higher demands to precision are met by the<br />
ViscoTrol rheo family.<br />
Due to unsufficiant cooling when in low rpm mode it<br />
is recommended to adjust the motor via the set point<br />
of the control device or adding an additional cooler.<br />
ViscoTrol<br />
The control units dispose of a Start-Stop switch and<br />
a setpoint potentiometer for manual operation.<br />
Interfaces:<br />
Analogue Interfaces: 4...20mA, E = setpoint<br />
rotational speed,<br />
A = Torque and actual rotational speed<br />
RS485 interface with Modbus Protocol<br />
Digital Release<br />
Notice<br />
A MODBUS interface requires the option<br />
PNKMODBUS and a free RS485 interface at the PI.<br />
The activation via 4-20 mA requires an 4-20mA<br />
analogue output for the setpoint rotational speed, as<br />
Delivery Scope Control Unit with power cable.<br />
Technical Data<br />
Performance 0.35 up to 2.2 kW<br />
Rotational Speed 1:250 (at sufficient<br />
Variation<br />
cooling of motor)<br />
Start Ramp Adjustable<br />
Torque Limiting Adjustable<br />
RPM Limiting Adjustable<br />
Resolution<br />
Torque Measurement<br />
5% (differentiated)<br />
Casing Protection<br />
Category<br />
IP54<br />
Power Supply Single phase supply 200 -<br />
240V<br />
Dimensions LxWxH 192x215x277mm<br />
well as respectively one analogue input 4-20mA for<br />
the actual rpm and torque. In addition, a digital<br />
output is required for the digital release.<br />
Order Code Description<br />
IR-VISCOTROL350 ViscoTrol350 control unit for three phase drives, 0,35 kW<br />
IR-VISCOTROL550 ViscoTrol550 control unit for three phase drives, 0,55 kW<br />
IR-VISCOTROL1<strong>10</strong>0 ViscoTrol1<strong>10</strong>0 control unit for three phase drives, 1,1 kW<br />
IR-VISCOTROL2200 ViscoTrol2200 control unit for three phase drives, 2,2 kW<br />
IR-VISCOTROL-MOT055 Asynchronous 0,55 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT075 Asynchronous 0,75 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT1<strong>10</strong> Asynchronous 1,<strong>10</strong> kW motor for Viscotrol<br />
IR-VISCOTROL-MOT150 Asynchronous 1,5 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT300 Asynchronous 3,0 kW motor for Viscotrol<br />
IR-VISCOTROL-FAN Additional fan for ViscoTrol asynchrous motor<br />
ZK-R-HI30-BK-IX-Y-01 ViscoTrol cable for LabManager/box, 4...20mA rotational speed set point and current value,<br />
digital disengange<br />
ZK-R-HI30-BS-R4-I-01 ViscoTrol cable RS485<br />
Automatic<br />
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ViscoTrol rheo<br />
The activation via 4-20 mA<br />
requires an 4-20mA<br />
analogue output for the<br />
setpoint rotational speed, as<br />
well as one analogue input 4-<br />
20mA for the torque The<br />
checkback signal of the<br />
actual rotational speed via the<br />
device-internal PFM-output<br />
requires an additional digital<br />
input. In addition, a digital<br />
output is required for the digital release. Notice: The<br />
deployment of the RS485 requires an additional<br />
RS485 interface module in the PI and a device<br />
component for binary protocoling.<br />
Note: For a MODBUS-interface the option<br />
PNKMODBUS and a single free RS485 at the PI is<br />
needed.<br />
Delivery Scope Control Unit (box) with power<br />
supply line<br />
Stirring and Dispersing<br />
Technical Data<br />
Order Code Description<br />
IR-VISCOTROL350-RHEO ViscoTrol350 control unit for three phase drives. 0,35 kW<br />
IR-VISCOTROL550-RHEO ViscoTrol550control unit for three phase drives, 0,55 kW<br />
IR-VISCOTROL750-RHEO ViscoTrol750 control unit for three phase drives, 0,75 kW<br />
IR-VISCOTROL-MOT075 Asynchronous 0,75 kW motor for Viscotrol<br />
IR-VISCOTROL-MOT1<strong>10</strong> Asynchronous 1,<strong>10</strong> kW motor for Viscotrol<br />
IR-VISCOTROL-FAN Additional fan for ViscoTrol asynchrous motor<br />
Cable<br />
Performance 0.35 to 0.75 kW<br />
Rotational Speed 1:250 (if motors sufficiently<br />
Variation cooled)<br />
Start Ramp Adjustable<br />
Torque Limiting Adjustable<br />
RPM Limiting Adjustable<br />
Resolution Torque 0.5%<br />
Measurement<br />
Casing Protection<br />
Category<br />
IP 20, IP54 at connection<br />
Power Supply 400V Rotating current<br />
Interfaces:<br />
Analogue interfaces 4...20mA, I = set point rpm, O =<br />
torque<br />
RS485 interface with Modbus RTU protocol<br />
Digital disengage<br />
Bestellcode Beschreibung<br />
ZK-R-HI31-BK-IA-Y-01 Cable for LabManager/box, rotational speed setpoint value, actual value torque actual value<br />
4...20mA., release via digital output, 3m<br />
ZK-R-HI31-BK-IP-Y-01 Cable for LabManager/box, rotational speed setpoint value, actual value torque actual value<br />
4...20mA., release via digital output, 3m<br />
Accessories for the ViscoPakt®-Family<br />
Cable<br />
Order Code Description<br />
ZK-R-HI02-BA-UP-Y-03 Cable for LabManager/box, Setpoint speed and actual value,<br />
torque current value, 0...<strong>10</strong>V, 3m<br />
ZK-R-HI02-BA-IP-Y-02 Cable for LabManager/box, Setpoint speed required and actual value,<br />
torque actual value, 0/4...20mA, 3m<br />
ZK-R-HI02-BS-R2-I-01 RS232 cable, Setpoint speed and actual value,<br />
torque actual value, On/Off, 3m<br />
Mounting Elements<br />
Bilateral mounting element for LabKit square<br />
aluminum profiles.<br />
In comparison to standard mounting elements with<br />
round rod, this element defines all axes of the stirrer<br />
drive.<br />
Order Code Description<br />
IR-VPMONT2 Mounting element for ViscoPakt stirrer drives on to LabKit aluminum profiles<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Stirrer Couplings<br />
These stirrer shaft coulings are made of POM, a<br />
mechanically stable light-weight plastic. The power<br />
transmission is conducted via a novel internally<br />
located construction with high-grade steel ball<br />
bearings.<br />
Standard version<br />
Version for magnetic stirrer heads<br />
Stirring and Dispersing<br />
The individual advantages are:<br />
� low-weight but highly stable construction<br />
� extremely low centrifugal forces due to the<br />
low weight<br />
� suited for stirrer shafts jacketed with glass,<br />
metal or PTFE<br />
� Rotational direction-independent (anti- and<br />
clockwise rotation equally possible)<br />
� version free of play (no vibration development<br />
or resonance)<br />
� suited for speeds up to 1200 rpm<br />
� high-power transmission up to 3 Nm<br />
� uncomplicated mounting of the stirring shaft<br />
in a Ø 8 mm and Ø <strong>10</strong> mm receptacle (clamp<br />
ring connection)<br />
� extra-long receptacle pin with Ø <strong>10</strong> mm,<br />
respectively 8 mm hexagon head, and a<br />
length of 90 mm, generates space (length can<br />
be shortened by user)<br />
� Temperature stability maximal +1<strong>10</strong>°C and<br />
minimal -20°C, respectively without stress<br />
Technical Data<br />
Stirring shaft receptacle,<br />
below<br />
8 mm and <strong>10</strong> mm<br />
Upper receptacle Ø <strong>10</strong><br />
Total length 190 mm<br />
Maximum axis offset <strong>10</strong> mm<br />
Technical Data<br />
Stirring shaft receptacle Interior-square<br />
SW6<br />
Upper receptacle Female hexagon<br />
SW8<br />
Total Length 190 mm<br />
Maximum axis offset <strong>10</strong> mm<br />
Order Code Description<br />
IR-VIPARK-BF-POM Light-weight, highly stable stirring coupling made of POM, standard version for stirrer shafts Ø<br />
8mm or <strong>10</strong>mm<br />
IR-VIPARK-VK-POM Light-weight, highly stable stirring coupling made of POM, for magnetic stirrer heads with interiorsquare<br />
SW5 for magnetic coupling<br />
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Bellows couplings<br />
In order to be able to bridge longer distances<br />
between the stirrer drive and stirring lead-through,<br />
we offer our flexible stirring shaft extensions. They<br />
consist of bellows couplings and high-grade steel<br />
shafts.<br />
Stirring and Dispersing<br />
Order Code Description Specifications<br />
IR-VIPARWV15019 Flexible stirring shaft extension made of 19 cm, shaft Ø 6mm, 2 bellows coupling max.<br />
high-grade steel<br />
150Ncm<br />
IR-VIPARWV45020 Flexible stirring shaft extension made of 20 cm, shaft Ø <strong>10</strong>mm, 2 bellows coupling max.<br />
high-grade steel<br />
450Ncm<br />
IR-VIPARWV45028 Flexible stirring shaft extension made of 28 cm, shaft Ø <strong>10</strong>mm, 2 bellows coupling max.<br />
high-grade steel<br />
450Ncm<br />
IR-VIPARWV<strong>10</strong>0021 Flexible stirring shaft extension made of 21 cm, shaft Ø <strong>10</strong>mm, 2 bellows coupling max.<br />
high-grade steel<br />
<strong>10</strong>00Ncm<br />
IR-VIPARWV<strong>10</strong>0029 Flexible stirring shaft extension made of 29 cm, shaft Ø <strong>10</strong>mm, 2 bellows coupling max.<br />
high-grade steel<br />
<strong>10</strong>00Ncm<br />
Magnetic stirrer heads<br />
Technical Data<br />
For stirring shafts-Ø 8 mm <strong>10</strong> mm<br />
Square connection<br />
for coupling<br />
Female<br />
square<br />
adapter<br />
SW6<br />
With grinding<br />
Female<br />
square<br />
adapter<br />
SW6<br />
Guide Tube<br />
(glas)<br />
NS 29/32<br />
max. torque 50 Ncm 50 Ncm<br />
max. rpm 1500 rpm 1500 rpm<br />
max. media temp. 250°C 250°C<br />
With grinding<br />
NS 29/32<br />
Advantages<br />
Order Code Description<br />
IR-RDFMAG8 magnetic stirrer head for 8 mm stirring shafts<br />
IR-RDFMAG<strong>10</strong> magnetic stirrer head for <strong>10</strong> mm stirring shafts<br />
� high performance power transmission 50<br />
Ncm<br />
� metal–free, no lubricants<br />
� easy-to-clean due to easy-to-access and<br />
smooth components<br />
� compact construction, low outer dimensions -<br />
Ø 35 mm, generates space on the lid<br />
� high rotational speed up to max. 1.500 rpm<br />
� high working temperature up to +250°C<br />
� excellent chemical stability (comparable with<br />
PTFE)<br />
� Suited for dry run<br />
� Sealed rotor prevents leakages<br />
� smooth, non-porous rotor prevents memory<br />
effects<br />
� extremely durable due to exchangeable<br />
durable wear parts<br />
Miscellaneous Accessories<br />
Order Code Description Specifications<br />
IB-SIND Inductive rotation speed monitor 3...300 Impulse /min, dimensions: M30 thread x 81 mm<br />
IR-VIPASFG Chuck size for glass stirrer with shaft Diameter 8mm, 2 bellows couplings<br />
IR-VIPARWS Stirring shaft protection, half-shell Adjustable length: 19 to 30 cm<br />
Special designs and further accessories available upon request.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Stirrer Blades<br />
According to the desired application, some stirrer<br />
blades are more suited than others to perform the<br />
task. In laboratories close to production, it is often<br />
preferred to use the same stirrer type as in<br />
production in order to reach maximum comparability.<br />
Anchor Stirrer Propeller<br />
Stirrer<br />
Turbine Stirrer Cross-Arm<br />
Stirrer<br />
Stirring and Dispersing<br />
Plane Stirrer /<br />
Turbo Stirrer<br />
Slanted Blade<br />
Stirrer<br />
We are able to produce and supply stirrer blades<br />
according to your specifications made of stainless<br />
steel, glass and other materials.<br />
Stirrer blades out of metal can be provided with a<br />
thin glass coating in order to increase media<br />
compatibility.<br />
Impeller Stirrer MIG-Stirrer Toothed Disc/<br />
Dissolver<br />
Stirrer<br />
Grating Stirrer Paddle Stirrer Spiral Ribbon<br />
Stirrer<br />
Stirrer type Recommended Application Speed Range Principal Viscosity Limit Diameter Ratio D/<br />
approx. rpm** Current approx. mPas (cSt) d<br />
Anchor stirrer In case of crust<br />
development, good<br />
exchange of heat,<br />
strong shear flow,<br />
medium to high-viscous<br />
20 ... 500 tangential 50,000 1.05 ... 1.1<br />
Propeller stirrer Good mixing effect,<br />
stirring of light solid<br />
matters, thickening<br />
agents<br />
200 ... 1800 axial 4,000 3 ... 6<br />
Pane stirrer Dispersing, dispersion 300 ... 1500 radial 1,000 2 ... 4<br />
(with blades)/ of gases, strong shear<br />
Turbo stirrer flow<br />
Impeller stirrer Good mixing effect 500 ... 1500 radial <strong>10</strong>,000 1.5 ... 2<br />
MIG-stirrer high mixing effect,<br />
strong shear flow for<br />
low to medium<br />
viscosities<br />
200 ... <strong>10</strong>00 axial <strong>10</strong>,000 1.05 ... 1.5<br />
Toothed disc/<br />
dissolver stirrer<br />
Particle break-up <strong>10</strong>00 ... 3000 radial <strong>10</strong>0,000 2 ... 5<br />
Turbine stirrer Highly viscous media,<br />
lacquers, medium to<br />
high rotation speeds<br />
400 ... 2200 axial 200,000 3 ... 6<br />
Automatic<br />
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Components<br />
Process Analytics<br />
and Sensors<br />
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Stirring and Dispersing<br />
Stirrer type Recommended Application Speed Range Principal Viscosity Limit Diameter Ratio<br />
approx. rpm** Current approx. mPas (cSt) D/d<br />
Cross-arm stirrer Shea flows in several<br />
fields, medium viscous<br />
liquids, good exchange of<br />
heat<br />
400 ... 800 tangential <strong>10</strong>,000 1.1 ... 2<br />
Slanted blade good axial mixing effect , 500 ... 2500 radial 1,000 2.5 ... 3.5<br />
stirrer<br />
shear flow, prevention of<br />
layer build-up<br />
Grating stirrer Medium viscosity, strong<br />
shear flow, good<br />
exchange of heat<br />
200 ... 700 tangential 5,000 1.4 ... 2<br />
Paddle stirrer Low rotation speed, strong 20 ... <strong>10</strong>0<br />
shear flow, very sparing at<br />
low rotation speeds<br />
tangential <strong>10</strong>0 1.5 ...3<br />
Helical ribbon Powerful shear flow, for 50 ... 200 axial 50,000 1.1 ... 1.5<br />
stirrer<br />
high-viscous liquids,<br />
suspensions, pastes<br />
**with D of approx. 20 cm<br />
The stated values do strongly vary within literature<br />
by more than one order of magnitude and are used<br />
for a first orientation. Our project department will<br />
gladly help you to find a suitable stirrer-drive.<br />
To help you, we require the following information<br />
Order Code Description<br />
IR-RBL-rt-rd-ws-wl-wd Stirrer blade<br />
rt = stirrer type:<br />
AN Anchor stirrer<br />
PR Propeller stirrer<br />
SC Plane or turbo stirrer<br />
IP Impeller stirrer<br />
MI MIG-stirrer<br />
ZA Toothed disc stirrer<br />
TU Turbine stirrer<br />
KR Cross arm stirrer<br />
ST Slant blade stirrer<br />
GI Grating stirrer<br />
BL Paddle stirrer<br />
SP Spiral stirrer<br />
rd = blade diameter in mm (d)<br />
ws = material:<br />
ES Stainless steel<br />
EG Glass coated stainless steel<br />
GL Glass<br />
wl = shaft length<br />
wd = shaft diameter<br />
Ordering example:<br />
Anchor stirrer of glass, diameter 15 cm, shaft<br />
diameter <strong>10</strong> mm, shaft length 30cm<br />
Order code: IR-RBL-AN-150-GL-300-<strong>10</strong><br />
from you:<br />
Stirrer type used, rotation speed, viscosity (or<br />
comparative information like water, motor oil,<br />
honey ...), mixing pot D, used stirrer D.<br />
Projecting Aide:<br />
Estimation of Viscosity<br />
Material Viscosity in mPas<br />
approx. at 20 ° C<br />
Acetone 0.33<br />
Alcohol 0.6<br />
Benzene 0.65<br />
Water 1<br />
Liqueur 3<br />
Condensed milk 7,5% 12<br />
Condensed milk <strong>10</strong>% 45<br />
Olive oil 80<br />
Edible oil 85<br />
Apple juice concentrate 300<br />
Egg liqueur 600<br />
Yogurt 900<br />
Glycerine 1,500<br />
Honey 2,000-<strong>10</strong>,000<br />
Mustard 11,000<br />
Print colours <strong>10</strong>0,000 – <strong>10</strong>0 Mill.<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Stirring and Dispersing<br />
ViscoGraph – Automation of Stirring Tests<br />
ViscoGraph allows the automation of stirringtechnological<br />
tests with the ViscoPakt Torque<br />
Measurement Stirrer.<br />
The Programme enables:<br />
� Measurement of the torque in dependency of the<br />
speed<br />
� User-defined Torque Profiles<br />
� Measurement of the Viscosity<br />
� Zero Torque Calibration<br />
With the buttons on the left, it is possible to call up<br />
the various functions of ViscoGraph. The current<br />
values of the test period, rotation speed etc., are<br />
presented in the view boxes.<br />
The diagrams present the procedure of speed and<br />
torque via the time.<br />
The speed profile can be defined via up to <strong>10</strong><br />
sampling points:<br />
it is possible to select for each speed sampling point,<br />
if the speed is approached via a jump or a ramp:<br />
The data is stored in the *.csv format and can<br />
undergo further processing with programmes such<br />
as MS-Excel.<br />
The measurement system can be extended by<br />
further measurement variables with the help of the<br />
digital measuring amplifier.<br />
The additionally captured measurement curves<br />
receive an own Y-axis in the diagram.<br />
Order Code Description<br />
SL-VISCOGRAPH ViscoGraph Control Software for automated Operation of ViscoPakt Measuring Stirrers<br />
SL-VISCOGRAPHAI ViscoGraph Control Software Upgrade for Voltage Measurement with IL-AINAMP1D<br />
SL-VISCOGRAPHPT ViscoGraph Control Software Upgrade for Temperature Measurement with I IL-PTAMP1D<br />
IL-AINAMP1D Digital Measuring Amplifier for -<strong>10</strong>...+<strong>10</strong>V, 0/4...20mA, RS232 V24 /RS485 Interface<br />
IL-PTAMP1D Digital Measuring Amplifier for Pt<strong>10</strong>0 Four-Wire Technology, RS232 V24 /RS485 Interface<br />
IL-MV1D-SN Power Supply Plug for digital Amplifier<br />
Customer-specific adjustments and extensions are possible.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 331<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
332<br />
Stirring and Dispersing<br />
Dispersing and Homogenising<br />
Drives<br />
These high-performance drives for laboratory<br />
applications meet all requirements to modern and<br />
compact laboratory drives and represent a<br />
guarantee for safe and successful working in the<br />
laboratory.<br />
Together with the accessories, you already dispose<br />
of a wide application range:<br />
� Homogenisation<br />
� Dispersing<br />
� Emulsifying<br />
� Suspending<br />
This can be utilised for the preparation of analyses<br />
as well as in reactor acceleration.<br />
The rotational speed of the drives can be adjusted<br />
continuously up to 35,000 rpm.<br />
The exchange of tools is fast and uncomplicated<br />
with the patented tool receptacle system.<br />
Tools<br />
The tools consist of rotor and stator. The rotor<br />
geometry generates a strong pumping effect. Due to<br />
this, the media is suctioned into the operational<br />
range between rotor and stator. Here, high<br />
frequency vertical and horizontal pulsations are<br />
generated. Due to the high exit speeds, ultrasonic<br />
frequencies are generated at the stator slits. This<br />
leads to cavitation.<br />
A balanced interaction between shear forces and<br />
percussion effects transfers the the liquid media<br />
intended for processing into the finest state. This<br />
significantly shortens process periods and reduces<br />
the heat input.<br />
The tools are made of acid-resistant high-grade<br />
steel 316L. They can be sterilised and are<br />
autoclaveable.<br />
The special shaft geometry enables fast tool<br />
exchange. PTFE rings prevent the medium from<br />
rising into the shaft tube.<br />
Drive 350 Watt Drive 1400 Watt Tool<br />
Order Code Description<br />
IR-DISPANTR350 Drive 350Watt, up to 35,000 rpm, for dispersing tools<br />
IR-DISPANTR750 Drive 750Watt, up to 35,000 rpm, for dispersing tools<br />
IR-DISPANTR850 Drive 850Watt, up to 35,000 rpm, for dispersing tools<br />
IR-DISPANTR1400 Drive 1400Watt, up to 35,000 rpm, for dispersing tools<br />
IR-DISPWZ040 Dispersing tool with quick coupling, diameter 4 mm<br />
IR-DISPWZ063 Dispersing tool with quick coupling, diameter 6.3 mm<br />
IR-DISPWZ140 Dispersing tool with quick coupling, diameter 14 mm<br />
IR-DISPWZ200-G Dispersing tool with quick coupling, coarse, diameter 20 mm<br />
IR-DISPWZ40-F Dispersing tool with quick coupling, fine, diameter 20 mm<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Here you will find:<br />
� Customised Application Programs<br />
� Seminars and Training Offers<br />
� <strong>Main</strong>tenance Contracts<br />
� Order Guide for Product Manuals<br />
Services<br />
Services<br />
Phases<br />
Services<br />
Planning Establishment<br />
/ Assembly<br />
Commissioning Operation<br />
Consultancy �� ��<br />
Training �� �� ��<br />
Realisation �� �� ��<br />
Support �� �� �� ��<br />
Service/<strong>Main</strong>ten<br />
ance<br />
��<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 333<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
334<br />
Services<br />
<strong>HiTec</strong> <strong>Zang</strong> - Your competent Project Partner !<br />
The company <strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong>, in addition to<br />
being a system retailer supplying systems and<br />
components, also offers a wide range of services.<br />
We are able to support you with our know-how<br />
gained in 30 years of project work for the process<br />
engineering industry covering all project phases:<br />
Services<br />
Phases<br />
Planning Establishment /<br />
Assembly<br />
Commissioning Operation<br />
Consultancy �� ��<br />
Training �� �� ��<br />
Realisation �� �� ��<br />
Support �� �� �� ��<br />
Service/<br />
<strong>Main</strong>tenance<br />
Our Service Portfolio in detail:<br />
� PMC technical consultancy,<br />
� Procedural consultancy,<br />
� Plant design for laboratory and<br />
� Mini-plants,<br />
� PMC, planning of basic version, realisation<br />
� and planning of application -oriented details,<br />
� Component selection for special<br />
� Problem solutions,<br />
� PMC, application establishment,<br />
� Control-oriented support,<br />
� Support for Commissioning,<br />
� Fault diagnosis and analysis,<br />
� Device coupling,<br />
� Sensor calibration,<br />
� Seminars and training,<br />
� Remote maintenance,<br />
� Order development.<br />
��<br />
Take advantage of our widespread know-how for<br />
your projects:<br />
� Research Process Control Systems,<br />
� Automated Laboratory Reactor Systems,<br />
� Mini- und Bench-Plant-Technology,<br />
� NAMUR-basis Operations,<br />
� Instrumenting, Sensors,<br />
� Spectrometry,<br />
� High-Precision Temperature Measurement,<br />
� Reaction Calorimetry,<br />
� Weighing and Dosing Technology,<br />
� Measuring and Control Technology,<br />
� Process Control Technology, PLC Technology,<br />
� LIMS-Systems,<br />
� Device Interfaces,<br />
� CAN-Bus, Profi-Bus-DP,<br />
� Remote Data Transmission, Remote<br />
<strong>Main</strong>tenance,<br />
� Remote Alarming via Phone, E-Mail or SMS,<br />
� Computer Networks<br />
� Quality Assurance Systems.<br />
Our experienced project engineers and technicians<br />
will support you all the way until your project is<br />
ideally realised. Whether you merely require<br />
consultancy, or you wish to couple an analysis<br />
device with a special protocol with a control system,<br />
or you require a complete ready-to-use plant,<br />
whatever it may be, you can count on our support.<br />
Just talk to us!<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Services<br />
Customised Application Programs<br />
<strong>HiTec</strong> <strong>Zang</strong> establishes application programs<br />
according to customer specifications. If required,<br />
we will gladly establish a duty record book<br />
Collection and Administration of Stirrer-related Data<br />
GyroDat is a program package for the projecting<br />
and realisation of tests applying a stirrer. The work<br />
environment includes the process control of the<br />
test progression, the collection, evaluation, the<br />
presentation, and archiving of the data.<br />
GyroDat consists of two modules. The<br />
administration, projecting, and evaluation were<br />
realised in the <strong>HiTec</strong> <strong>Zang</strong> HiBuilder, the process<br />
control programmed in the <strong>HiTec</strong> <strong>Zang</strong> -<br />
Labvision and HiText.<br />
Systematic Examinations:<br />
� Influence of the Stirrer Design<br />
� Influence of Flow Interrupters<br />
� Influence of Vessel Design<br />
� Properties of Media<br />
The Sequence of Operation<br />
Stirrer type, vessel type, flow interrupters, and<br />
revolutions are specified by the user and transferred<br />
by GyroDat to Labvision for automatic execution.<br />
The data collected in the course of the stirring test is<br />
transferred by Labvision to GyroDat for evaluation.<br />
GyroDat calculates the process characteristics and<br />
establishes the result diagrams.<br />
Calculated Data:<br />
� Re = f(Ne)<br />
� Md = f(n)<br />
� Idle time data of the stirrer drive<br />
containing the product requirement specifications<br />
in the forefront. The following shows an example<br />
based on the HiBuilder.<br />
Administration of the Project Data<br />
The user interface/work station of the GyroDat is<br />
designed for the graphic evaluation and simple<br />
comparison of various test data.<br />
Up to ten project steps can be parameterised in the<br />
project data window. A change of media during the<br />
test is taken into account. Data storage is<br />
conducted automatically.<br />
Administrated are:<br />
� 200 Project Template<br />
� <strong>10</strong>0 Stirrer Stands<br />
� <strong>10</strong>0 Stirrer<br />
� <strong>10</strong>0 Container<br />
� <strong>10</strong>0 Flow Interruptor<br />
� 50 Reference Media<br />
Presentation of the Data<br />
A freely designable protocol page (with HiBuilder)<br />
containing graphics, values, and comments can be<br />
printed out.<br />
Order Code Description<br />
SA-GYRODAT Program for the collection and administration of stirrer data<br />
Please also consider our precision measurement stirrer ViscoPakt-rheo, which is ideally suited to conduct<br />
stirring tests.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 335<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
336<br />
Seminars and Training<br />
The continuous vocational and advanced training<br />
for personnel is the most important investment for<br />
the future of your enterprise. Profound knowledge<br />
is an essential prerequisite for the successful<br />
realisation of your products. Our seminar training<br />
portfolio in regard to the selection of the topics and<br />
content is the result of our many years of practical<br />
experience in deploying laboratory automation and<br />
mini-plant technology.<br />
Due to the fact that we are aware that learning<br />
something is accomplished the fastest by actually<br />
doing something yourself in practice, our training<br />
mainly consists of practical training at our systems.<br />
The participants mainly conduct clearly set tasks<br />
independently.<br />
The training is conducted on our premises and, in<br />
the ideal case, is rounded off by support during the<br />
commissioning at the client plant.<br />
Your advantages:<br />
� Reduction of the Project Preparation Period<br />
� Reduction of the Project Running Period<br />
� Better Results<br />
� Optimal Utilisation of the Equipment<br />
� Staff Satisfaction<br />
Training Modules<br />
the training program is principally aligned to your<br />
individual requirements. The training schedule is<br />
arranged out of the following modules. A user<br />
introduction approximately requires ½ to 1 day, a<br />
complete training program between 5 and 8 days,<br />
depending on the existent knowledge of the<br />
participant.<br />
Up to four participants may participate without<br />
additional charge. The provision of the equipment<br />
for two participants is included in the price. For<br />
Services<br />
each of the other two participants, extra equipment<br />
is required.<br />
Level 1: User Training<br />
Introduction into the Lab/MSRmanager System<br />
Prerequisites: Windows experience, basic<br />
chemical-process-oriented experience.<br />
Introduction of the UI Software LabVision<br />
� Configuring and Parameterising<br />
� Multiplotter<br />
� Online-Graphics<br />
� Monitoring and Operating in PLS Images<br />
� Programming<br />
User Training at the UI/Work Station of a<br />
simulated Plant<br />
� Administration and Starting of the Project<br />
� Configuring and Parameterising<br />
� Monitoring and Operating<br />
� Establishment and Realisation of a recipe with<br />
HiBatch<br />
� Discussion, open issues<br />
Level 2: Project Manager Training<br />
Project Establishment in LabVision<br />
Prerequisites: Windows experience, basic<br />
knowledge of PMC technology.<br />
PMC-Basic Knowledge<br />
� Connection and Parameterisation of Sensors<br />
and Actors<br />
� Data Storage in the History Data Base<br />
� Setting up of the Plotters<br />
� Establishment and Dynamisation of PLS-<br />
Images<br />
� Linking of Signals<br />
� Process Report<br />
� Message Report<br />
� Data Export<br />
� Routing of Message Events<br />
� Visualisation of Message Events<br />
� Project Establishment with Project Modules<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
The following topics can be combined to form an<br />
individually aligned training program:<br />
� HiText, Control and Online Evaluation<br />
� Programming of Recipe Element Programs<br />
Services<br />
� Setting Up and Parameterisation of Controllers<br />
� Programming in IEC 61131 I<br />
� System Administration<br />
� Advanced Training<br />
� Applied Control Technology<br />
Order Code Description<br />
DS-SCHULTAS One daily rate, content according to prior agreement<br />
DS-SCHULQUIP Provision of the training equipment, one work station, maximum two participants per day<br />
<strong>Main</strong>tenance Contracts<br />
Software-Upgrade-Contract<br />
An Update is an improved program version with<br />
unmodified functional range, After the purchase of<br />
any of our software, the customer, upon request, will<br />
receive updates free of charge for the duration of<br />
one year.<br />
An upgrade is a further developed version which<br />
usually contains an extended functional range.<br />
Without a software upgrade contract (after expiry of<br />
the first year), an upgrade for any consecutive year<br />
costs 15 % of the catalogue price. The upgrade<br />
option expires 4 years after the initial purchase,<br />
respectively the last update.<br />
Order Code Description<br />
DS-UPGR Software Upgrade<br />
Hardware <strong>Main</strong>tenance Contract<br />
If a Hardware <strong>Main</strong>tenance Contract is concluded,<br />
we will annually check and calibrate your devices<br />
and upgrade them to the current state of technology.<br />
Faulty parts will be exchanged free of charge either<br />
in our works or directly at the location. Only the<br />
travelling expenses will be charged. Damage due to<br />
external influences is excluded.<br />
Order Code Description<br />
DS-VHW Hardware <strong>Main</strong>tenance Contract<br />
Support and Remote <strong>Main</strong>tenance Contract<br />
If a Support Contract is concluded, our Hotline is<br />
available for the answering of your queries, when<br />
establishing applications or for the quick solution of<br />
software problems.<br />
Order Code Description<br />
DS-VSW Support and Remote <strong>Main</strong>tenance Contract<br />
Upon request, we will conduct the installation<br />
subject to the charge of the according expenditures.<br />
Example: If a software was purchased 2 ½ years<br />
ago (no existing software upgrade contract) and the<br />
catalogue prices is stated as, e.g., 2800€, the price<br />
for the update amounts to 2 x 15% (due to the fact<br />
that the first year is free) of 2800€, therefore 840€.<br />
With a Software-Upgrade-Contract, you are entitled<br />
to the respectively most recent version. The annual<br />
costs amount to 15 % of the current catalogue price.<br />
If required, we will conduct remote maintenance.<br />
The contract will be aligned to your individual<br />
requirements.<br />
Automatic<br />
Laboratory<br />
Reactor Systems<br />
Reaction<br />
Calorimetry<br />
Fermentation<br />
technology<br />
Automation<br />
Hardware<br />
Automation<br />
Software<br />
Plant<br />
Construction and<br />
Technology<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 337<br />
Equipment and<br />
Components<br />
Process Analytics<br />
and Sensors<br />
Dosing Systems,<br />
Pumps<br />
Liquid-Handling,<br />
Autosampler<br />
Stirring and<br />
Dispersing<br />
Services
338<br />
Product Manuals<br />
The manuals to our products are usually delivered<br />
together with the product on a data carrier. If<br />
required, they can also be acquired as a printed<br />
paper version.<br />
Application Software<br />
Services<br />
Order Code Description<br />
ZH-LABVIS LabVision Manual<br />
ZH-HIBUILDER Manual to the evaluation program HiBuilder<br />
ZH-GYRODAT Manual to the evaluation program GyroDat<br />
ZH-KALDAS Manual to the evaluation program KalDas<br />
ZH-SOLIDOS SoliDos Manual<br />
ZH-VISCOPAKT ViscoPakt Manual<br />
ZH-RAMOS RAMOS Manual<br />
ZH-LABDOS LabDos Manual<br />
ZH-GRAVIDOS GraviDos Manual<br />
ZH-AUTOSAM AutoSam Manual<br />
ZH-ALFADOS AlfaDos Manual<br />
ZH-REGLER Manual Controllers and Controller Parameterisation<br />
ZH-HICON Manual to the adaptive Controller HiCon<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
018ML<strong>10</strong>B.............................................................279<br />
070ML30B.............................................................279<br />
280ML80B ............................................................279<br />
CG-ABK1C............................................................136<br />
CG-ABK1D............................................................136<br />
CG-ABK1I..............................................................136<br />
CG-ABK1M...........................................................136<br />
CG-ABK2C............................................................137<br />
CG-ABK2D............................................................137<br />
CG-ABK2I..............................................................137<br />
CG-ABK2M...........................................................137<br />
CG-ABKEX............................................................137<br />
CG-LABCOMMANDER.........................................275<br />
CG-LABCOMMANDER.........................................274<br />
CG-OMNIFERM-ABK..............................................42<br />
CK-RAID1..............................................................137<br />
CK-RAM2x<strong>10</strong>24....................................................137<br />
CK-RAM2x2048....................................................137<br />
CK-RAM2x512......................................................137<br />
CP-BCS232...........................................................140<br />
CP-DIGICAM1.......................................................158<br />
CP-DIGICAM2.......................................................158<br />
CP-DRUHPDJC....................................................140<br />
CP-DRUHPLJ.......................................................140<br />
CP-DRUHPLJC.....................................................140<br />
CP-INMON ...........................................................138<br />
CP-ISDNAD..........................................................175<br />
CP-M17TFT..........................................................139<br />
CP-M190TFT........................................................139<br />
CP-M20TFTWS ....................................................139<br />
CP-M22TFTWS.....................................................139<br />
CP-MODEM2........................................................175<br />
CP-MODEM4........................................................175<br />
CP-USV7...............................................................138<br />
CP-USV7O............................................................138<br />
CP-USV7O............................................................136<br />
CS-RS2322-PCI....................................................139<br />
CS-RS2324-PCI....................................................139<br />
CS-RS4852-PCI....................................................139<br />
CS-RS4854-PCI....................................................139<br />
CZ-EXMAUS.........................................................137<br />
CZ-USB-RS232.....................................................275<br />
CZ-USB-RS232.....................................................274<br />
DS-LVPROG.........................................................174<br />
DS-SCHULQUIP ..................................................337<br />
DS-SCHULTAS ....................................................337<br />
DS-UPGR..............................................................337<br />
DS-VHW ...............................................................337<br />
DS-VSW ...............................................................337<br />
HA-COMSERV<strong>10</strong>01..............................................132<br />
HA-MODEM4........................................................132<br />
HA-RS485 ............................................................131<br />
HA-V24LINK2 .......................................................131<br />
HA-V24LINKKLA...................................................131<br />
HA-V24LINKKLI....................................................131<br />
HD-RS2329 ............................................................92<br />
HD-RS2329(P)L....................................................130<br />
HD-RS2329L.........................................................<strong>10</strong>3<br />
HD-RS2329PL......................................................<strong>10</strong>3<br />
HD-RS485P..........................................................<strong>10</strong>3<br />
HE-EEXID.............................................................121<br />
HE-EEXII...............................................................121<br />
HE-EEXIPT<strong>10</strong>0.....................................................121<br />
HE-EEXIRS232.....................................................121<br />
Order Codes<br />
HE-EEXITH...........................................................121<br />
HE-EEXIU.............................................................121<br />
HK-AD20N.............................................................121<br />
HK-AD20NMUX16................................................123<br />
HK-AD20NMUX8..................................................123<br />
HK-AD24DMS4.....................................................255<br />
HK-AD24DMS4.....................................................253<br />
HK-AD24DMS4.....................................................206<br />
HK-AD24DMS4.....................................................125<br />
HK-AD24DMS4PTR..............................................267<br />
HK-AD24PKAL......................................................124<br />
HK-AD24PX8........................................................124<br />
HK-DA812UI.........................................................125<br />
HK-DEA16N..........................................................126<br />
HK-GRADOMV1...................................................267<br />
HK-GRADOMV1...................................................255<br />
HK-GRADOMV1...................................................253<br />
HK-GRADOMV1...................................................206<br />
HK-GRADOMV1D.................................................267<br />
HK-GRADOMV1D.................................................255<br />
HK-GRADOMV1D.................................................206<br />
HK-GRADOMV1D-SN...........................................267<br />
HK-GRADOMV1D-SN...........................................255<br />
HK-GRADOMV1D-SN...........................................206<br />
HK-HMUX..............................................................122<br />
HK-PHAMP.............................................................92<br />
HK-SER16ECB.....................................................127<br />
HK-SER16ECB.....................................................<strong>10</strong>4<br />
HK-SER8ECB.......................................................127<br />
HK-SER8ECB.......................................................<strong>10</strong>4<br />
HK-SER8ECB.........................................................72<br />
HP-B230V16H ......................................................128<br />
HP-B230V16R.......................................................128<br />
HP-LABCOM1 ......................................................130<br />
HP-SITEMPBEG1.................................................257<br />
HP-SITEMPWAE1 ...............................................256<br />
HP-WDOGEXT1-pa .............................................131<br />
HS-NGS153SN.....................................................133<br />
HS-NGS241A........................................................132<br />
HS-NGS241S........................................................132<br />
HS-NGS242..........................................................133<br />
HS-NGS242............................................................69<br />
HS-NGS243..........................................................133<br />
HS-NGS248..........................................................133<br />
HS-NGS248E........................................................133<br />
HS-NGS248S........................................................132<br />
HX-SIMPT1...........................................................134<br />
IB-FGVE-120-GMG3/4-ea....................................257<br />
IB-FVGE-1200-GMG1/4-ea..................................259<br />
IB-FVGE-60-GMG3/4-ea......................................257<br />
IB-LWDRU-NC-ea.................................................262<br />
IB-LWE-<strong>10</strong>0-sk-ea.................................................260<br />
IB-LWE-250-NC-ea...............................................261<br />
IB-LWE-250-sk-ea.................................................260<br />
IB-LWE-300-sk-ea.................................................260<br />
IB-PRKO-6-ma-ea.................................................258<br />
IB-SIND.................................................................328<br />
IB-SIND.................................................................262<br />
IFN-IV-MW1..........................................................223<br />
IFN-IV-MW2..........................................................223<br />
IL-AINAMP1D........................................................331<br />
IL-AINAMP1D........................................................135<br />
IL-AINAMP1D........................................................134<br />
IL-ALCOTECT-AIRS...............................................47<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 339
340<br />
IL-ALCOTECT-d-l....................................................47<br />
IL-AOUT1D...........................................................135<br />
IL-AOUT1D...........................................................134<br />
IL-AUTOSAM-B-DN..............................................314<br />
IL-AUTOSAM-BSCHU..........................................313<br />
IL-AUTOSAM-DA24..............................................314<br />
IL-AUTOSAM-DA24..............................................312<br />
IL-AUTOSAM-DN-6-x-x.........................................313<br />
IL-AUTOSAM-EN-6-x............................................313<br />
IL-AUTOSAM-FEACON........................................314<br />
IL-AUTOSAM-KL...................................................313<br />
IL-AUTOSAM-MB-2-3-K........................................312<br />
IL-AUTOSAM-MB-2-3-P........................................312<br />
IL-AUTOSAM-POLI...............................................314<br />
IL-AUTOSAM-R....................................................312<br />
IL-AUTOSAM-RF-d-l.............................................312<br />
IL-AUTOSAM-RS485............................................314<br />
IL-AUTOSAM-SPPS.............................................314<br />
IL-AUTOSAM-STLI...............................................314<br />
IL-AUTOSAM-STRE.............................................314<br />
IL-AUTOSAM-TAN................................................312<br />
IL-AUTOSAM-TVERL...........................................314<br />
IL-AUTOSAM-WASBO..........................................314<br />
IL-AUTOSAM-XL-<strong>10</strong>00-12....................................317<br />
IL-AUTOSAM-XL-2000-8......................................317<br />
IL-AUTOSAM-XL-500-14......................................317<br />
IL-AUTOSAM200...................................................311<br />
IL-AUTOSAM200-T-11-32.....................................311<br />
IL-AUTOSAM300..................................................308<br />
IL-AUTOSAM300-T-12-50.....................................308<br />
IL-AUTOSAM300-T-17-32.....................................308<br />
IL-AUTOSAM300-T-23-25.....................................308<br />
IL-AUTOSAM300-T-30-23.....................................308<br />
IL-AUTOSAM300-T-46-15.....................................308<br />
IL-AUTOSAM300-T-56-11.....................................308<br />
IL-AUTOSAM360..................................................309<br />
IL-AUTOSAM360-T-12-80.....................................309<br />
IL-AUTOSAM360-T-17-49.....................................309<br />
IL-AUTOSAM360-T-23-41.....................................309<br />
IL-AUTOSAM360-T-46-18.....................................309<br />
IL-AUTOSAM360-T-56-15.....................................309<br />
IL-CLARKAMP1D..................................................135<br />
IL-CLARKAMP1D..................................................134<br />
IL-DIN1D...............................................................135<br />
IL-DIN1D...............................................................134<br />
IL-DOUT1D...........................................................135<br />
IL-DOUT1D...........................................................134<br />
IL-Gmix-S-RAMP....................................................47<br />
IL-GMIX21...............................................................47<br />
IL-GMIX21-X...........................................................47<br />
IL-GMIX31...............................................................47<br />
IL-GMIX31-X...........................................................47<br />
IL-GMIX31-XET.......................................................47<br />
IL-GMIX41...............................................................47<br />
IL-GMIX41-X...........................................................47<br />
IL-GMIX41-XET.......................................................47<br />
IL-GRADO<strong>10</strong>00.....................................................267<br />
IL-GRADO<strong>10</strong>000...................................................267<br />
IL-GRADO<strong>10</strong>000D................................................267<br />
IL-GRADO<strong>10</strong>00D..................................................267<br />
IL-GRADO15000...................................................267<br />
IL-GRADO15000D................................................267<br />
IL-GRADO3000.....................................................267<br />
IL-GRADO3000D..................................................267<br />
Order Codes<br />
IL-GRADO7000.....................................................267<br />
IL-GRADO7000D..................................................267<br />
IL-GRADOADR.....................................................206<br />
IL-GRADOADR12.................................................267<br />
IL-GRADOADR12.................................................255<br />
IL-GRADOADR14.................................................267<br />
IL-GRADOADR14.................................................255<br />
IL-GRADOADV.....................................................267<br />
IL-GRADOADV.....................................................255<br />
IL-GRADOADV.....................................................206<br />
IL-GRADOAMP1D................................................135<br />
IL-GRADOAMP1D................................................134<br />
IL-GRADOAMP1D................................................<strong>10</strong>6<br />
IL-GRADOAMP1D-SN..........................................<strong>10</strong>6<br />
IL-GRADOEX........................................................267<br />
IL-GRADOEX........................................................266<br />
IL-GRADOMV1.....................................................<strong>10</strong>6<br />
IL-GRAVI-KAL<strong>10</strong>00...............................................267<br />
IL-GRAVI-KAL2000...............................................267<br />
IL-GRAVIDOSST1.................................................267<br />
IL-GRAVIDOSST1.................................................266<br />
IL-GRAVIHEAT<strong>10</strong>00..............................................267<br />
IL-GRAVIHEAT2000..............................................267<br />
IL-GRAVIHEAT250................................................267<br />
IL-GRAVIHEAT500................................................267<br />
IL-GRAVIHEATSON..............................................267<br />
IL-GRAVIRS..........................................................267<br />
IL-GRAVIRS..........................................................266<br />
IL-GRAVLBB<strong>10</strong>00.................................................268<br />
IL-GRAVLBB<strong>10</strong>00.................................................267<br />
IL-GRAVLBB2000.................................................268<br />
IL-GRAVLBB2000.................................................267<br />
IL-GRAVLBB250...................................................267<br />
IL-GRAVLBB250 ..................................................268<br />
IL-GRAVLBB500...................................................268<br />
IL-GRAVLBB500...................................................267<br />
IL-GRAVLBGRAD.................................................267<br />
IL-GRAVLBS150...................................................267<br />
IL-GRAVLBS300...................................................267<br />
IL-GRAVLBS500...................................................267<br />
IL-HISENSE-c-2......................................................51<br />
IL-HISENSE-c-4......................................................51<br />
IL-HISENSE-c-8......................................................51<br />
IL-HISENSE-c-x......................................................42<br />
IL-HISENSE-m-1.....................................................50<br />
IL-HISENSE-m-2.....................................................50<br />
IL-HISENSE-m-3.....................................................50<br />
IL-HISENSE-m-5.....................................................50<br />
IL-HISENSE-m-5.....................................................50<br />
IL-HISENSE-m-x.....................................................42<br />
IL-KALHEIZE50.......................................................34<br />
IL-KALHEIZES<strong>10</strong>0..................................................34<br />
IL-KALHEIZG50......................................................34<br />
IL-KALHEIZGL<strong>10</strong>0..................................................34<br />
IL-KALHEIZP<strong>10</strong>0.....................................................34<br />
IL-KALHEIZP50.......................................................34<br />
IL-KALKALIB<strong>10</strong>0.....................................................34<br />
IL-KALKALIB50.......................................................34<br />
IL-LIQUIDOS1.......................................................315<br />
IL-MV1D-SN..........................................................331<br />
IL-MV1D-SN..........................................................135<br />
IL-ODFERM-l...........................................................42<br />
IL-OXYTECT-l.........................................................48<br />
IL-OXYTECT-l.........................................................42<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
IL-PHADEC...........................................................235<br />
IL-PHADEC-PTFE.................................................235<br />
IL-PHADEC-SE.....................................................235<br />
IL-PHADEC-X.......................................................235<br />
IL-PHAMP1...........................................................<strong>10</strong>5<br />
IL-PHAMP1D.........................................................135<br />
IL-PHAMP1D.........................................................134<br />
IL-PHAMP1D.........................................................<strong>10</strong>5<br />
IL-PHAMP1D-SN..................................................<strong>10</strong>5<br />
IL-PHASEP............................................................211<br />
IL-PHFERM-l...........................................................48<br />
IL-PHFERM-l...........................................................42<br />
IL-PIPET1..............................................................317<br />
IL-PTAMP1D.........................................................331<br />
IL-PTAMP1D.........................................................135<br />
IL-PTAMP1D.........................................................134<br />
IL-RFT-SV-1..........................................................212<br />
IL-RFT-SV-MAG....................................................212<br />
IL-RFT-TR-1..........................................................212<br />
IL-RFT-TR-MAG....................................................212<br />
IL-SCIBOT-x..........................................................318<br />
IL-SCIBOTBIB.......................................................318<br />
IL-SOLIDOS-RS....................................................304<br />
IL-SoliDos-SF-G-1.................................................303<br />
IL-SOLIDOS-SF-V-1..............................................302<br />
IL-SOLIDOS-TD-G................................................303<br />
IL-SOLIDOS-TD-G-1.............................................303<br />
IL-SOLIDOS-TD-V-1.............................................303<br />
IL-SOLIDOS2-HEIZ...............................................302<br />
IL-SOLIDOS2-KF..................................................302<br />
IL-SOLIDOS2-SK-x...............................................302<br />
IL-SOLIDOS2-x ....................................................302<br />
IL-SOLIDOS2-x-ST ..............................................302<br />
IL-SOLIDOSADGD................................................302<br />
IL-SOLIDOSST1...................................................304<br />
IL-VERDA-THEL...................................................213<br />
IL-VERDA-TREG..................................................213<br />
IL-VERDA120........................................................213<br />
IP-B-K1-1800L-VA-GMG1/2-ep............................294<br />
IP-B-K2-3900L-ETFE/SIC.....................................295<br />
IP-B-REAKT1-4P..................................................296<br />
IP-B-REAKT1-FU..................................................296<br />
IP-B-V1-1200L-PTFE/FPM...................................298<br />
IP-B-V1-1200L-PTFE/FPM.....................................16<br />
IP-B-V2-5600L-SN6..............................................299<br />
IP-B-VPS-mc.........................................................300<br />
IP-P-E1-2700M-VA/FKM-ea..................................291<br />
IP-P-LABDOS-AE.................................................280<br />
IP-P-LABDOS-AE.................................................274<br />
IP-P-LABDOS-DISPENS......................................274<br />
IP-P-LABDOS-DISPPB.........................................275<br />
IP-P-LABDOS-DISPPB.........................................274<br />
IP-P-LABDOS-DOMAS.........................................274<br />
IP-P-LABDOS-P-EASY-E......................................274<br />
IP-P-LABDOS-P-EASY-TC...................................274<br />
IP-P-LABDOS-P-EASYLOAD...............................274<br />
IP-P-LABDOS-P-MULTI-4-5..................................274<br />
IP-P-LABDOS-P-VARIO........................................274<br />
IP-P-LABDOS-P-VARIO-3....................................274<br />
IP-P-LABDOS-P-VARIO-3E..................................274<br />
IP-P-LABDOS-P-VARIO-4....................................274<br />
IP-P-LABDOS-P-VARIO-4E..................................274<br />
IP-P-LABDOS-P<strong>10</strong>0..............................................274<br />
IP-P-LABDOS-P30................................................274<br />
Order Codes<br />
IP-P-LABDOS-RS232BA......................................275<br />
IP-P-LABDOS-RS232BA......................................274<br />
IP-P-LABDOS-RS485...........................................280<br />
IP-P-LABDOS-RS485...........................................279<br />
IP-P-LABDOS-RS485...........................................275<br />
IP-P-LABDOS-RS485...........................................274<br />
IP-P-LABDOS-RS485BA......................................275<br />
IP-P-LABDOS-RS485BA......................................274<br />
IP-P-LABDOS-SK.................................................274<br />
IP-P-LABDOS-T-12...............................................280<br />
IP-P-LABDOS-T-2.................................................280<br />
IP-P-LABDOS-T-25...............................................280<br />
IP-P-LABDOS-T-50...............................................280<br />
IP-P-M1-1<strong>10</strong>0M-PTFE/C/KER-SN4/6-ea..............286<br />
IP-P-M2-<strong>10</strong>00M-PTFE/C/KER-SN4/6-ea..............288<br />
IP-P-M3-1800M-PTFE-SN4/6...............................289<br />
IP-P-N1-PK-mc.....................................................285<br />
IP-P-N1-PK-STRG-E.............................................285<br />
IP-P-N1-PK-STRG-VI............................................285<br />
IP-P-P1-0150M-PTFE/KER-SN17-ea...................287<br />
IP-P-P1-0150M-VA/KER-SN16-ea........................287<br />
IP-P-P3-0600M-VA/KER-SN16-ea........................290<br />
IP-P-R1-18M-HM-SN2-ea.....................................292<br />
IP-P-R1-9M-HM-SN2-ea.......................................292<br />
IP-P-R2-<strong>10</strong>152M-HM-SF1/8-ea............................293<br />
IP-P-R2-18M-HM-SF1/8-ea..................................293<br />
IP-P-R2-288M-HM-SF1/8-ea................................293<br />
IP-P-R2-72M-HM-SF1/8-ea..................................293<br />
IP-P-SM1-PP -mc..................................................283<br />
IP-P-SM1-PTFE -mc.............................................283<br />
IP-P-SM1-VA -mc..................................................283<br />
IP-P-Z1-018ML<strong>10</strong>B-E............................................279<br />
IP-P-Z1-070ML30B-E............................................279<br />
IP-P-Z1-280ML80B-E............................................279<br />
IP-P-Z1-HEAT.......................................................279<br />
IP-SYRDOS-VCER...............................................282<br />
IP-SYRDOS-VCER...............................................281<br />
IP-SYRDOS-VHPR...............................................282<br />
IP-SYRDOS-VHPR...............................................281<br />
IP-SYRDOS1........................................................281<br />
IP-SYRDOS1-ss-V2/3...........................................281<br />
IP-SYRDOS1-ss-VDxx..........................................281<br />
IP-SYRDOS1-ss-VNDyy.......................................281<br />
IP-SYRDOS2-ss-V2/3...........................................282<br />
IP-SYRDOS2-ss-VDxx..........................................282<br />
IP-SYRDOS2-ss-VNDyy.......................................282<br />
IR-DISPANTR1400...............................................332<br />
IR-DISPANTR350.................................................332<br />
IR-DISPANTR750.................................................332<br />
IR-DISPANTR850.................................................332<br />
IR-DISPWZ040.....................................................332<br />
IR-DISPWZ063.....................................................332<br />
IR-DISPWZ140.....................................................332<br />
IR-DISPWZ200-G.................................................332<br />
IR-DISPWZ40-F....................................................332<br />
IR-MINISTIRR<strong>10</strong>...................................................324<br />
IR-RBL-rt-rd-ws-wl-wd ..........................................330<br />
IR-RDFMAG<strong>10</strong>......................................................328<br />
IR-RDFMAG8........................................................328<br />
IR-RDFMAG8..........................................................16<br />
IR-VIPA-MINI-RHEO-35........................................324<br />
IR-VIPA-MINI-RHEO-35..........................................19<br />
IR-VIPA-MINI-RHEO-35..........................................16<br />
IR-VIPA1<strong>10</strong>............................................................321<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 341
342<br />
IR-VIPA27..............................................................321<br />
IR-VIPA57..............................................................321<br />
IR-VIPARH1<strong>10</strong>.......................................................322<br />
IR-VIPARH16........................................................322<br />
IR-VIPARH27........................................................322<br />
IR-VIPARH57........................................................322<br />
IR-VIPARHP150....................................................323<br />
IR-VIPARHP220....................................................323<br />
IR-VIPARHP40......................................................323<br />
IR-VIPARHP75......................................................323<br />
IR-VIPARHPRS485...............................................323<br />
IR-VIPARHPUI......................................................323<br />
IR-VIPARHX7........................................................322<br />
IR-VIPARK-BF-POM.............................................327<br />
IR-VIPARK-VK-POM.............................................327<br />
IR-VIPARS.............................................................322<br />
IR-VIPARS.............................................................321<br />
IR-VIPARWS.........................................................328<br />
IR-VIPARWV<strong>10</strong>0021.............................................328<br />
IR-VIPARWV<strong>10</strong>0029.............................................328<br />
IR-VIPARWV15019...............................................328<br />
IR-VIPARWV45020...............................................328<br />
IR-VIPARWV45028...............................................328<br />
IR-VIPASFG..........................................................328<br />
IR-VISCOTROL-FAN............................................326<br />
IR-VISCOTROL-FAN............................................325<br />
IR-VISCOTROL-MOT055.....................................325<br />
IR-VISCOTROL-MOT075.....................................326<br />
IR-VISCOTROL-MOT075.....................................325<br />
IR-VISCOTROL-MOT1<strong>10</strong>......................................326<br />
IR-VISCOTROL-MOT1<strong>10</strong>......................................325<br />
IR-VISCOTROL-MOT150.....................................325<br />
IR-VISCOTROL-MOT300.....................................325<br />
IR-VISCOTROL1<strong>10</strong>0.............................................325<br />
IR-VISCOTROL2200.............................................325<br />
IR-VISCOTROL350...............................................325<br />
IR-VISCOTROL350-RHEO...................................326<br />
IR-VISCOTROL550...............................................325<br />
IR-VISCOTROL550-RHEO...................................326<br />
IR-VISCOTROL750-RHEO...................................326<br />
IR-VPMONT2........................................................326<br />
IS-F-0000.P.X.P.01.CX..........................................242<br />
IS-F-0045.P.H.0.00.CX..........................................242<br />
IS-F-0045.P.X.P.01.DL..........................................241<br />
IS-F-0045.P.X.P.01.DL..........................................241<br />
IS-F-0045.P.X.P.01.DX..........................................241<br />
IS-F-0045.P.X.P.01.DX..........................................241<br />
IS-F-0045.S.B.P.01.XX..........................................242<br />
IS-F-0045.S.N.P.01.XX.........................................242<br />
IS-F-0045.T.H.0.00.DX..........................................241<br />
IS-F-0045.T.H.0.00.DX..........................................241<br />
IS-F-0045.T.H.P.01.DL..........................................241<br />
IS-F-0045.T.H.P.01.DX..........................................241<br />
IS-F-0045.T.H.P.01.XL..........................................242<br />
IS-F-0045.T.H.P.01.XX..........................................242<br />
IS-F-0045.T.N.0.00.DX..........................................241<br />
IS-F-0045.T.N.0.00.DX..........................................241<br />
IS-F-0045.T.N.P.01.DL..........................................241<br />
IS-F-0045.T.N.P.01.DX..........................................241<br />
IS-F-0045.T.N.P.01.XL..........................................242<br />
IS-F-0045.T.N.P.01.XX..........................................242<br />
IS-F-0045.X.X.X.00.CX.........................................242<br />
IS-F-0085.P.H.0.00.CX..........................................242<br />
IS-F-0085.P.H.P.01.CX..........................................242<br />
Order Codes<br />
IS-F-0085.P.X.P.01.DL..........................................241<br />
IS-F-0085.P.X.P.01.DL..........................................241<br />
IS-F-0085.P.X.P.01.DX..........................................241<br />
IS-F-0085.P.X.P.01.DX..........................................241<br />
IS-F-0085.S.B.P.01.XX..........................................242<br />
IS-F-0085.S.N.P.01.XX.........................................242<br />
IS-F-0085.T.H.0.00.DX..........................................241<br />
IS-F-0085.T.H.0.00.DX..........................................241<br />
IS-F-0085.T.H.P.01.DL..........................................241<br />
IS-F-0085.T.H.P.01.DX..........................................241<br />
IS-F-0085.T.H.P.01.XL..........................................242<br />
IS-F-0085.T.H.P.01.XX..........................................242<br />
IS-F-0085.T.N.0.00.DX..........................................241<br />
IS-F-0085.T.N.0.00.DX..........................................241<br />
IS-F-0085.T.N.P.01.DL..........................................241<br />
IS-F-0085.T.N.P.01.DX..........................................241<br />
IS-F-0085.T.N.P.01.XL..........................................242<br />
IS-F-0085.T.N.P.01.XX..........................................242<br />
IS-F-0085.X.X.X.00.CX.........................................242<br />
IS-F-0125.S.B.P.01.XX..........................................242<br />
IS-F-0125.S.N.P.01.XX.........................................242<br />
IS-F-0125.T.B.P.01.XX..........................................242<br />
IS-F-0125.T.N.P.01.XL..........................................242<br />
IS-F-6300.BA.CON.DC.XX...................................243<br />
IS-F-6700-DA-CON-DC........................................244<br />
IS-F-LABTUC........................................................243<br />
IS-F-S601-P2........................................................242<br />
IS-F-S601-P20......................................................242<br />
IS-F-S601-P40......................................................242<br />
IS-F-TDMMV-AK-F..................................................35<br />
IS-F-TDMMV-AK-I...................................................35<br />
IS-F-TDMtc-tb-sa..................................................245<br />
IS-F-TDMtc-tb-sa....................................................35<br />
IS-FM-L30 0,0.......................................................246<br />
IS-FM-L30C2I........................................................246<br />
IS-FM-L30C5.........................................................246<br />
IS-FM-M12............................................................248<br />
IS-FM-M12V1NI....................................................248<br />
IS-FM-M13............................................................248<br />
IS-FM-M13V1NI....................................................248<br />
IS-FM-M14............................................................248<br />
IS-FM-M14V1NI....................................................248<br />
IS-FV-GAS-DISP...................................................249<br />
IS-FV-GAS-IG.......................................................249<br />
IS-FV-GAS-IGEX...................................................249<br />
IS-FV-GAS-MAN...................................................249<br />
IS-FV-GAS-tc-au...................................................249<br />
IS-FV-GAS-THG....................................................249<br />
IS-FV-GAS-THS....................................................249<br />
IS-G-IND1..............................................................254<br />
IS-G-REFL1..........................................................254<br />
IS-L-FA-ea.............................................................236<br />
IS-M-FEU1............................................................254<br />
IS-MOLECULEEYE...............................................228<br />
IS-MOLECULEEYEMUX......................................228<br />
IS-P-A-025-ma-ea.................................................251<br />
IS-P-A-1,6-ma-ea..................................................251<br />
IS-P-A-2,5-ma-ea..................................................251<br />
IS-P-A-6-ma-ea.....................................................251<br />
IS-P-R-6-ma-ea.....................................................251<br />
IS-P-TUBE-sd.......................................................253<br />
IS-P-Z-AA..............................................................252<br />
IS-P-Z-AA..............................................................251<br />
IS-PARTICLEYE- 2D-l...........................................232<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
IS-PARTICLEYE- 3D-l-t........................................232<br />
IS-PARTICLEYE- WV...........................................232<br />
IS-PARTICLEYE-AA6...........................................232<br />
IS-PARTICLEYE-EEX...........................................232<br />
IS-PARTICLEYE-S- l.............................................232<br />
IS-PTOT-A-16-ea..................................................252<br />
IS-PTOT-R-16-ea..................................................252<br />
IS-T-NICRNI-d-l.....................................................250<br />
IS-T-PT<strong>10</strong>0 1/5-VA-d-l...........................................250<br />
IS-T-PT<strong>10</strong>0-1/1-VA -d-l..........................................250<br />
IS-T-PT<strong>10</strong>0-1/1-VA-d-l...........................................250<br />
IS-T-PT<strong>10</strong>0-1/<strong>10</strong>-VA-d-l.........................................250<br />
IS-T-PT<strong>10</strong>0-1/3-VA-d-l...........................................250<br />
IS-T-PT<strong>10</strong>003B.......................................................90<br />
IS-T-PT<strong>10</strong>015G.......................................................90<br />
IS-T-PTKAL.............................................................90<br />
IS-TRUB-O-ea.......................................................233<br />
IS-TRUB-ORF-ea..................................................234<br />
IS-W-GRAVICRANE.............................................267<br />
IS-W-GRAVICRANE.............................................207<br />
IS-W-GRAVIPLATE...............................................267<br />
IS-W-GRAVIPLATE...............................................207<br />
IS-W-GRAVISTAND..............................................267<br />
IS-W-GRAVISTAND..............................................207<br />
IS-W-KMZ<strong>10</strong>00......................................................255<br />
IS-W-KMZ<strong>10</strong>00D...................................................255<br />
IS-W-KMZ<strong>10</strong>00k....................................................255<br />
IS-W-KMZ<strong>10</strong>0k......................................................255<br />
IS-W-KMZ15000...................................................255<br />
IS-W-KMZ15000D.................................................255<br />
IS-W-KMZ200k......................................................255<br />
IS-W-KMZ3000......................................................255<br />
IS-W-KMZ30000...................................................255<br />
IS-W-KMZ30000D.................................................255<br />
IS-W-KMZ3000D...................................................255<br />
IS-W-KMZ500k......................................................255<br />
IS-W-KMZ50k........................................................255<br />
IS-W-KMZ7500......................................................255<br />
IS-W-KMZ7500D...................................................255<br />
IV-DRUMIN16/1......................................................16<br />
IV-MB-FK1-2-1,5-UNF-ea.....................................268<br />
IV-MB-FK1-2-1,5-UNF-ea.....................................267<br />
IV-MB-FK1-2-1,6-GMG1/8-ea...............................216<br />
IV-MB-FK1-3-1,6-GMG1/8-ea...............................216<br />
IV-MB-FK2-2-1,5-UNF-ea.....................................216<br />
IV-MB-FK2-2-nw-ma-ea........................................217<br />
IV-MB-FK2-3-1,5-UNF-ea.....................................216<br />
IV-MB-FK2-3-nw-ma-ea........................................217<br />
IV-MB-GM1-2-nw-ma-ea.......................................218<br />
IV-MB-UM1-2-3-ma-ea..........................................219<br />
IV-MB-UM1-3-3-ma-ea..........................................219<br />
IV-MB-UM2-2........................................................267<br />
IV-MB-UM2-2........................................................219<br />
IV-MB-UM2-PS......................................................267<br />
IV-MB-UM2-PS......................................................219<br />
IV-MP-ELBU1........................................................222<br />
IV-MP-ELBU2........................................................222<br />
IV-MP-UG1-2-6-ma-ea..........................................222<br />
IV-MP-UK1-2-0,8-ma-ea.......................................267<br />
IV-MP-UK1-2-0,8-ma-ea.......................................222<br />
IV-MP-UM1-2-2-ma-ea..........................................222<br />
IV-MP-UM2-2-4-ma-ea..........................................222<br />
IV-MW1-wa-ma-ea................................................223<br />
IV-MW2-wa-1/4.....................................................223<br />
Order Codes<br />
IV-PB-FG1-2-15-ma-ea.........................................219<br />
IV-PB-FG2-2-15-ma-ea.........................................219<br />
IV-PB-FG3-3-20-ma-ea.........................................219<br />
IV-PP-FG1-3-20-ma-ea.........................................222<br />
IV-PP-UG1-2-13-ma-ea.........................................222<br />
IV-PP-UX1-2-ma-ea-kv.........................................222<br />
IW- GRAVIPF15000..............................................207<br />
IW- GRAVIPF3000................................................207<br />
IW- GRAVIPF7000................................................207<br />
IW-572-35..............................................................208<br />
IW-572-49..............................................................208<br />
IW-GRAVIREAKW.................................................208<br />
IW-GRAVITS<strong>10</strong>00.................................................207<br />
IW-GRAVITS<strong>10</strong>00D...............................................206<br />
IW-GRAVITS15000...............................................206<br />
IW-GRAVITS15000D............................................206<br />
IW-GRAVITS3000.................................................207<br />
IW-GRAVITS3000.................................................206<br />
IW-GRAVITS30000...............................................206<br />
IW-GRAVITS30000D............................................206<br />
IW-GRAVITS3000D...............................................206<br />
IW-GRAVITS7500.................................................207<br />
IW-GRAVITS7500.................................................206<br />
IW-GRAVITS7500D...............................................206<br />
IW-LP4200S..........................................................209<br />
IW-ME414S...........................................................209<br />
IW-PLS 4000-2......................................................208<br />
IW-PLS 5<strong>10</strong>-3........................................................208<br />
IW-QKE 36K0.5.....................................................208<br />
L-SONSCHR-1......................................................212<br />
LB-LABBOX1B........................................................77<br />
LB-LABBOX2B........................................................78<br />
LB-LABMAN1B.......................................................80<br />
LB-LABMAN2B.......................................................81<br />
LG-LABBOX1..........................................................72<br />
LG-LABBOX2-1.......................................................73<br />
LG-LABBOX2-2.......................................................73<br />
LG-LABMAN1.........................................................74<br />
LK-LABBOX1K........................................................69<br />
LK-LABBOX2K-1.....................................................70<br />
LK-LABBOX2K-2.....................................................70<br />
LK-LABMAN1K.......................................................71<br />
LP-AAP8UI..............................................................94<br />
LP-AE4PT4P...........................................................91<br />
LP-AE4PT4PA.........................................................91<br />
LP-AEAP8I..............................................................95<br />
LP-AEAP8IA............................................................95<br />
LP-AEAP8U.............................................................95<br />
LP-AEAP8UA..........................................................95<br />
LP-AEP8..................................................................88<br />
LP-AEP8A...............................................................89<br />
LP-DAP8.................................................................98<br />
LP-DAP8A...............................................................99<br />
LP-DAP8T.............................................................<strong>10</strong>0<br />
LP-DE4DA4P........................................................<strong>10</strong>0<br />
LP-DE4DA4PA......................................................<strong>10</strong>1<br />
LP-DEP8.................................................................96<br />
LP-DEP8A...............................................................97<br />
LP-DMS4DA4PT...................................................267<br />
LP-DMS8.................................................................93<br />
LP-DMSP8............................................................267<br />
LP-LP-DA4HZ4PA.................................................<strong>10</strong>1<br />
LP-PEAP...............................................................<strong>10</strong>4<br />
LP-PEAPSK15......................................................<strong>10</strong>4<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 343
344<br />
LP-PEAPSK24......................................................<strong>10</strong>4<br />
LP-PHRED24..........................................................92<br />
LP-PHRED24B........................................................92<br />
LP-PTP8..................................................................89<br />
LP-PTPRP8...........................................................124<br />
LP-PTPRP8.............................................................90<br />
LP-SER99.............................................................<strong>10</strong>2<br />
LP-THP8..................................................................92<br />
LZ-AKLES1.............................................................93<br />
LZ-AKLES1.............................................................93<br />
LZ-AKLES1.............................................................92<br />
LZ-AKLES1.............................................................90<br />
LZ-AKLES1.............................................................89<br />
LZ-AKPH.................................................................92<br />
LZ-AKRS9.............................................................<strong>10</strong>2<br />
LZ-AKTUB.............................................................<strong>10</strong>1<br />
LZ-AKTUB.............................................................<strong>10</strong>1<br />
LZ-AKTUB.............................................................<strong>10</strong>0<br />
LZ-AKTUB...............................................................97<br />
LZ-AKTUB...............................................................96<br />
LZ-AKTUB...............................................................89<br />
LZ-AKTUB...............................................................88<br />
LZ-AKTUB ..............................................................95<br />
LZ-AKTUB ..............................................................94<br />
LZ-AKTUB ..............................................................93<br />
LZ-AKTUS.............................................................<strong>10</strong>1<br />
LZ-AKTUS.............................................................<strong>10</strong>0<br />
LZ-AKTUS.............................................................<strong>10</strong>0<br />
LZ-AKTUS...............................................................99<br />
LZ-AKTUS...............................................................98<br />
LZ-BEFW19.............................................................83<br />
LZ-GRIFFLU............................................................83<br />
LZ-GRIFFRO...........................................................83<br />
LZ-PR19Z3HE.........................................................82<br />
LZ-PR7....................................................................82<br />
LZ-PRx....................................................................82<br />
LZ-USTAT5M...........................................................82<br />
LZ-USTAT6..............................................................82<br />
LZ-USTAT7..............................................................82<br />
MB-AAB8UI...........................................................118<br />
MB-AEB16VP........................................................118<br />
MB-DAB8R............................................................119<br />
MB-DAB8T_0.5A...................................................120<br />
MB-DEB8...............................................................119<br />
MG-MSRBOX1......................................................117<br />
MG-MSRBOX2......................................................117<br />
MG-MSRBOX2s....................................................117<br />
MG-MSRMAN .......................................................115<br />
P-USV7O...............................................................137<br />
SA-GYRODAT.......................................................335<br />
SA-KALDAS3..........................................................33<br />
SA-KALDAS3..........................................................31<br />
SA-KALDAS3..........................................................29<br />
SA-P-LABDOS-DOMAS.......................................275<br />
SA-P-LABDOS-DOMASM....................................275<br />
SD-HIBUILDER ....................................................191<br />
SF-ANWTAB.........................................................179<br />
SF-ANWTAB.........................................................179<br />
SF-ANWTAB.........................................................178<br />
SF-ANWTAB.........................................................178<br />
SF-ANWTAB.........................................................178<br />
SF-ANWTAB.........................................................177<br />
SF-ANWTAB.........................................................177<br />
SF-ANWTAB.........................................................177<br />
Order Codes<br />
SF-ANWTAB.........................................................146<br />
SF-ANWTAB ........................................................189<br />
SF-AWL.................................................................146<br />
SF-AWL ................................................................188<br />
SF-AWLPLUS.......................................................188<br />
SF-AWLPLUS.......................................................146<br />
SF-DATLOG..........................................................179<br />
SF-DATLOG..........................................................179<br />
SF-DATLOG..........................................................178<br />
SF-DATLOG..........................................................178<br />
SF-DATLOG..........................................................178<br />
SF-DATLOG..........................................................177<br />
SF-DATLOG..........................................................177<br />
SF-DATLOG..........................................................177<br />
SF-DATLOG..........................................................146<br />
SF-DATLOG .........................................................189<br />
SF-HICON ............................................................186<br />
SF-HICONx...........................................................146<br />
SF-HITUNE...........................................................178<br />
SF-HITUNE...........................................................146<br />
SF-HITUNE ..........................................................185<br />
SF-HITUNE ..........................................................179<br />
SF-HITUNE ..........................................................179<br />
SF-NAMSER128...................................................189<br />
SF-NAMSER16.....................................................189<br />
SF-NAMSER32.....................................................189<br />
SF-NAMSER4.......................................................189<br />
SF-NAMSER4.......................................................179<br />
SF-NAMSER4.......................................................179<br />
SF-NAMSER4.......................................................178<br />
SF-NAMSER4.......................................................178<br />
SF-NAMSER4.......................................................178<br />
SF-NAMSER4.......................................................177<br />
SF-NAMSER4.......................................................177<br />
SF-NAMSER4.......................................................177<br />
SF-NAMSER64.....................................................189<br />
SF-NAMSER8.......................................................189<br />
SF-NAMSERxx.....................................................146<br />
SF-PID16...............................................................185<br />
SF-PID16 ..............................................................177<br />
SF-PID16 .............................................................179<br />
SF-PID24...............................................................185<br />
SF-PID32...............................................................185<br />
SF-PID4.................................................................177<br />
SF-PID4...................................................................16<br />
SF-PID4.....................................................................7<br />
SF-PID4 ................................................................185<br />
SF-PID4 ...............................................................178<br />
SF-PID4 ...............................................................178<br />
SF-PID8.................................................................185<br />
SF-PID8.................................................................177<br />
SF-PID8...................................................................31<br />
SF-PID8...................................................................29<br />
SF-PID8.....................................................................9<br />
SF-PID8 ...............................................................179<br />
SF-PID8 ...............................................................178<br />
SF-PIDxx...............................................................146<br />
SF-PNKMSR.........................................................146<br />
SL-ACTIONTRACK...............................................163<br />
SL-ACTIONTRACK...............................................145<br />
SL-ALRRUF..........................................................158<br />
SL-ALRRUF..........................................................145<br />
SL-ANWINT..........................................................174<br />
SL-ANWINT..........................................................145<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
SL-BENRECH.......................................................173<br />
SL-BENRECH.......................................................145<br />
SL-BERICHT.........................................................165<br />
SL-BERICHT.........................................................149<br />
SL-BERICHT.........................................................145<br />
SL-BIBRILK...........................................................192<br />
SL-BIBRILK...........................................................156<br />
SL-BIBRILK...........................................................146<br />
SL-CLONLV ..........................................................145<br />
SL-DESIGN...........................................................152<br />
SL-DESIGN...........................................................145<br />
SL-DESIGNL.........................................................152<br />
SL-DESIGNL.........................................................146<br />
SL-DIAPROT.........................................................161<br />
SL-DIAPROT.........................................................145<br />
SL-EASYBATCH...................................................163<br />
SL-EASYBATCH...................................................145<br />
SL-EMLRUF..........................................................159<br />
SL-EMLRUF..........................................................145<br />
SL-EXPORT..........................................................172<br />
SL-EXPORT..........................................................145<br />
SL-FREMDPNK....................................................174<br />
SL-FREMDPNK....................................................174<br />
SL-FREMDPNK....................................................146<br />
SL-GOPBEFUEL...................................................167<br />
SL-GOPBIB...........................................................166<br />
SL-GOPBIB...........................................................165<br />
SL-GOPBIB...........................................................146<br />
SL-GOPBIBL.........................................................166<br />
SL-GOPBIBL.........................................................165<br />
SL-GOPDEST.......................................................167<br />
SL-GOPDOSI........................................................167<br />
SL-GOPDOSIGRAVI1...........................................267<br />
SL-GOPDOSIGRAVI1...........................................167<br />
SL-GOPDPWERT.................................................167<br />
SL-GOPDRUCK....................................................167<br />
SL-GOPDRUCKHALTEN......................................167<br />
SL-GOPEINWIEG.................................................167<br />
SL-GOPEND.........................................................167<br />
SL-GOPGRAVITARI..............................................267<br />
SL-GOPGRAVITARI..............................................167<br />
SL-GOPINERT......................................................167<br />
SL-GOPINERTHERST..........................................167<br />
SL-GOPKALOHEIZ...............................................167<br />
SL-GOPKALOONL ...............................................167<br />
SL-GOPKONTIDOS..............................................167<br />
SL-GOPMENGENDOS.........................................167<br />
SL-GOPPHREGELUNG.......................................167<br />
SL-GOPPROGRAMM...........................................167<br />
SL-GOPRATENDOS.............................................167<br />
SL-GOPREKTIF....................................................167<br />
SL-GOPRUECKDEST..........................................167<br />
SL-GOPRUEHR....................................................167<br />
SL-GOPSIEDEP...................................................167<br />
SL-GOPSTART.....................................................168<br />
SL-GOPSTOSSDOS.............................................168<br />
SL-GOPTEMP.......................................................168<br />
SL-GOPTEMPHALTEN.........................................168<br />
SL-GOPVAKHALTEN............................................168<br />
SL-GOPVAKU.......................................................168<br />
SL-GOPWAAGETARI...........................................168<br />
SL-GOPWARTET..................................................168<br />
SL-GOPWARTEZ..................................................168<br />
SL-GOPWBEDIENER...........................................168<br />
Order Codes<br />
SL-GOPWBEDINGUNG.......................................168<br />
SL-GOPWIEDERH................................................168<br />
SL-HIBATCH.........................................................165<br />
SL-HIBATCH.........................................................145<br />
SL-HIBATCHAP....................................................165<br />
SL-HIBATCHL.......................................................165<br />
SL-HIBATCHL.......................................................146<br />
SL-HIBATCHRT....................................................165<br />
SL-HILIMS.............................................................165<br />
SL-HILIMS.............................................................145<br />
SL-HILIMSL...........................................................165<br />
SL-HILIMSL...........................................................146<br />
SL-HILIMSSQL.....................................................145<br />
SL-HITEXT............................................................160<br />
SL-HITEXT............................................................145<br />
SL-HITEXTL..........................................................160<br />
SL-HITEXTL..........................................................146<br />
SL-JOURNAL........................................................171<br />
SL-JOURNAL........................................................165<br />
SL-JOURNAL........................................................145<br />
SL-KALDAS3........................................................145<br />
SL-LABCAM..........................................................158<br />
SL-LABCAM..........................................................145<br />
SL-LABVIPBAT.....................................................179<br />
SL-LABVIPBAT.......................................................71<br />
SL-LABVIPBAT.......................................................16<br />
SL-LABVIPBATE.....................................................31<br />
SL-LABVIPBATE.....................................................29<br />
SL-LABVIPBATE ..................................................178<br />
SL-LABVIPBATE ......................................................9<br />
SL-LABVIPBATL.....................................................70<br />
SL-LABVIPBATL.......................................................7<br />
SL-LABVIPBATL .................................................178<br />
SL-LABVIPBATP ..................................................179<br />
SL-LABVIPEASY .................................................178<br />
SL-LABVIPKON....................................................177<br />
SL-LABVIPKON......................................................71<br />
SL-LABVIPKONL..................................................177<br />
SL-LABVIPKONL....................................................70<br />
SL-LABVIPKONP..................................................177<br />
SL-LABVIS............................................................147<br />
SL-LABVIS..............................................................69<br />
SL-LABVOICE.......................................................145<br />
SL-LIQUIM............................................................316<br />
SL-LIQUIML..........................................................316<br />
SL-MICROBIB ......................................................146<br />
SL-MODBIBALR...................................................155<br />
SL-MODBIBALR...................................................155<br />
SL-MODBIBALR...................................................146<br />
SL-MODBIBALRL.................................................155<br />
SL-MODBIBALRL.................................................155<br />
SL-MULTIBATCH..................................................169<br />
SL-MULTIBATCH..................................................145<br />
SL-MULTIBATCH....................................................16<br />
SL-MULTIPROJ....................................................173<br />
SL-MULTIPROJ....................................................145<br />
SL-ONLGRA.........................................................150<br />
SL-ONLGRA.........................................................145<br />
SL-ONLGRAL.......................................................150<br />
SL-ONLGRAL.......................................................146<br />
SL-PNKDDE..........................................................174<br />
SL-PNKDDE..........................................................146<br />
SL-PNKLASENTEC..............................................174<br />
SL-PNKLASENTEC..............................................146<br />
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346<br />
SL-PNKMBUSSER...............................................146<br />
SL-PNKMODBUS.................................................174<br />
SL-PNKMTRx........................................................174<br />
SL-PNKMTRx........................................................146<br />
SL-PNKNAMSERA...............................................189<br />
SL-PNKOPC.........................................................174<br />
SL-PNKOPC.........................................................146<br />
SL-PNKPERF........................................................174<br />
SL-PNKPERF........................................................146<br />
SL-PNKSIM...........................................................145<br />
SL-PNKSPS..........................................................174<br />
SL-PNKSPS..........................................................146<br />
SL-PROJMOD.......................................................155<br />
SL-PROJMOD ......................................................145<br />
SL-REZGEN..........................................................168<br />
SL-RICAD..............................................................192<br />
SL-RIEDIT.............................................................156<br />
SL-RIEDIT.............................................................145<br />
SL-RIEDITL...........................................................156<br />
SL-RIEDITL...........................................................146<br />
SL-SCHANA..........................................................148<br />
SL-SCHANA..........................................................145<br />
SL-SCHANAL........................................................148<br />
SL-SCHANAL........................................................146<br />
SL-SCHERE..........................................................165<br />
SL-SCHERE..........................................................149<br />
SL-SCHERE..........................................................145<br />
SL-SCHEREL........................................................149<br />
SL-SCHEREL........................................................146<br />
SL-SCHPHA..........................................................165<br />
SL-SCHPHA..........................................................149<br />
SL-SCHPHA..........................................................145<br />
SL-SCHPHAL........................................................149<br />
SL-SCHPHAL........................................................146<br />
SL-SELFIL.............................................................172<br />
SL-SELFIL.............................................................145<br />
SL-SWITCHER ....................................................145<br />
SL-TELES.............................................................175<br />
SL-UEBMEL..........................................................157<br />
SL-UEBMEL..........................................................145<br />
SL-VISCOGRAPH.................................................331<br />
SL-VISCOGRAPHAI.............................................331<br />
SL-VISCOGRAPHPT............................................331<br />
SL-WEBVIS...........................................................173<br />
SL-WEBVIS...........................................................145<br />
SL-WEBVISL.........................................................173<br />
SL-WEBVISL.........................................................146<br />
SP-RQFEED-AC.....................................................52<br />
VA-FESTBETT........................................................53<br />
VA-HIFERM-FCU....................................................44<br />
VA-OMNIFERM-AIRPUM........................................42<br />
VA-OMNIFERM-BGR..............................................42<br />
VA-OMNIFERM-CHILL...........................................42<br />
VA-OMNIFERM-COOL...........................................42<br />
VA-OMNIFERM-ETOH............................................42<br />
VA-OMNIFERM-FE-<strong>10</strong>00........................................42<br />
VA-OMNIFERM-FE-2000........................................42<br />
VA-OMNIFERM-FE-250..........................................42<br />
VA-OMNIFERM-FE-600..........................................42<br />
VA-OMNIFERM-FOAM...........................................42<br />
VA-OMNIFERM-FOLE............................................42<br />
VA-OMNIFERM-GAS1............................................42<br />
VA-OMNIFERM-GASMF.........................................42<br />
VA-OMNIFERM-GASMF2.......................................42<br />
Order Codes<br />
VA-OMNIFERM-GASMF4MUX...............................42<br />
VA-OMNIFERM-LEV...............................................42<br />
VA-OMNIFERM-REDOX.........................................42<br />
VA-OMNIFERM-RQFEED.......................................42<br />
VA-RAMOSCON8...................................................40<br />
VA-RAMOSCTR......................................................39<br />
VA-RAMOSFI1........................................................39<br />
VA-RAMOSFTT8.....................................................40<br />
VA-RAMOSINKSHA................................................39<br />
VA-RAMOSMK250..................................................39<br />
VA-RAMOSMKX......................................................39<br />
VA-RAMOSOTR......................................................39<br />
VA-RAMOSTKS4....................................................39<br />
VA-RAMOSTKSE....................................................39<br />
VL-BAVA-GKB.......................................................2<strong>10</strong><br />
VL-BAVA-HWS<strong>10</strong>..................................................2<strong>10</strong><br />
VL-BAVA-HWS20..................................................2<strong>10</strong><br />
VL-BAVA-HWST....................................................2<strong>10</strong><br />
VL-BAVA-NOR<strong>10</strong>..................................................2<strong>10</strong><br />
VL-BAVA-NOR15..................................................2<strong>10</strong><br />
VL-BAVA-NOR25..................................................2<strong>10</strong><br />
VL-BAVM-GKB......................................................2<strong>10</strong><br />
VL-EDDEST............................................................21<br />
VL-EDDOSFL..........................................................21<br />
VL-EDDOSPU.........................................................21<br />
VL-EDSIM...............................................................21<br />
VL-EDUQUIP..........................................................21<br />
VL-EDVAK...............................................................21<br />
VL-HICLAVE-ABKPNK1..........................................12<br />
VL-HICLAVE-ABKPNK2..........................................12<br />
VL-HICLAVE-ABKPNK4..........................................12<br />
VL-HICLAVE-COOLP..............................................12<br />
VL-HICLAVE-GRAVI150.........................................12<br />
VL-HICLAVE-HEABAN-vol......................................12<br />
VL-HICLAVE-HYDR................................................12<br />
VL-HICLAVE-MAGHEAT.........................................12<br />
VL-HICLAVE-SC-n..................................................12<br />
VL-HICLAVE-STIRR-20..........................................12<br />
VL-HICLAVE-STIRR-50..........................................12<br />
VL-HICLAVE-ws-vol................................................12<br />
VL-KB-FK2-UM1...................................................217<br />
VL-KB-MB-FK1.....................................................268<br />
VL-KB-MB-FK1.....................................................267<br />
VL-KB-MB-FK1.....................................................216<br />
VL-KB-MB-GM1....................................................218<br />
VL-KB-MB-UM2....................................................267<br />
VL-KB-MB-UM2....................................................219<br />
VL-LABKIT-SP........................................................22<br />
VL-LABKIT-SP-FOCON..........................................22<br />
VL-LABKIT-SP-PHCON..........................................22<br />
VL-LABKITALR1........................................................7<br />
VL-LABKITALR2........................................................9<br />
VL-LABKITALR2-AWE..............................................9<br />
VL-LABKITALR2-RFT...............................................9<br />
VL-LABKITED.........................................................21<br />
VL-LABKITRCB1.....................................................31<br />
VL-LABKITRCF1.....................................................29<br />
VL-LABKITRCMDM................................................31<br />
VL-LABKITRCONLB...............................................31<br />
VL-LABKITRCONLF...............................................29<br />
VL-MINILAB-BU......................................................19<br />
VL-MINILAB-GRV125.............................................19<br />
VL-MINILAB-GRV250.............................................19<br />
VL-MINILAB-GRV75...............................................19<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
VL-MULTILAB-ABKPNK1.......................................16<br />
VL-MULTILAB-ABKPNK2.......................................16<br />
VL-MULTILAB-ABKPNK4.......................................16<br />
VL-MULTILAB-ABKPNK6.......................................16<br />
VL-MULTILAB-ABKPNK8.......................................16<br />
VL-MULTILAB-BU...................................................16<br />
VL-MULTILAB-CHILL-20.........................................16<br />
VL-MULTILAB-CHILL-40.........................................16<br />
VL-MULTILAB-CHILL-60.........................................16<br />
VL-MULTILAB-DEST..............................................16<br />
VL-MULTILAB-GRAVI500ml...................................16<br />
VL-MULTILAB-GRV250..........................................16<br />
VL-MULTILAB-GRV400..........................................16<br />
VL-MULTILAB-INERT.............................................16<br />
VL-MULTILAB-REKT ..............................................16<br />
VL-MULTILAB-RFC ................................................16<br />
VL-MULTILAB-VAKU...............................................16<br />
VL-SOLIDOS-BIN.................................................2<strong>10</strong><br />
W-GRAVIPF30000................................................207<br />
ZH-ALFADOS........................................................338<br />
ZH-AUTOSAM.......................................................338<br />
ZH-GRAVIDOS......................................................338<br />
ZH-GYRODAT ......................................................338<br />
ZH-HIBUILDER ....................................................338<br />
ZH-HICON ............................................................338<br />
ZH-KALDAS .........................................................338<br />
ZH-LABDOS..........................................................338<br />
ZH-LABVIS ...........................................................338<br />
ZH-RAMOS ..........................................................338<br />
ZH-REGLER ........................................................338<br />
ZH-SOLIDOS .......................................................338<br />
ZH-VISCOPAKT ...................................................338<br />
ZK-HM-HI01-OD-XA-I-01......................................212<br />
ZK-IT-HI01-BS-R2-I-03.........................................304<br />
ZK-IT-HI01-BS-R2-I-03.........................................283<br />
ZK-IT-HI01-BS-R2-I-03.........................................282<br />
ZK-IT-HI01-BS-R2-I-03.........................................281<br />
Order Codes<br />
ZK-IT-HI01-BS-R2-I-03.........................................280<br />
ZK-IT-HI01-BS-R2-I-03.........................................279<br />
ZK-LAB-HI01-IA-IA-O-01 .......................................89<br />
ZK-LAB-HI01-IA-IA-O-02........................................89<br />
ZK-LAB-HI01-IA-IP-O-01........................................89<br />
ZK-LAB-HI01-IA-IP-O-01........................................88<br />
ZK-LAB-HI01-IA-UA-O-01.......................................89<br />
ZK-LAB-HI01-IA-UP-O-01.......................................89<br />
ZK-LAB-HI01-IA-UP-O-01.......................................88<br />
ZK-LAB-HI06-OD-XX-I-01.....................................128<br />
ZK-LAB-HI99-IA-XA-Y-0.1.....................................254<br />
ZK-P-HI36-BS-R2-I-01..........................................275<br />
ZK-P-HI36-BS-R2-I-01..........................................274<br />
ZK-P-HI36-BS-R2-I-02..........................................275<br />
ZK-P-HI36-BS-R2-I-02..........................................274<br />
ZK-P-HI36-BS-R4-I-01..........................................275<br />
ZK-P-HI36-BS-R4-I-01..........................................274<br />
ZK-P-HI36-BS-R4-I-02..........................................275<br />
ZK-P-HI36-BS-R4-I-02..........................................274<br />
ZK-P-TL02-BS-R2-I-01.........................................289<br />
ZK-P-VB01-BS-R2-I-01.........................................300<br />
ZK-R-HI02-BA-IP-Y-02..........................................326<br />
ZK-R-HI02-BA-UP-Y-03........................................326<br />
ZK-R-HI02-BS-R2-I-01..........................................326<br />
ZK-R-HI30-BK-IX-Y-01..........................................325<br />
ZK-R-HI30-BS-R4-I-01..........................................325<br />
ZK-R-HI31-BK-IA-Y-01..........................................326<br />
ZK-R-HI31-BK-IP-Y-01..........................................326<br />
ZK-SF-KM01-IA-IA-I-01.........................................245<br />
ZK-SF-KM01-ID-XA-I-01 ......................................245<br />
ZK-SFV-RI01-ID-XX-I-01......................................249<br />
ZK-W-KE04-BS-R2-I-02........................................208<br />
ZK-W-KE06-BS-R2-I-01........................................208<br />
ZK-W-SA01-BS-R2-I-03........................................209<br />
ZK-W-SA01-BS-R2-I-03........................................209<br />
ZK-X-HI05-IA-IA-O-01...........................................131<br />
ZK-X-HW01-OD-XA-I-01.......................................212<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 347
348<br />
Table of Content<br />
New in this Edition.............................................................................................................................................4<br />
Automatic Laboratory Reactor Systems..........................................................................................................5<br />
Standard Laboratory Reactor Systems..........................................................................................................................6<br />
Parallel Reactor Systems............................................................................................................................................13<br />
LabKit- Small Reactor Systems for Education..........................................................................................................20<br />
Automated Laboratory Clarification Unit .....................................................................................................................22<br />
Modular Micro-Reaction Technology............................................................................................................................23<br />
Reaction Calorimetry.......................................................................................................................................26<br />
Reaction Calorimeters.................................................................................................................................................27<br />
Calorimetry Evaluation Program KalDas.................................................................................................................32<br />
Components for Reaction Calorimetry.........................................................................................................................34<br />
Fermentation Technology...............................................................................................................................36<br />
RAMOS® Bioprocess Optimisation in Shaking Flasks ...............................................................................................37<br />
Feeding and Sample Drawing in Shaking Flasks ........................................................................................................40<br />
OmniFerm® - Mini Fermentation System....................................................................................................................41<br />
HiFerm-FCU Customer-specific Fermenter Control Systems .................................................................................43<br />
Gmix – Gas Mixing Device.......................................................................................................................................45<br />
AlcoTect Alcohol Probe ...........................................................................................................................................47<br />
OxyTect Optical Dissolved Oxygen Probe ...............................................................................................................48<br />
Autoclavable pH-Probe ...............................................................................................................................................48<br />
HiSense Emission Analysis System ........................................................................................................................49<br />
RQFeed Feeding Algorithm .....................................................................................................................................52<br />
Packed Bed Reactor ...................................................................................................................................................53<br />
Laboratory Automation Hardware..................................................................................................................54<br />
LabManager®-System.................................................................................................................................................55<br />
MSRmanager-System............................................................................................................................................112<br />
Interface Cards..........................................................................................................................................................121<br />
PI Additional Devices ................................................................................................................................................128<br />
Display and Operating Elements ..............................................................................................................................135<br />
Laboratory Automation Software.................................................................................................................141<br />
LabVision®................................................................................................................................................................142<br />
HiLIMS Laboratory Information Management-System...........................................................................................180<br />
PI-Firmware-Modules................................................................................................................................................184<br />
HiBuilder Data Evaluation and Presentation..........................................................................................................190<br />
RI-CAD the CAD-Software for P&ID-flow diagrams...............................................................................................192<br />
Plant Construction and Miniplant Technology............................................................................................193<br />
LabKit Custom Reaction Equipment ....................................................................................................................198<br />
Custom Parallel Reactor System...............................................................................................................................200<br />
Custom Reaction Calorimeters .................................................................................................................................201<br />
Formulation and Handling Stations ...........................................................................................................................203<br />
Equipment and Components........................................................................................................................205<br />
Laboratory Scales......................................................................................................................................................206<br />
Electrical Base Discharge Valves ............................................................................................................................2<strong>10</strong><br />
Automatic Liquid Phase Separation ..........................................................................................................................211<br />
Glass Components ...................................................................................................................................................212<br />
Low Pulsation Total Evaporator ................................................................................................................................213<br />
Valves and Stop-Cocks ............................................................................................................................................214<br />
Process Analytics and Sensors....................................................................................................................224<br />
30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor
Table of Content<br />
MoleculeEye® ATR-FTIR-Spectroscopy....................................................................................................................225<br />
ParticleEye Particle Sizer.......................................................................................................................................229<br />
Turbidity Probe .........................................................................................................................................................233<br />
Fibre-Optic Submersible Reflection Probes ..............................................................................................................234<br />
Phase boundary Detector .........................................................................................................................................235<br />
Level Sensor..............................................................................................................................................................236<br />
Teflon® Flow Sensors ..............................................................................................................................................237<br />
Turbine Flow Sensor for Heat carrier Oil....................................................................................................................244<br />
Thermal Mass Flowmeters and Controllers ..............................................................................................................245<br />
Coriolis Mass Flowmeters and Controllers ...............................................................................................................247<br />
Laboratory Gas Counter............................................................................................................................................248<br />
Temperature Sensors ...............................................................................................................................................250<br />
Pressure Transmitters ...............................................................................................................................................251<br />
Hose Pressure Transmitter........................................................................................................................................253<br />
Humidity Sensors .....................................................................................................................................................254<br />
Distance and Rotational Speed Measurement..........................................................................................................254<br />
Weight Measuring and Load Cells ...........................................................................................................................255<br />
Monitors.....................................................................................................................................................................256<br />
Dosing Systems and Pumps.........................................................................................................................263<br />
Controlled Dropping Funnel GraviDos®....................................................................................................................264<br />
Controlled Dropping Funnel AlfaDos......................................................................................................................268<br />
Pumps, dosing pumps...............................................................................................................................................269<br />
Multi-Channel Dosing Systems .................................................................................................................................297<br />
Vacuum pumps..........................................................................................................................................................298<br />
Solid Matter Dosing System......................................................................................................................................301<br />
Liquid Handling and Autosampler................................................................................................................305<br />
Sample Drawing Systems and Pipetting Robots........................................................................................................306<br />
Stirring and Dispersing.................................................................................................................................319<br />
Measuring Stirrer ViscoPakt®....................................................................................................................................320<br />
ViscoTrol Control Unit for Three-Phase Stirrer Drive ............................................................................................325<br />
ViscoGraph – Automation of Stirring Tests ...........................................................................................................331<br />
Dispersing and Homogenising ..................................................................................................................................332<br />
Services..........................................................................................................................................................333<br />
<strong>HiTec</strong> <strong>Zang</strong> - Your competent Project Partner !..........................................................................................................334<br />
Customised Application Programs ............................................................................................................................335<br />
Seminars and Training ............................................................................................................................................336<br />
<strong>Main</strong>tenance Contracts ...........................................................................................................................................337<br />
Product Manuals ......................................................................................................................................................338<br />
<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 349