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HiTec Zang GmbH -- Main Catalogue 2009/10

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<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> • Ebertstrasse 30-32 • 52134 Herzogenrath • Germany<br />

General Office: +49 (0) 24 07 / 9<strong>10</strong> <strong>10</strong>0 • Fax: +49 (0) 2407 / 9<strong>10</strong> <strong>10</strong>99 • Internet: www.hitec-zang.com


Usage notes<br />

The informations within this catalog kann be reached via these indexes:<br />

Table of content 348<br />

Order codes 339<br />

To make the selection and combination of needed components easy, we assembled a couple of turnkey<br />

solutions and packages which are suitable for default applications:<br />

Basic automation systems 72<br />

Software packages 176<br />

Turnkey laboratory/minplant system 6<br />

Turnkey reaction calorimetery 28<br />

Parallel Reactor Systems 14<br />

Reactor Systems for Education 20<br />

Furthermore you will find overviews as charts for the following areas:<br />

Which signal type accords to which device? 83<br />

Which Modules for which Signal Type? 86<br />

Cables for Instrumentation <strong>10</strong>7<br />

Driver Programs for Laboratory Device Interfaces 1<strong>10</strong><br />

Which Proportional Valve for which Application? 220<br />

Which Pump for which Application? 269<br />

Which Stirrer Blade for which Application? 329<br />

If you notify us of your project details we will be happy to prepare the required components for you.<br />

To reach us directly:<br />

Department Phone +49(0)2407/9<strong>10</strong> - E-Mail<br />

Information -<strong>10</strong>12 info@hitec-zang.de<br />

Sales -<strong>10</strong><strong>10</strong> sales@hitec-zang.de<br />

Service -<strong>10</strong>26 service@hitec-zang.de<br />

Software -<strong>10</strong>17 software@hitec-zang.de<br />

Hardware -<strong>10</strong>14 hardware@hitec-zang.de<br />

Subject to technical changes, errors and misprints<br />

Windows 2000, Windows XP, Windows Vista and Teflon are registred trademarks.<br />

© <strong>2009</strong> <strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong><br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 3


4<br />

New in this Edition<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Here you will find:<br />

Automatic Laboratory Reator Systems<br />

� Standard LabKit Laboratory Reactor Systems<br />

� HiClave high-pressure autoclaves<br />

� MulitLab Parallel Reactor Systems<br />

� LabKit-ed Small Reactor Systems for Training Purposes<br />

� Laboratory Clarification Unit<br />

� Microreaction Technology<br />

Note:<br />

Custom made plants can be found in the chapter „Plant Construction and Miniplant Technology“.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 5<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


6<br />

Automatic Laboratory Reactor Systems<br />

Standard Laboratory Reactor Systems<br />

Automated laboratory reaction systems are an<br />

absolute necessity for today's product and process<br />

development and optimisation. Due to the much<br />

more intensive utilisation of the laboratory resources<br />

and the relief of the laboratory staff from routine<br />

activities, they pay off very quickly. They are a save<br />

way to achieve maximum reproducibility as well as<br />

an increase in quality and to gain new knowledge.<br />

Conventional laboratory reactor automation<br />

systems are limited to simple syntheses and are<br />

therefore no longer able to meet today's<br />

requirements.<br />

The fully-automateded <strong>HiTec</strong> <strong>Zang</strong> laboratory<br />

reactor systems are available as single and parallel<br />

reactor plants. Apart from the standard<br />

configurations, you can choose the set-up of the<br />

plant which accords to your demands from our<br />

LabKit program.<br />

Advantages:<br />

� easy to handle open system<br />

� NAMUR-conform automation with LABmanager/LabVision/HiBatch/HiLIMS<br />

� continuously expandable<br />

� space saving installation<br />

� electrically sinkable reactor vessel<br />

� optimal usage of the laboratory‘s capacity by<br />

operating 24 hours<br />

� best reproducibility<br />

� increase in quality<br />

� relief from routine jobs<br />

� reduction of the risk of accidents<br />

� GLP-compliant documentation<br />

� accessible via network, e.g. from the office<br />

� remote maintenance (dial-up by customer)<br />

Last fine-tuning before delivery<br />

<strong>HiTec</strong> <strong>Zang</strong> ALR-Systems are suited for the<br />

� Development of products and procedures<br />

� Optimisation of procedures<br />

� Safety-related tests<br />

� Scale-Up tests<br />

� Reaction calorimetry etc.<br />

The assembly of a laboratory reactor system out of<br />

individual components, e.g. out of a pH-controller, a<br />

dosing control, a vacuum controller, data collection,<br />

a control element, etc. used to be considered the<br />

best possible assembly. The capacity limits of such a<br />

conventional assembly are clearly demonstrated by<br />

LabKit due to its NAMUR-conform automation<br />

based on the LAB Manager System.<br />

Sophisticated details, such as the lowerable reactor<br />

tank, facilitate work.<br />

Options, Extensions<br />

Sensors for filling level, opacity, flow, pH, redox etc.,<br />

coupling of analysers etc., out of the chapter<br />

“Process Analytics and Sensors”, in-situ analytics,<br />

coupled multiple reactor systems, customer-specific<br />

machines out of the chapter “Customised Equipment<br />

and Miniplants” – the offered possibilities are<br />

virtually limitless.<br />

Standard systems<br />

The following depicted standard systems LabKitalr1,<br />

LabKit-alr2, LabKit-rcf, LabKit-rcb, LabKit-ed,<br />

and HiClave are complete, ready-to-use Automatic<br />

Laboratory Reactor Systems (ALR). They are suited<br />

for deployment in laboratories, pilot plants and miniplants.<br />

They can be aligned according to spacial<br />

conditions and upgraded by auxiliary modules.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Automatic Laboratory Reactor Systems<br />

LabKit-alr1 Standard-ALR-System<br />

Automatic lab reactor system in the basis version.<br />

Suitable for syntheses in a temperature range<br />

reaching from -<strong>10</strong> to +130 °C with reflux distillation.<br />

The system can be expanded with components from<br />

the LabKit-Construction Systems.<br />

Specification<br />

LabKit-alr1 ALR-standard system<br />

Rack Square section anodised aluminium profile.<br />

Reactor 1 litre plane ground container DN<strong>10</strong>0, cylindrical with heating jacket and manual PTFE<br />

base drain.<br />

Plane ground cover with centre neck NS29 for stirrer, side necks 2xNS29 slanted and<br />

1xNS29 straight, Seal DN120 Silicon/FEP, plane ground connector.<br />

Stirrer ViscoPakt-35 torque measuring stirrer, rotational speed 60..800 rpm, maximum torsion<br />

35 Ncm, including the optional RS232 interface.<br />

Accessories: light and high-strength stirrer coupling made of POM, standard agitator<br />

Heating/Cooling<br />

System<br />

closure, glass propeller stirrer.<br />

Heating/ cooling thermostat, working temperature range -25..150 °C in jacket, heating<br />

output 1 kW, refrigerating capacity 0.21 kW at 0 °C.<br />

Accessories: isolated heating tubes, heating connection adaptors, wide range<br />

tempering oil -40..165 °C.<br />

Dosing System A GraviDos Dosing System for liquids (regulated dropping funnel), 500 ml receiver<br />

tank, dosing valve (ETFE/Kalrez) controlled gravimetrically.<br />

Reflux cooling Intensive reflux cooler made of borosilicate glass, 250 mm long, NS29/32,<br />

Shutting valve for cooling water.<br />

Ventilation Air valve PVDF/Kalrez).<br />

Sensors Temperature sensor: Reactor internal temperature, thermostat bath temperature.<br />

Automation LabBox 1 with the following interfaces: 4 Pt<strong>10</strong>0 temperature measurement inputs, 4<br />

analogue inputs (current and voltage), 8 digital outputs, Sensor-/Actor power supply<br />

24 V 2.5 A, 2 RS232 interfaces.<br />

User PC : 1 CG-ABK1 <strong>HiTec</strong> display and control elements with premium 20“ TFT<br />

monitor.<br />

Materials <strong>Main</strong>ly borosilicate glass, PFA, PTFE, ETFE, PVDF. Seals in contact with media made<br />

of Kalrez, high-grade steel material 1.4571 (modifications possible).<br />

Order Code Description<br />

VL-LABKITALR1 Automatic Laboratory Reactor System, Basic Design<br />

Recommended software package<br />

Order Code Description<br />

SL-LABVIPBATL Software Package for LabBox1 and 2 to control small Batch Processes<br />

SF-PID4 Controller module with 4 PID- and application oriented controllers<br />

Recommended datapoint amount: <strong>10</strong>0<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 7<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


8<br />

Automatic Laboratory Reactor Systems<br />

LabKit-alr2 Standard-ALR-System<br />

Automatic Lab Reactor System in extended<br />

configuration. Suitable for syntheses in the<br />

temperature range from -20 to +180 °C with reflux<br />

distillation via programmable reflux separators.<br />

The system can be expanded with components from<br />

the LabKit-Construction Systems.<br />

Specification<br />

LabKit-alr2 ALR-Standard System with optional Modules<br />

Rack Square anodised aluminium profile, electrical fixture for lowering the reactor vessel,<br />

catch pan made of high-grade steel.<br />

Reactor 2 litre reactor with double jacket DN150, Duran glass, PTFE base drain with<br />

integrated PT<strong>10</strong>0 sensor, plane ground cover, seals Silicon/FEP, plane ground<br />

connector<br />

Stirrer Torque measuring stirrer ViscoPakt-rheo-57, rotational speed 50..2000 rpm,<br />

maximum torsion 57 Ncm, including the optional RS232 interface<br />

Accessories: light and high-strength stirrer coupling made of POM, standard agitator<br />

closure, glass propeller stirrer<br />

Heating/Cooling<br />

System<br />

Heating/cooling thermostat especially for tempering of external systems, working<br />

temperature range -40..200 °C in the jacket, heating output 1.5/3 kW, cooling<br />

capacity 0.7 kW at 0 °C<br />

Accessories: isolated heating tubes, heating connection adaptors, wide range<br />

tempering oil -90..200 °C<br />

Vacuum Laboratory vacuum system with chemical resistant vacuum pump < 8 mbar abs.,<br />

volume flow rate 1 m³/h, suction side separator, pressure side intensive cooler, safety<br />

valve<br />

Reflux Cooling Intensive reflux cooler out of borosilicate glass, 250 mm long, NS29/32<br />

Shutting valve for the cooling<br />

Monitoring of cooling water with floating-element meter<br />

Distillation distillate collecting scales, instrument read-out 0.01 g, weighing range 15<strong>10</strong> g<br />

2/2- way stop cock to shut off distillate collecting container and the pressure<br />

compensation.<br />

Optional: Glass reflux separator with vacuum jacket, silver-plated with viewing<br />

window, NSH+K 29/32 with PT<strong>10</strong>0 connector GL14, discharge GL14<br />

Ventilation Air escape valve (ETFE/Kalrez)<br />

Inerting Inerting valve (ETFE/Kalrez), pressure regulator from maximum 16bar to 0..1bar<br />

Dosing System A GraviDos Dosing System for liquids (regulated dropping funnel), 500 ml receiver<br />

tank, dosing valve (ETFE/Kalrez) controlled gravimetrically<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Automatic Laboratory Reactor Systems<br />

Sensors Temperatures: reactor interior space, thermostat, flow, return flow, steam dosing<br />

medium Reactor interior pressure, pH-value<br />

Automation LABbox2 with the following interfaces: 8 Pt<strong>10</strong>0 temperature measurement inputs, 8<br />

analogue inputs (Current & Voltage) of which 1 pH, 3 RS232, 4 GraviDos (DMS)<br />

Interfaces, 4 digital inputs, 8 digital outputs, 2 of which for 230 V connected sockets.<br />

Sensor power supply 24 V 1,5 A, actor power supply 24 V 3 A.<br />

User pc, 1 CG-ABK2 <strong>HiTec</strong> display and control element with premium 22“ TFT<br />

monitor, uninterrupted power supply and UPS management system<br />

Materials <strong>Main</strong>ly borosilicate glass, PFA, PTFE, ETFE, seals in contact with media made of<br />

Kalrez, high grade steel material 1.4571 (modifications possible)<br />

Dimensions D x W x H: 56 x 80 x 150 cm<br />

Order Code Description<br />

VL-LABKITALR2 Automatic Laboratory Reactor System, 2 Dosing Circuits, Reflux Boiling, Vacuum Distillation,<br />

Vacuum Control, Inerting, Stirrer Torque Measurement<br />

VL-LABKITALR2-AWE Collection plate made of high-grade steel<br />

VL-LABKITALR2-RFT Column and magnetc glas-reflux seperator with vaccuum jacket<br />

Recommended Software Package<br />

Order Code Description<br />

SL-LABVIPBATE Economy software package for LabBox2 and LabManager1 for batch operation<br />

SF-PID8 Controller module with 8 PID- and application oriented controllers<br />

Recommended datapoint amount: <strong>10</strong>0<br />

For high pressure reaction, in particular at multiphase<br />

systems, the HiClave laboratory pressure<br />

reactor systems have proven themselves to be a<br />

suited solution.<br />

They cover the volume range from <strong>10</strong> to 250 ml at a<br />

maximum pressure up to 300 bar and a maximum<br />

temperature of up to 300°C. Due to the pure metal<br />

cover gasket, the system is able to reach a tightness<br />

which enables highly precise gas consumption<br />

measurements. Up to 7 reactor connections are<br />

possible. At the reactors as of <strong>10</strong>0 ml content, the<br />

<strong>HiTec</strong> <strong>Zang</strong> Pressure Reaction Systems are suited<br />

for<br />

� Hydrogenation<br />

� Oxidations<br />

� Carbonylation<br />

� Polymerisation<br />

and further processes.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 9<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


<strong>10</strong><br />

Standard Systems<br />

Automatic Laboratory Reactor Systems<br />

HiClave plants dispose of a modular construction.<br />

The standard systems depicted in the following<br />

represent the basis for pressure reaction systems<br />

suited for a multitude of applications. They are<br />

adjustable to the respective requirements and can<br />

be equipped with the offered additional modules and<br />

components.<br />

Pressure Reactor System with Gassing and Balancing<br />

<strong>10</strong> ml and 20 ml Reactors<br />

Equipment<br />

The <strong>10</strong> ml and 20 ml reactors have<br />

a cover with cap nut and a central<br />

media connection with four-way<br />

connector. The middle connection<br />

of the four-way connector is<br />

allocated with the interior<br />

temperature sensor, the lateral<br />

ones usually with media connection<br />

and the manometer.<br />

The reactors tempered with a<br />

magnetic heating stirrer with<br />

heating block and agitated by a<br />

kinetic stirring rod.<br />

� Simple heating and stirring via a magnetic<br />

heating stirrer and a heating block attachment<br />

� Temperature Sensor (Pt<strong>10</strong>0)<br />

Pressure Reactor 20 ml, heated and agitated with Magnetic<br />

Stirrer; on the right: Reactor with fibre-optic ATR Sensor<br />

Connection Options<br />

� 1 x Temperature Sensor<br />

� 1 x Pressure Gauge<br />

� 1 x Media Connection<br />

Options<br />

� Other Connection Assignments<br />

50 ml Reaktor<br />

The 50 ml reactor a<br />

cover with cap nut<br />

and 3 connections.<br />

One of these can be<br />

equipped with a<br />

magnetic stirrer drive.<br />

The stirrer is passed<br />

through eccentrically.<br />

The other two<br />

connections are for<br />

the thermal sensor<br />

and and the media<br />

feed. If the stirrer<br />

drive is omitted in<br />

favour of magnetic<br />

stirrer, the now free<br />

connection can now<br />

be freely assigned.<br />

The reactors are<br />

heated via a heating<br />

sleeve and stirred<br />

overhead. In this<br />

case, the cooling can<br />

be conducted via a<br />

plate cooler.<br />

Alternatively, it is<br />

possible to heat and<br />

stir with a magnetic heating stirrer and heating block.<br />

Equipment:<br />

� Heating via Heating Sleeve<br />

� Stirring via Magnetic Stirring Head<br />

� Temperature Sensor (Pt<strong>10</strong>0)<br />

Connection Options<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


<strong>10</strong>0...250 ml Reactor<br />

Automatic Laboratory Reactor Systems<br />

The <strong>10</strong>0...250 ml rector<br />

have a flange cover with 7<br />

connections bolted by<br />

extension bolts. For better<br />

access, three of these<br />

connections have been<br />

placed on the outer side of<br />

the cover. The central<br />

nozzle is assigned with the<br />

magnetic stirrer head. The<br />

reactor is available in a<br />

high grade steel or<br />

Hastelloy version.<br />

The reactors are heated<br />

via a heating sleeve and<br />

can optionally be cooled<br />

by either a plate heater or<br />

an internal cooling circuit.<br />

The stirring is conducted<br />

with a magnetic stirring<br />

head, optionally either with<br />

a maximum torque of 20<br />

Ncm or 50 Ncm. The<br />

according fitting kits are available in high grade steel<br />

1.4571 (SS 316Tl) or in Hastelloy C4.<br />

Connection Options<br />

� 1 x Immersion Pipe for Temperature Sensor<br />

� 1 x Stirrer<br />

� 1 x Burst Disc made of metal for the safe<br />

limitation of the maximum pressure<br />

� 1 x Pressure Gauge<br />

� 1 x Valve for Pressure Release<br />

� 2 x freely assignable, e.g. for gas or liquid<br />

sampling<br />

Options<br />

� Hydrogenation/Gassing Module<br />

� Liquid and/or Gas Sampling<br />

� Cooling via Plate Cooler or Cooling Circuit<br />

� Hastelloy Version<br />

Hydrogenation Module<br />

The Hydrogenation Module VL-HICLAVE-HYDR<br />

enables the realisation of the complete<br />

hydrogenation process, including the inert gas<br />

rinsing and leak test of the reactor, without manual<br />

intervention. For this reason, there is no need for<br />

anyone to be in the risk area of the reactor while the<br />

same is under pressure. For this purpose, the<br />

reactor is charged with up to regulable pressure with<br />

inert gas an subsequently vented. This rinsing<br />

process can be repeated as often as required.<br />

Subsequently, a pressure test with inert gas will be<br />

conducted. The testing period and tolerance for<br />

passing the test must be entered.<br />

Only if the pressure test has been passed, will the<br />

reaction gas – in the upper example hydrogen – be<br />

released. Otherwise, the reactor is vented. In the<br />

next step, a rinsing with reaction gas is conducted,<br />

the setpoint pressure is established, and the<br />

reaction is started.<br />

A gas consumption measurement for the capture of<br />

kinetic data is integrated. The gas consumption can<br />

also be utilised as an abort criteria, i.e. the reaction<br />

is interrupted if the consumption has decreased<br />

below a predefined rate.<br />

a.) Parameter Template for Pressure Reactions b.) Protocol of a<br />

Pressure Reaction. Evaluation after a Pseudo First Order Kinetic.<br />

Automation<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 11<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


12<br />

Automatic Laboratory Reactor Systems<br />

The plant is monitored and operated via a selfexplanatory<br />

user interface. The measurement data<br />

are automatically captured and recorded in a<br />

Versions<br />

protocol. If a gas consumption measurement has<br />

been conducted, it is also possible to realise a<br />

kinetic evaluation of the consumption curve.<br />

Frame Square aluminum profile, anodised. High Grade Steel Platform.<br />

Reactor <strong>10</strong>...250 ml- High Grade Steel Reactor (opt. Hastelloy), 300 bar, 300°C. Optional<br />

450°C<br />

Stirrer Stirrer with magnetic coupling, Speed: 200..1500 rpm, Maximum Torque:20/50 Ncm,<br />

including analogue interface (Reactors ≥ 50ml).<br />

Or: Magnetic Heating Stirrer with Heating Block and Magnetic Stir Bar (Reactors ≤ 50<br />

Heating /Cooling<br />

System<br />

ml)<br />

Heating Sleeve/ Plate Cooler (alternatively Cooling Circuit), Operating Temperature<br />

Range:40..350°C in Jacket, Heating Output 700W. Or: Magnetic Heating Stirrer with<br />

Heating Block<br />

Sampling Manual with Sampling Valve<br />

Gassing Reaction gas pressure-controlled via MFC, including gas consumption measurement,<br />

by-pass valve.<br />

Inertisation Inert gas pressure-controlled. Exhaust via high pressure magnetic valve, burst disc.<br />

Dosing System, GraviDos High Pressure Dosing System. Optional High Pressure Pump and Scales.<br />

gravimetrically<br />

controlled<br />

Sensorics Temperatures: Reactor Interior Temperature, Jacket Temperature, Reactor Interior<br />

Pressure, Speed, ATR-FTIR.<br />

Automation For Example for two Autoclaves:<br />

LabBox2 with the following Equipment:<br />

Interfaces: 4 Pt<strong>10</strong>0 Temperature Measurement Inputs, 4 analogue Inputs (current and<br />

voltage), 4 RS232 Interfaces (Stirrer, Hydrogation Module), 4 GraviDos Connections, 8<br />

digital Outputs, of these 2 for Power Sockets switched to 230 V.<br />

Sensor Power Supply24V 1,5 A, Actor Power Supply 24V 3A.<br />

2 Safety Temperature Monitors.<br />

Workstation: 1 CG-ABK1 <strong>HiTec</strong> Display and Operating Component with high quality<br />

20“ TFT Monitor, Uninterrupted Power Supply and UPS Management System.<br />

This automation system is able to control 2 reactors.<br />

The extension to 4 reactors is possible.<br />

Materials <strong>Main</strong>ly High Grade Steel1.4571, other High Grade Steels, Hastelloy.<br />

Order Code Description<br />

VL-HICLAVE-SC-n Frame for HiClave Pressure Reactors, Piping, Sensorics, gravimetr. Dosing Unit 150ml<br />

VL-HICLAVE-ws-vol HiClave Pressure Reactor according to Specification ws-vol<br />

VL-HICLAVE-HEABAN-vol Heating Sleeve, 230V AC, 500 Watt, Duplex Temperature Sensor<br />

VL-HICLAVE-COOLP Plate Cooler for <strong>Main</strong>s Water or Thermostat Connection<br />

VL-HICLAVE-STIRR-20 Magnet-coupled Overhead Stirrer, 20Ncm<br />

VL-HICLAVE-STIRR-50 Magnet-coupled Overhead Stirrer, 50Ncm<br />

VL-HICLAVE-MAGHEAT Magnetic Stirrer with Plate Heating<br />

VL-HICLAVE-HYDR Hydrogenation and Gassing Module for HiClave Pressure Reactors with Mass Flow<br />

Controller<br />

VL-HICLAVE-GRAVI150 Additional gravimetr. Dosing Unit 150ml for HiClave Pressure Reactors<br />

VL-HICLAVE-ABKPNK1 Automation Unit with 20´´ Monitor and Workstation and SL-LABVIPEASY Software Package<br />

30 DP, for one HiClave Unit with gravimetric Dosing, Dosing, Tempering, Hydrogenation<br />

VL-HICLAVE-ABKPNK2 Automation Unit with 20´´ Monitor and Workstation and SL-LABVIPEASY Software Package<br />

<strong>10</strong>0 DP, for two HiClave Units with gravimetric Dosing, Dosing, Tempering, Hydrogenation<br />

VL-HICLAVE-ABKPNK4 Automation Unit with 20´´ Monitor and Workstation and SL-LABVIPEASY Software Package,<br />

300 DP for four HiClave Units with gravimetric Dosing, Dosing, Tempering, Hydrogenation<br />

n ( = Number of Reactors): 1 to 8<br />

ws ( = Material): High Grade Steel 1.4571 (SS 316Tl): e, Hastelloy C4: h, Special Material s<br />

vol ( =Operating Volume): <strong>10</strong>, 20, 50, <strong>10</strong>0, 150, 250 accordingly <strong>10</strong>, 20, 50, <strong>10</strong>0, 150 or 250 ml<br />

Special Designs, e.g. other volumes, connections, materials etc. are available upon request. Alternative<br />

dosing units can be found under the Section „Dosing Systems and Pumps“.<br />

Do you have Questions? Do not hesitate too ask!. Our project engineers will gladly help!<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Automatic Laboratory Reactor Systems<br />

Parallel Reactor Systems<br />

Reaching Objectives faster with the automated Parallel Synthesis<br />

The pressure to maximise productivity in the<br />

laboratory is consistently growing. At the same time,<br />

however, the demands on quality are also<br />

increasing.<br />

Standardised and client-specifically customised<br />

<strong>HiTec</strong> <strong>Zang</strong> parallel reactor systems are the answer<br />

to the increasing demands:<br />

� Shortened „Time to Market“<br />

� Improved Quality<br />

� Increased Reproducibility<br />

� Lower Costs<br />

You can ensure these advantages by:<br />

� Eliminating shortages through parallel<br />

operation<br />

� 24-hour, 7 day operation<br />

� Relief from routine activities<br />

� Optimal documentation and protocoling<br />

The <strong>HiTec</strong> <strong>Zang</strong> parallel reactor systems MultiLab<br />

and MiniLab significantly support and expedite<br />

research and development processes in the<br />

chemical and pharmaceutical industry. The flexibility<br />

of the parallel reactor systems overcomes the<br />

throughput restrictions of today's research and<br />

development processes.<br />

They help in shortening the “time-to-market” by<br />

expediting the optimisation processes for synthesis<br />

and alignment via the parallelisation of experiments<br />

and sophisticated automation and software<br />

solutions. Due to the possibility of unattended<br />

operation, the efficiency and the instrument<br />

utilisation is raised. All devices support batch, semibatch,<br />

continuous and multistage processes.<br />

With the parallel reactor systems, you are able to<br />

repeatedly and in parallel conduct experiments in<br />

great numbers and, consequently, decisively<br />

expedite the work process. By this, you save time,<br />

increase the efficiency and the capacity of your<br />

laboratory.<br />

The test conditions, such as temperature, pressure<br />

and pH-value may differ for every reactor.<br />

In case of the innovative tempering systems of the<br />

MultiLab and MiniLab, the otherwise usual tempering<br />

block for multi-reactor systems was intentionally<br />

omitted. Both systems allow a clear view into the<br />

reactor.<br />

The systems are suited for<br />

� Synthesis<br />

� Polymerisation<br />

� Distillation<br />

� Extraction<br />

� Crystallisation etc.<br />

Automation<br />

They neither restrict the creativity, nor do they<br />

require a specialist to operate. The user has full<br />

control over all system parameters all the time.<br />

All labour-intensive steps, from the planning of the<br />

experiment to the evaluation and documentation of<br />

the experimental data, are supported or completely<br />

automated. Even complex recipes can be<br />

established in a few minutes by combining the basis<br />

operations with the graphic HiBatch Recipe Editor.<br />

A recipe can be allocated to several reactors and<br />

individually parameterised. Due to this, the time and<br />

work expenditure even remains minimal when<br />

extensive parallel experiments are conducted.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 13<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


14<br />

Automatic Laboratory Reactor Systems<br />

MultiLab Multi-Reactor System<br />

MultiLab is a miniaturised fully automated laboratory<br />

reactor system. Therefore, any reaction that is<br />

usually conducted on the litre scale can now be<br />

carried out in the 250 or 400 ml MultiLab reactor<br />

under realistic plant conditions, fully automated and<br />

controlled independently by a <strong>HiTec</strong> <strong>Zang</strong><br />

LabManager with the leading LabVision laboratory<br />

automation software.<br />

MultiLab is a modular system and still flexible. It is<br />

available in a great variety ranging from the<br />

manually operated basis version to the individually<br />

configurable fully automated multi-reactor system.<br />

Even complex processes with educt pre-treatment,<br />

synthesis, reaction monitoring, and product postprocessing,<br />

as well as automatic sample drawing is<br />

possible.<br />

The special characteristic of the MultiLab parallel<br />

reactor system is its innovative tempering system. A<br />

high-grade steel spiral/coil holds the reactor<br />

temperature and cools, respectively heats the same,<br />

if necessary.<br />

MultiLab is suitable for all common processes:<br />

� Synthesis<br />

� Polymerisation<br />

� Distillation<br />

� Extraction<br />

� Crystallisation etc.<br />

Features<br />

� Modular compact design<br />

� Convenient and fast handling (exchange of a<br />

reactor in less than one minute)<br />

� Independent control of each reactor<br />

� Proprietary groundbreaking tempering<br />

system enables unhindered sight into the<br />

reactor<br />

� Only one chiller for multiple individually<br />

tempered reactors<br />

� Multiple dosing options (liquid, solid and<br />

gaseous, gravimetric and volumetric)<br />

� Automated sampling options<br />

� Fully automated control of reactor conditions<br />

like feed rates, temperature, pressure, pH and<br />

agitation<br />

� Multiple systems controlled by a single PC<br />

with a LAB Manager, LabVision and HiBatch<br />

recipe control software<br />

� 24 hour unattended operation<br />

� Inert construction materials: glass, PTFE<br />

� Individually expandable and upgradeable<br />

Easy Handling<br />

The exchangeable reactors of the MultiLab enable<br />

fast reaction to changing requirements. The unique<br />

and innovative heating/cooling system offers<br />

essential benefits. The glass vessel is electrically<br />

heated or cooled by a flow of cooling liquid out of a<br />

reservoir.<br />

Exchange of a reactor<br />

The reactor is released by actuating the release<br />

lever and can be removed after lifting the complete<br />

head construction.<br />

The temperature of the coil is registered and<br />

controlled and, in addition, can be limited, if<br />

necessary. For reactor volumes ranging from 75 to<br />

250 ml, the MiniLab System is alternatively<br />

available.<br />

Options<br />

� Distillation<br />

� Controlled reflux<br />

� Solid and gaseous dosing<br />

� Electric bottom outlet valve<br />

� Phase detection and separate bottling of<br />

organic/inorganic phase<br />

� ATR-FTIR online Monitoring<br />

� Automatic sampling and many more options<br />

� further options available upon request<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Module Description<br />

Automatic Laboratory Reactor Systems<br />

Module Basic Unit Equipment<br />

(common components of all<br />

reactors)<br />

Components per Reactor<br />

(one unit required for each reactor)<br />

Basic Module Tempering unit, rack with reactor lift,<br />

glas cover, 1 x NS29, 4 x NS19,<br />

high-grade steel quick release<br />

fastener, GL25 connection, anker or<br />

tilted blade stirrer, cardan shaft,<br />

sealing, vacuum-sealed, max.<br />

temperature 250 °C (monitor cooling<br />

media!), min. temperature<br />

dependant of thermostat. inside<br />

temperature sensor PT<strong>10</strong>0 PTFE<br />

coated, cables for stirrer and<br />

thermostat<br />

Vessel Reactor 250 ml, DN60, borosilicate<br />

glass, sealing silicone/FEP-coated<br />

Standard Cooling Unit Cooling thermostat -20 °C (flow<br />

temperature)<br />

Alternatives<br />

(other or extended features<br />

without specification)<br />

Reactor 400 ml<br />

base drain, manual base drain,<br />

electrical sensor sockets,<br />

electrical reactor lift,<br />

ViscoPakt -mini-rheo-35<br />

precision measurement stirrer,<br />

magnetic stirrer closure,<br />

propeller or impeller stirrer<br />

made of high-grade steel,<br />

glass thermometer, etc.<br />

Reactor 400 ml<br />

Cooling thermostat -40 °C.<br />

low temperature equipment :<br />

Cooling thermostat -60 °C,<br />

removable isolation jacket (per<br />

reactor)<br />

Reflux cooling Cooling water valve<br />

Cooling water monitor<br />

Dimroth cooler<br />

Distillation Distilling bridge<br />

Distillate weighing<br />

Pt<strong>10</strong>0 for steam temperature Additional cooler for reflux<br />

Collecting container for distillate cooling<br />

Rectification Hempel column 200 mm<br />

Vacuum jacket<br />

Micro column head according to Dr. Distillate weighing<br />

Kaminski, magnetically actuated Pt<strong>10</strong>0 in column<br />

Pt<strong>10</strong>0 column head<br />

Dimroth cooler<br />

Collecting container for distillate<br />

Filling material/Packages<br />

Vacuum Chemical-resistant vacuum pump Vacuum regulating valve<br />

Pressure sensor 0-1,6 bar<br />

Pressure relief valve<br />

Stronger vacuum pump<br />

Inerting Pressure regulator 16 bar to 0-1 Inerting valve, pressure relief valve<br />

bar<br />

1,3 bar<br />

Dosing Hanging scales Grado<strong>10</strong>00 Automatic refill<br />

Weighing container 500 ml<br />

Mounting panel for LabManager<br />

lateral refilling feed pipe<br />

(useful in case of more than 3<br />

Regulating valve<br />

modules)<br />

Other container sizes<br />

Volumetric Dosing Peristaltic pump Diaphragm, piston pumps,<br />

etc.<br />

Solid Dosing Solid doser SoliDos<br />

Inerting connection<br />

connection socket on to NS19 Inert gas heating<br />

pH-Measurement PH gel electrode pH 0-14<br />

lead-through 12 mm<br />

measuring amplifier pH<br />

Cover with sensor socket<br />

Redox-Potential Redox-electrode<br />

Cover with special sensor<br />

reference electrode<br />

socket (necessary at anchor<br />

lead-through 12 mm<br />

measuring amplifier mV<br />

stirrer!)<br />

Phase Limit Detection automatic base drain valve with Temperature measurement with<br />

Pt<strong>10</strong>0<br />

PhaDec phase limit detector<br />

regulating valve<br />

same Pt<strong>10</strong>0<br />

Gas Dosing Pressure regulator 16 bar to 0-1 Mass flow regulator<br />

bar<br />

Pressure relief valve 1,3 bar<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 15<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


16<br />

Automatic Laboratory Reactor Systems<br />

Order Code Description<br />

VL-MULTILAB-BU MultiLab multi reactor base module with tempering and stirrer unit and cover<br />

IR-VIPA-MINI-RHEO-35 ViscoPakt-rheo stirrer drive, 35 Ncm<br />

VL-MULTILAB-GRV250 MultiLab reaction vessel 250 ml, DN60, borosilcate glass, sealin silicon/FEP covered<br />

VL-MULTILAB-GRV400 MultiLab reaction vessel 400 ml, DN60, borosilcate glass, sealin silicon/FEP covered<br />

IR-RDFMAG8 Magnetic stirrer closing for 8 mm agitator<br />

VL-MULTILAB-CHILL-20 MultiLab cooling thermostat flow temperature -20 °C<br />

VL-MULTILAB-CHILL-40 MultiLab cooling thermostat flow temperature -40 °C<br />

VL-MULTILAB-CHILL-60 MultiLab cooling thermostat flow temperature -60 °C<br />

VL-MULTILAB-RFC MultiLab intensive reflux cooler<br />

VL-MULTILAB-DEST MultiLab destillation bridge, Pt<strong>10</strong>0 for fume temperature, catchment tank for destillate<br />

VL-MULTILAB-REKT MultiLab rectification attachment, Hempel-column 200 mm, micro column head magnetically<br />

activated, Pt<strong>10</strong>0 column head, Dimroth-cooler<br />

VL-MULTILAB-VAKU MultiLab vacuum control unit with vacuum control valve, pressure sensor 0-1,6 bar, pressure<br />

relief valve<br />

IP-B-V1-1200L-PTFE/FPM Chemical vacuum pump with alternating current motor 120W, 230V AC, 1200 l/h, end vacuum<br />

8 mbar, material PTFE/FFKM<br />

VL-MULTILAB-INERT MultiLab inerting unit with inerting valve and pressure control valve 1,3 bar<br />

IV-DRUMIN16/1 Pressure reducer 16 bar to 0-1 bar<br />

VL-MULTILAB-GRAVI500ml Gravimetric dosing module with hanging balance <strong>10</strong>00g, weighing vessel 500 ml, lateral refill<br />

nozle, control valve, cable<br />

VL-MULTILAB-ABKPNK1 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />

<strong>10</strong>0 data points for 1 MultiLab unit with 2 gravimetric dosing circuits, vacuum control,<br />

inerting, destillation/rectification<br />

VL-MULTILAB-ABKPNK2 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />

<strong>10</strong>0 data points for 2 MultiLab units with 2 gravimetric dosing circuits each, vacuum control,<br />

inerting, destillation/rectification<br />

VL-MULTILAB-ABKPNK4 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />

180 data points for 4 MultiLab units with 2 gravimetric dosing circuits each, vacuum control,<br />

inerting, destillation/rectification<br />

VL-MULTILAB-ABKPNK6 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />

300 data points for 6 MultiLab units with 2 gravimetric dosing circuits each, vacuum control,<br />

inerting, destillation/rectification<br />

VL-MULTILAB-ABKPNK8 Automation unit with 22" user terminal and LABVIPBAT and MULTIBATCH software package,<br />

560 data points for 8 MultiLab units with 2 gravimetric dosing circuits each, vacuum control,<br />

inerting, destillation/rectification<br />

The VL-MULTILAB-ABKPNK automation unit is a<br />

complete set of Windows XP or Vista operating<br />

system, installed LabVision software package an d<br />

uninterruptable power supply.<br />

The automation unit can be buildt individually from<br />

our LabManager-, UI- and LabVision program.<br />

Recommended software package at individual selection:<br />

Order Code Description<br />

SL-LABVIPBAT Standard package "Batch" for LabManager1<br />

SL-MULTIBATCH HiBatch extension for parallel synthesis<br />

Recommended datapoint modules: 50 per MultiLab unit.<br />

Recommended PI-modules<br />

Recommended controller amount: 4 per MultiLab unit<br />

Further extensions:<br />

Solid dosing (SoliDos), gas dosing, volumetrik<br />

dosing (LabDos) pH- a. redox measurement<br />

(pHAmp) and controlling, clouding measurement,<br />

phase seperation (PhaSep), autosampling device<br />

(AutoSam) and other hard- and software options<br />

from our LabKit and LabVision program.<br />

Order Code Description<br />

SF-PID4 Controller module with 4 PID- and application oriented controllers<br />

Should you have any queries, our sales experts will gladly help you!<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Automatic Laboratory Reactor Systems<br />

MiniLab mini reactor system<br />

The <strong>HiTec</strong> <strong>Zang</strong> MiniLab parallel reactor system<br />

distinguishes itself by its particularly small „footprint“.<br />

It offers high-performance at minimal required<br />

space and best reproducibility due to automatic<br />

operation mode.<br />

MiniLab-Module with GraviDos Liquid Doser and ViskoPakt-MINI<br />

stirring drives.<br />

The downsizing of reactor mixtures offers the<br />

opportunity to accelerate development processes by<br />

parallel operation of experiments. At the same time,<br />

precious reactants and expensive laboratory space<br />

are saved. Very small mixtures can however be a<br />

problem in regard to reproducibility. For this reason,<br />

volumes of 75-250 ml are ideal for initial<br />

optimisations.<br />

MiniLab is based on a compact heating/cooling<br />

system. Unlike conventional hot plates, the<br />

tempering plate is also able to cool. The low thermal<br />

mass makes quick temperature changes possible. In<br />

the course of this, several stations can be supplied<br />

with cooling agent by one common cryostat.<br />

Reactors with different reaction volumes can be<br />

used in any combination.<br />

MiniLab is suitable for all common processes:<br />

� Synthesis<br />

� Polymerisation<br />

� Distillation<br />

� Extraction<br />

� Solidification etc.<br />

Features<br />

� Particularly favourable geometry for dipping<br />

sensors<br />

� Individual temperature control for each<br />

individual reactor with only one cryostat<br />

� Reactor size optional 75, 125, or 250 ml<br />

� Low expenditure of reactants<br />

� Multiple upgrading possibilities<br />

� Can also be used as Single Reactor System<br />

� High-capacity and easy to handle automation<br />

� Mini reactor systems controlled by a single<br />

PC with a LabManager, LabVision, and<br />

HiBatch multi recipe control<br />

� Fully-automated control of reactor conditions<br />

like feed rates, temperature, pressure, pH,<br />

and agitation<br />

� Multiple dosing options (liquid, solid and<br />

gaseous, gravimetric and volumetric)<br />

� Automated sampling options<br />

� Easy and fast handling<br />

� Inert construction materials: Glass, PTFE<br />

� Proprietary groundbreaking tempering<br />

system enables unhindered sight into the<br />

reactor<br />

� Modular compact design<br />

� Individually expandable and upgradeable<br />

The exchangeable reactor of the MiniLab enables<br />

fast reaction to changing requirements. The unique<br />

and innovative heating/cooling system offers<br />

essential benefits. The glass is situated on a<br />

heating/cooling plate. The same is electrically<br />

heated or cooled by a flow of cooling liquid out of a<br />

reservoir.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 17<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


18<br />

Automatic Laboratory Reactor Systems<br />

Modular and flexible<br />

MiniLab is a miniaturised fully-automated laboratory<br />

reactor system. Every process which is normally<br />

conducted in a reactor with greater volume can also<br />

run in the 75 to 250 ml reactors of the MiniLab under<br />

realistic conditions; fully automated and individually<br />

controlled for each reactor by the leading laboratory<br />

automation software LabVision and HiBatch.<br />

125 ml Reaktor 250 ml Reaktor<br />

MiniLab is available in a great variety reaching from<br />

the manually operated basis version to the<br />

individually configurable fully-automated multireactor<br />

system.<br />

Even complex operating sequences with reactant<br />

pre-treatment, synthesis, reaction monitoring, and<br />

product finishing treatment, as well as sample<br />

drawing, are possible.<br />

With the MiniLab parallel reactor system you can<br />

conduct experiments in parallel repeatedly in great<br />

numbers and therefore accelerate the work process<br />

significantly. This will save you time, increase the<br />

efficiency and the capacity of your laboratory.<br />

The test conditions such as temperature, pressure,<br />

pH etc., may differ for every reactor and are<br />

simultaneously controlled in all reactors.<br />

The vessel can be easily removed or installed after<br />

lifting up the complete top construction. Hereby, all<br />

reactor sizes can be deployed. Up to six sockets<br />

situated on the reactor cover permit flexible<br />

equipping with additional devices.<br />

The temperature of the plate is registered and<br />

controlled. It is possible to set a limit for the<br />

temperature.<br />

Options<br />

� Distillation<br />

� Rectification with Reflux Separation<br />

� Solid Dosing<br />

� Gaseous Dosing<br />

� ATR-FTIR online Monitoring<br />

� Magnet Stirrer Drive<br />

� Automatic Sampling<br />

� more options available upon request<br />

Module Description<br />

Module Basic Unit Equipment Components per Reactor<br />

(common components of all<br />

reactors, only one necessary<br />

per Parallel Reactor System)<br />

(if necessary, one unit required for<br />

each unit)<br />

Basic Module Tempering unit, rack, reactor<br />

75...250 ml, seal ring<br />

Silicon/FEP cladded, high-grade<br />

steel quick release fastener,<br />

high-grade steel cover, 1 x<br />

NS29, 5 x NS19 stirrer drive of<br />

Mini-Stirrer, flexible shaft, GL25<br />

connection, stirrer sealing,<br />

vacuum-sealed, anchor or tilted<br />

blade stirrer, max. temperature<br />

250 °C (monitor cooling<br />

media !), min. temperature<br />

dependent of thermostat. Inside<br />

temperature sensor PT<strong>10</strong>0<br />

PTFE coated with stirrer and<br />

wiring for stirrer and thermostat.<br />

Vessel Reactor 250 ml, DN60,<br />

borosilicate glass, sealing<br />

silicone/FEP-coated<br />

Standard Cooling Unit Cooling thermostat -20 °C (flow<br />

temperature)<br />

Reflux Cooling Cooling water valve<br />

Cooling water monitor<br />

Dimroth cooler<br />

Distillation Distilling bridge<br />

Pt<strong>10</strong>0 for steam temperature<br />

Collecting container for distillate<br />

Alternatives<br />

(other or expanded properties<br />

or specifications)<br />

ViscoPakt-mini-rheo35<br />

precision measurement<br />

stirrer, magnetic stirrer<br />

closure, propeller or<br />

impeller stirrer made of<br />

high-grade steel,<br />

glass thermometer etc.<br />

Reactor vessels 75 ml and<br />

125 ml with vacuum jacket<br />

for deep temerature<br />

applications<br />

Cooling thermostat -45 °C.<br />

low temperature equipment:<br />

Cooling thermostat -83 °C,<br />

removable isolation jacket<br />

(per reactor)<br />

Distillate weighing<br />

Additional cooler for reflux<br />

cooling<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Automatic Laboratory Reactor Systems<br />

Continued: MiniPlant Module Description<br />

Module Basic Unit Equipment<br />

(common components of all<br />

reactors, only one necessary<br />

per Parallel Reactor System)<br />

Components per Reactor<br />

(if necessary, one unit required for<br />

each unit) )<br />

Rectification Hempel column 200 mm<br />

Micro column head according to<br />

Dr. Kaminski, magnetically<br />

actuated<br />

Pt<strong>10</strong>0 column head<br />

Dimroth cooler<br />

Collecting container for distillate<br />

Vacuum Chemical-resistant vacuum<br />

pump<br />

Vacuum regulating valve<br />

Pressure sensor 0-1,6 bar<br />

Pressure relief valve<br />

Inerting valve, pressure relief<br />

valve 1,3 bar<br />

Inerting Pressure regulator 16 bar to 0-<br />

1 bar<br />

Gravimetric Dosing Hanging scales Grado<strong>10</strong>00<br />

Weighing container 250 ml,<br />

lateral refilling feed pipe<br />

Regulating valve<br />

Alternatives<br />

(other or expanded properties<br />

or specifications)<br />

Vacuum jacket<br />

Distillate weighing<br />

Pt<strong>10</strong>0 in column<br />

Vigreux column<br />

Filling material/Packages<br />

Stronger vacuum pump<br />

Automatic refill<br />

Mounting panel for<br />

LabManager (useful in case<br />

of more than 3 modules)<br />

Other container sizes<br />

Volumetric Dosing Peristaltic pump Diaphragm, piston pumps,<br />

etc.<br />

Solid Dosing Solid doser SoliDos<br />

Inerting connection<br />

connection socket on to NS19 Inert gas heating<br />

pH Measurement PH gel electrode pH 0-14 Cover with special sensor<br />

lead-through 12 mm<br />

measuring amplifier pH<br />

socket<br />

Redox Potential Redox-electrode<br />

Cover with special sensor<br />

reference electrode<br />

socket (necessary at anchor<br />

lead-through 12 mm<br />

measuring amplifier MA<br />

stirrer!)<br />

Reaction Calorimetry Reactor with vacuum jacket<br />

Calorimetry evaluation module<br />

Gas Dosing Pressure regulator 16 bar to 0- Mass flow regulator<br />

1 bar<br />

Pressure relief valve 1,3 bar<br />

Order Code Description<br />

VL-MINILAB-BU MiniLab multi reactor base module with tempering and stirrer unit and cover<br />

IR-VIPA-MINI-RHEO-35 ViscoPakt-rheo stirrer drive, 35 Ncm<br />

VL-MINILAB-GRV75 MiniLab reactor vessel 75 ml, DN60, borosilicate glass, gasket silicone/FEP covered<br />

VL-MINILAB-GRV125 MiniLab reactor vessel 125 ml, DN60, borosilicate glass, gasket silicone/FEP covered<br />

VL-MINILAB-GRV250 MiniLab reactor vessel 250 ml, DN60, borosilicate glass, gasket silicone/FEP covered<br />

Further extensions:<br />

MiniLab can be extended with MultiLab system<br />

modules. There you will find suitable dosing<br />

systems, automation hard- and software, user<br />

interfaces and thermostats.<br />

Should you have any queries, our sales experts will gladly help you!<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 19<br />

Equipment and<br />

Components<br />

Process Analytics<br />

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20<br />

Automatic Laboratory Reactor Systems<br />

LabKit- Small Reactor Systems for Education<br />

Since 2002, laboratory automation, process control<br />

technology, and the basis operations of chemicalprocess<br />

engineering are included in the<br />

examination-relevant curriculum of chemical<br />

technicians and laboratory assistants. These topics<br />

should also not be omitted in the vocational training<br />

for chemists and process technicians. <strong>HiTec</strong> <strong>Zang</strong><br />

systems are already being used by numerous<br />

institutions for training, because they can be<br />

comprehended quickly.<br />

With LabKit-ed the substantial topics of modern<br />

laboratory practice can be conveyed, e.g.:<br />

� Chemical Process Engineering, Basis Operations<br />

� Control (monitoring, regulation)<br />

� Process Measuring and Control<br />

� Automation, Basic Functions<br />

� Batch, Semi-Batch and continuous Processes<br />

� Reaction Calorimetry<br />

� Recipe Control<br />

The system already becomes active at the planning<br />

stage. The P&ID editor supports the standardconform<br />

establishment of P&ID flow diagrams in<br />

accordance with EN ISO <strong>10</strong>628 (DIN28004) which<br />

are initially marked with the process and measuring<br />

control identifications according to DIN/EN19227.<br />

Specification<br />

A free version of RI-CAD, restricted to training<br />

purposes, can be requested on our website under:<br />

http://www.hitec-zang.de/de/downloads/ri-cad.html<br />

The P&ID flow sheet can be used later as the<br />

background picture for the displaying of control<br />

pictures (process pictures).<br />

In addition, the measurement and control system<br />

plan (MSR) and the circuit diagrams can be<br />

established with the same editor. It must be<br />

emphasised that the system is easy to comprehend<br />

and the handling can be comprehended in a very<br />

short period of time.<br />

The system is structured on a modular basis and<br />

can be adapted according to your special requests.<br />

With the optional Simulation Module, applications<br />

can be developed and pre-tested offline.<br />

We also train teachers in these fields of expertise.<br />

We will gladly forward you our proven teaching<br />

material (introduction manuals, exercises with<br />

solutions)!<br />

In case of interest, please ask us for further<br />

information on LabKit-ed.<br />

Rack anodised aluminium rack<br />

Reactor - 1 glass Reactor DN<strong>10</strong>0 with heating jacket and base discharge valve with<br />

integrated Pt <strong>10</strong>0 sensor manual<br />

- Glass cover with FEP-O-Ring silicone core<br />

- Stirrer shaft lead-through vacuum for <strong>10</strong> mm shaft, NS29<br />

- 2 tube connections for thermostats DN15 on to M16*1 with integratedPt<strong>10</strong>0-sensor<br />

GraviDos<br />

(Gravimetrical<br />

Dosing System)<br />

- 1 glass propeller stirrer<br />

1 GraviDos dosing System: the system consists of a glass storage container, which is<br />

suspended on a weighing system. The weight difference is registered and then the<br />

discharge regulated via valve. The system disposes of an integrated <strong>10</strong>00 g load cell,<br />

a 500 ml receiver tank, and a 2/2-way valve.<br />

Stirrer - 1 ViskoPakt torque stirrer, max. torque: 27 Ncm<br />

Dissolution: 0.07 Ncm, reproducibility: 1.5 Ncm, min. rotational speed: 150 rpm, max.<br />

rotational speed: 2000 rpm, standard stirrer lead-through (max 800 rpm).<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Automatic Laboratory Reactor Systems<br />

Tempering System - 1 circulation thermostat: with water pipes cooling coil, temperature range:<br />

35..200 °C, heating output: 2000 W, bath content: 3 litres, control via RS232,<br />

- 2 isolated metal tubes for thermostats, 150 cm<br />

- 1 2/2- way valve for cooling water supply to the thermostat<br />

Inerting - 1 binary valve for inert gas pipe<br />

- 1 pressure regulator from max. 16 bar suction pressure to 0.1..1 bar<br />

Venting/Deairing - 1 dead open binary valve<br />

- 1 Relief valve 0.1 bar made of glass for NS 29/32<br />

Instruments All sensors/actors including necessary fixtures and cables for connection to the <strong>HiTec</strong><br />

PI.<br />

Automation LabBox2-complete unit with integrated 24 V 1 A power supply sensors and and 24 V 3<br />

A power supply for actors.<br />

<strong>HiTec</strong> display and operation component including uninterrupted power supply and<br />

Power-Management-System for <strong>HiTec</strong> <strong>Zang</strong> PIs CG-ABK1.<br />

20" TFT Monitor.<br />

LabVision software package for training purposes with the following equipment: basic<br />

package with 300 data points, HiText – multitasking control and online evaluation,<br />

HiBatch Recipe Control, dialogue and protocol templates, online graphics, analogue<br />

chart recorder, event plotter, phase plotter, monitoring and messaging, Designer,<br />

P&ID-Editor, graphics library, data export, access monitoring and user administration,<br />

controller module with 4 P-, PI-, PID-, PD- or pH controller, NAMUR driver for serial<br />

interfaces, basic operations, charging, tempering, stirring, dosing, inerting,<br />

maintenance.<br />

Simulation LabVision-ed simulation version for training (VL-EDSIM) enables learning and training<br />

of automation technology and the process control by merely using a PC without PI<br />

and plant. It contains all essential LabVision modules, such as recipe control<br />

according to IEC and NAMUR, process visualisation, monitoring and messaging,<br />

online evaluation, etc.<br />

Basic operations such as dosing, temperature ramping, pressure and vacuum control,<br />

pH control, etc., can be established and tested. In order to avoid unnecessary waiting<br />

periods, the process simulation can be conducted in fast motion. The established<br />

applications can be transmitted to a LabKit-ed and tested under real conditions.<br />

Executable without PI under Windows 2000, XP and Vista.<br />

Optional equipment is available.<br />

Order Code Description<br />

VL-LABKITED Automatic Laboratory Reactor System for training, hard and software configuration according to<br />

table<br />

VL-EDDEST Expansion by distillation, reflux cooler, electronically controllable reflux separator, head<br />

temperature measurement and distillate scales, HiBatch basis operation distilling.<br />

VL-EDDOSFL LabKit-ed expansion by a volumetric dosing, a suspended receiver tank with a flowmeter and a<br />

pulse frequency controlled binary valve, HiBatch basis operation, volumetric dosing<br />

VL-EDVAK - vacuum control with the following components:<br />

-1 vacuum pump, flow rate: 20l/min, vacuum <strong>10</strong>0...<strong>10</strong>00 mbar absolute<br />

- activation via the power socket switched by the <strong>HiTec</strong> PI<br />

- 1 pressure sensor 0..1,6 bar absolute<br />

- HiBatch basis operation vacuum, 1 vacuum control valve , material: ETFE / Kalrez<br />

VL-EDDOSPU Expansion of a LabKit-ed by a volumetric and gravimetric dosing with pump and scales consisting<br />

of:<br />

- 1 scales, weighing range 3000 g, reproducibility 0.1 g, RS232 interface,<br />

- 1 magnetic diaphragm dosing pump 0.74 l/h (alternatively 1,1 or 2,1 l/h)<br />

- parts in contact with medium: PTFE<br />

- 1 dosing valve, material: ETFE,<br />

- HiBatch basis operation gravimetric dosing<br />

VL-EDSIM PI and process simulation package for one work station. Enables project establishment,<br />

parameterisation, programming, and simulation of the LabKit-ed without PI and plant.<br />

VL-EDUQUIP Case with training equipment such as Current and voltage transmitter, controlled loop simulator<br />

etc.<br />

Further information about training systems and didactic material can be found in the chapter Services &<br />

Didactics.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 21<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


22<br />

Automatic Laboratory Reactor Systems<br />

Automated Laboratory Clarification Unit<br />

The Laboratory Clarification Unit LabKit-sp<br />

enables the systematic investigation of the biological<br />

degradability of various liquid waste content<br />

substances. It consequently provides the basis<br />

information for the establishment of strategies for<br />

liquid waste purification. The unit enables the<br />

reproduction of clarification processes of large plants<br />

on a laboratory scale. It is also possible to conduct<br />

tests regarding the determination of the biological<br />

degradability according to OECD301A.<br />

The Unit comprises four levels:<br />

1.) Neutralisation with automated ph-Control, with<br />

ViscoPakt Stirrer, LabDos- Pump for the Feed,<br />

Overflow to the Denitrification.<br />

2.) Denitrification with O2-Measurement, pH-<br />

Measurement, ViscoPakt Stirrer, Interior<br />

Temperature Control (through electrical Heating with<br />

Heating Jacket), Overflow to the Nitrification.<br />

3.) Nitrification with O2-Control (through regulated<br />

Air Supply via a Base Frit), pH-Measurement,<br />

ViscoPakt-Stirrer, Interior Temperature Control<br />

(through electrical Heating with Heating Jacket),<br />

Foam Identification with automated Defoamer<br />

Addition, LabDos Pump for the transporting back the<br />

sludge into the Denitrification, Outlet into the Settling<br />

Tank.<br />

4.) Settling Tank with Overflow, Discharge Valve,<br />

LabDos Pump for the transporting back the sludge<br />

into the Denitrification.<br />

The Laboratory Clarification Unit is fully automated<br />

with a LabBox System and LabVision. It can<br />

naturally also be run manually.<br />

pH-Value, Temperature and Oxygen Concentration<br />

and further Measurement Variables are collected.,<br />

stored in the data base and graphically presented.<br />

The automation enables unattended operation and<br />

reproducibility at any given time.<br />

The permanent data recording leads to a consistent<br />

documentation of all process sequences.<br />

Neutralisation, Denitrification, Activation and Final Clarification<br />

Pilot Clarification Units deviant from this standard<br />

laboratory clarification unit, according to your<br />

specifications, are also offered by <strong>HiTec</strong> <strong>Zang</strong>.<br />

Order Code Description<br />

VL-LABKIT-SP Automated Laboratory Clarification Unit with LabBox PI and ABK1<br />

VL-LABKIT-SP-PHCON Automatic pH-Control<br />

VL-LABKIT-SP-FOCON Automatic Defoaming Control<br />

The plant is supplied in turnkey condition together with a LabBox2 Automation System and a ABK1<br />

Workstation with 20“ Monitor.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Automatic Laboratory Reactor Systems<br />

Modular Micro-Reaction Technology<br />

Micro-reaction technology opens up new ways to<br />

develop novel reaction processes and to construct<br />

advanced economic chemical plants. The<br />

advantages of the continuous operation mode in<br />

micro-structures are: ultra-fast mixing, highly<br />

effective heat transfer, short and controllable<br />

residence times, low system inertia for ideal process<br />

control and high safety due to extremely low holdup.<br />

The basic features of the micro-reaction technology<br />

for the development of new chemical processes and<br />

the production, both in the fine and mass chemical<br />

sector, offer significant potential for innovation and<br />

amortisation. Micro-modules can also be integrated<br />

into conventional plants without any problem.<br />

The micro-reaction technology enable to exactly<br />

control complex or critical reactions of fine chemistry<br />

(special products, agricultural and pharmaceutical<br />

chemicals), which considerably increases the<br />

operational safety of the chemical production.<br />

Economically attractive application possibilities have<br />

also been detected for bulk chemicals and polymers.<br />

The future technology of customised materials is not<br />

imaginable without micro-technology, as well. Microreactors<br />

allow the selective generation of nanoparticles<br />

for micro-electronics, the development of<br />

drug delivery systems for human medicine, and the<br />

realisation of new concepts within diagnostics.<br />

Micro-reaction modules enable basis process<br />

operations such as:<br />

� Mixing<br />

� Dispersing<br />

� Gassing<br />

� Precipitation<br />

� Heat Exchange, etc.<br />

<strong>HiTec</strong> <strong>Zang</strong>, in cooperation with the company<br />

Ehrfeld Mikrotechnik BTS, offers a complete<br />

package offer, which reaches from the individual<br />

module to process development and training, and as<br />

far as to engineering and the construction of ready<br />

to use fully automatic plants.<br />

The modules can flexibly be interconnected to<br />

precisely controllable reaction plants, with which a<br />

wide range of chemical syntheses can be conducted<br />

easily, quickly and cost-effective.<br />

The modular micro-reaction System represents an<br />

unique research and development platform for the<br />

development of new processes, both in laboratory<br />

scale and small-scale production.<br />

In addition, high flow modules are available, which<br />

also enable the mass production of chemicals.<br />

Dependent on the reaction conditions, these<br />

modules cover a flow rate ranging from 0.1 to <strong>10</strong>0<br />

ml/min with the modular micro-reaction system, and<br />

up to <strong>10</strong>00 litres/hour with the high flow modules.<br />

The modular micro-reaction system represents a<br />

unique tool for researchers out of the chemical and<br />

pharmaceutical sectors, to both develop new<br />

synthesis methods for the production of new<br />

chemical compounds and to improve existing<br />

methods.<br />

Hereby, one significant advantage is that the step<br />

from the development into production is conducted<br />

by simple „Numbering-Up“, e.g. the parallel<br />

connection of several identical sequences, instead<br />

of the expedient „Scale-Up“ procedure.<br />

Modular Micro-reaction System: Example for a single stage<br />

synthesis for heterogeneous conversions at solid catalysts<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 23<br />

Equipment and<br />

Components<br />

Process Analytics<br />

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Dosing Systems,<br />

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Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


24<br />

Special Features<br />

Automatic Laboratory Reactor Systems<br />

� Ideal ultra-fast mixing effect<br />

� Extremely short holding times<br />

� Avoidance of by-products<br />

� Robust against strong exothermal reaction<br />

� Increased operational safety<br />

� Minimal requirements to ambient conditions<br />

� Without scale-up in the production scale<br />

The Micro-reaction Technology enables to conduct<br />

single-stage and multi-stage syntheses throughout<br />

the whole range of research and development right<br />

to the production of chemical substances. Hereby, it<br />

is both possible to conduct reactions in the liquid<br />

and gas phases, as well as multi-phase in<br />

heterogeneous systems in the micro-reaction<br />

modules. In addition, there are special modules for<br />

the continuous precipitation of solids into microstructures<br />

so that it is also possible to process<br />

liquids carrying particles.<br />

The modular micro-reaction system developed by<br />

the company BTS/Ehrfeld Micro-Technology enables<br />

the user to change the plant configuration himself.<br />

Depending on the modules, it is possible to realise<br />

pressures up to <strong>10</strong>0 bar and temperatures in the<br />

range of -20 to 200 °C. Additional modules extend<br />

this working range. The CryoReactor, for instance,<br />

enables low temperature reactions down to -<strong>10</strong>0 °C.<br />

All materials in contact with media are mainly made<br />

of stainless steels like DIN 1.4571 or 1.4401. Seals<br />

are either made of PTFE or perfluorinated<br />

elastomers, such as FFKM. Other materials like<br />

Hastelloy are available on request.<br />

In order to run the Modular Microreaction System for<br />

laboratory-scale experiments, only some standard<br />

peripheral devices are necessary in addition. <strong>HiTec</strong><br />

<strong>Zang</strong> will gladly assist you with advice in selecting<br />

suited devices and is able to supply individual<br />

components as well as complete ready-to-use fullyautomated<br />

plants.<br />

There are approximately 30 different modules<br />

available, e.g.:<br />

� Mixer<br />

� Reactors<br />

� Heat Exchanger<br />

� Filter<br />

� Heating Modules<br />

� Sensors<br />

� Valves<br />

� Pumps etc<br />

All components of the modular micro-reaction<br />

system are mounted on a base plate with a square<br />

grid. One grid cell has the a length of 25 mm.<br />

Accordingly, the smallest lateral length of a module<br />

is 25 mm, including a 1 mm strong seal disc. The<br />

height of a module depends on its specific function.<br />

Base plates are available in the formats A3 (16x12<br />

grid cells), A4 (12x8 grid cells) and A5 (8x6 grid<br />

cells).<br />

Stand-alone-Module<br />

The direct connection concept of the Modular Microreaction<br />

System offers unique advantages. The<br />

plants can be assembled quickly and easily, and can<br />

be easily adjusted to the respective synthesis<br />

problem. Due to the consistent waiving of tube<br />

connections and screwings between the individual<br />

modules, dead storage is reduced to a minimum.<br />

In spite of this, reactors or heat exchangers can be<br />

connected to an already existing periphery as standalone<br />

modules with 1/8” Swagelok fittings. The high<br />

flow modules with 1/8” Swagelok fittings are also<br />

available in such a version.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Automatic Laboratory Reactor Systems<br />

The Automation Technology The LabManager/LabVision-System, with a special<br />

operating interface module (Ehrfeld BTS or Syntics),<br />

is very well-suited for micro-reaction plants. You can<br />

find further details on this topic in the chapter<br />

„Laboratory Automation Software“.<br />

In combination with our Liquid-Handling-Systems, it<br />

is possible to establish fully-automated screening<br />

equipment. Samples are provided programcontrolled.<br />

Test parameters are set according to plan<br />

and test samples are filled.<br />

Would you like to know more about the possibilities<br />

of this fascinating technology?<br />

Just give us a phone call. We will gladly advise you!<br />

Note<br />

Suitable pumps can be found in the chapter Dosing Systems and Pumps.<br />

Suitable sensors, eg. low dead space pressure receivers can be found in the chapter Process Analytics and<br />

Sensors.<br />

� Formulating Stations<br />

� Customer specific plant<br />

� Component for reaction calorimeters<br />

can be found in the chapter Construction and Miniplant Technology<br />

Reactant mixing pumps can be found in the chapter Dosing Systems and Pumps.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 25<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


26<br />

Here you will find:<br />

� LabKit TM -rcf Heat Flow Calorimetry (HFC)<br />

� LabKit TM -rcb Thermal Balance Calorimeter<br />

� KalDas TM Calorimetry Evaluation<br />

� Reaction calorimetry components<br />

Reaction Calorimetry<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Reaction Calorimeters<br />

Until now, reaction calorimeters and automatic<br />

laboratory reactors, which were able to handle more<br />

than only simple syntheses, had to be regarded<br />

separately. The <strong>HiTec</strong> <strong>Zang</strong> LabKit-rc reaction<br />

calorimeters combine both devices, whereby a<br />

flexible system is generated in every respect. As a<br />

calorimeter, LabKit-rc offers different operation<br />

modes and measuring methods, and as a lab<br />

reactor system, the whole flexibility of the LabKit<br />

laboratory reactor technology and the LAB<br />

manager’s research process control system.<br />

Up to now, reaction calorimeters were very costintensive.<br />

Nevertheless, they are necessary. The<br />

knowledge of the heat tone of a process is required<br />

for the safety-related and energetic evaluation.<br />

Many users are therefore on the lookout for a costeffective<br />

possibility to conduct calorimetric<br />

measurements already during process development.<br />

In addition, according to the opinion of leading<br />

scientists, the significance of reaction calorimetry<br />

for process analytics is underestimated by far. In the<br />

event of all exothermal and endothermal processes,<br />

the signal of the current heat output delivers<br />

additional information on the reaction progression,<br />

which is currently only rarely utilised.<br />

The Advantages:<br />

� Heat Flow and Thermal Balance are possible<br />

� Isothermal, Isoperibole and Adiabate Mode of<br />

Operation<br />

� Full ALR Functionality<br />

� Uncomplicated Evaluation<br />

� Easy-to-handle Open System<br />

� Upgradeable at all Times<br />

� Electrically lowerable Reactor Head<br />

� Best possible Reproducibility<br />

� GLP-conform Documentation<br />

� Access via Network, e.g. from the Office<br />

� Remote <strong>Main</strong>tenance (Tele-Service)<br />

Reaction Calorimetry<br />

The range of possible applications is very versatile<br />

and goes far beyond the classical measurement of<br />

heat tone and thermal conversion.<br />

LabKit-rc supports adiabate, isoperibole, and<br />

isothermal operation mode.<br />

LabKit-rc Systems are ready-to-use reaction<br />

calorimeters.<br />

To allow upgrading or modernising of existing<br />

laboratory reactors or existing reaction calorimeters,<br />

all necessary components are also individually<br />

available.<br />

The standard systems LabKit-rcf and LabKit-rcb<br />

depicted in the following, are complete, ready-forcommissioning,<br />

automatic reaction calorimeters,<br />

which can also be utilised as full-fledged Automatic<br />

Labor Reactor Systems (ALRS). They can be<br />

upgraded with the available additional modules and<br />

components of the LabKit program.<br />

Next to the standard calorimeters depicted in the<br />

following, we also manufacture client-specific<br />

plants and also offer the renovation, repair, and<br />

expansion of existing reaction calorimeters of<br />

various manufacturers.<br />

Information in regard to the individually<br />

manufactured reaction calorimeters can be<br />

found in the chapters Plant Construction, Miniplant<br />

Technology, and Customised Reaction<br />

Calorimeters.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 27<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


28<br />

Reaction Calorimetry<br />

LabKit-rcf Heat Flow Reaction Calorimeter<br />

LabKit-rcf, heat flow calorimeter with extension options<br />

Reaction calorimeter in a sophisticated<br />

configuration for heat flow calorimetry. The<br />

automatic laboratory reactor system is suitable e.g.<br />

for syntheses in the temperature range from -40 to<br />

+200 °C. The system is expandable with<br />

additional modules and components offered.<br />

System Construction<br />

As standard container, a double-walled 2 litre<br />

reaction vessel is used. Other containers are<br />

available.<br />

The reaction vessel is kept at a moderate<br />

temperature by high performance heating/cooling<br />

thermostats, which enables fast temperature<br />

control for isothermic use.<br />

Measurement Method<br />

The heat flow method is based on the<br />

measurement of the temperature difference<br />

between the reactor contents and temperature<br />

medium in the container jacket. For the heat flow<br />

over the reactor wall the relationship applies:<br />

Q& = k A⋅ΔT<br />

kond<br />

w<br />

The heat transition coefficient cannot generally be<br />

theoretically calculated. Since it can vary<br />

significantly during reaction (e.g. by modification<br />

of the viscosity, the specific heat of the reaction<br />

mixture, or by boundary layer formation), it is<br />

determined by calibration with defined heat output<br />

before and after the reaction.<br />

k<br />

w<br />

Q<br />

A =<br />

ΔT<br />

&<br />

kond<br />

RJ<br />

RJ<br />

The reaction calorimeter is extendable for heat<br />

balance calorimetry and can be optionally<br />

upgraded by<br />

� Online Evaluation<br />

� Inerting<br />

� Vacuum<br />

� Distillation<br />

� Reflux<br />

For reflux distillation, the reflux separator ratio is<br />

adjustable over a programmable reflux separator.<br />

For further information see "Components for<br />

reaction calorimetry"<br />

Example Version:<br />

LabKit-rcf with electrically lowerable <strong>10</strong>00 ml reactor with<br />

vacuum jacket, two gravimetric and one volumetric dosing<br />

circuits, vacuum control, reflux distillation and inerting.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Specification<br />

Reaction Calorimetry<br />

Rack Square anodised aluminum profile, electrical fixture for lowering the reactor<br />

vessel, catch pan made of high-grade steel.<br />

Reactor 2-Liter Double-walled glass container, tempering jacket, PTFE-bottom drain valve,<br />

Lid with Center neck and 6 Supports, safety-valve 200 mbar, ventilation valve<br />

Stirrer ViskoPakt rheo57 Precision stirrer drive with Speed control and Torque<br />

measurement, Anchor Stirrer<br />

Heating/Cooling System Heat-Cool-Thermostat -40 to +200 °C, Air-/ Compressor Cooling, Heating power 3<br />

kW, Cooling power to 3 kW at 200 °C, 0,7 kW at 0°C<br />

Dosing System One GraviDos Dose circuit for Liquids (Regulated drop funnel), 500 ml feed tank,<br />

gravimetric regulated<br />

Automation LabManager. Interfaces: 8 Pt<strong>10</strong>0 Precision-Temperature measurement inputs, 8<br />

analogue inputs (Current & Voltage) of which 1 pH, 4 RS232, 4 GraviDos (DMS)<br />

Interfaces, 4 digital inputs, 8 digital Outputs (current & voltage), controllable<br />

calibration heating 50 W glass (optionally stainless steel). Sensor power supply<br />

24 V 1,5 A, actor power supply 24 V 3 A.<br />

CA-ABK2, 22“ Monitor, Uninterrupted Power Supply with UPS-Management<br />

Software<br />

Sensors Calibrated temperature sensor for: reactor, thermostat, flow line, reflux, head and<br />

environment temperature, flowmeter in the heat carrier, preasure measurement<br />

0...1600 mbar abs., stirrer: rotational speed, torque<br />

Materials <strong>Main</strong>ly borosilicate glass, PTFE, PVDF, Viton, Stainless steel 1.4571 (changes<br />

possible)<br />

Evaluation see KalDas<br />

Order Code Description<br />

VL-LABKITRCF1 Reaction calorimeter for heat flow calorimetry<br />

VL-LABKITRCONLF Online-heat flow-Evaluation<br />

Special equipment is available e.g. for inerting,<br />

vacuum, reflux boiling and reflux distillation using<br />

the programmable reflux separator and intensive<br />

cooler in a mirrored glass vacuum jacket,<br />

Recommended software packages:<br />

as well as balancing of the cooling water and<br />

distillate. See lab kit structure system.<br />

Order Code Description<br />

SL-LABVIPBATE Software Package for LabManager1 for Operation of medium-sized Batch-Processes<br />

SF-PID8 Controller Module with 8 PID- and application oriented controllers<br />

SA-KALDAS3 Evaluation Program for Heat Flow and Thermal Balance Calorimetry on KabKit-rcb<br />

Recommended upgrades<br />

� MoleculeEye with fibre optic probe for differentiated, cinetic analysis<br />

Further information can be find in the chapter Process Analytics and Sensorics.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Components<br />

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Dosing Systems,<br />

Pumps<br />

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Stirring and<br />

Dispersing<br />

Services


30<br />

Reaction Calorimetry<br />

LabKit-rcb-Heat balance - Reaction Calorimeter<br />

LabKit-rcb, heat balance calorimeter with expansion.<br />

Reaction calorimeter in a sophisticated<br />

configuration for heat flow and heat balance<br />

calorimetry. The automatic lab reactor system is<br />

suitable e.g. for syntheses in the temperature<br />

range from -40 to +200 °C. The system is<br />

expandable with the offered additional modules<br />

and components.<br />

System Construction<br />

As standard container for heat balance calorimetry,<br />

a triple wall, 2 litre reaction container with<br />

evacuated outer jacket is used. Other containers<br />

are available.<br />

The reaction container is kept at a moderate<br />

temperature by high performance heating/cooling<br />

thermostats, which enables a fast temperature<br />

control for isothermic operation mode.<br />

It is upgradeable with options, e.g.:<br />

� Online-Evaluation<br />

� Vacuum<br />

� Distilling<br />

� Reflux<br />

� Inerting<br />

When distilling with reflux separators, the reflux<br />

component ratio can be regulated via an<br />

electrically controllable reflux separator.<br />

For further information, see „Components for<br />

Reaction Calorimetry“.<br />

LabKit-rcf with electrically lowerable 1 litre reactor with vacuum<br />

jacket, 3 gravimetric dosing circuits, vacuum control, reflux<br />

distillation and inerting.<br />

Measurement Method<br />

The heat balance method is based on the<br />

balancing of the tempering medium at the feed and<br />

discharge opening of the container jacket. The<br />

temperatures and the flow of the heat carrier are<br />

measured.<br />

Q& = m&<br />

⋅cp<br />

⋅ ΔT<br />

Kond<br />

öl<br />

öl<br />

RJVR<br />

The heat transition coefficient (KwA) is not required<br />

for the evaluation. This is particularly important in<br />

case of reactions where a coating develops at the<br />

vessel walls, as for example, during<br />

polymerisations and dispersions.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Specifications<br />

Reaction Calorimetry<br />

Rack Square anodised aluminum profile, electrical fixture for lowering the reactor<br />

vessel, catch pan made of high-grade steel.<br />

Reactor 2Liter Double jacket glass container with vacuum jacket, temper jacket, PTFEbottom<br />

drain valve, lid with centre neck and 6 supports, safety valve 200 mbar,<br />

ventilation valve<br />

Stirrer ViskoPakt rheo57 Precision-stirrer drive with speed control and torque<br />

measurement, Anchor Stirrer<br />

Heating/Cooling System Heat-cool-Thermostat, -40 to +200 °C, Air/ Compressor cooling, heating power 3<br />

kW, cooling power up to 3 kW (200 °C), 0,7 kW (0°C)<br />

Dosing System One GraviDos Dose circuit for liquids (regulated Drop funnel), 500 ml Feed tank,<br />

gravimetric regulated<br />

Automation LabManager. Interfaces: 8 Pt<strong>10</strong>0 Precision-Temperature measurement inputs, 8<br />

analogue inputs (Current & Voltage) of which 1 pH, 4 RS232, 4 GraviDos (DMS)<br />

Interfaces, 8 digital inputs, 8 digital Outputs (current & voltage), controllable<br />

calibration heating 50 W glass (optionally stainless steel)<br />

CA-ABK2, 22“ Monitor, Uninterrupted Power Supply with UPS-Management<br />

Software<br />

Sensors Calibrated temperature sensor for: reactor, thermostat, flow line, reflux, head and<br />

environment temperature, flowmeter in the heat carrier, preasure measurement<br />

0...1600 mbar abs., stirrer: rotational speed, torque<br />

Materials <strong>Main</strong>ly glass, PTFE, PVDF, Viton compound, stainless steel material 1.4571<br />

(subject to changes)<br />

Evaluation see KalDas<br />

Order Code Description<br />

VL-LABKITRCB1 Reaction calorimeter for Heat balance calorimetry<br />

VL-LABKITRCMDM Mass flow meter for the heat carrier<br />

VL-LABKITRCONLB Online heat balance evaluation<br />

Optional equipment is available, e.g. inerting,<br />

vacuum, reflux boiling and distilling via a<br />

electrically controlled reflux separator and intensive<br />

cooler made of metallised glass, with vacuum<br />

jacket as well as balancing of the cooling water<br />

and the distillate.<br />

For further information see LabKit system<br />

construction.<br />

Recommended software packages:<br />

Order code Description<br />

SL-LABVIPBATE Software Package for LabManager1 for Operation of medium-sized Batch-Processes<br />

SF-PID8 Controller module with 8 PID and application oriented controller<br />

SA-KALDAS3 Evaluation Program for Heat Flow and Thermal Balance Calorimetry on KabKit-rcb<br />

Recommended upgrades<br />

� MoleculeEye with fibre optic probe for differentiated, cinetic analysis<br />

Further information can be find in the chapter Process Analytics and Sensorics.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


32<br />

Reaction Calorimetry<br />

Calorimetry Evaluation Program KalDas<br />

Uncomplicated Evaluation!<br />

►<br />

KalDas is a new development in the field of reaction<br />

calorimetry. KalDas provides you with data that you<br />

need for model evaluations (e.g. scale up) and for<br />

energy and safety considerations.<br />

KalDas is based on the flexible control and data<br />

analysis software platform HiText and can therefore<br />

be easily customised to your special requirements.<br />

The acquired data can be evaluated at the push of a<br />

button and the results are displayed in a free<br />

configurable and a clearly arranged protocol.<br />

KalDas was primarily developed for the <strong>HiTec</strong><br />

reaction calorimeter. However, there is no<br />

constriction to any specific calorimeter, i.e. the<br />

program may be adapted to any other device.<br />

It is also possible to adjust the programming for<br />

special evaluations or data transfer, e.g. to programs<br />

for reaction kinetics.<br />

Heat inflow and dissipation of the stirrer, condenser,<br />

dosage flow as well as accumulated heat is<br />

considered in the calculation. If needed, the<br />

calculations may be expanded to heat balance<br />

calorimetry or other methods.<br />

KalDas is deployed for:<br />

� Product Development<br />

� Process Optimisation<br />

� Quality Assurance<br />

� Scale Up Tests<br />

� Plant Safety<br />

KalDas3 was completely newly designed based on<br />

the proven KalDas2. The programming in HiText<br />

warrants for optimal cooperation with LabVision and<br />

enables online calorimetry.<br />

KalDas ideally operates combined with the HiBatch<br />

Recipe Control. The steps related to reaction<br />

calorimetry are integrated like normal basis<br />

operations in the recipe.<br />

The delays of the measurement signals which lead<br />

to distortions in the course of the power output<br />

evaluation are corrected by special algorithms. This<br />

allows realistic presentation of the output power<br />

progression.<br />

Advantages:<br />

� Simple Handling<br />

� Online and Offline Evaluation in one Program<br />

� Flow and Balance Evaluation simultaneously<br />

possible<br />

� Dosing, Reflux, and Dissipation are<br />

considered<br />

� Intermediate Values (Outputs) are made<br />

transparent<br />

� Fully integrated in LabVision, optional Standalone<br />

Version<br />

� First Analyses are already possible during the<br />

running Test<br />

� Alignment to your possibly already existing<br />

Equipment is possible<br />

� Application-specific Expansions are possible<br />

due to HiText Programming<br />

� Full Functionality of an Automatic Laboratory<br />

Reactor is supported<br />

� Multi-stage Recipe-controlled syntheses are<br />

possible<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Reaction Calorimetry<br />

Product Description Menu-controlled evaluation program for calorimetry data, compilation of<br />

measurement data, characteristics determination, graphic presentation, inter alia<br />

of output and heat curves, etc.<br />

Delivery Scope CD-ROM, manual<br />

Order Code Description<br />

SA-KALDAS3 Evaluation Program for the Reaction Calorimetry on LabKit-rcf and -rcb<br />

For control operations, see LabVision Basis Operations.<br />

KalDas can also be aligned to your equipment!<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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Hardware<br />

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Software<br />

Plant<br />

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Technology<br />

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Process Analytics<br />

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34<br />

Reaction Calorimetry<br />

Components for Reaction Calorimetry<br />

Calibration Heating<br />

The calibration heating is required when conducting<br />

calorimetric measurements in reaction calorimeters<br />

or laboratory reactors. In particular for the<br />

establishment of the thermal capacity of a material<br />

within the scope of a heat flow calorimetry, a highprecision<br />

calibration heating is required which<br />

compensates the thermal resistance, e.g. as a result<br />

of aging and temperature influences. The heating<br />

output of the following devices can be steplessly<br />

Technical Data<br />

Power consumption 230 V, <strong>10</strong>0 W / 150 W<br />

Delivery of power 0 ... 50 W , 0 ... <strong>10</strong>0 W, <strong>10</strong>0 % duty cycle<br />

Uncertainty


Turbine Flowmeter for Heat Carrier Oil<br />

Thermal balance calorimetry requires the exact<br />

measurement of the flow rate of the heat carrier oil.<br />

The flow sensors are especially suited for this<br />

purpose and are frequently used as an alternative to<br />

the significantly more expensive Coriolis mass flow<br />

meters.<br />

In the sector of reaction calorimetry, they are<br />

particularly suited for the flow measurement of the<br />

heat carrier oil at temperatures of up to 350 °C.<br />

They are deployed as standard in our thermal<br />

balance calorimeters.<br />

Technical Data<br />

Reaction Calorimetry<br />

They function according to the principles of a<br />

turbine-type meter:<br />

Type Measuring Range<br />

in l/min<br />

Impulse/Litre Connection G<br />

TDM06 1 to <strong>10</strong> 2000 ½ inch<br />

TDM09 3 to 30 980 ½ inch<br />

The Advantages:<br />

Linearity +/-2 % v.M.<br />

Reproducibility +/-0.5 %<br />

Media Temperature -20 to 120, 180 or 350 °C<br />

Max. Working Pressure 20 bar<br />

Viscosity 0,1 to 6 mm²/s<br />

Materials High-grade steel 1.4305 and 1.4122, ceramic<br />

Seal Viton or Graphite<br />

Content of delivery: Sensor with mounted impulse amplifier<br />

Order code Description<br />

IS-F-TDMtc-tb-sa Turbine Flowmeter<br />

IS-F-TDMMV-AK-I LAB-PI Connection Cable for Turbine Flow Sensor , 4..20 mA<br />

IS-F-TDMMV-AK-F LAB-PI Connection Cable for Turbine Flow Sensor, NPN-OC<br />

tc = up to <strong>10</strong> litres/min: 06 / up to 30 litres/min: 09<br />

tb = Temperature Range 120,180, or 350 °C<br />

sa = Output Signal 4..20 mA: I / or frequencyanalogue<br />

NPN-OC: F<br />

� Compact<br />

� <strong>Main</strong>tenance-Free<br />

� Resistant against high Temperatures<br />

� Low Pressure Loss<br />

� High Working Pressure Range<br />

� Small Time Constant due to low-mass Rotor<br />

Example for an order:<br />

Flow sensor for 0-<strong>10</strong> litres/min, max. temperature<br />

180 °C, frequency-analogue output, open collector:<br />

IS-F-TDM06-180-F<br />

Information in regard to the individually<br />

manufactured reaction calorimeters can be<br />

found in the chapters Plant Construction,<br />

Miniplant Technology, and Customised Reaction<br />

Calorimeters.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Components<br />

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Dispersing<br />

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36<br />

Here you will find:<br />

Fermentation Technology<br />

� RAMOS® Bioprocess Optimisation in Shaking Flasks<br />

� FluidTrain Fed-batch and Sample Drawing in Shaking Flask<br />

� OmniFerm® - Mini-Fermenter System<br />

� HiFerm-FCU Client-specific Fermenter Control Systems<br />

� Gmix Precision Gas Mixing Device<br />

� AlcoTect sterilisable alcohol probe<br />

� HiSense Precision Exhaust Gas Analytics<br />

� RQFeed Feeding Algorithm for optimal Productivity<br />

� Packed Bed Reactor<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Fermentation Technology<br />

RAMOS ® Bioprocess Optimisation in Shaking Flasks<br />

RAMOS (Respiration Activity MOnitoring System) is<br />

the standard measurement system online<br />

determination of respiration activities of prokaryotic<br />

and eukaryotic cultures in shaking flasks.<br />

The respiration rate is usually directly proportional to<br />

the number of cells and therefore enables<br />

continuous monitoring of the growth progression.<br />

Clear Advantages<br />

� More information about your microbiological<br />

processes<br />

� Distinction of process-related and biological<br />

effects.<br />

� Replaces expensive experiments in the<br />

fermenter.<br />

� Identical cultivation conditions as in your<br />

reference shaking flask.<br />

� Easy handling<br />

� Reduction of development time for<br />

bioprocess and cultivation conditions<br />

� Provides ideal screening conditions.<br />

� Enables rapid characterisation and targeted<br />

optimisation of media.<br />

� Reduction of test period to the actually<br />

required time.<br />

� Shortens the „time-to-market“.<br />

RAMOS was developed in cooperation with the<br />

department of biochemical engineering (Aachen<br />

University of Technology - UAS).<br />

RAMOS supplies the required information for:<br />

� Process Development<br />

� Process Optimisation<br />

� Media Optimisation<br />

� Fermentation Validation<br />

� Scale-Up<br />

Until now, in numerous processes evaluated so far,<br />

RAMOS has contributed to reveal key insights and<br />

Fields of Application<br />

� Continuous growth monitoring of prokaryotic and<br />

eukaryotic cultures including mammalian cells in<br />

shaking flasks<br />

� 8-fold parallel online measurement of the<br />

respiration activity under sterile conditions<br />

� Easy determination of characteristic values<br />

(OTR, CTR, RQ, µmax, kLa ...)<br />

� Bioprocess optimisation through early<br />

identification of oxygen and substrate limitation or<br />

product inhibition<br />

� Bioassays (toxicity assay, proliferation assay)<br />

� Development of suitable conditions in the primary<br />

and secondary screening (culture duration,<br />

media, operating conditions)<br />

� Reduction of the development times for ideal<br />

culture media and media conditions<br />

� Mass balance of fermentation processes<br />

� Quality control<br />

Potential<br />

Many experiments which previously could only be<br />

carried out laboriously in a fermenter with gas<br />

analytics, can now be conducted much cheaper and<br />

moreover in a fraction of the time with RAMOS.<br />

RAMOS pays off within short time due to the<br />

reduction of laboratory hours and development<br />

periods. In addition, production costs can be<br />

consistently and significantly reduced due to more<br />

efficient strains and culture procedures which can be<br />

discovered with the help of RAMOS.<br />

Up To now the development of suitable media has<br />

always been neglected due to the large connected<br />

expenditures. Exemplary for this fact is that LBmedia<br />

were used for decades as standard media for<br />

Escherichia coli bacteria.<br />

Already the initial investigation with RAMOS led to<br />

the insight that this medium does not allow an<br />

optimum growth due to its insufficient buffer effect.<br />

One can securely analyse the behaviour of microbial<br />

cultures with the help of measuring curves delivered<br />

by RAMOS, e.g.:<br />

� substrate limitation<br />

� oxygen limitation<br />

� product inhibition<br />

� diauxic growth<br />

the decisive impulses for research that has been<br />

worked on for years.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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Software<br />

Plant<br />

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Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

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Dispersing<br />

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38<br />

The demand for equal cultivation conditions for<br />

micro-organisms in normal shaking flasks and in<br />

RAMOS-Measuring flasks was given priority in the<br />

development of the plant. For this reason, the design<br />

of the flask was devised, in regard to the gas and<br />

hydrodynamics, so that it accords to a normal<br />

shaking flask in the bottom part containing liquid.<br />

In addition, a method was developed which enables<br />

to determine the oxygen transfer merely out of the<br />

variation of the oxygen partial pressure in the head<br />

space of the measuring flasks (no invasive<br />

electrodes). The system is patented.<br />

To ensure equivalent cultivation conditions, the gas<br />

composition above the culture liquid in the flasks of<br />

the measuring plant is adjusted identically to the<br />

composition in a normal flask. For this purpose, the<br />

gas flow is set client-specifically (depending on the<br />

type of sterile seals used).<br />

The system handling can be learned very easily and<br />

quickly. Within a short period of time, you will not be<br />

able to imagine to work without RAMOS<br />

The RAMOS System<br />

Fermentation Technology<br />

The RAMOS system fits on a normal benchtop. It is<br />

delivered completely installed with flasks, sensors,<br />

shaker, incubator, and control PC including an<br />

uninterrupted power supply system.<br />

For the familiarisation with the new methods, we<br />

offer one to two-day seminars and training<br />

programmes.<br />

Measurement of the Oxygen Transfer Rate<br />

The oxygen transfer rate is the most suitable and<br />

most universal variable to characterise and quantify<br />

the physiological condition and the activity of an<br />

aerobe culture because almost every metabolic<br />

activity is combined with oxygen consumption.<br />

The online measurement of the oxygen transfer rate<br />

in shaken bioreactors is state-of-the-art, however it<br />

is technically very laborious. The determination of<br />

the oxygen transfer rate in shaken bioreactors<br />

(shaking flasks) under sterile conditions has yet not<br />

been possible. RAMOS closes this gap and<br />

therefore combines the advantages of shaking flasks<br />

(little space required, cost-efficient, the possibility of<br />

parallel operation) with those of a stirred bioreactor<br />

(online-measurement).<br />

OTR- Phenomena<br />

The figure gives a schematic selection of biological<br />

phenomena and their effect upon the oxygen<br />

transfer rate (OTR). The diagrams show how the<br />

behaviour of a microbial culture can be<br />

systematically analysed with the help of the<br />

measuring curves delivered by RAMOS.<br />

Measuring of the Carbon Dioxide Transfer Rate<br />

Next to the oxygen transfer rate, the carbon dioxide<br />

transfer rate (CTR) and the respiratory quotient (RQ)<br />

are important sources of information for<br />

microbiologists.<br />

The temporal development of OTR, CTR and RQ<br />

can be clearly monitored online.<br />

In addition, further process parameters are<br />

calculated hereof. The evaluation can be extended<br />

according to user specifications.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


The development of OTR, CTR and RQ can be<br />

viewed online at your screen. The user interface<br />

presents also further computed parameters. This<br />

analysis can be adapted and extended to customer<br />

needs.<br />

From the general overview, showing all of the 8<br />

flask, each flasks diagram can be selected<br />

individually.<br />

Fermentation Technology<br />

The diagramm show charts of the OTR, CTR and<br />

RQ of an yeast fermenetation with crabtree effect.<br />

Technical Data (RAMOS installation for 8+6 shaking flasks including shaker and incubator.)<br />

Dimensions width: 690 mm, height: 750 mm, depth: 490 mm<br />

Weight approx. 66 kg (device without cooling)<br />

Size of Shaking Tray 420 x 420 mm<br />

Measuring Flasks 8 graduated flasks (250 ml) plus 6 auxiliary perpendicular shaking flasks (250 ml)<br />

for sampling or 8 graduated flasks (500 ml). Other sizes on request<br />

Electrical Connections 230 V AC, 3 A, other voltages upon request<br />

Gas Connections none, intake of ambient air<br />

Resolution Oxygen transfer rate


40<br />

Fermentation Technology<br />

Feeding and Sample Drawing in Shaking Flasks<br />

Fluid-Train ® -Technology<br />

Pharmaceutically relevant products, such as insulin,<br />

antibodies, and many more, are synthesised by<br />

microorganisms and cell cultures in bioreactors.<br />

With the Fed-batch regulation, the pro- or eukaryotic<br />

cells are fed on a defined and regulated basis. Up to<br />

now, the use of this procedure was restricted to<br />

large-scale production to achieve optimal biomass,<br />

respectively product yield.<br />

RAMOS-Fed-batch provides fully automatic Fedbatch<br />

fermentation in shaking flasks. The parallel<br />

technology and the approved measurement<br />

procedure of the RAMOS were expanded by an<br />

automated dosing system.<br />

RAMOS-Fed-batch makes controlled feeding<br />

possible and regulates the dosing rates based on<br />

the oxygen transfer rate (OTR) or respiration<br />

quotient (RQ). The cell number-independant key<br />

parameter RQ gives information on the physiological<br />

condition and is evaluated from the oxygen and<br />

carbon dioxide transfer rate (CTR) and thus allows a<br />

metabolism-dependant regulated dosing. The<br />

targeted regulation of the ideal RQ value can<br />

therefore be utilised to achieve maximum product<br />

yield. Based on these results, a feeding algorithm<br />

was developed, which enables to to keep a<br />

physiological condition constant without drawing any<br />

samples and analytics. The dosing amount is<br />

precisely recorded by the software.<br />

Technical Data<br />

The innovative Fluid-Train Dosing and Sample<br />

Drawing Technology (FTT) ensures a comminglingfree<br />

dosing and sample drawing conducted through<br />

merely one tube. Consequently, it is possible to<br />

seperatly and sterilely dose two or optionally more<br />

different media into each individual shaking flask.<br />

The combination with the RAMOS measuring data<br />

enables the feeding of the cultures with exactly the<br />

required amount of substrate, which leads to ideal<br />

culture growth and ideal production, respectively.<br />

The diagram show a dosing control upon the OTR<br />

value. The starting set point of 0,004 mol/l*h is being<br />

reduced after 45 hrs. to 0,002 mol/l*h. After approx.<br />

ca. 60, 90 and <strong>10</strong>0 std. the feeding of media will be<br />

temporarily interrupted.<br />

Parallel, up to 24 samples are, either event or<br />

schedule-controlled, are drawn from the culture<br />

containers and deposited (AutoSam-s). This makes<br />

unattended operation over night or weekend<br />

possible.<br />

Rinsing and cleaning cycles warrant a<br />

contamination-free operation. The Fluid-Train<br />

Technology is applied for the fermentation of proand<br />

eukaryotic organisms.<br />

Receiver Bottle 2 Feed-Media Bottles, 1 Bottle NaOH, 1 Bottle ultra-pure Water<br />

Dosing Rate 1-2 ml per flask and dosing cycle, cycle period<br />

Order Code Description<br />

VA-RAMOSFTT8 Program-controlled dosing and sample drawing , 8 channels including 4 receivers<br />

VA-RAMOSCON8 RAMOS Dosing regulation for control variable = OTR, CTR or RQ, 8 channels<br />

RAMOSFTT8 requires an AutoSam sampling device IL-AUTOSAM-xx and if necessary a cooling<br />

incubatro IL-AUTOSAM-KL.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Fermentation Technology<br />

OmniFerm ® - Mini Fermentation System<br />

The OmniFerm-Mini bioreactor system is suited for<br />

the controlled cultivation of bacteria and yeasts, as<br />

well as plant, insect and mammalian cell cultures. It<br />

features an especially small footprint so that several<br />

fermenters can be placed on a laboratory bench.<br />

This small-scale fermentation system closes the gap<br />

between shaking flasks and laboratory fermenters.<br />

Results which were achieved in shaking flask<br />

cultures can be validated parallelly with minimal<br />

substrate use and time expenditure.<br />

The modular design and the multiple equipping<br />

options allow maximum flexibility compared to<br />

conventional systems.<br />

The basic unit consists of a glass vessel with a<br />

stainless steel lid individually including the required<br />

sockets (bore holes: 2 x Pg 13.5, 7 x UNF 1/4-32, 1<br />

x UNF 1/2-20 for exhaust cooler). The pH-value is<br />

measured with an invasive electrode and can<br />

optionally be controlled by CO2/base or acid/base.<br />

The reactor is aerated via the head space, a gassing<br />

tube or a gassing ring.<br />

The optionally integrated off-gas analytics system<br />

unit records the progression of the OTR, CTR, RQ,<br />

OT, CT, and µmax online. These values allow drawing<br />

conclusions in regard to the proliferation rate and the<br />

metabolic activity of the biological culture. Due to the<br />

integrated pO2-electrode, conclusions can be drawn<br />

out of comparison between dissolved oxygen and<br />

oxygen transfer rate.<br />

The fermentation control and regulation is based on<br />

a <strong>HiTec</strong> <strong>Zang</strong> MSRmanager system with a special<br />

interface module. Amongst others, it is possible to<br />

connect laboratory apparatuses like balances,<br />

special sensor systems, analysers, dosing systems,<br />

etc. Due to the proven PMC technology,<br />

simultaneous parallel operation of up to 8 reactors is<br />

possible in bus or star-shaped alignment. Highprecision<br />

dosing controllers ensure controlled<br />

feeding in semi-continuous and continuous<br />

operation mode.<br />

Characteristics<br />

� full laboratory fermenter functionality<br />

� high degree of automation<br />

� various types of sensors<br />

� control based on online analysis is possible<br />

� tempering without heat carriers<br />

Options<br />

� Client specific equipment<br />

� Free programmable recipe control<br />

� Freely configurable test report<br />

� OTR- and RQ-based feed regulation for optimal<br />

product yield, e.g. within pharmaceutical protein<br />

production<br />

� Gravimetric dosing<br />

You have the choice between containers with<br />

operating volumes of 150 to 2000 ml. The reactor<br />

can be removed quickly and easily for sterilisation or<br />

preparation.<br />

The stirrer is powered by a rpm-regulated DC motor.<br />

High-class shaft seals ensure maximum sterility.<br />

Alternatively or complementary, a magnet stirrer is<br />

available for shear-tolerant micro-organisms.<br />

The gas supply of the reactor can be optionally<br />

controlled by a rotary flow meter manually, or<br />

automated with high-quality mass flow controllers. It<br />

is likewise possible to control the gas mixture for the<br />

fermenter with a Gmix gas mixing station. For<br />

distinct off-gas analytics, the precise compliance of<br />

gas flow rates must be ensured. The Gmix gas<br />

mixing device meets the highest demands in this<br />

respect.<br />

The trend-setting automation software LabVision® in<br />

combination with the required extension modules,<br />

like EasyBatch and HiBatch-recipe control, allows<br />

the solution of complex and automation-technically<br />

demanding problems, like individual fed-batch<br />

operation in up to 8 reactors.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 41<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


42<br />

Technical Data<br />

Fermentation Technology<br />

A basic project including all functionalities necessary<br />

for standard batch operation, operating displays and<br />

parameterisations is expandable almost without<br />

limit. The detectable parameters are: pH, pO2, gas<br />

supply, gas mix, fed-batch control and chemostat<br />

operation mode.<br />

There are no limits of realisation to the model driven<br />

control based upon the established self describing<br />

programming language HiText.<br />

Dimensions width: 195 mm, depth: 300 mm, height: 500 mm<br />

Reactor Capacity 250 ml 600 ml <strong>10</strong>00 ml 2000 ml<br />

Working Capacity 150– 250 ml 300 – 600 ml 500 – <strong>10</strong>00 ml 500 – 2000 ml<br />

Bottle height (outer beand) 135mm 150mm 150mm 300mm<br />

Length of electrode 120 mm 120 mm 120 mm 225 mm<br />

Electrical Connection 230 V AC, 3 A<br />

Materials Glass, polished stainless steel 1.4573<br />

Sterilisation Auto-clavable<br />

Interfaces 2 x Pg 13.5, 7 x UNF 1/4-32, 1 x UNF 1/2-20<br />

Sensors temperature, optional pH, dissolved O2, Redox, level, foam, alcohol<br />

Pumps 4 rpm-regulated peristaltic pumps<br />

Temperature RT to 50 °C (optional, cooling with water or cooling agent)<br />

Gassing Dip tube, sparger or head space<br />

Shaft Sealing mechanical<br />

Order Code Description<br />

CG-OMNIFERM-ABK Control and Operating Unit for up to 8 OmniFerm Fermentation Units<br />

VA-OMNIFERM-FE-250 OmniFerm Fermentation Unit, reactor Capacity 150 to 250 ml, with four dosing pumps<br />

VA-OMNIFERM-FE-600 OmniFerm Fermentation Unit, reactor Capacity 300 to 600 ml, with four dosing pumps<br />

VA-OMNIFERM-FE-<strong>10</strong>00 OmniFerm Fermentation Unit, reactor Capacity 500 to <strong>10</strong>00 ml, with four dosing pumps<br />

VA-OMNIFERM-FE-2000 OmniFerm Fermentation Unit, reactor Capacity 500 to 2000 ml, with four dosing pumps<br />

VA-OMNIFERM-COOL Cooling functionality, integrate cooling coil for tapped water or thermostat, contol valve<br />

IL-OXYTECT-l Dissolved oxygen, autoclavable, PG 13.5 thread<br />

IL-PHFERM-l pH probe pH 0..14, 0 to 130°C, 0..<strong>10</strong> bar, autoclavable, PG 13.5 thread<br />

IL-ODFERM-l Cell count probe (optical density), autoclavable, PG 13.5 thread<br />

VA-OMNIFERM-CHILL Cooling thermostat 300 W at 15°C (provides up to 8 fermenters)<br />

VA-OMNIFERM-BGR Gassing Stirrer<br />

VA-OMNIFERM-AIRPUM Electronic controlled gasing pump for up to 4 fermenters, max. 550 l/h<br />

VA-OMNIFERM-GAS1 Gassing Control with pulsed Valve<br />

VA-OMNIFERM-GASMF Gassing Control with Massflow Controller<br />

VA-OMNIFERM-GASMF2 Gassingsregelung with two Massflow Controllers, e.g. Air and CO2<br />

VA-OMNIFERM-GASMF4MUX Gasing controll with massflow controller, tetra multiplexing, 4 gasses<br />

VA-OMNIFERM-REDOX Redox Sensor, auto-clavable, PG13.5 thread<br />

VA-OMNIFERM-LEV Level Sensor, auto-clavable<br />

VA-OMNIFERM-FOAM Foam Sensor, auto-clavable<br />

VA-OMNIFERM-FOLE Combination Sensor Level and Foam, auto-clavable<br />

VA-OMNIFERM-ETOH Alcohol Sensor, carrier gas supply, auto-clavable<br />

IL-HISENSE-m-x Exhaust Gas Analysis System for O2, OTR, CTR and CO2 for micro biology<br />

IL-HISENSE-c-x Exhaust Gas Analysis System for O2, OTR, CTR and CO2 for cell tissue cultures<br />

VA-OMNIFERM-RQFEED RQ-based Feeding<br />

X: amount of Channels, see HiSense, further volumes upon request<br />

Complementary products LabDos Precision Dosing Pump, AutoSam Sample Drawing System, Sterile Tube<br />

Pressure Sensor, Laboratory Scales can be found in other chapters.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Fermentation Technology<br />

HiFerm-FCU Customer-specific Fermenter Control Systems<br />

The level of automation of common bioreactors in<br />

microbiology and cell culture technology has a time<br />

lag of twenty years in relation to the automated<br />

laboratory reactor systems for chemical laboratories.<br />

<strong>HiTec</strong> <strong>Zang</strong> makes its experience of over 25 years in<br />

laboratory automation henceforth available for the<br />

customer-specific automated bioreactor.<br />

Example for a customised manufactured system with dosing<br />

pumps and touchscreen monitor.<br />

The advanced fermentation control unit HiFerm FCU<br />

allows the automated operation of a fermenter with<br />

an unprecedented level of automation.<br />

It is based on the MSRmanager automation system<br />

with a special interface module for sensors,<br />

actuators, and instruments.<br />

Sensors and actuators are connected with splash<br />

waterproof IP65 plugs and bushes, so that the<br />

connection is easy to install and, if necessary,<br />

disconnected quickly.<br />

The evaluation circuitry for oxygen, pH, temperature<br />

sensors etc. is integrated and can be expanded in<br />

various ways.<br />

For control of valves and pumps, analogue and<br />

digital outputs with short-circuit-proof semiconductor<br />

switches are provided.<br />

Analogue inputs for the connection of temperature<br />

sensors, electrodes, and miscellaneous sensors are<br />

digitalised with 24 bit and yield accordingly excellent<br />

measurement accuracy. Digital inputs allow<br />

connection of limit switches or malfunction<br />

annunciators of additionally connected devices.<br />

Via serial interfaces, laboratory devices like<br />

balances, special sensor systems, analysers, dosing<br />

systems, gas mixer, etc. can be connected.<br />

Dosing controllers for pump guided or gravimetric<br />

dosing are integrated. Thus, dosing systems can be<br />

driven by online measurement and analytic values.<br />

Interfaces<br />

� dissolved oxygen sensor (pO2),<br />

� direct connection for pH and redox sensors,<br />

(expandable to 2),<br />

� alcohol sensor,<br />

� 2 special inputs with current/voltage sources e.g.<br />

for a foam sensor,<br />

� 8 analogue inputs for flow rate controllers,<br />

temperature and pressure sensors etc.,<br />

� 8 analogue outputs for dosing pumps and stirrer<br />

control,<br />

� 16 digital outputs with short-circuit-proof<br />

semiconductor switch for magnetic valves,<br />

pumps, heater, etc.,<br />

� 14 digital inputs for fill level, pressure monitor,<br />

etc.,<br />

� 8 RS232 interfaces for balances, analysers,<br />

laboratory devices, etc.<br />

� 4 USB-Interfaces for keyboard, mouse, printer,<br />

memory stick, webcam, etc.<br />

With the automation software LabVision and the<br />

expansion modules, e.g. the EasyBatch or HiBatch<br />

Recipe Control, it is possible to realise complex and<br />

challenging automation tasks in an uncomplicated<br />

manner.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 43<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


44<br />

An user-friendly interface and an easy handling of<br />

the system assure a short preparation time.<br />

A basic project with the essential functions, views<br />

and parameterisations can be expanded nearly<br />

arbitrarily by the user.<br />

All analogue values are displayed as curves in a<br />

chart. Limit violations will be alerted and the whole<br />

event history is saved in all details. All values,<br />

parameters, and events are stored in an adaptive<br />

database.<br />

Features<br />

� expandable with analysers and special sensors<br />

� freely-programmable control software LabVision<br />

with numerous extension options<br />

� Complex Process Control is possible<br />

� touch screen for keyboard- and mouseless<br />

operation<br />

� automatic managed laboratory journal<br />

� optionally as complete system with pumps,<br />

sensors, etc.<br />

� Integration of other manufacturers' components is<br />

possible<br />

Order Code Description<br />

VA-HIFERM-FCU Fermenter Control Unit<br />

Fermentation Technology<br />

Fully automatic Research Fermenter (. Frings Bonn)<br />

Via the optional off-gas analysing module, the<br />

metabolic activity of biological cultures can be<br />

detected online via the respiration activity (OTR,<br />

CTR, RQ, OT, CT, µmax). With this knowledge you<br />

can easily draw conclusions in regard to substrate<br />

consumption and changes in metabolism or<br />

biomass.<br />

For dosing with fed-batch or continuous operation<br />

mode, up to five precision peristaltic pumps can be<br />

connected. They assure a secure and constant<br />

substrate supply for semi-continuous and continuous<br />

processes and a very accurate dosing of anti-foam,<br />

base or acid for pH control.<br />

Cell fermentater control unit<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Fermentation Technology<br />

Gmix – Gas Mixing Device<br />

The Gmix precision gas mixing device was<br />

especially developed for applications which require<br />

highest accuracy and reproducibility of gas mixtures.<br />

The gas mixing device is available in various<br />

configurations with one to four outlets. The gas<br />

mixture, consisting of up to four (opt. Six) gases, can<br />

be adjusted individually for every outlet.<br />

All inlets will be calibrated ex works upon customer<br />

request. Up to six gases for eache inlet can be<br />

calibrated. Default gases are air, N2, O2 and CO2.<br />

Units can be selected as ml/min (default: cm²/min)<br />

und g/min.<br />

The Gas Mixing Device Gmix is available both as a<br />

RAMOS expansion and as independant system.<br />

Application<br />

The application areas of the precision gas mixing<br />

device are, amongst others, all biological<br />

fermentations the require a gas composition. Due to<br />

the extremely precise gas mixture, the gas mixing<br />

device can also be deployed in physical technology<br />

and trace gas analytics. One further application area<br />

is the calibration of gas sensors.<br />

Advantages<br />

Flows and percentagae will be entered into and<br />

shown in self describing dialogue mass. The actual<br />

concentrations are kept constant with high class<br />

mass flow controllers (NO time multiplexing!).<br />

Thereby, an eminently consistent and precise dosing<br />

is assured. Due to the very compact design, the<br />

device requires little space.<br />

Control / Protective Devices<br />

Outlet pressures are measured and controlled for<br />

safety reasons.<br />

In case of exceedance of the adjusted outlet<br />

pressure, the gas supply will be automatically locked<br />

and an alarm signal will be activated.<br />

Operation with RAMOS<br />

During operation with RAMOS, the UI/work station of<br />

the gas mixing device is directly integrated in the<br />

RAMOS-software. The setpoint values are predetermined<br />

by the operator.<br />

The measured flow and fractions are indicated<br />

numerically and the temporal progression is<br />

displayed graphically.<br />

Customer specific solutions e.g. for aggressive<br />

gases can be buildt upon request.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 45<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


46<br />

Technical Data (Gas Mixing Device)<br />

Fermentation Technology<br />

Dimensions Width: 240 mm, Depth: 320 mm, Height: 150 mm with up to 4 inputs<br />

Width: 340 mm with 5 or 6 inputs<br />

Weight approx. 6 kg with up to 4 inputs, 8 kg with 5 or 6 inputs<br />

Inputs<br />

Amount 2 – 6 gases, pneumatic connection 6/4<br />

Gases Air, N2, Oxygen (O2), Carbon Dioxide(CO2) by default, non-condensing, other<br />

gases upon request. Up to 6 gases posisble. Distribution is freely selectable by<br />

the user.<br />

Inlet pressure according to specifications, up to 11 bar abs, from approx. <strong>10</strong> slm/Input, higher<br />

pressure upon request<br />

Outlets<br />

Amount 1, pneumatic connection<br />

Outlet pressure according to specification, up to <strong>10</strong> bar abs.<br />

Min. pressure difference Approx. 1 bar, according to specifications<br />

Control principle Thermal massflow controller. Each component is controlled on each outlet,<br />

NO multiplexing!<br />

Prefilter Inlet filter 20 µm<br />

Flows<br />

Operating range Default: 0,05 slm – 50 slm set value, Dynamic 1:30<br />

optionally smaller or greater, dynamics 1:<strong>10</strong>0<br />

Uncertainty Default: < 1,5 % of set value, opt. +/- 0,3% of set value, +0,5% of measured value<br />

Reproducibility


Fermentation Technology<br />

Order Code Description<br />

IL-GMIX21 Gas mixing device (2 Inlets, 1 Outlets) for non-condensing gases (Air, O2, N2, CO2)<br />

Inlet 0,05 to 5 slm, uncertainty ±1,5 % of span, Dynamic 1:30<br />

IL-GMIX31 Gas mixing device (3 Inlets, 1 Outlets) for non-condensing gases (Air, O2, N2, CO2)<br />

Inlet 0,05 to 5 slm, uncertainty ±1,5 % of span, Dynamic 1:30<br />

IL-GMIX41 Gas mixing device (4 Inlets, 1 Outlets) for non-condensing gases (Air, O2, N2, CO2)<br />

Inlet 0,05 to 5 slm, uncertainty ±1,5 % of span, Dynamic 1:30<br />

IL-GMIX21-X Gas mixing device with increased accuracy (2 Inlets, 1 Outlets) for non-condensing/corrosive gases<br />

(Air, O2, N2, CO2). Inlet 0,05 to 5 sLM, uncertainty ±(0,3 % of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />

IL-GMIX31-X Gas mixing device with increased accuracy (3 Inlets, 1 Outlets) for non-condensing/corrosive gases<br />

(Air, O2, N2, CO2). Inlet 0,05 to 5 sLM, uncertainty ±(0,3 % of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />

IL-GMIX41-X Gas mixing device with increased accuracy (4 Inlets, 1 Outlets) for non-condensing/ corrosive gases<br />

(Air, O2, N2, CO2). Inlet 0,05 to 5 sLM, uncertainty ±(0,3 % of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />

IL-GMIX21-XET Gas mixing device with increased accuracy , stainless steel model, dead volume optimised (2 Inlets, 1<br />

Outlets) for non-condensing/ corrosive gases (Air, O2, N2, CO2). Inlet 0,025 to 0,5 sLM, uncertainty ±(0,3<br />

% of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />

IL-GMIX31-XET Gas mixing device with increased accuracy , stainless steel model, dead volume optimised (3 Inlets, 1<br />

Outlets) for non-condensing/ corrosive gases (Air, O2, N2, CO2). Inlet 0,025 to 0,5 sLM, uncertainty ±(0,3<br />

% of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />

IL-GMIX41-XET Gas mixing device with increased accuracy , stainless steel model, dead volume optimised (4 Inlets, 1<br />

Outlets) for non-condensing/ corrosive gases (Air, O2, N2, CO2). Inlet 0,025 to 0,5 sLM, uncertainty ±(0,3<br />

% of span + 0,5 % of setpoint) Dynamic 1:<strong>10</strong>0<br />

IL-Gmix-S-RAMP Program Control for User-defined Profiles<br />

Systems with more outlets can be accomplished by<br />

cascading multiple devices or can be manufactured<br />

upon request.<br />

Upon request we can equip all devices with further<br />

options such as:<br />

System adjustments to special gases, aggressive<br />

gases, multiple gas datasets per inlet, analogue<br />

inputs 4...20 mA and controller for dissolved O2 and<br />

pH, digital input for externally control (standby, ramp<br />

start and stop).<br />

We are also able to construct a gas mixing device exactly according to your individual requirements and<br />

specifications!<br />

Order Code Description<br />

IL-ALCOTECT-d-l Alcohol Probe with Evaluation Unit for ethanol and methanol<br />

IL-ALCOTECT-AIRS Gas Supply synthetic air 20ml/min for alcohol probe, without gas bottle<br />

d: 19, 25 = Diameter 19 or 25 mm, l: <strong>10</strong>5, 120, 220, 320 = <strong>10</strong>5, 120, 220 or 320mm<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 47<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

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48<br />

Fermentation Technology<br />

OxyTect Optical Dissolved Oxygen Probe<br />

The OxyTect Alcohol Probe, amongst other<br />

application options, is suited for the monitoring of<br />

fermentation processes. The disadvantages<br />

connected with the conventional Clark probes are no<br />

longer existent.<br />

Product Features:<br />

� Exact online determination of the dissolved<br />

oxygen concentration<br />

� Compatible with the connections and signals of<br />

the conventional Clark probe<br />

� Sterilisable in-situ (SIP and CIP)<br />

� Auto-diagnosis<br />

� Immediately ready for measurement<br />

� High Durability<br />

� High Precision<br />

� Short Response Time<br />

� Exchangeable Sensor Cap<br />

Technical Data<br />

Probe Diameter 12mm<br />

Probe Length 120, 160, 225, 325 o. 425mm<br />

Process Connection PG-13,5 Thread<br />

Measuring Range 4 ppb/0,05%...300% O2 Air<br />

Saturation<br />

Detection Limit 0,01 Vol%<br />

Temperature Range -<strong>10</strong> °C bis 80 (130) °C<br />

Pressure Range -1...12bar<br />

Response Time < 30s<br />

98%<br />

Materials High Grade Steel, Silicone<br />

Output Signal 4..20mA, Clark-Signal,<br />

RS485 ( MODBus RTU<br />

Fieldbus), VP 8.0 Jack<br />

Power Supply 7..30V DC, 0,6W<br />

Order Code Description<br />

IL-OXYTECT-l Dissolved Oxygen Probe with Evaluation Electronics 4..20mA, Clark Signal, RS485 ( MODBus<br />

RTU Fieldbus), VP 8.0 Jack, autoclavable, PG 13.5 Thread<br />

L: 120, 160, 225, 325, 425mm = 120, 160, 225, 325 or 425mm<br />

Autoclavable pH-Probe<br />

This autoclavable ph-probe is in particular suited for<br />

the monitoring and controlling of fermentation<br />

processes.<br />

It is distinguished by especialially high durability and<br />

robustness.<br />

Product Features:<br />

� Low-<strong>Main</strong>tenance<br />

� 2 Pinhole Diaphragms<br />

� Duralid Electrolyte with high KCl-Content<br />

� High Durability<br />

� Fast and consistent Measurement Values<br />

� Proven H-Membrane<br />

� Low Alkaline Error<br />

� Extended application area in medias with<br />

extreme ion concentration, strongly oxidising<br />

characteristics, high alkali or acid concentrations<br />

or solvents<br />

� Integrated Pt<strong>10</strong>0<br />

Technical Data<br />

Probe Diameter 12mm<br />

Probe Length 120, 225, 325, 360 and<br />

425mm<br />

Process Connection PG-13,5 Thread<br />

Measurement Range 0 … 14 pH<br />

Measurement +- 0,1%<br />

Uncertainty<br />

Temperature Range 0 to 130 °C<br />

Pressure Range 0...<strong>10</strong>bar<br />

Connection SMEK- or VP- Plug-In Head<br />

Protection Class IP 68<br />

Order Code Description<br />

IL-PHFERM-l pH Probe pH 0..14, 0 to 130°C, 0..<strong>10</strong>bar, autoclavable PG 13.5 Thread<br />

l: 20, 225, 325, 360, 425 = 120, 225, 325, 360 and 425mm<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Fermentation Technology<br />

HiSense Emission Analysis System<br />

Precision Gas Analysis System for<br />

Biotechnology<br />

The HiSense Gas Analysis systems produced by<br />

<strong>HiTec</strong>, in contrary to conventional waste gas<br />

analysis technology, are also able to deliver the<br />

biological variables OTR, CTR and RQ. The devices<br />

are suited for R&D and laboratory applications within<br />

production and quality assurance.<br />

Measurement Technology:<br />

For the oxygen analysis, sensor are deployed which<br />

distinguish themselves by low interference, lownoise<br />

measurement results and long term stability.<br />

For the CO2- measurement, NDIR photometers and<br />

flow sensors with minimal zero point and inclination<br />

faults are deployed. Due to a novel special<br />

measurement method, the precise measurement of<br />

very minute activities both at small differences and<br />

minute measurement gas flows is possible.<br />

At the cell culture version, the deployment of<br />

additional measurement technology and the<br />

offsetting of unavoidable influences, e.g. total<br />

pressure, humidity etc., enables highly precise<br />

compensation. At conventional waste gas analysis<br />

methods and the low metabolic rates and long<br />

culture periods of cell cultures, the influence can be<br />

very significant and impede or even prevent a<br />

comparison of cultivations and make the deployment<br />

of a waste gas analysis system for quality assurance<br />

impossible. Usually, without the compensation of<br />

these factors, it is not possible to gain any useful<br />

measurement values at all.<br />

As the HiSense-c Precision Waste Gas Analysis<br />

System for cell culture and fermentation applications<br />

in addition, in most cases, is also able to perform the<br />

online determination of the true CO2 production<br />

(CER) at the usual carbonate buffer systems<br />

(optional pH input is required) usual in cell cultures.<br />

For this purpose, the faults are compensated which,<br />

due to the displacement of the of the HCO3-/-CO2<br />

balance by metabolites (e.g. lactate, NH3), make a<br />

useable measurement impossible. This is the only<br />

method that enables the determination of the actual<br />

RQ.<br />

The high measurement resolution enables reliable<br />

measurements under the usual conditions also at<br />

the low respiratory rates of animal cell cultures and<br />

within a very broad flow range (1.8 to <strong>10</strong>0.000 Ln/h,<br />

depending on version).<br />

For these measurements, hardly any expenditure for<br />

calibration is required.<br />

The software conducts all calculations, including all<br />

corrections/compensations, online. All measurement<br />

values are stored in a data base and can be<br />

displayed as current values or in the x-t-recorder.<br />

The export is conducted as data file (csv, txt and<br />

other formats) or via RS232/Windows-Pipe.<br />

Extension Options:<br />

The provision of further inputs/outputs, e.g. for<br />

pumps, valves and the arrangement of regulator<br />

circuits is possible on an optional basis.<br />

Additional inputs, e.g. for pH, temperature etc., are<br />

optionally provided for.<br />

Due to the free programmability in HiText Syntax<br />

(optional), additional algorithms, such as control and<br />

regulatory functions, can be integrated into the<br />

HiSenseTM Waste Gas Analysis Station. This also<br />

includes the RQFeed process for the optimisation of<br />

the productivity of cell cultures (if required, please<br />

request the respective special documentation). .<br />

A coupling with other systems, e.g. for<br />

control/regulation purposes is possible via network,<br />

RS232, RS485 and analogue interfaces (optional).<br />

Advantages:<br />

� 1 to 8(5) Measurement Channels for 1 to 4<br />

Fermenters, optional<br />

� High Resolution Measurement<br />

� Humidity Compensation (-c Version)<br />

� "True" OUR, CER and RQ Measurements (-c<br />

Version)<br />

� Low Interference<br />

� Possible Overpressure<br />

� Wear-resistant Sensor System<br />

� Compact Design<br />

� Additional Functions can be integrated<br />

� Optionally free Programmability<br />

� Numerous Coupling Options<br />

� Data Export is possible<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Technical Data (HiSense-m for microbiology)<br />

Fermentation Technology<br />

General<br />

Dimensions Width: 458 mm, Depth: 370 mm, Height: 140 mm at small flows<br />

Operating Voltage 1<strong>10</strong> – 230 V, 50 – 60 Hz<br />

Current Consumption 3 A<br />

Temperature Range 0 °C up to 30 °C<br />

Protection Category<br />

Measurement Channels<br />

IP 20<br />

Supply air/ Exhaust gas 1 … 5 (optionally) channels for measurment in supply or exhaust gas<br />

Operating Range of Flow 18 - 180 Ln/h (l/h at 0 °C / <strong>10</strong>13 mbar), optionally from 6 to 300 Ln/h<br />

Pressure Loss < <strong>10</strong>00 Pa<br />

Input Pressure<br />

O2 Measurement<br />

atmospheric, 3 bar absolute<br />

Principle Solid Electrolyte System<br />

Measurement Range 0 – 60 Vol. %<br />

Measurement Uncertainty +/- 1 % v. Measurement Range<br />

Resolution 0.02 Vol. % at 20 % O2, better upon request<br />

Long-term Drift < 0.2 Vol. %<br />

Relevant Resolution<br />

CO2-Measurement<br />

Difference, humidity, and pressure-corrected, resolution approx. 0.02 %<br />

Principle NDIR<br />

Measurement Range 0 – 20 Vol.%, others upon request<br />

Measurement Uncertainty +/- 1 % v. measurement range<br />

Resolution 0.02 Vol.% at 5 % CO2<br />

Zeropoint Drift < +/- 0.2 %<br />

Automatic Compensation Humidity, Absolute Pressure<br />

Relevant Resolution<br />

Mass Flow Measurement<br />

Difference, humidity, and pressure-corrected, resolution


Technical Data (HiSense-c for cell cultures)<br />

Fermentation Technology<br />

General<br />

Dimensions Width: 458 mm, Depth: 320 mm, Height: 280 mm at small flows<br />

Operating Voltage 1<strong>10</strong> – 230 V, 50 – 60 Hz<br />

Current Consumption 3 A<br />

Temperature Range 0 °C up to 30 °C<br />

Protection Category<br />

Measurement Channels<br />

IP 20<br />

Supply air/ Exhaust gas 2..8 (optionally) ch. for measurment in supply or exhaust gas of 1..4 fermenters<br />

Operating Range of Flow 1,8 - 20 Ln/h (l/h at 0 °C / <strong>10</strong>13 mbar), optionally higher<br />

Pressure Loss < <strong>10</strong>00 Pa<br />

Input Pressure<br />

O2 Measurement<br />

atmospheric, 3 bar absolute<br />

Principle solid electrolyte system, optionally paramagnetic<br />

Measurement Range 0..25 vol. %, paramagnetic 0..60 vol. %<br />

Measurement Uncertainty +/- 1 % v. Measurement Range<br />

Resolution 0.02 Vol. % at 20 % O2, better upon request<br />

Long-term Drift < 0.2 Vol. %<br />

Relevant Resolution<br />

CO2-Measurement<br />

Difference, humidity, and pressure-corrected, resolution approx. 0.02 %<br />

Principle NDIR<br />

Measurement Range 0..20 Vol.%, others upon request<br />

Measurement Uncertainty +/- 0.5 % v. measurement range<br />

Resolution 0.01 vol.% at 5 % CO2<br />

Zeropoint Drift < +/- 0.05 %<br />

Automatic Compensation humidity, absolute pressure<br />

Relevant Resolution<br />

Mass flow measurement<br />

difference, humidity, and pressure-corrected, resolution approx. 0.005 %<br />

Principle thermal mass flow measurement, CO2-corrected<br />

Standard all channels<br />

Measurement uncertainty better than 2 % of measurement range<br />

Reproducibility 0,2 % of measurement range<br />

Prefilter Measurement None, sterile filtration at the fermenter<br />

Sample Gases<br />

OTR-CTR<br />

At non-condensing ambient temperature, exhaust gas cooling required<br />

Measurement Values approx. <strong>10</strong> min, with 2 fermenters approx. 15 min<br />

Sensitivity OTR** approx. 1 x <strong>10</strong>-5 Mol/l<br />

at 1 l culture volume, 5 vvh (V gas / V liquid / h ) gassing rate<br />

Sensitivity CTR** approx. 1 x <strong>10</strong>-5 Mol/l<br />

at 1 l culture volume, 5 vvh gassing rate<br />

Heating Period 120 min<br />

Further Measurement pH, OTR, CTR, OT, CT, TQ, CER, CE, RQ (corrected TQ), growth rate and<br />

Variables<br />

Operation<br />

many peripheral values like solvant O2, CO2...<br />

PC Operation via software included in scope of delivery with graphic user<br />

interface. Data export to Excel or as text data file.<br />

Order Code Description<br />

IL-HISENSE-c-2 Gas Analysis System for the Determination of O2 and CO2, OTR, CER and RQ, 2 channels<br />

IL-HISENSE-c-4 Gas Analysis System for the Determination of O2 and CO2, OTR, CER and RQ, 4 channels<br />

IL-HISENSE-c-8 Gas Analysis System for the Determination of O2 and CO2, OTR, CER and RQ, 8 channels<br />

Additional in- and outlets and data interfaces are realised with the components contained in the chapter<br />

„Laboratory Automation, Hardware“.<br />

For free programmability, the software module HiText contained in the chapter „ Laboratory Automation,<br />

Software“ is required.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

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Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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52<br />

Fermentation Technology<br />

RQFeed Feeding Algorithm<br />

The development of highly productive scalable<br />

processes has significantly gained significance for<br />

industrial production of recombinant proteins. Since<br />

Fed-batch fermentations are comparatively reliable<br />

in operation and relatively easy to handle, they are<br />

widely distributed.<br />

Exactly tuned feeding of substrates can significantly<br />

increase the productivity. However, the control or<br />

even the regulation of the substrate feeding in a<br />

bioreactor is a great challenge. The compliance with<br />

ideal, as constant as possible culture parameters is<br />

of particular importance for cell cultures.<br />

Inappropriate culture conditions do not only lower<br />

the productivity of the cells, but also affect the<br />

chemical structure (e.g. of side chains) of the<br />

secreting protein (in particular the glycosylation)<br />

which causes an undesired heterogeneity of the<br />

active substance often combined with a significant<br />

influence upon the pharmacological effectiveness.<br />

Traditional feeding models are based on the<br />

parameters oxygen uptake rate (OUR) as well as<br />

offline measured cell density substrate<br />

concentration. Samples must be drawn during the<br />

process at regular intervals and subsequently<br />

analysed using external devices and rapid tests,<br />

respectively. Based on the result of these, the<br />

feeding rate is re-evaluated and adjusted. The<br />

regulation of the feeding rate based merely on these<br />

offline parameters often leads to suboptimal results.<br />

The <strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> has developed the novel<br />

regulation method “RQFeed” for cell cultures which<br />

is based on the respiration activity of the cells. The<br />

aerobic degradation of the substrate is accompanied<br />

by oxygen consumption (respiratory chain) which in<br />

ultimately influences the oxygen uptake OUR. This<br />

parameter thus allows to draw conclusions about the<br />

actual condition of the culture. Essential for the new<br />

Fed-batch technology is the RQFeed algorithm for<br />

the specific cultivation and production process. This<br />

algorithm is the result of intensive research into the<br />

cultivation progression as well as the deduction of<br />

according procedures and operational instructions.<br />

Organisms in aerobic fermentation consume oxygen<br />

and produce carbon dioxide. The cell-specific uptake<br />

rate of the essential substrates, e.g. glutamine and<br />

glucose, is closely connected with the oxygen<br />

uptake rate (OUR) and the carbon dioxide emission<br />

rate (CER). These two values enable the<br />

Order code Description<br />

SP-RQFEED-AC Feed Regulator based on RQ for Animal Cell Cultures<br />

Information to feed regulators for other cultures is available upon request.<br />

determination of the respiratory quotient (RQ), a key<br />

parameter that is independent of the number of<br />

cells. It reveals the different physiological states of<br />

the cell during batch cultivation and changes<br />

dependant on concentration of substrates and<br />

products so that alterations in the physiological<br />

condition can be detected and examined on a<br />

differentiated basis.<br />

Based on these findings, a feeding algorithm was<br />

developed which is able to maintain a desired<br />

physiological condition without the necessity of<br />

having to conduct offline measurements. This leads<br />

to a significant shortening of the fermentation<br />

periods, respectively to a significant increase in<br />

production rates.<br />

The diagram shows fermentation at two different RQ<br />

levels. At the RQ level 2, the productivity is not<br />

satisfactory, while Level 2 displays an ideal<br />

productivity.<br />

The RQFeed regulation algorithm is both suited for<br />

laboratory reactors as well as fermenters in pilot<br />

plants and in production. An exact determination of<br />

the RQ requires a controlled gas feed and an<br />

exhaust analysis system for the measurement of the<br />

CER and OUR.<br />

<strong>HiTec</strong> <strong>Zang</strong> offers the RQFeed regulation algorithm<br />

together with its OmniFerm laboratory fermenters in<br />

connection with a gas supply and analysis plant as<br />

an upgrading module for existing fermenters, but<br />

also on license basis for own use. In addition,<br />

training courses and instructions for the deployment<br />

of the algorithm in R&D applications and within<br />

large-scale production are also offered.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Packed Bed Reactor<br />

One alternative to stirred tank reactors are packed<br />

bed reactors with macroporous carriers for the<br />

cultivation of adherent animal cells which facilitates<br />

a continuous cultivation at high volume-oriented cell<br />

density and low shear stress. One significant<br />

advantage of this system is the opportunity to<br />

specially adjust the retention times of viruses and<br />

monoclonal antibodies under process conditions.<br />

When scaling up packed bed reactors, in particular<br />

the oxygen supply is problematic, as the height of<br />

the bed is restricted due to the oxygen depletion. A<br />

packed bed can, at minor overall lengths, be aerated<br />

up to <strong>10</strong> cm axially without occurring oxygen<br />

limitations in the upper sector of the packed bed. A<br />

further scale-up requires a radial aeration. By<br />

selecting a suited carrier, it is also possible to<br />

cultivate challenging cell types. In comparison to a<br />

stirred tank reactor, packed bed reactors possess a<br />

higher performance capacity in regard to the<br />

reachable volume-specific cell density and<br />

productivity. Due to the cell retention in the packed<br />

bed, integrated separation procedures using ceramic<br />

membranes are easy to realise. Additionally, the<br />

operation of a packed bed is very uncomplicated<br />

and cost-effective. The packed bed system has been<br />

used in the biochemical laboratory for the largescale<br />

production within the scope of the following<br />

projects:<br />

� Production of retroviral particles for genetherapeutic<br />

applications with the Paul-Ehrlich<br />

Institute and the Technical University Hamburg<br />

Harburg.<br />

� Production of monoclonal antibodies for in vitro<br />

diagnostics on novel ceramic carriers in<br />

cooperation with the company Therapharm<br />

Deutschland <strong>GmbH</strong>.<br />

Fermentation Technology<br />

Order Code Description<br />

VA-FESTBETT Packed Bed Reactor with microporous Carriers for the Cultivation of adherent Cell Cultures<br />

One of our main strengths is the construction of Special Custom Designs! Do not hesitate to contact<br />

us with any problem, we will help you to find a solution.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

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Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

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Technology<br />

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54<br />

Here you will find:<br />

Laboratory Automation Hardware<br />

� LabManager®-Laboratory Automation Systems<br />

� MSRmanagerAutomation Systems<br />

� Interface Cards<br />

� PI Additional Equipment external<br />

� Power Supplies<br />

� Simulation and Test Apparatuses<br />

� Display and Operating Components<br />

� Peripheral Devices<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


LabManager ® -System<br />

Laboratory Automation Hardware<br />

The LabManager system is an automation and/or<br />

process control system which isspecially suited for<br />

laboratory-, mini- and bench plants as well as for<br />

pilot plant stations. It is suitable for the automation of<br />

virtually all chemical-procedures reaching from<br />

batch, semi-batch and continuous processes.<br />

The LabManager system was developed in close<br />

cooperation with specialists from laboratories and<br />

pilot plant stations of major chemical companies. It<br />

has proved its worth in a great number of areas as a<br />

standard tool.<br />

In accordance with the requirements of the NAMUR<br />

Working Party for research process control computer<br />

systems (RPCCS), particular care has been directed<br />

to develop a user-friendly man-machine interface, a<br />

compact design, and a high application flexibility.<br />

The LabManager RPCCS especially distinguishes<br />

by the fact that it is also transparent and easy to<br />

handle for personnel inexperienced in automation<br />

technique even if they want to go into detail.<br />

LabManager, the Interface Genius!<br />

With help from the graphically programmable recipe<br />

control system HiBatch and a unit operation library, a<br />

customer without automation-technical knowledge<br />

can program the control program for a complex<br />

synthesis in a few minutes.<br />

The LabManager systems usually have a pay-back<br />

period below one year!<br />

� more intense use of your human and capitalresources<br />

� GLP/GMP raked working method without<br />

additional outlay<br />

� optimal reproducibility of your recipes, also<br />

after years<br />

� complete documentation of the entire process<br />

� savings during the instrumentation thanks to<br />

virtual devices<br />

� release of the lab personnel from routine<br />

activities<br />

� shorter "Time to Market" period for your<br />

products<br />

The most significant Results:<br />

� Increase of Quality<br />

� Lowering of danger potentials<br />

� Lowering of Costs<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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56<br />

Areas of Application<br />

Laboratory Automation Hardware<br />

The LabManager is particularly useful in the fields:<br />

� Chemistry<br />

� Pharmacology<br />

� Biotechnology<br />

� Food Technology<br />

� Environmental Technology<br />

� Quality Assurance<br />

� Experimental plants and test beds<br />

Applications<br />

Due to its unique flexibility, the possible applications<br />

in chemistry laboratories, in pilot plant stations, for<br />

Mini-Plants and in companies are virtually unlimited.<br />

Typical applications of the system in the fields of<br />

chemistry and pharmacology are:<br />

� Process Development<br />

� Process Optimization<br />

� One and multi boiler plants<br />

� Parallel reactor systems<br />

� High-Throughput-Experimentation<br />

� Bench Plant installations<br />

� Mini-Plant Installations<br />

� Continuous processes<br />

� Batch tasks<br />

� Semi batch tasks<br />

� Syntheses<br />

� Reaction calorimetry<br />

� Exothermic early warning system<br />

� Screening<br />

� Scale-Up<br />

� Polymerization<br />

� Distillation<br />

� Extraction<br />

� Crystallization<br />

� Production oriented Labs<br />

(Verification)<br />

� Raw material Control<br />

� Quality Assurance<br />

� Analysis Laboratories<br />

The system offers all the functionalities of the<br />

automation systems and process control<br />

engineering such as:<br />

� Measuring<br />

� Process control<br />

� Recipe control system<br />

� Automatic control<br />

� Process monitoring<br />

� Process visualization<br />

� Alarming<br />

� Online intervention<br />

� Logging<br />

� Filing<br />

All basic unit operations reaching from dosing up to<br />

sample drawing are automated (see Automation with<br />

the LabManager), all measured values are collected<br />

(see LabManager and Instrumentation), visualized<br />

(see LabVision), and automatically evaluated (see<br />

HiText and KalDas).<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Economic Feasibility Analysis<br />

Laboratory Automation Hardware<br />

The economic feasibility analysis is conducted<br />

using the example of a polymerisation process in the<br />

laboratory reactor.<br />

I. Manual Operation Mode<br />

Test:<br />

Operation Hours<br />

Weighing out 1<br />

Heating 1<br />

Dosing 4<br />

Secondary Polymerisation 4<br />

Emptying and Cleaning 1<br />

Total 11<br />

Start of test,e.g. at 7:30a.m., test completed at<br />

6:00p.m.<br />

According to this, only one test per day is possible!<br />

II. Automated Test Control with the<br />

LabManager<br />

Unattended procedure with:<br />

� Temperature Control<br />

� Dosing<br />

� Torque Monitoring<br />

� Recording of Test Data<br />

� Online Evaluation<br />

� Cleartext Protocol<br />

� Remote Alarming etc., if required<br />

Day Routine:<br />

First test start, e.g. at 8:00a.m., test completed at<br />

7:00p.m. In the meantime, the laboratory technician<br />

is free for the evaluation of last night's automatic run<br />

and the preparations for the next tests.<br />

Second test start, e.g. at 7:30p.m.<br />

Test completed at 6:30a.m. (unattended).<br />

According to this, two tests per day are now possible<br />

instead of one as before!<br />

The laboratory utilisation is improved by <strong>10</strong>0%.<br />

Cost Factors EUR<br />

Direct costs of the laboratory<br />

automation<br />

25,000.00<br />

Planning, familiarisation, plant<br />

upgrade<br />

<strong>10</strong>,000.00<br />

User Schooling 3,000.00<br />

Total Cost 38,000.00<br />

The amortisation period is evaluated out of the cost<br />

of one laboratory day (e.g. 750 Euro) and the total<br />

cost:<br />

Amortisation Period = 50 days!<br />

Even in the worst case scenario, assuming an<br />

improvement laboratory utilisation of merely 15%,<br />

which accords to a saving of 21,000 Euro annually,<br />

the amortisation period is still below one year!<br />

Additional beneficial Effects:<br />

GLP-conform mode of operation by a significant<br />

improvement of the documentation, the quality and<br />

reproducibility.<br />

A further Pay-Off Calculation for Chemistry<br />

Laboratories<br />

Catalyst Research Laboratory<br />

Test series (savings due to unattended night<br />

operation):<br />

Amortisation Period = 3 months!<br />

Colour R&D Laboratory<br />

Frequently changing recipes (savings due to<br />

simplified parameterisation via HiBatch recipe<br />

control and unattended night operation).<br />

Amortisation Period = 6 months!<br />

Naturally, similar results are achieved in continuous<br />

operation, if, instead of having personnel directly at<br />

the location, it is only necessary to have an on-call<br />

duty and remote alarming.<br />

It is a known fact that one day a product is launched<br />

on to the market earlier can result in six to sevendigit<br />

additional revenue.<br />

This clearly indicates how much laboratory<br />

automation is nowadays a must!!<br />

Using project moduls shortens the process of<br />

creating projects significantly.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 57<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


58<br />

Laboratory Automation Hardware<br />

Conventional Automation compared to LabManager ®<br />

With the application-oriented device components,<br />

typical automation basic functions, such as dosing,<br />

vacuum control, and the control of the reactor<br />

interior temperature, are realised in an<br />

uncomplicated manner.<br />

The application-oriented device components contain<br />

all required functionalities.<br />

The dosing device components additionally offer the<br />

possibility to automatically or manually refill the feed<br />

tank without dosing interruption. The<br />

parameterisation of controllers is no longer<br />

Example 1: A Dosing Circuit for Liquids<br />

necessary and thus, one of the greatest and most<br />

time-consuming problems in practice is eliminated.<br />

In contrary to conventional automation systems,<br />

almost all modifications, which may become<br />

necessary in the course of a running test, can now<br />

be realised without having to shut down the plant.<br />

In order to clearly demonstrate the cost-saving<br />

potential of the LabManager-System, several cost<br />

calculations for the conventional realisation of a few<br />

process and control tasks are compared with the<br />

according realisation by the LabManager-System.<br />

Realisation Method a.) Conventional b.) with the LabManager-System<br />

Costs:<br />

Operation Conventional realisation<br />

with EMSR/PLT +<br />

individual components<br />

EUR Realisation with LabManager +<br />

GraviDos from <strong>HiTec</strong>-<strong>Zang</strong><br />

Clarification of the Task 4 hours.* 320.00 2 hours 160.00<br />

Engineering 6 hours* 480.00 1 hours. 80.00<br />

Supply 4 hours* 320.00 1 hours 80.00<br />

Instrumentation of Components Pump, scales, valves, 2500.00 GraviDos complete, with feed tank and 1700.00<br />

Fittings<br />

fixtures for connection to reactor<br />

Additional Devices Interface for scales 500.00 none 0.00<br />

Additional Material Control cabinet, according<br />

cables and accessories<br />

etc.<br />

500.00 Included in deliver scope of GraviDos 0.00<br />

Realisation, Test 12 hours* 960.00 2 hours 160.00<br />

Documentation 4 hours* 320.00 No longer necessary as selfdocumenting<br />

0.00<br />

Costs<br />

* 80 EUR/hour<br />

Conventional 5900.00 <strong>HiTec</strong>-<strong>Zang</strong> 2180.00<br />

The savings due to the LabManager, according to<br />

the above calculation, already add up to 3720.00<br />

EUR! This is more than 60 %!<br />

Or, to express it differently, a conventional solution<br />

is 2.6 times more expensive!<br />

EUR<br />

Further savings are generated by the significantly<br />

reduced required space of the LabManagers and the<br />

significantly lower costs in case of later upgrading.<br />

Here, the typical saving can be up to<br />

70– 80 % !<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

Example 2: Dosing Control of Gases with Mass-Flow-Controller<br />

Costs:<br />

Operation Conventional realisation<br />

with EMSR/PLT +<br />

individual components<br />

EUR Realisation with<br />

LabManager<br />

Clarification 80 EUR/hour. 4 hours 320.00 1 hour 80.00<br />

Engineering 80 EUR/hour. 12 hours 960.00 1 hour 80.00<br />

Supply 80 EUR/hour. 4 hours 320.00 1 hour 80.00<br />

Instrumentation Mass-Flow-Controller 1500.00 Mass-Flow-Controller ready to<br />

connect<br />

1580.00<br />

Additional Devices Interface/Control Device/<br />

Regulator<br />

2000.00 Integrated in LabManager 0.00<br />

Additional Material Control cabinet , according<br />

cables and accessories<br />

500.00 Not necessary 0.00<br />

Realisation 80 EUR/Std. <strong>10</strong> hours 800.00 1 hour 80.00<br />

Documentation 80 EUR/Std. 4 hours 320.00 Not necessary 0.00<br />

Costs Conventional 6720.00 <strong>HiTec</strong>-<strong>Zang</strong> 1900.00<br />

The savings for this individual task already add up<br />

to far more than 4820.00 EUR, which is<br />

approximately 70 %!<br />

Or, to express it differently, a conventional solution<br />

is 3.5 times more expensive!<br />

The primal saving potential is however<br />

represented by its daily use, in particular in cases of<br />

frequently changing processes and frequently<br />

changing recipes. A new recipe control can be<br />

establishment by the laboratory technician with the<br />

help of LabVision's basis operations library within a<br />

timeframe which, if conventional methods were<br />

applied, would already be needed for the technical<br />

clarification alone.<br />

Additional significant savings are generated by the<br />

smaller footprint of the LabManagers and the lower<br />

costs in case of later upgrading.<br />

EUR<br />

Further substantial advantages in regard to costs,<br />

time, and result from the fact that the PLT system<br />

LabManager is easy to upgrade and expand in case<br />

the plant should require this at a later stage.<br />

The devices can expanded at any time by refitting<br />

of modules, panels and cards.<br />

The modification of the application software can be<br />

conducted by company-own personnel.<br />

Software modifications, new connection or exchange<br />

of sensors and actors can usually be realised while<br />

the plant is in operation without shutting it down.<br />

It is only possible to estimate the savings on a<br />

rudimentary basis, but according to the evaluation of<br />

long term users, they are considerable. These<br />

advantages are mainly demonstrated by the<br />

LabManager System in every day operation in<br />

laboratories and pilot plants.<br />

You want us to provide you with further arguments?<br />

We will gladly introduce you to experienced users of<br />

the LabManager System.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 59<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


60<br />

System Assembly<br />

Laboratory Automation Hardware<br />

An automation system is composed of a "Process-<br />

Interface (PI), in this case the LabManager and a<br />

User Interface (UI) which is a Personal Coumputer<br />

with Windos OS and LabVision Software.<br />

Functionality of the Process Interface<br />

The PI includes interfaces for the connection of the<br />

sensors, actuators, and devices. It is used for<br />

� Collecting<br />

� Converting and<br />

� Linking of Signals<br />

� Monitoring<br />

� Controlling<br />

� Automatic controlling etc.<br />

The LabManager and LabBox PIs are equipped for<br />

the special ambient conditions in the laboratory or<br />

pilot plant stations. The required space is kept to a<br />

minimum.<br />

Functionality of the User-Interface<br />

The UI, also referred to as work station, represents<br />

the interface between user and process. It is used<br />

for<br />

� parameterising<br />

� operating<br />

� monitoring<br />

� reporting<br />

� logging<br />

� saving<br />

� evaluation<br />

It is comprised of a special PC running under<br />

Windows XP or Windows Vista operating systems<br />

and the required LabVision-UI software modules.<br />

Service features<br />

The high functional level of the <strong>HiTec</strong> <strong>Zang</strong><br />

automation system, compared to a traditional<br />

automation system is particularly evident in regard to<br />

the following aspects.<br />

Interfaces<br />

The extensive choice of interfaces includes all<br />

currently available interfaces for sensors, actuators<br />

and devices.<br />

Interface panels with standardised connection<br />

sockets are available for the different types of<br />

interfaces.<br />

The construction and electric wiring of the<br />

connections comply with the recommendations and<br />

guidelines for laboratory devices of the chemical<br />

industry (NAMUR NE28 recommendation). Mistakes<br />

in the course of connecting are therefore excluded.<br />

Suitable connecting cables for the usual laboratory<br />

devices are available. For this reason, customers<br />

without special EMSR technical and electro<br />

technical knowledge are also able to connect<br />

sensors, actuators and laboratory devices<br />

independently.<br />

EMC robust interfaces guarantee a problem-free<br />

application also in case of deployment under rough<br />

conditions.<br />

Beyond the measurement value collection and<br />

control function units, the devices also include the<br />

most frequent process measurement and control<br />

(PMC) components for:<br />

� Signal input/output<br />

� Potential Separation<br />

� Amplifying<br />

� Filtering<br />

� Linearisation<br />

� Control<br />

� Automatic Control<br />

� Monitoring and Reporting (Alarming)<br />

� Supply of sensors and actuators with power<br />

External transducer, buffer amplifier etc. are not<br />

necessary anymore. Due to the consequently<br />

compact design of the devices, the required space is<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

reduced to a minimum so that they will fit in any rack<br />

or on any lab table. If conventionally constructed, a<br />

comparable technology would fill one or even<br />

several control cabinets.<br />

The possibility to mount the device directly on to the<br />

plant represents a significant help to save costs for<br />

project planning and cabling and allows an easy<br />

remounting of the instrumentation.<br />

LabManager mounted directly on the plant<br />

PMC Technical Functions<br />

� PID automatic controller (optional)<br />

� Adaptive automatic controller (optional)<br />

� Comparator<br />

� Ramp<br />

� Setpoint Value Generator (profiles)<br />

� Timer impulse<br />

� Timer Start Delay<br />

� Timer Falling Delay<br />

� Scales, Thermostat, Stirrer Communication<br />

� LabCom Communication<br />

� Temperature Compensation<br />

� Sample & Hold (scan and hold element)<br />

Mathematical Functions<br />

� Differentiator<br />

� Integrator<br />

� Adder<br />

� Subtractor<br />

� Multiplier<br />

� Divider<br />

� Averaging<br />

� Algebraic Polynomial<br />

Logical functions<br />

� AND-Element<br />

� OR-Element<br />

� XOR-Element<br />

� NOT-Element<br />

� Counter<br />

Switching Functions<br />

� Switch 1 to n<br />

� Switch n to 1<br />

� Monitored Output with/without Feedback Signal<br />

� Storage element (latch)<br />

Device components belong to the standard<br />

equipment of a PI and do not have to be ordered<br />

separately. (with exception of application-oriented<br />

device components, regulators, interface drivers)<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 61<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


62<br />

Laboratory Automation Hardware<br />

Modularity<br />

The PI devices can be adapted to modified or<br />

growing requirements at any time. It is therefore<br />

possible to upgrade a device, which was initially only<br />

used for measuring and monitoring, to a regulation<br />

and control system. In addition, a system can be<br />

extended almost infinitely by parallel connection of<br />

additional PIs.<br />

LabManager PIs are available in different casing<br />

sizes ranging from 6 to 20 free panel places. The<br />

LabBox1 and LabBox2 systems with 2 or 4 panel<br />

places are suited for smaller applications.<br />

The power supply for the sensor and the actuator<br />

can also be integrated into the devices.<br />

All devices are available as individually equipped<br />

basic devices or as devices with standard<br />

equipment.<br />

Connecting technology of the LabManager:<br />

standardised plug-and-socket connectors<br />

Safety<br />

Due to their integrated 32 bit processor, the PI<br />

devices are also able to run on an autonomous<br />

basis, i.e. without PC, and therefore comply with the<br />

requirements of the NAMUR safety standard<br />

category three. The CPU is monitored by a hardware<br />

watchdog device and boots automatically in case of<br />

troubles.<br />

To increase safety, an independent external<br />

watchdog device (HP-WDOGEXT1) is available.<br />

The UI (work station) is equipped with an<br />

uninterrupted power supply (UPS) and a UPS<br />

Management System. In case of a longer-lasting<br />

power failure, the UI will be shut down in a controlled<br />

manner.<br />

Alternative Connection Technology<br />

For plants with fixed wiring, the application of the<br />

MSRmanager System (process measurement and<br />

control - PMC) is intended, which uses terminal<br />

blocks with screw terminals instead of interface<br />

panels. The other functional features of the<br />

-manager are identical to those of the LabManager.<br />

A MSRmanager system can be extended with the<br />

same software and hardware options as a<br />

LabManager. You will find further information in the<br />

chapter „MSRmanager“.<br />

Connecting technology of the MSR-manager: terminal blocks with screw terminals<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


System Configurations<br />

Laboratory Automation Hardware<br />

LabVision supports different basic topologies and<br />

media for the coupling of PI and UI (user interface,<br />

respectively work station) in order to reach a suitable<br />

projecting of the system hardware.<br />

As standard, a PI is coupled with a UI through a<br />

RS232 serial interface. Light guides, RS485 twowire<br />

technology, or modems for 2 and 4 wire leased<br />

lines, or switched connection are available for the<br />

bridging of greater distances. The PIs can also be<br />

directly connected to a network via the Ethernet<br />

COM server. The UI can then be connected to every<br />

network socket.<br />

Several PIs can be connected to a UI via multiple<br />

interface cards.<br />

In order to run several independent applications,<br />

several LabVision licenses can work in parallel on a<br />

UI. All applications on UI use the same on-line data<br />

base so that every application can access the data<br />

points of other applications, if needed.<br />

With HiNet it is possible to cross-link several PIs to a<br />

UI. HiNet uses a RS485 twin wire as transmission<br />

medium and can cover distances up to approx. <strong>10</strong>00<br />

m on a normal telephone cable. HiNet is easy to<br />

project.<br />

An evaluation computer in the office can be linked to<br />

a LAN in order to retrieve data for the evaluation.<br />

Distributed systems can be realised with the<br />

platform-overlapping standard CORBA (Common<br />

Object Request Broker Architecture). The standard<br />

Ethernet <strong>10</strong>/<strong>10</strong>0/<strong>10</strong>00 MHz, RJ45 Twisted Pair is<br />

used as transport medium.<br />

Devices of other manufacturers and field buses,<br />

such as the PROFIBUS DP, or the HART protocol<br />

canbe integrated as well. For more information, see<br />

"Remote Access"<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 63<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


64<br />

Laboratory Automation Hardware<br />

Automation with the LabManager System<br />

The LabManager system is suitable for the<br />

automation of virtually all basic unit operations and<br />

functions such as:<br />

Temperature Regulation and Control<br />

Regulated temperature control by heat/cool<br />

thermostats, heating elements or steam for<br />

� heating and chilling reactions defined by random<br />

curves and/or profiles<br />

� distillation and reflux distillation<br />

� crystallization<br />

� determination of calorific key data<br />

� temperature-controlled dosing of exothermic<br />

mixtures<br />

The special device component for the temperature<br />

regulation cascade, in connection with the autoparameterisation<br />

module HiTune, cuts the timeconsuming<br />

parameterisation procedure down to a<br />

few minutes.<br />

For the reactions calorimetry, the LabKit-rc, as well<br />

as individual hardware and software modules are<br />

available for the refitting of existing plants.<br />

Dosing<br />

Controlled dosing of solid matters, liquids and gases<br />

via<br />

� Scales<br />

� Flow Rate Sensors<br />

� Clocked and proportional Valves<br />

� LabDos Peristaltic Pumps<br />

� SyrDos Syringe Dosers<br />

� AlfaDos -controlled Dropping Funnel<br />

� GraviDos-controlled Dropping Funnel<br />

� SolidDos Solid Matter Doser<br />

� Massflow Controller<br />

The self-parameterising dosing device components<br />

also enable an inexperienced user to configure a<br />

precisely working gravimetric dosing within a few<br />

minutes.<br />

Pressure and Vacuum<br />

Flexible strategies for the pressure regulation from<br />

vacuum up to high pressures also under difficult<br />

conditions.<br />

� Simple and dual sensor<br />

� Automatic changeover rough / detailed sensor<br />

� Vacuum and aeration program control<br />

� Inerting<br />

The self-parameterising device component vacuum<br />

regulation supports systems with and without<br />

ventilation/inerting.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

pH value / RedOx potential<br />

pH value and RedOx potentials can be monitored<br />

and controlled.<br />

� One-sided automatic control (acid or base)<br />

� Bilateral automatic control (acid and base)<br />

� Titration<br />

Stirring with Torque and Viscosity Recording<br />

The recording and control of the stirrer torque can<br />

supply important additional information about the<br />

process:<br />

� Viscosity<br />

� Dissipation<br />

� Reaction Progression<br />

Sampling<br />

Sampling and storage of liquids controlled with<br />

� Single valves<br />

� Multi-way valves<br />

� Pipetting Robot (AutoSam)<br />

In addition, many further, even more complex<br />

operations, such as phase separation,<br />

fractionated distillation or crystallisation, are<br />

available.<br />

Recipe Control<br />

Due to the extraordinarily powerful graphically<br />

programmable NAMUR and IEC compliant HiBatch<br />

recipe control module, users without automation<br />

technical experience can also establish complex<br />

recipe processes, e.g. multi-stage syntheses, within<br />

shortest time and have them conducted<br />

automatically (see HiBatch).<br />

For users who want to become operational as fast<br />

as possible, an extensive basis operation library<br />

(see SLGOPBIB) is available.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 65<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


66<br />

Instrumentation<br />

Laboratory Automation Hardware<br />

Principally all sensors, actuators and laboratory<br />

devices that have an interface or are supplied<br />

electrically can be linked in the automation, for<br />

example:<br />

Sensors<br />

� Temperature<br />

� Pressure<br />

� Flow<br />

� Level<br />

� Mass<br />

� pH/RedOx<br />

� Conductivity<br />

� Turbidity<br />

� Density<br />

� Gas concentration<br />

� Rotational speed<br />

� Phase bounderies<br />

Actuators<br />

� Actuators<br />

� Electrical and pneumatic bottom outlet valves<br />

� Pumps<br />

� Heating<br />

� Reflux Separators<br />

� Drives<br />

Laboratory Devices and Instrumenting<br />

Components<br />

� Scales (→ GraviDos)<br />

� Heating/cooling Thermostats<br />

� Stirrers (→ ViscoPakt)<br />

� Dosers (→ LabDos)<br />

� Phase Detection/Separation (→ PhaSep)<br />

� Analysers<br />

� Spectrometers (→ MoleculeEye)<br />

� Particle Sensor (→ ParticleEye)<br />

The LabManager Product Family<br />

The LabManager product family contains automation<br />

devices of different sizes that are built up in a<br />

modular way: The LabManager and the LabBoxes.<br />

This ensures that you always obtain a device which<br />

optimally meets your requirements. The connecting<br />

technology is uniformly based on connection boards<br />

with standardized plugs and sockets.<br />

Auxiliary Modules<br />

Further high-performance auxiliary modules and<br />

libraries extend the possibilities and facilitate work:<br />

� Adaptive automatic controllers for difficult control<br />

processes (SF-HICON)<br />

� LabCam for event controlled online picture<br />

documentation (SL-LABCAM)<br />

� IEC 61131 I control module in the PI, comparable<br />

to a SPS (SF AWL), SF-AWLPLUS<br />

� NAMUR RS232 interface driver for device<br />

couplings on UI and PI (SF-NAMSER)<br />

� On site mini terminal (HP-LABCOM1)<br />

� Remote <strong>Main</strong>tenance and Telecontrol<br />

� Remote Alarming<br />

� Auto-Tuning for Temperature Cascade Controller<br />

Libraries<br />

� Project module Library (SL-MODBIBALR)<br />

� Basis Operation Library (SL-GOPBIB)<br />

� Laboratory and Glass Apparatuses Library (SL-<br />

BIBRILK)<br />

☞<br />

You can find ready-to-use laboratory<br />

reactor systems in the chapter " Automated<br />

Laboratory Reactor Systems"<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


LabManager1 and 2<br />

Laboratory Automation Hardware<br />

The LabManager1 is the standard device for lab<br />

and pilot plant stations with up to 50 interfaces.<br />

The LabManager2 can be equipped with more than<br />

a hundred interfaces. The devices are equipped<br />

with a 32 bit CPU card with a real time operating<br />

system, a battery backed-up clock, battery backedup<br />

(UPS) and specially interference-resistant<br />

CMOS RAM for the saving of parameterisation,<br />

FLASH-ROM for the operating system, PCM<br />

control programs and a watchdog switching for the<br />

hardware and software monitoring as well as a<br />

serial interface for the operator console (UI). The<br />

devices are connected to a serial interface of the<br />

UI through a file transfer cable or a fibre-optic light<br />

guide. Up to eight devices can be operated from an<br />

UI.<br />

The power saving CMOS technology hardly<br />

produces lost heat so that the devices can be run<br />

without forced ventilation. Hence, high reliability<br />

and service life are guaranteed.<br />

Assembly Options<br />

In the standard assembly of the LabManager, the<br />

interface panels form the rear panel of the device.<br />

In case the LabManager is built into a control<br />

cabinet, the interface panels can be mounted on<br />

the door, on the back or on the sides. A specific<br />

panel frame is available for this purpose (see panel<br />

frame).<br />

The robust metal case of the LabManager is<br />

suitable for free-standing arrangement and for the<br />

mounting on 19-inch control cabinets.<br />

The user interfaces for the basic device functions<br />

are placed on the front panel of the LabManager.<br />

Properties:<br />

� 32 bit CPU<br />

� 1 MB CMOS-RAM<br />

� 6 MB FLASH store<br />

� PC<strong>10</strong>4 bus enlargement plug<br />

� battery buffered real-time clock<br />

� Watchdog (monitor switching)<br />

All devices are available with standard equipment<br />

or as basic devices for individual mounting.<br />

If one needs two outlets to be supplied with a<br />

LabManager device or if little place is available on<br />

site for the connecting technique, the interface<br />

panels can be distributed on a maximum of two<br />

outstations (see outstations). In any case though,<br />

the maximum cable length should not be more<br />

than 5 m.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


68<br />

LabBox1 and 2<br />

Laboratory Automation Hardware<br />

LabBox devices basically offer all characteristics of<br />

the LabManager devices but are designed for fewer<br />

interfaces and can only be equipped with internal<br />

sensor and actuator power supplies on a limited scale.<br />

These devices are preferably used for data logging or<br />

automation of small laboratory plants.<br />

They are respectively available with standard<br />

equipment or as a basic device for individual<br />

mounting.<br />

LabBox1 completely equipped LabBox2 completely equipped<br />

Complete Systems<br />

These ready-for-use complete systems possess<br />

proven equipment.<br />

The UI software must be individually selected since<br />

different LabVision software packages are required<br />

for different applications.<br />

LabBox1<br />

(LK-LABBOX1K)<br />

LabBox2<br />

(LK-LABBOX2K)<br />

LabManager1<br />

(LK-LABMAN1K)<br />

At any time, you can adapt a standard system to<br />

your increasing requirements by retrofitting<br />

modules.<br />

You will find a detailed description of these complete systems on the following pages.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

LabBox1 Complete System (LK-LABBOX1K)<br />

This complete system is suitable as a monitoring<br />

and data logging system.<br />

Equipment of the PI:<br />

� 4 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />

� 4 analogue inputs (0/4...20 mA or<br />

� -<strong>10</strong> V ... +<strong>10</strong> V) for the connection of analogue<br />

sensors for pressure, flow etc. and devices with<br />

analogue output such as pH meters, thermostats<br />

etc.<br />

Equipment of the UI:<br />

� State-of-the-art processor *<br />

� 1 GB RAM<br />

� Uninterrupted power supply (UPS)<br />

� UPS Management System<br />

� Pre-installed Windows XP or Windows Vista<br />

* The equipment is regularly adapted to the current standard.<br />

The UI can optionally be delivered in a desktop,<br />

tower or mini tower case and with modified<br />

equipment (see chapter Display and operating<br />

Components). The software is installed ready to use.<br />

The LabVision software update service is available<br />

for one year free of charge.<br />

The system consists of the following components:<br />

Amount Order Code Description<br />

1 LG-LABBOX1 LabBox1 standard device, for equipment see LG-LABBox1<br />

1 CG-ABK1 <strong>HiTec</strong> UI with UPS power supply and UPS management system,<br />

for equipment see CG-ABK1<br />

1 CP-M20TFTWS 20 Inch Widescreen TFT Monitor<br />

The LabBox1 can be upgraded with an additional<br />

panel with eight inputs or outputs. Up to four serial<br />

interface modules (HD-RS2329(P)L) can be<br />

equipped on the basis panel.<br />

The system can be upgraded with additional<br />

modules, e.g. internal power supply for sensors,<br />

data logger function (HS-NGS242), data logger<br />

function (SF-DATLOG), IEC 61131 I control module<br />

(SF-AWL, SF-AWLPLUS) etc.<br />

Delivery Scope Ready-to-use system (excl. LabVision software), LabBox1, UI with monitor and<br />

UPS, UI / PI cable, 230 V cable, manual<br />

Order Code Description<br />

LK-LABBOX1K LabBox1 standard system<br />

HS-NGS242 Optional 24 V internal power supply for actuators and sensors supply<br />

Recommended software package:<br />

Order Code Description<br />

SL-LABVIS LabVision basic package<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 69<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


70<br />

Laboratory Automation Hardware<br />

LabBox2 Complete System (LK-LABBOX2K)<br />

This complete system is for example suitable for the<br />

automation of lab reactor plants of medium<br />

complexity.<br />

Equipment of the PI:<br />

� 8 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />

� 8 analogue inputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V) for<br />

the connection of analogue sensors for pressure,<br />

flow etc. and devices with analogue output as pH<br />

meters, thermostats etc.<br />

� 8 analogue outputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V)<br />

For connecting devices with analogue input such<br />

as stirrer, thermostat, dosing pump etc.<br />

� 8 digital outputs (24 V, binary, PWM and PFM)<br />

For connecting binary actuators such as<br />

magnetic valves, heating, pumps, etc.<br />

� 2 serial RS232 interface modules for the<br />

connection of scales, devices and analysers with<br />

serial interface<br />

� Integrated sensor and actuator power supply<br />

Equipment of the UI:<br />

� State-of-the-art processor *<br />

� 1 GB RAM<br />

� Uninterruptible power supply (UPS)and UPS<br />

management system<br />

� Pre-installed Windows XP or Windows Vista<br />

* The equipment is regularly adapted to the current standard.<br />

The UI can optionally be delivered in a desktop,<br />

tower or mini tower case and with modified<br />

equipment (see chapter Display and operating<br />

Components). The software is installed and readyto-use.<br />

The LabVision software update service is<br />

available for one year free of charge.<br />

The system consists of the following components:<br />

Amount Order Code Description<br />

1 LG-LABBOX2-2 LabBox2 standard device with DAP8A, for equipment see LG-LABBOX2-2<br />

1 CG-ABK1 <strong>HiTec</strong> display and server components with UPS and UPS power supply<br />

management system, for equipment see CG-ABK1<br />

1 CP-M20TFTWS 20 Inch Widescreen TFT Monitor<br />

The system can be updated with additional modules,<br />

2 additional serial interfaces (HD-RS2329(P)L), IEC<br />

61131 I control module (SF-AWL, SF-AWLPLUS),<br />

adaptive controllers (SF-HICON), NAMUR interface<br />

driver for serial interfaces (SF-NAMSERxx) etc.<br />

Delivery Scope Ready to use system (excl. LabVision software), LabBox2, ABK1 with monitor and<br />

UPS, UI / PI cable, 230 V cable, manual<br />

Order Code Description<br />

LK-LABBOX2K-2 LabBox2 basic kit with LP-DAP8A<br />

Instead of the LP-DAP8A panel, a multi-purpose panel with 4 digital inputs and 4 digital outputs can be<br />

equipped.<br />

Order Code Description<br />

LK-LABBOX2K-1 LabBox2 standard system with LP-DE4DA4PA<br />

Recommended software packages (alternative):<br />

Order Code Description<br />

SL-LABVIPKONL Software package for LabBox2 For connecting small continuous-processes<br />

SL-LABVIPBATL Software package for LabBox2 For connecting small batch processes<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

LabManager Complete System (LK-LABMAN1K)<br />

This complete system is particularly suited for the<br />

automation of lab reactor plants of medium<br />

complexity.<br />

Equipment of the PI:<br />

� 8 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />

� 8 analogue inputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V) for<br />

the connection of analogue sensors for pressure,<br />

flow etc. and devices with analogue output as pH<br />

meters, thermostats etc.<br />

� 8 analogue outputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V)<br />

For connecting devices with analogue input as<br />

stirrer, thermostat, dosing pump etc.<br />

� 8 digital inputs (binary and frequency) for the<br />

connection of binary sensors such as filling level<br />

monitor, pressure regulators or status or alarm<br />

outputs of devices<br />

� 8 active digital outputs (24V, binary, PWM and<br />

PFM) For connecting binary actuators such as<br />

magnetic valves, heating, pumps, etc.<br />

� 2 RS232 serial interfaces for the connection of<br />

scales, devices and analysers with serial<br />

interface<br />

� Integrated sensor and actuator power supply<br />

� A free panel place for retrofitting<br />

Equipment of the UI:<br />

� State-of-the-art processor *<br />

� 1 GB RAM<br />

� Uninterrupted power supply (UPS)<br />

� UPS management system<br />

� Pre-installed Windows XP or Windows Vista<br />

* The equipment is regularly adapted to the current standard.<br />

The system consists of the following components:<br />

The UI can optionally be supplied in a desktop,<br />

tower or mini tower case and with modified<br />

equipment (see chapter Display and operating<br />

Components). The software is installed and readyto-use.<br />

The LabVision software update service is<br />

available for one year free of charge.<br />

The system can be updated with additional modules<br />

such as IEC 61131 I control module (SF-AWL, SF-<br />

AWLPLUS), adaptive automatic controllers (SF-<br />

HICON), NAMUR interface driver for serial<br />

interfaces (SF-NAMSERxx) etc..<br />

The free panel place can be equipped according to<br />

your requirements, for example with a thermocouple<br />

panel (LP-THP8 + interface card), a measurement<br />

module for load cells (HK-GRADOMS...) or a high<br />

precision temperature measurement module (HK-<br />

AD24PX8).<br />

Amount Order Code Description<br />

1 LG-LABMAN1 LabManager1 standard device, for equipment see LG-Labman1<br />

1 CG-ABK1 <strong>HiTec</strong> display and operating components with uninterrupted power supply and<br />

USV management, for equipment see UI1<br />

1 CP-M20TFTWS 20 Inch Widescreen TFT Monitor<br />

Delivery Scope Ready to use system (excl. LabVision software), LabManager1, UI with monitor<br />

and UPS, UI / PI cable, 230 V cable, manual<br />

Order Code Description<br />

LK-LABMAN1K Complete system with LabManager1<br />

Suitable software packages (alternative):<br />

Order Code Description<br />

SL-LABVIPBAT Software package for LabManager1 for running medium sized batch processes<br />

SL-LABVIPKON Software package for LabManager1 for running medium sized continuous-processes<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 71<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


72<br />

Standard Devices<br />

Laboratory Automation Hardware<br />

The standard devices possess proven equipment. At<br />

any time, you can adapt a standard system to your<br />

increasing requirements by retrofitting.<br />

These standard devices are included in the offered<br />

complete systems or are used for the extension of<br />

existing systems.<br />

LabBox1 Standard Device (LG-LABBOX1)<br />

This device is suited as measurement value collection and monitoring system<br />

For technical data, see LB-LABBOX1B.<br />

Equipment:<br />

� 4 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />

� 4 analogue inputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V) for<br />

the connection of analogue sensors for pressure,<br />

flow etc. and devices with analogue output such<br />

as pH meters, thermostats etc.<br />

Amount Order Code Description<br />

1 LB-LABBOX1B LabBox1 basic device<br />

1 HK-AD20NMUX8 analogue/digital 20 bit converter card solution, 8-channel multiplexer<br />

1 LP-AE4PT4PA NAMUR compliant plug-in panel with 4 0/4..20 mA current or <strong>10</strong> V..+<strong>10</strong> V<br />

voltage inputs, and 4 Pt<strong>10</strong>0 in two to four conductor technology<br />

1 HS-NGS242S 24 V DC, stabilised, 2,5 A<br />

The LabBox1 can be upgraded with an additional<br />

panel with eight inputs or outputs.<br />

Up to four serial interface modules (HD-<br />

RS2329(P)L) can be equipped. If more serial<br />

interfaced are intended to be equipped an additional<br />

card (HK-SER8ECB) is recommended.<br />

Delivery Scope LabBox1, UI/PI cable, power supply cable, manual<br />

Order Code Description<br />

LG-LABBOX1 LabBox1 standard device<br />

HK-SER8ECB Serial I/O card , 8 channels<br />

The system can be upgraded with additional<br />

modules, such as an integrated power supply for<br />

sensors and actuators (HS-NGS242), data logger<br />

function (SF-DATLOG), IEC 61131 I control module<br />

(SF-AWL, SF-AWLPLUS) etc.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

LabBox2 standard device (LG-LABBOX2)<br />

This standard device, amongst other applications, is<br />

particularly suited for the automation of lab reactor<br />

plants of medium complexity<br />

Equipment:<br />

� 8 Pt<strong>10</strong>0 inputs (-200 °C ... +600° C)<br />

� 8 analogue inputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V) for<br />

the connection of analogue sensors for pressure,<br />

flow etc. and devices with analogue output such<br />

as pH meters, thermostats etc.<br />

� 8 analogue outputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V)<br />

For connecting devices with analogue input such<br />

as stirrer, thermostat, dosing pump etc.<br />

� 8 digital outputs (24 V, binary, PWM and PFM)<br />

For connecting binary actuators such as<br />

magnetic valves, heating, pumps, etc.<br />

� Integrated sensor and actuator power supply<br />

� 2 serial RS232 interface modules for the<br />

connection of balances, devices and analysers<br />

with serial interface<br />

The standard device consists of the following components:<br />

All panel places of the device are assigned.<br />

The device can be upgraded with additional modules<br />

such as an IEC 61131 I control module (SF-AWL,<br />

SF-AWLPLUS), adaptive automatic controller (SF-<br />

HICON), NAMUR interface driver for serial<br />

interfaces (SF-NAMSERxx) as well as two more<br />

serial interfaces.<br />

For technical data, see LB-LABBOX2B.<br />

Amount Order Code Description<br />

1 LB-LABBOX2B LabBox basic device<br />

1 HK-AD20NMUX16 Analogue/digital 20 bit converter card resolution, 16 channel multiplexer<br />

1 LP-AEP8A Connection panel/board with 8 0/4..20 mA current or <strong>10</strong> V..+<strong>10</strong> V voltage<br />

inputs, integrated sensor<br />

1 LP-PTP8 NAMUR compliant interface panel for 8 Pt<strong>10</strong>0 in two to four conductor<br />

technology<br />

1 HK-DA812UI D/A 8 x 12 bit converter card, for analogue output -<strong>10</strong> ... <strong>10</strong> V or 0/4...20 mA<br />

1 LP-AAP8UI Interface panel for eightfold analogue output with current outputs (0/4...20<br />

mA) and voltage outputs (-<strong>10</strong>..+<strong>10</strong> V)<br />

1 HK-DEA16N digital input/output card with 2 x 8 inputs and 2 x 8 outputs.<br />

1 LP-DAP8A Interface panel with 8 digital outputs, 24V relays change-over contact, max. 3<br />

A resilient, 3 A power supply (short-circuit -proof)<br />

1 HK-SER8ECB additional serial card SER8ECB for the serial interface<br />

1 HS-NGS243 DC supply 24 V / 3 A calendared for actuators.<br />

1 HS-NGS241A DC supply 24 V / 1.5 A calendared for sensors.<br />

2 HD-RS2329L 9-pin RS232 interface<br />

Delivery Scope LabBox2, UI / PI cable, power supply cable, manual<br />

Order Code Description<br />

LG-LABBOX2-1 LabBox2 standard device 1 with DE4DA4PA<br />

Instead of the LP-DE4DA4PA panel, a panel<br />

LP-DAP8A with 8 digital outputs can be equipped.<br />

Order Code Description<br />

LG-LABBOX2-2 LabBox2 standard device 2 with LP-DAP8A<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 73<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


74<br />

Laboratory Automation Hardware<br />

LabManager Standard Device (LG-LABMAN1)<br />

This standard device is particularly suited for the<br />

automation of lab reactor plants of medium<br />

complexity.<br />

Equipment:<br />

� 8 Pt<strong>10</strong>0 inputs (-200 °C ... +600 °C)<br />

� 8 analogue inputs (0/4...20 mA or -<strong>10</strong> ... +<strong>10</strong> V)<br />

for the connection of analogue sensors for<br />

pressure, flow etc. and devices with analogue<br />

output such as pH meters, thermostats etc.<br />

� 8 analogue outputs (0/4...20 mA or -<strong>10</strong>...+<strong>10</strong> V)<br />

For connecting devices with analogue input<br />

such as stirrer, thermostat, dosing pump etc.<br />

� 8 digital inputs (binary and frequency) for the<br />

connection of binary sensors such as filling<br />

level monitor, pressure monitors or status or<br />

alarm outputs of devices<br />

� 8 active digital outputs (24 V, binary, PWM and<br />

PFM) for connecting binary actuators such as<br />

magnetic valves, heating, pumps, etc.<br />

� 2 RS232 serial interfaces for the connection of<br />

balances, devices and analysers with serial<br />

interface<br />

� Integrated sensor and actuator power supply<br />

� A free panel place for retrofitting<br />

� Serial add-on card SER16ECB for serial<br />

interfaces<br />

The standard device consists of the following components:<br />

The device can be upgraded with additional<br />

modules such as an IEC 61131 I control module<br />

(SF-AWL, SF-AWLPLUS), adaptive automatic<br />

controller (SF-HICON) or NAMUR interface driver<br />

for serial interfaces (SF-NAMSERxx) etc.<br />

The free panel place can be randomly equipped,<br />

for example with a thermocouple panel (LP-THP8<br />

+ interface card), a measurement module for load<br />

cells (LP-DMS4DA4PT + HK-AD24DMS4) or a<br />

high precision temperature measurement module<br />

(LP-PTPRP8 + HK-AD24PX8).<br />

For technical data, see LB-LABMAN1B.<br />

Amount Order Code Description<br />

1 LB-LABMAN1B LabManager basic device<br />

1 HK-AD20N Analogue/digital 20 bit converter card solution, floating secondary bus for the<br />

connection of multiplexer cards<br />

1 HK-HMUX Semiconductor 16 channel multiplexer card<br />

1 LP-AEP8A Plug-in panel with 8 0/4..20 mA current or -<strong>10</strong> V..+<strong>10</strong> V voltage inputs, integrated<br />

sensor feeding<br />

1 LP-PTP8 NAMUR compliant Interface panel for 8 Pt<strong>10</strong>0 in two to four conductor<br />

technology<br />

1 HK-DA812UI D/A 8 x 12 bit converter card, for analogue output -<strong>10</strong> ... <strong>10</strong> V, or 0/4...20 mA<br />

1 LP-AAP8UI Interface panel for fourfold analogue output with current (0/4...20 mA) and<br />

voltage outputs (-<strong>10</strong>..+<strong>10</strong> V)<br />

1 HK-DEA16N Digital input/output card with 2 x 8 inputs and 2 x 8 outputs, binary inputs,<br />

frequency and event count, binary outputs, pulse-width and pulse frequency<br />

modulations<br />

1 LP-DAP8A Interface panel with 8 digital outputs, 24 V relay change-over switch, capable of<br />

bearing maximum of 1 A, LED display,<br />

1 LP-DEP8 Interface panel with 8 active digital inputs<br />

1 HS-NGS241A DC supply 24 V / 1,5 A calendared for sensors<br />

1 HS-NGS243 DC supply 24 V, 3 A calendared for actuators<br />

1 HK-SER8ECB Additional channel serial interface card SER8ECB<br />

2 HD-RS2329PL 9-pin RS232 interface<br />

Delivery Scope LabManager1, UI/PI cable, power supply cable, manual<br />

Order Code Description<br />

LG-LABMAN1 LabManager1 standard device<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

Basis devices for individual supply<br />

A basic device for individual mounting will be<br />

equipped with interface cards and interface panels<br />

according to your requirements.<br />

LabBox1<br />

basis device<br />

(LB-LABBOX1B)<br />

2 free panel places<br />

LabBox2<br />

basis device<br />

(LB-LABBOX2B)<br />

4 free panel places<br />

LabManager1<br />

basis device<br />

(LB-LABMAN1B)<br />

6 free panel places<br />

LabManager2<br />

basis device<br />

(LB-LABMAN2B)<br />

13 free panel places<br />

Example of special<br />

building:<br />

LabManager3 basis<br />

device (LABMAN3B)<br />

20 free panel places<br />

A LabManager PI is for exampleassembled as<br />

follows:<br />

� a basic device (LB-LABMAN1B),<br />

� an analogue/digital converter card (HK-AD20N),<br />

� a multiplexer card (HK-HMUX)<br />

� two interface panels (for example LP-AEP8 & LP-<br />

PTP8) as well as<br />

� a UI, e.g. a CG-ABK1 with<br />

� LabVision software.<br />

This configuration includes eight universal potentialfree<br />

analogue inputs and eight inputs for Pt<strong>10</strong>0<br />

temperature sensors and is suitable for monitoring<br />

and data logging.<br />

If the system is not supposed to be updated later, a<br />

LabBox would be the more cost-efficient alternative.<br />

If more than seven interface panels, including the<br />

basis panel, are needed, it is necessary to use a<br />

double height LabManager2. Seven more panel<br />

places are available due to the additional height unit.<br />

In case of even greater interface requirement,<br />

several more devices can be run by one UI.<br />

Common Features<br />

All devices are equipped with a CPU32 card, a basis<br />

panel and a power supply.<br />

A power supply for sensors and actuators can<br />

optionally be integrated into the devices in order to<br />

obtain a compact and comprehensive automation<br />

solution.<br />

The corresponding UI LabVision software will also<br />

be individually customised to your precise<br />

requirements.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Stirring and<br />

Dispersing<br />

Services


76<br />

LabBox Basis Device<br />

Laboratory Automation Hardware<br />

As an intelligent central processing unit, a LabBox<br />

basis device contains a 32 bit controller card<br />

(CPU32), a basis panel and a power supply for the<br />

cards.<br />

Next to a low heat device socket for the power<br />

supply and the main switch, the basis panel has a<br />

RS232 interface (opt. RS485 or Ethernet) for the<br />

connection of the UI. Up to four more serial<br />

interfaces can be mounted on the basis panel.<br />

A minimum system can be arranged for example as<br />

follows:<br />

� a basic device (e.g. LB-LABBOX1B)<br />

� an analogue/digital converter card with 8-channel<br />

multiplexers (HK-AD20NMUX8) with<br />

� an interface panel (e.g. LP-AE4PT4P) and<br />

� a user interface UI (CG-ABK1).<br />

With this setup, a LabBox is suitable for monitoring<br />

and data logging with four universal potential-free<br />

analogue inputs (-<strong>10</strong>..+<strong>10</strong> V, 0/4-20 mA) for the<br />

connection of any analogue sensors and/or signals<br />

and four inputs for the connection of Pt<strong>10</strong>0<br />

temperature sensors. The device is integrated to the<br />

LK-LABBOX1K standard system package in this<br />

configuration.<br />

If the system is supposed to be upgraded later with<br />

a total of more than eight interfaces, a LabBox2,<br />

LabManager1 or LabManager2 is the more costefficient<br />

alternative.<br />

LabBox1, example configuration LabBox2, example configuration<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

LabBox1 Basis Device (LB-LABBOX1B)<br />

Extension Reserve<br />

Reserve equipped with<br />

(1) panel 1 all available panels*<br />

(2) panel 2 all available panels*<br />

(3) SER 1 HD-RS2329L, HD-RS485P<br />

(4) SER 2 HD-RS2329L, HD-RS485P<br />

(5) SER 3 HD-RS2329L, HD-RS485P<br />

(6) SER 4 HD-RS2329L, HD-RS485P<br />

(7) internal<br />

2 interface cards plus HK-SER8ECB, sensor / actuator power supply with HS-<br />

NGS243<br />

* With the exception of PSER99 due to the installation depth of the interface modules RS2329L, RS2329PL and RS4859P<br />

Technical Data<br />

Case 3 HE desktop case<br />

Basis Panel UI interface (PC), 230 V~ connection and function LEDs<br />

CPU CPU32 card, 32 bit Embedded Controller with watchdog<br />

Extension Reserve See table<br />

Dimensions Depth: 3<strong>10</strong> mm<br />

Width: 236 mm<br />

Height: 145 mm (3 HE)<br />

Working Temperature 0 to 50 °C, non-condensing<br />

Storing Temperature 0 to 50 °C<br />

IP Protection Category IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory devices<br />

Power Consumption From 30 W to 140 W, depending on the configuration<br />

Operating Voltage 230 V +<strong>10</strong>, -20 %<br />

Delivery Scope LabBox1 basis device, cable for the connection to the 9-pin RS232 interface of<br />

the UI, 9-pin, 230 V cable, manual<br />

Order Code Description<br />

LB-LABBOX1B LabBox1 basis device for individual equipping<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

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and Sensors<br />

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Stirring and<br />

Dispersing<br />

Services


78<br />

Laboratory Automation Hardware<br />

LabBox2 Basis Device (LB-LABBOX2B)<br />

Extension Reserve<br />

Reserve supplied with<br />

(1) panel 1 all available panels*<br />

(2) panel 2 all available panels*<br />

(3) panel 3 all available panels*<br />

(4) panel 4 all available panels*<br />

(5) SER 1 HD-RS2329L, HD-RS485P<br />

(6) SER 2 HD-RS2329L, HD-RS485P<br />

(7) SER 3 HD-RS2329L, HD-RS485P<br />

(8) SER 4 HD-RS2329L, HD-RS485P<br />

(9) internal 4 interface cards, sensor / actuator power supply<br />

HS-NGS243, HS-NGS241A,<br />

HS-NGS153SN, HS-NGS245SN<br />

* With the exception of PSER99 due to the installation depth of the interface modules RS2329L, RS2329PL and RS4859P<br />

Technical Data<br />

Case 3 HE desktop units<br />

Basis panel UI interface (PC), 230 V~ connection and indication LEDs<br />

CPU CPU32 card, 32 bit Embedded Controller with watchdog<br />

Extension Reserve See table<br />

Dimensions Depth: 3<strong>10</strong> mm<br />

Width: 342mm<br />

Height: 145 mm (3 HE)<br />

Working Temperature 0 to 50 °C, non-condensing<br />

Storing Temperature 0 to 50 °C<br />

IP protection class IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory device<br />

Power Consumption From 30 W to 240 W, depending on the configuration<br />

Operating Voltage 230 V +<strong>10</strong>, -20 %<br />

Delivery Scope LabBox2 basis device, cable for the connection to the 9-pin RS232 interface of<br />

the UI, 9-pin, 230 V cable, manual<br />

Order Code Description<br />

LB-LABBOX2B LabBox2 basis device for individual equipping<br />

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LabManager Basis Devices<br />

As an intelligent central processing unit, a<br />

LabManager basic device contains:<br />

Laboratory Automation Hardware<br />

� one 32 bit controller card (HK-CPU32),<br />

� one HK-SER8ECB card to connect up to 6(8)<br />

HD-RS2329(p) RS232 interface modules<br />

� a LP-BASIS1 or 2 basis panel and<br />

� a power supply for the cards.<br />

The basis panel is part of the standard equipment of<br />

a basic device and does not have to be ordered<br />

separately.<br />

Next to a low heat device socket for the power<br />

supply, the basis panel (LP-BASIS2) has a potentialfree<br />

RS232 interface for the connection of the UI. Up<br />

to six additional serial interfaces can be connected<br />

to the basis panel.<br />

LabManager1, front view<br />

LabManager2, front view<br />

Basis panel: LP-BASIS2<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Stirring and<br />

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80<br />

Laboratory Automation Hardware<br />

LabManager1 Basis Device (LB-LABMAN1B)<br />

The device is assembled with the offered interface cards and panel models and is equipped with the<br />

available extra modules.<br />

Extension Reserve<br />

Reserve can be equipped with<br />

(1) Panel 1 all available panels<br />

(2) Panel 2 all available panels<br />

(3) Panel 3 all available panels<br />

(4) Panel 4 all available panels<br />

(5) Panel 5 all available panels<br />

(6) Panel 6 all available panels<br />

(7) SER 1 HD-RS2329L, HD-RS2329PL, HD-RS485P<br />

(8) SER 2 HD-RS2329L, HD-RS2329PL, HD-RS485P<br />

(11) internal 7 interface cards, sensor-/ actuator power supply, HS-NGS243, HS-NGS241A,<br />

HS-NGS153SN, HS-NGS245SN<br />

Technical Data<br />

Case 3 HE desktop units<br />

Basis Panel Floating UI interface (PC), 230 V~ connection and indication LEDs<br />

CPU HK-CPU32 card, 32 bit Embedded Controller with watchdog, HK-SER8ECB card<br />

Extension Reserve Depth: 370 mm<br />

Width: 450 mm (19“)<br />

Height: 145 mm (3 HE)<br />

Dimensions See table<br />

Working Temperature 0 to 50 °C, non-condensing<br />

Storing Temperature 0 to 50 °C<br />

IP Protection Category IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory devices<br />

Power consumption 30 W to 240 W, depending on the configuration (without 230 V switching outputs)<br />

Operating Voltage 230 V +<strong>10</strong>, -20 %<br />

Delivery Scope LabManager, cable for the connection to the 9-pin RS232 interface of the UI,<br />

power supply cable, manual<br />

Order Code Description<br />

LB-LABMAN1B LabManager1 basis device for individual equipping<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

LabManager2 Basis Device (LB-LABMAN2B)<br />

The device is assembled with the offered interface cards and panel models and is equipped with the<br />

available extra modules.<br />

Extension Reserve<br />

Reserve Can be equipped with<br />

(1) Panel 1 all available panels<br />

(2) Panel 2 all available panels<br />

(3) Panel 3 all available panels<br />

(4) Panel 4 all available panels<br />

(5) Panel 5 all available panels<br />

(6) Panel 6 all available panels<br />

(7) Panel 7 all available panels<br />

(8) Panel 8 all available panels<br />

(9) Panel 9 all available panels<br />

(<strong>10</strong>) Panel <strong>10</strong> all available panels<br />

(11) Panel 11 all available panels<br />

(12) Panel 12 all available panels<br />

(13) Panel 13 all available panels<br />

(14) SER1 HD-RS2329L, HD-<br />

RS2329PL, HD-RS485P<br />

(15) SER2 HD-RS2329L, HD-<br />

RS2329PL, HD-RS485P<br />

(18) internal 12 interface cards, sensor<br />

/ actuator power supply<br />

HS-NGS241A<br />

HS-NGS248<br />

Technical Data<br />

Case 6 HE desktop units<br />

Basis Panel Potential-free UI interface (PC), power supply and indication LEDs<br />

CPU HK-CPU32 card, 32 bit Embedded Controller with watchdog, HK-SER8ECB card<br />

Dimensions Depth: 370mm<br />

Width: 450mm (19“)<br />

Height: 280mm / 6HE<br />

Extension Reserve See table<br />

Working Temperature 0 to 50 °C, non-condensing<br />

Storing Temperature 0 to 50 °C<br />

IP Protection Category IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory device<br />

Power Consumption 30 W to 1500 W, depending on the configuration (without 230 V switching outputs)<br />

Operating Voltage 230 V +<strong>10</strong>, -20 %<br />

Delivery Scope LabManager, cable for the connection to the 9-pin RS232 interface of the UI, 230<br />

V cable, manual<br />

Order Code Description<br />

LB-LABMAN2B LabManager basis device for individual equipping<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 81<br />

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Components<br />

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Stirring and<br />

Dispersing<br />

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82<br />

Outstations (LZ-USTAT)<br />

Laboratory Automation Hardware<br />

The use of a space-saving outstation is<br />

recommended as a ideal solution in case of limited<br />

space. Up to two outstations can be connected to a<br />

LabManager. The case is made of anodized<br />

aluminum. A 24 V DC power supply primarily used<br />

by the binary outputs is integrated into every<br />

outstation.<br />

Dimensions Depth: 80 mm<br />

Width: 605 mm (LZ-USTAT6), 666 mm (LZ-USTAT7)<br />

Example Assembly<br />

for LZ-USTAT6<br />

Height: 141 mm<br />

Consequently, actuators (for example valves) can be<br />

connected directly, i.e. without the need of external<br />

power supply.<br />

Of course, the outstation can be equipped according<br />

to the specific application.<br />

It is connected to the LabManager via a 3 m<br />

(maximum 5 m) cable.<br />

a) LP-PHRED24B, LP-AEP2x4, LP-AEP8, LP-AAP8UI, LP-DE4DA4P, LP-DAP8A<br />

b) LP-PHRED24B, LP-AEP2x4, LP-AEP8, LP-AAP8UI, LP-DEP8, LP-DAP8<br />

c) LP-PHRED24B, LP-AEP2x4, LP-AEP8, LP-AAP8UI, LP-DEP8, LP-DAP8A<br />

Order Code Description<br />

LZ-USTAT6 Outstation for LabManager with 6 panel places<br />

including 3 m connecting cable for the LabManager<br />

LZ-USTAT7 Outstation for LabManager with 7 panel places<br />

including 3 m connecting cable for the LabManager<br />

LZ-USTAT5M Extension of the connecting cable to 5 m<br />

The feasibility of other interface combinations must<br />

be coordinated with our design department on an<br />

individual basis.<br />

Panel Frame (LZ-PR..)<br />

If the LabManager is built into a control cabinet, the<br />

interface panels can be mounted on the door, on the<br />

rear or on the sides, or into 19” slide-in modules<br />

(e.g. Located above or beneath the LabManager).<br />

One or several panel frames are screwed to a<br />

suitable section for this purpose.<br />

Order Code Description<br />

LZ-PR7 Panel frame for the installation of 7 panels into control cabinet<br />

LZ-PRx Panel frame for control cabinet installation. Panel number according to customer<br />

specifications<br />

LZ-PR19Z3HE Panel frame for 19“ rack installation of 7 Panels<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Case Accessories<br />

Mounting Bracket (LZ-BEFW19)<br />

Laboratory Automation Hardware<br />

The mounting brackets allow the installation into<br />

19 inch cabinets.<br />

Order Code Description<br />

LZ-BEFW19 Mounting bracket for 19 inch cabinets<br />

Handle Bars (LZ-GRIFFxx)<br />

The various handle bars improve the handling, or, if<br />

used as stands, guarantee the stable upright stand<br />

of the devices.<br />

Order Code Description<br />

LZ-GRIFFLU Wing handle bars for LAB PIs<br />

LZ-GRIFFRO Front handle bars for LAB PIs<br />

LAB PI interfaces<br />

The interfaces for the process are usually found on<br />

the PI (LabManager and LabBox). Serial interfaces<br />

and bus interfaces are an exception. These can be<br />

provided on the PI and on the UI (See UI interfaces).<br />

Which signal type accords to which sensor, actuator, or device?<br />

The following table displays via which signal type the<br />

different instrumentation components such as<br />

sensors, actuators and laboratory devices<br />

communicate and how they can be connected to the<br />

LAB PIs.<br />

.<br />

The PI is equipped with interface panels with<br />

standardized NAMUR compliant connections. There<br />

are suitable panels for the connection of virtually all<br />

actuators, sensors and devices present in the lab.<br />

Many laboratory devices have several connections<br />

for selection, for example analogue I/O or RS232.<br />

As far as practical applications are concerned, the<br />

analogue interfaces are more uncomplicated since<br />

less modifications have to be carried out and a multimeter<br />

suffices as a test apparatus, if one is required.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 83<br />

Equipment and<br />

Components<br />

Process Analytics<br />

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Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


84<br />

Task, sensor intended for<br />

connection<br />

/actuator/device<br />

Laboratory Automation Hardware<br />

Panel/interface<br />

module<br />

Signal type, connection, driver Reference source for<br />

sensor/actuator/device<br />

Sensors<br />

Temperature (Absolute, difference)<br />

Pt<strong>10</strong>0 LP-PTP8 Connected directly See sensors/Pt<strong>10</strong>0<br />

Pt<strong>10</strong>0, accuracy LP-PTPRP8 Connected directly See sensors/Pt<strong>10</strong>0<br />

Thermocouples LP-THP8 Connected directly See sensors/Thermocouples<br />

Four wire Transmitter LP-AEP8A 0-20 mA, Connected directly upon request<br />

Two wire Transmitter LP-AEP8A 4-20 mA, Connected directly upon request<br />

Temperature controller LP-DEP8 Binary See temperature controller/ watchdog device<br />

Pressure (absolute, relative, difference)<br />

2 conductor transmitters (pressure and<br />

rough vacuum)<br />

LP-AEP8A 4-20 mA, Connected directly See sensors / pressure sensors<br />

Pirani vacuum measuring instrument Various with Serial, NAMUR-Serial Driver<br />

(precise vacuum) with RS232 interface HD-RS232(P)L .<br />

(possible analogue connector) upon request<br />

Pressure controller<br />

Flow gas<br />

LP-DEP8 Binary See pressure controller/watchdog device<br />

Mass flow rate Mass Flow Meter LP-AEP8A voltage or current signal, sensor<br />

feeding<br />

See sensors/pressure sensors<br />

Mass flow rate Mass Flow Controller LP-AEAP8IA, Input and output: voltage or current upon request<br />

LP-AEAP8UA signal, sensor feeding<br />

Mass flow rate Mass Flow Meter and Various with Serial, NAMUR-Serial Driver upon request<br />

Controller<br />

HD-RS232(P)L<br />

Volumetric with gas meter LP-AEP8 Frequency Signal, HK-DEA16F upon request<br />

Gravimetric with gas bottle on balance Various with Driver for scales by Scaltec, Kern, See laboratory devices/scales<br />

Liquid flow<br />

HD-RS232(P)L Sartorius, and Mettler available<br />

Mass flow rate of Coriolis LP-AEP8 0/4...20 mA On request<br />

Volumetric with turbine wheel sensor LP-DEP8 Frequency signal on HK-DEA16N See sensors / Teflon flow<br />

Gravimetric with balance Various with HD- Drivers for scales from SCATLTEC, See laboratory device / balance<br />

RS232(P)L Kern, Sartorius, and Mettler in every<br />

<strong>HiTec</strong> <strong>Zang</strong> PI.<br />

Gravimetric with GraviDos (separately) LP-AEP8A DMS load cell with GRADOMV1 See laboratory device/dosage systems<br />

Gravimetric with GraviDos (System) LP-AEP8DMS DMS load cell with HK-AD24DMS See laboratory device/dosage systems<br />

Flow controller<br />

Level<br />

LP-DEP8 Binary signal on HK-DEA16N, See flow controller and watchdog device<br />

Gravimetric with GraviDos (separately) LP-AEP8A DMS load cell with GRADOMV1 See Laboratory Devices /Dosing Systems<br />

Gravimetric with GraviDos (System) LP-AEP8DMS DMS load cell onHK-AD24DMS See Laboratory Devices /Dosing Systems<br />

Conductive, capacitive LP-AEP8(A) 0...<strong>10</strong> V, 0/4...20 mA Upon request<br />

Trickling method, hydrostatic pressure LP-AEP8(A) 0...<strong>10</strong> V, 0/4...20 mA Upon request<br />

Gravimetric with balance Various with HD- Drivers for balances of SCATLTEC, See laboratory device/balance<br />

RS232(P)L Kern, Sartorius, and Mettler in every<br />

<strong>HiTec</strong> <strong>Zang</strong> PI.<br />

Level controller<br />

Mass<br />

LP-DEP8(A) Binary signal on HK-DEA16N See level controller<br />

with lab balance Various with HD- Drivers for balances of SCATLTEC, See laboratory device/scale<br />

RS232(P)L Kern, Sartorius, and Mettler in every<br />

<strong>HiTec</strong> <strong>Zang</strong> PI.<br />

Gravimetric with GraviDos (separately) LP-AEP8A DMS load cell on GRADOMV1 See laboratory device/dosage systems<br />

Gravimetric with GraviDos (System)<br />

pH/Rhedox<br />

LP-AEP8DMS DMS load cell on HK-AD24DMS See laboratory device/dosage systems<br />

Glass-probe, short distance LP-PHRED24 Directly connected electrode signal upon request<br />

Glass-probe, long distance LP-AEP8(A) Electrode signal directly connected via<br />

cable booster IL-PHAMP1<br />

upon request<br />

Ext. pH measuring instrument<br />

Distance<br />

LP-AEP8(A) 0...<strong>10</strong> V, 0/4...20 mA upon request<br />

Inductive, optical proximity sensor<br />

Rotation speed<br />

LP-DEP8A Binary signal and feeding on HK-<br />

DEA16N<br />

Sensors/distance<br />

Inductive, optical proximity sensor<br />

Electrical heating<br />

LP-DEP8A Binary signal and feeding on HK-<br />

DEA16N<br />

Actuators<br />

Sensors/rotation speed<br />

Heating dome, calorific, immersion HP-B230VxxA Binary and PWM, 230 V~, Connected upon request<br />

heater<br />

directly<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

Continued: Which signal type on which sensor, actuator or device?<br />

Task, connected Panel/interface Signal type, connection, driver Reference source for<br />

Sensor/actuator/device module<br />

sensor/actuator/device<br />

Valve on/off and 3/2 paths, reflux divisor<br />

Magnetic valve LP-DAP8A Binary, direct connection See Laboratory Devices/Valves<br />

Engine valve digital driving LP-DAP8x 2 x binary outputs for on and off upon request<br />

Final position acknowledgement<br />

Proportionally to valve<br />

LP-DEP8(A) 2 x binary inputs for on and off upon request<br />

Magnetic valve LP-DAP8T HK-DEA16N, PWM See laboratory device/ proportional<br />

valve<br />

Engine valve analogue driving LP-AAP8UI 0...<strong>10</strong> V, 0/4...20 mA upon request<br />

Engine valve digital driving LP-DAP8x 2 x binary outputs for on and off upon request<br />

Final position acknowledgement LP-DEP8(A) 2 x binary inputs for on and off upon request<br />

Position acknowledgement<br />

Multipath Valve<br />

LP-AEP8 1 x analogue input for position upon request<br />

With stepping motor drive<br />

Scales<br />

HD-RS232(P)L,<br />

HD-RS485P<br />

Serial, NAMUR-Serial Driver<br />

Laboratory device<br />

upon request<br />

Lab Scales from Scaltec, Sartorius, Various with HD- Drivers for scales from SCATLTEC, Kern, Sartorius, See laboratory devices/Scales<br />

Kern, and Mettler<br />

Analysers, Spectrometers<br />

RS232(P)L and Mettler in every <strong>HiTec</strong> <strong>Zang</strong> PI.<br />

GC, HPLC, NIR, ... HD-RS232(P)L, Serial connection to the PI through a NAMUR serial upon request<br />

Torque measuring stirrer<br />

HD-RS485P driver or serial connection to the UI through a PI<br />

driver<br />

ViscoPakt analogue IO LP-AEP8(A),<br />

LP-AAP8UI,<br />

LP-AEAP8U(A),<br />

LP-AEAP8I(A)<br />

See laboratory devices<br />

ViscoPakt Serial<br />

Dosing pump<br />

HD-RS232(P)L NAMUR-Serial Driver See laboratory devices/measuring<br />

stirrer<br />

Diaphragm pump LP-DAP8 Pulse frequency, HK-DEA16N See laboratory devices / dosing<br />

pumps<br />

Tube pump, reciprocating pump LP-DAP8 HK-DA816UI 0-<strong>10</strong> V or 0/4..20 mA See laboratory devices / dosing<br />

pumps<br />

Serial dosing pumps HD-RS232(P)L, Serial, NAMUR-Serial Driver See laboratory devices / dosing<br />

Solid Doser<br />

HD-RS485P<br />

pumps<br />

SOLIDOS<br />

Heating/cooling thermostat<br />

LP-DAP8 Pulse Frequency See laboratory devices/ solid<br />

matter dosing apparatus<br />

Analogue EA LP-AEP8(A), Inputs and outputs: 0...<strong>10</strong> V, 0/4...20 mA See laboratory devices/<br />

LP-AAP8UI,<br />

LP-AEAP8<br />

moderating device<br />

Serial Interface Various with Serial, NAMUR-Serial Driver<br />

See laboratory devices/<br />

HD-RS232(P)L, (Drivers for common thermostats of Haake, Huber, moderating device<br />

Calibrating-heating<br />

HD-RS485P Julabo, Laude already integrated)<br />

HD-RS232(P)L<br />

Abbreviation:<br />

Serial,<br />

NAMUR-driver<br />

See laboratory devices/ calibrating heating<br />

PWM: Pulse Width Modulated<br />

PFM: Pulse Frequency Modulated<br />

x: arbitrary alphabetic character<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

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Automation<br />

Hardware<br />

Automation<br />

Software<br />

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Laboratory Automation Hardware<br />

Which Modules for which Signal Type?<br />

The following table gives an overview of which card/<br />

panel combinations are suitable for frequently used<br />

signal and/or connection types.<br />

For each case, you can find a more detailed<br />

description of the possibilities in the description of<br />

the modules, cards, and panels.<br />

You can find suitable connecting cables for the<br />

laboratory devices of different manufacturers under<br />

"Cables for Instrumentation“.<br />

Signal Connection possibility for possible cards possible panels<br />

Analogue Output<br />

voltage and current Heating/cooling thermostats<br />

setpoint and actual value, stirrer<br />

torque, pressure feeder, flow meter<br />

HK-AD20NMUX8,<br />

HK-AD20NMUX16, HK-AD20N +<br />

HK-HMUX<br />

4-conductor Pt<strong>10</strong>0 Pt<strong>10</strong>0 direct temperature sensor HK-AD20NMUX8,<br />

HK-AD20NMUX16, HK-AD20N +<br />

HK-HMUX<br />

LP-AEP8, LP-AEP8A,<br />

LP-AE4PT4P, LP-AEAP8U(A), LP-<br />

AEAP8I(A)<br />

LP-PTP8, LP-AE4PT4P<br />

4-conductor accuracy Pt<strong>10</strong>0 Pt<strong>10</strong>0 direct temperature sensor HK-AD24PX8 LP-PTPRP8<br />

Thermocouples direct thermocouples HK-AD20NMUX8,<br />

HK-AD20NMUX16, HK-AD20N +<br />

HK-HMUX<br />

LP-THP8<br />

pH/RedOx directly connected pH and RedOx HK-AD20NMUX8,<br />

IL-PHAMP1 external to LP-AEP8,<br />

electrodes<br />

HK-AD20NMUX16, HK-AD20N + LP-AEP8A, LP-AE4PT4P,<br />

Load Cells<br />

HK-HMUX<br />

LP-AEAP8U(A), LP-AEAP8I(A),<br />

LP-PHRED24 with HK-PHAMP<br />

(just for LZ-USTAT)<br />

GraviDos load cell<br />

Analogue output<br />

HK-AD24DMS4 LP-DMS4DA4PT,<br />

2xHK-AD24DMS4, LP-DMS8<br />

voltage and current Heating/cooling thermostats set HK-DA812UI LP-AAP8UI, LP-AEAP8U(A), LPpoint,<br />

stirrer rotation speed setpoint<br />

value, proportional valves...<br />

AEAP8I(A)<br />

Combined analogue input and output<br />

voltage or current Heating/cooling thermostats set HK-DA812UI + HK-AD20NMUX8, LP-AEAP8U(A), LP-AEAP8I(A)<br />

point and actual value, stirrer HK-AD20NMUX16, HK-AD20N +<br />

Digital output<br />

rotation speed setpoint value and<br />

actual value, massflow controller<br />

setpoint value and actual value ...<br />

HK-HMUX<br />

Digital Magnetic valves, drive valves, HK-DEA16N LP-DAP8, LP-DAP8A,<br />

pumps, monitors, switching boxes<br />

LP-DE4DA4P, LP-DA230V8<br />

Pulse Width Modulated<br />

Magnetic valves, engine valves, HK-DEA16N LP-DAP8, LP-DAP8A,<br />

(PWM)<br />

pumps, floodgates, switching<br />

boxes<br />

LP-DE4DA4P, LP-DAP8T<br />

Pulse Frequency Modulated Dosing pumps with pulse HK-DEA16N LP-DAP8, LP-DAP8A,<br />

(PFM)<br />

Digital input<br />

activation, reflux divisors, solid<br />

matter dosing apparatus SOLIDOS<br />

LP-DE4DA4P<br />

Binary Boundary value senders,<br />

controllers, proximity sensors,<br />

status signals of devices<br />

HK-DEA16N LP-DEP8(A), LP-DE4DA4P<br />

Events < 50Hz Belt weigher, gas volume counter HK-DEA16N LP-DEP8(A), LP-DE4DA4P<br />

Frequency < 50Hz<br />

Serial interfaces<br />

Turbine wheel flow meter, energy<br />

counter, proximity sensors<br />

HK-DEA16N LP-DEP8(A), LP-DE4DA4P<br />

RS232, RS485 Balance, stirrers, Heating/cooling HD-RS2329L, HD-RS2329PL, HD- Basis panel, LP-SER99, LPthermostats,<br />

analysers, robots RS485P<br />

PHRED24 (only for LZ-USTAT)<br />

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Interface Panels for Analogue Input<br />

Laboratory Automation Hardware<br />

Different systems are available for analogue input,<br />

which differ in respect to accuracy and electric<br />

robustness. The combined HK-AD20NMUX8 and<br />

HK-AD20NMUX16 AD converter multiplexer cards<br />

can be used for smaller systems.<br />

8 Voltage and Current Inputs (LP-AEP8)<br />

The panel for analogue input is<br />

designed for collecting voltages<br />

of -<strong>10</strong>...+<strong>10</strong> V and current<br />

signals of 0/4 ... 20 mA.<br />

Laboratory devices such as<br />

heat/cool thermostats or mixers<br />

and measuring sensors can be<br />

connected to the eight potentialfree<br />

and EMC robust inputs.<br />

� 8 analogue inputs for voltage and current of<br />

0/4 ... 20 mA (6-pin tuchel socket DIN45322)<br />

� Combinable with other analogue input panels<br />

An example out of many possible applications is the<br />

recording of a pressure with a pressure sensor due<br />

to 4...20 mA two wire technology. This gives out 4<br />

mA at 0 mbar and 20 mA at <strong>10</strong>00 mbar.<br />

The measured electric value is converted to a mbar<br />

value in the PI by appropriate scaling of the data<br />

point. For this purpose, the parameters in LabVision<br />

must be set to the following values:<br />

Minimum process value 0<br />

Maximum process value <strong>10</strong>00<br />

Minimum interface value 4<br />

Maximum interface value 20<br />

EMC robust HK-HMUX multiplexer cards together<br />

with a HK-AD20N AD converter card are<br />

recommended for bigger systems.<br />

For each of the different signal and sensor types,<br />

suitable NAMUR standard compliant interface<br />

panels are available.<br />

Each interface panel for analogue input has 8 inputs<br />

while HK-HMUX multiplexer cards and the HK-<br />

AD20NMUX16 have 16 channels.2 panels can be<br />

connected to each card. Here it is possible to<br />

combine different panels, for example a panel for<br />

thermocouples with a panel for Pt<strong>10</strong>0 feelers.<br />

To protect unused inputs against corrosion and dust,<br />

you can cover them with plastic caps.<br />

Connection examples for the LP-AEP8 and LP-AEP8A analogue<br />

input interface panels<br />

Note: When using a LP-AEP8A panel, you can<br />

connect sensors with a twin or quadruple wire<br />

connection directly to a socket, i.e. without external<br />

power supply.<br />

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Technical Data<br />

Laboratory Automation Hardware<br />

Signal 0/4 ... 20 mA and -<strong>10</strong> ... +<strong>10</strong> V<br />

Connection type 6-pin socket, DIN 45322<br />

Usable with HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />

For the evaluation of Analogue signals such as stirrer rotation speed, torque, pressure, fill level,<br />

temperature output of a thermostat, pH-value on IL-PHAMP1 (external), etc<br />

Product description Interface panel with 8 inputs of 0/4..20 mA current or -<strong>10</strong> V..+<strong>10</strong> V voltage<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-AEP8 Interface panel with 8 current and voltage inputs<br />

LZ-AKTUB Caps for tuchel Sockets<br />

Suitable connecting cables for laboratory devices and sensors<br />

Order Code Description<br />

ZK-LAB-HI01-IA-UP-O-01 Analogue input cable with open ends for voltage<br />

ZK-LAB-HI01-IA-IP-O-01 Analogue input cable with open ends for 0/4..20 mA twin conductor<br />

For other cables, see "Cables for Instrumentation“.<br />

8 Voltage and Current Inputs with Power Supply (LP-AEP8A)<br />

The panel for analogue input is<br />

designed for collecting voltages<br />

of -<strong>10</strong>...+<strong>10</strong> V and current<br />

signals of 0/4 ... 20 mA.<br />

Laboratory devices such as<br />

heating/cooling thermostats or<br />

stirrers and measuring sensors<br />

can be connected to the eight<br />

potential-free and EMC robust<br />

inputs.<br />

� 8 analogue inputs for voltage and current of<br />

0/4 ... 20 mA (6-pin tuchel socket)<br />

� sensor feeding<br />

� combinable with other analogue input panels<br />

You can connect sensors with a twin or quadruple<br />

wire connection directly to a socket of the LP-AEP8A<br />

panel, i.e. without external power supply. Therefore,<br />

Technical Data<br />

connecting requires only few seconds since the<br />

connection to a power supply is not necessary.<br />

Connection examples for sensors as voltage and<br />

current transmitters in two and four wire technology<br />

Signal 0/4 ... 20 mA and -<strong>10</strong> ... +<strong>10</strong> V<br />

Connection type 6-pin socket, DIN 45322<br />

Usable with HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />

For the collecting of Analogue signals such as stirrer rotation speed, torque, pressure, fill level,<br />

temperature output of a thermostat,<br />

pH-value on IL-PHAMP1 (external), etc.<br />

Product Description Interface panel with 8 current or voltage inputs of 0/4..20 mA, or <strong>10</strong> V..+ <strong>10</strong> V, 24<br />

V sensor feeding through free contacts or in the 4 ... 20 mA low potential circuit<br />

(additional power unit necessary, for example HS-NGS241A, other voltages<br />

available upon request)<br />

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Laboratory Automation Hardware<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-AEP8A Interface panel with 8 current and voltage inputs, sensor power supply 24 V<br />

LZ-AKTUB Caps for tuchel Sockets<br />

Suitable connecting cables for laboratory devices and sensors:<br />

Order Code Description<br />

ZK-LAB-HI01-IA-UP-O-01 Analogue input cable with open ends for voltage<br />

ZK-LAB-HI01-IA-UA-O-01 Analogue input cable with open ends for voltage with feeding<br />

ZK-LAB-HI01-IA-IP-O-01 Analogue input cable with open ends for 0/4..20 mA twin conductor<br />

ZK-LAB-HI01-IA-IA-O-01 Analogue input cable with open ends for 0/4..20 mA twin conductor with feeding<br />

ZK-LAB-HI01-IA-IA-O-02 Analogue input cable with open ends for 0/4..20 mA four conductor with feeding<br />

For other cables, see "Cables for Instrumentation“.<br />

8 Pt<strong>10</strong>0 Temperature Sensor Inputs (LP-PTP8)<br />

Up to 8 Pt<strong>10</strong>0 or other<br />

resistance feelers can be<br />

connected directly to this panel.<br />

� 8 inputs for Pt<strong>10</strong>0 and<br />

resistance feelers (4-pin<br />

LEMO socket model S1)<br />

� Combination with other<br />

analogue input panels<br />

possible<br />

The wire length does not have any influence on the<br />

measuring accuracy in the quadruple wire<br />

technique. The resolution is better than 0.01 °C<br />

The measured value delivered by the resistance<br />

feeler is linearised and converted to °C. The<br />

resolution depends on the interface cards used. The<br />

signals of the measuring sensor can be calibrated<br />

via the software.<br />

Technical Data<br />

Connection example for a PT <strong>10</strong>0 connection panel<br />

Signal Pt<strong>10</strong>0 signal twin, triple and quadruple wiring connection<br />

Connection type 4-pin socket, model LEMO S1<br />

Usable with HK-AD20NMUX8, HK-AD20NMUX16, HK-HMUX<br />

For the evaluation of Temperatures through Pt<strong>10</strong>0 sensors<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-PTP8 NAMUR compliant interface panel for Pt<strong>10</strong>0 with twin to quadruple wire technology<br />

LZ-AKLES1 Caps for LEMO S1<br />

You can find customise temperature sensors ready for connection in "Process Analytics/Sensors"<br />

Automatic<br />

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Calorimetry<br />

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90<br />

Laboratory Automation Hardware<br />

8 High Precision Pt<strong>10</strong>0 Inputs (LP-PTPRP8)<br />

This panel is designed<br />

especially for AD24PX8<br />

precision measurement cards.<br />

For further information, see<br />

under precision temperature<br />

measurement module and HK-<br />

AD24PX8.<br />

Connection example for a PT <strong>10</strong>0-P connection panel<br />

Order Code Description<br />

LP-PTPRP8 Interface panel for Pt<strong>10</strong>0 on HK-AD24PX8 with two and four wire system<br />

LZ-AKLES1 Caps for LEMO S1<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Suited Precision Temperature Sensors<br />

Order Code Description<br />

IS-T-PT<strong>10</strong>015G Pt<strong>10</strong>0 Temperature Sensor, Measurement Uncertainty ±(0,15 °C + 0,002·|ϑ |) absolute<br />

IS-T-PT<strong>10</strong>003B Pt<strong>10</strong>0 Temperature sensor, Measurement Uncertainty: ±(0,03 °C + 0,0005·|ϑ |) absolute<br />

IS-T-PTKAL Calibration Certificate for Pt<strong>10</strong>0<br />

You can find customised temperature sensors ready for connection in "Process Analytics/Sensors"<br />

Delivery Scope PT<strong>10</strong>0 temperature sensor<br />

cable and connector (for LP-PTPRP8)<br />

calibration certificate upon request<br />

Further sensors can be found in the chapter "Process analytics and Sensors"<br />

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Laboratory Automation Hardware<br />

4 Analogue Inputs and 4 Pt<strong>10</strong>0 Inputs (LP-AE4PT4P(A))<br />

Technical Data<br />

This panel respectively<br />

combines four channels of the<br />

panels LP-AEP8(A) and LP-<br />

PTP8.<br />

For connection information, see<br />

LP-AEP8 and LP-PTP8.<br />

For connection diagram, see<br />

LP-AEP8(A) and LP-PTP8.<br />

Signal 0/4 ... 20 mA, -<strong>10</strong> ... +<strong>10</strong> V and Pt<strong>10</strong>0 resistance feeler<br />

Connection type see LP-AEP8(A) and LP-PTP8<br />

Usable with HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />

For the evaluation of Temperatures through Pt<strong>10</strong>0 sensors,<br />

Analogue signals such as mixer rotation speed & torque,<br />

fill level, temperature output of a thermostat, pH value / RedOx on IL-PHAMP1<br />

(external) etc.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-AE4PT4P Interface panel with 4 Pt<strong>10</strong>0 and 4 voltage/current inputs<br />

LP-AE4PT4PA Interface panel with 4 Pt<strong>10</strong>0 and 4 voltage/current inputs<br />

with 24 V = sensor power supply on free contacts<br />

For further information see LP-AEP8(A) and LP-PTP8.<br />

8 Thermocouple Inputs (LP-THP8)<br />

This panel is suitable for the<br />

connection of up to 8<br />

thermocouples through a 2-pin<br />

LEMO plug model 1S. The cold<br />

junction compensation occurs<br />

electronically (turn-off enabled).<br />

� 8 inputs for thermocouples<br />

(2-pin LEMO socket)<br />

� Electronic cold junction<br />

compensation<br />

� Combination with other<br />

analogue input panels<br />

possible<br />

The measured value is linearised during the<br />

measurement and converted to °C. The integrated<br />

cold junction compensator corrects influences of the<br />

ambient temperature. The resolution is better than<br />

0,1 °C.<br />

Technical Data<br />

Signal For direct connection of thermocouples<br />

Connection type 2-pin socket, model LEMO S1<br />

Usable with HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />

For the evaluation of Temperatures through thermocouples<br />

Connection example for the thermocouple interface<br />

Automatic<br />

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Laboratory Automation Hardware<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-THP8 Interface panel for thermocouples<br />

LZ-AKLES1 Caps for LEMO S1<br />

You can find customised temperature sensors ready for connection in "Process Analytics/Sensors"<br />

2 pH/RedOx and 4 RS232 Interfaces (LP-PHRED24)<br />

The pH/RedOx interface panel allows the direct<br />

connection of pH/RedOx electrodes. The panels can<br />

be optionally equipped with 9-pin RS232 interfaces.<br />

The compensation of the temperature of the pH<br />

value can be done on the LabManager. The<br />

delivered demo programs perform interactively the<br />

calibration (HiText or HiText-light software modules<br />

are necessary for that).<br />

The panel can be supplied with one or two<br />

pH/RedOx booster modules (HK-PHAMP) and up to<br />

four 9-pin RS232 interfaces (HD-RS2329L).<br />

� up to 2 connections for pH or RedOx<br />

electrodes<br />

� up to 4 serial RS232 interfaces<br />

Note: Only for the mounting on LZ-USTAT! The<br />

external IL-PHAMP1 should be used for standard<br />

devices (see laboratory devices, external pH<br />

booster).<br />

Connection example for the pH//RedOx interface panel.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-PHRED24 Interface panel for pH/RedOx and RS232 interfaces<br />

LP-PHRED24B Interface panel for pH/RedOx with battery monitoring and RS232 interface<br />

LZ-AKPH Caps for pH sockets<br />

Can be supplied with the following modules:<br />

Order Code Description<br />

HK-PHAMP Amplifier for pH and RedOx electrodes<br />

HD-RS2329 9-pin RS232 interface<br />

Technical Data PHAMP<br />

Signal mV (is buffered with the HK-PHAMP booster),<br />

RS232 signal, 24 V<br />

Connection type > <strong>10</strong>0 MΩ<br />

Usable with -1<strong>10</strong>0....1<strong>10</strong>0 mV<br />

For the evaluation of Hf-socket, D-SUB-9<br />

Signal HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16<br />

Connection type pH value (direct electrode connection),<br />

RedOx potential (direct electrode connection),<br />

opt. battery voltage.<br />

Power supply build in lithium cell battery<br />

You can find suitable cables for devices with serial interface in the chapter “Cables for Instrumentation”.<br />

In the chapter Measurment Amplifiers IL-PHAMP1, you can find an external measuring amplifier for<br />

connection to analogue inputs as an alternative to the internal amplifiers.<br />

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Laboratory Automation Hardware<br />

4 DMS Bridge Inputs, 4 Digital Outputs (LP-DMS4DA4PT)<br />

Technical Data<br />

This panel is suitable for the<br />

connection of up to four<br />

GraviDos dosing apparatus<br />

systems or DMS full bridges<br />

and/or load cells, torque sensors<br />

etc. based on DMS. The panel is<br />

designed to work with precision<br />

DMS modules HK-AD24DMS4.<br />

Connection example for GraviDos systems and magnetic valves.<br />

Signal direct connection of DMS bridges and dosing valves (max. 500mA per channel)<br />

Connection type 6 pin socket, Type LEMO S1; 3 pin connector, DIN 41524<br />

Usable with HK-AD24DMS4<br />

For the evaluation of weight, force, flow, torque...<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DMS4DA4PT Interface panel for 4 DMS full bridges and 4 activated digital outputs (500 mA)<br />

LZ-AKLES1 Caps for LEMO S1<br />

LZ-AKTUB Caps for tuchel sockets<br />

For suitable weighing systems, see "Sensors“, "Load cells“ and "GraviDos“.<br />

8 DMS Bridge Inputs (LP-DMS8)<br />

This panel is suitable for the<br />

connection of up to eight<br />

GraviDos dosing systems or DMS<br />

full bridges and/or load cells,<br />

torque sensors etc. based on<br />

DMS. The panel is designed to<br />

work with precision DMS modules<br />

HK-AD24DMS4.<br />

Technical Data<br />

Connection example for GraviDos systems and load cells<br />

Signal For direct connection of DMS bridges<br />

Connection type 6-pin socket, Type LEMO S1<br />

Usable with 1x or 2 x HK-AD24DMS4<br />

For the evaluation of weight, force, flow, torque...<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DMS8 Interface panel for 8 DMS full bridges<br />

LZ-AKLES1 Caps for LEMO S1<br />

For suitable weighing systems, see "Sensors“, "Load cells“ and "GraviDos“.<br />

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94<br />

Laboratory Automation Hardware<br />

Interface Panels for analogue Output<br />

A panel for the current and voltage output and a<br />

combined input/output panel are available on choice<br />

for analogue output.<br />

8 Voltage and Current Outputs (LP-AAP8UI)<br />

This panel is used for<br />

connecting laboratory devices<br />

with analogue voltage or<br />

current inputs for control and<br />

regulation purposes.<br />

The LP-AAP8UI panel uses<br />

eight NAMUR compliant 6-pin<br />

tuchel sockets for the output of<br />

analogue signals.<br />

� 8 analogue outputs<br />

� Voltage of -<strong>10</strong>...+<strong>10</strong> V and current of 0/4 ... 20<br />

mA (6-pin tuchel socket) working resistance<br />

of maximum 500 Ω<br />

An example out of many possible applications is<br />

driving a stirrer. It is supposed to run at 0 rpm with 0<br />

V and at 2000 rpm with <strong>10</strong> V. The rotation speed can<br />

be directly determined by suitable scaling of the data<br />

point.<br />

This means that the stirrer rotates at 300 rpm, if the<br />

a value of 300 is allocated to the data point. For this<br />

purpose, the parameters in LabVision will be set to<br />

the following values:<br />

Minimum process value 0<br />

Maximum process value 2000<br />

Minimum interface value 0<br />

Maximum interface value <strong>10</strong><br />

Technical Data<br />

Connection example for stirrers and pumps<br />

The value of the output data point can be set by the<br />

user through a control module (SL-HiText), an<br />

automatic controller (SF-PIDxx) or by direct value<br />

assignment.<br />

Signal 0/4 ... 20 mA, -<strong>10</strong> ... +<strong>10</strong> V<br />

Connection type 6-pin socket, DIN 45322<br />

Usable with HK-DA812UI<br />

For the evaluation of Analogue actuators, for example control valves, dosing pumps, temperature<br />

theoretical value of a thermostat, stirrer rotation speed, external automatic<br />

controllers, for example mass flow rate or pressure etc.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-AAP8UI Panel for analogue output, current and voltage<br />

LZ-AKTUB Caps for LEMO S1<br />

For suitable connecting cables for laboratory devices and final control elements, see “Cables for<br />

instrumentation”.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

8 Combined analogue Inputs/Outputs (LP-AEAP8xx)<br />

Technical Data<br />

This panel has combined<br />

connections for analogue input/<br />

output. It is particularly suitable<br />

for the connection of devices<br />

which are driven by an<br />

analogue theoretical value and<br />

supply on analogue actual<br />

value.<br />

Connetion example for a mass flow controller<br />

Signal 0/4 ... 20 mA, -<strong>10</strong> ... +<strong>10</strong> V<br />

Connection type 6-pin socket, DIN 45322<br />

Usable with HK-DA812UI and on choice with HK-AD20NMUX8, HK-AD20NMUX16, HK-<br />

HMUX<br />

For the evaluation of Measure flow controllers, heat/cool thermostats, measuring stirrers<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-AEAP8I Multi-purpose panel with 8 0/4 ... 20 mA current inputs, 8 0/4 ... 20 mA current outputs<br />

LP-AEAP8IA Multi-purpose panel with 8 0/4 ... 20 mA current inputs, 8 0/4 ... 20 mA current outputs, 24 V<br />

sensor power supply<br />

LP-AEAP8U Multi-purpose LabManager panel with 8 ±<strong>10</strong> V voltage inputs, 8 ±<strong>10</strong> V voltage outputs<br />

LP-AEAP8UA Multi-purpose LabManager panel with 8 ±<strong>10</strong> V voltage inputs, 8 ±<strong>10</strong> V voltage outputs, 24 V<br />

sensor power supply<br />

LZ-AKTUB Caps for tuchel sockets<br />

For suitable connecting cables for laboratory devices and final control elements, see "Cables for<br />

instrumentation“.<br />

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96<br />

Interface panels for digital input<br />

Laboratory Automation Hardware<br />

Beyond the pure recording of binary states (in/out),<br />

digital inputs of <strong>HiTec</strong> <strong>Zang</strong> PIs can be used for<br />

frequency measurement.<br />

8 digital inputs (LP-DEP8)<br />

The panel for digital input is<br />

suitable for the connection of<br />

switches, limiting value<br />

transmitters and other digital<br />

transmitters with NAMUR<br />

compliant turn-off levels. For a<br />

maximally simple external<br />

wiring the inputs are placed<br />

over intern pull-up resistors and<br />

pulled up to 24 V.<br />

� 8 digital inputs, active (Pull-up against 24 V),<br />

opto-electronically isolated.<br />

� for limit switches and digital status signals<br />

� 3-pin tuchel socket 180 °<br />

� one or two LP-DEP8 connectable to a HK-<br />

DEA16N card<br />

� Inputs with NAMUR compliant turn-off levels<br />

Technical Data<br />

� With optional sensor power supply (WP-DEP8A)<br />

� Also suitable for frequency measurement<br />

Connection example for fill limit switches<br />

Signal NAMUR NE28 compliant input level and pin assignment<br />

Connection type 3-pin socket, DIN 41524<br />

Usable with HK-DEA16N<br />

For the evaluation of Switch contacts, fill level switches, press switches, digital status signals of devices<br />

etc.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DEP8 Digital input interface panel with active 24 V inputs<br />

LZ-AKTUB Caps for tuchel sockets<br />

For suitable connecting cables for sensors and monitors, see “Cables for instrumentation”.<br />

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Laboratory Automation Hardware<br />

8 Digital Inputs with Sensor Power Supply (LP-DEP8A)<br />

This panel has no pull-up<br />

resistor like the LP-DEP8,<br />

however it delivers extra 24 V<br />

on every socket (-pin3) for the<br />

supply of on available<br />

connected sensor. Optional a<br />

pull-up resistor can be<br />

provided in the connector or<br />

in the sensor.<br />

� for limiting value modulators with<br />

electronics and digital status signals<br />

� one or two LP-DEP8A suitable for<br />

connection to a HK-DEA16N/F card<br />

� Inputs with NAMUR compliant turn-off levels<br />

Technical Data<br />

Connection example for proximity and fill level sensors<br />

Signal NAMUR NE28 compliant input level and pin assignment<br />

Connection type 3-pin socket 180 °, DIN 41524<br />

Usable with HK-DEA16N<br />

For the evaluation of Proximity sensors, switch contacts, fill level switches, push switches, digital status<br />

signals of devices etc., Sensor feeding on pin 3<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DEP8A Digital input interface panel with active 24 V supply and sensor power supply<br />

LZ-AKTUB Caps for tuchel sockets<br />

For suitable connecting cables for sensors and monitors, see “Cables for instrumentation”.<br />

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98<br />

Interface Panels for Digital Output<br />

Laboratory Automation Hardware<br />

Not only binary switching actions (in/out, on/off) but<br />

also pulse width and pulse frequency modulated<br />

output are included in the digital output. The<br />

switching voltage is 24 V.<br />

8 passive digital outputs (LP-DAP8)<br />

This panel offers for every<br />

connection a relay switching<br />

contact which can be freely<br />

connected by the customer.<br />

� 8 digital outputs, relay contacts, a<br />

changeover switch per output, a maximum of<br />

1 A, 30 V on a 3-pin tuchel plug<br />

� Control LED for every channel<br />

� For the connection of magnetic valves,<br />

drives, heating, dosing pumps, etc...<br />

� up to two LP-DAP8 connectable to a HK-<br />

DEA16N card<br />

Technical Data<br />

For digital output, the following types of connection<br />

are available<br />

� passive changeover switch (LP-DAP8)<br />

� Active 24V changeover switch for the direct<br />

connection of valves, smaller motors...(LP-<br />

DAP8A)<br />

� Active 24V transistor outputs for proportional<br />

magnetic valves...(LP-DAP8T)<br />

Signal Contacts of a passive one pin change-over switch<br />

Connection type 3-pin plug, DIN 41524<br />

Usable with HK-DEA16N<br />

For connecting Valves, reflux divisors, motors, digital control inputs on devices etc.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DAP8 Digital output interface panel, passive change-over contacts<br />

LZ-AKTUS Caps for tuchel plugs, passive change-over contacts<br />

For suitable connecting cables for valves, actuators etc. see "Cable for Instrumentation“.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


8 active digital outputs (LP-DAP8A)<br />

Laboratory Automation Hardware<br />

This panel offers at each<br />

connection a normally open and<br />

normally closed contact with an<br />

active switch voltage of 24 V for<br />

direct activation of actuators. For<br />

power supply, depending on the<br />

power required, a HS-NGS241A<br />

to HS-NGS248 can be installed.<br />

Up to two LP-DAP8A can be<br />

connected to a HK-DEA16N or<br />

HK-DEA16n card.<br />

� 8 active digital outputs, changeover switch,<br />

24 V, a maximum of 1 A, on a 3 pin tuchel<br />

plug, max 3 A<br />

� Short-circuit proof<br />

� Control LED for every channel<br />

� For the direct connection of magnetic valves,<br />

drives, heating, dosing pumps, etc..<br />

Technical Data<br />

Connection example for magnetic valves<br />

Signal Active change-over switch (normally open contact +24 V, normally closed contact<br />

+24 V), capable of bearing 1 A<br />

Connection type 3 pin plugs, DIN41524<br />

Usable with HK-DEA16N, HS-NGS241A to HS-NGS248<br />

For connecting 24 V consumers as magnetic valves, engine valves, reflux divisors, motors, digital<br />

control inputs on devices etc.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DAP8A Digital output interface panel, active outputs<br />

LZ-AKTUS Caps for tuchel plugs<br />

For suitable connecting cables for valves, actuators etc., see "Cable for Instrumentation“.<br />

8 Active Outputs for high Switching Frequencies (LP-DAP8T)<br />

This panel allows the direct<br />

connection of proportional<br />

magnetic valves. Because of the<br />

high switching frequency of up to<br />

1 kHz, MOSFET switches are<br />

integrated. For power supply,<br />

depending on the required<br />

power, a HS-NGS241A to HS-<br />

NGS248 can be installed.<br />

� 8 active controlled current outputs<br />

� for the direct connection of proportional<br />

magnetic valves<br />

� LED control display<br />

� up to two LP-DAP8T connectible to a HK-<br />

DEA16N card<br />

� combinable with other LP-DAPxx panels<br />

� Short-circuit proof<br />

Connection example of a proportional magnetic valve<br />

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<strong>10</strong>0<br />

Technical Data<br />

Laboratory Automation Hardware<br />

Signal active digital output 0 ...<strong>10</strong>00 Hz, 500 mA, max. 3A total<br />

Connection type 3 pin plugs, DIN41524<br />

Usable with HK-DEA16N, HS-NGS241A to HS-NGS248<br />

For connecting Proportional magnetic valves etc.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DAP8T Digital output interface panel, active outputs<br />

LZ-AKTUS Caps for tuchel plugs<br />

For suitable connecting cables for valves, actuators etc., see "Cable for Instrumentation“.<br />

4 Digital Inputs and 4 Digital Outputs (LP-DE4DA4P)<br />

This panel combines four<br />

channels of the LP-DEP8 and<br />

LP-DAP8 panels. See in the<br />

according section for detailed<br />

information.<br />

Technical Data<br />

Connection example for fill level switches<br />

Signal NAMUR compliant input level, passive one pin change-over contact<br />

Connection type see LP-DEP8, LP-DAP8<br />

Usable with HK-DEA16N<br />

For connecting Switch contacts, fill level switches, push switches, valves, reflux divisors,<br />

motors, digital control inputs on devices etc.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DE4DA4P Multi-purpose panel with 4 digital inputs and 4 digital outputs<br />

LZ-AKTUB Caps for tuchel sockets<br />

LZ-AKTUS Caps for tuchel plugs<br />

For suitable connecting cables for valves, actuators etc., see "Cable for Instrumentation“.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

4 Digital Inputs and 4 Digital Outputs and Feeding (LP-DE4DA4PA)<br />

This panel respectively combines<br />

four channels of the LP-DEP8<br />

and LP-DAP8A panels. See in the<br />

according section for detailed<br />

information.<br />

Technical Data<br />

Connection example for magnetic valves and fill level switches.<br />

Signal NAMUR compliant input level, active change-over contact (normally open contact<br />

+24 V, normally close contact +24 V), capable of bearing 1 A<br />

Connection type See LP-DEP8, LP-DAP8A<br />

Usable with HK-DEA16N, HS-NGS241A to HS-NGS245<br />

For connecting Switch contacts, fill level switches, push switches, valves, reflux divisors, motors,<br />

digital control inputs on devices etc.<br />

Delivery Scope Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-DE4DA4PA Combination panel 4 digital inputs DEP8, 4 active digital outputs DAP8A<br />

LZ-AKTUB Caps for tuchel sockets<br />

LZ-AKTUS Caps for tuchel plugs<br />

For suitable connecting cables for valves, actuators etc. see "Cable for Instrumentation“.<br />

4 Digital Outputs, 4 Heating Elements and Feeding (LP-DA4HZ4PA)<br />

This panel combines four<br />

channels for low-voltage<br />

heatings with four channels of<br />

the panel.<br />

For details, see LP-DAP8(A).<br />

Technical Data<br />

Signal 44 V AC, max. 2,5 A per output, active change-over contact (normally open<br />

contact +24 V, normally close contact +24 V), capable of bearing 1 A<br />

Applicable with HK-DEA16N, HS-NGS44AC<br />

For the Connection of Switch Contacts, Liquid Level Switch , Pressure switches, Low Voltage Heatings<br />

Scope of Delivery Panel with fastening Screws, Cable for internal cabling<br />

Order Code Description<br />

LP-LP-DA4HZ4PA Combination Panel 4 digital Outputs 24 V 1 A, 4 Low Voltage Heatings<br />

LZ-AKTUB Covers for Tuchel-socket<br />

For suited connection cables for valves, actuators etc., see chapter "Cables for Instrumenting“.<br />

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<strong>10</strong>2<br />

Serial Interfaces<br />

Laboratory Automation Hardware<br />

Serial interfaces can be provided on the PI and on<br />

the UI, (see also PC cards). Simpler laboratory<br />

devices as dosing pumps and balance will usually<br />

be connected directly to the PI so that they can<br />

simply be included in control loops. Laboratory<br />

devices with complex functionality such as analysers<br />

or titrating apparatuses are rather connected directly<br />

to the UI (see PC plug-in cards).<br />

Panel for 9x RS232 (LP-SER99)<br />

The ninefold RS232 panel can<br />

carry up to nine 9 pin serial<br />

interface modules. It can be<br />

used on the LAB and PMC PI<br />

devices.<br />

Additionally, HD-RS2329L, HD-<br />

RS2329PL or HD-RS485P<br />

interface modules are required<br />

on the panel depending on the<br />

number of interfaces. For<br />

increased performance, an<br />

additional HK-SER8ECB or HK-<br />

SER16ECB card is<br />

recommended.<br />

Order Code Description<br />

LP-SER99 Panel for 9 serial HD-RS2329 interface modules<br />

LZ-AKRS9 Caps<br />

For suitable connecting cables, see "Cables for Instrumentation".<br />

In the PI two different techniques are used: A serial<br />

interface, which is multiplexed to eight channels, is<br />

implemented on the CPU. Due to this, the connected<br />

devices can only communicate one after another<br />

and slow devices slow down the whole<br />

communication.<br />

The eightfold RS232 HK-SER8ECB module is<br />

suitable for universal use and achieves higher<br />

performance. Every channel has a 64 byte FIFO<br />

storage, so that the connected devices can<br />

communicate parallel.<br />

For communication, there are different technologies.<br />

You can find further information in the chapter<br />

"Driver Programs for Laboratory Device Interfaces“.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

RS232 Interface Module (HD-RS2329(P)L)<br />

The serial interface modules are optionally available<br />

with or without separation of the potential.<br />

HD-RS2329L<br />

Technical Data<br />

Potential separation improves the interference<br />

resistance.<br />

HD-RS2329PL<br />

Signal RS232, V24<br />

Connection type 9 pin plugs, D-SUB<br />

Usable with Basis panel, LP-SER99<br />

For connecting Balances, analysers, control systems, devices with RS232 interface<br />

Product Description RS232 interface module to mount on the LabManager or LabBox<br />

Delivery Scope Interface module with cable for internal connection<br />

Order Code Description<br />

HD-RS2329L RS232 interface module with power supply for LabCom<br />

HD-RS2329PL RS232 9 pin interface module with potential separation and power supply for LabCom (max. 4<br />

units in one LabBox)<br />

RS485 Interface Module (HD-RS485P)<br />

HD-RS485P<br />

Technical Data<br />

Signal RS485<br />

Connection type 9-pin plugs, D-SUB<br />

Usable with Basis panel, LP-SER99<br />

For connecting Analysers, control systems, devices with RS485 interfaces<br />

Product description RS485 interface module with potential separation to mount on the<br />

LabManager or LabBox, Cable, standard driver for HK-CPU32, HK-SER16ECB or<br />

HK-SER8ECB<br />

Delivery Scope Interface module with cable for internal connection<br />

Order Code Description<br />

HD-RS485P RS485 9-pin Interface Module with Potential Separation<br />

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<strong>10</strong>4<br />

Laboratory Automation Hardware<br />

16 Channel Serial Interface Card (HK-SER16ECB)<br />

The HK-SER16ECB card has sixteen independent<br />

SIO channels with FIFO storing and supports<br />

RTS/CTS hardware handshake.<br />

Order Code Description<br />

HK-SER16ECB 16 channel serial interface card for the PI<br />

HK-SER8ECB 8 channel serial interface card for the PI<br />

Panel for Instrumentation Power Supply (LP-PEAP)<br />

If the power supply for the activation of inputs and<br />

outputs is not integrated in the device, the external<br />

power supply is possible via the LP-PEAP panel.<br />

If required, external components can be energised<br />

via the panel if a HS-NGSxxxx is integrated.<br />

For every channel, an additional serial interface<br />

module, like HD-RS2329PL, is required.<br />

The card can also be delivered with 8 channels (HK-<br />

SER8ECB).<br />

LP-PEAP Panel for supplying external power to feed sensors/actuators through<br />

inputs/outputs or feeding external components through on integrated power<br />

supply.<br />

LP-PEAPSK15 Plug and cable loom of cables for ± 15 V supply<br />

LPPEAPSK24 Plug and cable loom of cables, safeguard for +24 V supply<br />

Order Code Description<br />

LP-PEAP Panel for connection of external power supply<br />

LP-PEAPSK15 ±15 V= supply for LP-PEAP, including plug and cable<br />

LP-PEAPSK24 +24 V= supply for LP-PEAP, including plug and cable<br />

☞<br />

For LP-PEAPSK15 and LP-PEAPSK24, a suitable power<br />

supply HS-NGSxxxx is necessary!<br />

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Measuring Amplifiers<br />

Laboratory Automation Hardware<br />

External Measuring Amplifier for pH/Redox<br />

The external buffer amplifier for pH and Redox<br />

electrode is integrated in a plug.<br />

The electrodes can be directly connected without pH<br />

measuring device. The cable with integrated<br />

amplifier is connected to a common analogue input.<br />

Temperature compensation and calibration are<br />

realised in a special device component in the PI.<br />

As the sensitive electrode signal is buffered directly<br />

in the plug, the cable can be extended without<br />

increasing the sensitivity.<br />

The voltage of the integrated Lithium cell can be<br />

tested at the plug.<br />

Advantages:<br />

� Space-Saving<br />

� Cable can be extended<br />

Product Description Buffer Amplifier for pH/Redox integrated in cable plug type HFS 13/4, input<br />

voltage -1<strong>10</strong>0....1<strong>10</strong>0 mV, input resistance > <strong>10</strong>0 MΩ, integrated lithium cell<br />

Delivery Scope Cable with integrated amplifier<br />

Manual with example for temperature compensation and calibration<br />

Order Code Description<br />

IL-PHAMP1 Cable with integrated amplifier pH/Redox electrodes<br />

Digital Measuring Amplifier for pH/Redox<br />

The external digital buffer amplifier for pH- and<br />

Redox electrodes does not require an own power<br />

supply when connected to a LAB-PNC.<br />

The electrodes can be directly connected without<br />

ph-measuring device.<br />

The temperature compensation is integrated. The<br />

calibration is conducted with a special module in the<br />

PNC.<br />

The sensitive electrode signal is directly digitalised<br />

and can be transmitted over long distances without<br />

any errors to the PNC.<br />

The voltage of the integrated Lithium battery can be<br />

read off via the serial interface.<br />

The amplifier can be connected to any RS232 V24<br />

interface.<br />

Advantages:<br />

� Integrated Temperature Compensation<br />

� Space-Saving Design<br />

� Extendable Cable<br />

Product Description Digital Buffer Amplifier for pH/RedOx with temperature compensation, input<br />

voltage-1<strong>10</strong>0....1<strong>10</strong>0mV, input resistance > <strong>10</strong>0 MΩ, integrated Lithium battery<br />

Delivery Scope Measuring Amplifier, Cable, Manual<br />

Order Code Description<br />

IL-PHAMP1D Digital Amplifier for pH- and Redox-Electrodes, RS232 V24 interface, incl. cable<br />

IL-PHAMP1D-SN Plug-In Power Supply for digital amplifier for pH- and Redox electrodes<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com <strong>10</strong>5<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


<strong>10</strong>6<br />

Laboratory Automation Hardware<br />

Measuring Amplifier for Load Cells and GraviDos<br />

The external is integrated into a plug housing.<br />

Load measuring cells or GraviDos weighing cells<br />

can be directly connected. The cable with the<br />

integrated amplifier is connected to a standard<br />

analogue input.<br />

The power supply of the amplifier is conducted via<br />

the interface and no additional power supply is<br />

required.<br />

In case a higher measuring precision is required, the<br />

digital measuring amplifier IL-GRADOMV1D, or the<br />

internal quadruple measuring system LP-<br />

DMS4DA4PT should be given preference.<br />

Advantages:<br />

� Space-Saving Design<br />

� Extendable Cable<br />

Product Description DMS Amplifier for DMS Full and Half-Bridge, Output Signal 4..20mA<br />

Delivery Scope Cable with integrated Amplifier<br />

Manual with Calibration Example<br />

Order Code Description<br />

IL-GRADOMV1 Cable with integrated Measuring Amplifier for DMS Load Cells<br />

You will find suited load cells in the according chapters Load Cells and under GraviDos.<br />

Digital Measuring Amplifier for Load Cells and GraviDos<br />

The digital measuring amplifier is suited for all <strong>HiTec</strong><br />

<strong>Zang</strong> load cells ( with the exception of the types with<br />

integrated measuring amplifier) as well as all other<br />

voltage-supplied DMS cells.<br />

� Integrated Calibration Function<br />

� Integrated Taring Function<br />

Technical Data:<br />

Input LEMO Jack Type S1<br />

Interface RS232 V24, Sub-D 9 pole, Power<br />

Supply on Pin 9<br />

If operated on an interface without<br />

power supply, a plug-in power<br />

Connection<br />

Measuring<br />

Bridge<br />

Bridge Supply<br />

Voltage<br />

supply is required.<br />

6 pole LEMO-Plug, Type<br />

FFA.1S.306.CLACxx<br />

5V<br />

Power Supply Via DataPlug, Sub-D 9, 5 V, 50 mA<br />

Dimensions L approx. 142 mm, W approx. 52<br />

mm, H approx. 23 mm, with Plug<br />

Product Description Digital DMS Amplifier for DMS Full and Half-Bridge, RS232 V24 Interface<br />

Delivery Scope Amplifier, RS232 Cable, Manual<br />

Order Code Description<br />

IL-GRADOAMP1D Digital Measuring Amplifier for DMS Load Cells, RS232 V24 Interface, incl. Cable<br />

IL-GRADOAMP1D-SN Plug-In Power Supply for digital amplifier for DMS load cells<br />

You will find suited load cells in the according chapters Load Cells and under GraviDos.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Cables for Instrumentation<br />

Laboratory Automation Hardware<br />

The following table presents ready to connect<br />

manufactured cables for various standard laboratory<br />

devices and instrumentation components. The offer<br />

is expanded continuously.<br />

If your device is not listed here, we can produce<br />

cables according to your specifications.<br />

Manufacturer, Device, Model,<br />

Interface<br />

kind<br />

Signal, Interface Panel / Module Cable Order Code<br />

LabManager and LabBox Cables<br />

Analogue Input, free cable ends<br />

voltage analogue LP-AEP8(A), LP-AEAP8U(A) ZK-LAB-HI01-IA-UP-O-01<br />

voltage, with 24 V sensor feed analogue LP-AEP8A, LP-AEAP8UA ZK-LAB-HI01-IA-UA-O-01<br />

0/4..20 mA twin wire analogue LP-AEP8(A) ZK-LAB-HI01-IA-IP-O-01<br />

0/4..20 mA twin wire with feed analogue LP-AEP8A ZK-LAB-HI01-IA-IA-O-01<br />

0/4..20 mA quadruple wire, opt. 24 V sensor feed<br />

Analogue Output, free cable ends<br />

analogue LP-AEP8A ZK-LAB-HI01-IA-IA-O-02<br />

Voltage analogue LP-AAP8UI ZK-LAB-HI01-OA-UP-O-01<br />

0/4..20 mA<br />

Digital Input, free cable ends<br />

analogue LP-AAP8UI ZK-LAB-HI01-OA-IP-O-01<br />

For switches, controllers<br />

Digital Output, free cable ends<br />

digital PDEP8 ZK-LAB-HI01-ID-XX-O-01<br />

For valves etc., 3 weirs: normally open and<br />

normally closed contact<br />

Pressure Transmitter<br />

digital LP-DAP8(A) ZK-LAB-HI01-OD-XX-O-01<br />

Pressure transmitter Kellar model series 21 analogue 4-20 mA current, twin wire on LP-AEP8A ZK-SP-KL21-IA-IA-I-01<br />

Pressure transmitter Kellar model series 23<br />

Heating/cooling Thermostats<br />

analogue 4-20 mA current, twin wire on LP-AEP8A ZK-SP-KL23-IA-IA-I-01<br />

Lauda thermostat model<br />

analogue temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A) ZK-T-LD01-BA-UP-Y-01<br />

C6CS/C12CS/C20CS/K6KS/K12KS/K20KS<br />

temperature set point, 0..<strong>10</strong> V on LP-AAP8UI<br />

Lauda thermostat model<br />

analogue temperature actual value, 0..<strong>10</strong>V on LP-AEP8(A) ZK-T-LD01-BA-KP-Y-01<br />

C6CS/C12CS/C20CS/K6KS/K12KS/K20KS<br />

temperature actual value channel 1 & set point, 4-20<br />

mA on LP-AEAP8I(A)<br />

Lauda thermostat model<br />

serial temperature actual value<br />

ZK-T-LD01-BS-R2-I-02<br />

C6CS/C12CS/C20CS/K6KS/K12KS/K20KS<br />

temperature actual value, set point<br />

Lauda thermostat model USH400 analogue temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A)<br />

temperature set point, 0..<strong>10</strong> V on LP-AAP8UI<br />

ZK-T-LD03-BA-UP-Y-01<br />

Jucheim thermostat model 80-4 / 90-4 analogue temperature actual value, 0..20 mA on LP-AEP8(A)<br />

temperature set point, 0..20 mA on LP-AAP8UI<br />

ZK-T-JH01-BA-IP-Y-01<br />

Julabo thermostat model FM50MH analogue temperature set point, 0..20 mA on LP-AAP8UI<br />

temperature working sensor 0-<strong>10</strong> V on LP-AEP8(A)<br />

Ext. temperature sensor, 0-<strong>10</strong> V on LP-AEP8(A)<br />

set point feedback, 0-<strong>10</strong> V on LP-AEP8(A)<br />

ZK-T-JU01-BA-KP-Y-01<br />

Julabo thermostat model FM50MH analogue temperature set point, 0..20 mA on LP-AAP8UI<br />

temperature working sensor 0-<strong>10</strong> V on LP-AEP8(A)<br />

ext. temperature sensor, 0-<strong>10</strong> V on LP-AEP8(A)<br />

ZK-T-JU01-BA-KP-Y-02<br />

Julabo thermostat model HP / SP / TP analogue temperature set point, 0..20 mA on LP-AAP8UI<br />

ext. temperature sensor, 0-<strong>10</strong> V on LP-AEP8(A)<br />

int. temperature sensor, 0-<strong>10</strong> V on PAEP8<br />

set point feedback, 0-20 mA on LP-AEP8(A)<br />

ZK-T-JU02-BA-KP-Y-01<br />

Julabo thermostat model ATS3 / ATS2 analogue temperature set point, 0..20 mA on LP-AAP8UI<br />

temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A)<br />

2 x 4-pin tuchel on thermostat<br />

ZK-T-JU04-BA-KP-Y01<br />

Julabo thermostat RS232 temperature set point, ext. temperature sensor,<br />

int. temperature sensor, set point feedback<br />

ZK-T-JU00-BS-R2-I-01<br />

Eurotherm thermostat type RD4455 model 99 analogue temperature set point, 0..<strong>10</strong> V on LP-AAP8UI<br />

temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A)<br />

ZK-T-ET99-BA-UP-Y01<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com <strong>10</strong>7<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


<strong>10</strong>8<br />

Laboratory Automation Hardware<br />

Huber thermostat model Tango analogue temperature set point, 0..<strong>10</strong> V on LP-AAP8UI<br />

Bath temperature actual value, 0..<strong>10</strong> V on LP-AEP8(A)<br />

Open cable end<br />

ZK-T-HU04-BA-UP-O-01<br />

Huber thermostat model Tango analogue temperature set point, 4..20 mA on LP-AAP8UI<br />

temperature actual value, 4..20 mA on LP-AEP8(A)<br />

Open cable end<br />

ZK-T-HU04-BA-IP-O-01<br />

Huber thermostat model Tango(unistat<br />

control)<br />

RS232 temperature set point, actual value via RS232 ZK-T-HU01-BS-R2-I-01<br />

Huber thermostat model Tango (unistat<br />

control)<br />

RS485 temperature set point, actual value via RS485 ZK-T-HU01-BS-R4-I-01<br />

Thermostat Huber compatible control RS232 temperature set point, actual value via RS232 ZK-T-HU02-BS-R2-I-01<br />

Thermostat Huber compatible control RS485 temperature set point, actual value via RS485 ZK-T-HU02-BS-R4-I-01<br />

Haake thermostat analogue temperature set point, 4..20 mA on LP-AAP8UI<br />

ZK-T-HA01-BA-IP-Y-01<br />

temperature actual value, 4..20 mA on LP-AEP8(A)<br />

Haake thermostat RS232 temperature set point, temperature actual value ZK-T-HA01-BS-R2-I-01<br />

<strong>HiTec</strong> Laboratory Devices (see also stirrer and solid doser)<br />

Hitec model Kaloheiz, control input analogue voltage, 6 pin tuchel on LP-AAP8UI ZK-KAL-HI04-OA-UP-I-01<br />

Hitec model Kaloheiz, voltage monitor analogue voltage, 6 pin tuchel on LP-AEP8(A) ZK-KAL-HI04-IA-UP-I-01<br />

Hitec model Kaloheiz, current monitor<br />

Lab Balances/Scales<br />

analogue voltage, 6 pin tuchel on LP-AEP8(A) ZK-KAL-HI04-IA-UP-I-02<br />

Kern balance model EW 3000-2M RS232 RS232, 5pol. Hoshiden plug / D-Sub9 socket on<br />

ZK-W-KE01-BS-R2-I-01<br />

RS2329(P)L<br />

Kern balance model GS RS232 RS232, 25pin-plug - 9pin-socket ZK-W-KE02-BS-R2-I-01<br />

Kern balance model PB 4002-2 RS232 RS232, 9pin-plug - 9pin-socket ZK-W-KE03-BS-R2-I-01<br />

Sartorius / Scaltec balance model SBC RS232 RS232, 25pin-plug - 25pin-socket ZK-W-SA01-BS-R2-I-01<br />

Sartorius / Scaltec balance model SBC RS232 RS232, 9pin-plug - 9pin-socket ZK-W-SA01-BS-R2-I-03<br />

Sartorius / Scaltec balance model SBC mixed RS232, D-Sub9 socket on RS2329,<br />

tare on LP-DAP8 (passive panel)<br />

ZK-W-SA01-BK-R2P-Y-02<br />

Sartorius / Scaltec balance model SBC mixed RS232, D-Sub9 socket on RS2329,<br />

ZK-W-SA01-BK-R2A-Y-02<br />

tare on LP-DAP8A (active panel)<br />

Mettler balance model PM/AM 25 pin RS232 25 pin, 15 pin Mettler plug ZK-W-ME01-BS-R2-I-01<br />

Mettler balance model PM/AM 9 pin RS232 9 pin, 15 pin Mettler plug ZK-W-ME01-BS-R2-I-02<br />

Mettler balance model PG<br />

Magnetic Valves<br />

RS232 9 pin, 9 pin ZK-W-ME02-BS-R2-I-01<br />

Magnetic valves (on/off), plug models 2508, digital 24 V, 4 pol. ISO4400 socket / tuchel socket<br />

ZK-VMB-HI41-OD-XA-I-01<br />

DIN 43650 form A<br />

on LP-DAP8A<br />

Magnetic valves (on/off), plug models 2508, digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />

ZK-VMB-HI42-OD-XA-I-01<br />

DIN 43650 form B<br />

LP-DAP8A<br />

Magnetic valves (on/off), plug models 2508, digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />

ZK-VMB-HI43-OD-XA-I-01<br />

DIN 43650 form C<br />

LP-DAP8A<br />

Magnetic valves (proportional), plug models digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />

ZK-VMP-HI41-OD-XA-I-01<br />

2506, DIN 43650 form A<br />

LP-DAP8T, PWM<br />

Magnetic valves (proportional), plug models digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />

ZK-VMP-HI42-OD-XA-I-01<br />

2506, DIN 43650 form B<br />

LP-DAP8T, PWM<br />

Magnetic valves (proportional), plug models digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />

ZK-VMP-HI42-OD-XA-I-01<br />

2506, DIN 43650 form C<br />

Magnetic valves type Buerkert<br />

(proportional)<br />

cable head <strong>10</strong>54/<strong>10</strong>57 (Valve 0127)<br />

LP-DAP8T, PWM<br />

digital 24 V, 4 pol. ISO4400 socket / tuchel socket on<br />

LP-DAP8T, PWM<br />

ZK-VMP-BU04-OD-XA-I-<br />

01<br />

Magnetic valves type Buerkert<br />

(proportional)<br />

cabel head <strong>10</strong>94<br />

analogue 4..20 mA on LP-AAP8UI ZK-VMP-BU03-OA-IA-I-01<br />

Knauer multi-path valve model HPLC7 RS232 ZK-VMO-KN07-BS-R2-I-01<br />

VICI AG Valco-Multi directional control RS232 ZK-VMO-VI01-BS-R2-I-01<br />

valve<br />

Dosing Pumps<br />

<strong>HiTec</strong> <strong>Zang</strong> pump, LabDos mixed set point 4-20 mA on LP-AAP8UI<br />

Start/Stop on LP-DAP8A<br />

ZK-HI36-OK-IP-Y-01<br />

<strong>HiTec</strong> <strong>Zang</strong> pump, LabDos RS232 set point and status information, 9pin/9pin ZK-P-HI36-BS-R2-I-01<br />

ISMATEC pump model ISM736 mixed set point 4-20 mA on LP-AAP8UI<br />

ZK-P-IS01-OK-IP-Y-02<br />

Start/Stop on LP-DAP8A<br />

ISMATEC pump model MC-Z / MS-Z analogue set point 0-5,7/0-<strong>10</strong> V voltage passive LP-AAP8UI ZK-P-IS03-OA-UP-I-01<br />

ISMATEC pump Reglo Digital hose pump RS232 ZK-P-IS04-BS-R2-I-01<br />

Knauer pump RS232 ZK-P-KN00-BS-R2-I-01<br />

Prominent Pump model Gamma analogue stroke amount set point 4..20 mA on LP-AAP8UI ZK-P-PR01-OA-IP-I-01<br />

Telab pump model BF414 RS232 stroke frequency, stroke volume ZK-P-TL02-BS-R2-I-01<br />

Telab pump model BF414, before 2000 analogue stroke frequency set point, 4...20 mA LP-AAP8UI<br />

stroke volume set point, 4...20 mA LP-AAP8UI<br />

9 pin Sub-D plug<br />

ZK-P-TL02-OA-IP-Y-01<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

Telab pump model BF414, after 2000 analogue stroke frequency set point, 4...20 mA on LP-AAP8UI<br />

stroke volume set point, 4...20 mA on LP-AAP8UI<br />

15 pin HD-plug<br />

Telab pump model BF414, before 2000 analogue stroke frequency set point, 0...<strong>10</strong> V on LP-AAP8UI<br />

stroke volume set point, 0...<strong>10</strong> V on LP-AAP8UI<br />

9 pin Sub-D plug<br />

Telab pump model BF414, after 2000 analogue stroke frequency set point, 0...<strong>10</strong> V on LP-AAP8UI<br />

stroke volume set point, 0...<strong>10</strong> V on LP-AAP8UI<br />

15 pin Sub-D plug<br />

Telab pump model BF414, before 2000 analogue stroke frequency set point, 4...20 mA LP-AAP8UI<br />

stroke volume set point, 4...20 mA LP-AAP8UI<br />

release on LP-DAP8<br />

9 pin Sub-D plug<br />

Telab pump model BF414, after 2000 analogue stroke frequency set point, 4...20 mA on LP-AAP8UI<br />

stroke volume set point, 4...20 mA on LP-AAP8UI<br />

release on LP-DAP8<br />

15 pin HD-plug<br />

Telab pump model BF414, before 2000 analogue stroke frequency set point, 0...<strong>10</strong> V on LP-AAP8UI<br />

stroke volume set point, 0...<strong>10</strong> V on LP-AAP8UI<br />

release on LP-DAP8<br />

9 pin Sub-D plug<br />

Telab pump model BF414, after 2000 analogue stroke frequency set point, 0...<strong>10</strong> V on LP-AAP8UI<br />

stroke volume set point, 0...<strong>10</strong> V on LP-AAP8UI<br />

release on LP-DAP8<br />

15 pin Sub-D plug<br />

Telab pump model BF414, before 2000 digital Pulse on LP-DAP8, release on LP-DAP8<br />

9 pin Sub-D plug<br />

Telab pump model BF414, after 2000 digital Pulse on LP-DAP8, release on LP-DAP8<br />

15 pin Sub-D plug<br />

ZK-P-TL02-OA-IP-Y-02<br />

ZK-P-TL02-OA-UP-Y-01<br />

ZK-P-TL02-OA-UP-Y-02<br />

ZK-P-TL02-OK-IP-Y-01<br />

ZK-P-TL02-OK-IP-Y-02<br />

ZK-P-TL02-OK-UP-Y-01<br />

ZK-P-TL02-OK-UP-Y-02<br />

ZK-P-TL02-OD-XP-Y-01<br />

ZK-P-TL02-OD-XP-Y-02<br />

Dosing Apparatus<br />

Metrohm Dosimat 665 RS232 set point, actual value ZK-DL-MO01-BS-R2-I-01<br />

Metrohm Titrino 718 RS232 complete Titrino command tree ZK-DL-MO02-BS-R2-I-01<br />

Solid Dosing Apparatus<br />

Solidos controller Hitec ViscoPact and<br />

ViscoPact.rheo<br />

(from firmware 2.<strong>10</strong>, March 2001)<br />

Solidos controller Hitec ViscoPact and<br />

ViscoPact.rheo<br />

(from firmware 2.<strong>10</strong>, March 2001)<br />

Solidos controller Hitec ViscoPact and<br />

ViscoPact.rheo<br />

analogue rotational speed set point voltage 0..<strong>10</strong> V<br />

on LP-AAP8UI<br />

rotational speed actual value voltage 0..<strong>10</strong> V<br />

on LP-AEP8(A)<br />

rotational speed actual value voltage 0..<strong>10</strong> V<br />

on LP-AEP8(A)<br />

analogue rotational speed set point current 0/4..20 mA<br />

on LP-AAP8UI<br />

rotational speed actual value current 0/4..20 mA on LP-<br />

AEP8(A)<br />

torque actual value current 0/4..20 mA<br />

on LP-AEP8(A)<br />

RS232 rotational speed set point,<br />

rotational speed actual value,<br />

torque actual value, on/off<br />

Stirrer drives<br />

Heidolph stirrer model RZR 2<strong>10</strong>2 analogue torque actual value 4-20 mA on LP-AEP8(A)<br />

rotational speed actual value 4-20 mA<br />

on LP-AEP8(A)<br />

<strong>HiTec</strong> stirrer model ViscoPact and<br />

ViscoPact-rheo<br />

(from firmware 2.<strong>10</strong>, March 2001)<br />

<strong>HiTec</strong> stirrer model ViscoPact and<br />

ViscoPact-rheo<br />

(from firmware 2.<strong>10</strong>, March 2001)<br />

<strong>HiTec</strong> stirrer model ViscoPact and<br />

ViscoPact-rheo<br />

rotational speed set point 4-20 mA on LP-AAP8UI<br />

analogue rotational speed set point voltage 0..<strong>10</strong> V<br />

on LP-AAP8UI<br />

rotational speed actual value voltage 0..<strong>10</strong> V<br />

on LP-AEP8(A)<br />

rotational speed actual value voltage 0..<strong>10</strong> V<br />

on LP-AEP8(A)<br />

analogue rotational speed set point current 0/4..20 mA<br />

on LP-AAP8UI<br />

rotational speed actual value current 0/4..20 mA<br />

on LP-AEP8(A)<br />

torque actual value current 0/4..20 mA on LP-AEP8(A)<br />

RS232 rotational speed set point, actual value,<br />

torque actual value,<br />

on/off<br />

IKA stirrer model Eurostar analogue rotational speed actual value voltage on LP-AEP8(A)<br />

torque actual value voltage on LP-AEP8(A)<br />

ZK-R-HI02-BA-UP-Y-03<br />

ZK-R-HI02-BA-IP-Y-02<br />

ZK-R-HI02-BS-R2-I-01<br />

ZK-R-HD02-BA-IP-Y-01<br />

ZK-R-HI02-BA-UP-Y-03<br />

ZK-R-HI02-BA-IP-Y-02<br />

ZK-R-HI02-BS-R2-I-01<br />

ZK-R-IK01-BA-UP-Y-01<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

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Autosampler<br />

Stirring and<br />

Dispersing<br />

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1<strong>10</strong><br />

Laboratory Automation Hardware<br />

IKA stirrer model Eurostar mixed rotational speed actual value voltage on LP-AEP8(A)<br />

torque actual value voltage on LP-AEP8(A)<br />

set point on RS232, serial measured on HD-plug<br />

ZK-R-IK01-BK-R2-Y-01<br />

IKA stirrer model Eurostar RS232 RS232 serial interface 9-pin DSub ZK-R-IK01-BS-R2-I-01<br />

IKA stirrer model Eurostar<br />

Sensors<br />

RS232 RS232 serial interface 15-pin HD ZK-R-IK01-BS-R2-I-02<br />

Brooks flow rate sensor model 5850TR analogue Flow rate sensor 15-pin D-Sub<br />

ZK-SFM-BR01-BA-UA-Yactual<br />

value on LP-AEP8A, set point on LP-AAP8UI 01<br />

Brooks flow rate sensor model 5850TR RS232 Flow rate sensor 15-pin D-Sub<br />

actual value, set point<br />

ZK-SFM-BR01-BS-R2-I-01<br />

Bronkhorst flow rate controller model analogue LP-AEAP8UA + 24V feeding ZK-CFM-BK21-BA-UA-I-01<br />

F-xxxaa-FAB/FBB/GAB/GBB-xx-a<br />

Bronkhorst flow rate controller model MFC<br />

F-xxxx-FA/FB/GA/GB-xx and F-xxxaa-FAC/<br />

FBC/GAC/GBC-xx-a<br />

Bronkhorst flow rate controller model<br />

F-xxxaa-FCB/FDB/GCB/GDB-xx-a<br />

Bronkhorst flow rate controller model MFC<br />

F-xxxx-FC/FD/GC/GD-xx and<br />

F-xxxaa-FCC/FDC/GCC/GDC-xx-a<br />

Laboratory gas meter type TG, impulse<br />

output<br />

analogue LP-AEAP8UA +/- 15 V feeding ZK-CFM-BK22-BA-UA-I-01<br />

analogue LP-AEAP8IA + 24 V feeding<br />

First choice type<br />

ZK-CFM-BK23-BA-IA-I-01<br />

analogue LP-AEAP8IA +/- 15 V feeding ZK-CFM-BK24-BA-IA-I-01<br />

binary 5-pin plug DIN51524 device-side to 3-pin plug DIN51524<br />

for connection to DEP8A<br />

ZK-SFV-RI01-ID-XX-I-01<br />

Watchdog<br />

0/4..20mA twin wire<br />

PC Cables<br />

analogue Watchdog -plug ZK-X-HI05-IA-IA-O-01<br />

<strong>HiTec</strong> Null modem cable RS232 RS232, 2x 9-pin-SubD ZK-IT-HI<strong>10</strong>-BS-R2-I-01<br />

<strong>HiTec</strong> RS232 extension RS232 RS232 9-pin ZK-IT-HI11-BS-R2-I-01<br />

<strong>HiTec</strong> UI Com1 RS232 25-pin to 25- pin RS232 ZK-IT-HI01-BS-R2-I-01<br />

<strong>HiTec</strong> UI Com1 RS232 9- pin to 9-pin, RS232 ZK-IT-HI01-BS-R2-I-02<br />

<strong>HiTec</strong> UI Com1<br />

Miscellaneous, periphery<br />

RS232 25-pin to 9-pin, RS232 ZK-IT-HI01-BS-R2-I-03<br />

Labcom cable ZK-LAB-HI07-BS-R2A-I-01<br />

<strong>HiTec</strong> type B230V16H, B230V16R digital LP-DAP8A, LP-DAP8T ZK-LAB-HI06-OD-XX-I-01<br />

Jeti spectrometer RS232 RS232 9-pin ZK-X-JE01-BS-R2-I-01<br />

Pt<strong>10</strong>0 extension analogue LEMO socket/plug 4-pin ZK-XX-HI11-BA-PX-I-01<br />

Edwards Typ Active-Gauge-Display (AGD)<br />

for Active-Pirani-Gauge (APG)<br />

analogue analogue voltage on LPAEP8 ZK-X-EW01-IA-UP-I-01<br />

Driver Programs for Laboratory Device Interfaces<br />

Laboratory devices with serial interfaces can be<br />

integrated into the system via serial interface of the<br />

PI or the UI.<br />

Devices connected to the PI can be linked without<br />

problems to control loops such as sensor or final<br />

control elements.<br />

Devices connected to the UI can also be integrated<br />

as sensors or final control elements in control loops;<br />

however, values needed for automated control must<br />

be permanently replaced through the UI PI interface.<br />

Driver<br />

According to the complexity of the protocol, different<br />

kinds of drivers maybe useful. Drivers can partially<br />

be parameterised by the user, for the other part, they<br />

must be parameterised by a programmer.<br />

Integrated Drivers<br />

For most lab balances from Scaltec, Kern, Sartorius<br />

and Mettler, as well as heating/cooling thermostats<br />

by Huber, Julabo, Lauda or Thermo-Haake, interface<br />

drivers are already integrated.<br />

NAMUR Driver<br />

Laboratory devices with an ASCII log according to<br />

NAMUR- NE28 recommendation can simply be<br />

connected to the PI via the NAMUR driver (see<br />

NAMUR driver).<br />

PI Driver<br />

Laboratory devices with more complicated logs, in<br />

particular binary logs, can be connected to a serial<br />

interface of the UI via specific PI drivers (see PI<br />

driver).<br />

Specific Drivers<br />

For laboratory devices with more complicated logs,<br />

in particular binary logs, which are supposed to be<br />

connected directly to the PI, a driver must be<br />

programmed by our programming department.<br />

Where appropriate, a communication processor<br />

maybe necessary.<br />

HiText Driver<br />

Laboratory devices with more complicated logs can<br />

be connected to a serial interface of the UI via a<br />

driver written in HiText. The HiText driver can be<br />

programmed by the customer himself or by our<br />

programming department.<br />

The following table presents the available driver programs for various standard laboratory devices<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

and instrumentation components. The offer is<br />

continuously expanded.<br />

If your device is not listed here, do not hesitate to<br />

ask for it.<br />

Manufacturer, device, model<br />

Heating/cooling Thermostats<br />

Signal type, connection, card,<br />

driver<br />

Required interface panel / module, cable Driver Order Code<br />

Huber unistat set point output -O and<br />

actual value-I*<br />

RS232, NAMUR-driver HD-RS2329(P)L, ZK-T-HU01-BS-R2-I-01 SF-NAMTHHU1<br />

Julabo set point output -O and actual<br />

value-I*<br />

RS232, NAMUR-driver HD-RS2329(P)L, ZK-T-JU00-BS-R2-I-01 SF-NAMTHJUL1<br />

Haake thermostat F6-C35 * RS232, NAMUR-driver HD-RS2329(P)L, ZK-T-HA01-BS-R2-Y-01 SF-NAMTHHAK1<br />

Lauda set point output -O and actual<br />

value-I*<br />

Stirrer<br />

RS232, NAMUR-driver HD-RS2329(P)L, ZK-T-LD01-BS-R2-I-01 SF-NAMTHLAU1<br />

ViscoPakt * RS232, NAMUR-driver HD-RS2329(P)L, ZK-R-HI02-BS-R2-I-01 SF-NAMRUVIPA1<br />

Heidolph RS232, NAMUR-driver HD-RS2329(P)L, ZK-R-IK01-BS-R2-I-01 SF-NAMIRUPV<br />

IKA Powervisc<br />

Dosing Pumps<br />

RS232, NAMUR-driver HD-RS2329(P)L,<br />

ZK-R-IK01-BS-R2-I-01 (9 pin),<br />

ZK-R-IK01-BS-R2-I-02 (15 pin)<br />

SF-NAMIRUPV<br />

TELAB BF414, 9-pin SUB-D RS232, NAMUR-driver HD-RS2329(P)L, ZK-P-TL02-BS-R2-I-01 SF-NAMDPTEL1<br />

Knauer K1800 RS232, NAMUR-driver HD-RS2329(P)L, ZK-P-KN00-BS-R2-I-01 SF-NAMDPKNA1<br />

Knauer K501 RS232, NAMUR-driver HD-RS2329(P)L, ZK-P-KN00-BS-R2-I-01 SF-NAMDPKNA2<br />

Metrohm Dosino Titrator 718 PI-driver PC-COM-Port ZK-DL-MO02-BS-R2-I-01 SF-PNKMTRx<br />

x = 1,2,4,8<br />

Metrohm Dosino Dosimat 665 PI-driver PC-COM-Port ZK-DL-MO01-BS-R2-I-01 LV-PNKMTRx<br />

x = 1,2,4,8<br />

Ismatec hose pump Reglo Digital PI-driver HD-RS2329(P)L, ZK-P-IS04-BS-R2-I-01 LV-PNKDPISM1<br />

Ismatec wobbling piston Relgo FMI<br />

Multipath Valves<br />

PI-driver HD-RS2329(P)L, ZK-P-IS04-BS-R2-I-01 LV-PNKDPISM1g<br />

Knauer HPLC7 RS232, NAMUR-driver HD-RS2329(P)L, ZK-VMO-KN07-BS-R2-I-01 SF-NAMMVKNA1<br />

Besta MW1 / MW2 multi-path valves<br />

Massflow-Meter and Controller<br />

RS232, NAMUR-driver HD-RS2329(P)L SF-NAMMWVAL1<br />

Bronkhorst set point output and actual<br />

value-E<br />

RS232, NAMUR-driver HD-RS2329(P)L, ZK-CFM-BK00-BS-R2-T-01 SF-NAMMFBRON1<br />

Brooks set point output and actual<br />

value-E<br />

Massflow meter & Controller<br />

RS232, NAMUR-driver HD-RS2329(P)L, ZK-CFM-BR01-BS-R2-I-02 SF-NAMMFBROO1<br />

ModBus-devices PI-driver PC-COM-Port,<br />

SF-PNKMBUSx<br />

PC-RS485<br />

x = 1,2,4,8<br />

* Most of the devices of this manufacturer are already implemented as device components, so that additional<br />

drivers are only required in special cases.<br />

PI-driver: additional module for LabVision<br />

NAMUR driver: parameterisation of the module NAMSER-X (additionally required)<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

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Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

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Pumps<br />

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Stirring and<br />

Dispersing<br />

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112<br />

Laboratory Automation Hardware<br />

MSRmanager-System<br />

MSRmanager front view with mounted fastening angles<br />

The MSRmanager is mainly used in installations of<br />

the process and chemical engineering industry,<br />

research, environmental and process engineering,<br />

test facility automation and the manufacturing<br />

industry.<br />

It is deployed instead of the LAB-PI’s if the<br />

installation is to be hardwired.<br />

The main emphasis was put on compact<br />

construction and flexibility. One of many advantages<br />

in comparison to usual PLC or process computer<br />

based solutions derives from the possibility to<br />

change the parameters during the runtime without<br />

having to stop the installation. Especially during<br />

challenging projects of automation, the<br />

MSRmanager shows its unique features.<br />

Universal, free from potential and flexible interfaces<br />

save many transducers, interface and driver circuits.<br />

Using minimal space, the MSRmanager enables to<br />

even fulfil the most complex tasks which could either<br />

not be accomplished at all or only at great expense<br />

using conventional equipment.<br />

Because of its wide field of possible applications and<br />

its universal connection technology, the<br />

MSRmanager is an economical alternative to many<br />

other systems.<br />

The broad spectrum of available inputs and outputs<br />

even includes serial interfaces. To connect balances,<br />

analysers, dosing units etc., up to 15 serial<br />

interfaces can be installed.<br />

The MSRmanager system can be easily expanded<br />

and used for diverse applications. It is possible to<br />

realize networked systems and to include controllers<br />

from other manufacturers.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


MSRmanager Organisation<br />

Laboratory Automation Hardware<br />

In order to realize installations for applications with<br />

up to 240 inputs/outputs, an MSRmanager can be<br />

equipped with the required interface cards and<br />

terminal blocks.<br />

The suitable modules can be found in the chapter<br />

MSRmanager Interfaces. A serial interface with<br />

potential isolation for connection to the Operator-<br />

Console (control computer) is provided.<br />

The Connection Technology<br />

Sensors and positioners are connected to the PI unit<br />

via terminal blocks. They are connected to the input/<br />

output cards by ribbon cable. Therefore, there is a<br />

plug on every terminal module to connect the ribbon<br />

cable. The signalling lines are applied with screwing<br />

terminals at the terminal block<br />

CG-ABK1x or CG-ABK2x are used as the control<br />

computer.<br />

The PI-UI coupling is accomplished via RS232 and<br />

up to <strong>10</strong> m long data cables (as standard, a 3 m<br />

cable will be delivered, other lengths upon request).<br />

The cabling can optionally be done by RS485 or<br />

optical fibres with up to 2000 m length.<br />

(HAV24LINK...).<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

Components<br />

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114<br />

Free standing mounting installation<br />

Laboratory Automation Hardware<br />

The terminal blocks can either be mounted on the<br />

backside of the MSRmanager or on the top-hat rail<br />

or in a cabinet.<br />

Basic Devices<br />

MSRmanager-Basic Device<br />

The basic device contains the interface cards and<br />

the subsystems. The electronic frame is a solid 19inch<br />

chassis made of metal, which is suitable for<br />

freestanding mounting as well as for integrating into<br />

19-inch cabinets.<br />

The minimum configuration includes the circuit<br />

board with the bus, a 32-bit CPU, a watchdog circuit<br />

and a serial Operator-Console interface which is<br />

potential-isolated.<br />

The power saving CMOS-technology does not<br />

create much heat so that the device does not have<br />

to be ventilated. Therefore, there are no specific<br />

conditions as to where to install it.<br />

The minimal configuration consists of the basic<br />

device, a <strong>HiTec</strong> UI (e.g. CG-ABK1), a HK-AD20N<br />

analogue/digital conversion card and a HK-HMUXmultiplexor<br />

card with terminal block (e.g. MB-<br />

MSRmanager rear view Clamping yoke for ribon cable and Cable outlet<br />

The ribbon cables to the MSRmanager can be<br />

tailored accordingly. For each input/output card there<br />

are various terminal blocks available. The example<br />

shown here is the terminal block MB-AEB16V.<br />

We look forward to supporting your project planning!<br />

A terminal block mounted on a system rail<br />

AEB16VP). This system is well suited for e.g. data<br />

logging with 16 zero potential universal analogue<br />

inputs.<br />

Onto this device, thermal elements, Pt<strong>10</strong>0, voltage<br />

and current emitting sensors, etc. can be coupled in<br />

arbitrary combinations.<br />

The device can be upgraded to up to 240 analogue<br />

and 128 binary interfaces (with PLC subsystem) so<br />

that it is adaptable to every task.<br />

The indicators and control elements for basic<br />

operations are located on the front panel of the<br />

MSRmanager. The “DC“ display indicates the status<br />

of the power supply. The “Busy“ display signalizes<br />

the operational status. The “COM“ display indicates<br />

the traffic to and from the Operator Console.<br />

Upon request, the terminal block can be mounted on<br />

the device rear panel.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Hardware<br />

Configuration of the MSRmanager Basic Device:<br />

� 19 inch, 3HE slide-in module or desktop chassis<br />

� 14 slots (optional 19), one of which is occupied<br />

by the CPU card<br />

� Battery backed real time clock<br />

� Watchdog (monitoring circuit)<br />

� Zero potential serial port for the UI (control<br />

computer)<br />

Reserves for extensions<br />

On the back of the MSRmanager there are ports for<br />

the control computer and an optional 6 serial<br />

interfaces.<br />

Up to a maximum of four DIN system rails (top-hat<br />

rails) can be attached to the back of the terminal<br />

blocks to save additional space. For strain relief of<br />

the ribbon cables there is a clamping mechanism.<br />

Optionally the MSRmanager can be delivered with a<br />

24 V or 48 V power supply instead of a 230 V~ one.<br />

Reserve supplied with<br />

13 slots HK-AD20N, HK-HMUX, HK-DEA16N, HK-DA812UI, HK-SER8ECB, HK-<br />

SER16ECB<br />

6 serial interfaces on<br />

basis panel<br />

HD-RS2329(P)L, HD-RS485P<br />

1 panel slot for<br />

LP-SER99<br />

HD-RS2329(P)L, HD-RS485P<br />

Internal Power supply, control voltage, digital terminal blocks HS-NGS242, HS-NGS241S<br />

Technical Data<br />

Casing 3 HE desktop case<br />

Basis panel UI-Interface, 230 V~ power supply and indicator LEDs<br />

CPU CPU 32 card, 32 bit embedded controller with watchdog<br />

Development reserve See table<br />

Dimensions Depth: 370 mm<br />

Width: 450 mm (19“)<br />

Height: 145 mm (3 HE)<br />

Working temperature 0 - 50 °C, non-condensing<br />

Storing temperature 0 - 50 °C<br />

IP protection class IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory device<br />

Power consumption From 30 W to 140 W, depending on the configuration<br />

Operating voltage 230 V +<strong>10</strong>/-20 %, opt. widerange <strong>10</strong>0 to 240 V.<br />

Delivery Scope MSRmanager<br />

power supply cable<br />

manual<br />

cable to connect to the 9-pin RS232 interface of UI<br />

Order Code Description<br />

MG-MSRMAN MSRmanager basic device<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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Plant<br />

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Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

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Stirring and<br />

Dispersing<br />

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116<br />

MSRbox Basic Device<br />

Laboratory Automation Hardware<br />

The MSRbox-basis devices are, with exception of<br />

the reduced mounting possibilities, to a large extent<br />

identical with the MSRmanager basis device. They<br />

carry the required interface cards, sub systems, and<br />

hardware options. The electronics chassis is a<br />

robust metal casing, which is both suited for free<br />

mounting and for the assembly in control cabinets.<br />

The minimum configuration includes the circuit<br />

board with the bus, a CPU and multifunction card,<br />

the CMOS-RAM and a watchdog circuit as well as<br />

serial interface to the control computer, which is<br />

potential-isolated.<br />

The power saving CMOS-technology minimises lost<br />

heat so that the device does not have to be<br />

ventilated. Therefore there are no specific conditions<br />

as to where to install it.<br />

The basic device, in connection with a <strong>HiTec</strong> UI (e.<br />

g. CG-ABK1), a HK-AD20NMUX8 card with terminal<br />

block (e. g. MB-AEB16VP) already represents the<br />

hardware of a data logging system with 8 potentialfree,<br />

universal analogue input channels.<br />

Configuration of the MSRbox Basic Device:<br />

� 3HE slide-in module or desktop chassis<br />

� Battery backed real time clock<br />

� Watchdog (monitoring circuit)<br />

� serial port for the control computer (UI)<br />

Extension Reserve:<br />

To this device, thermal elements, Pt<strong>10</strong>0, voltage and<br />

current emitting sensors, etc. can be coupled in<br />

arbitrary combination<br />

The devices can be upgraded with the available<br />

interfaces and consequently adjusted to any<br />

application purpose.<br />

The indicators and control elements for basic<br />

operations are located on the front panel of the<br />

MSRmanager. The “DC“ display indicates the status<br />

of the power supply. The “Busy“ display signals the<br />

operational status. The “COM“ display indicates the<br />

traffic to and from the Operator-Console.<br />

For strain relief of the ribbon cables there is a<br />

clamping mechanism.<br />

Upon request, the terminal blocks can be mounted<br />

on the device rear panel.<br />

At the MG-MSRBOX2 up to HS-NGS243 can be<br />

integrated for activated sensors and actuators. If the<br />

peripheral power supply can be the MG-MSRBOX2<br />

is a space safing alternative in the MG-MSRBOX1<br />

and MG-MSRBOX2.<br />

On the rear of the MSRbox, there are connections<br />

for UI/workstations and up to four serial ports for<br />

connection of suitable devices.<br />

MSRbox1 MSRbox2S (1/2 19“) MSRbox2<br />

slots 2 (+ 1 CPU) 5 (+1 CPU) 5 (+1 CPU)<br />

supplied with HK-AD20NMUX8, HK- HK-AD20NMUX8, HK- HK-AD20NMUX8, HK-<br />

AD20NMUX16, HK- AD20NMUX16, HK- AD20NMUX16, HK-<br />

DEA16N, HK-DA812UI, HK- DEA16N, HK-DA812UI, HK- DEA16N, HK-DA812UI, HK-<br />

AD24DMS4, HK-SER8ECB, AD24DMS4, HK-SER8ECB, AD24DMS4, HK-SER8ECB,<br />

HK-SER16ECB<br />

HK-SER16ECB<br />

HK-SER16ECB<br />

serial interfaces Max. 4 HD-RS2329L, HD- Max. 4 HD-RS2329L, HD- Max. 4 HD-RS2329L, HD-<br />

RS2329PL, HD-RS485P RS2329PL, HD-RS485P RS2329PL, HD-RS485P<br />

internal Power supply for digital Power supply for digital Power supply digital terminal<br />

terminal blocks (control terminal blocks (control blocks (control voltage) ma.<br />

voltage)<br />

current) by main power<br />

supply<br />

2xNGS243<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Technical Data<br />

Laboratory Automation Hardware<br />

Case 3 HE desktop units<br />

Basis panel UI interface (PC), power supply and indication LEDs 230V<br />

CPU HK-CPU32 card, 32 bit Embedded Controller with watchdog<br />

Extension Reserve See table<br />

Working temperature 0 to 50 °C, non-condensing<br />

Storing temperature 0 to 50 °C<br />

IP Protection Category IP20, complies with EN6<strong>10</strong><strong>10</strong> safety regulations for EMSR and laboratory device<br />

Power consumption 30 W to 140 W<br />

Operating voltage 230 V +<strong>10</strong>/-20 %, opt. widerange <strong>10</strong>0 to 240 V.<br />

MSRbox1 MSRbox2S MSRbox2<br />

Dimensions Depth: 318 mm<br />

Width: 236 mm (1/2 19“)<br />

Height: 145 mm (3 HE)<br />

Depth: 318 mm<br />

Width: 236 mm (1/2 19“)<br />

Height: 145 mm (3 HE)<br />

Delivery Scope MSRbox device<br />

power supply cable<br />

manual<br />

cable to connect to the 9-pin RS232 interface of UI<br />

Order Code Description<br />

MG-MSRBOX1 MSRbox1 basis device to equip individually<br />

MG-MSRBOX2 MSRbox2 basis device to equip individually<br />

MG-MSRBOX2s MSRbox2s basis device to equip individually<br />

Terminal Blocks for PMC PIs<br />

For the connection of practically all existent sensors,<br />

actors, and devices to the MSRmanager and<br />

MSRboxes used in practice, you will find the suited<br />

terminal blocks in the following.<br />

Terminal blocks (universal-) analogue Input<br />

This terminal block is an<br />

extended version of the MB-<br />

AEB16V. It features an<br />

additional terminal strip for<br />

the reference voltage in<br />

order to connect the Pt<strong>10</strong>0 in<br />

four wire circuit.<br />

Thus, it is suitable for all<br />

kinds of sensors and signals.<br />

� Screw-type terminals for 16 test ports<br />

� Voltage -<strong>10</strong>...+<strong>10</strong> V, Pt<strong>10</strong>0, resistance sensor,<br />

current 0/4...20 mA,<br />

� Thermocouples<br />

� Integrated electronic compensation of cold<br />

junctions for thermocouples<br />

� Precision current source 1 mA for Pt<strong>10</strong>0<br />

� Additional terminal strip for the connection of<br />

a current source<br />

� Mounted on DIN-system rails<br />

Technical Data<br />

Depth: 318 mm<br />

Width: 342mm (3/4 19“)<br />

Height: 145 mm (3 HE)<br />

The blocks are connected to the interface card by a<br />

ribbon cable.<br />

Please indicate the desired length in your order. The<br />

default length is 180 cm. (max. 3 m).<br />

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Laboratory Automation Hardware<br />

Product description Terminal block for HK-HMUX, HK-AD20NMUX8, HK-AD20NMUX16 with 16<br />

analogue inputs and comparator for thermocouples, additional terminal strip for<br />

conductors 3 and 4 of Pt<strong>10</strong>0 in four wire circuit<br />

Dimensions Width: 112 mm<br />

Depth: 77 mm<br />

Height: 72 mm<br />

Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />

Order Code Description<br />

MB-AEB16VP Terminal block for voltage, current, Pt<strong>10</strong>0 and thermocouples<br />

Terminal Block for Voltage and Current Output<br />

This terminal block is used to<br />

control devices with analogue<br />

inputs via current or voltage.<br />

� Screw-type terminals for 8 current and<br />

voltage outputs<br />

� For 8 channels either 0/4...20 mA or -<strong>10</strong>...+<strong>10</strong><br />

V<br />

� For the connection of thermostats, stirrers,<br />

analogue actuators etc.<br />

� Integrated protection from noise voltages<br />

� Mounted on DIN-system rail<br />

Technical data<br />

Product description Terminal block for D/A-converter-card-HK-DA812UI,<br />

8 x -<strong>10</strong>..+<strong>10</strong> V voltage outputs and parallel 8 x 0/4..20 mA current outputs<br />

Dimensions Width: 67 mm<br />

Depth: 77 mm<br />

Height: 72 mm<br />

Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />

Order Code Description<br />

MB-AAB8UI Terminal block for voltage and current output<br />

Terminal Block with 8 digital Inputs<br />

This terminal block<br />

enables the connection of<br />

switches, alarm units,<br />

binary detectors, etc. to<br />

the MSRmanager. Up to 2<br />

MB-DEB8-blocks can be<br />

connected to a HK-<br />

DEA16N card by ribbon<br />

cable. The range of the<br />

input voltage is NAMUR-compliant or optional from 5<br />

to 24 V.<br />

� Eight NAMUR-consistent inputs<br />

(or optionally 5 – 24V)<br />

� Screw-type terminals<br />

� Mounted on DIN-system rails<br />

� Integrated protection from noise voltages<br />

Technical Data<br />

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Laboratory Automation Hardware<br />

Product description Terminal block for HK-DEA16x, 8 digital inputs, NAMUR compliant<br />

Dimensions Width: 67 mm<br />

Depth: 77 mm<br />

Height: 50 mm<br />

Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />

Order Code Description<br />

MB-DEB8 Terminal Block for digital Entry<br />

Terminal block with 8 Relay outputs<br />

This terminal block is the default<br />

one, since it is universally<br />

applicable and electrically most<br />

robust. The outputs are passive,<br />

i.e. they can connect external<br />

current sources.<br />

� Screw-type terminals<br />

� Switching voltage up to 40 V AC or DC<br />

� Switching current up to 2 A<br />

� 1 NO contact and 1 NC contact (passive)<br />

� For the connection of magnetic valves,<br />

drives, heaters, etc.<br />

� Mounted on DIN-system rails<br />

Technical Data<br />

Product description Terminal block for HK-DEA16x, 8 relay outputs, 1 break contact element, 1 shutter<br />

(passive), LED control (requires HS-NGS241S in addition)<br />

Dimensions Width: 112 mm<br />

Depth: 77 mm<br />

Height: 50 mm<br />

Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />

Order Code Description<br />

MB-DAB8R Terminal block digital output, 8 relay outputs<br />

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Laboratory Automation Hardware<br />

Terminal Block with 8 Transistor Outputs<br />

The transistor terminal block<br />

is equipped with transistors<br />

as emitter followers. It is<br />

operated only to control<br />

electronic devices or small<br />

consumer loads. The<br />

outputs are active. If the<br />

outputs are to be operated<br />

in active mode a 24 V power<br />

supply (HS-NGS24xx) is required.<br />

� Screw-type terminals<br />

� Switching voltage up to 24 V<br />

� Active outputs, switching current up to 0,5 A<br />

(other values are optional)<br />

� Mounted on DIN-system rails<br />

In the standard version, all 8 output channels are<br />

secured via separate (self-resetting) multifuses,<br />

max. 0,5 A.<br />

Technical Data<br />

Product description Terminal block for HK-DEA16x, 8 active emitter follower outputs,<br />

up to 24 V, 0,5 A<br />

Dimensions Width: 67 mm, Depth: 77 mm, Height: 50 mm<br />

Delivery Scope Terminal block, cable for the interface card, connecting diagram<br />

Order Code Description<br />

MB-DAB8T_0.5A Terminal block digital output, with 8 transistor outputs<br />

Serial Interfaces<br />

For the PMC devices the same modules for serial<br />

interfaces are available as for the LabManager (see<br />

Special Terminal Blocks<br />

LabManager, serial ports).<br />

For special applications, e.g. extreme environmental<br />

conditions like splash water etc., we build special<br />

customized solutions for the terminal blocks like the<br />

shown stainless steel IP65.<br />

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Laboratory Automation Hardware<br />

Intrinsically safe inputs/ outputs (Ex-equipment)<br />

For applications, which have a high explosive risk, in<br />

zone 1 the inputs and outputs of the MSRmanager<br />

can be equipped with IS power supply and loop<br />

powered supplies. The inherently safe circuits are<br />

[EEx ib] certified. The MSRmanager can be<br />

installed outside the hazardous area if it is not<br />

encapsulated or inside the hazardous area if<br />

encapsulated with overpressure type "p" following<br />

DIN EE50016 / VDE 0170/0171 Part 3. The<br />

configuration is user-specific, if desired including<br />

certification by the TÜV. The protective chassis of<br />

the MSRmanager and the control PC is also userspecific.<br />

Product Description Upgrade for applications in hazardous areas<br />

[Eex-ib](zone 1), per I/O - interface, Eex-ia (zone 0) on application<br />

Order Code Description<br />

HE-EEXIU Intrinsic safety for voltage inputs and outputs 0..<strong>10</strong> V<br />

HE-EEXII Intrinsic safety for current inputs and outputs 0..20 mA<br />

HE-EEXID Intrinsic safety for digital inputs and outputs 20 V<br />

HE-EEXIRS232 Intrinsic safety for serial ports TxD, RxD<br />

HE-EEXIPT<strong>10</strong>0 Intrinsic safety for Pt<strong>10</strong>0 inputs<br />

HE-EEXITH Intrinsic safety for thermocouples<br />

Interface Cards<br />

Analogue/Digital-Converter Card<br />

This card contains a 24-bit analogue /digital<br />

converter with a programmable amplifier. A<br />

potential free secondary bus is provided for the<br />

connection of multiplexer cards (HK-HMUX). To an<br />

A/D card up to 15 relays or semiconductor<br />

multiplexer cards can be connected, with a total of<br />

240 analogue measuring channels.<br />

� High precision with 24 bit resolution<br />

� up to 15 multiplexers (HK-HMUX) on one A/Dconverter<br />

card (= 240 Channels)<br />

� potential free secondary bus for connecting<br />

multiplexer-cards<br />

� Potential isolation secondary bus /bus 1500 V<br />

Technical Data<br />

HK-AD20N Analogue/Digital-Converter Card<br />

Resolution 24 Bit guaranteed Resolution<br />

Measurement Range Voltage –0,125 V...+0,125 V, -1...+1 V, -<strong>10</strong>...+<strong>10</strong> V, current 0/4..20 mA,<br />

Absolute Measurement<br />

Uncertainty of one<br />

(during maintenance<br />

interval)<br />

Pt<strong>10</strong>0 -200..+600 °C, Thermocouples (NiCr-Ni) -200...+1373 °C<br />

-<strong>10</strong>...+<strong>10</strong> V: 0,05 %<br />

-1...+1 V: 0,05 %<br />

-125 mV..+125 mV: 0,05 %<br />

0/4...20 mA: 0,15 %<br />

Pt<strong>10</strong>0 -50...+300 °C: 2 °C, Resolution 0,01 °C<br />

Thermocouples (NiCr-Ni) -50...+300 °C: 2 °C, Resolution 0,1 °C<br />

Delivery Scope Analogue/Digital-Converter card<br />

Order Code Product Description<br />

HK-AD20N Analogue/Digital-Converter card with 20 bit resolution<br />

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Multiplexer Cards<br />

Laboratory Automation Hardware<br />

The <strong>HiTec</strong> multiplexer cards enable the direct<br />

connection of analogue sensors and signal sources<br />

such as thermocouples, resistive sensors, voltage or<br />

current-supplying devices, etc.. Transducers are not<br />

needed and can be saved in the budget.<br />

As alternative connection methods, different<br />

Semiconductor-Multiplexer Cards<br />

The semiconductor multiplexer card offers all<br />

properties for process operation under rough<br />

conditions. The electric strength of the used<br />

semiconductor switches is 350 V.<br />

interface panels and terminal blocks are available,<br />

which are connected via ribbon cables with the<br />

multiplexer card<br />

☞ A multiplexer card requires at least one<br />

connection module for operation.<br />

The semiconductor multiplexer cards are<br />

characterized by the following properties:<br />

� 16 potential free differential inputs for mixed<br />

connection of different analogue signals and<br />

sensors<br />

� suitable for electrically rough process operation<br />

� Potential isolation between bus and input (1500<br />

V)<br />

� Total sampling rate approx. 40 channels per<br />

second<br />

� Electronic cold junction compensation for<br />

thermocouples<br />

� Up to 15 HK-HMUX on one A/D-Converter card<br />

240 channels (please note: Limited to number of<br />

free slots!)<br />

To a semiconductor multiplexer card, a MB-AEB16xx terminal block or up to two of the following panels can<br />

be connected:<br />

Suited Connection Panels Order Code<br />

Connection panel with 4 current/voltage inputs and 4 Pt<strong>10</strong>0 inputs LP-AE4PT4P<br />

Combi-panel with 4 voltage-/current inputs with power supply and 4 Pt<strong>10</strong>0 inputs LP-AE4PT4PA<br />

Combi-panel 8 current inputs 0/4...20 mA, 8 current outputs 0/4...20 mA LP-AEAP8I<br />

Combi-panel 8 current inputs 0/4...20 mA with sensor feed,<br />

8 current Outputs 0/4...20 mA<br />

LP-AEAP8IA<br />

Combi-panel 8 voltage inputs ±<strong>10</strong> V, 8 voltage outputs ±<strong>10</strong> V LP-AEAP8U<br />

Combi-panel 8 voltage inputs ±<strong>10</strong> V with sensor feed,<br />

8 voltage outputs ±<strong>10</strong> V<br />

LP-AEAP8UA<br />

Connection panel with 8 current and voltage inputs LP-AEP8<br />

Connection panel with 8 current and voltage inputs with sensor feed LP-AEP8A<br />

Connection panel with 8 PT<strong>10</strong>0 sensors LP-PTP8<br />

Connection panel with 8 thermocouples LP-THP8<br />

Description Semiconductor-multiplexer-card, with 16 universal, potential free analogue-inputchannels<br />

and 1 mA reference current source for resistive sensors.<br />

Order Code Article Description<br />

HK-HMUX semiconductor Multiplexer Card with 16 channels<br />

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Laboratory Automation Hardware<br />

Analogue Measurement Card, 8/16 Channels<br />

This card is designed for LAB and MSRbox systems<br />

and contains a 24-Bit-analogue/digital converter with<br />

programmable amplifier. The card posses an<br />

integrated 8 or 16 channel multiplexer.<br />

Technical data<br />

Resolution: 20 Bit<br />

Measurement Range: Voltage -0.125 V...+0.125 V, -1...+1 V, -<strong>10</strong>...+<strong>10</strong> V, current 0/4...20 mA,<br />

Absolute measurement<br />

uncertainty of one<br />

(within maintenance<br />

interval):<br />

To a HK-AD20NMUX16 analogue measurement<br />

card a MB-AEB16xx or up to two of the following<br />

panels can be connected:<br />

Pt<strong>10</strong>0 -200...+ 600 °C, Thermocouples (NiCr-Ni) -200...+1373 °C<br />

-<strong>10</strong>...+<strong>10</strong> V: 0.05 %<br />

-1...+1 V: 0.05 %<br />

-125 mV..+ 125 mV: 0.05 %<br />

0/4..20 mA: 0.15 %<br />

Pt<strong>10</strong>0 -50...+300 °C: 0.2 °C, Resolution 0.01 °C<br />

Thermocouples (NiCr-Ni) -50...+3 00 °C: 2 °C, Resolution 0.1 °C<br />

To a HK-AD20NMUX8 analogue measurement card<br />

one of the following panels can be attached:<br />

Description Order Code<br />

Connection panel with 4 current/voltage inputs and 4 Pt<strong>10</strong>0 inputs LP-AE4PT4P<br />

Combi-panel with 4 voltage-/current inputs with power supply and 4 Pt<strong>10</strong>0 inputs LP-AE4PT4PA<br />

Combi-panel 8 voltage inputs -<strong>10</strong>V ... +<strong>10</strong> V, 8 voltage outputs -<strong>10</strong>V...+<strong>10</strong>V LP-AEAP8U<br />

Combi-panel 8 voltage inputs -<strong>10</strong>V ... +<strong>10</strong> V, 8 voltage outputs -<strong>10</strong>V...+<strong>10</strong>V with sensor feed LP-AEAP8UA<br />

Combi-panel 8 current inputs 0/4...20 mA, 8 current outputs 0/4...20 mA LP-AEAP8I<br />

Combi-panel 8 current inputs 0/4...20 mA with sensor feed,<br />

8 current Outputs 0/4...20 mA<br />

LP-AEAP8IA<br />

Connection panel with 8 current and voltage inputs LP-AEP8<br />

Connection panel with 8 current and voltage inputs with sensor feed LP-AEP8A<br />

Connection panel with 8 PT<strong>10</strong>0 sensors LP-PTP8<br />

Connection panel with 8 thermocouples LP-THP8<br />

Product Description Semiconductor-multiplexer card, with 16 universal, potential free analogue input<br />

channels and 1 mA reference current source for resistance feeler.<br />

Order Code Description<br />

HK-AD20NMUX8 Analogue measurement card, 8 channels, 20 Bit AD-converter<br />

HK-AD20NMUX16 Analogue measurement card, 16 channels, 20 Bit AD-converter<br />

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Laboratory Automation Hardware<br />

Precision Acquisition Card, 8 Channels Pt<strong>10</strong>0<br />

The precision measuring card HK-AD24Pxx was<br />

developed for applications with the highest demands<br />

in resolution and measuring accuracy. Due to its<br />

eight-channel specification the cost-use relation of<br />

this card is particularly favourable in applications<br />

which need several channels, e.g. reaction<br />

calorimetry.<br />

Special Properties<br />

� Highest accuracy: 24 Bit Resolution<br />

� Relative differential measurement uncertainty<br />

� ≤ ±0,001 °C in range -180 to 266 °<br />

� 8 channels are virtually simultaneously<br />

captured in < 1 s<br />

� Self calibrating<br />

� 8 channels for Pt<strong>10</strong>0<br />

Applications<br />

� High precision temperature measurement, e.g. in<br />

calorimetry<br />

� Calibration measurements with sensors<br />

� Precision voltage measurements in quality<br />

control applications<br />

Technical Data<br />

The HK-AD24Pxx-cards have a very exact converter<br />

and a precision current source for resistive sensors.<br />

On eight inputs temperatures can be monitored with<br />

highest resolution over a very large temperature<br />

range.<br />

The modern circuit design makes compensation<br />

elements unnecessary. By self calibration,<br />

temperature- and aging influences are reduced to<br />

the extremely low long-time drift value of the highprecision<br />

reference elements.<br />

The temperature sensors are connected via a<br />

connection panel with connectors according to<br />

NAMUR standard. Suitable temperature sensors in<br />

different precision classes are available upon<br />

request with calibration certificate.<br />

Sensor/signal: Pt<strong>10</strong>0 / voltage<br />

Range: -180 to +266 °C<br />

Number of channels: 8<br />

Absolute measurement ≤ ±0,01 °C (≤ ±0,03 °C) after calibration<br />

uncertainty v.E.<br />

(within maintenance<br />

period):<br />

Relative measurement ≤ ±0,001 °C (≤ ±0,003 °C)<br />

uncertainty for<br />

differential<br />

measurement:<br />

Added measuring < 1 mW with sampling / 1 s (minimal self heating of the Pt<strong>10</strong>0)<br />

power:<br />

To use this card the connection panel LP-PTPRP8 is necessary.<br />

Delivery Scope: Card with 8 Analogue-inputs for voltage and resistive sensors, manual<br />

Order Code Description<br />

HK-AD24PX8 Precision measurement card with 8 channels for Pt<strong>10</strong>0, Abs. Differential measurement<br />

uncertainty 0,01 °C<br />

HK-AD24PKAL Industry calibration certificate for HK-AD24PX8<br />

Panel<br />

Delivery Scope: Panel with holding bolts, cable for internal connection<br />

Order Code Description<br />

LP-PTPRP8 Panel for HK-AD24PX<br />

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Laboratory Automation Hardware<br />

Precision Measuring Card analogue for GraviDos Load Cell<br />

This card for strain gauges (DMS) – full bridge is<br />

suited for the connection of up to four GraviDos<br />

dosing systems, load cells, torque pickups, etc.<br />

� high precision 24 bit analogue/digital<br />

converter<br />

� integrative measurement due to the<br />

deployment of individual converters per<br />

channel<br />

� Minimisation of temperature drift due to Chop<br />

Operation<br />

Technical data<br />

Sensor/signal: DMS (strain gauge) full bridge<br />

Measurement Range:: Dependent on the measurement cell<br />

Number of Channels: 4<br />

Resolution: 24 Bit<br />

Absolute measurement<br />

uncertainty v.E.:<br />

(within maintenance period)<br />

≤ ±0,1 %<br />

Measurement Resolution: ≤ ± 0,01 %<br />

Delivery Scope: Card with manual<br />

Order Code Description<br />

HK-AD24DMS4 Plug-in card with 4 channels for strain gauge (DMS) bridges and 4 digital outputs<br />

(semiconductor)<br />

You can find suited load cells in the chapter "Process Analytics and Sensors“.<br />

To operate this card, one of the following connector panels is required:<br />

Order Code Suitable Panels<br />

LP-DMS4DA4PT Combination Panel with 4 DMS (strain gauge) inputs and 4 digital outputs (semiconductor)<br />

LP-DMSP8 Connector Panel with 8 DMS (strain gauge) inputs (at 2 cards)<br />

Remark: For MSR (process measurement and control) systems, the terminal block (AEB4DMS) is available.<br />

Analogue-Output Card, 8 Channels<br />

The digital/analogue converter card enables the<br />

output of voltages or currents for control and<br />

regulation purposes.<br />

� Potential isolation between output and bus<br />

(<strong>10</strong>00 V Isolation)<br />

� current- and voltage Outputs<br />

Technical Data<br />

Resolution 12 Bit<br />

Number of channels: 8<br />

voltage outputs -<strong>10</strong>..+<strong>10</strong> V max. 2 mA<br />

current outputs 0/4..20 mA<br />

Absolute uncertainty:<br />

(within maintenance period)<br />

≤ ±0.2 %<br />

Product Description D/A-Converter card 8 x 12 Bit, for analogue-output voltage and current.<br />

Order Code Description<br />

HK-DA812UI 8 x analogue output card 0...20 mA and –<strong>10</strong>...+<strong>10</strong> V, 12 Bit<br />

Automatic<br />

Laboratory<br />

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Laboratory Automation Hardware<br />

To the HK-DA812UI analogue output card the following connection modules can be attached:<br />

Order Code Description<br />

LP-AAP8UI Panel for analogue-output, current and voltage<br />

LP-AEAP8U LabManager combi-panel 8 voltage inputs ±<strong>10</strong> V, 8 voltage outputs ±<strong>10</strong> V<br />

LP-AEAP8UA LabManager combi-panel 8 voltage inputs ±<strong>10</strong> V, 8 voltage outputs ±<strong>10</strong> V, sensor feed 24 V<br />

LP-AEAP8I LabManager combi-panel 8 current inputs 0/4...20 mA with sensor feed,<br />

8 current outputs 0/4...20 mA<br />

LP-AEAP8IA LabManager combi-panel 8 current inputs 0/4...20 mA with sensor feed,<br />

8 current outputs 0/4...20 mA<br />

MB-AAB8UI MSRmanager connection block for voltage and current output ±<strong>10</strong> V and 0/4...20 mA<br />

Digital-In/Output Card<br />

The digital-input/output card is needed, if valves,<br />

monitors etc. are to be directly switched over the<br />

MSRmanager or binary senders such as switches<br />

and limit value transmitters are to be queried. The<br />

card is inserted into the internal MSRmanager bus.<br />

The pulse-width modulated output allows quasicontinuous<br />

control of heaters, motorized control<br />

valves, etc.. Thus, there is no necessity for<br />

expensive thyristor actuators or additional control<br />

electronics.<br />

The pulse area modulation is an extended form of<br />

pulse frequency modulation (PFM), which minimises<br />

the pulse amount and consequently prevents<br />

damage to the actuator (e.g. a magnet valve).<br />

� 16 Optio-coupler outputs for Bit-, Byte-, pulse<br />

width and frequency modulated output (max. 1<br />

kHz)<br />

� Defined selectable reset status<br />

� 16 isolated digital inputs 24 V NAMURconforming<br />

� Frequency and event counting (max. 4kHz)<br />

� Inputs optionally recording/non-recording for bitand<br />

byte input (edge detection)<br />

Product Description Digital-Input/Output card with 2 x 8 inputs and 2 x 8 outputs, inputs selectable<br />

recording/non-recording, frequency and event counting, outputs selectable pulse<br />

width modulated, pulse frequency modulated, defined reset status.<br />

Order Code Description<br />

HK-DEA16N Digital-Input/Output card Standard, 16 DE, 16 DA<br />

The following connection modules can be attached:<br />

Order Code Description<br />

LP-DEP8 Digital input connection panel with 8 active 24 V input<br />

LP-DEP8A Digital input connection panel with 8 passive 24 V input and sensor feeding<br />

LP-DAP8 Digital output connection panel with 8 passive output<br />

LP-DAP8A Digital output connection panel with 8 active 24 V output<br />

LP-DAP8T Digital output connection panel with 8 active transistor outputs<br />

LP-DE4DA4P Combi-panel with 4 active digital inputs, 4 passive digital outputs<br />

LP-DE4DA4PA Combi-panel with 4 active digital inputs, 4 active digital outputs<br />

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Serial Input/Output Card<br />

Laboratory Automation Hardware<br />

The SER8 and SER16 interface cards with 8 or 16<br />

SIO channels each, ensure optimal performance of<br />

the serial interfaces. As every channel possesses an<br />

own SIO component with character buffer, optimal<br />

performance is achieved. Up to 2 cards, therefore a<br />

maximum of 32 channels, are possible.<br />

� Independent SIO channels with FIFO memory,<br />

supports RTS/CTS-Hardware-Handshake.<br />

Requires a interface module (HD-RS2329(P)L or<br />

HD-RS485P) per used channel.<br />

� Parallel processing of all channels, which leads<br />

to reduction of delay.<br />

� Maximum transmission rate 19200 baud (per<br />

channel)<br />

� 8/16 Channels<br />

� Faster processing in comparison to serial<br />

interfaces of the CPU32<br />

Order Code Description<br />

HK-SER8ECB Serial Input/Output Card, 8 Channels<br />

HK-SER16ECB Serial Input/Output Card, 16 Channels<br />

To these cards, the following interface modules can be connected:<br />

Order Code Description<br />

HD-RS2329L RS232 Interface Module, 9-pin, with LabCom feeding<br />

HD-RS2329PL RS232 Interface Module, 9-pin, electrically insulated, with LabCom feeding<br />

HD-RS485P RS485 Interface Module , 9-pin , electrically insulated<br />

All serial interfaces can communicate with the automation unit in different manners:<br />

� default device driver für known laboratory devices<br />

� NAMUR device driver for "unknown" laboratory devices<br />

� HiText control programm<br />

Further informations can be found in the chaptor Laboratory Automation Software.<br />

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PI Additional Devices<br />

Laboratory Automation Hardware<br />

The PI-additional devices conduce to expand the<br />

functionality of the PI.<br />

Switch Box 2x230V<br />

External connection box with two single pole<br />

switched (edition -H) or two double pole (edition -R)<br />

mains sockets. Control inputs for connection to LP-<br />

DAP8T or LP-DAP8A. When controlled by a LP-<br />

DAP8 or MB-DAB8x an external power suppply is<br />

needed.<br />

The control can happen with a control voltage of up<br />

to a maximum of 24 V DC. The outputs can also be<br />

controlled pulse width or pulse frequency modulated<br />

HP-B230V16R is not suitable for switching<br />

frequencies above 1 Hertz.<br />

Technical Data<br />

Operating<br />

voltage/current<br />

2x230 V AC, sum load 16 A / 3680 VA, Edition HP-B230V16H: unipolar wiring,leak<br />

current 5 mA minimum load <strong>10</strong>0 mA; Edition HP-B230V16R: double pole<br />

switching<br />

Connection type <strong>Main</strong>s plug<br />

Control signal Max. 24 V DC<br />

Usable with Panel LP-DAP8T, LP-DAP8A, Cable, ZK-LAB-HI06-0D-XX-I-01<br />

For switching Pumps, Heater Jackets, Heater Domes...<br />

Delivery Scope Switch box with fixed mains cable 2.5 m<br />

Order Code Description<br />

HP-B230V16H Socket switch box 2 x 230 V, sums load 16 A, single-pole switched, semi-conductor switcher<br />

HP-B230V16R Socket switch box 2 x 230 V, sums load 16 A, dual-pole switched, capacity relais<br />

ZK-LAB-HI06-OD-XX-I-01 Cable for connection to LAB-PI (2 necessary)<br />

Special Construction:<br />

HP-B400V16A electrical socket switchboard three-phase switched, rated voltage 400 V, 16 A per<br />

phase. Connection type: 16A CEE connector.<br />

If used with the panel DAP8T, the panel must be Please state in the order, if this is the case.<br />

modified.<br />

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LabCom Mini Terminal<br />

Laboratory Automation Hardware<br />

LabCom is a local mini terminal for LabManager,<br />

LabBox, and MSRmanager systems. It provides<br />

access to the most important process variables right<br />

at the plant. LabCom is predominantly used, if the<br />

control PC is not in direct proximity of the plant or if it<br />

must be ensured that with a disturbance or a total<br />

failure of the control PC, most important functions for<br />

operating and monitoring remain ensured.<br />

Particularly if several LAB/PMC devices are<br />

attached to a control PC, it is recommended to equip<br />

each device with a LabCom.<br />

Properties and Functions<br />

� Local display of important process values<br />

� Free definable dialogue for operation<br />

guidance<br />

� Local input possibility for values and<br />

parameter<br />

� Local alarming by flashing LEDs and acoustic<br />

signals<br />

� Shutdown button starts shutdown program in<br />

critical situations<br />

� Watchdog circuit monitors the PI and alarms<br />

on errors<br />

LabCom is connected to a specially equipped serial<br />

interface of the Lab/PMC device and supplied with<br />

power from the same.<br />

The following structure is an example for several<br />

LAB/PMC devices (up to eight possible) mounted on<br />

an operating panel:<br />

The LCD display presents 4 x 20 characters and can<br />

be allocated with display and input fields in random<br />

order. Identifiers and number formats can be<br />

selected individually. The layout is easy and<br />

uncomplicated to create with a mask editor.<br />

The following Display Elements are designated:<br />

� Alphanumeric Text<br />

� Numeric Data Point Values<br />

� Date<br />

� Time<br />

Up to 16 different masks can be defined. A mask can<br />

be selected by using the Page-Up/ Down keys on<br />

the LabCom terminal or by assigning the mask<br />

number per program.<br />

LabCom is set up as a device component within the<br />

Lab /MSRmanager systems. This provides various<br />

logical inputs/outputs as data points which are<br />

assigned to the individual functionalities.<br />

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Technical Data<br />

Laboratory Automation Hardware<br />

Dimensions: 222 mm x <strong>10</strong>5 mm x 40 mm<br />

Housing: ABS<br />

Protection: IP64<br />

Screen: Plexiglas<br />

Control codes: ANSI<br />

Product Description LCD-Terminal for LabManager system, with 4 x 20 character display, Stop-button,<br />

Alarming function, Input keyboard, Hand held terminal (additionally HD-RS2329L<br />

needed, optional: Connection cable ZK-LAB-HI07-BS-R2-I-01)<br />

Order Code Description<br />

HP-LABCOM1 Local Hand Terminal<br />

HD-RS2329(P)L PI-RS232 Interface module with power supply for LabCom<br />

Delivery scope: Mini-Terminal with connection cable 3 m<br />

Other possibilities, e.g. Light-up display, large display or device without keyboard, on request.<br />

Watchdog Device<br />

The external watchdog device is a systemmonitoring<br />

device which is used if increased safety<br />

is necessary. It monitors a temperature, a further<br />

arbitrary sensor with a 4..20 mA signal as well as<br />

hard and software components of the automation<br />

system.<br />

If one of the adjustable limit values is exceeded, or<br />

in case of a failure of the automation system, the<br />

cut-off circuit of the system is interrupted via a<br />

potential-free switching contact and an alarm is<br />

sounded.<br />

A short circuit proof voltage for the supply of a<br />

sensor (e.g. pressure sensor) is available (12 V,<br />

max. 35 mA).<br />

The following conditions can be monitored:<br />

� Pt-<strong>10</strong>0-Element for monitoring an adjustable<br />

safety temperature within the range 0..300 °C;<br />

connection via 4-pin Lemosa socket with feeler<br />

break recognition.<br />

� 4 – 20 mA input with cable-break recognition,<br />

monitoring of an adjustable limit value in the<br />

range 4-20 mA. Connection via 6-pin Tuchel<br />

(DIN45327) plug. To this input, any sensor can be<br />

attached for monitoring any physical variable,<br />

e.g. a pressure sensor for monitoring of an<br />

adjustable maximum pressure.<br />

� Monitoring of the automation system,<br />

transmission of a binary toggle signal in 1 to 9 s<br />

intervals via the binary output to the automation<br />

system, monitoring of the response from the<br />

automation system via a binary input. Connection<br />

via 5-pin 180 ° Tuchel-plug (DIN41524).<br />

Each monitoring condition can be activated<br />

individually.<br />

If one of these events occurs, an early warning is<br />

released and a built-in piezo buzzer is sounded.<br />

Therefore, a potential-free contact is provided for the<br />

control of an external signal generator. If this early<br />

warning is not acknowledged within an adjustable<br />

time (5 s – 500 s) using the “suppress”-key, the cutoff<br />

circuit is interrupted over an open potential-free<br />

contact. With the “acknowledge”-key, the alarm can<br />

be acknowledged.<br />

Safety can be further increased by building a<br />

switched output of the PI into the cut-off circuit and<br />

the PI redundantly monitors the watchdog device as<br />

well as the same physical parameters.<br />

With the help of a key, an individual alarm condition<br />

can be simulated in order to check the electronics.<br />

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Technical Data<br />

Laboratory Automation Hardware<br />

Connections 4-pol. LEMO socket for PT-<strong>10</strong>0<br />

6-pol. DIN-socket DIN 45327 for 4-20 mA signal<br />

Switched output for signal generator<br />

Switched output for triggering the cut-off function via 4-pol. DIN-socket DIN41524<br />

Dimensions Depth: 41 mm, Width: 165 mm, Height: <strong>10</strong>3 mm<br />

Power supply 9V..12 V / 200 mA<br />

Environmental 0..45 °C, max.95 % humidity, no bedewing<br />

conditions<br />

Delivery Scope Y-connection cable for connection to a digital input and a digital output of a LAB or<br />

PMC-PI<br />

Order Code Description<br />

HP-WDOGEXT1-pa External System monitoring device<br />

ZK-X-HI05-IA-IA-O-01 Cable for 4 – 20 mA sensors with Tuchel-plug and one open end<br />

pa = PI connection: L: LAB PIs, M: PMC PIs<br />

UI-PI-Coupling<br />

The <strong>HiTec</strong> <strong>Zang</strong> PI’s can be coupled in various ways<br />

with the UI.<br />

Depending on distance or surrounding field<br />

conditions, a suitable medium can be selected.<br />

Media Specials Max. distance<br />

RS232 default 7m<br />

RS485 <strong>10</strong>0m accross simple telefon line,<br />

<strong>10</strong>00m accross rdt-cable<br />

Fibre optics shortened live expectance mit Kunststoff-LL bis ca. 20m<br />

mit Glaslichtleiter 2000m<br />

T1 accross given telephon line approx. <strong>10</strong>km<br />

COM-Server over networkk (own network segment necessary) random<br />

UI-PI Coupling via Optic Cables<br />

With unfavourable electrical conditions like strong<br />

magnetic interference fields or placing of the<br />

transmission cable outside a data communication is<br />

recommended between the PI (LAB/PMC<br />

managers or box) and the UI (system controller) via<br />

fibre-optics. For distances to 50 m a less expensive<br />

plastic light conductor can be used. For larger<br />

distances up to 2000 m an optical glass-fibre cable<br />

is necessary.<br />

The module HA-V24LINK2 is attached to the<br />

normal RS232-UI-interface of the PI.<br />

Order Code Description<br />

HA-V24LINK2 Optical modem (PC-side) for synthetic fibre with separate power supply<br />

HA-V24LINKKLI Synthetic fibre for indoors<br />

HA-V24LINKKLA Synthetic fibre for outdoors<br />

UI-PI Coupling via RS485<br />

If the distance between MSR manager and system<br />

controller is more than 7 m data communication<br />

according to the RS485 standard is recommended.<br />

With the help of the option RS485, distances up to<br />

2000 m can be bridged.<br />

Order Code Description<br />

HA-RS485 Level-converter RS485<br />

The level converter is attached to a normal RS232<br />

interface and can be used on both the UI and on the<br />

PI side.<br />

Alternatively, a RS485 interface can be built into the<br />

PI in place of the RS232-UI-interface. Likewise, a<br />

RS485 interface card can be built into the UI. In this<br />

case the level converters are omitted.<br />

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Laboratory Automation Hardware<br />

UI-PI Coupling via LAN<br />

With the help of a COM-Server, <strong>HiTec</strong> PIs<br />

(LAB/PMC manager or box) can be connected via<br />

Ethernet LAN with the UI (system controller).<br />

Order Code Description<br />

HA-COMSERV<strong>10</strong>01 Com-Server Twisted-Pair or Coax <strong>10</strong>0 Mbit on RS232<br />

UI-PI Coupling via Leased Line<br />

With the help of a special leased-line modem <strong>HiTec</strong><br />

PIs (LAB/MSRmanager or Box) can be connected<br />

Order Code Description<br />

HA-MODEM4 Leased line modem pair for 4 wire connection<br />

DC power supply<br />

A 24 V DC power supply is needed for running the<br />

connection block and interface panels or for feeding<br />

other devices, e.g. sensors and actuators.<br />

Power units are needed for the connection blocks<br />

MB-DAB8R, MB-DAB8T DAB8T and for activating<br />

the panels LP-AEP8A, LP-DAP8A, LP-AEAP8IA,<br />

LP-AEAP8UA, LP-DE4DA4PA.<br />

Some of the devices have smoothed, and some<br />

stabilised outputs.<br />

It should be clarified with the responsible network<br />

administrators, whether the network can handle the<br />

additional load, or whether an own net segment<br />

must be established.<br />

using a 4-core telecom line. The maximum distance<br />

amounts to <strong>10</strong>,000 m.<br />

Power supply 24 V, 0,7 A regulated<br />

Technical Data<br />

Product description 24 V DC Power supply on connection block, stabilised,<br />

0.7 A continuous load, 1A 70 % ED duty cycle for DIN-System rail mounting,<br />

For usage with MSRmanager or switchboard mounting<br />

Environmental 0..45 °C, max. 95 % humidity, non condensing<br />

conditions<br />

Dimensions Depth: 112 mm, Width: 77 mm, Height: 64 mm<br />

Order Code Description<br />

HS-NGS241S Power supply 24 V, 0.7 A regulated, top-hat rail fitting<br />

Power supply 24 V, 7,5 A regulated<br />

Technical Data<br />

Product Description 24 V power supply on, stabilized, 7.5 A.<br />

Possible fitting into LabManager2<br />

Dimensions Depth: 220 mm, Width: 170 mm, Height: 120 mm<br />

Order Code Description<br />

HS-NGS248S Power supply 24 V, 7.5 A, regulated<br />

Power supply 24 V, 1.5 A<br />

Technical Data<br />

Product description 24 V power supply on, stabilized, 1.5 A for DIN system rail fitting.<br />

Possible fitting into LabManager1/2, LabBox2, MSRbox 2, MSRmanager.<br />

Dimensions Depth: 1<strong>10</strong> mm, Width: 55 mm, Height: 75 mm<br />

Order Code Description<br />

HS-NGS241A Power supply 24 V, 1.5 A, smoothed, system rail fitting<br />

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Laboratory Automation Hardware<br />

Power supply 24 V, 2.5 A<br />

Technical Data<br />

Product Description 24 V power supply, smoothed, 2.5 A, for DIN-system rail fitting. Possible fitting into<br />

LabBox1, MSRbox 1.<br />

Dimensions Depth: 1<strong>10</strong> mm, Width: 55 mm, Height: 75 mm<br />

Order Code Description<br />

HS-NGS242 Power supply 24 V, 2.5 A, smoothed, system rail fitting<br />

Power supply 24 V, 3 A<br />

Technical Data<br />

Product description 24 V power supply, smoothed, 3 A, DIN-system rail fitting.<br />

Possible fitting into LabManager1 a. 2, LabBox2, MSRbox 2, MSRmanager.<br />

Dimensions Depth: 1<strong>10</strong> mm, Width:<strong>10</strong>0 mm, Height: 75 mm<br />

Order Code Description<br />

HS-NGS243 Power supply 24 V, 3 A, smoothed, system rail fitting<br />

Power supply 24 V, 8 A<br />

Technical Data<br />

Product Description 24 V power supply, smoothed, 8 A.<br />

Possible fitting into LabManager2<br />

Dimensions Depth: 200 mm, Width: 170 mm, Height: <strong>10</strong>5 mm<br />

Order Code Description<br />

HS-NGS248 Power supply 24 V, 8 A, smoothed<br />

Power supply 24 V, 8 A extern<br />

Technical Data<br />

Product description 24 V power supply, smoothed, 8 A, for external use<br />

Connection cable for external use<br />

Suitable to active LabManager interfaces or USTAT.<br />

Dimensions Depth: 200 mm<br />

Width: 170 mm<br />

Height: <strong>10</strong>5 mm<br />

Order Code Description<br />

HS-NGS248E Power supply 24V , 8 A, smoothed, external use<br />

Power supply 15 V, 2.8 A<br />

Technical Data<br />

Product description 15 V power supply, controlled, 2.8 A.<br />

switching power supply for DIN-system rail fitting.<br />

Possible fitting into LabManager1/2, LabBox2, MSRbox 2, MSRmanager.<br />

Dimensions Depth: 1<strong>10</strong> mm, Width: 55 mm, Height: 75 mm<br />

Order Code Description<br />

HS-NGS153SN Power supply 15 V, 2.8 A, controlled, switching power supply, System Rail Fitting<br />

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Simulation Devices<br />

Pt<strong>10</strong>0 Simulator<br />

Laboratory Automation Hardware<br />

With this simulator, the user can check the<br />

measuring accuracy and function of the Pt<strong>10</strong>0 and<br />

voltage measuring inputs. Temperatures of 0, 30,<br />

<strong>10</strong>0, and 300 °C can be simulated. Additionally there<br />

is a variable adjustment possibility. The tolerance of<br />

the reference resistances is 0,02 %.<br />

Order Code Description<br />

HX-SIMPT1 Pt<strong>10</strong>0 Simulator<br />

Further simulation and test control units can be found in „Training and Education Modules“.<br />

Digital Signal Converter<br />

The <strong>HiTec</strong> <strong>Zang</strong> digital signal converters convert<br />

analogue and digital signals into RS232 or RS485<br />

ModBus protocols. They can be deployed, if the<br />

number of measuring channels is so low that the<br />

deployment of a Lab-PNC is not cost-effective.<br />

They are also suited as interfaces for small<br />

HiBuilder projects, e.g. as a supplement to LabDos<br />

or AutoSam in case additional signals need to be<br />

collected or additional actors require to be activated.<br />

Module Overview<br />

In LabManager/LabVision projects, they can be<br />

deployed on a supplementary basis, if the sampling<br />

rate of the internal interfaces is not sufficient to, e.g.,<br />

register a rapid pressure rise.<br />

� Power Supply via Interface Cable or Plug-In<br />

Power Supply 24V<br />

� RS232 and RS485 ModBus Interface<br />

� Compact Metal Casing<br />

Technical Data:<br />

Interface RS232 V24 and RS485, ModBus<br />

Protocol, Power Supply 24V via<br />

RJ48.<br />

If operated on an interface without<br />

power supply, a plug-in power<br />

supply is required.<br />

Dimensions L approx. 142 mm, W approx. 52<br />

mm, H approx. 23 mm, with Plug<br />

Connection Description Plug Order Code<br />

Current and -<strong>10</strong>...<strong>10</strong>V, 0/4..20mA, 24bit ADU, Measuring 6-pole Jack, DIN 45322 IL-AINAMP1D<br />

Voltage ON Uncertainty 0,1%<br />

Pt<strong>10</strong>0<br />

Measuring Range -200..+600 °C, Four Wire Lemo Type 1S, 4-pole IL-PTAMP1D<br />

Temperature<br />

Sensor<br />

Technology<br />

DMS-Bridge Digital DMS Amplifier for DMS Half and Full-<br />

Bridges<br />

Lemo Type 1S, 6-pole IL-GRADOAMP1D<br />

Current and<br />

Voltage OFF<br />

0...<strong>10</strong>V, 0/4..20mA, Uncertainty 0,1% 6 pole Jack, DIN 45322 IL-PHAMP1D<br />

pH-Probe, pH 0...14, Temperature with Pt<strong>10</strong>0, VarioPin -Device Socket IL-CLARKAMP1D<br />

Temperature integrated Temperature Compensation<br />

O2, Clark Probe O2-Messverstärker VarioPin -Device Socket IL-AOUT1D<br />

Digital ON Binary, Frequency and Event Counting, 24V 3-pole Jack, DIN 41524 IL-DIN1D<br />

Digital OF Binary, pulse width modulated, pulse<br />

frequency modulated, active (24V) or<br />

passive<br />

3-pole Plug, DIN 41524 IL-DOUT1D<br />

Delivery Scope Amplifier, Manual, (Please order cable separately)<br />

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Laboratory Automation Hardware<br />

Order Code Description<br />

IL-AINAMP1D Digital Measuring Amplifier for -<strong>10</strong>...+<strong>10</strong>V, 0/4...20mA, RS232 V24 /RS485 Interface<br />

IL-PTAMP1D Digital Measuring Amplifier for Pt<strong>10</strong>0 Four Wire Technology, RS232 V24 /RS485 Interface<br />

IL-GRADOAMP1D Digital Measuring Amplifier for DMS Load Cells, RS232 V24 /RS485 Interface<br />

IL-PHAMP1D Digital Measuring Amplifier for pH- und Redox-Electrodes, RS232 V24 /RS485 Interface<br />

IL-CLARKAMP1D Digital Measuring Amplifier for Clark O2-Electrodes, RS232 V24 /RS485 Interface<br />

IL-AOUT1D Analogue Output for -<strong>10</strong>...+<strong>10</strong>V, 0/4...20mA, RS232 V24 /RS485 Interface<br />

IL-DIN1D Digital Converter for 24V Binary, Frequency and Event Counting. RS232 V24 /RS485 Interface<br />

IL-DOUT1D Digital Output passive and active 24V, RS232 V24 /RS485 Interface<br />

ZK-MV-BS-R4-I-01 RS485 Cable for Digital Measuring Amplifier with 24V Power Supply via Pin 1<br />

IL-MV1D-SN Plug-In Power Supply for Digital Measuring Amplifier<br />

Display and Operating Elements<br />

A display and operation component (OC) for a <strong>HiTec</strong><br />

<strong>Zang</strong> System consists of a special PC with Windows<br />

XP or Windows Vista operating system and<br />

LabVision-UI software.<br />

The OC, as a component of an automation system,<br />

must meet special requirements:<br />

� Uninterupted Power Supply (UPS) with Shut<br />

Down Interface<br />

� LabVision compatible UPS Management<br />

� EMV-robust<br />

� Run-In System Test<br />

These requirements are not met by normal office<br />

PCs. <strong>HiTec</strong> OCs are devices with adjusted and<br />

proven hardware. The devices are tested with ready<br />

to use, already installed software in the complete<br />

system before dispatch.<br />

The OC software LabVision is based on a database<br />

system, which increases the hardware requirements.<br />

As the database and the operating system could be<br />

damaged in case of a current failure, a <strong>HiTec</strong> OC is<br />

principally equipped with an uninterrupted power<br />

supply system and a UPS Management System.<br />

During a current failure, the system runs buffered by<br />

storage batteries. Before the storage battery<br />

capacity is used up, the system is shut down in a<br />

defined manner.<br />

The normal equipment version comprises a<br />

Standard UPS. This must not be deeply discharged,<br />

as may happen if the whole plant is switched off via<br />

a main switch. Should the UPS be separated from<br />

the net, this must be done in charged condition at<br />

the operator panel. If this can not be ensured, the<br />

Online UPS CP-USV7O should be used, which is<br />

equipped with a deep discharge protection.<br />

PC-Hardware is subject to extremely fast innovation.<br />

According to this fact, <strong>HiTec</strong> <strong>Zang</strong> occasionally<br />

adapts the models to the state of technology. For<br />

this reason, it does not really make sense to present<br />

the current devices, which will soon be out of date.<br />

We rather offer a selection of two devices: The<br />

standard version with standard equipment and<br />

performance according to the current state of the<br />

technology and a device with upscale equipment<br />

and performance. Details in regard to the current<br />

equipment are gladly forwarded upon request.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 135<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


136<br />

Casing Design<br />

Laboratory Automation Hardware<br />

Our display and operation components are available<br />

in four differently designed casings.<br />

For useunder rough conditions, it is advisable to use<br />

the industrial PC with protected drives and the<br />

option to be installed in 19 inch system cabinets.<br />

The standard casing is the midi tower.<br />

Desktop Microcube Midi tower 19 Inch Industrial PC<br />

Depth: 375 mm<br />

Width: 415 mm<br />

Height: 165 mm<br />

Products similar to photos!<br />

<strong>HiTec</strong>-ABK1<br />

Depth: 335 mm<br />

Width: 2<strong>10</strong> mm<br />

Height: 269 mm<br />

The <strong>HiTec</strong> ABK1 is used for applications of small<br />

and medium size, e.g. in connection with a LabBoxor<br />

LabManager1 PI.<br />

The basic configuration can be upgraded with the<br />

offered options such as the DVD burner etc..<br />

You have the choice between four different casing<br />

designs. By default, the device is delivered as midi<br />

tower.<br />

Depth: 500 mm<br />

Width: 2<strong>10</strong> mm<br />

Height: 380 mm<br />

Basic Equipment*:<br />

Depth: 500 mm<br />

Width: 482,6 mm (19“)<br />

Height: 177 mm (4 HE)<br />

� Single-Core processor<br />

� at least 2 GB RAM<br />

� fast SATA hard disk (> 250GB)<br />

� DVD/CD Drive<br />

� Sound card<br />

� UPS and UPS Management Software<br />

� Windows-Keyboard and Wheel-Mouse<br />

� Windows XP© or Windows Vista© preinstalled<br />

*As of 3/<strong>2009</strong>. The equipment is consistently aligned to the<br />

proven state of the technology.<br />

Order Code Description<br />

CG-ABK1C <strong>HiTec</strong> Display and Operating Component in Micro Cube Casing, with UPS System<br />

CG-ABK1M <strong>HiTec</strong> Display and Operating Component in Midi Tower Casing, with UPS System<br />

CG-ABK1D <strong>HiTec</strong> Display and Operating Component in Desktop Casing,with UPS System<br />

CG-ABK1I <strong>HiTec</strong> Display and Operating Component in 19inch industrial Casing, with UPS System<br />

CP-USV7O Upgrading: Online UPS System 700 VA, secured against deep discharge, incl. software<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


<strong>HiTec</strong>-ABK2<br />

Laboratory Automation Hardware<br />

The <strong>HiTec</strong> ABK2 is used for medium and greater<br />

applications, e.g. in connection with a LabManager2<br />

PI or several PIs with a multitude of LabVision<br />

entities.<br />

You have the choice between four different casing<br />

designs. By default, the device is delivered as midi<br />

tower.<br />

For increased data protection, the ABK2 can be<br />

equipped with a RAID System.<br />

Basic Equipment*:<br />

� Dual-Core processor<br />

� at least 4096 MB RAM<br />

� fast SATA hard disk (> 500GB)<br />

� DVD/CD Recorder<br />

� Sound card<br />

� UPS and UPS Management Software<br />

� Windows-Keyboard and Wheel-Mouse<br />

� Windows XP© or Windows Vista© preinstalled<br />

*As of 3/<strong>2009</strong>. The equipment is consistently aligned to the<br />

proven state of the technology.<br />

The ABK2 enables the connection of a second<br />

monitor. With this, it is for example possible to<br />

assign the manual operation level and the recipe<br />

control each to an own monitor.<br />

Order Code Description<br />

CG-ABK2C <strong>HiTec</strong> Display and Operating Component in Micro Cube Casing, with UPS System<br />

CG-ABK2M <strong>HiTec</strong> Display and Operating Component in Midi Tower Casing, with UPS System<br />

CG-ABK2D <strong>HiTec</strong> Display and Operating Component in Desktop Casing,with UPS System<br />

CG-ABK2I <strong>HiTec</strong> Display and Operating Component in 19 inch industrial Casing, with UPS System<br />

CK-RAID1 Mirrored Disc RAID 1 (with intelligent Controller Card)<br />

For supplementary components, see "UI Additional Components“, for suited monitors, see "Monitors“.<br />

Expansions<br />

Order Code Description<br />

CK-RAM2x512 Memory Expansion by 1 Gigabyte DDR2-RAM for <strong>HiTec</strong> AKB<br />

(additional 2 x 512 MB Brand-RAM for Dual-Channel Technology)<br />

CK-RAM2x<strong>10</strong>24 Memory Expansion by 2 Gigabyte DDR2-RAM for <strong>HiTec</strong> AKB<br />

(additional 2 x 1 Gigabyte Brand-RAM for Dual-Channel Technology)<br />

CK-RAM2x2048 Memory Expansion by 4 Gigabyte DDR2-RAM für <strong>HiTec</strong> AKB<br />

(additional 2 x 2 Gigabyte Brand-RAM for Dual-Channel Technology )<br />

P-USV7O Upgrading: Online UPS System 700 VA, secured against deep discharge, incl. Software<br />

Ex Industrial PC<br />

This computer is suited for direct use in areas with a<br />

risk of explosions. Equipped with stainless steel<br />

casing for PC and monitor with plastic foil keyboard.<br />

Further information upon request.<br />

Order Code Description<br />

CG-ABKEX <strong>HiTec</strong> Display and Operating Component in Explosion Protective Casing, with UPS System<br />

CZ-EXMAUS Wireless mouse for operation in explosive areas<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 137<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


138<br />

Fileserver<br />

Laboratory Automation Hardware<br />

We offer fileservers with Windows and Linux<br />

operating systems. Please request for our current<br />

models and specifications.<br />

UPS Power Supply Standard<br />

If the control system is intended to keep running in<br />

case of a power failure, an uninterrupted power<br />

supply (UPS) must be provided for the fileserver,<br />

ABKs, PIs, and, where required, for the most<br />

important devices of the primary instrumenting.<br />

To ensure controlled shutdown of the computer in<br />

case of electrical power outage, a UPS management<br />

system is required in addition.<br />

The Standard UPS may not be deeply discharged as<br />

this may occur if the plant is completely shut down<br />

via a main switch. If the UPS is intended to be<br />

disconnected from the net for a longer period, it<br />

must be shut down at the operator panel. If this can<br />

not be ensured, it is advisable to use the online<br />

UPS CP-USV7O.<br />

� Monitoring Output for UI<br />

� Power Output 700 VA<br />

� Maximum Bridging Period approx. 15 min.<br />

Upon request, we are also able to deliver online<br />

UPS with greater performance, e.g. with <strong>10</strong>00 or<br />

2000 VA.<br />

Order Code Description<br />

CP-USV7 UPS System supply 700 VA for <strong>HiTec</strong> display and operating components including software<br />

Note: CP-USV7 is already included in the delivery scope of all <strong>HiTec</strong> <strong>Zang</strong> work stations.<br />

UPS Power Supply Online<br />

Online UPS constantly provides equal voltage<br />

quality and is secured against deep discharge.<br />

It is intended for usage in cases where, after a<br />

power failure longer than the maximum bridging<br />

operation period, the shutdown of the UPS cannot<br />

be ensured.<br />

� Secured against deep discharge<br />

� Sinus voltage<br />

� Controlled voltage<br />

� Monitoring Output for UI<br />

� Power Output 700 VA<br />

� Maximum Bridging Period approx. 15 min.<br />

Upon request, we are also able to deliver online<br />

UPS with greater performance, e.g. with <strong>10</strong>00 or<br />

2000 VA.<br />

Order Code Description<br />

CP-USV7O Online UPS System 700VA, secured against deep discharge, including software<br />

Monitors<br />

Our monitors all meet the requirements of the current ergonomics regulations.<br />

Industrial Monitor<br />

The metal casing contains a 19 inch TFT Monitor<br />

and protects the same under rough conditions. It is<br />

prepared for the installation into a 19 inch control<br />

cabinet. If intended to install it free-standing or as<br />

part of a transportable system, it is recommended to<br />

install it in a plastic casing with handles (CZ-<br />

KTRAG).<br />

Technical Data<br />

Dimensions Depth: 116 mm, Width: 483 mm, Height: 399 mm<br />

Order Code Description<br />

CP-INMON Industrial monitor for mounting in control cabinet<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Standard Monitors<br />

17 Inch TFT Monitor<br />

� Resolution 1280 x <strong>10</strong>24 pixels<br />

� Low Radiation according to TCO03<br />

� 36 months warranty by manufacturer<br />

Laboratory Automation Hardware<br />

Order Code Description<br />

CP-M17TFT 17 Inch TFT Colour Monitor<br />

19 Inch TFT Monitor<br />

� Resolution up to 1280 x <strong>10</strong>24 pixels<br />

� Low Radiation according to TCO03<br />

� 36 months warranty by manufacturer<br />

Order Code Description<br />

CP-M190TFT 19 Inch TFT Colour-Monitor<br />

20 Inch Widescreen TFT Monitor<br />

� Resolution up to 1680 x <strong>10</strong>50 pixels<br />

� Low Radiation according to TCO03<br />

� 36 months warranty by manufacturer<br />

� Refresh Rate: 60 Hz<br />

� Adjustable height<br />

� with Swivel Base<br />

� Refresh Rate: 60 Hz<br />

� Adjustable height<br />

� with Swivel Base<br />

� Refresh Rate: 60 Hz<br />

� Adjustable height<br />

� with Swivel Base<br />

This monitor is as high as a normal 17 inch monitor but has a greater width. It is therefore easier to arrange<br />

windows, e.g. the recipe control and the analogue pen recorder, next to each other. This is also beneficial for<br />

operator ergonomics. In many cases, this is a real alternative to a second monitor.<br />

Order Code Description<br />

CP-M20TFTWS 20 Inch Widescreen TFT Monitor<br />

22 Inch Widescreen TFT Color Monitor<br />

� Resolution up to 1680 x <strong>10</strong>50 pixels<br />

� Low Radiation according to TCO03<br />

� 36 months warranty by manufacturer<br />

� Refresh Rate: 60 Hz<br />

� Adjustable height<br />

� with Swivel Base<br />

This monitor is as high as a normal 19 inch monitor but has a greater width. It is therefore easier to arrange<br />

windows, e.g. the recipe control and the analogue pen recorder, next to each other. This is also beneficial for<br />

operator ergonomics. In many cases, this is a real alternative to a second monitor.<br />

Order Code Description<br />

CP-M22TFTWS 22 Inch Widescreen TFT Monitor<br />

(Other models upon request!)<br />

Serial Interfaces for the Operating Components (OC)<br />

The following serial interfaces serve both for the<br />

connection of several PIs to one UI and for the<br />

connection of devices.<br />

The interfaces can be addressed via a HiText<br />

Program or with <strong>HiTec</strong> UI device drivers.<br />

Order Code Description<br />

CS-RS2322-PCI PCI Plug-in card for <strong>HiTec</strong> <strong>Zang</strong> Ocs (operating components) with 2 RS 232 interfaces<br />

Plug&Play, only 1 IRQ per card (interrupt sharing). Max. 921 kbps<br />

CS-RS2324-PCI PCI Plug-in card for <strong>HiTec</strong> <strong>Zang</strong> Ocs (operating components) with 4 RS 232 interfaces<br />

Plug&Play, only 1 IRQ per card (interrupt sharing) Max. 921 kbps<br />

CS-RS4852-PCI PCI Plug-in card for <strong>HiTec</strong> <strong>Zang</strong> Ocs (operating components) with 2 RS-422/485 interfaces<br />

Optically isolated isolated, Plug&Play, only 1 IRQ per card (interrupt sharing). Max. 921 kbps<br />

CS-RS4854-PCI PCI Plug-in card for <strong>HiTec</strong> <strong>Zang</strong> Ocs (operating components) with 4 RS-422/485 interfaces<br />

Optically isolated, Plug&Play, only 1 IRQ per card (interrupt sharing).<br />

Max. 921 kbps<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 139<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


140<br />

Periphery<br />

Laboratory Automation Hardware<br />

The following peripheral devices have been tested<br />

on <strong>HiTec</strong>h operating components (OC) and are<br />

supported by LabVision.<br />

Barcode Scanner<br />

The extremely high-performance, compact, handheld<br />

scanner is ideal for utilisation in the laboratory<br />

sector. The device offers quick and precise scanning<br />

with or without contact and can be easily configured<br />

for application in the <strong>HiTec</strong>-<strong>Zang</strong> OCs.<br />

The device is compatible with LabVision.<br />

Order Code Description<br />

CP-BCS232 Hand-held Barcode Scanner, RS232 connection to OC with driver and manual<br />

Printer<br />

The following printers are suited as standard PC-,<br />

protocol-, document- and pen recorder printers. Only<br />

robust and proven devices by acclaimed<br />

manufacturers are offered. The scope of delivery<br />

includes cables and manuals.<br />

Order Code Description<br />

CP-DRUHPDJC Hewlett Packard Colour Ink Jet Printer A4, Colour, with single feed feeder, with single sheet<br />

feeder, for printing of flow charts, screenshots, etc.<br />

CP-DRUHPLJ Hewlett Packard Black/White Laser Printer A4<br />

CP-DRUHPLJC Hewlett Packard Colour Laser Printer A4<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Here you will find:<br />

Laboratory Automation Software<br />

Laboratory Automation Software<br />

� LabVision® Software for Laboratory Automation<br />

� LabVision® Project Module<br />

� EasyBatch TM Table based Recipe Control<br />

� HiBatch TM Basis Operation based Recipe Control and Administration<br />

� Basis Operation Library for HiBatch TM<br />

� HiLIMS TM Laboratory Information Management System<br />

� PI-Firmware Modules, Regulator Modules, programmable logic controller (PLC)<br />

� HiBuilder TM Data Evaluation and Presentation<br />

� RI-CAD TM Uncomplicated Drawing of piping and instrumentation diagram (P&ID)<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 141<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


142<br />

LabVision®<br />

Advantages<br />

Laboratory Automation Software<br />

Maximum Automation, with Minimum Engineering<br />

LabVision is a modular visualisation and automation<br />

software system for automation devices from <strong>HiTec</strong><br />

<strong>Zang</strong> as well as other providers. Your system is<br />

presented on the display for monitoring and<br />

operating. Your process is monitored, controlled, and<br />

regulated, all processes are logged and archived.<br />

The process plant is presented on the monitor as a<br />

dynamic flow diagram for monitoring and operating.<br />

The online evaluation already delivers important<br />

information regarding the process during runtime.<br />

The process data chain reaches from the definition<br />

of the experiment right to the Laboratory Information<br />

Management System.<br />

Various advantages<br />

� Complete documentation of all process<br />

events<br />

� Intensive use of your resources<br />

� Consistent presentation of values, events and<br />

phases<br />

� Relief from routine tasks<br />

� Savings on Instrumentation thanks to virtual<br />

devices<br />

� Realisation of a consistent data process<br />

chain from the work order to the Laboratory<br />

Information Management System<br />

LabVision is one of the most efficient and<br />

outstanding modern process visualisation tools.<br />

Within the area of research process control systems<br />

(RPCS) it has an outstanding position. The System<br />

is particularly suited for visualising and automating<br />

continuous and batch processes in laboratories, pilot<br />

plants, mini-plants, and production in chemistry,<br />

pharmacy, bio and food technology. Due to its<br />

flexibility it can be used also in other areas such as<br />

waste management, solar and environmental<br />

technology.<br />

Its special strength is its flexible application<br />

range. LabVision fulfills the requirements of the<br />

NAMUR working group - AK 2,4 for research<br />

process control systems and is hereby ready for<br />

frequently changing or modified tasks.<br />

LabVision can be used on different complexity<br />

levels. If you want to use LabVision merely as a<br />

user, one day of instruction is usually sufficient to get<br />

acquainted with the handling.<br />

Even if you wish to establish automation projects for<br />

changing assemblies yourself, you can learn this<br />

within one day.<br />

This is enabled by the Project Module Library, which<br />

contains predefined project modules for all important<br />

basic functions such as tempering, dosing, pH or<br />

vacuum regulation, distilling etc..<br />

Specialists who wish to learn the complete range of<br />

possibilities of parameterisation and programming,<br />

merely require one week for familiarisation instead<br />

of the several months of schooling usually required<br />

for conventional process control systems.<br />

Features that convince:<br />

� Easy to use, minimum learning effort<br />

� As RPCS according to NAMUR standards online<br />

configurable and parameterised.<br />

� Project modules for fast and easy application<br />

development<br />

� Histo-Database for consistent storage of values,<br />

text, and events.<br />

� Support of the basic operations concept for batch<br />

processes (NAMUR NE 33)<br />

� Support of GLP and TQM by resource<br />

administration and automatic documentation<br />

� Scalable from small measurement acquisition<br />

systems up to networked process control<br />

systems with shared online-databases<br />

� English language version available, other<br />

languages upon request<br />

� Personalised user interface<br />

LabVision increases your efficiency, by relieving you<br />

from routine activities. Processes driven once can<br />

be repeated at any time, even after years, with<br />

optimum reproducibility, because all steps are made<br />

at the correct point in time, all materials are added<br />

and adjusted automatically and correctly. Parameters<br />

are set automatically to the correct value.<br />

The securing of the reproducibility and the optimal<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

documentation of all parameters, values and events<br />

contribute to an improvement in quality.<br />

The user interface has the following properties:<br />

� Operation to XP- and Vista-Standard<br />

� Logically object orientated and context sensitive<br />

� Self explanatory operating symbols with dynamic<br />

hint windows<br />

� Personalised (desktop can be stored and reloaded)<br />

� Protection from unauthorised access (own user<br />

administration)<br />

� Remotely controllable via network & modem<br />

User Requirements<br />

LabVision can be used on different levels of<br />

complexity and detail and requires appropriate levels<br />

of knowledge from the user (see also training course<br />

offer).<br />

1. Operation by shift personnel<br />

Operating and monitoring the current system by<br />

shift changing personnel requires a briefing of<br />

approx. half a day.<br />

2. Operation by personnel with minimum<br />

training<br />

With a training course of approx. two days, the<br />

service personnel is in the position to<br />

parameterise pre-fabricated applications for<br />

starting and operation. With the help of the basic<br />

operations library for batch running, also the<br />

minimum trained user is in a position to create,<br />

parameterise, and operate a complex recipe<br />

operational sequences with smallest time<br />

expenditure.<br />

3. Project engineering and operation by well<br />

trained personnel<br />

Well trained users (approx. one week) can<br />

address and use substantial details of the<br />

system according to his/her request with this<br />

easy to handle system. The user is able to<br />

independently create display and control<br />

screens, as well as control programs and online<br />

analyses of any complexity.<br />

4. Projects using well trained automation<br />

specialists<br />

The well trained automation engineering<br />

specialist (at least one week) can use functions<br />

of this completely open system in detail. Display<br />

and control screens can be created as well as<br />

control programs and online analyses of any<br />

complexity. Also the possibilities of the process<br />

interface (PI) for increased safety standards e.g.<br />

by use of the PLC Functionality of the LAB/MSR<br />

manager can be used.<br />

Libraries<br />

Libraries prearranged to the usual application cases<br />

support the user to save time and costs when<br />

establishing the project (see Laboratory Automation<br />

Software, SL-GOPBIB, SL-MODBIBALR, SL-<br />

BIBRILK and EN/ISO <strong>10</strong>628).<br />

Data Objects<br />

The following types of data points ( = data objects)<br />

are supported:<br />

� Input<br />

� Output<br />

� Variable<br />

� Text<br />

� Monitoring<br />

� Device Components<br />

Data points can be used for values and for parameters.<br />

Thus it is for example simply possible to<br />

change controller parameters dynamically with the<br />

program.<br />

Data points can be defined and administered on the<br />

different automation units (LAB/MSR Manager and<br />

display and control units (UI)).<br />

For each data point defaults for the diagram scaling<br />

and the format of numeric displays can be made.<br />

These defaults are taken over by the visualisation<br />

objects.<br />

Device components provide higher functionalities in<br />

the PI, e.g.:<br />

� application oriented controller<br />

� Integrators<br />

� Differentiators<br />

� Programmers<br />

� Device Communication etc.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

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Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Laboratory Automation Software<br />

All data objects are administrated in the onlinedatabase.<br />

Particular features of the online-database<br />

are:<br />

� Fastest known access mechanism at present<br />

� High throughput<br />

� Multi - Client / multi - server principle,<br />

expandable by further clients and servers<br />

Values, events, and text objects are stored in the<br />

history data base. For data reduction, only values<br />

which changed significantly are stored. This delta-x,<br />

delta-t procedure reduces the stored quantity of data<br />

to a minimum.<br />

Safety<br />

LabVision puts a special emphasis on safety. The<br />

Application Manager constantly checks all modules<br />

and alarms in case of a module failure, whereby the<br />

remaining general system remains stable.<br />

Numeric and other non-critical errors cause only<br />

error messages and can be treated by programming<br />

and do not obstruct the further operational sequence.<br />

HiText programs with formula errors cannot<br />

be started at all.<br />

LabVision protects, to a large extent, your parameterisation<br />

from errors when configuring and from<br />

faulty operation and incorrect input during the runtime.<br />

This is guaranteed, amongst others, by the<br />

bottom-up technique during the application establishment,<br />

the extensive use of prefabricated objects,<br />

as well as the examination of the input values.<br />

The access control with user administration prevents<br />

unintentional and unauthorised interventions.<br />

During a power failure, the system is shut down after<br />

completion of an emergency operation phase.<br />

The resource administration guarantees that during<br />

the definition of new data points, only available, i.e.<br />

existing, not already assigned interfaces are used.<br />

Deleting of a process becomes effective only after<br />

acknowledgement of at least one safety query.<br />

PI control programs are stored safely from<br />

interferences in the non volatile FLASH-memory.<br />

Even the value history can be buffered in the PI, in<br />

order to bridge brief failures of the UI (e.g. during<br />

maintenance and servicing), and to ensure a<br />

continuous documentation of the experiment/test<br />

data. The data is entered automatically with the reavailability<br />

of the UI.<br />

Special Features<br />

LabVision varies from conventional PLS in essential<br />

points. Especially significant in this regard are the<br />

relation to the capacity of the system, simple<br />

handling and transparency.<br />

Online Changeability<br />

One important feature is the capability of LabVision<br />

for online-configuration and online-parameterisation.<br />

It does not differentiate between construction phase<br />

and runtime. This means for you that, for example in<br />

case of an unplanned necessary intervention into<br />

the process or in the event of a malfunction, you do<br />

not need to shut down and reactivate your plant.<br />

This is the reason for the special suitability as FPLS<br />

for F & E applications in the laboratory or pilot plant<br />

stations. Conventional systems do not dispose of<br />

this ability. It is however indispensable for flexible<br />

and efficient operation in the laboratory or pilot plant<br />

stations.<br />

Visual Configuration Ability<br />

The visual configuration of interfaces of a LAB-<br />

Manager PNC is especially simple and comfortable.<br />

You are able to select the interface type, e.g. Pt <strong>10</strong>0,<br />

in a display of the available connection panel of your<br />

individually equipped LAB-Manager with the list<br />

selection field. The respectively suited free plug-in<br />

connections are marked. The programme proposes<br />

the first free plug-in connection via a blinking<br />

marking. You must now simply select the same or<br />

any other free connection by clicking on to it.<br />

The current and the historic values of the connected<br />

sensor are immediately available for visualisation<br />

and further processing.<br />

Even the connection of any random laboratory or<br />

analysis devices via serial interfaces can be realised<br />

in a simple way with the freely parameterisable<br />

NAMUR device component.<br />

The only data required to be entered into the entry<br />

mask are the interface parameters contained in the<br />

respective device manual.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Module Overview<br />

Laboratory Automation Software<br />

LabLision is modularly structured. The LabVision<br />

basis module SL-CLABVIS can be equipped with the<br />

depicted modules.<br />

The basis module is equipped with 30 data points.<br />

The number of data points can be adjusted to the<br />

project size accordingly. The progression is 30, <strong>10</strong>0,<br />

180, 300, 560, <strong>10</strong>00, 3000 and <strong>10</strong>000 data points.<br />

Modules and data points can be upgraded at any<br />

time. This is conducted after clearance via the<br />

download from our website server or by forwarding a<br />

data carrier.<br />

Modules as Full Versions<br />

A LabVision license contains the free update<br />

authorisation for one year. Software versions<br />

adjusted to the respective client system can be<br />

requested via download from our website server. As<br />

soon as you are entered in our E-mail list, you will<br />

automatically be informed of available new software<br />

updates for your system.<br />

The base module can be extended using the<br />

following modules in full and light-Versions:<br />

Order Code Option / Function<br />

SL-HITEXT HiText- Multi-tasking Control and Online-Evaluation<br />

SL-EASYBATCH Table based Recipe control module<br />

SL-HIBATCH Recipe control module with graphical recipe process-editor<br />

SL-ACTIONTRACK ActinnTracker to record user activaties as EasyBatch program<br />

SL-REZGEN Recipe series generator<br />

SL-DIAPROT Dialog and Protocol forms with tables incl. graphics<br />

SL-ONLGRA Full version online charts with reference curve presentation, MDI-capable<br />

SL-SCHANA Full version analogue plotter, MDI-capable<br />

SL-SCHERE Event plotter<br />

SL-SCHPHA Phase plotter<br />

SL-BERICHT Full version process report, batch orientated<br />

SL-UEBMEL Full version monitoring and reporting<br />

SL-LABCAM LabCam, Digital Camera module, event controlled digital-photo documentation<br />

SL-DESIGN Worksheet designer<br />

SL-RIEDIT P&ID-Editor according to EN/ISO <strong>10</strong>628<br />

SL-EXPORT Full version automatic data export and externally controlled<br />

SL-SELFIL Selectors and Filters<br />

SL-BENRECH Access monitoring with user administration<br />

SL-JOURNAL Parameterisable electronic laboratory notebook<br />

SL-MULTIBATCH HiBatch extension for parallel synthesis<br />

SL-MULTIPROJ Multiple starting of LabVision on one computer<br />

SL-LABVOICE Voice output for messages, alarms and HiText modules<br />

SL-EMLRUF Alarm call via e-mail (also suitable for text messages)<br />

SL-ALRRUF Alarm call via telephone call with voice message<br />

SL-PROJMOD Project modules generator and editor for LabVision<br />

SL-KALDAS3 KalDas 3.0<br />

SL-ANWINT Programmable interface for Visual-Basic, C++ or DELPHI<br />

SL-CLONLV Cloning tools for LabVision (parallel reactor system)<br />

SL-SWITCHER Administration of different versions of LabVision on one PC<br />

SL-HILIMS Laboratory information management system with local SQL Database<br />

SL-HILIMSSQL HiLIMS multi user server software without SQL server licence<br />

SL-PNKSIM Emulator for <strong>HiTec</strong> Pis (incl. HiSim)<br />

SL-WEBVIS Remote maintenance of active LabVision projects via TCP/IP<br />

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Module as Light-Version<br />

Laboratory Automation Software<br />

Different modules are also available as a lightversion.Different<br />

modules are also available as a<br />

light-version. The Light versions are dimensioned so<br />

that they are sufficient in most cases. Modules in the<br />

full version and light version can be combined.<br />

Order Code Option / Function<br />

SL-HITEXTL HiText light, 4 Programs each <strong>10</strong>0 lines<br />

SL-HIBATCHL Recipe Control-Module light with max. 20 steps<br />

SL-ONLGRAL Online charts light, 2 diagram pages each 8 curves<br />

SL-SCHANAL Analogue Plotter light with 2 plot pages each 8 curves<br />

SL-SCHEREL Event Plotter light (without hints)<br />

SL-SCHPHAL Phase Plotter light (max. 3 phases)<br />

SL-DESIGNL Designer light, one worksheet with max. 400 Visualisation-Objects<br />

SL-RIEDITL P&ID-Editor light, one worksheet with max. 120 Visualisation-Objects<br />

SL-WEBVISL WebVision light, only multi plotter visualisation<br />

SL-HILIMSL Single-User HiLIMS licence with local SQL database (max. 4 GB)<br />

LAB/MSRmanager PI-Module<br />

Order Code Option / Function<br />

SF-PIDxx xx = 4, 8, 16, 24, 32, or 64 PID controller or application oriented device components<br />

SF-HICONx x = 1, 2 ,4 or 8 fully adaptive controller<br />

SF-NAMSERxx NAMUR driver for xx = 4, 8, 16, 32, 64 or 128 serial interfaces<br />

SF-AWL Instruction List EN 61131 PLC Module , including Programming Desktop<br />

SF-AWLPLUS Extended Instruction List Module with structured Text in HiText-orinted Syntax<br />

SF-HITUNE Automatic parameterisation for PID controllers<br />

SF-ANWTAB User defined linearisation table<br />

SF-DATLOG Data Logger Function, Data Buffering in the PI in case of UI Failure<br />

SF-PNKMSR Serveral PI’s at one computer<br />

External PI Drivers<br />

Order Code Option / Function<br />

SL-PNKPERF PI-Driver for Braun Perfusor<br />

SL-PNKSPS PI-Driver for Siemens S5/S7, 3964(R) protocol and AEG Modicon<br />

SL-PNKLASENTEC PI-Driver for Lasentec FBRM - particle systems<br />

SL-PNKMTRx PI-Driver for Metrohm titrators (x = 1, 2, 4, 8 Devices)<br />

SL-FREMDPNK LabVision access module for solely foreign-PI systems (with Dongle)<br />

SL-PNKOPC PI-Diver for OPC-DA (Version 1+2), OPC-Client<br />

SL-PNKDDE PI-Driver for DDE data exchange<br />

SL-PNKMBUSSER PI-Driver for ModBus devices over serial PC interface<br />

Further PI drivers e.g. ProfiBUS- and CANBUS-systems are available upon request.<br />

Miscellaneous<br />

Order Code Option / Function<br />

SL-TELES Remote maintenance<br />

Libraries<br />

Order Code Option / Function<br />

SL-GOPBIB Basis Operation Library<br />

SL-MICROBIB Base for Ehrfeld Library (Microbib Content)<br />

SL-MODBIBALR Project Module Library for Designer, Full Version<br />

SL-BIBRILK Glass and Laboratory Devices Library for P&ID-Editor<br />

Notice: Software which is allocated to products, like KalDas is to Reaction Calorimetry, can be found in the<br />

according chapters of the respective products.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


The LabVision Base Module<br />

Laboratory Automation Software<br />

The LabVision base module is the minimum software<br />

configuration of the LabVision program system.<br />

It is sufficient for systems with small application statistics<br />

and a small degree of automation. It can be<br />

equipped with the upgrade modules in full or light<br />

versions. The number of data points can be extended.<br />

This is conducted after clearance via the download<br />

from our website server or by forwarding a data<br />

carrier. A LabVision license has a one year's free<br />

update authorisation.<br />

A minimum or demo version of some of the modules<br />

can be found in the base module. The base module<br />

is equipped with 30 data points and contains the<br />

functions:<br />

Order Code Option / Function<br />

SL-LABVIS LabVision base module with 30 data points<br />

System Requirements<br />

LabVision demands the following minimum<br />

requirements from the UI:<br />

� Single-Core CPU<br />

� 1 GB RAM (Vista),<br />

� 1 GB free hard drive space<br />

� Windows-Vista or Windows-XP<br />

� 2 button mouse<br />

� 1 x serial port or USB2Serial connector<br />

� Configuring and Parameterising<br />

� Monitoring and reporting of alarms, without<br />

reactions and long text messages 3 predefined<br />

message classes<br />

� Designer limited to one worksheet and 30<br />

visualisation objects<br />

� P&ID-Editor limited to 50 graphic objects<br />

� Online charts limited to 8 curves, one page<br />

� Analogue plotter limited to 8 curves and one<br />

axis<br />

� Progress report basic features<br />

� HiText limited to one program and 30 lines<br />

� Device components for <strong>HiTec</strong> PIs<br />

� Demo project module samples<br />

� Data export in text or table files, limited to<br />

manual start<br />

� System in German and/or English<br />

LabVision is tested exclusively on <strong>HiTec</strong> <strong>Zang</strong> UI.<br />

Perfect function is not guaranteed on other machines.<br />

Absolute necessary safe shutting down of the<br />

data base in the case of power failure can only be<br />

guaranteed with <strong>HiTec</strong> <strong>Zang</strong> UIs and UPSs.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

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Software<br />

Plant<br />

Construction and<br />

Technology<br />

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The Multi-Plotter System<br />

Laboratory Automation Software<br />

The multi-plotter is an innovative, integrated plotting<br />

system. It displays, clarity and consistency not seen<br />

until now, current and historical process conditions in<br />

the form of values (analogue plotters), events (event<br />

plotters) and process phases (phase plotters).<br />

The diagram can be printed out directly, or can be<br />

inserted into documents using the clipboard.<br />

The presented period can be changed manually,<br />

over a worksheet or a HiText program.<br />

The presented values can be directly exported to<br />

spreadsheet programs.<br />

The Analogue Plotter<br />

The analogue plotter presents the analogue values<br />

as curves. It can plot up to forty pages with 8 curves<br />

on up to 8 axes each. The representation can be<br />

randomly spread and zoomed.<br />

When reading off values, you are supported by<br />

the read-off cursor in the form of a vertical line.<br />

With a mouse-click you set the position which will be<br />

read off. The values can be read directly at the<br />

cursor or in the allocated table column below the<br />

diagram window.<br />

With the delta-t trend cursor, you set the trend<br />

display interval. In the column Value Table Trend<br />

you can directly read off the trend for each curve.<br />

The analysis cursor supports you during graphic<br />

analysis with min, max, average and gradient etc..<br />

Significant curve sections can be highlighted with a<br />

text comment after clicking on to them.<br />

The plotter can be configured online, i.e. you can<br />

create new curves and modify all settings at any<br />

time. The curves can optionally also be displayed,<br />

either linear or logarithmically, un-smoothed or<br />

smoothed.<br />

Time domains of interest can be retrieved in many<br />

ways. In connection with the export module, the<br />

presented pen recorder page can be passed for<br />

numeric value export to the export module (e.g. via<br />

Excel) with a mouse click.<br />

Order Code Description<br />

SL-SCHANA Analogue plotter (MDI), 40 pages with each 8 curves<br />

SL-SCHANAL Analogue plotter light, 1 window limited to 2 plotting pages with each 8 curves<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


The Event Plotter<br />

Laboratory Automation Software<br />

The event plotter provides a symbolic explanation of<br />

monitored events, messages, comments etc. Each<br />

occurring event is displayed with its own symbol.<br />

If the mouse cursor is moved over an event symbol, a<br />

popup will appear that will display all important<br />

information to the event.<br />

If you click on an event symbol, the progress report is<br />

opened and the appropriate plain text message with<br />

source note is displayed.<br />

Order Code Description<br />

SL-SCHERE Event plotter with clear text indication window and additional option<br />

SL-SCHEREL Event plotter light, no hint-function (no clear text indication window)<br />

The Phase Plotter<br />

The phase plotter provides a visualisation of the<br />

temporal operational sequence, e.g. the process<br />

phases or the sequence of recipe steps.<br />

It enables the direct allocation of the value curves<br />

and events to the phases (defined in plain text).<br />

Order Code Description<br />

SL-SCHPHA Phase Plotter<br />

SL-SCHPHAL Phase Plotter light, limited to 3 parallel phases<br />

The Progress Report<br />

If the mouse cursor is directed at a phase bar, a<br />

popup will appear that contains information to the<br />

event. Per mouseclick on to a phase bar, the<br />

according period in the process record will be<br />

opened.<br />

Order Code Description<br />

SL-BERICHT Progress Report, batch orientated extended search possibility<br />

In the progress report all events, values or parameters<br />

are recorded, the presentation of which as a<br />

curve would not be useful or not possible. These<br />

include comments from the operator, process messages<br />

and monitoring reports including their respective<br />

text information, pictures, and LabCam Videos.<br />

With the help of the many filter possibilities, you can<br />

also select the respective interesting information fast<br />

and safely even out of many thousands of entries.<br />

Where required, the progress report also delivers<br />

the batch protocol.<br />

The report can also be printed or exported to<br />

EXCEL.<br />

Note: The basic program only contains a progress<br />

report with simple search, export and filter<br />

possibilities.<br />

Automatic<br />

Laboratory<br />

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Plant<br />

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Technology<br />

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The Online Chart<br />

Laboratory Automation Software<br />

The online charts represent xt-diagrams. In contrast<br />

to the analogue plotters, the curves are drawn<br />

in the diagram on the left-hand side. The time axis<br />

can be marked alternatively with absolute time or<br />

relative to the start time, i.e. beginning with zero.<br />

An insertable read-off cursor supports easy<br />

reading off of the values.<br />

For online or offline comparisons, historical values<br />

or calculated values can be inserted as curves.<br />

For online and offline comparison, it is possible to<br />

blend in the historic values or calculated setpoints<br />

as curves. These reference curves can be preset<br />

out of recorded LabVision data values or Excel<br />

data files.<br />

Current Value<br />

Set Points<br />

The graphics can be printed out directly or be<br />

pasted into documents from the clip board.<br />

Additionally, the event and phase plotters can be<br />

viewed. The diagrams can be marked with a title.<br />

A memo can also be inserted for additional<br />

information.<br />

The starting time, representation period, heading<br />

and additional text as well as phase texts can be<br />

set manually or by a HiText program.<br />

The online charts module offers 40 pages with<br />

respectively up to eight curves.<br />

Respectively one axis can be placed on the right or<br />

left side of the diagram.<br />

Order Code Description<br />

SL-ONLGRA Full version Online charts with reference curve presentation, MDI-capable<br />

SL-ONLGRAL Online charts light, limited to 2 diagrams each of 8 curves, no reference curves<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Display and Control Graphics<br />

Laboratory Automation Software<br />

Your system can be driven completely from the<br />

display and control pictures in manual operation.<br />

Therefore external display and control elements<br />

are unnecessary.<br />

Even operators not educated in detail with the<br />

system are immediately able to find the significant<br />

elements and can arrange the displayed values<br />

directly.<br />

Due to the clear presentation, the operation is to a<br />

large extent self-explanatory. The operating<br />

possibilities can be limited user specifically.<br />

Therefore, also lesser qualified shift personnel can<br />

be made familiar with the operation with little time<br />

expenditure.<br />

The design scope is virtually limitless. The functionality<br />

is extraordinarily versatile: e.g. each of the<br />

display and control objects explains itself with a<br />

freely generateable text message, if the mouse<br />

cursor moves over the object.<br />

Even the control philosophy can be set. You have<br />

the choice between control objects, which can be<br />

operated directly, e.g. by clicking on to them with<br />

the mouse, or control objects, which must first be<br />

opened by clicking a (hand) symbol, to exclude<br />

inadvertent operation.<br />

Critical values can additionally be provided with an<br />

acknowledgement window. By depositing user<br />

definable RTF-formatted text and diagrams via<br />

popups, complex operating instructions or maintenance<br />

instructions can be blended in as an<br />

additional help next to the operating and display<br />

elements.<br />

The Designer<br />

The designer is your tool for setting display and<br />

control views (process pictures), protocol forms,<br />

operating panels for devices etc..<br />

In addition you do not need any special know-how<br />

or programming knowledge. Larger plant pictures<br />

can be distributed on several sides.<br />

In order to make your plant flow sheet "dynamic"<br />

you only need to draw the desired display and<br />

control objects on the worksheet and link with the<br />

appropriate data points. In the library provided you<br />

find everything from the trip switch to the pointer<br />

instrument. The visualisation objects indicate not<br />

only the value of the connected data point, but<br />

visualise also limiting and warning value violations<br />

by flashing symbols.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

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Software<br />

Plant<br />

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Technology<br />

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Laboratory Automation Software<br />

Data point names and physical units are<br />

automatically blended in and the settings of the<br />

display range etc. are automatically assigned from<br />

the associated data points.<br />

Also, complex dialogue elements like e.g. forms for<br />

inputting experimental parameters with save and<br />

load functions or with a symbol, minimizable<br />

control panels can be simply created without any<br />

programming.<br />

A freely expandable library of pre-defined display<br />

and control panels is included in the delivery.<br />

In connection with prefabricated project modules<br />

(see project modules), you gain immediately<br />

deployable visualisation objects which are already<br />

linked with the according inputs/outputs and<br />

component devices. Complete sub-projects,<br />

respectively plant basis operations can be set up<br />

and visualised in this manner with one mouse click.<br />

The used control and display components are<br />

constantly advanced and are updated to the<br />

current windows technology.<br />

In addition to the standard display and control<br />

objects, the Designer offers complex elements, like<br />

e.g.<br />

� registers for organising and grouping of<br />

extensive visualisations<br />

� panels for saving and loading of all values in a<br />

group of elements<br />

� dynamic assignment of screen position<br />

� dynamic blending in/out of visualisation objects<br />

You can create your own reusable combined<br />

visualisation objects and add them to the library.<br />

With application oriented device components<br />

typical automation specific basic functions and<br />

basic unit operatoins will be realises. The are e.g<br />

� Dosing<br />

� Vacuuum control and<br />

� reactor inside temperature control<br />

Thus a dosing circuit will be realised with a dosing<br />

device component, a balance and a pump<br />

connected to a LabManager. Instead of a balance<br />

a GraviDos weighing cell and instead of a pump a<br />

valve can be used.<br />

Up to now this functionality could only be<br />

established using a PID-controller with a programm<br />

or a ramping device component. This demanded<br />

instrumental and control knowledge to realise and<br />

parameterise the controller.<br />

The application oriented dosing device<br />

components on the other hand contain the<br />

complete controlling functionality including an<br />

option to refill receiver tank without interrupting the<br />

dosing. The parameterisation of the controller and<br />

therefore the biggest and most time consuming<br />

problem in general is completely omitted. The<br />

project modules are based on these application<br />

oriented device components.<br />

Further information can be found under PI-<br />

Firmware-Modules.<br />

Order Code Description<br />

SL-DESIGN Designer<br />

SL-DESIGNL Designer light, limited to 1 worksheet with 400 visualisation objects<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


LabVision ® Project Modules<br />

Laboratory Automation Software<br />

Establishment of Automation Projects in Record Time!<br />

The LabVision Project Module Technology marks a<br />

new generation of automation software of yet unknown<br />

user-friendliness and functionality.<br />

Project modules enable the visual establishment of<br />

projects with preconditioned, ready to function modules<br />

per Drag and Drop Technology. This means<br />

that a project is established by moving the required<br />

modules of the needed functionalities out of a<br />

browser window on to the work sheet.<br />

Project modules are combined out of different<br />

LabVision objects, e.g.:<br />

� Data Points<br />

� Device Components<br />

� Operating Objects<br />

� Visualisation Objects<br />

� Monitoring Objects<br />

� HiText Programmes<br />

� Pen Recorders etc.<br />

Completed project modules of the most common<br />

configurations are available as a library. These<br />

merely require to be adjusted to the hardware<br />

equipment in the course of importing. This significantly<br />

shortens the development period for<br />

projects.<br />

Examples:<br />

Reactor Rectification Column<br />

Dosing Module Tempering Unit<br />

Stirring Drive Stirrer Blade<br />

Distillate Weighing Vacuum Control<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 153<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


154<br />

Laboratory Automation Software<br />

Due to a library administration of the generated<br />

project modules, it is possible to easily secure and<br />

transmit various work statuses of a module in a<br />

compressed data file analogue to LabVision Project<br />

Administration.<br />

A gravimetric dosing module, for example, consists<br />

of a dosing regulator, the data points for the scales,<br />

pump and cut-off valve, the respective monitoring<br />

and the graphic display and operating objects. In<br />

comparison to conventional work procedures, the<br />

project establishment time shrinks from a few days<br />

to a few, which is especially effective in case of<br />

frequently changing assemblies to a point where the<br />

expenditure in time and effort can be neglected.<br />

Even users with limited automation experience can<br />

securely establish a demanding automation project.<br />

The project modules bring along the required<br />

process measurement and control functions and<br />

visualisation elements. This means that the data<br />

points, for the inputs and outputs, the control<br />

components, the user interface etc, are<br />

automatically applied and can be immediately<br />

deployed.<br />

An Example:<br />

A 1 litre plant with a stirred reactor, a gravimetric<br />

dosing, vacuum control, rectification and distillate<br />

weighing is intended for automation.<br />

The required modules are merely pulled over from<br />

the browser window on to the work sheet.<br />

A display for operating and monitoring combined out<br />

of the project modules then looks as follows:<br />

After the parameters of the regulator modules, for<br />

temperature, dosing and vacuum have been set with<br />

the help of the automatic parameterisation function,<br />

the plant can already be run via the operating display<br />

in flow chart presentation.<br />

The performance of the project module is illustrated<br />

in the following example. The projected screen has<br />

been created in under <strong>10</strong> minutes.<br />

The ALR (Automatic Laboratory Reactor) Project<br />

Module Library contains all required modules for the<br />

automation project establishment of a flexible<br />

laboratory reactor system:<br />

� Temperature Regulation cascade with<br />

Thermostat<br />

� Gravimetric or volumetric Dosing<br />

� Solid Dosing<br />

� Vacuum Regulation<br />

� pH Regulation<br />

� Distillation<br />

� Rectification<br />

� Crystallisation<br />

� Hydration<br />

� Phase Separation<br />

� Sample collector<br />

� Stirring etc.<br />

A project established on the basis of a project<br />

module library is HiBatch compatible. This means<br />

that it can be used as a basis for the recipe control<br />

system and the basis operation library.<br />

Already deployed modules are marked in colour in<br />

the project module browser of the library.<br />

The modules can be shared, so that e.g. an<br />

expansion by further dosing circuits can be easily<br />

realised.<br />

The data points for the connection of the required<br />

scales, pumps, and valves are applied automatically.<br />

The technical documentation can be established<br />

automatically by the push of a button.<br />

The context menus of the individual modules, which<br />

can be reached by pressing the mouse on the right<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

side, contain a graphic display of the connection<br />

panels of the LabManager, which then displays on to<br />

which plug-in positions the required instrumenting<br />

components, such as scales, stirrer drive,<br />

thermostat, valves etc. need to be connected.<br />

The user interface is extremely functional. By<br />

clicking on to the hand symbols of the operating<br />

objects the parameterising dialogues are opened.<br />

This prevents that unintended operation actions are<br />

triggered unintentional mouse clicks.<br />

As the project modules are based on the standard<br />

design objects, they can be randomly arranged or<br />

Projectmodule Libraries:<br />

extended/upgraded by the user. The module library<br />

is aligned to <strong>HiTec</strong> <strong>Zang</strong> instruments and laboratory<br />

devices, but can also easily be adapted to other<br />

components.<br />

►<br />

Projecting could not be easier!<br />

Order Code Description<br />

SL-MODBIBALR ALR-Project Module Library for Designer, Full Version.<br />

All project modules of the light library and additionally<br />

- Stirring misc. actuators (Output of a setpoint rm to a stirrer and torque display)<br />

- volumetric dosing with analogue controlled pump<br />

- gravimetric surge dosing with GraviDos (Demands: amount)<br />

- gravimetric amount dosing with GraviDos (Demands: amount, time)<br />

- gravimetric flow rate dosing with GraviDos (Demands: dosing rate, time)<br />

- gravimetric conti dosing with GraviDos (Vorgabe: dosing rate)<br />

- Destillation (Destillation with jacket temperature control)<br />

- Rectification (multilevel destillative seperation)<br />

- Christalisation<br />

- Gasing with MFC<br />

- Flow rate counter/Integrator for gas meter and flow through sensor<br />

- Calotrend (simple online Flow-calorimetry)<br />

- Titration<br />

- Filling<br />

SL-MODBIBALRL ALR-Project Module Library light for Designer<br />

- pumping with LabDos and SyrDos<br />

- pH_control (pH-value-control for base and/or acid dosing)<br />

- Inerting (establish inerte atmosphere by continued vacuumation / inerting)<br />

- volumetric dosing with LabDos a. SyrDos<br />

- gravimetric surge dosing with GraviDos (Demands: amount)<br />

- gravimetric amount dosing with GraviDos (Demands: amount, time)<br />

- gravimetric flow rate dosing with GraviDos (Demands: dosing rate, time)<br />

- gravimetric conti dosing with GraviDos (Vorgabe: dosing rate)<br />

- temperature control with thermostat and temperature cascade controller<br />

- SoliDos (Solid dosing with SoliDos)<br />

- Stirring with ViscoPakt (Output of a setpoint to a stirrer and torque display)<br />

- Inerting (Inlet of intergas)<br />

- Vacuum control<br />

- Reflux destillation<br />

- Automatic phase seperation with PhaSep<br />

- Automatic sample taking and filling with AutoSam and LabDos or SyrDos<br />

Order Code Description<br />

SL-PROJMOD Project Module Generator (Generation of Project Modules)<br />

SL-MODBIBALR ALR-Project Module Library for Designer, Full Version.<br />

SL-MODBIBALRL ALR-Project Module Library light for Designer with Dosing, Tempering, Stirring, Vacuum<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 155<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


156<br />

P&ID-Editor<br />

Laboratory Automation Software<br />

The P&ID-Editor Software Module for LabVision<br />

(modulename RI-Editor) is mainly identical with the<br />

stand-alone Version RiCAD. In LabVision, it is possible<br />

to dynamise the piping and instrumentation<br />

diagram (P&ID) with the Designer, this means provide<br />

the same with display and operating elements,<br />

and use them as user interfaces.<br />

The P&ID-Editor (linked in to the Designer) was<br />

specially developed for drawing control flow sheets<br />

according to the EN ISO <strong>10</strong>628 standard. It serves<br />

for the creation of the static background images of<br />

display and control diagrams.<br />

In the tool palette you will find all the necessary<br />

drawing tools.<br />

This tool can also be expediently put to use during<br />

the planning stage for „standard conforming“<br />

drawing of the plant.<br />

The library elements contain additional information,<br />

which can be freely expanded by e.g. suppliers or<br />

with maintenance information.<br />

Universities and other educational institutions may<br />

request a free RI-CAD version including library!<br />

Order Code Description<br />

SL-RIEDIT Piping and instrumentation diagram (P&ID) Editor<br />

SL-RIEDITL Piping and instrumentation diagram (P&ID) Editor Iight, limited to one worksheet with max.<br />

120 graphic objects<br />

Laboratory Components Library<br />

The library SL-BIBRILK for the P&ID-Editor contains<br />

presentations of the components in a laboratory<br />

reactor system which are more detailed and more<br />

realistic than in the EN ISO <strong>10</strong>628 library for the<br />

P&ID-Editor.<br />

Here you will find the glass reactors in varying<br />

constructions and sizes and glass devices like reflux<br />

separators, coolers, containers etc. also other lab<br />

devices in a descriptive form.<br />

Order Code Description<br />

SL-BIBRILK Glass and lab devices library for P&ID-Editor<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Monitoring and Reporting<br />

Laboratory Automation Software<br />

In the register monitoring/reporting you are able to<br />

define your monitoring conditions and different<br />

reporting options.<br />

If one of the specified monitoring conditions is<br />

fulfilled, this is entered in the monitoring report<br />

(extended alarm journal) and in the progress report,<br />

as is the going and the acknowledging of the<br />

monitored event.<br />

Extended Monitoring and Reporting Module<br />

Complex plants require sophisticated, flexible alarm<br />

strategies. For this reason the extended alarm<br />

module was developed. In this way, various reactions<br />

to limit and warning value violations can be<br />

established by the user.<br />

As monitoring conditions, beyond the usual static<br />

comparisons of limit and warning values, dynamic<br />

comparisons between data points or fault conditions,<br />

e.g. conductor breakage, can be set.<br />

Both the message and the confirmation are recorded.<br />

In case of important alarms a horn, for example,<br />

can be switched on or a control program can be<br />

started for the selective processing of the incident.<br />

Certain notifications of emergency can alternatively<br />

be shown delayed.<br />

Order Code Description<br />

SL-UEBMEL Extended monitoring and reporting module<br />

In the message report, the danger and warning<br />

messages are listed and acknowledged, if necessary.<br />

In the lower table window, the current messages are<br />

always indicated. The upper table is for acknowledging.<br />

As needed, it can be filtered and scrolled,<br />

in order to show previous messages outside of the<br />

represented range.<br />

Projectable message categories make it possible to<br />

establish the message behaviour of the categories<br />

centrally<br />

� Danger report<br />

� Warning report<br />

� Operation report<br />

and optionally user-defined message categories.<br />

The standard version is part of the LabVision Basic<br />

Module.<br />

For a better overview, the user can have the notifications<br />

of emergencies sorted, e.g. according to the<br />

message time.<br />

Alarms and messages, as well as acknowledgement<br />

requiring and non-acknowledgement requiring<br />

messages are differentiated.<br />

� User defined report categories<br />

� Long text reports<br />

� Complex alarm handling by control program<br />

As an addition for this module, telephone, fax, and<br />

E-mail are available.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 157<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


158<br />

Multi-LabCam System<br />

Laboratory Automation Software<br />

Certain process conditions and events can be best<br />

documented photographically. Examples are collections<br />

of turbidity, colour change, precipitation, etc..<br />

The modern server system architecture permits the<br />

integration of several different image sources<br />

(LabCams, Videostreams etc.) which can be<br />

provided by the own PC or by completely different<br />

computers.<br />

The LabCam module offers the possibility to document<br />

visual procedures automatically event-controlled<br />

or in programmed intervals and by manual triggering<br />

as digital pictures or videos. The digital pictures<br />

are inserted reduced in size into the progress<br />

report.<br />

A photo in full size or the recorded video is displayed<br />

by clicking with the mouse. The current live images<br />

can be integrated in work sheets and are also available<br />

in WebVision Modules for remote diagnostics<br />

without restriction.<br />

The image files are freely available for further use.<br />

� Documentation of visual statuses and events<br />

� Monitoring of the system from the office<br />

� Visual remote monitoring<br />

Cameras with a higher resolution are available upon<br />

request. Individual cameras (only photo function,<br />

without video recording function, as well as without<br />

programmable image trigger or WebVision support)<br />

can also be connected directly to the LabVision<br />

computer without the auxiliary module depicted<br />

above.<br />

A Multi-LabCam generates completely new<br />

possibilities!<br />

Order Code Description<br />

SL-LABCAM LabCam, Digital-Camera Module, event controlled digital-photo and video documentation<br />

CP-DIGICAM1 Digital-Camera, resolution 640 x 480 points, color<br />

CP-DIGICAM2 Digital-Camera, resolution <strong>10</strong>24 x 768 points, color<br />

Telephone-Alarm Call<br />

With the help of the telephone alarm call module,<br />

telephone calls can be triggered automatically with<br />

defined events. Event-dependent, one or several<br />

texts can be announced. In addition, the announcement<br />

of current measured values is possible.<br />

A library of letters, numbers and standard words are<br />

included. Optionally, further words and complete<br />

sentences can be added customer-specifically.<br />

In a control program, one or more telephone<br />

numbers can be called as a reaction to a certain<br />

event e.g. staff on call during plant disturbance or<br />

the service personnel after completion of batch can<br />

be called and the appropriate message announced<br />

in plain language.<br />

Order Code Description<br />

SL-ALRRUF Telephone alarm call with speech output<br />

Furthermore, it is possible, depending on date and<br />

time, to activate different call numbers, so that an<br />

on-call service can be arranged in advance even<br />

over several days. If unexpected deviations arise,<br />

e.g. as a result of illness, the settings can also be<br />

changed by remote maintenance.<br />

The confirmation of the received call is entered in to<br />

the progress report by key code.<br />

☞ Required is the option SL-HITEXT(L)<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


E-mail Alarm<br />

Laboratory Automation Software<br />

E-mail messages, as prepared event-dependent<br />

texts, can be sent to different e-mail addresses and<br />

forwarded to you mobile phone as text message<br />

Order Code Description<br />

SL-EMLRUF Alarm Call by E-mail<br />

Control and Online-Evaluation<br />

In the field of control and online evaluation,<br />

LabVision is a class of its own. Available are the<br />

graphical recipe procedure control EasyBatch and<br />

HiBatch, the plain text language HiText, Instruction<br />

List according to EN 61131, and AWLplus with<br />

structured text in HiText-oriented syntax (see PI-<br />

Firmware Modules) and the device components (see<br />

LabManager-System, System Construction). This<br />

offer considers the realisation, that depending upon<br />

your problem definition, each programming type<br />

disposes of its special specific suitability.<br />

HiText The Universal Text Language<br />

HiText is a plain text language for control, onlineevaluation<br />

and communication. HiText was developed<br />

in cooperation with users from the chemical<br />

industry with the aim to achieve a self explanatory<br />

and self-documenting language, useful for everyone.<br />

As also users with no programming experience are<br />

able to learn HiText in a short time, the language<br />

enjoys highest acceptance, in particular for the<br />

applications in laboratories and pilot stations.<br />

The module contains a comfortable editor with many<br />

helpful functions, a multitasking capable interpreter<br />

and a process visualisation tool with debugging<br />

assistant.<br />

The syntax check takes place direct during the input.<br />

by the control program as a reaction to certain<br />

incidents.<br />

☞<br />

Required is the option SL-HITEXT(L) and an<br />

internet access.<br />

Programming of Algorithms<br />

Algorithms are best programmed in HiText with<br />

English key words. Example: Calculations,<br />

programmed relationships (If..., then...).<br />

In the German version, German language elements<br />

are used instead.<br />

Programming Processes/Recipes<br />

Processes/Recipes can be programmed in text form<br />

in HiText, table based in EasyBatch or graphically as<br />

HiBatch sequences to NAMUR and EN/IEC<br />

standards.<br />

Errors are underlined and are clearly marked. Only<br />

formal error free programs can be started.<br />

For the calculation of mathematical expressions<br />

there are, apart from the basic functions, all<br />

important mathematical functions available. Setpoint<br />

value specifications for controllers can be created<br />

with random progression (Profile).<br />

The common control types<br />

� Logic control<br />

� Process control<br />

� Timing control<br />

can be implemented also in mixed form.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 159<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


160<br />

Laboratory Automation Software<br />

HiText is multitasking capable, i.e. several programs<br />

can run at the same time. Therefore you can clearly<br />

separate different tasks such as process control,<br />

monitoring, executing necessary reactions, online<br />

analysis etc. and retain the overview even in complex<br />

projects.<br />

For example, specifications of temperature ramps do<br />

not have to laboriously be interwoven in a single<br />

sequential program during simultaneous monitoring<br />

of a pH and a temperature window. Rather, each<br />

individual function is formulated as its own program,<br />

whereby in particular the re-usability of modules and<br />

the long-term maintainability are ensured.<br />

A HiText program is self-explanatory and self-documenting,<br />

so that you can attach it directly as documentation<br />

of the process cycle to your GMP or GLP<br />

documents.<br />

You can follow, interrupt, start and end the program<br />

progression online in the editor window. The values<br />

can even be changed during the run-time. In addition,<br />

you can also use variables instead of numbers,<br />

the values of which are allocated using the<br />

dialog forms or files.<br />

If necessary, a HiText program can co-operate with a<br />

subordinate PLC, an IEC 61131 IL-PI control program<br />

or device components and take over the<br />

function of a superordinate group control level.<br />

Common data points (variables) enable an uncomplicated<br />

data exchange with the PI.<br />

Beyond that, the modules of the HiBatch basic<br />

operations library are written in HiText. The user can<br />

Order Code Description<br />

SL-HITEXT HiText Full version<br />

SL-HITEXTL HiText light, max. 4 Programs each <strong>10</strong>0 lines<br />

therefore program new unit operations themselves<br />

and extend the library.<br />

HiText Language Elements<br />

The tab card language elements contain the<br />

available commands.<br />

You create a HiText program, by dragging the language<br />

elements or instructions simply with the<br />

mouse into the word processor window or by entering<br />

them directly using the keyboard.<br />

In the tab card functions you will find functions of the<br />

areas: arithmetics, trigonometry, text, and time/date.<br />

These functions support the implementation of<br />

online analysis programs and timing control etc.<br />

The following program example shows you how<br />

easily HiText is to understand and to apply:<br />

The command lines Output "...." to Report create the<br />

following entries in the progress report, which are<br />

automatically provided with a time stamp.<br />

This short example can only offer a first impression<br />

of the user-friendliness and only a small section of<br />

the capabilities of HiText and LabVision.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Dialogue and Protocol forms<br />

Laboratory Automation Software<br />

Protocol forms with display and input objects,<br />

diagrams, graphics, switches etc. can be created<br />

with the graphical editor, without even having to<br />

program a single line. These forms can not only be<br />

used for online-presentation of the data, but also as<br />

an extension to printed documents.<br />

Together with HiText you can automatically evaluate<br />

your experiment and present it directly in a suitable<br />

form.<br />

To every diagram there is a value table, which<br />

contains all the presented values and using the<br />

HiText program or manually this can be edited for<br />

further use.<br />

The form of the diagrams can be adjusted and fitted<br />

in many ways:<br />

� Multi axis, x-t, x-y<br />

� Multi-curves<br />

� Multi-diagram<br />

� Curve attribute lines, plot symbols<br />

� Fill areas<br />

� Subsidiary Lines<br />

� Linear or logarithmic scaling<br />

� Auto scaling<br />

Order Code Description<br />

SL-DIAPROT HiText Dialog and Protocol forms with diagram and tables<br />

The dialog and protocol masks are also being used<br />

within the electronic laboratory journal.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 161<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


162<br />

Laboratory Automation Software<br />

EasyBatch and ActionTracker- Table-based Recipe Control<br />

Recipe Control – The easy Way!<br />

EasyBatch<br />

Reproducibility and clear documentation of a test<br />

procedure are the requirements to assure quality<br />

and to reduce development times. This can only<br />

be reached in the scope of reasonable expenditure<br />

through automation of the procedure already in the<br />

research laboratory. Up to now, only the text-based<br />

language HiText or the graphical sequential function<br />

chart Hibatch were available for programming.<br />

As a new option of unmatched simplicity, EasyBatch<br />

is now available. EasyBatch enables uncomplicated<br />

table-based and and self-documenting<br />

programming. The operation can be conducted on<br />

an intuitive basis. EasyBatch can also be used in<br />

combination with the manual operation mode and<br />

ensures reproducibility in an easy manner.<br />

EasyBatch is even simpler to handle as HiText and<br />

HiBatch and is in particular suited for the<br />

programming of processes of simple to medium<br />

complexity.<br />

EasyBatch is also ideally suited for the control of<br />

fermenters, microreaction technology plants, and<br />

robots.<br />

An own table column is provided for all parameters<br />

and values, such as times and amounts, intended<br />

for regulation. The first column contains the order to<br />

be performed. In the simplest case, a programme<br />

only consists of set and wait orders. It represents<br />

recipe establishment without the necessity of<br />

programming knowledge and a minimum<br />

expenditure of time.<br />

� More time for Core Tasks due to a more<br />

efficient Mode of Operation<br />

� Automatic Test Control , also during the Night<br />

and Weekends<br />

� Modification of the Programme Parameters<br />

and the Procedure also during the actual Run<br />

Time is possible<br />

� Ideal Documentation due to consistent and<br />

complete Recording of Measurement Values,<br />

Sequences, Events and manual Interventions<br />

� Supports the GLP and GMP-conform<br />

Operation Mode<br />

Command Description<br />

Wait Programme waits until the time set in the parameter column hh:mm:ss has expired before executing next line<br />

Wait for Programme waits for the fulfillment of the condition in the the parameter column before executing next line<br />

Wait until Programme waits until /for the stated date or time before executing next line<br />

Set Allocates the respective values stated in the current line to the data points stated in the column head<br />

Ramp Establishes ramps for all setpoint values in the time stated in the parameter column to the end values stated in the<br />

current line<br />

Start Starts the HiText programme stated in the parameter column<br />

Stop Stops the HiText programme stated in the parameter column<br />

Pause Interrupts the HiText programme stated in the parameter column<br />

If Branches out to the stated programme line, if the condition in the parameter column is fulfilled<br />

Continue if Branches out without condition to the programme line stated in the column „line“<br />

Acknowledge Opens a window containing the message stated in the parameter column and interrupts the programme until the<br />

operator acknowledges (click on to OK)<br />

Full flexibility is reached through further commands<br />

such as „Wait until“, „Ramp“, If , The<br />

table listed below, depicts the commands in detail.<br />

As a special solution, HiText programmes can be<br />

integrated into the procedure, which are controlled<br />

with the programme Start/Stop/Pause.<br />

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Laboratory Automation Software<br />

The command parameters, such as time intervals,<br />

conditions, e.g. "pH > 6,5" or a HiText programme<br />

name are entered into the parameter column. The<br />

last column, if necessary, serves for the entry of<br />

comments by the operator for relevant information<br />

which can not be automatically captured.<br />

In the MultiWriter, occurring events, values and<br />

sequence phases are consistently presented.<br />

A batch protocol containing all events, operation<br />

interventions, value modifications etc., can be<br />

established and archived automatically in HiLIMS.<br />

This warrants for the ideal backup of test results and<br />

reproducibility at any time.<br />

The LabVision Project Modules represent the ideal<br />

basis for EasyBatch. The deployed modules<br />

automatically allocate the EasyBatch programme<br />

table so that the laboratory work can be immediately<br />

commenced after a project has been established.<br />

The EasyBatch Module is therefore the ideal tool to<br />

automate frequently changing applications with<br />

minimum expenditure.<br />

ActionTracker Action Recorder<br />

The operator operates the plant manually with the<br />

help of the operating screen. All setpoint value<br />

modifications are automatically recorded in the table.<br />

All value modifications are added as a line of the<br />

table by the ActionRecorder. Consequently, there is<br />

a clear and reproducible description of the actual<br />

procedure in table form available at the end of each<br />

process. In other words: A workable programme is<br />

automatically established by the operating activities<br />

of the operator without the necessity of any further<br />

action.<br />

The chain of activities recorded in table form can<br />

now be automatically repeated without any further<br />

effort. It is possible, during the run time or before the<br />

repeated start of the table, to enter intervals,<br />

setpoints, comments, conditions etc.<br />

Usually, before repeated execution, the table is<br />

edited to consolidate the same. Setpoints which<br />

were modified shortly after another can be<br />

summarised in one line and certain operatorsupported<br />

tasks such as the reaching of a certain<br />

value (in this case: Wait pH > 7) can be integrated<br />

into the programme.<br />

If values are modified by the operator during<br />

realisation, the table is automatically accordingly<br />

adjusted. This ensures that the procedure is<br />

documented and reproducable <strong>10</strong>0% at any given<br />

time.<br />

Order Code Description<br />

SL-EASYBATCH Table-based Recipe Control<br />

SL-ACTIONTRACK ActionTracker for the Recording of Operation Activities as EasyBatch Programme<br />

Remark: EasyBatch and ActionTracker require SL-HITEXT(L) and SL-DIAPROT.<br />

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Laboratory Automation Software<br />

HiBatch Recipe Control and Administration<br />

Reproducibility and clear documentation of an<br />

experimental process are the conditions for<br />

increased quality and shortening of development<br />

times. The basis for this is the automation of the<br />

procedure even in the development laboratory.<br />

The recipe module HiBatch, available as extension<br />

to HiText, enables the creation of recipe flow<br />

diagrams by linking unit operations with the help of a<br />

graphical recipe editor. HiBatch is even simpler to<br />

handle than HiText. Even complex recipe flow diagrams<br />

can be created to IEC and NAMUR norms in<br />

clear form with minimum time expenditure. By<br />

clicking an operation in the flow diagram you open<br />

the appropriate dialog form, in order to input parameters<br />

and values such as quantities and times.<br />

A unit operation can be used several times, also<br />

parallel or at the same time. The process plan is<br />

checked and executed automatically. The active<br />

steps are colour indicated and freely selectable<br />

control values are displayed directly in the flow<br />

diagram.<br />

Whole experiment series can be run automatically in<br />

series on one reactor or parallel on multiple reactors.<br />

With a unit operation library to the NAMUR standard,<br />

application of the recipe control program HiBatch<br />

gives you a number of further advantages:<br />

� Recipe creation without programming<br />

knowledge in minimum time<br />

� More time for qualified base activities from<br />

more efficient work methods<br />

� Automatic experiment control, also over night<br />

and at the weekend<br />

� Changing of program parameters and the<br />

procedure even possible during runtime<br />

� Optimal documentation by complete<br />

recording of measurement data, procedures,<br />

events and manual intrusion<br />

� Simplified and safe transfer of the EMSR-<br />

Know-How from the lab to pilot plant and the<br />

production stage<br />

� Supports the GLP and GMP suited methods<br />

The input parameters are checked with freely<br />

definable plausibility criteria and if necessary,<br />

corrected. The parameter sets can be saved for<br />

further future use.<br />

Also for running recipe process control, you can still<br />

change the parameters and temporarily interrupt the<br />

process at any time, e.g. for manual actions.<br />

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Laboratory Automation Software<br />

Thanks to the open programming in HiText the<br />

system can be added to without problems using<br />

preloaded and saved functionalities, e.g. a scaling<br />

function for the basis recipe, automatic<br />

parameterisation of whole series of experiments,<br />

automated evaluation, or administration of the<br />

parameters and results.<br />

You can write your own basic operations with HiText<br />

or make use of the basic operations library (SL-<br />

GOPBIB). For the establishment of special basic<br />

operations you may call upon our respective<br />

services offered.<br />

In the multi-plotter, events, values, and process<br />

phases are consistently presented.<br />

A batch protocol with all events, operator<br />

interventions, value changes etc. is automatically<br />

established. This guarantees an optimal<br />

reproducibility of the process even after manual<br />

interventions.<br />

The electronic laboratory journal eJournal and the<br />

laboratory information management system HiLIMS<br />

complete HiBatch. They create a consitent process<br />

chain from the contract to the control of the complete<br />

R&D process to the final report.<br />

For simpler applications EasyBatch might be of<br />

choice.<br />

Note: HiBatch requires HiText.<br />

Order Code Description<br />

SL-HIBATCH Recipe control module with graphical editor<br />

SL-HIBATCHL Recipe control module with graphical editor, Light-Version, limited to 20 steps<br />

SL-HIBATCHAP Recipe control module with graphical editor for closed basic operations library<br />

SL-HIBATCHRT Recipe control runtime module, limited to running and parameterisation of recipe process<br />

plans<br />

Additionally recommende modules:<br />

Order Code Description<br />

SL-GOPBIB <strong>HiTec</strong> Basic Operations Library for HiBatch<br />

SL-GOPBIBL <strong>HiTec</strong> Basic Operations Library Light for HiBatch<br />

SL-SCHERE Event plotter<br />

SL-SCHPHA Phase Plotter<br />

SL-BERICHT Extenderter Ablaufbericht mit Batch/Rezeptur-Filter<br />

SL-JOURNAL Parametrierbares elektronisches eLabor-Journal<br />

SL-HILIMSL Single-User HiLIMS licence with local SQL database (max. 4 GB)<br />

SL-HILIMS Laboratory information management system with external SQL-database<br />

Please note our discounted<br />

Software packages with their proven module collection.<br />

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166<br />

Basic Operations Library<br />

Laboratory Automation Software<br />

With the <strong>HiTec</strong> <strong>Zang</strong> basic operations library you<br />

have a tool at hand, with which you can respond<br />

quickly and flexibly to continuous new demands.<br />

The progress program is arranged out of standard<br />

components. Therefore, even a synthesis of high<br />

complexity can be programmed with minimum time<br />

expenditure.<br />

The elements of the basic operations library are<br />

written in the self-documenting language HiText.<br />

Therefore you can make randomly many individual<br />

adjustments by changing the control program.<br />

Likewise, you can also edit the dialogue forms with a<br />

comfortable Designer where necessary.<br />

If required, our application developers can create<br />

further basic operations according to your<br />

requirements.<br />

The basic operations are available individually or as<br />

a library.<br />

Basic Unit Operations:<br />

Order Code Description<br />

SL-GOPBIB <strong>HiTec</strong> Basic Operations Library for HiBatch<br />

- Pressure (the program controls a pressure regulation with setpoint ramp)<br />

- Pressure_Hold (simple pressure regulation)<br />

- Vacuum_Hold (vacuum control)<br />

- Control Program (types or versions of a control program)<br />

- SoliDos (solid dosing with SoliDos)<br />

- PH_Regulation (pH-value-regulation for base and/or acid metered addition)<br />

- Inert_Establish (establishment of inert atmosphere by repeated drawing of vacuum/inerting)<br />

- Fill (metered addition without regulator)<br />

- Distilling (distillation with jacket -temperature regulation)<br />

- Weighing-in (weighing in by hand with reporting)<br />

- Inerting (addition of inert gas )<br />

- Reflux Distillation (waiting for setpoint temperature and initialised time )<br />

- Boiling Point Recognition of boiling points for subsequent distilling)<br />

- Rectifying (control of a rectification column)<br />

- Vacuum (program to run vacuum ramps)<br />

- Repeat (determines the number of passes of a recipe cycle)<br />

- Wait_Condition (waiting until freely-definable condition is fulfilled)<br />

- Wait_Operator (waits for acknowledgement by operator)<br />

- as well as all basic operations of the options SL-GOPBIBL<br />

SL-GOPBIBL <strong>HiTec</strong> Basic Operations Library Light for HiBatch<br />

- Surge_Doser (fastest possible gravimetric dosing of the stated amount)<br />

- Batch Amount_Doser (gravimetric dosing of the stated amount within the stated time)<br />

- Batch Rate_Doser (gravimetric dosing at the stated rate during the stated time )<br />

- Conti (-nuous) Doser (continuous dosing with consistent dosing rate)<br />

- Temperature_Hold (temperature control)<br />

- Dosing (gravimetric dosing)<br />

- Dosing_Gravi (gravimetric dosing from load cell, without refilling)<br />

- Final Operation (end step of recipes with export possibilities)<br />

- Stirring (input of a setpoint temperature to stirrer)<br />

- Initial Operation (start/initial step for a recipe)<br />

- Taring_Gravi (taring of a load cell)<br />

- Taring_Scales (taring of a scales)<br />

- Tempering (program to run heating and cooling ramps)<br />

- Value Output (output of a new value to a data point)<br />

- Wait (taking of adjustable idle time)<br />

- Wait_Until (waiting for the set point of time)<br />

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Individual Basic Operations:<br />

Laboratory Automation Software<br />

Order Code Basis Operations Description<br />

SL-GOPBEFUEL Fill Charge dose without controller. The pump power is reduced towards the<br />

end of the dose automatically to come as accurate as possible to the desired<br />

amount.<br />

SL-GOPDEST Distil Distillation with jacket temperature regulation.<br />

The setpoint value for the jacket temperature results from the current reactor<br />

inner temperature plus the setpoint difference between inner and jacket<br />

temperature. The setpoint difference between inner and jacket temperature<br />

is given by the user. Small setpoint differences mean sparing distillation!<br />

The reflux fraction ratio can be controlled dependent of the head<br />

temperature.<br />

SL-GOPDOSI Dose Gravimetric dosing of one balance with setpoint value ramp and controller.<br />

SL-GOPDOSIGRAVI1 Dose_Gravi1 Gravimetric dosing from one load cell (e.g. Hitec <strong>Zang</strong> GraviDos) with set<br />

value ramp and controller. Without refilling of the feed tank.<br />

SL-GOPDPWERT Value Output Output of a new value to a data point<br />

SL-GOPDRUCK Pressure The program controls a pressure regulation.<br />

The setpoint is controlled via ramp to the final value.<br />

SL-GOPDRUCKHALTEN Pressure Hold The program controls a pressure regulation.<br />

The predetermined setpoint is directly issued to the regulator.<br />

Transition is possible according to time or through structural transition (e.g. if<br />

a parallel path is completed).<br />

SL-GOPEINWIEG Weighing Weighing of a substance "manually". The weighed quantity is recorded to<br />

the progress report.<br />

SL-GOPEND Final Operation This operation serves as final step for recipes.<br />

There is the possibility to automatically start an arranged export out of this<br />

recipe step. As time period for the export, the period from the start of the<br />

recipe and the start of the export is applied. Prerequisite for the function of<br />

the export is the utilisation of the initial operation out of the basic operation<br />

library, as well as the full version of the data export module.<br />

SL-GOPGRAVITARI Taring_GraviDos Program for resetting a load cell (e.g. Hitec <strong>Zang</strong> GraviDos)<br />

SL-GOPINERT Inerting The program serves to open a binary and proportional inerting valve. It can<br />

optionally be opened for a certain period or as long as a parallel path is<br />

running.<br />

SL-GOPINERTHERST Inert_Provision To provide an inert atmosphere by n-fold turning vacuum pulling /inerting to<br />

pressure with vacuum control<br />

SL-GOPKALOHEIZ CaloHeater The program is used to control a calorimetric heater (e.g. <strong>HiTec</strong> <strong>Zang</strong><br />

KaloHeiz). Thereby, a defined heat load can be switched on to the reactor for<br />

a certain time period.<br />

SL-GOPKALOONL OnlineCalo The program offers simple online reaction calorimetry evaluation.<br />

SL-GOPKONTIDOS Continuous_ Doser Continuous gravimetric dosing with consistent dosing rate.<br />

SL-GOPMENGENDOS Batch amount Doser Gravimetric dosing of the stated amount in the stated period of time.<br />

SL-GOPPHREGELUNG pH Control PH Value Control for base and/or acid metered addition via pH value<br />

regulator. Transition is possible after reaching a pH tolerance limit or through<br />

structural transition (e.g. if a parallel path is completed).<br />

SL-GOPPROGRAMM Control Program Starting or execution of a HiText program<br />

SL-GOPRATENDOS Batch Rate Doser Gravimetric dosing with the stated rate during the stated period of time<br />

SL-GOPREKTIF Rectification Fractionated distillation, discharge of several fractions, control according to<br />

temperature or pressure difference. Consistent linear or exponential column<br />

head control.<br />

SL-GOPRUECKDEST Reflux destillation The programm will wait until the next initialised setpoint temperature during<br />

the destillation is reached and then waits for a certain amount of time.<br />

SL-GOPRUEHR Stirring The program gives as an output the setpoint rotational speed of a stirrer.<br />

Stirring can either take place for a certain time or until a parallel step is<br />

complete.<br />

SL-GOPSIEDEP Boiling Point This program offers the detection of boiling points (e.g. for following<br />

distillation).<br />

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Individual Basic Operations (continued):<br />

Laboratory Automation Software<br />

Order Code Basis Operations Description<br />

SL-GOPSTART Initial Operation Start step for a recipe with the possibility to carry out initialisations and<br />

settings.<br />

SL-GOPSTOSSDOS Surge_Doser Fastest possible dosing of the stated amount.<br />

SL-GOPTEMP Tempering Program for driving heating/cooling ramps<br />

SL-GOPTEMPHALTEN Temp_Hold The program controls a temperature regulation. The predetermined setpoint<br />

is issued directly to the regulator when controlling interior temperature, and<br />

directly to the thermostat when controlling the jacket temperature. Transition<br />

is possible according to time or through structural transition (e.g. if a parallel<br />

path is completed).<br />

SL-GOPVAKHALTEN Vacuum_Hold The program controls a vacuum regulation. The predetermined setpoint is<br />

issued directly to the regulator. Transition is possible according to time or<br />

through structural transition (e.g. if a parallel path is completed).<br />

SL-GOPVAKU Vacuum The program controls vacuum regulation. The setpoint value is run to a<br />

desired end value using a ramp.<br />

SL-GOPWAAGETARI Tare_Scales Program for resetting a balance<br />

SL-GOPWARTET Wait_Until Program for holding for an arbitrary waiting time.<br />

SL-GOPWARTEZ Wait Program for holding until an arbitrary time.<br />

SL-GOPWBEDIENER Wait_Operator Waits until the operator presses OK.<br />

SL-GOPWBEDINGUNG Wait_Condition Waits until the condition is fulfilled.<br />

SL-GOPWIEDERH Repeat Determines the number of passes of a recipe cycle.<br />

As long as the counter is smaller than the number of repetitions, the right<br />

output of the of the element is used, otherwise, the lower output.<br />

Recipe Series Generator<br />

The recipe series generator, in connection with<br />

HiBatch, allows automatic parameterisation and<br />

execution of experiment series. RezGen generates a<br />

whole experiment series automatically out of a few<br />

specifications. The desired parameters are varied<br />

within defined ranges from experiment to<br />

experiment. This results in:<br />

� Great time savings when conducting serial or<br />

parallel experiments<br />

� Increase of the Laboratory Performance<br />

� Shortened „Time to Market"<br />

For the parameters intended to be varied, the<br />

operator merely needs to predefine the initial value,<br />

the final value, and the increase from experiment to<br />

experiment.<br />

RezGen will then produce an experiment plan, which<br />

contains all variations. Unnecessary variations can<br />

be excluded.<br />

If, for example, experiments are to be conducted at<br />

four different temperatures, and one reactant is to be<br />

added metered at each temperature in three<br />

different quantities, this will result in 12 variations.<br />

The control recipes automatically generated out of<br />

one basic recipe, can, in a suitable assembly,<br />

Order Code Description<br />

SL-REZGEN Recipe Series Generator<br />

conducted in automatic mode in succession or<br />

simultaneously in a parallel reactor system.<br />

The variable parameters are entered into the basic<br />

recipe form.<br />

The intended variations of individual parameters are<br />

specified in the factor plan.<br />

The individual work recipes are generated out of the<br />

entered data. In the Release form, the work recipes<br />

can be released or disabled.<br />

Informations about StatGen for compiling multi factorial test planing for the statistic experiment planing<br />

upon request.<br />

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MultiBatch<br />

Laboratory Automation Software<br />

The definition of parallel experiments is made<br />

possible as simple as can be by the HiBatch<br />

extension MultiBatch. A recipe established as a<br />

sample can be applied to a random number of<br />

reactors with MultiBatch. The recipes can be<br />

individually parameterised and the progression<br />

individually modified.<br />

You define all parallel experiments by allocating the<br />

sample recipe to the reactors intended for use with<br />

the help of the reactor allocation chart.<br />

Allocation of the reactors for the sample recipe.<br />

MultiBatch will then generate an entity for each<br />

reactor. In order to be able to differentiate, the<br />

names of the recipes are indexed with the attached<br />

reactor identification number.<br />

Order Code Description<br />

SL-MULTIBATCH MultiBatch Option for HiBatch<br />

The entities can be started, held, and completed<br />

independent of each other and have separate data<br />

records.<br />

The recipe procedures are initially the same at the<br />

respective parallel experiments. Individual<br />

procedures can however be individually modified.<br />

Cloner<br />

Display of the allocated reactors.<br />

The cloner is a benefical tools too multiplicate<br />

control structures. Creating a parallel reactor project<br />

will be a lot easier with the cloner. After the project<br />

has been created for one reactor it can be cloned to<br />

all further reactors. The user decides which objects<br />

will be cloned.<br />

The cloned objects will signed by indices attached to<br />

the data point name eg. Valve[2] .<br />

The channel number will be assigned automatically,<br />

but can be changed later.<br />

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170<br />

Laboratory Automation Software<br />

eJournal, the electronic Laboratory Notebook (ELN)<br />

Test Documentation as it should be!<br />

The electronic laboratory notebook eJournal<br />

represents more than an adequate substitute for the<br />

paper-bound laboratory notebook. The eJounal<br />

automatically protocols all information gained in the<br />

course of the test progression. In addition, it is also<br />

possible to consistently present and archive test<br />

regulations, material properties of the educts and<br />

products, laboratory analyses and further<br />

information. This significantly increases productivity<br />

and prevents the loss of knowledge through<br />

employee turnover.<br />

The trend towards the electronic document is<br />

becoming more and more evident. The American<br />

FDA (Food and Drug Administration) is pushing the<br />

deployment of electronic media within<br />

documentation. Due to the Electronic Signature Act,<br />

digitally signed electronic documents are legally<br />

equivalent to hand-signed paper documents. The<br />

increase of productivity in the research industry due<br />

to the change to an electronic system is estimated to<br />

be 50%.<br />

A computer-supported laboratory notebook offers<br />

significant advantages: reading and writing mistakes<br />

are eliminated, a retrieval function enables the fast<br />

search for experiments and results. The<br />

manipulation-secure filing with electronic signature<br />

is made possible. Test parameters, measurement<br />

data, and evaluated results are presented clearly on<br />

protocol pages.<br />

The laboratory personnel is supported with<br />

additional functionalities (e.g. automated evaluation)<br />

and, in particular, relieved of bothersome routine<br />

activities such as the noting of measurement values.<br />

An electronic laboratory notebook is particularly a<br />

„must-have“, if the laboratory process (synthesis<br />

laboratory, fermentation laboratory) must run GLPconform<br />

(Good Laboratory Practice) or a validated<br />

mode of operation is required.<br />

Advantages:<br />

� Standardised Mode of Operation<br />

� Relief of Laboratory Personnel from Routine<br />

Activities<br />

� Elimination of Reading and Writing Mistakes<br />

� Manipulation-secure Filing<br />

� Easier Retrieval of Experiments<br />

� A Contribution towards the paperless<br />

Laboratory<br />

� Individually configurable<br />

� Online Evaluation and Spreadsheet<br />

� Full Text Retrieval in individual or all pdf-<br />

Documents<br />

� Export of the Test Report as pdf or rtf Data<br />

File<br />

The following diagram illustrates the information flow<br />

between the individual modules of the LabVision<br />

System.<br />

Recording<br />

In the electronic laboratory notebook all relevant<br />

values, parameters, and results, as well as eventual<br />

defining text and comments, of a test are recorded<br />

and stored. It is also possible to automatically<br />

integrate digital photographs made event-driven or<br />

according to schedule with the LabCam Module<br />

during the test.<br />

The recorded data is presented in freely<br />

configurable report pages with tables and graphic<br />

value and text fields. This warrants for an optimal<br />

documentation of the test progression at all times.<br />

Manual processing of the data is no longer required,<br />

which eliminates one major source for mistakes.<br />

Unattended operation is now possible – night time<br />

and weekends are now available for experimenting.<br />

A multitude of tests can now be processed in a<br />

minimum of time.<br />

Protocoling<br />

The batch protocol containing all values, events,<br />

operating interventions, value changes, etc. is<br />

established automatically. Digital photographs,<br />

chemical formulas, laboratory analysis data, links to<br />

data files or websites, comments etc. can just be<br />

integrated. eJournal therefore represents a major<br />

step in the direction of a paperless laboratory.<br />

Authenticity and integrity of the information are<br />

secured.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

The protocol can be aligned to the special<br />

requirements of your laboratory. It contains, amongst<br />

others, a first page with general information, one<br />

page with information to the educts and products<br />

and plant properties, one page with analysis values,<br />

as well as protocol pages with the recorded<br />

measurement values, events, and comments. The<br />

layout of the protocol pages can be designed freely<br />

with the form generator.<br />

To enable a better overview and clarity, the recorded<br />

values are also graphically presented. The<br />

laboratory notebook can be exported as pdf or rtf<br />

data file for further processing. The manipulationsecure<br />

pdf data file can be transmitted e.g. per Email.<br />

The rtf data file can be reworked with a word<br />

processing program.<br />

Evaluation<br />

Evaluation and documentation of the experimental<br />

data are supported or completely automated. The<br />

recorded data can be evaluated automated with<br />

HiText and presented in tables or various<br />

presentation forms, e.g. as a set of curves, average<br />

values with minimum and maximum bars or<br />

standard deviations. Self-calculating tables are also<br />

possible.<br />

Data import/export<br />

For data exchange to third party software multiple<br />

options are available<br />

� scv-file<br />

� text file<br />

� Windows Pipe<br />

� apis<br />

Order Code Description<br />

SL-JOURNAL eJournal, parameterisable, electronic laboratory notebook<br />

eJournal requires SL-HITEXT and SL-DIAPROT.<br />

Comprehensive Documentation<br />

A comprehensive synthesis regulation is elementary<br />

for the explicit performance of a reaction. It contains,<br />

respectively interconnects all information required to<br />

make the reaction reproducible. These include<br />

statements to the test assembly, the recipe<br />

workflow, the data of the reactants and solvents and<br />

test parameters such as periods, quantities, and<br />

pressures. The storage of the synthesis regulation<br />

ensures the availability of all information required for<br />

a later repetition of a test.<br />

Savin of the sythesis directive ensures an availability<br />

of all information within the systems to reproduce the<br />

the experiments.<br />

Organisational, procedural, and chemical<br />

information are also registered in the eJounal to<br />

enable the precise allocation of the other data.<br />

The eJournal structures the data in such a manner<br />

that it can easily be retrieved with the help of the<br />

HiLIMS Laboratory-Information-Management-System<br />

and are available for further use. This ensures<br />

that new and proven synthesis regulations, including<br />

the knowledge of the synthesised substances, are<br />

not lost and available at all times.<br />

Informations about LIMS can be found under<br />

HiLIMS Laboratory-Information-Management-<br />

System.<br />

We will create your own laboratory journal according<br />

to your specifications.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Data Export<br />

Laboratory Automation Software<br />

The data export server supports the manual and<br />

automatic exporting of values and protocol files in<br />

the file formats<br />

� Excel SYLK (slk)<br />

� Text format (csv)<br />

� Excel direct export (xls)<br />

� HTML format (.html)<br />

For predetermined times, several export jobs can be<br />

defined and implemented manually or automatically.<br />

In addition, there is also the possibility to control the<br />

export via HiText program, e.g. in order to export the<br />

data automatically at the end of an experiment.<br />

A data export can also be started directly from the<br />

analogue pen recorder.<br />

The data points intended for export can be selected<br />

individually. The number of places before and after<br />

the decimal point can be determined.<br />

Numeric data exported are subject to a data<br />

reduction. The reduction is optionally conducted by<br />

forming the:<br />

� average value<br />

� max value<br />

� min value<br />

� unaveraged<br />

� interpolate<br />

The reduction interval is freely definable.<br />

One data point can be entered several times e.g. to<br />

export average, min and max values. The time can<br />

be issued optionally either absolute or relative to a<br />

freely selectable start time.<br />

An export that can be started manually is already<br />

contained in the Basic Version.<br />

Order Code Description<br />

SL-EXPORT LabVision export module, Option for automatic or <strong>HiTec</strong>-controlled Exports<br />

Selectors and Display Filters<br />

The display filters help to handle larger arising data<br />

floods at plants, e.g. by limiting the time domains.<br />

Selectors serve as user-specific classification<br />

criterion, e.g. when looking for or sorting the data<br />

points and in the protocols. Selectors can be defined<br />

by the user in a separate form freely.<br />

Example:<br />

System1, System2, to wait, to be calibrated, no<br />

operation.<br />

The selectors offer the possibility to select a group of<br />

data points during selection, in reports etc.<br />

The selectors can be linked by the operators<br />

� plus<br />

� without<br />

� )thereof(<br />

Order Code Description<br />

SL-SELFIL Selectors and filters for LabVision<br />

Example: (Reactor1 plus cooling unit) thereof (all<br />

without required values)<br />

All data points are selected by this selection except<br />

the setpoint value data points of Reactor1 and the<br />

cooling unit.<br />

This option also extends the filter possibilities<br />

� Project Modules<br />

� Progress Report<br />

� Message Report<br />

� Data Point Selection<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

Access Control and User Administration<br />

The access supervision is active in:<br />

� Modules e.g. project administration, control<br />

program editor...<br />

� Windows with critical data point parameterisation<br />

possibilities<br />

� Objects established by the user such as<br />

programs, flow sheets and recipes and individual<br />

operating objects.<br />

For every user, authorisations can be assigned<br />

individually. A user must first register with name and<br />

password before he can operate the system.<br />

The user administration can, according to an<br />

adjustable inactivity period, automatically lock the<br />

system to prevent operation.<br />

Order Code Description<br />

SL-BENRECH Access and user administration for LabVision<br />

Multiple Projects<br />

Several plants each with its own PI can be driven<br />

with an UI.<br />

The option "multiple projects" makes it, in each case,<br />

possible to start on one UI several projects with its<br />

own LabVision.<br />

Order Code Description<br />

SL-MULTIPROJ Multiple Projects with LabVision<br />

WebVision<br />

WebVision enables to operate and monitor<br />

LabVision from an external computer (Client) via a<br />

network connection (TCP/IP).<br />

Running LabVision projects can be accessed from<br />

one or several computers connected via network<br />

without the necessity of having to install a Labvision<br />

system at these locations.<br />

The WebVision user interface is mainly identical with<br />

the same of LabVision.<br />

For WebVision integrations, the access control is<br />

obligatory.<br />

Each project has then an independent control<br />

interface.<br />

For licensing the data points of all simultaneously<br />

active applications are added together.<br />

WebVision supports the same modules (work<br />

sheets, multichart recorders, process reports,<br />

message reports, and LabCam) according to the<br />

optional equipment of the currently assembled<br />

LabVision-System.<br />

The LabVision User Administration is supported.<br />

Work sheet operator operations can be permitted or<br />

prohibited by the Labvision computer depending on<br />

the user setting. WebVision operating activities are<br />

protocolled in the process report.<br />

Several WebVision installations can respectively<br />

access (simultaneously) on to one or more<br />

LabVision Systems in the net. The LabVision or<br />

HiText uer interface must not be active for this<br />

purpose. Worksheets can both be displayed and<br />

operated in WebVision.<br />

A "Chat Function" enables the communication<br />

between the user of the LabVision System and the<br />

WebVision users. The „light“ version is limited to the<br />

display of the multichart recorder.<br />

Order Code Description<br />

SL-WEBVIS Access to active LabVision projects via TCP/IP LAN connection<br />

SL-WEBVISL Only MultiChart recorder visualisation of active LabVision-Projects<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Components<br />

Process Analytics<br />

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Dispersing<br />

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Laboratory Automation Software<br />

Activation Module for PI of other Manufacturers<br />

If Labvision is intended to be exclusively run by a PI<br />

of other manufacturers, a dongle is required for the<br />

administration of the program options.<br />

Order Code Description<br />

SL-FREMDPNK LabVision Activation Module for PI of other Manufacturers ( with Dongle)<br />

PI-Drivers<br />

The PI driver makes the communication between the<br />

UI with a PI possible. The PI Driver for the <strong>HiTec</strong> PIs<br />

LabManager, LabBox, MSR manager and MSR box<br />

is supplied free of charge with the devices. A <strong>HiTec</strong><br />

PI can be simulated by the special PI driver<br />

PNKSIMMAN. Due to this, it is possible to provide<br />

an application without an attached PI.<br />

PI Driver for other PIs and Field Bus Systems<br />

The PI driver for (external) other manufacturers' PIs ,<br />

a software connection to existing automation<br />

software or data bases, as well as fieldbus systems,<br />

can be operated parallel to PI drivers.<br />

Next to the PI drivers for the <strong>HiTec</strong> PIs, drivers for<br />

various laboratory instruments and PIs of other<br />

manufacturers are available. LabVision can<br />

integrate several PI drivers and consequently<br />

communicate with different Pis simultaneously. PI<br />

drivers are available for a broad range of devices.<br />

The range is consistently extended by us. For this<br />

reason, if you require a driver for an automation unit<br />

that is not listed in this catalogue please inquire if<br />

there is a connection possibility in the mean time.<br />

If required, our programming department will<br />

establish customer-specific PI drivers for any device.<br />

Order Code Option / Function<br />

SL-PNKPERF PI-Driver for Braun Perfusor<br />

SL-PNKSPS PI-Driver for Siemens S5/S7, 3964(R) protocol and AEG Modicon<br />

SL-PNKLASENTEC PI-Driver for Lasentec FBRM - particle systems<br />

SL-PNKMTRx PI-Driver for Metrohm Dosimat 665 and 765, Titrino 718 and 702,<br />

and Liquino over Dosing Interface 846 (x = 1, 2, 4, 8 Devices)<br />

SL-PNKOPC PI-Driver for OPC-DA (version 1+2), OPC-Client<br />

SL-PNKDDE PI-Driver for DDE data exchange<br />

SL-PNKMODBUS PI-Driver for ModBus devices over serial PC interface<br />

SL-FREMDPNK LabVision access module for externally manufactured -PI systems (with Dongle)<br />

Further drivers upon request.<br />

Programming-Interface<br />

The module ANWINT makes it possible to access<br />

from other programs (Visual basic, C++, Pascal...)<br />

the current values of the data points being written<br />

and read. A briefing of one day by our programmers<br />

is mandatory.<br />

Order Code Description<br />

SL-ANWINT Programming interface for LabVision<br />

DS-LVPROG Instruction into „SL-ANWINT“ programming for LabVision<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Remote Connection<br />

LabVision offers different possibilities for the<br />

remote connection of the UI.<br />

Connection via<br />

� Internet<br />

� Network (LAN)<br />

� Modem<br />

� ISDN<br />

Applications<br />

� remote maintenance<br />

� remote support<br />

� remote diagnosis<br />

� software maintenance<br />

� remote control<br />

� data transfer<br />

Laboratory Automation Software<br />

Remote <strong>Main</strong>tenance/ Remote Support<br />

� Support and Fault remedy without delay<br />

� Short service-reaction times, particular in<br />

critical situations<br />

� Savings on service costs<br />

With the help of this „Remote Access“ software, the<br />

UI can be operated from a remote work station.<br />

This computer virtually makes a second keyboard<br />

and monitor available, so that all functions can be<br />

carried out like at the UI itself. Both monitors<br />

therefore display the same screen image.<br />

In addition, file transfer is possible in both<br />

directions.<br />

All keyboard and mouse actions, also screen<br />

settings, are communicated via the telephone or<br />

LAN network.<br />

Consequently, fault detection and remedy, network<br />

maintenance, file transfer, installation of updates,<br />

etc. can be carried out quickly and cost effectively.<br />

Other possibilities not yet mentioned here are in<br />

preparation, or can be arranged according to<br />

customer specifications.<br />

Order Code Description<br />

SL-TELES Tele-Service, remote connection to an UI for remote maintenance<br />

CP-MODEM2 External Modem for analogue telephone networks<br />

CP-MODEM4 External Modem for leased lines<br />

CP-ISDNAD ISDN-Adapter-card for digital networks<br />

Price Structure<br />

The sale price is determined from the number of<br />

data points and the selected options. This ensures<br />

that you must only purchase what you really need.<br />

All inputs and outputs are counted as data points,<br />

inputs and outputs of device components, except<br />

controllers, monitoring conditions and text data<br />

points.<br />

Local variables and/or indicators in HiText and AWL<br />

(Instruction List) do not count as data points.<br />

The necessary number of data points can be<br />

evaluated as follows:<br />

Number of data points = number of the inputs<br />

and outputs * automation factor<br />

Level of Tasks Automation<br />

Automation<br />

Factor<br />

Minimum Only recording of measurement 1<br />

Low Recording of measurement, limit-value monitoring, simple regulation 2<br />

Medium Recording of measurement, limit-value monitoring, control, regulation 4<br />

High Recording of measurement, limit-value monitoring, control, regulation,<br />

complex prompting<br />

8<br />

In regard to the number of data points, there is the Our application advisors will gladly discuss with you<br />

choice between 30, <strong>10</strong>0, 180, 300, 560, and <strong>10</strong>00. your automation project and arrange a suitable<br />

package. The packages can be upgraded by<br />

program options and data points at any time.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 175<br />

Equipment and<br />

Components<br />

Process Analytics<br />

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Stirring and<br />

Dispersing<br />

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176<br />

LabVision ® standard packets<br />

Laboratory Automation Software<br />

For the most frequent applications, the following<br />

LabVision standard packages were arranged. They<br />

save you laborious arranging of the individual<br />

modules and are, in addition, lower-priced than the<br />

sum of the single modules.<br />

Overview of all LabVision Software packets<br />

LabVision module<br />

Order code packet<br />

SL-LABVIS<br />

(LabVision base module with 30 data points)<br />

SL-HITEXT<br />

(HiText- Multi-tasking Control and Online-Evaluation)<br />

SL-HIBATCH<br />

(Recipe control module w. graphic recipe editor)<br />

SL-EASYBATCH<br />

(Table based recipe control module)<br />

SL-ACTIONTRACK<br />

(Recording of activities as EasyBatch program)<br />

SL-GOPBIB<br />

(<strong>HiTec</strong> basic unit operations library f. HiBatch)<br />

SL-DIAPROT<br />

(Dialog and Protocol forms with tables incl. graphics)<br />

SL-ONLGRA<br />

(Online charts with reference curve presentation)<br />

SL-SCHANA<br />

(Analogue plotter, MDI-capable)<br />

SL-SCHERE<br />

(Event plotter)<br />

SL-SCHPHA<br />

(Phase plotter)<br />

SL-UEBMEL<br />

(Monitoring and Reporting)<br />

SL-DESIGN<br />

(Designer)<br />

SL-MODBIBALR<br />

(Project Module Library for Designer)<br />

SL-PROJMOD<br />

(Project modules generator and editor for LabVision)<br />

SL-RIEDIT<br />

(RI-Editor according to EN ISO <strong>10</strong>628)<br />

SL-BIBRILK<br />

(Glass a. Laboratory Devices Library for P&ID-Editor)<br />

SL-EXPORT<br />

(LabVision export module, automatic or exports)<br />

SL-SELFIL<br />

(Selectors and filter functionality)<br />

SL-BENRECH<br />

(Access and user administration for LabVision)<br />

SF-AWLPLUS<br />

(Instruction List Module with structured Text )<br />

SL-BERICHT<br />

(Progress Report, batch orientated extended search)<br />

SL-JOURNAL<br />

(Parameterisable electronic laboratory notebook)<br />

SL-WEBVIS<br />

(Remote maintenance of projects via TCP/IP)<br />

1 Light-Version: one worksheet, max. 200 objects<br />

2 Light-Version: 4 programms with <strong>10</strong>0 code lines each<br />

3 Light-Version: consisting of dosing, tempering and vacuum<br />

4 Light-Version: max. 120 objects<br />

5 Light-Version: 2 plotter pages with 8 curves each<br />

SL-LABVIPKONL<br />

For continuous and batch processes, individual<br />

packages are intended. The packages can also be<br />

individually extended later.<br />

The packages already contain the minimum data<br />

point amount of 30 and must be extended to the<br />

number required for the application.<br />

SL-LABVIPKON<br />

SL-LABVIPKONP<br />

SL-LABVIPEASY<br />

x x x x x x x x<br />

x 2 x x x x x x x<br />

x<br />

SL-LABVIPBATL<br />

SL-LABVIPBATE<br />

SL-LABVIPBAT<br />

SL-LABVIPBATP<br />

x 8 x x x<br />

x 9 x x x<br />

x x x x x x<br />

x x<br />

x 5 x x x 5 x 5 x 5 x x<br />

x 6 x x x 6 x 6 x 6 x x<br />

x 7 x 7 x x x<br />

x x x<br />

x 1 x x x 1 x 1 x x x<br />

x 3 x x x 3 x 3 x x x<br />

x<br />

x 4 x x x 4 x 4 x x x<br />

x x<br />

x x x<br />

x x x<br />

x x<br />

x x<br />

x x<br />

x x<br />

6 Light-Version: Events will only shown as shortened hints<br />

7 Light-Version: max. 3 phases<br />

8 Light-Version: max. 20 steps<br />

9 Light-Version: limited library see "Basic unit operations library"<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

Conti-light Software packet for LabBox 1 and 2<br />

This software package is made for LabBox1 and 2<br />

PIs and is suited for the automation of small<br />

continuous processes. (Description, see chart<br />

above)<br />

Order Code Description<br />

SL-LABVIPKONL Software packet for LabBox1 & 2 for running small continuous-processes<br />

Recommended PI-Modules<br />

Order Code Description<br />

SF-PID4 Controller module with 4 PID and application oriented controllers<br />

SF-NAMSER4 NAMUR-Driver for serial interfaces<br />

SF-ANWTAB User defined linearisation table<br />

SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />

Conti-standard Software packet for LabManager1<br />

This software package is designed for the<br />

LabManager1 for the automation of medium<br />

continuous processes. (Description, see chart<br />

above)<br />

Order Code Description<br />

SL-LABVIPKON Software packet for LabManager1 for running medium sized continuous processes<br />

Recommended PI-Modules<br />

Order Code Description (PI modules)<br />

SF-PID8 Controller module with 8 PID and application oriented controllers<br />

SF-NAMSER4 NAMUR-Driver for serial interfaces<br />

SF-ANWTAB User defined linearisation table<br />

SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />

Conti-plus Software packets for LabManager1 and 2<br />

This software package is designed for automation<br />

with the LabManager1 or 2 for large continuous<br />

processes. (Description, see chart above)<br />

Order Code Description<br />

SL-LABVIPKONP Software packet for LabManager1 or 2 for running large continuous processes<br />

Recommended PI-Modules<br />

Order Code Description (PI modules)<br />

SF-PID16 Controller module with 16 PID and application oriented controllers<br />

SF-NAMSER4 NAMUR-Driver for serial interfaces<br />

SF-ANWTAB User defined linearisation table<br />

SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 177<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


178<br />

Laboratory Automation Software<br />

EasyBatch Software packets for LabBox1 and 2 and LabManager<br />

This software package is designed for automation of<br />

small batch and continuous processes with any<br />

automation unit.<br />

(Description, see chart above)<br />

Bestellcode Beschreibung<br />

SL-LABVIPEASY Software packet EasyBatch for LabBox1 & 2 for running small batch-processes<br />

Recommended PI-Modules<br />

Order Code Description (PI modules)<br />

SF-PID4 Controller module with 4 PID and application oriented controllers<br />

SF-NAMSER4 NAMUR-Driver for serial interfaces<br />

SF-ANWTAB User defined linearisation table<br />

SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />

Batch-light Software packets for LabBox1 and 2<br />

This software package is designed for automation<br />

of small batch processes with the LabBox1 and 2.<br />

(Description, see chart above)<br />

Order Code Description<br />

SL-LABVIPBATL Software packet for LabBox1 & 2 for running small batch-processes<br />

Recommended PI-Modules<br />

Order Code Description (PI modules)<br />

SF-PID4 Controller module with 4 PID and application oriented controllers<br />

SF-NAMSER4 NAMUR-Driver for serial interfaces<br />

SF-ANWTAB User defined linearisation table<br />

SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />

Batch-economy software packets for LabBox2 and LabManager1<br />

This software package contains equipment<br />

components which are sufficient to run a laboratory<br />

reactor system in batch operation mode. An<br />

according plant, for example, is the LabKit2.<br />

(Description, see chart above)<br />

Order Code Description<br />

SL-LABVIPBATE Economy software package for LabBox2 and LabManager1 designed for batch processes<br />

Recommended PI-Modules<br />

Order Code Description (PI modules)<br />

SF-PID8 Controller module with 8 PID and application-oriented controllers<br />

SF-NAMSER4 NAMUR-Driver for serial interfaces<br />

SF-ANWTAB User defined linearisation table<br />

SF-HITUNE Auto parameterisation for temperatur controll SF-PIDxx<br />

SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

Batch-standard software packets for LabManager1<br />

This software package is designed for the<br />

automation of medium-sized batch processes with<br />

the LabManager1.<br />

(Description, see chart above)<br />

Order Code Description<br />

SL-LABVIPBAT Software packet for LabManager1 for medium sized batch-processes<br />

Recommended PI-Modules<br />

Order Code Description (PI modules)<br />

SF-PID8 Controller module with 8 PID and application oriented controllers<br />

SF-NAMSER4 NAMUR-Driver for serial interfaces<br />

SF-HITUNE Automatic parameterisation for temperature cascade controller SF-PIDxx<br />

SF-ANWTAB User defined linearisation table<br />

SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />

Batch-plus Software packets for LabManager1 or 2<br />

This software package is designed for automation of<br />

giant sized batch processes with the LabManager1<br />

and 2.<br />

(Description, see chart above)<br />

It consists of the following modules:<br />

Order Code Description (Number of Data Points)<br />

SL-LABVIPBATP Software packet for LabManager1 and 2 for giant sized batch-processes<br />

Recommended PI-Modules<br />

Order Code Description (PI modules)<br />

SF-PID16 Controller module with 16 PID and application oriented controllers<br />

SF-ANWTAB User defined linearisation table<br />

SF-NAMSER4 NAMUR-Driver for serial interfaces<br />

SF-HITUNE Automatic parameterisation for temperature cascade controller SF-PIDxx<br />

SF-DATLOG Data Logger Function, data buffering in the PI in case of UI failure<br />

All software packages are discounted.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 179<br />

Equipment and<br />

Components<br />

Process Analytics<br />

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Stirring and<br />

Dispersing<br />

Services


180<br />

Laboratory Automation Software<br />

HiLIMS Laboratory Information Management-System<br />

Finally, the sure way to Retrieval!<br />

The general development towards the electronic<br />

document is becoming more and more evident. Due<br />

to the Electronic Signature Act, digitally signed<br />

electronic documents are legally equivalent to handsigned<br />

paper documents. The American FDA (Food<br />

and Drug Administration) is pushing the deployment<br />

of electronic media within documentation. Laboratory<br />

Information Management Systems (LIMS) are<br />

entering the laboratories, where they are replacing<br />

laboratory notebooks or books on paper basis.<br />

Just one irretrievable test can represent more costs<br />

than the investment in a LIMS, as patent claims can<br />

not be defended, liability claims can not be repulsed<br />

or for the simple cause that tests need to be<br />

repeated.<br />

Advantages of the Electronic Information<br />

Administration:<br />

� Support of laboratory-internal procedures<br />

� Secure retrieval of test results<br />

� Increase of productivity<br />

� Prevention of mistakes<br />

� Internal availability of knowledge<br />

� Protection of knowledge from exterior access<br />

� Protection of information from manipulation<br />

� Securing of information for re-use<br />

� Secure own claims and prevent liability claims<br />

The term LIMS covers a wide range. The LIM<br />

systems are just as varied as the laboratories they<br />

are applied in, e.g. a laboratory for medical<br />

diagnostics, a laboratory for productionaccompanying<br />

tests, or a chemical development<br />

laboratory.<br />

HiLIMS is the special LIMS for the F&E laboratory.<br />

There, next to to increasing the efficiency and<br />

shortening the „time to market“, the LIMS serves the<br />

purpose of protecting intellectual property and<br />

avoiding liability claims through electronic<br />

documentation and archiving. The last mentioned<br />

also serve to enable the fast retrieval of information<br />

gained in the tests (batch and continuous operation<br />

mode) by searching the electronic laboratory<br />

notebooks.<br />

The data of test series, parallel experiments, or<br />

freely arranged tests can be visually compared in<br />

various graphics and can be compressed in freely<br />

configurable reports. In comparison to the<br />

conventional mode of operation, it is no longer<br />

required to actually „handle“ the data. This<br />

eliminates many sources of error right from the<br />

beginning and drastically reduces the reworking<br />

periods. According to a study (CENSA 2004), the<br />

increase of productivity in the research industry due<br />

to the change to an electronic system is estimated to<br />

be 50%.<br />

A LIMS should consistently cover the complete F&E<br />

process chain from the placing of the order, over the<br />

control and attendance, right to the final report.<br />

A LIMS consists at least out of the basic modules<br />

measurement value logging and measurement value<br />

evaluation. Further modules provide for the<br />

connection of the hardware in the measuring line,<br />

the connection of the ERP systems, controlling<br />

software, data protection infrastructure etc.. LIMS<br />

can also be realised as distributed systems, so that<br />

it is possible to enter and call up data from different<br />

work places. HiLIMS can image all essential parts of<br />

a laboratory and supports both the administration of<br />

static (e.g. material data) and dynamic data (e.g.<br />

temperature progressions).<br />

Modern laboratory automation and analysis devices<br />

produce huge amounts of raw data, e.g. a recipe<br />

control system with online analytics and<br />

chemometrics, which would remain more or less<br />

useless without subsequent efficient data<br />

administration and data evaluation. For the purpose<br />

of data transfer, the EDP connection to automated<br />

laboratory reactor systems, chromatography data<br />

systems, instruments etc. is required.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Special features of the HiLIMS:<br />

Laboratory Automation Software<br />

� Fast relational SQL Database<br />

� Self-explaining User Interface<br />

� Network and Multi-User Capability<br />

� Smooth Integration in LabVision/HiBatch<br />

� R&D-oriented<br />

� Very versatile<br />

� Integrated forms and Form Designer<br />

� Integrated Data Mining, Evaluation and<br />

Reporting<br />

� Various Import and Export Possibilities<br />

The usual question whether to „Make or Buy“ does<br />

not arise any longer, as HiLIMS can be so flexibly<br />

aligned to various tasks that an individual<br />

programming is no longer cost-effective.<br />

There are virtually no limits to the integration of<br />

measurement devices, sensors and analysis devices<br />

into the measurement line. The control line can also<br />

be randomly extended by mathematical processing<br />

and evaluation of the measurement values, sample<br />

management, settlement etc..<br />

HiLIMS is the last but very important link of the<br />

processing chain consistently integrated into the<br />

LabVision/HiBatch program system. It attaches itself<br />

directly on to the data tables of the electronic<br />

laboratory notebook and the LabVision data base. I<br />

can however also be adjusted as independent<br />

program to other systems.<br />

Planning and Organising<br />

The processing chain commences with the order.<br />

The same contains the organisational data, e.g.<br />

customer, order ID, deadline, as well as the test<br />

specifications.<br />

The order form is freely configurable with the form<br />

editor. Informa tion deposited in the data base such<br />

as customer, laboratory and product, can be<br />

selected via selective lists. In addition, text fields for<br />

freely editable text, tables, and graphics can be<br />

integrated.<br />

Administration and Documentation<br />

All relevant information such as order, recipe, test<br />

parameter, measurement values, events, laboratory<br />

data or laboratory notebook are deposited in the<br />

LIMS data base in such a manner that they can be<br />

retrieved via freely configurable search queries the<br />

fastest possible way. This, beyond the better internal<br />

organisation, is useful for the securing of property<br />

rights and liability issues.<br />

The archived recipes and parameter sets can be retransferred<br />

to the HiBatch recipe control system in<br />

order to, if necessary, repeat a batch run or test<br />

program. An adjustment to special requirements,<br />

including the connection of laboratory and analysis<br />

devices, can be conducted by <strong>HiTec</strong> <strong>Zang</strong>, an<br />

external service provider or the user himself.<br />

Administration of:<br />

� Recipe data<br />

� Batch data<br />

� Educt and product data<br />

� Sample data<br />

� Documents<br />

Searching and Retrieval<br />

Due to the deployment of HiLIMS as knowledge<br />

base, the generated research knowledge is made<br />

easily accessible and the transparency is increased.<br />

A query can be established by the user either based<br />

on forms or scripts. This may contain various criteria<br />

such as organisational dates, material data,<br />

measurement values, laboratory data etc. The freely<br />

configurable search forms are self-explaining and<br />

support standard procedures. Individually configured<br />

search forms can be used as predefined search<br />

dialogues after they have been logged.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 181<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


182<br />

Elements of the Search Dialogues:<br />

Laboratory Automation Software<br />

� Organisational Data<br />

� Dates, times, time domains<br />

� Values, value ranges of measurement values,<br />

analyses data, etc.<br />

� Keywords, terms<br />

The search dialogue forms may contain search<br />

elements in random combination.<br />

The search dialogue forms can also be established<br />

by the user with the form designer. For this purpose,<br />

the required search elements are merely integrated<br />

into the form via drag and drop.<br />

As the result of a search, all data records that<br />

accord to the search query will be displayed.<br />

The user is able to remove single tests from the list<br />

and before the start of the evaluation and<br />

complement the list via the switch “Attach Single<br />

Test”, e.g. for a reference test.<br />

Alternatively a script-based (expert search) search is<br />

possible. More complex search terms can be<br />

generated via the And and Or links and by the<br />

setting of brackets.<br />

Errors in the search script will be detected and<br />

displayed.<br />

Different search scripts can be stored for later use.<br />

Evaluation<br />

The data of the tests retrieved with the search<br />

function can be evaluated in a diversity of manners.<br />

The simplest case is the direct comparison of<br />

selected variables in diagram form. For this purpose,<br />

various diagrams are available for selection, e.g.<br />

array of curves, average values with min/max bars<br />

or standard deviations.<br />

The protocol of the evaluation consists, e.g. of a<br />

cover sheet with the general information and<br />

possibly a copy of the order with the protocol pages<br />

following.<br />

The layout of the protocol pages is established with<br />

the form designer.<br />

Evaluation Possibilities:<br />

� Evaluation of test series and parallel tests<br />

� Comparative presentation<br />

� Statistical evaluation<br />

� Freely programmable evaluation<br />

The stored information such as order, recipe,<br />

laboratory notebook, report data table, raw data, can<br />

be displayed or exported as data file for further<br />

processing.<br />

Setting<br />

The master data is created with the table-based<br />

master data editor. The user is also able to create<br />

data base fields and tables himself, e.g. part<br />

numbers or materials with material data. In the<br />

course of establishing an order, in the laboratory<br />

notebook, in case of queries or when designing the<br />

report, it is now possible to immediately gain access<br />

to the created data base fields and tables via the<br />

selective list.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

User Administration<br />

In the user administration, the users are allocated to<br />

different groups such as administrator and user. The<br />

user must log in and his respectively stored data are<br />

assigned an ID.<br />

Device Coupling<br />

For the coupling of analysis devices, spectrometers,<br />

etc., there are various interfaces and protocols at<br />

disposal.<br />

� OPC<br />

� ModBus<br />

� Text data files<br />

� csv-data files<br />

� MS-Excel ® -tables<br />

� Device-DLL etc.<br />

For the coupling with other software, such as ERP<br />

and chemometrics programs, individual<br />

programming is available.<br />

Technical Data:<br />

Database<br />

System<br />

Microsoft SQL Server ® as of Version<br />

2000.<br />

Basic Version is delivered with free<br />

version of SQL-Server Express, limited<br />

to 4 GB.<br />

1 to unlimited (dependent of database<br />

server and client licenses)<br />

1 to unlimited<br />

Number of<br />

Users<br />

Client<br />

Licenses<br />

Modules - Basic Version (single-user)<br />

- Multi-user extension<br />

- SQL-Database server<br />

- User Administration<br />

- Electronic Signature<br />

- Device Driver<br />

- Client-specific adjustments to ERP<br />

Program<br />

- Client-specific adjustments to<br />

Chemometry Program<br />

HiLIMS is also available as LabVision-Module (SL-<br />

HILIMS-C) and as stand-alone software (SL-HILIMSSA-C).<br />

Order Code Description Data Point<br />

Extra<br />

Charge<br />

SL-HILIMSL Single-User License HiLIMS light Option for LabVision including local SQL-<br />

Database Volume 4 GB<br />

yes<br />

SL-HILIMSSQL-S HiLIMS Serverl License for Multi-User Version<br />

Notice: Requires additional SQL-Server License<br />

no<br />

SL-HILIMS-C HiLIMS Option LabVision<br />

Notice: Requires HiLIMS Server and also additional SQL-Client License<br />

yes<br />

SL-HILIMSSA-C Stand-alone Workplace Client (HiBuilder Version, without LabVision run<br />

capable)<br />

Notice: Requires HiLIMS Server and also additional SQL-Client License<br />

no<br />

SL-SQLSERV SQL Server License without Client Licenses no<br />

SL-SQLCLNT SQL-Client License per Workplace no<br />

HiLIMS requires eJournal.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 183<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


184<br />

PI-Firmware-Modules<br />

Laboratory Automation Software<br />

The PI firmware auxiliary modules can be used to<br />

upgrade the PI‘s for fulfilling specialist tasks, which<br />

would otherwise not be possible with the basic<br />

setup. These modules are software modules<br />

(Firmware).<br />

Controller Modules<br />

The <strong>HiTec</strong> <strong>Zang</strong> PIs can be equipped with up to 32<br />

controller modules. Next to the standard PID<br />

regulators, so-called application-oriented<br />

controllers are available for the typical procedural<br />

regulation tasks.<br />

Example for a PID Controller Parameterisation Panel<br />

for lines which are difficult to control and to achieve<br />

a special quality of control, the adaptive control<br />

module SF-HICON is available.<br />

All control parameters are passed over data points<br />

and can be dynamically re-parameterised. It is<br />

therefore possible to control non-linear lines without<br />

any problems.<br />

You can choose between Standard PID controllers<br />

and application-oriented controllers.<br />

Standard PID-Controller<br />

The smallest version of the MSRmanager controller<br />

module consists of 4 controllers.<br />

The controllers can be individually set. The type is<br />

individually selectable:<br />

� P<br />

� I<br />

� PD<br />

� PDTz (Tz = shortened D amount)<br />

� PID<br />

� PIDTz<br />

� PH (for pH-control)<br />

The controllers have the characteristics of industrial<br />

controllers such as variable regulation value<br />

limitation, auxiliary regulation value cut-in, tolerance<br />

band, jolt-free takeover, and "anti-windup"<br />

functionality.<br />

Target and actual values, auxiliary regulation values<br />

and regulation values are set via a configuration<br />

menu with the corresponding data-points<br />

(input/output). The sampling interval is adjustable<br />

with a resolution of 1/<strong>10</strong>s.<br />

The regulation value limitation works alternatively<br />

before or after the cutting in of the auxiliary<br />

regulation value and permits the specification of a<br />

maximum and a minimum for the regulation value.<br />

Starting the I-proportion in the case of longer<br />

persisting offsets is prevented (anti-windup). The<br />

specification of a tolerance band is useful when<br />

heating/cooling or regulating pH values.<br />

For the output of the regulation values digital bit and<br />

byte, pulse-width modulated and similar outputs are<br />

made use of.<br />

Since all control variables are linked with data<br />

points, cascaded or guided controller systems and<br />

special functions, e.g. dynamic limitation, mapping<br />

controller, split outputs etc., can be implemented<br />

without any problems.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Application-oriented Controllers<br />

Application-oriented controllers are controllers<br />

respectively optimised for special tasks, e.g.:<br />

Laboratory Automation Software<br />

� Batch Dosing Control<br />

� Continuous Dosing Control<br />

� Vacuum Control<br />

� pH Control<br />

� Temperature Cascade Control<br />

The application-oriented controllers are selfparameterising<br />

or are automatically adjusted by a<br />

controller optimisation program. This saves you the<br />

according time when establishing an application.<br />

The achieved control qualities can only be reached<br />

with PID controllers with a lot of effort and knowhow.<br />

With the help of application-oriented controllers, the<br />

laboratory personnel is able to solve problems which<br />

would usually require to call a control technician.<br />

Order Code Description<br />

SF-PID4 4 controller modules Type P to PIDTz and application oriented controllers<br />

SF-PID8 8 controller modules Type P to PIDTz and application oriented controllers<br />

SF-PID16 16 controller modules Type P to PIDTz and application oriented controllers<br />

SF-PID24 24 controller modules Type P to PIDTz and application oriented controllers<br />

SF-PID32 32 controller modules Type P to PIDTz and application oriented controllers<br />

Auto tuning for temperature cascade controllers<br />

With the module "HiTune", the PID controller can be<br />

automatically parameterised. This is particularly<br />

favourably for stages, whose behaviour is subject to<br />

different influences e.g. a reactor inner temperature<br />

control, which is known for instance to be<br />

dependent on the material properties, the filling level<br />

and the stirrer speed.<br />

The appropriate process applying conventional<br />

modes of operation would require at least some<br />

hours, often days.<br />

The parameterisation of the controller takes place<br />

automatically during the running up to the setpoint<br />

values. The following diagram shows the controller<br />

behaviour at different setpoint value changes.<br />

Order Code Description<br />

SF-HITUNE Automatic parameterisation for temperature cascade controller SF-PIDxx<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 185<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


186<br />

Adaptive Regulation with HiCon<br />

Laboratory Automation Software<br />

HiCon is a highly developed, fully-adaptive controller<br />

for the LAB/MSRmanager system.<br />

With HiCon you allow a first-class control<br />

engineering specialist to work for you. This also<br />

ideally regulates stages for which a PID controller<br />

cannot be parameterised satisfactorily. Also in the<br />

course of the usually demanding and timeconsuming<br />

parameterisation of the inner<br />

temperature control of reactors, HiCon proves its<br />

strength, when it comes to fast run-up with minimum<br />

overshooting.<br />

A field test, which was conducted to compare HiCon<br />

with other regulation procedures such as PID and<br />

fuzzy-controllers, showed that HiCon is superior to<br />

all other procedures.<br />

The adjusting (parameterising) of PID controllers is<br />

conducted in practice, predominantly via direct trial.<br />

This requires special experience and is, in particular<br />

with slow-acting processes such as temperature<br />

runs, extremely time-consuming and unsatisfactory.<br />

To make things worse, only a more or less<br />

acceptable regulation quality is usually obtained,<br />

which is far away from the optimum. If the process<br />

changes during the run-time, or operating pointdependently,<br />

then the controller adjustment again<br />

becomes more difficult, if not even impossible.<br />

In reagrd to all these points, the adaptive controller<br />

HiCon represents the remedy. It adapts fast and<br />

automatically to variable process properties, but it<br />

can also - as a better alternative to the PID controller<br />

- be operated with fixed parameters, by switching off<br />

adaptation after a single controller parameter<br />

optimisation.<br />

If, necessary, a later follow-up optimisation can be<br />

carried out at any time, without disturbing or<br />

interrupting the process cycle.<br />

Order Code Description<br />

SF-HICON 1 HiCon Controller module adaptive<br />

HiCon supplies an outstanding regulation quality<br />

also for processes with pure delay elements, for<br />

processes with integral components and for<br />

processes with extensive dead times, which would<br />

be difficult to control with conventional controllers, if<br />

at all. In contrast to the PID-controller, HiCon<br />

delivers an equally optimal regulation quality both in<br />

the reference (setpoint value changes) and in the<br />

interference behaviour (interference to the controlled<br />

variable).<br />

Adaptive controllers have been available for<br />

decades. They have not however become generally<br />

accepted, because their handling was complicated,<br />

their behaviour not always stable and the price too<br />

high. The results of many years of development<br />

have been put into HiCon, which was "fine-tuned" in<br />

practical tests. The result is an industry-suited<br />

adaptive controller, which is robust and easy to<br />

deploy.<br />

Outstanding advantages compared to conventional<br />

controllers:<br />

� significant time saving during controller<br />

parameterisation<br />

� principally improved regulation quality<br />

� significantly better control for processes with<br />

integral times or dead times<br />

� optimal reference and interference variable<br />

control<br />

� Online-Adaptation of variable process<br />

properties<br />

Since this controller processes substantially more<br />

information about the process than a PID controller,<br />

it is clearly superior. Its efficiency is particularly<br />

evident at stages with dead time and double<br />

integrating behaviour, which can hardly be regulated<br />

with PID controllers. After a setpoint value change<br />

or a malfunction of the process, all status deviations<br />

are reduced to zero.<br />

The regulating behaviour merely depends on one<br />

setting parameter, the controller sensitivity, which<br />

can be adjusted between 0 and <strong>10</strong>0%. The standard<br />

value for this parameter is 50% and does not have<br />

not to be adjusted for most processes. Principally,<br />

an increase of the parameter means an increase of<br />

the controller activity, i.e. the controller intervenes<br />

more often, the actuator is more agitated and uses<br />

more adjustment energy.<br />

In a PI, up to four HiCon controllers can be<br />

operated.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

IEC 61131 IL– PLC Functionality for the PI<br />

The IEC 61131 IL module and device components<br />

bring extended PLC functionality into all <strong>HiTec</strong> PIs.<br />

The IEC 61131 IL (instruction list) is a proven control<br />

language and is internationally standardised via the<br />

EN 61131. The <strong>HiTec</strong> PIs MSRmanager, MSRbox,<br />

LabManager and LabBox can independently<br />

execute control functions, i.e. without participation of<br />

the UI (work station). For this purpose, the IEC<br />

61131 IL-control language and dynamic device<br />

components are available, which can be active even<br />

with a switched off PC. Therefore, the <strong>HiTec</strong> LAB<br />

and MSR-systems fulfil the safety-relevant NAMUR<br />

category three.<br />

The Instruction List control rounds off the LAB- /<br />

MSRmanager-System and simultaneously<br />

complements the application range in the direction<br />

of larger projects.<br />

As it is implemented on the PI, it significantly<br />

increases the security and enables the programming<br />

of even the most complex security and running<br />

routines which are realised without involvement of<br />

the UI.<br />

The PI-technically oriented language statement list<br />

(IEC 61131 IL) and device components are an ideal<br />

supplement to the application technology oriented<br />

HiText control and evaluation language. Their<br />

application is recommended then, if the control<br />

functions must be executed particularly safely, thus<br />

also in case of a failure of the UI-PC, or increased<br />

requirements on the performance are demanded.<br />

It must be emphasised that IEC 61131 IL and device<br />

components are "online capable", i.e., during a<br />

running program, a modified program can be loaded<br />

into the PI, which then takes over the control at the<br />

start of the next cycle.<br />

The programs are stored permanently and safely in<br />

the FLASH memory of the PI.<br />

IEC 61131 IL has access to all PI data points.<br />

Interesting is also the possibility to implement<br />

randomly complex alarm reactions directly in the PI,<br />

which range right up to the controlled shutting down<br />

of the system, e.g. in case of UI malfunction.<br />

An IEC 61131 IL program is started automatically<br />

immediately after the switching on of the PI and can<br />

execute several thousand operations per second.<br />

By using debugging functions such as break points,<br />

single-sequence and monitored printouts, you are<br />

supported during the program development.<br />

Symbolic variables and field variables are<br />

supported.<br />

Permanent (value remains after Reset and Power-<br />

Off) and non-permanent variables are supported.<br />

Characteristics:<br />

� IEC 61131 compatible<br />

� Indirect addressing<br />

� Sub-program technology<br />

� Cyclic and continuous execution<br />

� Combinable with device components<br />

� Binary and Analogue value processing<br />

� Online download capability<br />

� Simplest data exchange with the UI<br />

� Extended Alarm processing for the PI<br />

An Instruction List program is started automatically<br />

immediately after switching on the PI and is able to<br />

realise several thousands of operations per second.<br />

The Language Elements<br />

IEC 61131 IL-control supports the following IEC<br />

61131 commands:<br />

Operator Meaning<br />

LD Load operant<br />

ST Save operant<br />

S<br />

R<br />

Set, reset, depending on operant<br />

AND<br />

OR<br />

XOR<br />

ADD<br />

SUB<br />

MUL<br />

DIV<br />

GT<br />

GE<br />

EQ<br />

NE<br />

LE<br />

LT<br />

Boolean AND<br />

Boolean OR<br />

Boolean exclusive-OR<br />

Addition<br />

Subtraction<br />

Multiplication<br />

Division<br />

Compare on „Greater than“<br />

Compare on „Greater/Equal“<br />

Compare on „Equal“<br />

Compare on „Not Equal“<br />

Compare on „Less/Equal“<br />

Compare on „Less than“<br />

JMP Jump to given code-line<br />

NOP No Operation<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 187<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


188<br />

Data Types<br />

Laboratory Automation Software<br />

Mode Type<br />

PI-Data points All types of the PI<br />

Word memory Analogue, digital 32 bit<br />

Bit memory Bool<br />

Digital-inputs direct addressed Bool<br />

Digital-outputs direct<br />

addressed<br />

Bool<br />

Constants Integer and floating points<br />

Functional Elements<br />

TP Timer Pulse<br />

TON Timer Switch-on delay<br />

TOF Timer Switch-off delay<br />

CTU Counter Counter (up)<br />

CTD Counter Counter (down)<br />

CTUD Counter Up/down Counter<br />

F_TRIG Pos. edge detecting Flip-Flop<br />

R_TRIG Pos. edge detecting Flip-Flop<br />

SR RS-Flip-Flop with priority setting<br />

RS RS-Flip-Flop with priority re-setting<br />

The number of system functional elements present<br />

amounts to:<br />

� 30 Timers<br />

� <strong>10</strong> Counters<br />

� <strong>10</strong>0 RS-Flip-Flop-Functions<br />

The optional direct addressing of the digital inputs<br />

and outputs enables accelerated access to these<br />

inputs and outputs. Additionally, this direct access is<br />

protected from faulty parameterisation or<br />

manipulation via the user interface.<br />

Used data points are easily available in all other<br />

modules of the UI and the PI; i.e. they can be<br />

connected with visualisation objects or can be used<br />

in HiText programs.<br />

The Program Editor<br />

The easy to use editor (such as the HiText-Editor)<br />

offers many debug functions such as Breakpoint,<br />

Step-Over, Trace-Into, CPU-Window, and Watch<br />

Window with value change function.<br />

Online help functions are integrated. The reserved<br />

language elements are marked and comment areas<br />

are pointed out in colour (Syntax Highlighting).<br />

Entered programs are verified for correct language<br />

application in the LabManager before being loaded<br />

and activated.<br />

Test Auxiliaries<br />

The monitoring of terms supports troubleshooting,<br />

in particular during the development phase. Here,<br />

the current values of freely selectable data points<br />

and flags are displayed and constantly updated.<br />

Instruction List - plus (structured Text)<br />

An Instruction List (IEC 61131 IL) program can be<br />

written as structured text in HiText-oriented syntax<br />

with Instruction List-Plus. The program is<br />

transformed into the Instruction List syntax before<br />

execution.<br />

An uncomplicated exchange of program parts is<br />

possible with the HiText-Editor via the clipboard.<br />

Before the actual transfer of the completed program<br />

into the LAB-/MSRmanager, a vigorous syntax and<br />

error verification is conducted.<br />

Order Code Description<br />

SF-AWL IEC 61131 IL (Instruction List)<br />

SF-AWLPLUS IEC 61131 IL (Instruction List) plus HiText oriented strucured Text<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


NAMUR - Driver<br />

Laboratory Automation Software<br />

The freely parameterisable NAMUR - driver for serial<br />

interfaces enables the linking of any laboratory<br />

devices and analysers via serial interfaces of the PI,<br />

as long as the interface protocols of these devices<br />

principally accord to the NAMUR recommendations<br />

NE28.<br />

A serial interface can be split up logically into several<br />

channels. The individual channels are respectively<br />

addressed via their own data points. Furthermore,<br />

there is the possibility to connect bus capable<br />

devices.<br />

In the configuration table, the interface parameters<br />

out of the respective equipment manual are<br />

transferred.<br />

Order Code Description<br />

SF-NAMSER4 NAMUR-driver for 4 serial interfaces on the PI<br />

SF-NAMSER8 NAMUR-driver for 8 serial interfaces on the PI<br />

SF-NAMSER16 NAMUR-driver for 16 serial interfaces on the PI<br />

SF-NAMSER32 NAMUR-driver for 32 serial interfaces on the PI<br />

SF-NAMSER64 NAMUR-driver for 64 serial interfaces on the PI<br />

SF-NAMSER128 NAMUR-driver for 128 serial interfaces on the PI<br />

SL-PNKNAMSERA NAMUR-Driver for serial interfaces of the UI<br />

Example: An interface configured for a stirrer allows:<br />

� Setting of required speed<br />

� Requesting the current speed<br />

� Monitoring of error status<br />

As template a changable "general NAMUR device"<br />

is available. Here Inputs and Outputs need to be<br />

defined. The defined device can be used as<br />

template for a device component.<br />

Certain "external devices" where generated using<br />

this technology (eg. Knauer pumps, Heidolph<br />

stirrers) and need this device driver to work properly.<br />

For predetermined parameterisations for lab devices see „Driver Programs for Lab Devices“.<br />

User Tables<br />

Next to the standard linearisation tables for<br />

thermocouples, etc., firmly implemented in the PI<br />

and LAB PIs, up to four personal linearisation tables<br />

can be defined by the user. These are called user<br />

tables.<br />

With the help of a user table, a function can be<br />

described discretely using sampling points. A<br />

function is described, by entering the 64 equidistant<br />

sampling points between the smallest and largest<br />

values of the input into a table.<br />

Order Code Description<br />

SF-ANWTAB User defined linearisation tables<br />

Data logger function for PI<br />

The data logging module for Lab/MSR Manager and<br />

the Lab/MSR Box PI stores the resulting data in<br />

case of a failure of the UI. As soon as the UI is back<br />

online, the data is automatically transferred to the<br />

UI.<br />

Order Code Description<br />

SF-DATLOG Data logger module for <strong>HiTec</strong> PIs<br />

A selection between characteristic curve,<br />

thermoelement and resistance sensor can be made.<br />

In this way, devices can be linked without any<br />

problems even if their characteristics are only<br />

available as tables.<br />

Equipped user tables can later be used as interface<br />

type when defining a new data point.<br />

Technical Data:<br />

512 kB memory, page administration up to 64 kB,<br />

roll memory.<br />

Storage of up to 32.000 events.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 189<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


190<br />

Laboratory Automation Software<br />

HiBuilder Data Evaluation and Presentation<br />

Decisive for the development of HiBuilder was the<br />

demand by many users for a program that combines<br />

the easy handling of the table-oriented programs<br />

with the practically unlimited possibilities of a high<br />

level language compiler and in addition offers a<br />

publication-suitable graphical presentation for the<br />

technical-scientific documentation.<br />

HiBuilder distinguishes itself through the following<br />

performance features:<br />

� Online Coupling for Data Collection<br />

(LabVision)<br />

� Unproblematic Handling of even greatest Data<br />

Quantities<br />

� Super fast Arithmetics<br />

HiBuilder offers an enormous functionality:<br />

� HiText Syntax for randomly complex<br />

Evaluation Programs and Work Sheets<br />

� Publication-suitable graphical Presentation<br />

� Form Generator for Dialogue forms ,<br />

Protocols and Reports<br />

� Data Editor for Data Selection and Reduction<br />

� Signal Processing<br />

� Mathematical and statistic Functions<br />

� Windows Copy Function for Tables,<br />

Diagrams, and Forms<br />

� Data Export and Import for MS-EXCEL,<br />

Databases etc.<br />

HiBuilder can be coupled online via network with the<br />

PMC computer, so that the current process data is<br />

available at the work place without delay. With<br />

HiBuilder, it is possible to establish complete<br />

evaluation programs with the comfortable Windows<br />

user interface with only a fraction of the usual time<br />

expenditure. For this purpose, dialogue elements,<br />

e.g. input fields, buttons, option buttons etc. are<br />

available. Examples are the RAMOS Software,<br />

LiquiMaster, DosiMaste, KalDas etc.<br />

�<br />

Calculating sheets in HiText-Syntax enable even the<br />

most complex calculations to be conducted in a<br />

clear manner.<br />

The graphical presentation accords to the general<br />

perception in regard to the form of diagrams<br />

contained in technical-scientific publications.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Laboratory Automation Software<br />

Preconditioned diagram layouts can be randomly<br />

adjusted according to the requirements. A freely<br />

editable value table is attached to every diagram.<br />

Diagrams can be transferred to plotters, matrix, inkjet<br />

or laser printers, imported by a word processing<br />

or a DTP-program and post-edited under Windows<br />

with graphics programs e.g. CorelDraw or Designer.<br />

The monitor display accords exactly to the print<br />

document (WYSIWYG Principle).<br />

The design possibilities of the diagrams are varied:<br />

� Free axes allocation of the values , xy- or xt-<br />

Presentation<br />

� Various line types, colours and thicknesses,<br />

error bar presentation, and various plot<br />

symbols<br />

� Freely placeable axes<br />

� Scaling linear, logarithmic and automatic<br />

� Coarse and fine raster, extra raster,<br />

subsidiary lines<br />

Order Code Description<br />

SD-HIBUILDER Program for Data Evaluation and graphical Presentation.<br />

The legend and the explanatory text can be placed<br />

freely. There is a data table to every diagram.<br />

Modifications to the table are directly assumed by<br />

the graphics.<br />

With the help of the Form Generator it is possible to<br />

establish protocols and self-calculating forms.<br />

In this manner, you can equip your evaluation<br />

programs with an appealing and easy to handle user<br />

interface.<br />

The graphic and the table values can now be<br />

assumed by a word processing program, e.g. MS-<br />

Word, via the Windows clipboard and consequently<br />

integrated into a report in an uncomplicated manner.<br />

The applications mentioned here only represent a<br />

small section of the various possibilities of HiBuilder.<br />

The calculating sheets and the statistic functions<br />

especially aligned to the measurement value<br />

evaluation open the user the opportunity to realise<br />

the automation of evaluations of virtually any<br />

complexity.<br />

With this, HiBuilder closes the currently demanded<br />

consistent data chain reaching from the sensor up to<br />

the presentation. There is no more chance for<br />

(careless) mistakes. This will save you time and<br />

money as well as trouble.<br />

For examples for the application of HiBuilder, see<br />

the chapters Reaction Calorimetry, Services, and<br />

Application Programming.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 191<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


192<br />

Laboratory Automation Software<br />

RI-CAD the CAD-Software for P&ID-flow diagrams<br />

RI-CAD is available as stand-alone Software for<br />

Windows and as LabVision module.<br />

It is used to establish control flow diagrams without<br />

the necessity of longer familiarisation periods.<br />

RI-CAD was especially developed for drawing<br />

control flow diagrams according to the EN ISO<br />

<strong>10</strong>628 standard.<br />

In the tool palette you will find all the necessary<br />

drawing tools.<br />

This tool can also be expediently put to use during<br />

the planning stage for the standard-conform drawing<br />

of the plant.<br />

The library elements contain additional information<br />

which can be freely expanded by e.g. suppliers or<br />

with maintenance information.<br />

Universities and other educational institutions<br />

can apply for a free of charge RI-CAD licence,<br />

including the EN ISO <strong>10</strong>628 library!<br />

Order Code Description<br />

SL-RICAD P&ID-Editor stand-alone Software to create control flow diagrams.<br />

Laboratory Components Library<br />

The library SL-BIBRILK for the P&ID-Editor contains<br />

presentations of the components in a laboratory<br />

reactor system which are more detailed and more<br />

realistic than in the EN ISO <strong>10</strong>628 library for the<br />

P&ID-Editor.<br />

Here you will find glass reactors in varying<br />

construction versions and sizes and glass devices<br />

like reflux separators, coolers, containers, etc. also<br />

other lab devices graphically presented.<br />

Order Code Description<br />

SL-BIBRILK Glass and lab devices library for P&ID-Editor<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Here you will find:<br />

Plant Construction and Miniplant Technology<br />

� Customised Reaction Equipment<br />

� Customised Parallel Reactor Systems<br />

� Customised Reaction Calorimeters<br />

� Customised Formulating Stations<br />

Note:<br />

Plant components can be found under<br />

• Equipment and Components,<br />

• Process Analytics and Sensors,<br />

• Dosing Systems and Pumps,<br />

• Stirring and Dispersing,<br />

• Liquid Handling and Autosampler.<br />

Individually manufactured laboratory robot system can be found under Liquid Handling and Autosampler.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 193<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


194<br />

Plant Construction and Miniplant Technology<br />

The demands in chemistry are different everywhere.<br />

For this reason, there exists no such thing as the<br />

universal plant. Wherever the properties or<br />

possibilities of our Standard Laboratory Reactor<br />

Systems are not convenient or sufficient, this calls<br />

for the deployment of our LabKit systems<br />

customised according to client specifications:<br />

� customised reactor apparatus<br />

� customised reaction calorimeters<br />

� customised formulation devices<br />

A LabKit Laboratory Reactor System is individually<br />

designed to your specific requirements and<br />

commissioned turnkey-ready by our project<br />

engineers directly in your company.<br />

We manufacture LabKit Systems like:<br />

� Laboratory Installations<br />

� Bench Plants<br />

� Mini Plants<br />

� Pilot Plants<br />

They are applied for product and process<br />

development, process optimisation, etc.<br />

Characteristics:<br />

� Client-specific Solutions<br />

� Single and Multi Reactor Systems<br />

� Batch, Semi-Bacth or continuous Operation<br />

� Fully automated<br />

� Various possibilities for Upgrades<br />

Advantages<br />

� perfectly fitted to your needs<br />

� open system with easy handling<br />

� continuously expandable<br />

� space-saving installation<br />

� electrically lifted reactor vessel<br />

� optimal usage of the laboratory‘s capacity by<br />

operating 24 hours<br />

� best reproducibility<br />

� increase in quality<br />

� relief from routine jobs<br />

� reducing the risk of accident<br />

� GLP-compliant documentation<br />

� accessible via network, e.g. from the office<br />

� remote maintenance (dial-up by customer)<br />

Possibilities<br />

� single and multi stage syntheses<br />

� distillation reflux<br />

� crystallisation<br />

� polymerisation and polycondensation<br />

� hydrogenation with consumption measurement<br />

� reaction calorimetry<br />

� temperature, pressure, and vacuum control<br />

� dosing of solids and gases<br />

� dosing liquids, gravimetric and volumetric with<br />

pumps or with gas pressure via valves<br />

� continuous weighing of distillate<br />

� titration<br />

� phase separation<br />

� stirrer RPM control and torque measurement<br />

� regulation the pH basic and/or acid<br />

� controlling the recipe compliant with the NAMUR<br />

basic operational concept<br />

� coupled multi reactor systems<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Plant Construction and Miniplant Technology<br />

Construction example: LabKit double jacket reactor system each<br />

with a three-jacket glass reactor for deep temperature handling up<br />

to -80°C reactor inside temperature, with freeze desalination and<br />

dosing unit for gases at -90°C, three volumetric and one<br />

gravimetric dosing circuits, inerting system with electronic reactor<br />

lift.<br />

LabKit Modules<br />

You have the choice between different mounting<br />

frames, vessels, gadgets, and other components for<br />

instrumentation and automation.<br />

The composition of a laboratory system with single<br />

components, like pH dosing controller, vacuum<br />

controller, data acquisition, master control (e.g. PLC)<br />

etc. was regarded the best equipment during the last<br />

years. It is the limits of these conventional systems<br />

where LAB-Kit shows its superiority due to its<br />

NAMUR-compliant automation based on the<br />

LabManagersystems.<br />

The following summary shortly depicts some of the<br />

modules. More detailed descriptions of the same<br />

can be found in other chapters.<br />

Frames<br />

The frames are made of anodised aluminum square<br />

profiles and/or round profile high-grade steel.<br />

Optionally, an electrical lifting device for the reactor<br />

can be installed.<br />

Reactors<br />

Verfügbar sind Glasgefäße, auch spezielle Anfertigungen<br />

von <strong>10</strong>0 ml bis <strong>10</strong>0 l, in unterschiedlichen<br />

Bauformen, mit Einfach- oder Doppelmantel. Deckel<br />

mit Öffnungen nach Bedarf. Für höhere Drücke sind<br />

geprüfte Glasreaktoren oder Edelstahl- und Hastelloygefäße<br />

von 20 ml bis 20 l verfügbar.<br />

Cooler, reflux seperator etc. custom-made products<br />

on demand.<br />

Stirrer<br />

The torque signal delivers substantial additional<br />

information for processes which are associated with<br />

viscosity modification. In many cases, the torque<br />

signal, which is easily traceable, can be consulted<br />

as a indicator for the product quality.<br />

The ViscoPakt torque measuring stirrer is a stirrer<br />

drive with a high torque, with speed regulation and<br />

torque monitoring. It has outstanding measuring<br />

accuracy (see ViscoPakt). Anchor, beam, or<br />

propeller stirrers can be used. In special cases, the<br />

torque can be transmitted by a magnetic clutch.<br />

Heating/Cooling System<br />

Heating-/cooling thermostats in different versions<br />

made by Huber and Julabo, as well as other<br />

manufacturers, can be used within a range of -80 to<br />

+300 °C. Alternatively, a regulated rod heater or<br />

heating mantle or a cooling coil can be deployed.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 195<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


196<br />

Dosing Systems<br />

Plant Construction and Miniplant Technology<br />

The LabDos peristaltic pump is the cost-effective<br />

solution for the volumetric dosing of liquids. For<br />

precise dosing of smallest amounts and under high<br />

pressure the SyrDos dosing system is availble.<br />

For higher demands, gravimetric dosing with<br />

GraviDos or laboratory scales with dosing pump is<br />

advisable. The innovative GraviDos dosing system is<br />

first choice for gravimetric dosing even for high<br />

pressure dosing.<br />

For special cases (exothermic reactions, risk of<br />

clumping due to crystallization...), time profiles can<br />

be programmed. The dosing process can also be<br />

linked with other variables (e.g. temperature, pH...)<br />

or integrated into control circuits.<br />

Gases can be valve-controlled, or alternatively, be<br />

proportioned via dosing pumps, balances, load cells<br />

or mass flow meters.<br />

For hydration purposes the hydration unit VL-<br />

HICLAVE-HYDR is available.<br />

<strong>HiTec</strong> <strong>Zang</strong> solids doser SoliDos is suited for dosing<br />

of free flowing solids.<br />

Pressure/Vacuum<br />

The glass reactors can generally be used in<br />

pressure ranges from vacuum to slight over<br />

pressure. Special designs, e.g. 2 L reactors made<br />

for up to 5 bar over pressure are possible. The<br />

required work protection equipment can optionally<br />

be provided.<br />

For pressure measurements, proven piezo-resistive<br />

pressure sensors with stainless steel diaphragms<br />

are used. For more precise measurement during<br />

vacuum operation, a tandem sensor system with<br />

measurement range switching can also be used.<br />

Over the entire pressure range, the internal pressure<br />

can be regulated very exactly with suitable sensor<br />

and valve configurations. The setpoints values are<br />

precisely reached and held within a short time.<br />

Control takes place with proportionally controlled<br />

solenoid valves.<br />

For the vacuum range up to approximately <strong>10</strong> mbar,<br />

we mount vacuum systems, chemical membrane<br />

pumps. For low pressures, we deploy rotary vane<br />

pumps. We principally equip vacuum systems and<br />

pumps with a cold-trap (chargeable with (dry) ice).<br />

Automatic Sample Bottling<br />

Samples can be drawn automatically or processcontrolled<br />

and subsequently bottled with an<br />

AutoSam sample collector.<br />

Aditional liquid-handling operations and downstream<br />

processing can be realised..<br />

Options, Extensions<br />

In-Situ sensors for the filling level, turbidity, flow rate,<br />

pH, Redox, etc. Connection of analysers for<br />

sophisticated control strategies, coupled multireactor<br />

systems and many client-specific plants.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Materials<br />

Plant Construction and Miniplant Technology<br />

Borosilicate glass, PTFE, PFA, Kalrez and highgrade<br />

steel are mainly used as standard materials. If<br />

required, other materials can be deployed.<br />

Automation<br />

LabManager(and LabBox) provide the necessary<br />

interfaces for connection of the laboratory devices,<br />

sensors and actors, reaching from the temperature<br />

sensor to the dosing pump, to the proven connection<br />

boards with NAMUR-conform connections.<br />

The devices are able to replace the electronics of<br />

various individual devices of the conventional<br />

laboratory automation, such as doser, controller, pen<br />

recorder, titrators, transducers, data loggers etc.<br />

Predefined project modules for basic functions, e.g.<br />

Dosing, Tempering, Vacuum Control, etc, also<br />

enable the user inexperienced in automation<br />

applications to establish a fully automated<br />

application within a short period of time.<br />

Application-oriented controllers for dosing, vacuum,<br />

pH, temperature, etc. , ideally accomplish their tasks<br />

and do not require expert knowledge for<br />

parameterisation.<br />

Visualisation<br />

With LabVision, the plant can be operated and<br />

monitored from the display; recipes can be<br />

established, values monitored etc.<br />

Recipe Control<br />

For a versatile recipe control and management<br />

either the table based EasyBatch or HiBatch with a<br />

grafical recipe editor and its extensive basic unit<br />

operation library are available.<br />

Evaluation and Presentation<br />

The LabVision module HiText enables evaluation<br />

already during the runtime of a process.<br />

The electronic laboratory journal eJournal presents<br />

all relevant test parameter and data.<br />

The laboratory journal protocols are deposited in the<br />

data base of the Laboratory Information<br />

Management System HiLIMS and can easily be<br />

retrieved and consolidated to reports.<br />

Reaction Calorimetry<br />

During almost all exothermal and endothermal<br />

processes, the signal of the current heat output<br />

provides additional information about the reaction<br />

process, the merit of which is still often<br />

underestimated.<br />

Further information can be found in the chapter<br />

Custom Reaction Calorimeter.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 197<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


198<br />

Plant Construction and Miniplant Technology<br />

LabKit Custom Reaction Equipment<br />

The modular LabKit assembly system enables the<br />

customer-specific construction of laboratory and<br />

miniplant plants wherever the standard systems are<br />

not sufficient. A base frame made of aluminum or<br />

high-grade steel aligned to the available space is<br />

equipped with the respectively required process<br />

hardware, instrumenting and automation<br />

components.<br />

Summary LabKit Module<br />

Notice: You can find information regarding the<br />

standard laboratory systems LabKit-ALR1, LabKit-<br />

ALR2, LabKit-rcf, LabKit-rcb, and LabKit.ed in the<br />

chapter Automatic Laboratory Reaction systems.<br />

The PI and suited software packages must be<br />

arranged according to the equipment and the<br />

desired level of automation.<br />

Base Frame Anodised square aluminum profile, high-grade steel collecting tray, power<br />

distribution. Optional high-grade steel round profile with powder-coated<br />

connecting elements.<br />

Reactors Standard glass vessels from <strong>10</strong>0ml up to 50 litres with tempering jacket, optional<br />

vacuum jacket, or O-ring sprinkler, manual or automatic bottom discharge valve,<br />

cover with sockets according to requirements and feasibility, custom designs<br />

according to customer specifications, high-grade steel up to 300 bar, special<br />

materials.<br />

Lowering Device Electric lifting device for the reactor with manual switch.<br />

Stirring Drives ViskoPaktxx and ViskoPakt-rheoxx precision stirring drives with RPM control and<br />

torque measurement.<br />

Stirring Blades Propeller, turbo, blade, and anchor stirrer can be selected. Other type and special<br />

designs available upon request.<br />

Dosing, gravimetric Gravimetric dosing with GraviDos (controlled dropping funnel) or via dosing pump<br />

(e.g. <strong>HiTec</strong> <strong>Zang</strong> LabDos) and laboratory scales.<br />

Dosing, volumetric Dosing with membrane pump, dosing with peristaltic pump (see chapter<br />

Instrumenting , Pumps).<br />

Dosing Minute Dosing with syringe doser or LabDos peristaltic pump (see chapter Instrumenting,<br />

Quantities<br />

Pumps).<br />

Gas Dosing Gas dosing via Mass-Flow-Controller.<br />

Sequential Multi-Dosing 2/3 – way or multi-way valve for the selection of the feed tank.<br />

via Scales<br />

Solid Dosing, volumetric SoliDos solids doser.<br />

Solid Dosing,<br />

SoliDos solids doser combined with GraviDos.<br />

gravimetric<br />

Heating/Cooling Heating/Cooling thermostats manufactured by Huber, Julabo, Lauda etc. with<br />

Systems<br />

connection to the LAB-xxx PI.<br />

Sensors Temperature sensor for: reactor, thermostat, supply line, reflux and steam. Interior<br />

pressure, pH value, vacuum up to 2.5 bar and working temperature up to 130°C.<br />

Redundant monitoring of the jacket temperature with shut-down function.<br />

Pressure Measurement, Pressure pick-up 0-1.6 bar absolute, others available upon request.<br />

simple<br />

Pressure Measurement, Tandem pressure pick-up system for increased precision in the vacuum range 0-<br />

tandem<br />

250 mbar/1.6 bar absolute.<br />

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Plant Construction and Miniplant Technology<br />

Continuation Summary LabKit Module<br />

Vacuum Control Laboratory vacuum system with chemical-resistant vacuum pump < 8mbar<br />

absolute, suction-side separator, cold trap, relief valve, lock valve (PVDF/Kalrez).<br />

Other vacuum systems available upon request.<br />

Pressure Control Pressure control module (Standard up to 1,6 bar) combined with inerting. Venting<br />

/Inerting<br />

valve and air relief valve with control. .<br />

Pressure Relief Spring-loaded ball and socket relief valve made of glass for unpressurised<br />

systems closed against atmosphere. Bursting disc for pressure systems. Safety<br />

valves.<br />

Inerting, simple Inerting (only for unpressurised systems with venting, otherwise, pressure and<br />

safety monitoring is necessary). Vent valve with control. Optional pressure relief<br />

valve with control.<br />

Reflux Separator Vacuum-jacketed reflux separator with electrically controllable reflux separation<br />

ratio (see chapter Equipment and Components, Reflux Separator).<br />

Reflux Cooling Intensive reflux condenser made of borosilicate glass.<br />

Optional lock valve for the cooling water. Cooling water monitoring with rotary<br />

flowmeter.<br />

Distillation Glass reflux separator with electrically controllable reflux separation ratio (see<br />

chapter Equipment and Components, Reflux Separator), vacuum jacket, silvercoated<br />

with viewing window (optional), NSH+K 29/32 with PT<strong>10</strong>0 connection,<br />

distillate collecting scales, 2/2- way shut off to separate the distillate collecting<br />

tank from the distillate flow and from the venting.<br />

Phase Separation Automatic phase separation in the bottom discharge valve.<br />

pH Control, Titration Two AlfaDos dosing systems (optional GraviDos or dosing pumps) for acid and<br />

base with pH control module.<br />

Sampling Automatic sampling optionally on the basis of a valve cascade (for a small number<br />

of samples), a multi-way valve (for a medium number of samples), sample<br />

collector (see chapter Liquid Handling and Sample Drawing, AutoSam) or a<br />

pipetting robot (for large numbers of samples).<br />

Reaction Calorimetry Heat-flow calorimetry, heat balance calorimetry, online (option), calibration<br />

heating.<br />

Extended Temperature Extension of the heating/cooling system and the sealing materials to accord to<br />

Range<br />

lower or higher temperatures available upon request.<br />

Materials <strong>Main</strong>ly borosilicate glass, PFA, PTFE, ETFE, PVDF, seals in contact with media<br />

out of Kalrez, high-grade steel material 1.4571 (subject to modification)<br />

Special solutions available upon request.<br />

Multiple examples of our plant construction can be found on our website www.hitec-zang.de.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 199<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


200<br />

Plant Construction and Miniplant Technology<br />

Custom Parallel Reactor System<br />

Custom-made Parallel Reactor System for crystallisation<br />

screening with turbidity sensor. Joint heated dosing vessel.<br />

The general development is moving towards<br />

increasingly smaller volumes and to parallel<br />

preparations. We dispose of experience in parallel<br />

reactor systems reaching from the ml to the litre<br />

scale, and from 4 to 48 reactors. Experience has<br />

taught us that these systems must also meet<br />

individual requirements. For this reason, there is no<br />

such thing as “the” reactor parallel system.<br />

Application<br />

� Parallel Syntheses<br />

� Active Ingredient Screening<br />

� Bioprocess Monitoring etc.<br />

In addition to our standardised parallel reactor<br />

systems MultiLab and MiniLab, we also construct<br />

client-specific parallel reactor systems for all<br />

possible kinds of application.<br />

Your Advantages<br />

� Individually designed<br />

� Various possibilities<br />

� Reators reaching from the ml to the litre scale<br />

� Adapted Dosing Technology<br />

� Adapted Stirring Technology<br />

� Adapted Tempering Technology<br />

Further examples for Parallel Reactor Systems:<br />

Fourfold parallel reactor system with 250ml double jacket reactors<br />

for deep temperature synthesis and sample taking.<br />

Threefold parallel reactor system with 2 l reactors, parallel,<br />

selective dosing from the receiver tanks a, b and p.<br />

Parallel reactor systsm with 2 reactors<br />

and MultiLab tempering system.<br />

Further examples for parallel reactor systems can be<br />

found on our website.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Plant Construction and Miniplant Technology<br />

Custom Reaction Calorimeters<br />

Customer specific reaction calorimeter with heated cover and<br />

front side special nozzle.<br />

Next to the standard reaction calorimeters LabKit-rcf<br />

and LabKit-rcb, <strong>HiTec</strong> <strong>Zang</strong> also offers customised<br />

calorimeters. <strong>HiTec</strong> <strong>Zang</strong> also modernises existing<br />

calorimeters.<br />

Up to now, reaction calorimeter and laboratory<br />

reactors which can perform more than simple<br />

syntheses needed to be regarded separately. <strong>HiTec</strong><br />

<strong>Zang</strong> LabKit-rc reaction calorimeters combine the<br />

two devices, which leads to a flexible system<br />

versatile in every aspect. As a calorimeter, the<br />

LabKit-rc offers various operational modes and<br />

measuring methods, as laboratory reaction system,<br />

the complete flexibility of the LabKit laboratory<br />

reaction technology and the LabManagerresearch<br />

process control system.<br />

Next to the classic deployments in the security<br />

laboratory, the reaction calorimetry is increasingly<br />

also establishing itself as an effective method within<br />

process development and process optimisation. For<br />

selective reaction control and risk analysis of<br />

chemical reactions, it is necessary to know the<br />

reaction heat output and the respective temporal<br />

progression at operational conditions.<br />

The following components are available:<br />

� Precision Temperature Measurement Module<br />

� Calibrated Temperature Sensors<br />

� Flowmeter for Heat Carriers<br />

� Controllable proportional Calibration Heating<br />

� HiCon adaptive Controller for ideal isothermal<br />

effect<br />

� Basis Operation Calorimetry with Online<br />

Evaluation<br />

� KalDas Evaluation Software for Heat Flow and<br />

Heat Balance Calorimetry<br />

You will find a detailed description in the chapter<br />

Components for Reaction Calorimetry. The<br />

application possibilities are various and go far<br />

beyond the classic measurement of the heat tone<br />

and thermal conversion.<br />

For the dimensioning of cooling systems, reliable<br />

data regarding the energy potential of a reaction<br />

mixture, as well as the heat transfer rate and the<br />

properties and/or the heat storage capability must be<br />

at hand, this often in dependency of the mixture and<br />

temperature.<br />

The reliable evaluation of complex chemical<br />

processes requires variable test equipment, which<br />

can be aligned to the conditions of the process<br />

intended for examination.<br />

For this reason, the systems can be arranged in<br />

such a manner that all functions of the laboratory or<br />

operational assembly can also be realised in the<br />

calorimeter.<br />

Examples for our customised recation calorimeters<br />

can be found on our website.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 201<br />

Equipment and<br />

Components<br />

Process Analytics<br />

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Pumps<br />

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Stirring and<br />

Dispersing<br />

Services


202<br />

Plant Construction and Miniplant Technology<br />

Components for Reaction<br />

Calorimeters<br />

These modules will enable you to upgrade your<br />

default reactor systems to a reacton calorimeter and<br />

thus making it possible to receive additional<br />

important and significant values within the an early<br />

stage of the process develeopment. Constraints to<br />

the functionality and the experiments will nearly not<br />

occur.<br />

Easy Evaluation<br />

You will find an evaluation program for heat flow and<br />

heat balance calorimetry which can be adapted to<br />

any device in the chapters Reaction Calorimetry/<br />

Calorimetry Evaluation Program KalDas.<br />

Calibration Heater<br />

A calibration heater is required for calorimetric<br />

measurements at laboratory reactors.<br />

In particular for the establishment of the heat<br />

capacity of a material within the scope of a heat flow<br />

calorimetry, a very precise calibration heating is<br />

required, which corrects changes of the heating<br />

resistor, e.g. due to deterioration and temperature<br />

influences. For further information see chapter<br />

Components for Reaction Calorimetry.<br />

Thermostats<br />

Reaction calorimeters require thermostats with high<br />

cooling capacity and low thermal mass.<br />

We will gladly advise you to help to find the device<br />

best suited to your requirements.<br />

Temperature Control<br />

For isothermal calorimeter operation, exceptionally<br />

effective cascade controllers are required. You will<br />

find suited controllers in the chapter Laboratory<br />

Automation Software in the section controller<br />

modules.<br />

Temperature Measurement with maximum<br />

Precision<br />

This high precision temperature measurement<br />

module meets the highest requirements in terms of<br />

resolution and measurement precision. You find<br />

detailed information in the chapter Laboratory<br />

Automation Hardware,under cards, HK-AD24P8.<br />

Sensors for the Reaction Calorimetry<br />

Sensors that accord to the particular high demands<br />

of reaction calorimetry can be found under LAB-PI<br />

Interfaces/Precision-Pt<strong>10</strong>0 Inputs.<br />

Turbine-Flow Sensors for Heat Carrier Oil<br />

The heat balance calorimetry requires the exact<br />

measurement of the flow rate of the heat carrier oil.<br />

These flow sensors (IS-F-TDM...) are especially<br />

suited for this purpose and are frequently used as an<br />

alternative to the significantly more expensive and<br />

more voluminous Coriolis mass flowmeters.<br />

Measurement Stirrer<br />

The heat incorporated by the stirring can be<br />

measured with the high-resolution ViskoPakt rheo<br />

stirring drives. You will find further information in the<br />

chapter “Stirring and Dispersing”.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Plant Construction and Miniplant Technology<br />

Formulation and Handling Stations<br />

The programme-controlled formulation stations are<br />

used for the automatic establishment and<br />

adjustment of formulations to certain target variables<br />

such as final volume and viscosity. The required<br />

basis operations, e.g. filling with liquids and solids,<br />

stirring, measuring, dosing etc., are executed<br />

programme-controlled. This consequently leads to<br />

varied applications in the chemical, pharmaceutical,<br />

biotechnical, cosmetics and food industry. Due to the<br />

availability of custom designs and the flexible<br />

automation system, the hardware and software<br />

application possibilities are virtually unlimited.<br />

The devices are arranged by combing the different<br />

components of our mechatronic modular system<br />

with our laboratory automation systems, laboratory<br />

devices and our sensor/actor components.<br />

The processes are programmed with the selfexplaining<br />

script language HiText or the graphic<br />

sequential function chart HiBatch. For this reason,<br />

they can be easily adapted to modified conditions by<br />

the user. The protocols can be automatically<br />

established. The protocol layout can be flexibly<br />

designed.<br />

The protocols can be automatically stored in the<br />

data base of the HiLIMS Laboratory Information<br />

Management System. HiLIMS supports the<br />

uncomplicated and efficient administration of all<br />

parameters and data.<br />

With the help of freely establishable search queries,<br />

the protocols are quickly retrieved when needed.<br />

Drehtellertyp<br />

The presented formulation station produces up to 8<br />

formulations fully automatically in exchangeable<br />

containers with a volume reaching from 1 to 5 litres.<br />

The user charges the tray before the test-start with<br />

stirring tanks that contain a random sample amount.<br />

Linear Type<br />

As an alternative to the formulating stations based<br />

on rotary plates or AutoSam sample collectors, a<br />

After the start of the test, the predefined samples are<br />

adjusted exactly to the predefined viscosity and<br />

target amount by adding doses of certain educts in<br />

consecutive order. The stirrer is cleansed<br />

automatically to ensure contamination is excluded.<br />

Due to the high-resolution torque coverage of the<br />

ViscoPakt-X7 torque measurement stirrer, it is<br />

possible to reach ideal reproducibility and therefore<br />

a consistent product quality during different tests.<br />

In comparison to the manual procedure conducted<br />

in the past, the automatic formulation usually leads<br />

to time saving in regard to the test period of 70 %,<br />

and 80 % in regard to the handling period. The payback<br />

period of the plants is accordingly short. To be<br />

stated as additional advantages are the increased<br />

reproducibility and product quality, as well as the<br />

automatically established documentation.<br />

The required sensor system can be fully integrated<br />

and enable measurement directly in the tanks. In<br />

comparison to the in situ sensor system, the<br />

measurement sensor is spared and can be easier<br />

exchanged and calibrated.<br />

Properties<br />

� Flexible Construction<br />

� Comprehensive Tank Selection<br />

� Fully automated<br />

� Freely programmable<br />

� Flexible Sensor System<br />

� Short Pay-Back Period<br />

Please note the versatile xyz-robots in the chapter<br />

Liquid Handling.<br />

pneumatically driven linear type is available for<br />

special applications.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 203<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


204<br />

Plant Construction and Miniplant Technology<br />

Special Application Cases<br />

� Ex- Zone<br />

Components<br />

Viscosity Measurement<br />

Precision measurement stirrers of the ViscoPakt-<br />

Rheo Series enable a in situ measurement of the<br />

viscosity and, with the help of the automatic fluid<br />

handling system, e.g. the automatic adjustment of<br />

the viscosity. In particular low viscous media, can be<br />

measured with the ViscoPakt-Rheo X7.<br />

Further components of our Miniplant Technology:<br />

� Laboratory Scales<br />

� Reactor Weighing<br />

� Electric Bottom Discharge Valves<br />

� Automatic Liquid Phase Separation<br />

� Valves and Shut-Offs<br />

� Multi-way Valves<br />

� Little available Construction Depth<br />

Properties<br />

� Pneumatic Drive<br />

� Bottling of sampling bottles. Bottle size 250 ml<br />

(plastic or glass, other sizes available upon<br />

request.<br />

Options<br />

� Programme-controlled handling of liquids and<br />

solids.<br />

� Automatic Sensor System (pH, RedOx,<br />

conductivity, ion-selective electrodes,<br />

turbidity, pO2, viscosity, in situ spectroscopy).<br />

� LIMS Coupling<br />

Technical Data (ViscoPakt-Rheo X7)<br />

MaximumTorque 7Ncm<br />

Resolution 0,003 Ncm<br />

Reproducibility 0,05 Ncm<br />

Minimum RPM 40U/min<br />

Maximum RPM 3000 u/min<br />

Uncertainty RPM 0,1 %<br />

Chuck 1-<strong>10</strong>mm<br />

Drive Weight ca. 900g<br />

Diameter Motor 70mm<br />

Length across axis<br />

approx.<br />

250mm<br />

For further information, see chapter Stirring and<br />

Dispersing, ViskoPakt.<br />

can be found in the chapter„Equipment and<br />

Components“. Further devices and components can<br />

be found in the chapters:<br />

� Process Analytics and Sensors<br />

� Dosing Systems and Pumps<br />

� Liquid Handling and Sample Drawing<br />

� Stirring and Dispersing<br />

� Custom Reaction Calorimeters<br />

Please note our customised robots in the chapter Liquid-Handling and Sampling.<br />

Talk to our engineerss about our special requirements!<br />

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206<br />

Laboratory Scales<br />

<strong>HiTec</strong> <strong>Zang</strong> is a competent partner for scales of a<br />

wide range of manufacturers. Your advantages are:<br />

Equipment and Components<br />

� Ideal alignment to the LabManager system<br />

� Competent consultancy in the selection of the<br />

suited scales<br />

� Competent consultancy in case of interface<br />

problems<br />

� Low-cost calibration service<br />

GraviDos ® Suspended Scales<br />

As a space-saving alternative to electronic<br />

laboratory scales, the GraviDos Suspended Scale<br />

has in many cases proven to be very useful. Using<br />

the available adaptors, it can be directly attached to<br />

the rodding of a laboratory plant.<br />

They can be queried faster than standard laboratory<br />

scales, which positively influences dosing and flow<br />

control. In addition, air movements are less<br />

disturbing to them than to platform scales.<br />

The GraviDos Suspended Scale is connected to a<br />

GraviDos Measuring Amplifier. The digital version<br />

disposes of a serial interface.<br />

The GravidosDos Dosing system is based on the<br />

GraviDos Suspended Scales. Further information<br />

can be found in the Chapter „Dosing Systems and<br />

Pumps“.<br />

In order to be able to establish an offer that meets<br />

your requirements, we need to know the weighing<br />

range and the required resolution. The serial<br />

interface is standard at most models. In spite of this,<br />

you should also state if you require one. Further<br />

requirements, such as documentation according to<br />

GLP, and other demanded special features should<br />

also be stated.<br />

Technical Data<br />

Measuring Resolution approx. 0,01% of Unit<br />

Measuring Uncertainty approx. 0,1% of Unit<br />

Dimensions Load Cell<br />

(without rodding)<br />

200x40x50mm<br />

Higher precision is available upon request.<br />

Delivery Scope Suspended Scales with signal cable for the connection to GraviDos<br />

Measuring Board or Measuring Amplifier<br />

Order Code Description<br />

IW-GRAVITS3000 GraviDos Suspended Scales 3000g, including cable<br />

IW-GRAVITS7500 GraviDos Suspended Scales 7500g, including cable<br />

IW-GRAVITS15000 GraviDos Suspended Scales 15kg, including cable<br />

IW-GRAVITS30000 GraviDos Suspended Scales 30kg, including cable<br />

IW-GRAVITS<strong>10</strong>00D GraviDos Suspended Scales 1.000g, integrated measuring amplifier , RS232, including cable<br />

IW-GRAVITS3000D GraviDos Suspended Scales 3.000g, integrated measuring amplifier, RS232, including cable<br />

IW-GRAVITS7500D GraviDos Suspended Scales 7.500g, integrated measuring amplifier, RS232, including cable<br />

IW-GRAVITS15000D GraviDos Suspended Scales 15kg, integrated measuring amplifier, RS232, including cable<br />

IW-GRAVITS30000D GraviDos Suspended Scales 30kg, integrated measuring amplifier, RS232, including cable<br />

HK-GRADOMV1 Measuring Amplifier 1 Channel, external measuring amplifier for connection to analogue input<br />

HK-GRADOMV1D Digital Measuring Amplifier external, 1 Channel, with RS232 V24 Interface<br />

HK-GRADOMV1D-SN Plug-In Power Supply for Digital Measuring Amplifier HK-GRADOMV1D<br />

HK-AD24DMS4 Measuring System 4 Channels, Board for <strong>HiTec</strong> <strong>Zang</strong> PNC Panel<br />

IL-GRADOADV Square Adaptor, adapter piece for load cell to square aluminium assembly systems<br />

IL-GRADOADR Round Adaptor, adapter piece for load cell to 12mm tube assembly systems<br />

You will find further information to the measuring amplifiers and more in the chapters „Laboratory Automation<br />

Hardware“ and „External Measuring Amplifiers“.<br />

Information to the GravDos Dosing Systems can be found in the Chapter „Dosing Systems and Pumps“.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


GraviDos ® Desktop Scales<br />

Equipment and Components<br />

The GraviDos desktop<br />

scales represent a spacesaving<br />

alternative to<br />

electronic laboratory<br />

scales. Without the foot<br />

element, they can, in<br />

addition, be directly<br />

attached to the rodding of a<br />

laboratory plant. The<br />

GraviDos desktop scales<br />

are connected to a<br />

GraviDos measurement<br />

amplifier.<br />

Order Code Description<br />

IW-GRAVITS<strong>10</strong>00 GraviDos desktop scales 1.000g<br />

IW-GRAVITS3000 GraviDos desktop scales 3.000g<br />

IW-GRAVITS7500 GraviDos desktop scales 7.500g<br />

IS-W-GRAVISTAND Desktop stand with levelling screws<br />

IS-W-GRAVIPLATE Weighing plate, diameter 140mm<br />

IS-W-GRAVICRANE Hose guide to weighing vessel<br />

GraviDos ® Platform Scales<br />

GraviDos platform scales represent a robust<br />

alternative to electronic laboratory scales for<br />

deployment under rough conditions.<br />

The GraviDos System enables shorter and more<br />

consistent measuring periods than electronic<br />

laboratory scales. This in turn enables a more<br />

consistent flow during dosing regulation. The<br />

GraviDos platform scales are connected to a<br />

GraviDos measurement amplifier.<br />

The scales dispose of adjustable foots for levelling.<br />

The Advantages:<br />

� Robust Construction for In-Process Applications<br />

� Ideal Alignment to the LabManager-System<br />

� Ideal Regulating Properties due to a high Sampling Rate<br />

Technical Data<br />

Dimensions Weighing Platform 300mm x 300mm<br />

Measurement Range 3kg, 7.5kg, 15kg, 30kg<br />

Measurement Resolution 0.01%<br />

The three-element hose guide ensures the stable<br />

guidance of the hose into the vessel.<br />

Further information can be found in the chapter<br />

“Dosing Systems and Pumps”.<br />

Technical Data<br />

Height Weighing Plate 70mm<br />

Diameter Weighing Plate 140mm<br />

Maximum Height of Holder 400mm<br />

Maximum Width 160mm<br />

Measurement Range 1kg, 3kg, 7,5kg<br />

Delivery scope Desktop scales with signal cable for<br />

connection to a GraviDos<br />

measurement card or measurement<br />

amplifier<br />

Delivery Scope Platform scales with signal cable for connection to a GraviDos measurement card<br />

or measurement amplifier<br />

Order Code Description<br />

IW- GRAVIPF3000 Platform scales for a maximum load of 3,000g<br />

IW- GRAVIPF7000 Platform scales for a maximum load of 7,500g<br />

IW- GRAVIPF15000 Platform scales for a maximum load of 15,000g<br />

W-GRAVIPF30000 Platform scales for a maximum load of 30,000g<br />

Ex-Equipment is available upon request.<br />

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208<br />

Reactor Weighing<br />

Equipment and Components<br />

An exact measurement of the filling level in the<br />

reactor is difficult to realise, as the measurement<br />

transmitters are too large and dispose of too low<br />

resolution. One alternative is the weighing of the<br />

complete reaction vessel. In order to achieve a high<br />

resolution at the lowest cost, the tare weight of the<br />

plant is compensated by balance weights. The<br />

variable weight of the tempering oil (due to thermal<br />

expansion) can be compensated by the LabManager<br />

on a calculated basis.<br />

Technical Data<br />

Weighing Range As required<br />

Measurement 1 g at 50 kg<br />

Resolution<br />

Order Code Description<br />

IW-GRAVIREAKW GraviDos reactor weighing module<br />

Kern Scales<br />

Kern scales are our low-cost alternative.<br />

� Good Quality at a low Price<br />

� 3 Years Guarantee by Manufacturer<br />

� Optional Self-Calibration<br />

� Outstanding Cost/Performance Ratio<br />

Preferential Types of System Scales:<br />

Example for reactor weighing with GraviDos load cell: 60 kg<br />

construction. Above: view of the complete plant, left: load cell,<br />

right:balance weights for tare compensation.<br />

Model Weighing Range [g] Reading Precision [g] Weighing Plate Remark<br />

572-35 1.5<strong>10</strong> 0,01 ø 150 Robust metal casing<br />

Including RS232<br />

572-49 15.<strong>10</strong>0 0,1 160x200 Robust metal casing<br />

Including RS232<br />

PLS 5<strong>10</strong>-3 5<strong>10</strong> 0,001 128x128 Back-lit Display<br />

Very robust metal casing<br />

Including RS232<br />

PLS 4000-2 4.000 0,01 165x165 Back-lit Display<br />

Very robust metal<br />

casing<br />

Including RS232<br />

QKE 36K0.5 36.<strong>10</strong>0 0,5 340x240 Self-explanatory filling<br />

level control<br />

Including RS232<br />

Order Code Description<br />

IW-572-35 Precision laboratory scales, Kern Type 572-35, Max. 1,5<strong>10</strong>g, resolution 0.01g, reproducibility<br />

0.01g, incl. RS232<br />

IW-572-49 Precision laboratory scales, Kern Type 572-35, Max. 15,<strong>10</strong>0g, resolution 0.1g, reproducibility<br />

0.1g, incl. RS232<br />

IW-PLS 5<strong>10</strong>-3 Precision laboratory scales, Kern Type PLS 5<strong>10</strong>-3, Max. 5<strong>10</strong>g, resolution 0.001g, reproducibility<br />

0.001g, incl. RS232<br />

IW-PLS 4000-2 Precision laboratory scales, Kern Type PLS 4000-2, Max. 4000g, resolution 0.01g, reproducibility<br />

0.01g, incl. RS232<br />

IW-QKE 36K0.5 Large desktop scales, Kern Type QKE 36K0.5, resolution 0.5g, reproducibility 0.5g, incl. RS232<br />

ZK-W-KE04-BS-R2-I-02 Connection cable Kern scales Type IW-572 and Typ QKE, RS232, 3m<br />

ZK-W-KE06-BS-R2-I-01 Connection cable Kern scales Type IW-PLS, RS232, 3m<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Sartorius Scales<br />

Sartorius scales represent the proven industrial<br />

standard with a particularly wide range of different<br />

types:<br />

� Proven industrial Standard<br />

� Extremely robust<br />

� Made in Germany<br />

� Calibrated Version available<br />

� Optional Self-Calibration<br />

� Ex-Version available<br />

� Good Cost/Performance Ratio<br />

Features of the Extend Series:<br />

� Internal motor-driven alignment weight<br />

element<br />

� Fully automatic calibration and alignment<br />

function isoCAL<br />

� ReproTEST for quick determination of<br />

reproducibility<br />

� ISO/GLP-conform protocoling<br />

Available in 2 Versions<br />

Depending on the application complexity, you can<br />

select between Extend precision scales models<br />

including or without an internal alignment weight<br />

element. Both scales model series are ideally suited<br />

for deployment as testing instrument in the quality<br />

assurance system. The measurement range of the<br />

scales is 0.001 to 8200 g. As an example, the<br />

following depicts the ED6202S with a weighing<br />

range of 0.01 up to 6200g.<br />

Sartorius ED6202S<br />

Equipment and Components<br />

Secured against unauthorised Modifications<br />

The access to the scales menu can be locked via a<br />

code determined by you. With this, you are able to<br />

secure your settings against manipulations and<br />

unauthorised modifications.<br />

In combination with a connected printer, the scales<br />

of the Extend series meet the demands of the<br />

ISO/GLP-conform protocoling to <strong>10</strong>0%.<br />

Quality QA:<br />

Sartorius also offers platform scales with a weighing<br />

range of 0.1g up to 65 kg.<br />

Quality QA is based on a modular concept: display<br />

unit and weighing platform can be mounted<br />

separately.<br />

Technische Daten<br />

Weighing Range 6200 g<br />

Reading Precision 0.01g<br />

Weighing Plate 180 x 180 mm<br />

Order Code Description<br />

IW-LP4200S Sartorius scales LP42000S incl. RS232<br />

ZK-W-SA01-BS-R2-I-03 Connection cable Sartorius scales to <strong>HiTec</strong>-PI, 9-pole RS232. 3 m<br />

Sartorius ME414S<br />

Technische Daten<br />

Weighing Range 4<strong>10</strong> g<br />

Reading Precision 0.0001g<br />

Weighing Plate ø 90, weighing space<br />

166 x 248<br />

Order Code Description<br />

IW-ME414S Sartorius scales ME414S incl. RS232<br />

ZK-W-SA01-BS-R2-I-03 Connection cable Sartorius scales to <strong>HiTec</strong>-PI, 9-pole RS232. 3 m<br />

Take advantage of the experience of our project engineers. We will gladly advise you!<br />

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Services


2<strong>10</strong><br />

Equipment and Components<br />

Electrical Base Discharge Valves<br />

Automatic base discharge valves enable the<br />

program-controlled discharge of the reactor content.<br />

Base discharge valves actuated by electric drive, in<br />

comparison to the pneumatically-driven ones, have<br />

the advantage that the opening degree can be<br />

adjusted continuously.<br />

The combination with the phase detector PhaDec<br />

enables conducting additionally automatic phase<br />

separation and extraction.<br />

Automatic base discharge valves, in comparison to<br />

manually operated valves, offer the following<br />

Advantages:<br />

� Minimisation of the risk of injuries<br />

� Automatic discharge at the ideal point of time<br />

� Enables automation of phase separation in<br />

combination with PhaDec<br />

The <strong>HiTec</strong> <strong>Zang</strong> electrical base discharge valves are<br />

based on proven manual base discharge valves<br />

made by different manufacturers. These are<br />

equipped with a special electrical drive and a control<br />

system.<br />

An important feature is that no extra headroom is<br />

required for this.<br />

NORMAG-valve with electrical drive<br />

Especially important and advantageous is the<br />

possibility to operate the valve manually at any time,<br />

e.g. in case of a power failure.<br />

Die Ansteuerung erfolgt über Bedientaster RS232<br />

Schnittstelle. Eine Positionsregelung sorgt für<br />

optimale Reproduzierbarkeit.<br />

Optional können 24V Binärein- und Ausgänge<br />

vorgesehen werden, jeweils für auf und zu.<br />

Technical Data<br />

Ambient temperatur 40 °C<br />

Operating voltage 24V DC<br />

Control RS232, opt. 2x Binär 24V<br />

Response RS232, opt. 2x Binär 24V<br />

Industrial Protection IP30<br />

Delivery Scope Drive and control unit with connection cable and manual<br />

GKB-valve with electrical drive<br />

HWS-Ventil <strong>10</strong> mm Type T/PT HWS-Ventil 20 mm Type H<br />

Order Code Description<br />

VL-BAVM-GKB Manual base discharge valve Type Glas Keller, for 250 and 400 ml<br />

VL-BAVA-GKB Electrical drive for base discharge valve Type Glas Keller<br />

VL-BAVA-NOR<strong>10</strong> Electrical drive for base discharge valve Type NORMAG nominal width <strong>10</strong> mm, GL25<br />

VL-BAVA-NOR15 Electrical drive for base discharge valve Type NORMAG nominal width <strong>10</strong> mm, GL32<br />

VL-BAVA-NOR25 Electrical drive for base discharge valve Type NORMAG nominal width <strong>10</strong> mm, GL45<br />

VL-BAVA-HWST Electrical drive for base discharge valve Type HWS Standard T and T/PT nominal width <strong>10</strong>mm<br />

VL-BAVA-HWS<strong>10</strong> Electrical drive for base discharge valve Type HWS Typ short version <strong>10</strong><br />

VL-BAVA-HWS20 Electrical drive for base discharge valve Type HWS Typ short version 20<br />

VL-SOLIDOS-BIN Option Binärein- und Ausgänge<br />

The drives can also be adjusted by us to fit other valves.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Equipment and Components<br />

Automatic Liquid Phase Separation<br />

The <strong>HiTec</strong> <strong>Zang</strong> PhaSep phase separation module<br />

is in particular deployed in the automatic separation<br />

and separate bottling of liquid phases out of reactors<br />

or collecting vessels, e.g. after reactions with phase<br />

transfer catalysis, after azeotropic distillations or<br />

extractions.<br />

The application of PhaSep is not limited to<br />

transparent or conductible fluids.<br />

Properties<br />

� Robust und economic<br />

� Integratable into any system<br />

� Universally deployable for all liquid phases –<br />

even for not transparent or non-conductible fluids<br />

� Resistant to pressure and chemicals<br />

� Also deployable as temperature sensor<br />

� Easy to operate<br />

� Inert materials: glass, high-grade steel, Hastelloy,<br />

PEEK, PTFE<br />

� Full integration into the HiBatch recipe control<br />

The sensor can alternatively be mounted into the<br />

base discharge valve, the discharge tubing, or from<br />

above into the reaction vessel.<br />

PhaSep requires a control valve (see electrical base<br />

discharge valves) for regulation of the discharge<br />

speed and, if necessary, a separation valve for<br />

separate bottling.<br />

<strong>Main</strong> Areas of Deployment<br />

� Extraction<br />

� Extractive Distillation<br />

� Azeotropic Distillation<br />

� Phase Transfer Catalysis<br />

PhaSep operates with most fluids, regardless<br />

whether they are liquid or gas, conductive or nonconductive,<br />

transparent or not. As long as there is a<br />

clear phase limit, the phases are securely<br />

separated.<br />

Order Code Description<br />

IL-PHASEP Liquid phase separation module<br />

PhaSep phase separation module with PhaDec Sensor at a 5-l<br />

research reactor. Detector 6 mm PTFE in automatic base<br />

discharge, on the left: control and separation valve as well as<br />

collecting vessel. Additional buttons for manual operation.<br />

Initialising mask of the basis operation PhaSep.<br />

You can find suited electrical base discharge valves in the section Electrical Base Discharge Valves<br />

PhaSep as a stand-alone system is available upon request.<br />

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Laboratory<br />

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212<br />

Glass Components<br />

Reflux Separator<br />

Reflux separators enable the adjustment of the<br />

reflux ratio, i.e. the division of the occurring<br />

condensate in reflux and discharge at rectification<br />

columns.<br />

Two differently constructed types are available:<br />

Typ 1 comprises a pivot/rotary funnel with a sealed<br />

magnet which can be turned from the outside with<br />

an electric magnet to the positions reflux and<br />

discharge.<br />

Typ 2 operates with a ball and pocket valve, which<br />

can be moved from the outside via an electric<br />

magnet to the positions reflux and discharge. The<br />

Equipment and Components<br />

advantage in this case is that the discharge nozzle is<br />

tightly sealed due to the ball and pocket valve in the<br />

reflux position.<br />

Both types can be directly connected to a digital<br />

output of a LAB-PI and be activated via pulse<br />

frequency, pulse width or pulse area modulation can<br />

be activated.<br />

An extra reflux control device is therefore no longer<br />

required.<br />

The reflux division ratio can be pre-determined,<br />

dependant of temperature, e.g. by the HiBatch basis<br />

operation „Distilling“.<br />

Reflux separator Type 1 with funnel Reflux separator Type 2 with ball and pocket valve<br />

Order Code Description<br />

IL-RFT-TR-1 Reflux separator with funnel , NS29<br />

IL-RFT-TR-MAG Electric magnet for reflux separator with funnel<br />

ZK-X-HW01-OD-XA-I-01 Cable for reflux separator with funnel, Tuchel plug for connection to LAB-PI<br />

IL-RFT-SV-1 Reflux separator with ball and pocket valve, from NS19<br />

IL-RFT-SV-MAG Electric magnet for reflux separator with ball and pocket valve<br />

ZK-HM-HI01-OD-XA-I-01 Cable for reflux separator with ball and pocket valve, Tuchel plug for connection to LAB-PI<br />

Sensor Protection Tube<br />

This sensor protection tube protects the sensitive<br />

measuring head of pH electrodes or other electrodes<br />

and serves as an extension at the same time.<br />

Order Code Description<br />

L-SONSCHR-1 Sensor Protection Tube made of glass, dimensions according to specifications<br />

Further glass parts, components and equipment for the laboratory and mini-plant technology, and special<br />

designs are available upon request.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Equipment and Components<br />

Low Pulsation Total Evaporator<br />

Low pulsation vapour dosing with quick responding<br />

behaviour to load changes is required for many<br />

technical applications.<br />

The new evaporator concept enables low pulsation<br />

total evaporation with very good dynamics. The<br />

essential features are the evaporation in very narrow<br />

channels, the strict partitioning of the apparatus into<br />

a cooled feed sector and a hot evaporation and<br />

overheating sector, as well as the fact that the<br />

construction can be disassembled for cleaning<br />

purposes.<br />

the cooling of the liquid in-feed prevents preliminary<br />

evaporation of the fed liquid, which leads the phase<br />

transition to take place with low pulsation and in a<br />

defined range on a very short section. An additional<br />

absorption volume is consequently no longer<br />

necessary.<br />

The defined evaporation in narrow channels with low<br />

liquid volume ensures controlled and low pulsation<br />

evaporation with very fast responding behaviour to<br />

load changes.<br />

Technical Data<br />

Working Range 2 - 120 g/h<br />

Pressure 0 to <strong>10</strong> bar<br />

Temperature 0 to 400 °C<br />

Heating Exchangeable, electric heating<br />

cartridge 230 V, max. 400 W<br />

Medias Amongst others, water,<br />

methanol, iso-octane, petrol,<br />

SiCl4<br />

Material High-grade steel 1,4301,<br />

1,4571 (special materials, e.g.<br />

Hastelloy available upon<br />

request)<br />

Media<br />

Pipe, Ø6 mm<br />

Connection<br />

Order Code Description<br />

IL-VERDA120 Laboratory Evaporator max. 120g/h (H2O)<br />

IL-VERDA-TREG Universal Temperature Controller<br />

IL-VERDA-THEL Thermo Element in a high-grade steel tube<br />

Suited liquid pumps can be found under LabDos Peristaltic Pumps.<br />

Versions Welded or demountable (with<br />

O-Ring seal made of Viton,<br />

Temperature: max. 200 °C;<br />

(Teflon upon request)<br />

Applications<br />

Precise evaporation of liquid dosed feed materials in<br />

laboratories and pilot plants.<br />

� Fuel Cell<br />

� Car Exhaust Catalysis<br />

� Reaction Technology<br />

� Vapour Reforming<br />

� Process Technology ...<br />

The laboratory evaporator is also available as<br />

complete device with temperature control and<br />

dosing.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

Components<br />

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Dosing Systems,<br />

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Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


214<br />

Valves and Stop-Cocks<br />

Valves, stop-cocks, flaps, etc. are required in large<br />

numbers for the control of the material flows in<br />

laboratory reactor plants, pilot plant stations, and<br />

mini-plants.<br />

Here you will find the special valve you require for<br />

your laboratory, pilot plant, or mini-plant station. You<br />

can select between open/closed valves and<br />

proportional valves. All valves can be directly<br />

connected to our LAB- and PMC-PIs.<br />

Also in this sector, you can count on our<br />

competence in the planning stage and acquisition of<br />

the suited products by acclaimed manufacturers.<br />

Application Areas<br />

� Addition/Feed of Reactants<br />

� Extraction of Products<br />

� Discharge of Reaction Vessels<br />

� Venting and Deairing<br />

� Inerting<br />

� Vacuum Generation<br />

� Cooling and Heating Agents Control<br />

� Switching between different reservoir containers,<br />

feeds, etc.<br />

� Safety: Preliminary Locking, Pressure Relief,<br />

Emergency Cooling ...<br />

� Ex-Area Zone 1 and 2: intrinsically safe and<br />

pressure-sealed magnetic valves, pneumatic<br />

valves balanced or controlled from the non-risk<br />

area.<br />

Equipment and Components<br />

You can, in particular, expect from us competent<br />

advice and an individual concept aligned to your<br />

special requirements, respectively for your case of<br />

application.<br />

Our know-how covers many manufacturers and<br />

construction types, so that we are able to exactly<br />

correspond to your requirements. Do not hesitate to<br />

ask!<br />

For the most important tasks in the laboratory, you<br />

will find a selection of proven standards under<br />

“Preferential Types”, which will facilitate the selection<br />

for you.<br />

Advantages and Performance:<br />

� All valves can be activated via the digital<br />

outputs of our PIs<br />

� Complete delivery with cable and plug for<br />

direct connection to your LAB-xxx PI<br />

� Hydraulic design and alignment to the media<br />

of your plant, available auxiliary energy etc.,<br />

established by our engineering department<br />

� Consultancy and alignment to your<br />

automation devices completely from one<br />

single source<br />

To establish the lay out design of a valve, we require<br />

some information, which you can, if desired,<br />

coordinate together with our project engineers:<br />

Work Conditions:<br />

Flow Rate (often, estimation is sufficient)<br />

Suction Pressure (p1), Back Pressure (p2)<br />

Working Temperature (media, ambient)<br />

Special ambient conditions (explosion protection,<br />

flammable/corrosive materials...)<br />

Media:<br />

Description, Aggregate Condition, in case of<br />

mixtures, hydraulic, rheological, chemical and<br />

physical features<br />

Valve Type:<br />

Gate valve, change-over valve- (2/3-way), rest<br />

position, secure position<br />

Auxiliary Energy:<br />

Compressed air//inert gas available?, Pressure?<br />

Connections:<br />

Deployed/ required tubing, hoses and connection<br />

elements?<br />

Special Requirements:<br />

Safety-relevant aspects, final position display /<br />

monitoring, cleaning possibilities, behaviour in case<br />

of auxiliary energy failure, media separation CIPcompatible<br />

etc..<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Which Valve for which Application?<br />

The following table will help you to find the suited<br />

valve for a multitude of applications.<br />

Equipment and Components<br />

IV-MB-FK2-2-1,6..<br />

IV-MB-FK1-3-1,6..<br />

In case of any uncertainties, our project department<br />

will gladly help you.<br />

IV-MB-FK1-2-1,6..<br />

Task<br />

Locking of smaller Flows + + + o +<br />

Locking of medium Flows + + o +<br />

Locking of large Flows + + +<br />

Viscose, abrasive Media +<br />

Distributing + o +<br />

Selecting + o +<br />

Mixing + o +<br />

Control Valve for Liquid<br />

Dosing via the Force of Gravity<br />

(e.g. GraviDos)<br />

+ + o o<br />

Suction-side Valve at Pump<br />

Dosing for Vessel Switching<br />

+ + o o<br />

Additional Locking Valve at<br />

Dosing into Vacuum<br />

+ o<br />

Reactor Venting o o + o<br />

Reactor Deairing o o + o<br />

Inert Gas Feed o o + o<br />

Gas Feed + + o o<br />

Reactor Discharge Stop-Cock + +<br />

Sample Bottling o o o +<br />

High Pressure +<br />

Ex-Area + + o o o<br />

+ = well suited, o = limited suitability, upon request<br />

IV-MB-GM1-2-2...<br />

Multi-way channels can be found in the following pages.<br />

Preferential Types<br />

(A selection of standard types for typical<br />

laboratory applications)<br />

We have arranged a selection of preferential types<br />

for the most frequent laboratory applications which<br />

have proven to be especially effective.<br />

Preferred Types of Connection<br />

SN4/6 Screwing for hose with diameter interior/exterior 4.0/6.0 mm<br />

GMGx/x Thread Bushing G x/x inch e.g. G3/8 = 3/8 inch cylindrical G-thread<br />

IV-MB-UM1-2-3...<br />

IV-MB-UM1-3-3...<br />

IV-MB-UM2-2-..<br />

IV-PB-FG1-2-15..<br />

IV-PB-FG2-2-15..<br />

IV-PB-FG3-3-20..<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 215<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


216<br />

Universal Laboratory Valve<br />

This low dead storage laboratory valve is particularly<br />

suited in the low pressure and low viscosity area for:<br />

� Distributing<br />

� Mixing<br />

� Switching of small Flows<br />

� As a Control Valve for Liquid Dosing via the<br />

Force of Gravity<br />

� As a Suction-side Valve at Pump Dosing for<br />

Vessel Switching<br />

� As an additional locking Valve when Dosing<br />

� For Dosing of aggressive, highly pure and sterile<br />

Media<br />

Technical Data<br />

Equipment and Components<br />

Amongst others, it is deployed in the GraviDos-<br />

Dosing System.<br />

Flow Rate Kv-Value 3-way: 0.047 m³/h, accords to 15 l/h H2O at approx. p=<strong>10</strong>0 mbar<br />

(≈1 m height difference), 2-way: 0.06 m³/h<br />

Mode of Operation Open/Closed magnetic valve<br />

Rest Position dead, closed<br />

Nominal Width 1.6 mm / 1.5 mm<br />

Media Connection G 1/8“, UNF<br />

Media Temperature 0 to 50 °C<br />

Ambient Temperature max. 55 °C<br />

Pressure Range 0 to 2 bar<br />

Dead Storage Volume 85 μl<br />

Casing Material PVDF, ETFE<br />

Seal Material FFKM (Kalrez, similar to Simrez, Chemraz, Perlast)<br />

Media Compatibility Against almost all chemicals, except freons and highly halogenated solvents<br />

Flow Direction random<br />

Operational Voltage 24V DC<br />

Power Consumption 3.4 W warm<br />

Protection Category IP 40<br />

Ex-Version no<br />

Order Code Description<br />

IV-MB-FK1-2-1,6-GMG1/8-ea Universal 2/2-way laboratory valve nominal width 1.6 mm, Kv 0.06 m³/h, with 3 m cable for<br />

connection to LAB-PI (plug) or MSR-PI (open ends)<br />

IV-MB-FK1-3-1,6-GMG1/8-ea Universal 3/2-way laboratory valve nominal width 1.6 mm, Kv 0.047 m³/h, with 3 m for<br />

connection to LAB-PI (plug) or MSR-PI (open ends)<br />

IV-MB-FK2-2-1,5-UNF-ea Universal 2/2-way laboratory valve nominal width 1,5 mm, Kv 0,039 m³/h, with 3 m cable for<br />

connectino to LAB-PI plug or MSR-PI (open ends)<br />

IV-MB-FK2-3-1,5-UNF-ea Universal 3/2-way laboratory valve nominal width 1,5 mm, Kv 0,047 m³/h, with 3 m cable for<br />

connectino to LAB-PI plug or MSR-PI (open ends)<br />

VL-KB-MB-FK1 Valve holding element for LabKit-ALU System<br />

ea = Electrical Connection<br />

T Tuchel plug for LAB-PI<br />

O Open ends for PMC-PI<br />

Order Example:<br />

3/2 way valve, media connection, thread bushing G<br />

1/8“, cable for LabManager/box<br />

Order Code: IV-MB-FK1-1,6-3-GMG1/8-T<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Equipment and Components<br />

Universal Laboratory Valve with Manual Emergency Actuation<br />

An universal magnetic valve for application where a<br />

manual actuation is possibly necessary in<br />

emergency cases:<br />

� Reactor Venting and Deairing<br />

� Addition of Inert Gases<br />

� Distributing<br />

� Mixing<br />

� Interruption of small Flows<br />

� As a Control Valve for Liquid Dosing via the<br />

Force of Gravity<br />

Technical Data<br />

Flow Rate, Kv Value 0.25 m³/h (accords to approx. 30 l/min air at Δp=<strong>10</strong>0 mbar) to 0.40 m³/h<br />

Mode of Operation Open/Closed or 2/3-way magnetic valve<br />

Rest Position dead, closed<br />

Nominal Width 3, 4, 5 mm<br />

Media Connection G1/4“<br />

Media Temperature -30 to +80°C at EPDM, 0 to +80°C at FKM<br />

Ambient Temperature max. 55°C<br />

Pressure Range 0-8 bar at DN3, 0-3 bar at DN5<br />

Casing Material PP and PVDF<br />

Seal Material EPM, FKM, media separation via diaphragm , FFKM optional<br />

Media Compatibility bases, many solvents, many oils,<br />

acids and salt solutions should be verified in individual cases<br />

Operational Voltage 24V DC<br />

Power Consumption 8 W<br />

Protection category IP 65<br />

Order Code Description<br />

IV-MB-FK2-2-nw-ma-ea Universal 2/2-way laboratory valve with manual emergency actuation with 3 m cable for<br />

connection to LAB-PI (plug) or MSR-PI (open ends)<br />

IV-MB-FK2-3-nw-ma-ea Universal 3/2-way laboratory valve with manual emergency actuation with 3 m cable for<br />

connection to LAB-PI (plug) or MSR-PI (open ends)<br />

VL-KB-FK2-UM1 Valve holding element for LabKit-ALU-System<br />

nw = Nominal Width<br />

3 3 mm 0,25 m³/h<br />

4 4 mm 0,30 m³/h<br />

5 5 mm 0,40 m³/h<br />

ma = Media Connection:<br />

GMG1/4 Thread Bushing G 1/4“<br />

ea = Electrical Connection<br />

T Tuchel plug for LAB-PI<br />

O Open ends for MSRmanager<br />

Order Example:<br />

3/2 way valve, DN3, Kv 0.25 m³/h, media connection<br />

thread bushing G 1/4“,<br />

Cable for<br />

LabManager/box.<br />

Order Code: IV-MB-UM1-3-GMG1/4<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 217<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


218<br />

Inerting, Venting and Deairing Valve<br />

This valve is particularly suited for:<br />

� Reactor Venting<br />

� Reactor Deairing<br />

� Addition of Inert Gases<br />

Amongst other applications, this valve is deployed in<br />

reactor systems operating under high pressure.<br />

Technical Data<br />

Equipment and Components<br />

Flow Rate, Kv Value 0.12 m³/h (accords approx. 15 l/min air at Δp=<strong>10</strong>0 mbar) up to 0.55 m³/h<br />

Mode of Operation Open/Closed magnetic valve<br />

Rest Position dead, closed<br />

Nominal Width 2 bis 6mm<br />

Media Connection G1/8 bis G3/8<br />

Media Temperature -<strong>10</strong> to +<strong>10</strong>0°C at FKM, up to 180° at graphite/PTFE<br />

Ambient Temperature max. 55 °C<br />

Pressure Range 0 to 25 bar at NW 2 mm, 0 to 2,5 bar at NW 6 mm<br />

Casing Material High grade steel<br />

Seal Material FKM, PTFE/Graphite or EPDM<br />

Media Compatibility bases, many solvents, many oils,<br />

acids and salt solutions should be verified in individual cases<br />

Operational Voltage 24V DC<br />

Power Consumption 8 W<br />

Protection Category IP 65<br />

Ex-Version Optional (pressure sealed)<br />

Order Code Description<br />

IV-MB-GM1-2-nw-ma-ea Universal 2/2-way laboratory valve nominal width 2.0 mm, Kv 0.12 m³/h, with 1.5 m cable for<br />

connection to LAB-PI or MSR-PI<br />

VL-KB-MB-GM1 Valve holding element for LabKit-ALU-System<br />

nw = Nominal Width<br />

2 2 mm 0,12 m³/h<br />

2,5 2,5 mm 0,16 m³/h<br />

3 3 mm 0,23 m³/h<br />

4 4 mm 0,30 m³/h<br />

6 6 mm 0,55 m³/h<br />

ma = Media Connection:<br />

GMG1/8 Thread Bushing G 1/8“<br />

GMG1/4 Thread Bushing G 1/4“<br />

GMG3/8 Thread Bushing G 3/8“<br />

ea = Electrical Connection<br />

T Tuchel plug for LAB-PI<br />

O Open ends for PMC-PI<br />

Order Example:<br />

2 way valve, media connection thread bushing G<br />

1/8, cable for LabManager/box.<br />

Order Code: IV-MB-GM1-2-2-GMG1/8<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


High Pressure Magnetic Valve<br />

This high pressure valve features an exceptional<br />

pressure resistance of 4<strong>10</strong> bar. The directly<br />

controlled magnetic valve operates with a nipple<br />

seal.<br />

Application Areas:<br />

� Ventilation and Deairing of Reactor<br />

� Feeding of Inert Gas<br />

� Distribution<br />

� Mixing<br />

� Interruption of small Flows<br />

� Control Valve for the Dosing of Liquids via the<br />

Force of Gravity<br />

Technical Data<br />

Equipment and Components<br />

Seat Diameter 1,5mm<br />

Operation Modes Open/Closed 2/2-Way Magnetic Valve<br />

Idle Position Currentless Closed<br />

Nominal Width 1,5 mm<br />

Media Connection G1/4“<br />

Media Temperature -<strong>10</strong>...80°C<br />

Ambient Temperature max. 35°C<br />

Pressure Range 0-4<strong>10</strong>bar<br />

Casing Material High Grade Steel 1.4305/1.4<strong>10</strong>4<br />

Seal Material PTFE, PEEK<br />

Media Compatibility Bases, many solvents, many oils, acids and salt solutions. Please verify the<br />

individual cases.<br />

Operational Voltage 24V DC<br />

Power Consumption <strong>10</strong>0 W<br />

Protection Class IP 65<br />

Order Code Description<br />

IV-MB-UM2-2 2/2-Way High Pressure Valve 24V, 4 A<br />

IV-MB-UM2-PS Power Supply for 2/2-Way High Pressure Valve, 24V, 4 A, with Auxiliary Contactor<br />

VL-KB-MB-UM2 Valve Retaining Element for V-MB-UM2-2 Valve at the LabKit-ALU-System<br />

Further valves (further information available upon request).<br />

Order Code Description<br />

IV-MB-UM1-2-3-ma-ea Universal 2/2-way laboratory valve Ex nominal width 3.0 mm, Kv 0.23 m³/h<br />

IV-MB-UM1-3-3-ma-ea Universal 3/2-way laboratory valve Ex nominal width 3.0 mm, Kv 0.23 m³/h<br />

IV-PB-FG1-2-15-ma-ea 2/2-way ball valve nominal width 15 mm, Kv 11 m³/h<br />

IV-PB-FG2-2-15-ma-ea 2/2-way diaphragm valve nominal width 15 mm, Kv 7 m³/h<br />

IV-PB-FG3-3-20-ma-ea 3/2-way electric-pneumatical Open/Closed valve,nominal width 20 mm, Kv 7 m³/h<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 219<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


220<br />

Adjustment and Control Valves<br />

Equipment and Components<br />

Valves, stop-cocks, flaps, etc. are required in large<br />

numbers for the control of the material flows in<br />

laboratory reactor plants, pilot plant stations, and<br />

mini-plants.<br />

Material flows are often also integrated into control<br />

circuits. In this case, it is necessary to adjust these<br />

with continuously operating adjustment devices. For<br />

this purpose, adjustment valves are deployed.<br />

Application Areas<br />

� Pressure Control<br />

� Vacuum Control<br />

� Mass Flow Control for Heating and Cooling<br />

Media<br />

� Fast Temperature Regulation via Mixing<br />

Regulations<br />

� Mastering of exothermal Reactions through<br />

Temperature Control via:<br />

� Mass Flow of deployed Materials<br />

� Cooling/Heating agent Flow<br />

� Cascaded Temperature Control, e.g. subordinate<br />

Mass Flow Control for Heating Steam<br />

� Mass Flow Regulations<br />

� Controlled Release/Pressure Generation<br />

according to predetermined Profiles<br />

� Material Flow Regulation in continuously<br />

operating Plants<br />

� Level Control via Feed and Discharge<br />

� Ex-Area Zone 1 and 2 with intrinsically safe Valve<br />

Positioners<br />

In simple cases, it is also possible to operate with<br />

open/closed valves, if a certain generated pulsation<br />

does not matter (PWM-modulation, two-step<br />

control). Please do not hesitate to ask us. We will<br />

gladly also propose low-cost solutions to you, if this<br />

is possible.<br />

Advantages, Services<br />

Which Proportional Valve for which Application?<br />

With the help of the following table you will be able<br />

to find the suited valve for a multitude of<br />

applications.<br />

� All valves can be activated via the analogue<br />

outputs (panels AAP, AEAP..) of our PIs<br />

� Complete delivery with cable and plug for<br />

direct connection to your LAB-xxx PI<br />

� Hydraulic design and alignment to the media<br />

of your plant, available auxiliary energy etc.,<br />

established by our engineering department<br />

� Upon request, integration of your application<br />

programs by our application programmers<br />

� Upon request, design, installation and<br />

parameterisation of your control circuits by<br />

our engineering department<br />

� Ready-to-use software modules, e.g. vacuum/<br />

pressure control...<br />

� Establishment of complicated controller<br />

structures: self-adapting controllers, cascade<br />

controllers, characteristics controllers...<br />

� Consultancy and alignment to your<br />

automation devices completely from one<br />

single source<br />

In addition, we are also able to equip valve types out<br />

of the chapter “ Valves and Stop-Cocks” (e.g. ball<br />

valves, diaphragm valves) with continuously<br />

operating actuators. Also with these, to a certain<br />

extent, it is possible to conduct controlled operation.<br />

For higher quality regulations, we are also able to<br />

design characteristics regulations aligned to the<br />

respective application.<br />

For the most important tasks in the laboratory, you<br />

can find a selection of proven standards under<br />

“Preferential Types”, which will facilitate the selection<br />

for you.<br />

In case of any uncertainties, our project department<br />

will gladly assist you.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Equipment and Components<br />

IV-MP-UM...<br />

Task \ Type<br />

Pressure Control + +<br />

Vacuum Control + o +<br />

Mass Flow Control Small Flow + +<br />

Mass Flow Control Large Flow + o<br />

Mass Flow, viscose, abrasive Media o +<br />

Level Control + o o o<br />

Heating/Cooling Media, Temperature Control + + +<br />

Quick Temperature Control + + o<br />

Ex-Area +<br />

+ = well suited, o = limited suitability, upon request<br />

Electromagnetic Control Valve<br />

These electromagnetic proportional valves with<br />

outstanding features are the most cost-effective<br />

possibility to proportionally reduce material flows.<br />

Features<br />

� Low Hysteresis<br />

� Low Pressure Dependency<br />

� High Manipulating Speed<br />

� Simple Activation<br />

Applicable for:<br />

� Pressure Control<br />

� Vacuum Control<br />

� Mass Flow Control in Heating and Cooling<br />

Medias<br />

� Further Applications within Reactor Systems<br />

Technical Data<br />

IV-PP-UG1-2-13<br />

IV-PP-FG1-3-20..<br />

IV-PP-UX1-2...<br />

There are two methods to connect the<br />

valves to <strong>HiTec</strong>-<strong>Zang</strong> PIs.<br />

IV-PP-FG2-2-15...<br />

� Direct connection to a digital output<br />

(PWM 400 Hz an LP-DAP8T). The<br />

available power output of the digital<br />

output must be observed. This<br />

solution is particularly advisable in<br />

case of several valves are deployed.<br />

� 4..20mA analogue output (LP-AAP8UI or (LP-<br />

AE4AA4P...) via electronics IV-MP-ELBU...<br />

For the supply with operational voltage, a digital<br />

output (LP-DAP8A) or an external power supply<br />

source with according 24 V power output can be<br />

used.<br />

Flow Rate, Kv Value DN 0.8: approx. 0.02 m³/h, DN 2: 0.1 m³/h, DN 4: 0.33 m³/h, DN 6: 0.7 m³/h<br />

Qair (5 bar on atm.) DN 0.8: approx. 1,500 l/h, DN 2: 6,600 l/h, DN 4: 21,800 l/h, DN 6: 46,200 l/h<br />

Suited Vacuum Pump DN 2: approx. 1,000-3,000 l/h, DN 4: 3,000-8,000 l/h, DN 6: 8,000-16,000 l/h<br />

Mode of Operation 2/2-way magnetic valve with electronics 4-20 mA<br />

Rest Position dead, closed, zero point cut-off<br />

Nominal Width 0.8 + 2 + 4 + 6 mm<br />

Media Connection DN 0.8: G 1/8“, DN 2 + DN 4: G 1/4“, DN 6: G 3/8“<br />

Media Temperature -<strong>10</strong> to +90°C<br />

Ambient Temperature max. +55°C<br />

Pressure Range DN 0.8: 0-12 bar, DN 2: 0-8 bar, DN 4 u. DN 6: 0-2 bar<br />

Activation 4-20 mA with electronics or directly to LP-DAP8T<br />

Power Supply 24 V DC<br />

Power Output DN 0.8: 4 W, DN 2 + 4: 8 W, DN 6: 15 W<br />

Casing Material High-grade steel, DN 6 brass!<br />

Seal material FPM, Viton, Kalrez, PTFE<br />

Media Compatibility Almost all chemicals; acids and salt solutions need to be verified in individual<br />

cases, DN 6 only neutral gases (cold trap in case of vacuum application!)<br />

Hysteresis < 5%<br />

Reproducibility < 0.5 % of final value<br />

Response Time (90%) < 50 ms<br />

Protection Category IP 65<br />

Ex-Version No<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 221<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


222<br />

Equipment and Components<br />

Order Code Description<br />

IV-MP-UK1-2-0,8-ma-ea 2/2-way magnetic control valve, nominal width 0.8 mm, Kv 0.02 m³/h, with 1,5 m cable for<br />

connection to LAB-PI or MSR-PI<br />

IV-MP-UM1-2-2-ma-ea 2/2-way magnetic control valve, nominal width 2 mm, Kv 0.1 m³/h, with 1,5 m cable for<br />

connection to LAB-PI or MSR-PI<br />

IV-MP-UM2-2-4-ma-ea 2/2-way magnetic control valve, nominal width 4 mm, Kv 0.33 m³/h, with 1,5 m cable for<br />

connection to LAB-PI or MSR-PI<br />

IV-MP-UG1-2-6-ma-ea 2/2-way magnetic control valve, nominal width 6mm, Kv 0.7 m³/h, with 1,5 m cable for<br />

connection to LAB-PI or MSR-PI, only avaialable in brass!<br />

IV-MP-ELBU1 Separate electronics 4-20mA and 0-<strong>10</strong>V for IV-MP... proportional valves<br />

IV-MP-ELBU2 Integrated electronics 4-20mA for IV-MP proportional valves except -08<br />

ma = Media connection:<br />

GMG1-8 Thread Bushing G 1/8“, only DN 0.8<br />

GMG1-4 Thread Bushing G 1/4“, only DN 2 + 4<br />

GMG3-8 Thread Bushing G 3/8“, only DN 6<br />

SN6/SN4-6 Hose diameter=4mm, hose screwing, interior/exterior diameter 4/6mm for DN2<br />

SN<strong>10</strong>/SN8-11 Hose diameter=8mm, hose screwing, interior/exterior diameter 8/11mm for DN4<br />

SN15/SN<strong>10</strong>-15 Hose diameter=<strong>10</strong>mm, hose screwing, interior/exterior diameter <strong>10</strong>/15mm for DN6<br />

ea = Electrical Connection<br />

Order Example:<br />

T Tuchel plug for LAB-PI<br />

2/2-way magnetic control valve, nominal width 2<br />

O Open ends for PMC-PI<br />

mm, hose olive for di = 6, for LabBox<br />

Order Code: IV-MP-UM1-2-2-SN6-T<br />

Further Control Valves (Further information upon request):<br />

Order Code Description<br />

IV-PP-UG1-2-13-ma-ea 2/2-way electro-pneumatic slanted fit control valve, nominal width 13 mm, Kv 2.8 m³/h,<br />

integrated valve positioner<br />

IV-PP-FG1-3-20-ma-ea 3/2-way electro-pneumatic control valve, nominal width 20 mm, Kv 7 m³/h, with integrated<br />

valve positioner<br />

IV-PP-UX1-2-ma-ea-kv 2/2-way electro-pneumatic precision control valve with integrated valve positioner<br />

Multi-Way Valves<br />

These multi-way valves are intended for the<br />

distribution or combining of materials at low<br />

pressures. For the connection to the LAB-System, a<br />

serial interface is required at the UI/workstation.<br />

Multi-Way Valve for Small Flows<br />

Possible versions with 3/4/6/12/24-way distributor<br />

and 6-way sample feeding<br />

Typical applications are:<br />

� Bottling of Samples<br />

� Dosing out of many Preparation Drums<br />

Technical Data<br />

Nominal Width 0.75 mm, 1.5 mm<br />

Mode of Operation Rotor with step motor drive<br />

Media Connection 1/16 inch (1.58 mm), ¼ - 28<br />

Fittings<br />

Pressure Range 21 oder 68 bar at 6-way<br />

Flow Direction random<br />

Material Rotor PEEK/PCTFE<br />

Media<br />

Compatibility<br />

Operating Voltage 24V DC<br />

Activation RS232<br />

Ex-Version no<br />

Almost all chemicals, except<br />

acids containing sulphur and<br />

nitrogen and several solvents<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Equipment and Components<br />

Order Code Description<br />

IV-MW1-wa-ma-ea Multi- way valve with 1.5 m cable for connection to LAB-PI or PMC-PI<br />

IFN-IV-MW1 NAMUR driver for multi-way valve IV-MW1<br />

wa = Number of Positions 4, 6, 12 or 24.<br />

ma = Media Connection: UNF1/4“<br />

We advise to obtain feedback from our project<br />

department before placing an order for this valve.<br />

Multi-Way Valve for Medium Flows<br />

1/16 Fittings for 1/16 inch tubes, nominal<br />

width of valve: 0.75 mm.<br />

1/8 Fittings for 1/8 inch tubes, nominal<br />

width of valve 1.5 mm.<br />

Technical Data<br />

Nominal Width 4.6 mm<br />

Mode of Operation Rotor with step motor drive<br />

Media Connection Fittings for 1/4 inch tubes<br />

(6.35 mm)<br />

Media Temperature 50 °C<br />

Ambient<br />

40 °C<br />

Temperature<br />

Pressure Range 6 bar liquid<br />

Flow Direction random<br />

Material Stator PPS<br />

Material Rotor PTFE<br />

Media Compatibility Almost all chemicals<br />

Operational Voltage 24V DC<br />

Activation RS232<br />

Protection Category IP30<br />

Ex-Version optional<br />

Order Code Description<br />

IV-MW2-wa-1/4 Multi-way valve with 1.5 m cable for connection to LAB-PI or PMC-PI<br />

IFN-IV-MW2 NAMUR driver for multi-way valve IV-MW1<br />

wa = Number of Positions 4, 6.<br />

We advise to obtain feedback from our project department before placing an order for this valve.<br />

Further equipment and components can be found in<br />

the chapters:<br />

� Process Analytics and Sensors<br />

� Dosing Systems and Pumps<br />

� Liquid Handling and Sample<br />

� Stirring and Dispersing<br />

� Customised Reaction Calorimeters<br />

The present catalogue, due to the limited space, can only present an extract of all available equipment and<br />

components.<br />

<strong>HiTec</strong> <strong>Zang</strong>, amongst many other articles, also retails thermostats of the leading manufacturers, including<br />

respective accessories, e.g. hoses, heat carrier oil and pressure rising pumps.<br />

We will gladly assist you to find the ideal choice for your particular case of application.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 223<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


224<br />

Process Analytics and Sensors<br />

Here you will find a selection of instruments for<br />

process analytics, as well as sensors and monitors,<br />

which are suited for laboratory and mini-plant<br />

technology.<br />

All sensors are suited for deployment with the Laband<br />

MSR/PMC managers.<br />

Process Analytics and Sensors<br />

Notice:<br />

In case of interest, please contact us for information<br />

regarding special topics such as VIS-, NIR- or US-<br />

Spectroscopy.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Process Analytics and Sensors<br />

MoleculeEye ® ATR-FTIR-Spectroscopy<br />

Online-Monitoring of Reactions via<br />

ATR-FTIR Spectroscopy<br />

MoleculeEye ATR-probe in a MultiLab 250 ml reactor<br />

In order to be able to follow reactions, a great<br />

number of online-sensors are available. The majority<br />

of these however have one great disadvantage: they<br />

are not able to deliver substance-specific<br />

information. Spectroscopic methods are able to fill<br />

this gap. One of these is the Fourier Transformation-<br />

Infrared Spectroscopy (FTIR). Due too its very high<br />

absorption speed, this represents one of the most<br />

effective methods.<br />

IR-spectrometers, both in regard to quality and<br />

quantity, deliver outstandingly well evaluable<br />

spectrums, which also deliver utilisable information<br />

about unknown substances.<br />

Due to the narrow absorption band in the middle<br />

infrared band, this method is also suited for multicomponent<br />

analysis. In addition, it is also able to<br />

deliver information about transition conditions of a<br />

reaction, regardless whether this concerns an<br />

enzyme or a catalyst, via intermediates or transient<br />

aggregates. It is even possible to still gain<br />

information about individual substances out of multicomponent<br />

mixtures.<br />

All IR-active substances are detectable. As there are<br />

only a few non-IR-active substances (pure elements,<br />

a few simple compounds), this method is universally<br />

deployable.<br />

To draw samples and to transport them into the<br />

laboratory is the classic method – but it is laborious<br />

and time-consuming.<br />

With an ATR-probe, the laboratory is virtually directly<br />

brought into the reactor. ATR-FTIR-spectroscopy is<br />

therefore currently the most effective method for<br />

online-evaluation. It allows parallel determination of<br />

substances both according to type as well as<br />

amount.<br />

Advantages<br />

General:<br />

� Time saving due to online- in-situ measurement<br />

methods<br />

� Improvement of the product quality by minimising<br />

of by-products<br />

� Easy handling, mechanically robust, portable<br />

� Neither adjusting nor maintenance necessary<br />

� Minute sample amounts, no preliminary sample<br />

preparation necessary<br />

� Inert, free of reagents<br />

� No falsification of the sample due to transfer (e.g.<br />

as at HPLC)<br />

� Also deployable in small vessels<br />

� No sample wastage<br />

The MoleculeEye within Chemistry:<br />

� Fingerprint-Measurements<br />

� Recognition of intermediate products<br />

� Temperature and pressure-resistant<br />

� Chemically robust, explosion-protected<br />

The MoleculeEye within Biotechnology:<br />

� Delivers an exact image of the physiology of the<br />

bioprocess<br />

� Early problem detection<br />

� No contamination<br />

� Sterilisable sensor<br />

The MoleculeEye ATR-Diamond – Probe<br />

The novel fibre-optic MoleculeEye probe utilises the<br />

principle of the attenuated total reflection (ATR).<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 225<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


226<br />

Process Analytics and Sensors<br />

The ATR-Principle with diamond prism<br />

The ATR-crystal is made of diamond and connected<br />

to the fixture without seal elements. The<br />

MoleculeEye probe is therefore insensitive in regard<br />

to chemical and mechanical influences. A light ray<br />

which reaches an optically less dense media out of<br />

an optically dense one in a flat angle is reflected at<br />

the boundary area. But not exactly at the boundary<br />

area: the ray penetrates into the optically less dense<br />

media a few µm . Certain frequency components of<br />

the light are substance-specifically absorbed in the<br />

less dense media. This leads to the generation of<br />

absorption spectrums that are registered by the<br />

spectrometer.<br />

The MoleculeEye probe is highly inert, resistant<br />

against chemicals, pressure, and high temperatures<br />

and can therefore be installed in reactors without<br />

any problems. The 6mm probe fits into even the<br />

smallest reactors.<br />

The ATR-principle also functions in strongly coloured<br />

solutions, in emulsions and highly solid-containing<br />

suspensions, as the measurement merely takes<br />

place in a very thin layer at the crystal. Substances<br />

are partially, depending on their IR-absorption,<br />

detectable up to the trace range.<br />

MoleculeEye ATR Hand Probe<br />

The simple technical construction makes the method<br />

robust, its speed allows real-time measurement and<br />

consequently direct process guidance.<br />

The method is able to measure in the trace range<br />

and also delivers information to intermediate<br />

products and transition conditions.<br />

For this reason, it is particularly suited for<br />

examinations of reaction mechanisms. In<br />

comparison to similar effective methods, e.g. mass<br />

spectrometry, it is significantly more cost-effective<br />

and easier to handle.<br />

The <strong>HiTec</strong> <strong>Zang</strong> MoleculeEye FTIR Spectrometer<br />

System disposes of a fibre-optic ATR-Sensor with<br />

unique properties:<br />

� Diameter of only 6 mm<br />

� Simple Coupling with pin and socket<br />

connector<br />

� Outstanding long-term Stability<br />

� No Adjusting and Compensating necessary<br />

� Outstanding Measurement Accuracy and<br />

Linearity<br />

� Ideal Signal/Disturbance Ratio, consequently<br />

high Measurement Sensitivity<br />

� Fast Real Time Measurement, high Time<br />

Resolution<br />

� Several Sensors at one Spectrometer<br />

possible (Multiplexer)<br />

� Adaptation to spectrometers made by Bruker,<br />

Mettler, Nicolet, Perkin-Elmer, Jasco, and<br />

others is possible<br />

� Coupling to LabManager System is possible<br />

� Special Designs/solutions available<br />

Application Areas<br />

� Chemistry, Biotechnology, Pharmaceutics, Food,<br />

Environment ...<br />

� All IR-active substances detectable<br />

� Solid and liquid samples, non-transparent and<br />

solid-containing liquids and emulsions<br />

MoleculeEye ATR Probe mounted in a 2 litres<br />

LabKit Reaction Plant<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Process Analytics and Sensors<br />

Up to 6 probes can be connected to a spectrometer<br />

with a multiplexer unit. Parallel experiments are<br />

therefore possible without any problem.<br />

MoleculeEye ATR Probes in the MultiLab Parallel Reactor<br />

System<br />

MoleculeEye ATR-flow through cell for MRT plants<br />

Areas of Deployment and Examples<br />

Polymer Analysis: ATR-FTIR delivers both<br />

information regarding the chemical composition as<br />

well as the molecule size. Naturally, one can also<br />

just follow the progression of the reaction.<br />

FTIR spectrums of a polymerisation process.<br />

Catalysis: The IR-spectrums of adsorbates and<br />

transition conditions of a reaction differ from the<br />

spectrums of these substances in solution. These<br />

differences are due to the binding of the substrate to<br />

the catalyst. In this way, information about such<br />

conditions can be gained. Due to the measurement<br />

in an extremely thin layer surrounding the crystal,<br />

the solids do not interfere with the analysis.<br />

Reaction Technology: Following the reaction<br />

progress<br />

FTIR spectrums in the progression of a Grignard<br />

reaction.<br />

Protein Analysis: The normal IR analysis at<br />

proteins is strongly disturbed by the high and broadbanded<br />

adsorption of the functionally essential<br />

water. At ATR- robes, the water hardly causes<br />

disturbance, as only a thin layer is transilluminated.<br />

Diamond does not adsorb proteins, for which reason<br />

the ATR-crystal does not cause any disturbance.<br />

Monitoring of Clarification Plants: Parallel<br />

analysis of organic acids, carbonhydrates,<br />

carbonate, hydrogencarbonate, phosphate,<br />

hydrogenphosphate, carboxlate, and many further<br />

parameters in water and clearing sludge.<br />

Food: CO2 in Beer<br />

FTIR-spectrums of CO2 in beer and comparative solutions.<br />

Chemicals: Butylacetate and Toluene compared .<br />

ATR-FTIR-spectrums of Butylacetate and Toluene compared.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 227<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


228<br />

Pharmaceuticals: Caffein, Ascorbic Acid,<br />

Acetylsalicylic Acid.<br />

Process Analytics and Sensors<br />

ATR-FTIR-spectrums of Caffein, Ascorbic Acid, and Acetylsalicylic<br />

Acid compared.<br />

Technical Data<br />

The fibre optic probe with SMA connector<br />

Diamond-ATR MIR Probe head diameter: 6 mm, Length: 20 cm<br />

Standard Probe (extension possible)<br />

Materials In contact with media: Hastelloy, Gold, Diamond<br />

Length of Light Guide Standard 150 cm, optional up to 400 cm (with cooled detector )<br />

Measurement Principle ATR 45 °, double reflection<br />

Spectral Range Standard probe 3 to 18 µm (at standard length)<br />

Temperature Range -<strong>10</strong>0 to 150°C<br />

Pressure Range -1 up to <strong>10</strong>0 bar (up to 300 bar available upon request)<br />

Spectrometer FTIR-Spectrometer with light guide coupling, extendable standard software<br />

Detection Sensitivity < 1% (up to 0.02%)<br />

Detector MCT (mercury cadmium telluride), nitrogen-cooled, 3 -18 µm<br />

(3300 - 600 cm-1 ), thermo-electrical cooling 3 - 8 µm (3300 - 1250 cm-1 )<br />

Multiplexer Optional: six-fold Multiplexer, e.g. for parallel reactor systems<br />

Delivery Scope Compact, robust, FT-IR spectrometer with industry-hardened protective housing.<br />

MCT-detector (fl.N2), MIR, 12,000-600 cm-1, typical hold time: 8 h, incl. alignment optics.<br />

Diamond-ATR-Probe (MIR)<br />

Data System P4 > 3 GHz, 512 MB RAM, > 80 GB HDU, DVD-writer, LAN, 20“-<br />

TFT-flat screen monitor, colour printer, Windows XP Professional.<br />

Software package for analytics and research.<br />

Extensions Multiplexer unit for 6 probes<br />

Program for the establishment and control of process-relevant settings for cyclic<br />

measurements, communication with external process control systems (fieldbus or<br />

4-20 mA interfaces) and visualisation. The run-time component necessary for<br />

operation is included in the delivery scope. Communication with process control<br />

systems requires further hardware and, possibly, control-system specific<br />

programming.<br />

Program for the control of cyclic measurements, communication with external<br />

process control systems (fieldbus or 4-20 mA interfaces) and visualisation.<br />

Software package for quantitative analysis.<br />

Software package for chromatography-couplings<br />

Order Code Description<br />

IS-MOLECULEEYE MIR Spectrometer system with fibre-optic ATR diamond probe<br />

IS-MOLECULEEYEMUX Multiplexer unit for 6 probes<br />

Further accessories and extensions are available upon request. <strong>HiTec</strong> <strong>Zang</strong> also offers ready-to-use<br />

complete systems, individual components and special designs!<br />

If you have any special questions, our consultant engineer will gladly advise you. Test measurements can be<br />

conduced!<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Process Analytics and Sensors<br />

ParticleEye Particle Sizer<br />

LabKit-rc Reaction Calorimeter with ParticleEye-3D-Probe<br />

The ParticleEye In-Situ Particle Sizer enables the<br />

identification of geometrical particle characteristics<br />

and their respective changing conditions under test<br />

and production conditions already during the<br />

reaction.<br />

The unique dynamic focussing allows for an<br />

extensive measurement range of 0,5 to 4000 μm<br />

due to the continuous focus-depth variance.<br />

Multiple scatterings are not registered due to the<br />

patented opto-mechanical construction of the<br />

sensors. A laser beam is guided into the measuring<br />

probe through a single mode fibre with a diameter of<br />

merely 4 μm and dynamically focussed into the<br />

product intended for analysis by special optics.<br />

The dynamic focus represents the decisive<br />

advantage compared to conventional turbidimetry<br />

FBRM® (Registered Mettler-Toledo/Lasentec<br />

trademark).<br />

Features:<br />

� High Precision<br />

� Compact Construction<br />

� Robust<br />

� Ideal PAT-Sensor<br />

Options<br />

� In Situ stability control in the production process<br />

� Inline product monitoring in real time<br />

� Online quality control for the prevention of<br />

redundant laboratory analyses<br />

� Optimisation of the solid matter quality and purity<br />

� Improvement of productivity at the formulation of<br />

new products<br />

� Quality control 24h on 365 days throughout the<br />

year<br />

� Most simple function control of the PAT sensors<br />

due to the deployment of reticles<br />

� Improved control<br />

Applications<br />

� Crystallisation<br />

� Precipitation<br />

� Release<br />

� Fermentation<br />

� Homogenisation<br />

� Polymerisation<br />

� Agglomerations of Particle Systems<br />

� Dispersion<br />

� Granulation<br />

� Dissolution<br />

� Flocculation<br />

� Optimisation of Grinding Processes<br />

� Stability Analyses at Dispersed Phase Systems<br />

Advantages:<br />

� All particles are counted and presented as<br />

quantity distribution, length distribution,<br />

surface distribution, and volume distribution<br />

� Highest possible selectivity and sensitivity<br />

under original production conditions<br />

� Improvement of the safety at the scale up and<br />

production<br />

� Accelerated product development<br />

� High concentrations are possible<br />

� Measurement periods from 1 to 300 sec<br />

� Temperatures of -120°C to 220°C are possible<br />

� The additional option to in-situ sterilise the<br />

PAT sensors in deactivated condition up to a<br />

temperature of 165°C<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 229<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


230<br />

Sensors<br />

Available are dynamic 2D and 3D sensors with<br />

different characteristics.<br />

Process Analytics and Sensors<br />

Data Visualisation and Presentation<br />

The data evaluation can be conducted on the basis<br />

of the particle size distribution according to ISO<br />

66141.<br />

Measuring data is available in form of graphics and<br />

tables. Up to five distribution diagrams can be<br />

presented at the same time.<br />

Reference data, which may derives from previously<br />

recorded measurements or any other data which<br />

has been entered with the help of an integrated<br />

editor, can be faded into the distribution diagrams.<br />

For cumulative distributions, it is possible to<br />

additionally, or instead of the reference data, to fade<br />

in a distribution range of selectable band width.<br />

The presentation is available as cumulative curve or<br />

as trend diagram. Up to eight characteristics (of d<br />

01 to d99) can be presented as trend data, e.g. the<br />

transition variable according to DIN D0.1 to D99.9,<br />

count rate, intensity, fraction ratios, optional<br />

analogue signals 0V to <strong>10</strong>V or 4 to 20 mA. Any<br />

statistical moments from 0 to 3 can be utilised.<br />

Data Storage and Re-evaluation<br />

The distribution, statistical, respectively trend data<br />

available as measuring data can be exported to<br />

other programmes such as Word, Excel etc., and<br />

printed out or used otherwise in this form, via the<br />

clipboard.<br />

Measuring data in Excel format can be transported<br />

into a customer-related evaluation programme<br />

through a continuous data transfer.<br />

Measurable Products<br />

Over 6000 different products have already been<br />

measured. Why not take advantage from the<br />

experience of our product specialists?<br />

Measurable are all particles and drops that dispose<br />

of an optical reflection feature, reaching from<br />

aluminium oxide to sugar crystals.<br />

As the particles commence to agglomerate as of a<br />

concentration of 1Vol%, the particle collectives are<br />

usually at hand as particle systems (PSyA) under<br />

process conditions. The respectively generated<br />

particular fingerprints therefore represent<br />

reproducible characteristics for the PAT control.<br />

Due to the ascertainability of agglomerate<br />

structures, you can consequently cover broader<br />

particle distributions compared to a laser diffraction<br />

spectrometer (PSD). It is possible to present the<br />

total scope of your products as variable<br />

characteristic via the time.<br />

The measurements with PAT sensors in original<br />

concentrated products therefore present fingerprints<br />

of the actual particle system distribution under<br />

production conditions!<br />

The changes during production are collected and<br />

presented in-situ, therefore under original condition,<br />

by the PAT sensors.<br />

If the products intended for measurement are diluted<br />

online, the sensors will register the particle size<br />

distribution of the discretely existent particles<br />

continuously as under laboratory conditions.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Application Examples<br />

Process Analytics and Sensors<br />

Process Particle Change Evaluation<br />

Drop Formation Drops of various<br />

components are<br />

homogenised<br />

Intrusion of pigments in<br />

emulsions<br />

Distribution of the drop<br />

formation during the<br />

polymerisation<br />

Distribution of pigments in<br />

the emulsion<br />

Drops increase in size and<br />

stabilise<br />

Significant shifting of the distribution<br />

After the emulsion is homogeneous, the<br />

emulsion raw data are subtracted from the data<br />

pigments + emulsion = distribution of the<br />

pigments<br />

Fine fraction reduced in favour of the coarse<br />

fraction<br />

Grinding – wet or dry Reduction of particle size Change of distribution – higher fine fraction<br />

Germ formation at<br />

precipitation<br />

Particle Breakage or<br />

Cleavage<br />

Particles grow out of the<br />

nanoscale<br />

Change of distribution – cumulative higher fine<br />

fraction<br />

Reduction of particle size Change of distribution – higher fine fraction –<br />

reduced coarse fraction<br />

Growth of the Particles Increase of particle size Change of distribution – higher coarse fraction<br />

Agglomeration and<br />

Coagulation Processes<br />

Particles form particle<br />

systems<br />

Change of distribution - higher coarse fraction –<br />

reduced fine fraction<br />

Dissolution Particles dissolve Reduction of number of counts<br />

Change of form at the<br />

Crystallisation<br />

Sensor Head with Measuring Window<br />

Technical Data:<br />

Particles deform Change of distribution function<br />

Pressure 3 bar, optional to 64 bar<br />

Measuring Medium<br />

Temperature<br />

5...85°C, optional -120...20°C, 5° to 125°C, -20..165°C, 5 to 220°C<br />

Parts in contact with High Grade Steel 1.4571, sulphur-free, optional Hastelloy C276, Hastelloy C2,<br />

Measuring Medium Hastelloy C4, Sapphire Glass, Hifluor (FKM)® or Kalrez<br />

Sensor/Probe Length 260 mm, optional 350mm<br />

Sensor Diameter 8mm, 18mm or 22mm<br />

Sensor Cable Length <strong>10</strong>m<br />

Sensor Window Sapphire Glass, Quality Category MIL– PRF-1383B <strong>10</strong>-5<br />

Sensor Protection Category IP 68<br />

Scanner Speed 1 m/s, optional 2m/s<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

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Automation<br />

Software<br />

Plant<br />

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Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

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Stirring and<br />

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232<br />

Technical Data:<br />

Configuration Examples<br />

Process Analytics and Sensors<br />

Device Configuration Characteristics<br />

2D ORM (optical backreflection) passive Signal<br />

Capture System >5 µm exclusively based on the<br />

duration of the particles in the focus for consistent<br />

Reynold numbers.<br />

2D ORM active Signal Capture System >2µm based<br />

on the patented sensor technology (see above) plus<br />

runtime-levelling signal capture method.<br />

3D ORM active Signal Capture System >2µm with<br />

in-depth focus based on a controlled 3mW laser<br />

3D ORM active Signal Capture >0.8µm with in-depth<br />

focus + Selective Scanning based on a controlled<br />

5mW laser system and double screening.<br />

3D ORM IPAS active Signal Capture System >1µm<br />

with in-depth focus + Selective Scanning + controlled<br />

open signal system based on a <strong>10</strong>mW laser system,<br />

regulable between1 and <strong>10</strong>mW with multiple<br />

screening.<br />

APAS active Multi Capture Signal Capture System<br />

>500nm with 3D ORM in-depth focus + Selective<br />

Scanning (SMF)+ controlled open signal system<br />

based on a 25mW laser system, regulable between1<br />

and 25mW with multiple screening.<br />

„Multiscattering“ Signals and turbidity are not<br />

processed by the patented sensor technology.<br />

Counting of all captured particles and their size.<br />

Especially designed for rough industrial deployment<br />

– no moving parts in the sensor.<br />

Upgraded through a dynamic scanning system and a<br />

consequently higher count rate.<br />

Upgraded through in-depth scanning and better<br />

resolution.<br />

Upgraded through dynamic and controlled in-depth<br />

scanning and better resolution.<br />

Partially open system for R&D tasks based on the<br />

APAS system. Input raw signals from the sensor are<br />

trapped and are, if required, available to the<br />

researchers.<br />

Advanced Particle Analysing System. Completely<br />

open System for R & D tasks. Input raw signals from<br />

the sensor, as well as the signals of the individual<br />

processing steps, are trapped and are, if required,<br />

available to the researchers.<br />

Order Code Description<br />

IS-PARTICLEYE-S- l ParticleEye Particle Measurement System, static; comprises sensor, electronics and software<br />

module<br />

IS-PARTICLEYE- 2D-l ParticleEye Particle Measurement System, dynamic 2D; comprises sensor, electronics and<br />

software module<br />

IS-PARTICLEYE- 3D-l-t ParticleEye Particle Measurement System, dynamic 3D; comprises sensor, electronics and<br />

software module<br />

IS-PARTICLEYE-AA6 6 Analogue Outputs 4...20mA for ParticleEye Particle Measurement System<br />

IS-PARTICLEYE-EEX Ex-Equipment for ParticleEye Particle Measurement System<br />

IS-PARTICLEYE- WV <strong>Main</strong>tenance Contract for ParticleEye Particle Measurement System<br />

l: Sensor Length :<br />

t: according to table, only concerns 3D sensor.<br />

Type Measurement<br />

Range in µm<br />

Max. Concentration<br />

in %<br />

125 0,5 – 125 80<br />

250 1 – 250 60<br />

500 1 - 500 50<br />

<strong>10</strong>00 2 - <strong>10</strong>00 40<br />

2000 5 - 2000 30<br />

3000 30 - 3000 25<br />

4000 20 - 4000 20<br />

Options:<br />

� Special Materials<br />

� Other Sensor Forms and Diameters<br />

� EEX-Version<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Turbidity Probe<br />

Process Analytics and Sensors<br />

Turbidity measurement probe in a high-grade steel<br />

protective tube. Probe measures in retro-reflection<br />

(backscatter) with IR-light (880nm). The diameter is<br />

12 mm, the length between 120 and 407 mm. The<br />

optical window is made of sapphire and sealed with<br />

a Kalrez- sealing ring (FDA-conform).<br />

Applications:<br />

� Crystallisation<br />

� Precipitation<br />

� Releasing<br />

� Fermentation<br />

Characteristics:<br />

� High Accuracy<br />

� Compact Construction<br />

� Robust<br />

Technical Data:<br />

Measurement Principle Retro-reflection (backscatter)<br />

Measured Material Temperature –30...130°C<br />

Temperature<br />

Pressure 0...6 bar<br />

Parts in Contact with<br />

Measured Material<br />

High-grade steel 1,4404 or 1,4435, sapphire, Kalrez<br />

Probe Tube Dimensions of probe 12 x 120/205/297/407 mm<br />

Measurement Range <strong>10</strong>...4000 FTU (display in other measurement units possible)<br />

Output signal 0/4...20 mA<br />

Operational Voltage Transmitter <strong>10</strong>0...240 V AC<br />

Protection Category Transmitter sealed front-side, resulting protection category dependant of mounting<br />

EEX EEX probe category 1...3, Zone 0...2, T4...T6<br />

Connection to the LabManager:<br />

The probe is delivered ready to connect with a cable and a Tuchel plug for the direct connection to an<br />

analogue input panel AEP8A. Please coordinate the feed with our project department.<br />

Order Code Description<br />

IS-TRUB-O-ea Turbidity probe made of high-grade steel 1,4404, for direct connection to an analogue input panel<br />

ea=Electrical Connection:<br />

T Tuchel plug for LabManager<br />

O Open ends for MSRmanager<br />

Order Example:<br />

Turbidity probe made of high-grade steel 1,4571,<br />

probe tube <strong>10</strong> mm, with connection 1.5 m for<br />

LabManager Panel LP-AEP8A, coordinate the probe<br />

length with our project department when placing<br />

order.<br />

Order Code: IS-TRUB-O-O<br />

Available upon request:<br />

� Materials: Hastelloy C4<br />

� other probe designs and diameters<br />

� EEX Versions<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

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Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

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Stirring and<br />

Dispersing<br />

Services


234<br />

Process Analytics and Sensors<br />

Fibre-Optic Submersible Reflection Probes<br />

With the Superior Optical Material –<br />

Sapphire<br />

These reflection submersion probes convince with a<br />

robust design and an uncompromising choice of<br />

materials regarding all parts in contact with media.<br />

With sapphire as optical material, they are virtually<br />

absolutely resistant to abrasion and corrosion and<br />

therefore also stable when deployed with<br />

concentrated acids and bases. They are also<br />

resistant against pressure and temperature peaks.<br />

The application range reaches from the simple<br />

turbidity measurement in liquids right to the<br />

characterisation of solids. All probes are designed<br />

for the direct installation into vessels and tubings.<br />

They can be flexibly aligned to individual<br />

requirements, due to the diversity of available<br />

materials, process connections, pressure and<br />

temperature ranges.<br />

Advantages:<br />

� abrasion and corrosion-free sapphire optics<br />

� chemical stability<br />

� verifiable process suitability<br />

� application range from UV to NIR<br />

� compatible with all spectrometer types<br />

� varied versions and special designs<br />

� robust and extremely stable<br />

The application range reaches from the simple<br />

turbidity measurement with fibre-optic turbidity<br />

measurement systems right to the identification and<br />

characterisation of solids.<br />

Technical Details<br />

Typical Applications<br />

� Reaction tracing of heterogeneous reactions in<br />

the chemical synthesis in the NIR<br />

� determination of residual solvent concentration at<br />

solids directly in driers<br />

� Homogeneity of solid compounds directly in the<br />

mixer<br />

Our product portfolio is not restricted to fibre-optical<br />

probes. It includes everything you may need for the<br />

implementation of probes in processes and the<br />

coupling to practically every spectrometer type.<br />

You can rely on us to find an ideal solution!<br />

Light Spot 1 mm<br />

Dimension<br />

6 mm<br />

Diameter<br />

Alternative 12 mm<br />

Submersion Depth As of <strong>10</strong>0 mm<br />

Standard Materials High-grade steel DIN 1,4435/316L, sapphire<br />

Process Connections DIN or ANSI flanges<br />

Screwings e.g. Swagelok, PG 13.5, further connections available upon request<br />

Temperature max. 280°C (continuous operation)<br />

Pressure 0–<strong>10</strong>0 bar<br />

Order Code Description<br />

IS-TRUB-ORF-ea Fibre-optic reflection probe<br />

ea=Electrical Connection:<br />

T Tuchel plug for LabManager<br />

O Open ends for MSRmanager<br />

Options:<br />

Alternative materials: high-grade steel DIN 1.4571 /<br />

SS316Ti, Titanium, Hastelloy, PVDF, PP, PTFE, etc.<br />

Further constructions, dimensions, and<br />

specifications available upon request.<br />

Conformity Statement 97/23/EU according to EU<br />

Pressure Equipment Directive.<br />

You can find fibre-optic probes for the MIR sector<br />

under „MoleculeEye“.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Process Analytics and Sensors<br />

Phase boundary Detector<br />

The <strong>HiTec</strong> <strong>Zang</strong> PhaDec is a robust and costefficient<br />

detector system for the detection of phase<br />

boundaries. PhaDec is in particular used for the<br />

automatic separation and separate bottling of liquid<br />

phases out of reactors or collecting vessels, e.g.<br />

after reactions with phase transfer catalysis, after<br />

azeotropic distillations or after extractions.<br />

<strong>Main</strong> Application Areas:<br />

� Extraction<br />

� Extractive Distillation<br />

� Azeotropic Distillation<br />

� Phase Transfer Catalysis<br />

Other Application Areas:<br />

� Filling Level Monitor<br />

� Flow Monitor<br />

� Leakage Monitor<br />

PhaDec utilises the different heat conductivity of the<br />

phases to recognise the boundary areas. Therefore,<br />

the application of the PhaDec is not limited to<br />

transparent or conductive liquids. Deployed as<br />

sensor is a special resistance sensor, which can<br />

also be used as a temperature sensor.<br />

The sensor can optionally be installed into the base<br />

discharge valve, the discharge line or into the<br />

reaction vessel from above.<br />

Advantages<br />

� Robust and cost-effective<br />

� Integrateable into any system<br />

� Universally applicable for all liquid phases –<br />

even at non-transparent and non-conductive<br />

fluids<br />

� Pressure-resistant and chemically stable<br />

� Also deployable as temperature sensor<br />

� Inert materials: glass, high-grade steel,<br />

Hastelloy, PEEK, PTFE<br />

Technical Data Phadec<br />

PI-Connectors to Pt<strong>10</strong>0-Input, Analog Input, Analog Output, Digital output<br />

Cable Length 200 cm (modification possible)<br />

Ambient Temperature -20 up to +70 °C<br />

Technical Data Phadec-x<br />

PhaDec operates with virtually all fluids, regardless<br />

whether liquid or gas, conductive or not conductive,<br />

transparent or not. As long as there is a clear phase<br />

boundary, the PhaDec will generate evaluable<br />

signals.<br />

The sensor is available with all known jacket<br />

materials. A preliminary lead time for the discharge<br />

of the main part of the lower phase is considered in<br />

the basis operation.<br />

The reaction period of the PhaDec depends on the<br />

type of sensor deployed. Sensors with a metal jacket<br />

and small outer dimensions react most rapidly. For<br />

quick response, we recommend an exterior diameter<br />


236<br />

Level Sensor<br />

Robust high-quality level sensor for industrial<br />

applications.<br />

� High Accuracy<br />

� Compact Construction<br />

Conductive Liquids > 1 μScm -1<br />

� Limit Area Detection<br />

to Liquids < 1 μScm -1<br />

Technical Data:<br />

Process Analytics and Sensors<br />

Measurement Principle Conductometric via scattering potential<br />

Measurement Media<br />

Temperature<br />

Max. 180°C<br />

Parts in Contact with<br />

Measurement Media<br />

High-grade steel 1,4571, Hastelloy available upon request<br />

Probe Tube d = <strong>10</strong> mm<br />

Measurement Range According to customer specifications<br />

Output Signal 0 - <strong>10</strong> V DC<br />

Supply Voltage ± 15 V DC<br />

Protection Category IP 54<br />

EEX Upon request<br />

Connection to the LabManager:<br />

The probe is delivered ready to connect with a cable<br />

and a Tuchel plug for the direct connection to an<br />

analogue input panel AEP8A. Please coordinate the<br />

feed with our project department.<br />

Order Code Description<br />

IS-L-FA-ea Level pick-up sensor, conductometric, made of high-grade steel 1,4571, probe tube<br />

<strong>10</strong>mm, with connection cable 1.5m for LabManager Panel LP-AEP8A<br />

ea=Electrical Connection:<br />

T Tuchel plug for LabManager<br />

O Open ends for MSRmanager<br />

Please coordinate the probe length with our project<br />

department when placing order!<br />

Order Example:<br />

Level pick-up sensor, conductometric, made of highgrade<br />

steel 1,4571, probe tube <strong>10</strong>mm, with<br />

connection cable 1.5m for LabManager Panel LP-<br />

AEP8A<br />

Please coordinate the probe length with our project<br />

department when placing order!<br />

Order Code: IS-L-FA-T<br />

available upon request:<br />

� Materials: Hastelloy C4<br />

� other probe designs and diameters<br />

� Float, PTC thermistor, ultrasonic, radar,...flow<br />

sensors and monitors<br />

� EEX Versions<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Teflon ® Flow Sensors<br />

Process Analytics and Sensors<br />

Due to new manufacturing technologies, the parts in<br />

contact with media of the Teflon flow sensors are<br />

completely made of Teflon ® and ruby. The resulting<br />

special properties, in particular the excellent<br />

resistance against most chemicals, give the sensor<br />

the suitability for a wide application range. The ruby<br />

bearing minimises friction and wear and guarantees<br />

high durability.<br />

Versatile: The One-Way - Click - Sensor (open)<br />

This outstanding product received an award at the<br />

„Salon International des Innovations“ in Geneva and<br />

is internationally protected by patent.<br />

For the high-pressure range, the sensors are also<br />

available in a high-grade steel casing.<br />

The Advantages<br />

� low cost<br />

� maintenance-free<br />

� sealless<br />

� extremely compact<br />

� little pressure decline<br />

� great flow range<br />

� Ex- version available<br />

� high working pressure range<br />

� high chemical resistance<br />

� sterilisable version (up to 160 °C)<br />

� one-way version for hardening materials<br />

� optionally, threaded or hose connection<br />

� high resolution (up to 1<strong>10</strong>.000 impulses per<br />

litre)<br />

� high durability and consistency due to ruby<br />

bearings<br />

� little response time due to low-mass rotor<br />

(approx. 15 mg)<br />

Application Areas<br />

� Chemical Industry<br />

� Pharmaceutical industry<br />

� Bio-Technology<br />

� Food Technology<br />

� Flow Measurement<br />

� Dosing of Feed Tanks<br />

� Continuous Dosing<br />

� Bottling and Charging<br />

� Flow Monitoring<br />

� Consumption Counter<br />

� Heat Counter<br />

The flow generating part of the sensor can easily be<br />

exchanged in case of hardening media and sterilised<br />

with up to 120 °C.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 237<br />

Equipment and<br />

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Dispersing<br />

Services


238<br />

The Functional Principle<br />

Process Analytics and Sensors<br />

The media is put into a rotational motion by a spiral<br />

flow former (worm) and actuates the virtually<br />

weightless rotor.<br />

The rotor is optically scanned in the course of which<br />

a frequency-analogue rectangular signal<br />

proportional to the flow speed is generated. This<br />

can, if necessary, be transformed to current, voltage<br />

or serial signals with one of the available measuring<br />

transducers.<br />

As the optical scan, at the light guide models, is<br />

conducted via a cable which is up to 40 m long, the<br />

sensors are particularly suited for the EX area.<br />

The sensor also operates with turbid media such as<br />

ink or diffuse media such as milk. Problems are only<br />

to be expected in case of strongly light scattering<br />

media such as latex or suspensions with titanium<br />

dioxide. Solid particles usually do not interfere.<br />

Merely fibres should be removed by a filter.<br />

Sensor Type Series S4.5 / 0.1 – 1.5 l / min<br />

The sensors of the type series S4.5 are available<br />

with hose and threaded connection. The connection<br />

cable of the standard version is cladded with Tefzel,<br />

a plastic material with properties similar to Teflon,<br />

but better elasticity.<br />

Technical Data<br />

Available Versions<br />

The sensors are available with the nominal widths<br />

4.5 mm, 8.5 mm and 12.5 mm, respectively with<br />

copper or light guide cable connection. The nominal<br />

widths 4.5 and 8.5 mm are only available in the<br />

standard version or as click-sensor with hose or<br />

threaded connection. The nominal width 12.5 mm, in<br />

the standard version, is available with threaded<br />

connection.<br />

The light-guide version is particularly suited for<br />

applications in explosive environments or in case of<br />

higher temperatures.<br />

The Click-sensor version enables sterilisation up to<br />

160°C, as well as the exchange of the measuring<br />

insert in case of hardened media.<br />

Measurement Range 0.06-2 litres/min<br />

Nominal Width 4.5 mm<br />

Connection for Media Hose nozzle 7mm or 1/8“ conical outer thread NPT<br />

Working Pressure 20 bar / 2MPa<br />

Pressure Decline approx. 200 mbar at 75% flow<br />

Max. Temp. Media 80 °C, with plastic light-guide 1<strong>10</strong> °C, with glass light-guide 180 °C<br />

Viscosity Range 0.8-<strong>10</strong>mm²/s, higher with calibration<br />

Signal Line TEFZEL® or light guide<br />

Output Signal 1<strong>10</strong>.000 Impulses = 1l<br />

Output Frequency <strong>10</strong>0 Hz - 3.1 kHz<br />

Reproducibility ± 0.15 %<br />

Linearity Faults ± 1%<br />

Protection Category IP 65, Click-Sensor IP 50<br />

Length 52 mm<br />

Max. Diameter 17 mm<br />

Length of Cable Intake 47 mm<br />

* The measurement range, in case of reduced demands to linearity, can be extended.<br />

Special designs for increased linearity in case of<br />

very low flows are available upon request. The<br />

stated values and measurement values are based<br />

on laboratory measurements with water at 20°C, as<br />

well as the manufacturer's statements in regard to<br />

the properties of the materials. The manufacturer<br />

reserves the right to modify/align the specifications<br />

to the state of the technology at any time.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Process Analytics and Sensors<br />

Measuring Transducer<br />

Standard version available with:<br />

� Transducer 6<strong>10</strong>0 with different signal outputs<br />

� Flow Calculator 6200<br />

� Dosing Calculator 6500<br />

� Plug for direct connection to <strong>HiTec</strong> <strong>Zang</strong><br />

LabManager<br />

� Connections according to customer specifications<br />

The light-guide version requires transducer 6700IR.<br />

For Order Code see the table “Order Codes“.<br />

Sensor Type Series S8.5 / 0.8 - 20 l / min<br />

The sensors of the type series S8.5 are available<br />

with hose and threaded connection. The connection<br />

cable of the standard version is cladded with Tefzel,<br />

a plastic material with properties similar to Teflon,<br />

but better elasticity.<br />

Technical Data<br />

IS-F-0045.T.H.P.01.DX disposable sensor with tubing connector<br />

The light-guide version is particularly suited for<br />

applications in explosive environments or in case of<br />

higher temperatures.<br />

The Click-sensor version enables sterilisation up to<br />

160°C, as well as the exchange of the measuring<br />

insert in case of hardened media.<br />

Measurement Range 1.0-20 litres/min<br />

Nominal Width 8.5 mm<br />

Connection for Media Hose nozzle 12mm or 1/4´´ conical outer thread NPT<br />

Working Pressure 15 bar / 1.5MPa<br />

Pressure Decline approx. 200 mbar at 75% flow<br />

Max. Temp. Media 80 °C, with plastic light guide 1<strong>10</strong> °C, with glass light guide 180 °C<br />

Viscosity Range 0.8-<strong>10</strong>mm²/s, higher calibration<br />

Signal Line TEFZEL® or light guide<br />

Output Signal 6.350 Impulses/litre = 1Impulss/157µl<br />

Output Frequency 40 Hz - 2.2 kHz<br />

Reproducibility ± 0.15 %<br />

Linearity Fault ± 1.5 %<br />

Protection Category IP 65, Click-Sensor IP 50<br />

Length 60 mm<br />

Max. Diameter 22 mm<br />

Length of Cable Intake 47 mm<br />

* The measurement range, in case of reduced demands to linearity, can be extended.<br />

Special designs for increased linearity in case of<br />

very low flows are available upon request. The<br />

stated values and measurement values are based<br />

on laboratory measurements with water at 20°C, as<br />

Measuring Transducer<br />

Standard version available with:<br />

� Transducer S6000 u. S6<strong>10</strong>0 with different signal<br />

outputs<br />

� Flow Calculator 6200<br />

� Dosing Calculator 6500<br />

� Plug for direct connection to <strong>HiTec</strong> <strong>Zang</strong><br />

LabManager<br />

� Connections according to customer specifications<br />

well as the manufacturer's statements in regard to<br />

the properties of the materials. The manufacturer<br />

reserves the right to modify/align the specifications<br />

to the state of the technology at any time.<br />

The light-guide version requires transducer 6700 IR.<br />

For Order Code see the table “Order Codes“.<br />

Type IS-F-0085.T.P.01.XX<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 239<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


240<br />

Process Analytics and Sensors<br />

Sensor- The sensors Type of the type Series series S12.5 S 12.5 / have 2.5 a-<br />

40 l / min<br />

threaded connection. The connection cable of the<br />

standard version is cladded with Tefzel, a plastic<br />

material with properties similar to Teflon, but better<br />

elasticity.<br />

Technical Data<br />

The light-guide version is particularly suited for<br />

applications in explosive environments or in case of<br />

higher temperatures.<br />

Measurement Range 2-40 litres /min<br />

Nominal Width 12.5 mm<br />

Connection for Media 1/2“´outer thread BSP<br />

Working Pressure <strong>10</strong> bar max.<br />

Working Pressure approx. 200 mbar at 75% flow<br />

Max. Temp. Media 80 °C, with plastic light guide 1<strong>10</strong> °C, with glass light guide 180 °C<br />

Viscosity Range 0.8 - <strong>10</strong> mm²/s, higher with calibration<br />

Signal Line TEFZEL® or Light Guide<br />

Output Signal 2050 Impulses/litre = 1 Impulse/488µl<br />

Output Frequency 22 - 1200 Hz<br />

Reproducibility ± 0.15 %<br />

Linearity Fault ± 3 %<br />

Protection Category IP 65<br />

Length 72 mm<br />

Max. Diameter 26 mm<br />

Length of Cable Intake 47 mm<br />

* The measurement range, in case of reduced demands to linearity, can be extended.<br />

Special designs for increased linearity in case of<br />

very low flows are available upon request. The<br />

stated values and measurement values are based<br />

on laboratory measurements with water at 20°C, as<br />

Measuring Transducer<br />

Standard version available with:<br />

� Transducers S6000 and S6<strong>10</strong>0 with different<br />

signal outputs<br />

� Flow Calculator 6200<br />

� Dosing Calculator 6500<br />

� Plug for direct connection to <strong>HiTec</strong> <strong>Zang</strong><br />

LabManager<br />

� Connections according to customer specifications<br />

The light-guide version requires transducer 6700 IR.<br />

For Order Code see the table “Order Code”.<br />

well as the manufacturer's statements in regard to<br />

the properties of the materials. The manufacturer<br />

reserves the right to modify/align the specifications<br />

to the state of the technology at any time.<br />

Type IS-F-0125.T.B.P.01.XX with screwing connection<br />

Documentation to the special version up to 200 bars is forwarded upon request!<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Signal Connection<br />

Process Analytics and Sensors<br />

For the uncomplicated integration into your<br />

automation technology, measuring transducer-power<br />

supply units are available with the usual standard<br />

signals. The sensors can be directly connected to<br />

the <strong>HiTec</strong>-PIs with HK-DEA16N cards via special<br />

cables (IS-F-LABTUC) without a separate<br />

measuring transducer. For independent operation,<br />

flow calculators and dosing controller- components<br />

are available.<br />

The sensors, in the standard version, can also be<br />

operated without measuring transducer-power<br />

supply unit. The supply voltage is 5 V at approx. 15<br />

mA, the amplitude of the output signal is approx. 3 V<br />

at min. load resistance 1 kOhm.<br />

Working Range<br />

The sensors are available for the measurement<br />

ranges 0.1 – 1.5l/min, 0.8-18l/min and 2-40l/min.<br />

The specifications apply for the viscosity range of<br />

0.8-<strong>10</strong> mm²/s (water at 20 °C = 1chour = 1mm²/s,<br />

lubricating oil SAE30 at <strong>10</strong>0°C or ISO VG<strong>10</strong> at 40 °C<br />

= approx. <strong>10</strong> mm²/s).<br />

PFA Disposable Turbine Flowmeters - 5-30 V DC power supply series<br />

The sensors can also be deployed beyond this<br />

range, if it is taken into consideration that this leads<br />

to a change of the impulse rate and the calibration.<br />

The upper limit of the viscosity then accords to the<br />

viscosity of liquids with a similar viscosity as<br />

shampoo.<br />

Any mounting position is possible.<br />

Special Designs<br />

Upon request, special designs are available. If the<br />

standard versions do not meet your demands, do<br />

not hesitate to contact us. We will do our best to help<br />

you.<br />

Examples<br />

Special designs in high-grade steel up to 200 bar,<br />

special connections, special cable materials,<br />

modified flow ranges, special dosing and flow<br />

controls.<br />

Order Code Description Connection Flowrate l/min<br />

IS-F-0045.T.H.P.01.DX PFA turbine flowsensor 4.5 disposable 7 mm hosebarb 0,06 - 2,0<br />

IS-F-0045.T.H.0.00.DX PFA tube 4.5 only 7 mm hosebarb 7 mm hosebarb 0,06 - 2,0<br />

IS-F-0045.P.X.P.01.DX Electronics 4.5 only - -<br />

IS-F-0045.T.N.P.01.DX PFA turbine flowsensor 4.5 disposable 1/8" NPT 0,06 - 2,0<br />

IS-F-0045.T.N.0.00.DX PFA tube 4.5 only 1/8" NPT 1/8" NPT 0,06 - 2,0<br />

IS-F-0045.P.X.P.01.DX Electronics 4.5 only - -<br />

IS-F-0085.T.H.P.01.DX PFA turbine flowsensor 8.5 disposable 12 mm hosebarb 0,5 - 20,0<br />

IS-F-0085.T.H.0.00.DX PFA tube 8.5 only 12 mm hosebarb 12 mm hosebarb 0,5 - 20,0<br />

IS-F-0085.P.X.P.01.DX Electronics 8.5 only - -<br />

IS-F-0085.T.N.P.01.DX PFA turbine flowsensor 8.5 disposable 1/4" NPT 0,5 - 20,0<br />

IS-F-0085.T.N.0.00.DX PFA tube 8.5 only- 1/4" Thread 1/4" NPT 0,5 - 20,0<br />

IS-F-0085.P.X.P.01.DX Electronics 8.5 only - -<br />

PFA Disposable Turbine Flowmeters; 5 V DC series Low Voltage<br />

Order Code Description Connection Flowrate l/min<br />

IS-F-0045.T.H.P.01.DL PFA disposable turbine flowsensor 4.5 - 5 Vdc 7 mm hosebarb 0,06 - 2,0<br />

IS-F-0045.T.H.0.00.DX PFA tube 4.5 only 7 mm hosebarb 7 mm hosebarb 0,06 - 2,0<br />

IS-F-0045.P.X.P.01.DL Electronics 4.5 only - 5 Vdc - -<br />

IS-F-0045.T.N.P.01.DL PFA disposable turbine flowsensor 4.5 - 5 Vdc 1/8" NPT 0,06 - 2,0<br />

IS-F-0045.T.N.0.00.DX PFA tube 4.5 only 1/8" NPT 1/8" NPT 0,06 - 2,0<br />

IS-F-0045.P.X.P.01.DL Electronics 4.5 only - 5 Vdc - -<br />

IS-F-0085.T.H.P.01.DL PFA disposable turbine flowsensor 8.5 - 5 Vdc 12 mm hosebarb 0,5 - 20,0<br />

IS-F-0085.T.H.0.00.DX PFA tube 8.5 only 12 mm hosebarb 12 mm hosebarb 0,5 - 20,0<br />

IS-F-0085.P.X.P.01.DL Electronics 8.5 only - 5 Vdc - -<br />

IS-F-0085.T.N.P.01.DL PFA disposable turbine flowsensor 8.5 - 5 Vdc 1/4" NPT 0,5 - 20,0<br />

IS-F-0085.T.N.0.00.DX PFA tube 8.5 only- 1/4" Thread 1/4" NPT 0,5 - 20,0<br />

IS-F-0085.P.X.P.01.DL Electronics 8.5 only - 5 Vdc - -<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 241<br />

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Components<br />

Process Analytics<br />

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Dosing Systems,<br />

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Stirring and<br />

Dispersing<br />

Services


242<br />

Process Analytics and Sensors<br />

PFA Turbine Flowmeters Fixed - 5-30 Vdc power supply series<br />

Order Code Description Connection Flowrate l/min<br />

IS-F-0045.T.H.P.01.XX PFA turbine flowsensor 4.5 7 mm hosebarb 0,06 - 2,0<br />

IS-F-0045.T.N.P.01.XX PFA turbine flowsensor 4.5 1/8" NPT 0,06 - 2,0<br />

IS-F-0085.T.H.P.01.XX PFA turbine flowsensor 8.5 12,5 mm hosebarb 0,5 - 20,0<br />

IS-F-0085.T.N.P.01.XX PFA turbine flowsensor 8.5 1/4" NPT 0,5 - 20,0<br />

IS-F-0125.T.B.P.01.XX PFA turbine flowsensor 12.5 1/2" BSP/NPT 2,0 - 40,0<br />

PFA Turbine Flowmeters Fixed; 5 Vdc series Low Voltage<br />

Order Code Description Connection Flowrate l/min<br />

IS-F-0045.T.H.P.01.XL PFA turbine flowsensor 4.5 - 5 Vdc 7 mm hosebarb 0,06 - 2,0<br />

IS-F-0045.T.N.P.01.XL PFA turbine flowsensor 4.5 - 5 Vdc 1/8" NPT 0,06 - 2,0<br />

IS-F-0085.T.H.P.01.XL PFA turbine flowsensor 8.5 - 5 Vdc 12 mm hosebarb 0,5 - 20,0<br />

IS-F-0085.T.N.P.01.XL PFA turbine flowsensor 8.5 - 5 Vdc 1/4" NPT 0,5 - 20,0<br />

IS-F-0125.T.N.P.01.XL PFA turbine flowsensor 12.5 - 5 Vdc 1/2" BSP/NPT 2,0 - 40,0<br />

Stainless Steel Turbine Flowmeters - 5-30 Vdc power supply series<br />

Order Code Description Connection Flowrate l/min<br />

IS-F-0045.S.N.P.01.XX SS Turbine flowsensor 4.5 NPT 1/4" NPT 0,06 - 2,0<br />

IS-F-0045.S.B.P.01.XX SS Turbine flowsensor 4.5 BSP 1/4"BSP 0,06 - 2,0<br />

IS-F-0085.S.N.P.01.XX SS Turbine flowsensor 8.5 NPT 3/8" NPT 0,5 - 20,0<br />

IS-F-0085.S.B.P.01.XX SS Turbine flowsensor 8.5 BSP 3/8" BSP 0,5 - 20,0<br />

IS-F-0125.S.N.P.01.XX SS Turbine flowsensor 12.5 NPT 1/2" NPT 2,0 - 40,0<br />

IS-F-0125.S.B.P.01.XX SS Turbine flowsensor 12.5 BSP 1/2"BSP 2,0 - 40,0<br />

PVDF Disposable Turbine Flowmeters 5-30 Vdc<br />

Order Code Description Connection Flowrate l/min<br />

IS-F-0045.P.H.0.00.CX PVDF Disposable rotor tube 4.5; Hose Barb; Clip<br />

mounting<br />

0,03 - 2,0<br />

IS-F-0085.P.H.P.01.CX PVDF Disposable Turbine Flowmeter 8.5; Hose Barb; 5-30 Vdc;<br />

Clip<br />

0,3 - 20,0<br />

IS-F-0085.P.H.0.00.CX PVDF Disposable rotor tube; Hose Barb; Clip<br />

mounting<br />

0,3 - 20,0<br />

IS-F-0000.P.X.P.01.CX Electronic pick-up; 5 - 30 Vdc; clipmounting -<br />

IS-F-0045.X.X.X.00.CX Mounting Clip in behalf of the 0045 flowmeters -<br />

IS-F-0085.X.X.X.00.CX Mounting Clip in behalf of the 0085 flowmeters - -<br />

Dosing pumps monitors<br />

In connection with a projected flow through sensor<br />

the monitor can measure and validate the flow .<br />

The dosing pump monitors can be controlled via<br />

RS232, USB, Ethernet or optionally via an analogue<br />

interface.<br />

Order Code Description<br />

IS-F-S601-P2 Dosing pumps monitors for monitoring of flow rates from 0,06 to 2 l/min<br />

IS-F-S601-P20 Dosing pumps monitors for monitoring of flow rates from 0,5 to 20 l/min<br />

IS-F-S601-P40 Dosing pumps monitors for monitoring of flow rates from 1,5 to 40 l/min<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Measuring Transducer<br />

LAB-PI-Connection Cable<br />

Process Analytics and Sensors<br />

The electronics integrated into this connection cable<br />

supplies the sensor with current and aligns the<br />

frequency-analogue sensor output signal with a<br />

digital input with frequency counting options of a<br />

Lab-PI. The cable is fixed to the sensor and can be<br />

directly connected to a digital input with a 24V DC<br />

transducer power supply unit (LP-DEP8A).<br />

Technical Data<br />

Supply Voltage 24V DC, via LAB-PI<br />

Current Consumption < 50 mA<br />

Output signal Level 23 V rectangular<br />

Output Signal 0 – 2.5 kHz (sensor frequency)<br />

Cable Length 200 cm (modification possible)<br />

Ambient Temperature -20 up to +70 °C<br />

Suited for the sensor type series: S4.5/8.5/12.5PFA-H/T/D-T<br />

Not available for sensors in light guide version!<br />

Order Code Description<br />

IS-F-LABTUC Level converter and supply for flow sensor with Tuchel plug for digital input<br />

Measuring Transducer 6<strong>10</strong>0 D/A<br />

The measuring 6<strong>10</strong>0 D/A supplies the sensor with<br />

current and converts the frequency-analogue sensor<br />

output signal into the electrical standard signals<br />

0V...<strong>10</strong>V or 0 / 4 - 20mA for further processing in the<br />

automation devices with voltage or current inputs.<br />

The current outputs are passive (without current).<br />

Technical Data<br />

Power supply 12 - 30 V DC or 115 – 240 V DC<br />

Current Consumption < 50 mA<br />

Output Signal 0 / 4 - 20 mA or 0V ... <strong>10</strong>V<br />

Width 71 mm<br />

Height 71 mm<br />

Depth 90 mm<br />

Protection Category IP30<br />

Ambient Temperature -20 to +70 °C<br />

Suited for the sensor type series: S4.5/8.5/12.5 cable types P and T<br />

Order Code Description<br />

IS-F-6300.BA.CON.DC.XX Measuring transducer 0-<strong>10</strong>V, 0/4 - 20 mA and supply for flow sensor<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Components<br />

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244<br />

Process Analytics and Sensors<br />

Measuring Transducer 6700 D/A for Light Guide Sensors<br />

The measuring transducer 6700 D/A supplies the<br />

sensor with current and converts the frequencyanalogue<br />

sensor output signal into the electrical<br />

standard signals 0 / 4 - 20mA for further processing<br />

in the automation devices with voltage or current<br />

inputs.<br />

Technical Data<br />

Supply Voltage 12 - 30V DC<br />

Current Consumption 230 mA<br />

Output Signal 0 / 4 - 20 mA<br />

Width 71 mm<br />

Height 71 mm<br />

Depth 90 mm<br />

Protection Type IP30<br />

Ambient Temperature -20 to +70°C<br />

Suited for the sensor type series: S4.5/8.5/12.5<br />

Cable Type F<br />

The current outputs are passive (without current).<br />

Order Code Description<br />

IS-F-6700-DA-CON-DC Measuring Transducer and supply for light guide sensors, output 0 - <strong>10</strong>V, 0/4 - 20mA<br />

Additional transducers upon request.<br />

Turbine Flow Sensor for Heat carrier Oil<br />

These flow sensors were developed for the<br />

measurement of the volume flow of water, fuel,<br />

heating oil, heat carrier oil, cooling agents,<br />

pharmaceutical, chemical and cryogenic liquids,<br />

liquid gases and solvents.<br />

Within the sector of the reaction calorimetry, they are<br />

particularly suited for the flow measurement of the<br />

heat carrier oil at temperatures of up to 350°C.<br />

They are deployed by default in our heat flow<br />

calorimeters. Due to their extremely short response<br />

time and the high resolution, they are also extremely<br />

well suited for chemical or pharmaceutical bottling<br />

and dosing plants. They operate according to the<br />

principle of the turbine-type meter.<br />

They operate according to the principle of the<br />

turbine-type meter.<br />

Type Measurement Range Impulses / l Connection<br />

in l/min<br />

G<br />

TDM06 1 to <strong>10</strong> 2000 ½ inch<br />

TDM09 3 to 30 980 ½ inch<br />

The Advantages:<br />

� compact<br />

� maintenance-free<br />

� resistant against high temperatures<br />

� low pressure decline<br />

� high working pressure range<br />

� fast response time due to low-mass rotor<br />

Application Areas<br />

� Chemical Industry<br />

� Pharmaceutical Industry<br />

� Heat Carrier Flow Measurement<br />

� Bottling and Charging<br />

� Flow Monitoring<br />

� Consumption Counter<br />

� Heat Counter<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Technical Data<br />

Process Analytics and Sensors<br />

Linearity ±2% v.M.<br />

Reproducibility ±0.5%<br />

MediaTemperature -20 to 120, 180 or 350°C<br />

Max. Operating 20 bar<br />

Pressure<br />

Viscosity 0.1 to 6 mm²/s<br />

Materials High-grade steel 1,4305 and 1,4122, ceramic<br />

Seal Viton or graphite<br />

Delivery Scope : Sensor with mounted impulse amplifier<br />

Order Code Description<br />

IS-F-TDMtc-tb-sa Turbine-type flow sensor<br />

ZK-SF-KM01-IA-IA-I-01 LAB-PI connection cable for turbine-type flow sensor, 4..20mA<br />

ZK-SF-KM01-ID-XA-I-01 LAB-PI connection cable for turbine-type flow sensor, NPN-OC<br />

tc = to <strong>10</strong>l/min: 06 alternatively up to 30l/min: 09<br />

tb = Temperature Range 120, 180 or 350 °C<br />

sa = Output Signal 4..20mA: I<br />

or frequency-analogue NPN-OC: F<br />

Order Example:<br />

Flow sensor for 0-<strong>10</strong>l/min, max. temperature 180°C, frequencyanalogue<br />

output, open collector: IS-F-TDM06-180-F<br />

Thermal Mass Flowmeters and Controllers<br />

The thermal flowmeters serve for the measurement<br />

of the mass flow of liquids. They operate on the<br />

basis of the calorimetric principle.<br />

The digital LIQUI-FLOW® Series L30 Mass-<br />

Flowmeter/controller was developed for measuring<br />

ranges between 2 and 20 kg/h (final value). It<br />

represents an ideal supplement to the larger<br />

measurement ranges of the smaller product family<br />

(up to the minute ranges of 30 mg/h). The mass<br />

flowmeter is based on a straight 316L high grade<br />

steel tube. A temperature sensor and a heating<br />

winding are mounted in thin film technology on the<br />

exterior side of the tube. The sensor signal is<br />

generated by the measurement of the current<br />

necessary for a consistent slight increase of the<br />

liquid.<br />

The Advantages:<br />

� Compact Design<br />

� Straight Measuring Tube<br />

� <strong>Main</strong>tenance-Free<br />

� Extensive Operational Range<br />

� Short Response Time<br />

Application Areas:<br />

� Chemistry<br />

� Pharmaceutics<br />

� Filling and Bottling<br />

� Flow Monitoring<br />

� Metering<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 245<br />

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Components<br />

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Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


246<br />

Technical Data<br />

Process Analytics and Sensors<br />

Physical Characteristics<br />

Accuracy, Standard ±1% of Final Value (at calibration under operational conditions)<br />

Span 2...<strong>10</strong>0%<br />

Reproducibility 0,2% of Final Value typical for H2O<br />

Setting Time Sensor 1...2 seconds, Controller 4...<strong>10</strong> seconds<br />

Max. Operational Pressure <strong>10</strong>0 bar<br />

Pressure Loss 35...350 mbar (based on 2...20 kg/h H2O)<br />

Operational Temperature 5...70°C<br />

Temperature Sensitivity ±0,2% of Final Value/°C<br />

Position Dependency Non-sensitive<br />

Heating Period<br />

Mechanical<br />

Characterisics<br />

30 minutes for highest accuracy; 3 minutes for an accuracy of ±2% of Final<br />

Value<br />

Material High Grade Steel 316L, electropolished (parts in contact with media). Other<br />

materials are available upon request.<br />

Process Connections 1/4” or 6 mm clamp ring connection; 1/4” vacuum connection, orbital welded.<br />

Other connections are available upon request.<br />

Gaskets towards the<br />

exterior<br />

Metallic<br />

Baffle Plate (in the Kalrez-6375. Others are available upon request.<br />

Controller Valve)<br />

Protection Class IP65<br />

Electrical<br />

Characteristics<br />

Supply Voltage +15...24 Vdc<br />

Output Measuring Device max. 18,5 Watt; Controller max. 22 Watt<br />

Output/Setpoint Value 0...5 (<strong>10</strong>) Vdc or 0 (4)...20 mA (active Output Signal)<br />

analogue<br />

Output/Setpoint Value Standard RS232, Optional Profibus-DP®, DeviceNet, Modbus-RTU, FLOWdigital<br />

BUS<br />

Electrical Connection Analogue/RS232/Supply 8-pole DIN-Connector male, Bus Systems-5-pole<br />

M12-Socket female<br />

Calibration Reference : Verifed by the NKO (National Calibration Service), is based on<br />

international standards.<br />

Liquid : Standard Calibration Liquid: H2O. For other liquids, please contact us.<br />

Models and Flow Ranges<br />

Mass Flowmeter for Liquids<br />

Model Minimum Flow Maximum Flow<br />

L30 0,0 0,04…2 kg/h 0,4…20 kg/h<br />

Mass Flow Controllers for Liquids<br />

Model Minimum Flow Maximum Flow<br />

L30C2I (Kv-max: 2,37x<strong>10</strong>-3) 0,04…2 kg/h 0,4…20 kg/h<br />

L30C5I (Kv-max: 6,93x<strong>10</strong>-2) 0,04…2 kg/h 0,4…20 kg/h<br />

Based on liquids with thermal characteristics equal to H2O.<br />

Delivery Scope: Sensor with Manual<br />

Order Code Description<br />

IS-FM-L30 0,0 Thermal Mass Flowmeter 0,04…2 kg/h to 0,4…20 kg/h<br />

IS-FM-L30C2I Thermal Mass Flowmeter(Kv-max: 2,37x<strong>10</strong>-3) 0,04…2 kg/h to 0,4…20 kg/h<br />

IS-FM-L30C5 Thermal Mass Flowmeter (Kv-max: 6,93x<strong>10</strong>-2) 0,04…2 kg/h to 0,4…20 kg/h<br />

Further flowmeters and devices in EX design are available upon request, for example, the μ-FLOW Series<br />

for the smallest possible flow amounts with measurement ranges reaching between 1,5...30 mg/h to 0,1...2<br />

g/h equivalent to water.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Process Analytics and Sensors<br />

Coriolis Mass Flowmeters and Controllers<br />

These mass flow sensors serve for the<br />

measurement and the control of the mass flow of<br />

liquid. They operate according to the Coriolis<br />

principle. They offer, compared to all other<br />

flowmeters, the great advantage that the mass flow<br />

is measured independent of the material<br />

characteristics. With them, multiple-phase materials<br />

can also be measured on an interference-free basis.<br />

The Advantages:<br />

� Real Mass Flow Measurement<br />

� Suited for Gasses and Liquids<br />

� Independent of Material Characteristics<br />

� Compact Design<br />

� <strong>Main</strong>tenance-Free<br />

� Extensive Operational Range<br />

� Low Response Time<br />

Application Areas<br />

� Chemistry<br />

� Pharmaceutics<br />

� Dosing<br />

� Filling and Bottling<br />

� Flow Monitoring<br />

� Metering<br />

Technical Data<br />

Physical Characteristics M12 / M13 / M14<br />

Accuracy, Standard Gases 0.5% p.M. Liquids 0.2% p.M.<br />

Span<br />

Reproducibility 0.05% v.M. ±1/2 [ZS x <strong>10</strong>0/flow]% (Digital Output) (ZS = Zero Stability)<br />

Setting Time(Regler) (


248<br />

Models and Flow Ranges<br />

Mass Flowmeters for Liquids<br />

Model Smallest Measurement<br />

Range<br />

Process Analytics and Sensors<br />

Nominal Highest Measurement<br />

Range<br />

M12 0.1…5g/h 1…<strong>10</strong>0g/h 2…200g/h<br />

M13 1…50g/h <strong>10</strong>…<strong>10</strong>00g/h 20…2000g/h<br />

M14 0.03…1kg/h 0.1…<strong>10</strong>kg/h 0.3…30kg/h<br />

Mass Flow Controllers for Liquids<br />

Model Smallest Measurement<br />

Range<br />

Nominal Highest Measurement<br />

Range<br />

M12V1NI 0.1…5g/h 2…<strong>10</strong>0g/h 4…200g/h<br />

M13V1NI 1…50g/h 20…<strong>10</strong>00g/h 40…2000g/h<br />

M14V1NI 0.03…1kg/h 0.2…<strong>10</strong>kg/h 0.6…30kg/h<br />

Delivery Scope: Sensor with Manual<br />

Order Code Description<br />

IS-FM-M12 Coriolis Mass Flowmeter 1…<strong>10</strong>0g/h<br />

IS-FM-M13 Coriolis Mass Flowmeter <strong>10</strong>…<strong>10</strong>00g/h<br />

IS-FM-M14 Coriolis Mass Flowmeter 0.1…<strong>10</strong>kg/h<br />

IS-FM-M12V1NI Coriolis Mass Flowmeter 1…<strong>10</strong>0g/h<br />

IS-FM-M13V1NI Coriolis Mass Flowmeter <strong>10</strong>…<strong>10</strong>00g/h<br />

IS-FM-M14V1NI Coriolis Mass Flowmeter 0.1…<strong>10</strong>kg/h<br />

Further flowmeters and devices in EX design are available upon request.<br />

Laboratory Gas Counter<br />

Drum-Type Gas Counter<br />

Wet Gas version<br />

Drum gas counters are universally deployable for<br />

volume measurement of flowing gases, in particular<br />

in case of minute and medium flow quantities, e.g. in<br />

the laboratory sector where utmost precision is<br />

demanded.<br />

Correction factors that consider gas type,<br />

temperature, humidity, etc. are therefore not<br />

required.<br />

Drum gas counters do not require maintenance and<br />

no power supply (as long as they are not operated<br />

with the option “pulse generator”).<br />

Advantages of the drum gas counter:<br />

� Housing and measuring drum are made of<br />

high quality plastics<br />

� Welded measuring drum – not soldered<br />

� Housing and measuring drum are resistant in<br />

regard to sealing liquid – in case an acid<br />

should generate out of the same<br />

� Epoxy coating for the measuring drum not<br />

required<br />

� Magnetic coupling instead of an O-Ring for<br />

drum shaft<br />

� PVC gas counter made of transparent PVC<br />

� 4-chamber measuring drum<br />

� Totalising roll counting mechanism (8-digit)<br />

� Large one-needle instrument dial<br />

� Magnetic coupling (between measuring drum<br />

and counting mechanism)<br />

� Filling level indicator (for adjustment of the<br />

sealing liquid level)<br />

� Recordings for manometer/thermometer<br />

� Viton seal<br />

� Circular bubble<br />

� Device foots can be levelled<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Performance Data<br />

Process Analytics and Sensors<br />

� Measurement Accuracy:<br />

± 0.2% at nominal flow (exact value is stated in<br />

calibration certificate),<br />

approx. ± 0.5% above the measurement range<br />

� Maximum input pressure:<br />

50 mbar at housings made of thermoplastics,<br />

500 mbar (0.05 MPa) at housings of high-grade<br />

steel<br />

Available Types<br />

Available Versions (materials):<br />

Type Flow Display (Standard Version)<br />

Minimum Maximum Standard Lowest Resolution Highest Resolution<br />

[l/h] [l/h] [l/h] [l]<br />

[l]<br />

TG 01 0.1 30 <strong>10</strong> 0.0005 (1) 999,9999 (1)<br />

TG 05 1 60 50 0.002 9,999,999.9<br />

TG 1 2 120 <strong>10</strong>0 0.01 99,999,999<br />

TG 3 5 360 300 0.02 99,999,999<br />

TG 5 <strong>10</strong> 600 500 0.02 99,999,999<br />

TG <strong>10</strong> 20 1200 <strong>10</strong>00 0.1 99,999,999<br />

TG 20 <strong>10</strong>0 4000 3200 0.2 999,999,990<br />

TG 25 <strong>10</strong>0 7000 5000 0.1 999,999,990<br />

TG 50 200 18000 <strong>10</strong>000 0.5 999,999,990<br />

(1) Display at the EDU 32<br />

Accessories (optional):<br />

� Thermometer (Gas), Measurement Range 0-<br />

60°C<br />

� Thermometer (Sealing Liquid),<br />

Measurement Range 0-60°C<br />

� Manometer, Measurement Range <strong>10</strong>mbar<br />

Differential Pressure<br />

� Digital Display Unit, with Interface RS232 and<br />

Analogue Output, (Impulse Generator required in<br />

Gas Counter)<br />

Housing Measuring<br />

Drum<br />

Version<br />

PVC-transparent PVC-grey 5<br />

PP-grey PP-grey 6<br />

PVDF PVDF 7<br />

PE-el PE-el 8<br />

1.4571 PVC-grey 1<br />

1.4571 PE-el 2<br />

1.4571 PP-grey 3<br />

1.4571 PVDF 4<br />

In case of any questions regarding the chemical<br />

resistance, please contact us. Both plastic and highgrade<br />

steel housings are welded.<br />

Options (installed in Gas Counter):<br />

Impulse Generator (for connection to Digital Display<br />

Unit/Computer)<br />

� Standard Version<br />

� Ex Version<br />

Slanted Tube Filling Level Indicator for Sealing<br />

Liquid „HPLI“<br />

Roll Counting Mechanism, resettable, 6 -digit<br />

(instead of totalising roll counting mechanism)<br />

Order Code Description<br />

IS-FV-GAS-tc-au Laboratory gas counter, wet gas version<br />

IS-FV-GAS-IG Impulse generator for connection to digital display unit/LAB- or PMC-PI<br />

IS-FV-GAS-IGEX Impulse generator for connection to digital display unit/LAB- or PMC-PI, Ex Version<br />

IS-FV-GAS-THG Thermometer (Gas), measurement range 0-60°C<br />

ZK-SFV-RI01-ID-XX-I-01 Connection cable for connection to DEP8A<br />

IS-FV-GAS-THS Thermometer (sealing liquid), measurement range 0-60°C<br />

IS-FV-GAS-MAN Manometer, measurement range <strong>10</strong> mbar differential pressure<br />

IS-FV-GAS-DISP Digital display unit, with interface RS232 and analogue output, (impulse generator required in<br />

gas counter)<br />

tc = Type code according to table types<br />

au = Version according to table versions (materials)<br />

Order Example: Type TG5 in PVDF with impulse generator for LabManager:<br />

Order Codes: IS-FV-GAS-TG5-7 and IS-FV-GAS-IG<br />

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Temperature Sensors<br />

Pt<strong>10</strong>0 Sensors<br />

Process Analytics and Sensors<br />

Pt<strong>10</strong>0 sensors have asserted themselves as<br />

standard in laboratories and pilot plants due to their<br />

high accuracy. They are available in different<br />

versions and dimensions.<br />

Accuracy Categories<br />

DIN Class A = ½ DIN B<br />

DIN B = ±(0.3+ 0.005|ϑ|)°C<br />

1/3 DIN B = ±(0.1+ 0.0016|ϑ|)°C<br />

1/5 DIN B = ±(0.06+ 0.001|ϑ|)°C<br />

1/<strong>10</strong> DINB= ±(0.03+ 0.0005|ϑ|)°C<br />

Diameter d = 2/3/6mm, Length l = 50/<strong>10</strong>0/300/600mm<br />

Technical Data<br />

Material: High-grade steel 1,4541 (V4A) (food and<br />

chemical resistant with the exception of chlorine)<br />

Temperature Range: -200 to 500°C<br />

Four-wire Technology<br />

Cable: 3 m, individual wires Teflon-isolated<br />

Outer cladding silicone, with bend protection.<br />

Lemo Plug Size 1<br />

The Pt<strong>10</strong>0 sensors are delivered ready to connect<br />

with a cable and a Lemo plug for direct connection<br />

to a Pt<strong>10</strong>0-Panel PTP8.<br />

Order Code Description<br />

IS-T-PT<strong>10</strong>0-1/1-VA-d-l Pt<strong>10</strong>0 Sensor DIN B, high-grade steel cladding 1,4541, with cable for LAB-PI Panel PTP8<br />

IS-T-PT<strong>10</strong>0-1/3-VA-d-l Pt<strong>10</strong>0 Sensor 1/3 DIN B, high-grade steel cladding 1,4541, with cable for LAB-PI Panel PTP8<br />

IS-T-PT<strong>10</strong>0 1/5-VA-d-l Pt<strong>10</strong>0 Sensor 1/5 DIN B, high-grade steel cladding 1,4541, with cable for LAB-PI Panel PTP8<br />

IS-T-PT<strong>10</strong>0-1/<strong>10</strong>-VA-d-l Pt<strong>10</strong>0 Sensor 1/<strong>10</strong> DIN B, high-grade steel cladding 1,4541, with cable for LAB-PI Panel PTP8<br />

Diameter d = 1/1.6mm, Length l = <strong>10</strong>0/250/<strong>10</strong>00mm<br />

Order Code Description<br />

IS-T-PT<strong>10</strong>0-1/1-VA -d-l Pt<strong>10</strong>0 Sensor DIN B, high-grade steel jacket 1,4541, with cable for LAB-PI Panel PTP8<br />

Special Designs<br />

� Precision Temperature Sensor (see under<br />

Precision Measurement Card)<br />

� Temperature Range -200 to 500°C, 600°C<br />

� Other Cladding Materials (Glass, Titanium ...)<br />

Calibration Certificates<br />

Manufacturer's Certificate or DKD certificate<br />

(German Calibration Service) upon request.<br />

Thermo- Elements<br />

Thermo-elements are available in various materials<br />

and dimensions. Especially small diameters are also<br />

available. This, in connection with their extremely<br />

broad temperature range, makes them<br />

indispensable.<br />

Connection to the LabManager:<br />

The cladded thermo-elements are delivered ready to<br />

connect with a cable and a Lemo plug for direct<br />

connection to a thermo-element Panel (LP-THP8).<br />

Accessories<br />

Screwing fixtures with slide function, process<br />

connection with G ¼ inch, glass thread GL or<br />

standard grinding.<br />

Technical Data:<br />

Material Cladding Tube: High-Grade Steel<br />

(food and chemical resistant with the exception of<br />

chlorine compounds)<br />

Temperature Range: -200 to 800°C<br />

Lemo-Plug Size 1 for LAB-PI<br />

Available upon request:<br />

� Open cable ends for MSRmanager<br />

� Other Cladding Materials (Glass, Titanium ...)<br />

� Area Sensor<br />

� Special Designs<br />

Order Code Description<br />

IS-T-NICRNI-d-l Thermo-element NiCr-Ni with connection cable for LAB-PI Panel THP8<br />

Diameter d = 0.5/1/2mm, Length l = <strong>10</strong>0/250/500/<strong>10</strong>00mm<br />

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Pressure Transmitters<br />

Standard Pressure Transmitters<br />

Process Analytics and Sensors<br />

Robust high-quality pressure transmitter for<br />

industrial deployment. These pressure transmitters<br />

can be directly connected to <strong>HiTec</strong> PIs. We offer<br />

three different types of pressure transmitters:<br />

� Relative Pressure:<br />

Atmospheric pressure as reference pressure,<br />

e.g. for filtration/vacuum filtration<br />

� Absolute Pressure:<br />

Vacuum reference, in particular for reactors,<br />

vacuum, distillation, steam pressure<br />

� Differential Pressure:<br />

2 Connections,<br />

filling level, pump monitoring...<br />

Technical Data:<br />

Properties:<br />

� High Accuracy<br />

� Compact Design<br />

� In Situ Digital<br />

Display available<br />

� High Overload<br />

Capability<br />

(5- to <strong>10</strong>-fold, dependant of Measurement<br />

Range)<br />

Connection to the LabManager<br />

The sensor is delivered ready to connect with a<br />

cable and a Tuchel plug for direct connection to an<br />

analogue input Panel LP-AEP8A. The power supply<br />

is conducted via Pin 5 = +24V and Pin 6 = GND.<br />

Measurement Principle Piezo-resistive<br />

Characteristic Line<br />

Deviation<br />

0.25% of Range<br />

Reproducibility 0.05 % of Range<br />

Hysteresis Fault 0.1 % of Range<br />

Stability/Year 0.2 % of Range<br />

Response Time (<strong>10</strong> - 90%) 1 ms<br />

Temperature Dependency Usually< 0.2% of Range/<strong>10</strong>K<br />

Measurement Media<br />

Temperature<br />

-30 to +<strong>10</strong>0°C<br />

Ambient Temperature -20 to +80°C<br />

Parts in Contact with<br />

Measurement Media<br />

High-Grade Steel 1,4571, 1,4542<br />

Pressure Connection G ¼“B (others upon request)<br />

Output Signal 4 - 20mA<br />

Supply Voltage <strong>10</strong> - 30 V DC unregulated, two-wire switching with plug-on display 13 - 30 V DC<br />

Electrical Connection Angle plug 4-pole, DIN 43 650<br />

Protection Category IP 65<br />

EEX Upon request<br />

Dimensions L approx. <strong>10</strong>0 mm, D approx. 48 mm with plug<br />

Order Code Description<br />

IS-P-R-6-ma-ea Pressure Transmitter 0- 6 bar relative with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />

IS-P-A-025-ma-ea Pressure Transmitter 0- 0.25 bar absolute with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />

IS-P-A-1,6-ma-ea Pressure Transmitter 0- 1.6 bar absolute with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />

IS-P-A-2,5-ma-ea Pressure Transmitter 0- 2.5 bar absolute with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />

IS-P-A-6-ma-ea Pressure Transmitter 0- 6 bar absolute with connection cable 1.5m for LAB-PI Panel LP-AEP8A<br />

IS-P-Z-AA Electronic plug-on display<br />

Nn<br />

ma=Media Connection:<br />

GMG1/4 Outer Thread G ¼“<br />

GMG1/2 Outer Thread G ½“<br />

ea=Electrical Connection:<br />

T Tuchel-plug for LAB-PI<br />

O Open ends for PMC-PI<br />

Order Example:<br />

Pressure Transmitter 0 – 0.25 bar absolute, G1/2“,<br />

with connection cable 1.5 m for LabManager<br />

Panel LP-AEP8A<br />

Order Code: IS-P-A-025-GMG1/2-O<br />

Available upon request:<br />

� Materials: Hastelloy C4<br />

� Other Measurement Ranges<br />

� Front-flush Diaphragm<br />

� Differential Pressure<br />

� EEX Versions<br />

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Process Analytics and Sensors<br />

Low Dead Space - pressure transducer<br />

This robust pressure transducer is suited for<br />

applications where particular low dead spaces are<br />

required, e.g. within micro-reaction technology.<br />

The measuring media does not come in contact with<br />

any metals.<br />

Features :<br />

� Metal- free Measuring Circuit<br />

� High Precision<br />

� Compact Design<br />

� Digital display available in-situ<br />

� High Overload Capability<br />

The pressure transducer can be directly connected<br />

to the <strong>HiTec</strong> PNCs.<br />

The pressure transducer is available for the<br />

measurement of relative and absolute pressure.<br />

Technical Data:<br />

Dead Volume 250µl<br />

Measuring Principle Piezo-resistive<br />

Characteristics Deviation 0,25% of Range<br />

Reproducibility 0,05 % of Range<br />

Hysteresis Fault 0,1 % of Range<br />

Stability/Year 0,2 % of Range<br />

Response Time (<strong>10</strong> - 90%) 1 ms<br />

Temperature Dependency Usually< 0,2% of Range /<strong>10</strong>K<br />

Measuring Media<br />

Temperature<br />

-0 to +<strong>10</strong>0°C<br />

Ambient Temperature -20 to +80°C<br />

Parts in Contact with PFA, PEEK, Kalrez Gaskets<br />

Measuring Media<br />

Connection to the LabManager<br />

The sensor is delivered in ready-to-connect<br />

condition with a cable and a Tuchel plug for the<br />

direct connection to an Analogue-Entry-Panel LP-<br />

AEP8A. The power supply is conducted via Pin 5 =<br />

+24V and Pin 6 = GND.<br />

For connection to a panel without sensor power<br />

supply (e.g. LP-AEP8), you additionally require a<br />

24V power supply unit.<br />

Output Signal 4 - 20mA<br />

Supply Voltage <strong>10</strong> - 30 V DC not controlled, two-wire circuit, with plug-on display 13 - 30 V DC<br />

Electrical Connection Angle Plug 4-pole, DIN 43 650<br />

Protection Category IP 65<br />

EEX Upon Request<br />

Dimensions L approx. <strong>10</strong>0 mm, D approx. 48 mm with plug<br />

Order Code Description<br />

IS-PTOT-R-16-ea Low Dead Space pressure transducer 0- 16 bar relative with connection cable 1,5m for LAB-<br />

PNC Panel LP-AEP8A<br />

IS-PTOT-A-16-ea Low Dead Space pressure transducer 0- 16 bar absolute with connection cable 1,5m for LAB-<br />

PNC Panel LP-AEP8A<br />

IS-P-Z-AA Electronic Plug-On Display<br />

Nn<br />

ea=Electrical Connection:<br />

T Tuchel-Plug for LAB-PNC<br />

O Open Ends for MSR-PNC<br />

Example Order:<br />

pressure transducer 0 - 16 bar abs., with connection<br />

cable 1,5 m for LabManager Panel LP-AEP8A,<br />

Order Code: IS-PTOT-A-16-T<br />

Other Measurement Ranges are available upon request.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Process Analytics and Sensors<br />

Hose Pressure Transmitter<br />

These novel pressure transmitters measure the<br />

pressure or the differential pressure at normal hoses<br />

from the exterior. For this reason, they are<br />

particularly suited for sterile applications. No<br />

mounting parts are required in the hose. The plant is<br />

completely sterilised and the hose is merely inserted<br />

into the sensor after sterilisation. The novel<br />

measurement principle is subject to legal protection.<br />

The Advantages:<br />

� Suited for sterile applications<br />

� Media compatibility determined by hose<br />

� Subsequent mounting possible<br />

� Differential and absolute pressure<br />

measurement<br />

� The sensor can be operated with all load cell<br />

amplifier types<br />

Technical Data:<br />

The sensor can, in particular, be used for pressure<br />

measurement and filter monitoring in bio-technical,<br />

sterile plants.<br />

Due to the measurement principle, the specification<br />

is strongly dependant of the hose (diameter, wall<br />

thickness, material). For this reason, the values<br />

stated below are only to be considered as guideline<br />

values. In particular in case of thin hoses and great<br />

wall thicknesses, greater deviations may occur. In<br />

practice, in case great care is directed at the<br />

calibration, significantly better specifications are<br />

usually reached at hose diameters >=<strong>10</strong> mm.<br />

Measurement Principle Measuring of the hose wall force from the exterior<br />

Resolution < 1 mbar<br />

Characteristic Line Deviation * < 50 mbar<br />

Zero Point Stability < 30 mbar<br />

Reproducibility* < 20 mbar<br />

Hysteresis Faults* < 30 mbar<br />

Stability/Year* < 50 mbar/a<br />

Response Time (<strong>10</strong> - 90%)* approx. 1 sec<br />

Temperature Dependency Calibration at operating temperature ± 5°C expedient<br />

Measurement Media Temperature * <strong>10</strong> to +50°C<br />

Ambient Temperature <strong>10</strong> to +40 °C<br />

Parts in Contact with Media Hose material<br />

Hose Diameter 3 to 22 mm<br />

Output Signal 6 conductor-resistance bridge<br />

Electrical Connection 6-pole LEMO-plug Size 1<br />

Protection Category IP 20<br />

Ex-Protection Equipment Upon request<br />

Dimensions 140x120x45mm<br />

* with silicone hose 22mm<br />

Order Code Description<br />

IS-P-TUBE-sd Pressure Transmitter 0 – 2 bar, for hose diameter of 3mm to 22mm, absolute and differential<br />

pressure with connection cable 1.5m for 6-conductor measurement amplifier<br />

HK-GRADOMV1 Measurement amplifier 1 channel, external measurement amplifier for connection to analogue input<br />

HK-AD24DMS4 Measurement system 4 channels, card for <strong>HiTec</strong> <strong>Zang</strong> PNC panel<br />

*** requires LP-DMS4DA4PTR<br />

sd = Exterior Hose Diameter in mm<br />

Special designs available upon request.<br />

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Humidity Sensors<br />

Process Analytics and Sensors<br />

The humidity sensor IS-M-FEU1 has a linear<br />

operational range of 0-<strong>10</strong>0%. Trough laser trimming<br />

down to 2 %, the sensor can be exchanged in most<br />

cases without the need of additional calibration. The<br />

sensor is delivered without housing. When installing<br />

it, care must be taken that the humidity diffusion to<br />

the sensor is not disturbed.<br />

Technical Data:<br />

Measurement Uncertainty ± 2 %, 0-<strong>10</strong>0%, not condensing<br />

Linearity Fault ± 0.5 % typical<br />

Hysteresis Fault ± 0.8 % of range<br />

Reproducibility ± 0.5 %<br />

Stability ± 1 % in 5 years<br />

Response Time 1/e 15 s in slowly agitated air<br />

Operational Range 0 - <strong>10</strong>0%, not condensing<br />

Working temperature Range -40 to 85°C<br />

Output Signal 0.8V at 0%, 4V at <strong>10</strong>0%<br />

Temperature Dependency 0.22%/°C of reading value<br />

Dimensions 6mm x 9mm x 19mm<br />

Connection to the LabManager:<br />

Scaling of the Analogue Input:<br />

The sensor is delivered ready to connect with a<br />

cable and a Tuchel plug for direct connection to an<br />

analogue input Panel LP-AEP8A. The power supply<br />

is conducted via Pin 5 = +24V and Pin 6 = GND.<br />

For the connection to a panel without sensor supply<br />

LP-AEP8, you additionally require an adapter cable<br />

with wall power supply ZK-LAB-HI99-IA-XA-Y-0.1.<br />

Interface Value Process Value<br />

0.8 V 0 %<br />

4 V <strong>10</strong>0%<br />

Under laboratory conditions, the temperature fault is<br />

situated within the scope of the measurement<br />

uncertainty and does not need to be corrected.<br />

Increased temperature range available upon<br />

request.<br />

Order Code Description<br />

IS-M-FEU1 Humidity sensor with connection cable for LabManager Panel LP-AEP8A<br />

ZK-LAB-HI99-IA-XA-Y-0.1 Adapter cable for AEP8 (not actived!) with wall power supply for the sensor 24V DC<br />

Distance and Rotational Speed Measurement<br />

Inductive Proximity Switch<br />

With the help of a proximity switch, the position of an<br />

object and the rotational speed at a rotating object<br />

can be measured and monitored.<br />

The Sensor generates an impulse at every approach<br />

to the optical, respectively magnetic marking. The PI<br />

collects the pulse frequency and calculates the<br />

rotational speed hereof.<br />

Inductive Proximity Switch as a Rotational Speed Sensor<br />

Order Code Description<br />

IS-G-REFL1 Infrared reflection sensor, max. switching frequency <strong>10</strong>0Hz, exterior diameter 12mm<br />

IS-G-IND1 Inductive proximity switch<br />

Suited cards and connection modules: HK-DEA16F with LP-DEP8A or MB-DEB8 with cable adapter.<br />

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Process Analytics and Sensors<br />

Weight Measuring and Load Cells<br />

KMZ<strong>10</strong>00 to KMZ30000<br />

KMZ50k to KMZ<strong>10</strong>00k<br />

The load cells can be used for:<br />

� Vessel Weighing<br />

� Reactor Content Measurement (see Reactor<br />

Weighing)<br />

� Gravimetric Dosing (see also GraviDos)<br />

A load measuring system consists of a load cell IS-<br />

W-KMZxxxx, and, optionally, an external<br />

measurement amplifier HK-GRADOMV1 or a PIinternal<br />

measurement system HK-AD24DMS4 for<br />

four channels.<br />

The digital measuring amplifier HK-GRADOMV1D<br />

enables the connection to a serial interface.<br />

Technical Data (KMZ<strong>10</strong>00 to 3000)<br />

Measurement<br />

Approx. 0.01%<br />

Resolution<br />

Measurement<br />

Approx. 0.1% p.U.<br />

Uncertainty<br />

Dimensions<br />

approx. 195x40x52 mm<br />

(without rodding)<br />

Ex-Protection optional<br />

Connection 6 pole LEMO-plug, Type<br />

FFA.11S.306.CLACxx<br />

Technical Data (KMZ50k to <strong>10</strong>00k)<br />

Accuracy Classes D1, C3, C4, C6<br />

Calibratable Up to 6000 Parts<br />

Approvals OIML, NTEP, Ex, GOS<br />

Order Code Description<br />

IS-W-KMZ<strong>10</strong>00 Load cell, 0 to <strong>10</strong>00g, including cable<br />

IS-W-KMZ3000 Load cell, 0 to 3000g, including cable<br />

IS-W-KMZ7500 Load cell, 0 to 7500g, including cable<br />

IS-W-KMZ15000 Load cell, 0 to 15 kg, including cable<br />

IS-W-KMZ30000 Load cell, 0 to 30 kg, including cable<br />

IS-W-KMZ<strong>10</strong>00D Load cell, 0 to <strong>10</strong>00 g, integrated measurement amplifier, RS232 interface, including cable<br />

IS-W-KMZ3000D Load cell, 0 to 3000 g, integrated measurement amplifier, RS232 interface, including cable<br />

IS-W-KMZ7500D Load cell, 0 to 7,5 kg, integrated measurement amplifier, RS232 interface, including cable<br />

IS-W-KMZ15000D Load cell, 0 to 15 kg, integrated measurement amplifier, RS232 interface, including cable<br />

IS-W-KMZ30000D Load cell, 0 to 50 kg, integrated measurement amplifier, RS232 interface, including cable<br />

IS-W-KMZ50k Load cell, 0 to 50 kg, including cable<br />

IS-W-KMZ<strong>10</strong>0k Load cell, 0 to <strong>10</strong>0 kg, including cable<br />

IS-W-KMZ200k Load cell, 0 to 200 kg, including cable<br />

IS-W-KMZ500k Load cell, 0 to 500 kg, including cable<br />

IS-W-KMZ<strong>10</strong>00k Load cell, 0 to <strong>10</strong>00 kg, including cable<br />

HK-GRADOMV1 Measurement amplifier 1 channel, external measurement amplifier for connection to<br />

analogue input<br />

HK-GRADOMV1D Digital measurement amplifier 1 channel, external measurement amplifier, RS232 interface<br />

HK-GRADOMV1D-SN Power supply for digital measurement amplifier HK-GRADOMV1D<br />

HK-AD24DMS4 Measuring system 4 channels, Card for <strong>HiTec</strong> <strong>Zang</strong> PNC panel<br />

IL-GRADOADV Adapter-square, manifold measuring cell to square aluminum construction system<br />

IL-GRADOADR12 Adapter-round, manifold measuring cell to 12 mm tube construction systems<br />

IL-GRADOADR14 Adapter-round, manifold measuring cell to 14 mm tube construction systems<br />

Informationen zu den Messverstärkern und weitere Informationen finden Sie in den Kapiteln Laborautomatisierung<br />

Hardware, Externe Messverstärker und Laborgeräte und Komponenten, Waagen.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 255<br />

Equipment and<br />

Components<br />

Process Analytics<br />

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Dosing Systems,<br />

Pumps<br />

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Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


256<br />

Monitors<br />

Process Analytics and Sensors<br />

Monitors serve for the monitoring of limit values.<br />

They usually have a (binary) switching output or a<br />

passive switching contact.<br />

Temperature Monitor and Safety Temperature Limiter<br />

If there is possibility of damage and harm to persons<br />

and expensive equipment in case of the breakdown<br />

of the automation technology or deployed devices<br />

and components, a redundant, certified temperature<br />

monitoring, which deactivates the plant, if required,<br />

is absolutely compulsory.<br />

The external certified temperature monitor,<br />

respectively safety temperature limiter, monitors a<br />

temperature which is regulable via a potentiometer.<br />

In the case the set limit value is exceeded, the<br />

switching circuit can for example be interrupted via a<br />

potential-free switching contact and an alarm could<br />

be triggered.<br />

Temperature Monitor<br />

If the set temperature limit value is not reached, or<br />

should a fault such as a sensor breakage, short<br />

circuit or power failure, occur within the permissible<br />

temperature range, the device will shut down without<br />

delay. As soon as no malfunction is pending, it is<br />

necessary to unlock, if the device is set on<br />

temperature limiter function (TL). This unlocking can<br />

be realised by a push-button on the device or via an<br />

external push-button.<br />

Technical Data<br />

For safety reasons, it is in most cases advisable to<br />

use a normally closed contact (NCC).<br />

The temperature monitors may only be deployed<br />

together with an additional control system such as<br />

the LabManager System.<br />

The temperature monitor, respectively safety<br />

temperature limiter are intended for mounting on<br />

standard rails and must be installed in a control box,<br />

respectively control cabinet.<br />

The temperature monitor, respectively safety<br />

temperature limiter is integrated into the existing<br />

Emergency Stop circuit or deployed in connection<br />

with a suited contactor.<br />

The safety temperature limiter accords to the Safety<br />

Category SK 3 of DIN/EN 954-1.<br />

Adjustable Sensor Input Resistance Thermometer (PT<strong>10</strong>0, 3-wire)<br />

Thermal Element (Types J, K, T, E, R, S, B)<br />

Measuring Circuit Sensor Breakage Identification<br />

Monitoring<br />

Short Circuit Identification (only at PT<strong>10</strong>0)<br />

Output Relay, Change-over Contact, max. 3A, 250 VAC<br />

Display LED supply voltage, fault message sensor breakage, lock ON<br />

Resetting 1 push-button on front panel or external push-button<br />

Versions Smallest Setting Step 1C°<br />

Input Measuring Range<br />

PT <strong>10</strong>0 DIN EN 60751 0... 400°C<br />

Fe-CuNi (J) DIN EN 60584 0... 400°C<br />

NiCr-Ni (K) DIN EN 60584 0... 400°C<br />

Cu-CuNi (T) DIN EN 60584 0... 400°C<br />

NiCr-CuNi (E) DIN EN 60584 0... 400°C<br />

Dimensions Depth: <strong>10</strong>0 mm<br />

Width: 22 mm<br />

Height: <strong>10</strong>2 mm<br />

Mounting Snap-on mounting on standard 35 mm rail<br />

Power Supply 115/230VAC or 24VDC<br />

Ambient Conditions <strong>10</strong>..55°C, max. 85% humidity, no bedewing<br />

Order Code Description<br />

HP-SITEMPWAE1 External Temperature Monitor for PT<strong>10</strong>0 or Thermal Elements<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Safety Temperature Limiter<br />

Process Analytics and Sensors<br />

If the permissible temperature limit is exceeded, or<br />

at the occurrence of a malfunction, the STL will,<br />

without delay, switch the plant to an operationally<br />

safe condition. The device can be deployed in<br />

connection with the resistance pick-ups of the type<br />

Pt<strong>10</strong>0.<br />

The limit temperature T can be adjusted via a<br />

frontally located scaled potentiometer. Unintended,<br />

respectively unauthorised setting of the limit value is<br />

prevented by a lead-sealable transparent cover.<br />

Technical Data<br />

Sensor Connection Resistance Thermometer PT <strong>10</strong>0, 3-wire according to EN 60751/IEC 781<br />

Measuring Circuit Monitoring Sensor Breakage Identification, Short Circuit Identification<br />

Output Relay, Change-over Contact, max. 3A, 250 VAC<br />

Display LED supply voltage, fault message sensor breakage, lock ON<br />

Resetting 1 push-button on front panel or external push-button<br />

Temperature Ranges Type A: 0...200°C, Type B: <strong>10</strong>0...300°C, Type C: 200...500°COther<br />

Measuring Ranges -200...+700 °C available upon request<br />

Dimensions Depth: 121 mm, Width: 42 mm, Height: 82 mm<br />

Power Supply 115/230VAC or 24VDC<br />

Mounting Snap-on mounting on standard 35 mm rail<br />

Ambient Conditions <strong>10</strong>..55°C, max. 85% humidity, no bedewing<br />

Order Code Description<br />

HP-SITEMPBEG1 External Safety Temperature Limiter for Pt<strong>10</strong>0<br />

Flow Monitors<br />

Low-cost flow monitors with fixed switching point.<br />

Robust mechanical flow monitor for monitoring of<br />

cooling and heating circuits.<br />

The connection to the LabManager/box is conducted<br />

via digital input. The monitor is suited for looping into<br />

a monitor chain.<br />

Technical Data:<br />

Switching Point 60 l/h, 120 l/h permanent adjustment<br />

Operational Pressure 7 bar at 20°C, 3.5 bar at 80°C<br />

Measured Media Temperature Max. +<strong>10</strong>0°C<br />

Ambient Temperature -25°C to +70°C<br />

Parts in Contact with Housing PP, seal FKM, spring made of high-grade steel<br />

measurement Media<br />

Connection R ¾“ Inner thread, corner mount version<br />

Stability Water, silicone oil, in case of chemicals, verification is necessary<br />

problematic: some solvents, materials containing chlorine, oxidants<br />

Switching Contact Normally open contact<br />

Switching Load Max. 5A AC/ 0.3A DC/ 250 V<br />

EEX in intrinsically safe electric circuits Zone 1<br />

Dimensions Length approx. <strong>10</strong>0 mm, width approx. 64 mm<br />

Order Code Description<br />

IB-FVGE-60-GMG3/4-ea Flow monitor 60 l/h, R ¾“, with connection cable 1.5 m for LAB- or PMC-PI<br />

IB-FGVE-120-GMG3/4-ea Flow monitor 120 l/h, R ¾“, with connection cable 1.5 m for LAB- or PMC-PI<br />

ea=Connection<br />

T Tuchel plug for LAB-PI<br />

O Open ends for PMC-PI<br />

Order Example:<br />

Flow monitor 120 l/h, R ¾“, with connection cable<br />

1.5 with open ends for LabManager<br />

Order Code: IB-FVGE-120-GMG3/4-O<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 257<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


258<br />

Pressure Monitor<br />

Process Analytics and Sensors<br />

Robust mechanical pressure monitor for industrial<br />

application.<br />

� For Pressure Monitoring independent of the<br />

Pressure Measurement<br />

� High Overload Capacity<br />

The connection to a LabManager/box is conducted<br />

via a digital input. The device is suited for integration<br />

into a monitor chain.<br />

Technical Data:<br />

Setting Range 0,5 - 6 bar relative<br />

Hysteresis Fixed 0,15 bar<br />

Maximum permissible<br />

Pressure<br />

16 bar<br />

Measurement Media<br />

Temperature<br />

Max +85°C<br />

Ambient Temperature -25°C to +70°C<br />

Parts in Contact with<br />

Measurement Media<br />

High Grade Steel 1.4571 + 1.4<strong>10</strong>4<br />

Pressure Connection Outside Thread G 1/2“<br />

Resistance Many chemicals except chloric ones, HCI, oxidants<br />

Switching Contacts 1-pole changeover switch<br />

Switching Capacity Max. 5A AC, 0,3A DC, 250V AC/DC<br />

Electrical Connection Angular Connector 4-pole, DIN 43 650<br />

Protection Class IP 54<br />

EEX In intrinsically safe electrical circuits Zone 1<br />

Compression-proof enclosed version is available.<br />

Dimensions L approx. <strong>10</strong>5 mm, W approx. 112 mm with Jack<br />

Order Code Description<br />

IB-PRKO-6-ma-ea Pressure Monitor 0 - 6 bar relative, with connection cable 1,5m for LAB- or MSR-PNC<br />

ma=Media Connection<br />

AG1/2 Screw Socket G ½“<br />

ea=electrical Connection<br />

T Tuchel-Connector for LAB-PNC<br />

O Open Ends for MSR-PNC<br />

Example Order:<br />

Pressure Monitor 0 - 6 bar rel., G1/2“, with<br />

connection Cable 1,5 m with open ends for<br />

LabManager<br />

Order Code: IB-PRKO-6-AGG1/2-O<br />

Available upon request:<br />

� Other Switching Ranges<br />

� Differential Pressure<br />

� EEX Version<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Process Analytics and Sensors<br />

Flow Monitor with visual Flow Control<br />

Robust mechanical flow indicator (rotameter) with<br />

adjustable switching point for monitoring of cooling<br />

and heating circuits.<br />

The connection to the LabManager/box is conducted<br />

via an active digital input with 24V DC power supply.<br />

The monitor is suited for looping into a monitor<br />

chain.<br />

Technical Data:<br />

Adjustment Range 24 l/h to 1200 l/h<br />

Operational Pressure max. 7 bar<br />

Repeat Accuracy 2%<br />

Switching Point<br />

Accuracy<br />

± 5%<br />

Measured Media<br />

Temperature<br />

Max. +80°C<br />

Ambient Temperature max. +65°C<br />

Parts in Contact with<br />

Measured Media<br />

Housing PP, seal BUNA N<br />

Connection G 1/4“ Inner thread<br />

Stability Water, silicone oil, in case of chemicals, verification is necessary<br />

problematic: some solvents, materials containing chlorine, oxidants<br />

Supply Voltage 24 V DC<br />

Switching Contact Normally open and closed contact<br />

Switching Load max. 1 A, 24 V DC<br />

EEX no<br />

Dimensions 78 x 60 x 61 mm<br />

Order Code Description<br />

IB-FVGE-1200-GMG1/4-ea Flow monitor 1200 l/h, G ¼“, with connection cable 1.5 m for LAB- or PMC-PI<br />

ea=connection<br />

T Tuchel plug for LAB-PI<br />

O Open ends for PMC-PI<br />

Order Example:<br />

Flow monitor 1200 l/h with visual indicator, G 1/4“,<br />

with connection cable 1.5 m with Tuchel plug for<br />

LAB-PI<br />

Order Code: IB-FVGE-1200-GMG1/4-T<br />

Available upon request:<br />

� Greater Flow Rates and Connection Diameters<br />

� Materials: Brass, Cr-Ni-Steel<br />

� As Sensor 0-<strong>10</strong> V or Impulse Output<br />

� Without Electronics as visual Flow Indicator<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 259<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


260<br />

Filling Level Monitor<br />

Optically<br />

Process Analytics and Sensors<br />

Optical filling level monitor for monitoring of the filling<br />

level in reactors, feed tanks, thermostats, collecting<br />

containers.<br />

Features<br />

� No moving parts<br />

� Parts in contact with media made of DURAN-<br />

Glass<br />

� Compact design<br />

� Conductive and non-conductive liquids, which<br />

absorb IR or are penetrable by IR<br />

Technical Data:<br />

Diameter of the Glass<br />

Rod (Sensor)<br />

12mm<br />

Glass Rod Lengths <strong>10</strong>0/250/300mm<br />

Used Light IR<br />

Parts in Contact with<br />

measured Media<br />

DURAN Glass<br />

Installation Glass rod 12 mm in GL-screwing or similar<br />

Switching Contacts PNP, normally open and closed contact<br />

Switching Load Max. 0.2A, 30V DC<br />

Response Time 0.65ms<br />

Supply Voltage <strong>10</strong>- 30V DC<br />

Electrical Connection Cable 2 m<br />

Protection Category IP 65<br />

EEX Upon request<br />

Dimensions Diameter max. approx. 20 mm<br />

Order Code Description<br />

IB-LWE-<strong>10</strong>0-sk-ea Opto-electronic level monitor <strong>10</strong>0 mm,<br />

with connection cable 2 m for LAB- or PMC-PI<br />

IB-LWE-250-sk-ea Opto-electronic level monitor 250 mm,<br />

with connection cable 2 m for LAB- or PMC-PI<br />

IB-LWE-300-sk-ea Opto-electronic level monitor 300 mm,<br />

with connection cable 2 m for LAB- or PMC-PI<br />

sk=Switching Contact:<br />

NC Normally closed contact: opens with<br />

rising level<br />

NO Normally open contact: closes with<br />

rising level<br />

Thermal<br />

The phase detector PhaDec can also be used as<br />

filling level monitor. It functions with all liquids<br />

independent of optical or other properties.<br />

The functional principle of these monitors is based<br />

on total reflection. The end of the glass rod is slightly<br />

grinded at an angle of 45°. As long as the rod is<br />

suspended in air, incoming light at the conical end is<br />

totally reflected. As soon as the rod end submerges<br />

into a more dense material than air, no more<br />

reflection occurs and the reflection sensor does not<br />

receive anymore light.<br />

The glass rod d = 12 mm can be inserted with<br />

standard GL-25 screwings and with according<br />

adaptors in grindings NS 29/32.<br />

The monitor is connected at an active digital input of<br />

the LabManager/box. The monitor is not suited for<br />

looping into a monitor chain.<br />

ea=Connection<br />

T Tuchel plug for LAB-PI<br />

O Open ends for PMC-PI<br />

You will find further information under PhaDec<br />

Phase Limit Detector.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Floaters<br />

Process Analytics and Sensors<br />

Filling level monitor based on a floater mechanism<br />

are utilised to monitor the filling levels in feed tanks,<br />

thermostats and collecting containers.<br />

� No auxiliary energy necessary<br />

� No special requirements to the media<br />

� Applicable as normally open and closed contact<br />

(depending on installation)<br />

The monitor is connected at an active digital input of<br />

the LabManager/box. The monitor is not suited for<br />

looping into a monitor chain.<br />

Technical Data:<br />

Parts in Contact with<br />

measured Media<br />

PVDF<br />

Installation Vertical<br />

Switching Contact NOC<br />

Switching Load 25W, 24V<br />

Supply Voltage Not required<br />

Electrical Connection Tuchel plug of LAB-PI or open ends for PMC-PI<br />

Protection Category IP67<br />

EEX No<br />

Dimensions approx. Ø 27 mm<br />

Order Code Description<br />

IB-LWE-250-NC-ea Filling level monitor based on floater mechanism<br />

ea=Connection<br />

T Tuchel plug for LAB-PI<br />

O Open ends for PMC-PI<br />

Order Example:<br />

Level monitor (at limit exceedance), with connection<br />

cable 2 m with Tuchel-plug for LAB-PI<br />

High Pressure Float Monitor<br />

This filling level monitor based on a floater<br />

mechanism is suited for applications at very high<br />

pressures.<br />

The floater has two switching points.<br />

� No auxiliary energy necessary<br />

� No special requirements to the media<br />

� Applicable both as normally open and closed<br />

contact<br />

The monitor is connected at an active digital input of<br />

the LabManager/box.<br />

Order Code: IB-LWE-250-NC-T<br />

Available upon request:<br />

� Floater, posistor, ultra-sonic, radar...flow sensors<br />

and monitors<br />

� EEX versions<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 261<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


262<br />

Technical Data:<br />

Process Analytics and Sensors<br />

Connection Casing Aluminum<br />

Process Connection Screwing thread G 1/2'' in downward direction<br />

HD Version Slide Tube 12 mm (optionally 14 mm) total length: 200 mm<br />

Switching Points L1 = 60 mm change-over switch, L2 = 155 mm change-over switch<br />

Floater PN80 Titanium<br />

Density <strong>10</strong>00 kg/m¨<br />

Pressure <strong>10</strong>0 bar<br />

Temperature 150 °C<br />

Measurement Value High-grade steel 1,4571, with connection casing and thread<br />

Transmitter<br />

Connection Casing Aluminium positioned with 60mm clearance<br />

Process Connection Screwing thread G 1/2'' in downward direction<br />

Order Code Description<br />

IB-LWDRU-NC-ea Floater magnetic switch made of high-grade steel 1,4571 with connection casing<br />

ea=Connection<br />

T Tuchel-plug for LAB-PI<br />

O Open ends for PMC-PI<br />

Order Example:<br />

Level monitor (at limit exceedance), with connection<br />

cable 2 m with Tuchel-plug for LAB-PI<br />

Order Code: IB-LWDRU-NC-T<br />

Rotational Speed Monitor<br />

The rotational speed monitor is mainly used for the<br />

monitoring of stirring drives.<br />

Scanning is mainly conducted inductively.<br />

For this purpose, a small marking in form of an<br />

electrically conductive area is placed on the rotating<br />

object. The sensor compares the impulse frequency<br />

with the set threshold and switches in case of<br />

shortfall.<br />

Available upon request:<br />

� Floater, posistor, ultra-sonic, radar...flow sensors<br />

� EEX Version<br />

Order Code Description<br />

IB-SIND Inductive rotational speed monitor, threshold adjustable 3 - 300 impulses /min,<br />

Dimensions M30 thread x 81 mm<br />

Suited cards and connection modules: HK-DEA16N, LP-DEP8A, MB-DEB8<br />

This catalogue, due to the limited space, can only contain an excerpt of the most important products.<br />

In case you do not find what you require in the catalogue, please do not hesitate to contact us!<br />

Our experienced project engineers will gladly help you!<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Here you will find:<br />

� GraviDos® Gravimetric Dosing<br />

� AlfaDos Controlled Dropping Funnel<br />

� Pumps and Dosing Pumps<br />

� Vacuum Pumps<br />

� Reactant mixing pump<br />

� Multi-Channel Dosing Systems<br />

� SoliDos Solid Doser<br />

Dosing Systems and Pumps<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 263<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


264<br />

Dosing Systems and Pumps<br />

Controlled Dropping Funnel GraviDos ®<br />

The innovative dosing system GraviDos functions as<br />

a classical dropping funnel according to the force of<br />

gravity principle and consequently does not need<br />

any pumps. Due to this, the problems which always<br />

occur with pumps, like media incompatibility, suction<br />

problems, bubbles, etc. are eliminated. The integrated<br />

weighing system requires so little space that<br />

several dosing-units can be integrated without<br />

problems into a compact laboratory.<br />

In addition, it results in a considerable saving of cost<br />

since no expensive balances and pumps are<br />

needed.<br />

Fields of Application<br />

� Gravimetric dosing<br />

� Tank content measurement<br />

� Reactor content measurement<br />

� Mass flow rate measurement<br />

� pH-control<br />

� Titration<br />

A GraviDos system consists of a glass feed tank<br />

which is hung on the weighing system. The weight<br />

change is registered and the drain controlled by a<br />

magnetic valve. It consists of a real mass flow rate<br />

control, which does not have to be "metered" for<br />

different materials and remains unaffected by<br />

bubbling.<br />

Optionally, a pulsation-free dosing can be achieved<br />

by deploying a proportional valve. Dosing under<br />

vacuum or pressure is possible, if a pressure<br />

compensation pipe is provided.<br />

Properties and Functions<br />

� Low-cost gravimetric dosing<br />

� Compact and robust<br />

� No need for pumps<br />

� Easy to clean<br />

� Large dosing-range<br />

� Refilling without dosing interruption<br />

� Optional pulsation-free dosing<br />

� Resistant to aggressive media<br />

� Ex-suitable design available<br />

The weighing systems are available graded from 1,5<br />

kg to 15 kg, feed tanks from 500 ml to 2000 ml<br />

(above as a special production).<br />

There are GraviDos-connection boards available for<br />

the connection of four or eight weighing systems.<br />

One GraviDos dosing device occupies a channel on<br />

the GraviDos board of the LabManager. An on/off<br />

valve occupies a channel on a digital-output-board.<br />

A proportioning valve occupies a channel on an<br />

analogue-output-board.<br />

For the dosage of liquids with high viscosity, an<br />

auxiliary pressure on the feed tank can be applied, if<br />

required.<br />

A maximum of six GraviDos cards can be integrated<br />

into a PI, which corresponds to 24 channels.<br />

A HiText example application is attached. For an<br />

operation with the recipe control system HiBatch,<br />

there is the base command „Dose Gravi" (SB-<br />

DOSGRAVI). This also allows refilling during<br />

operation without interrupting the dosing process.<br />

GraviDos in a controlled circuit<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


A complete system consists of<br />

� a feed tank<br />

� a proportioning valve IV-MP-UK1 for continuous<br />

dosing or a magnetic valve IV-MB-FK1 for pulsed<br />

dosing<br />

� a suspended balance IL-GRADO-xxxx,<br />

� an external single channel measuring amplifier<br />

HK-GRADOMV1 to be connected to an analogue<br />

input socket<br />

Alternatively:<br />

� a measurement card HK-AD24DMS4<br />

� a LP- DMS4DA4PTR board for four channels<br />

(four controlled dosing circuits)<br />

Alternatively:<br />

� two measurement cards HK-AD24DMS4<br />

� a panel LP-DMS4 for four channels (eight dosage<br />

controlled circuit s)<br />

� a LP-DAP8T panel<br />

Alternatively:<br />

� a digital suspended balance to be connected to a<br />

serial interface<br />

If automatic refilling is desired, further digital outputs<br />

and valves are required.<br />

In case only one to two dosing circuits are required,<br />

it is possible to merely use the measurement<br />

amplifier HK-GRADOMV1 instead of a whole<br />

measurement system. It is connected to normal<br />

analogue input.<br />

The optional Ex-adapter enables the operation of the<br />

GraviDos load cell in explosive environments.<br />

In the standard version all parts in contact with<br />

media are only made of glass, ETFE and Kalrez .<br />

Custom designs made of other materials are<br />

available.<br />

Blast protection category inherent control [EEx ia]<br />

IIC for zone 0.1 or 2.<br />

Application Examples:<br />

Gravimetric Dosing (controlled dropping funnel)<br />

The classical dropping funnel or dosing mechanisms<br />

with pumps and balances are replaced by GraviDos.<br />

GraviDos (unpressurised system)<br />

Dosing Systems and Pumps<br />

Precise Dosing of large Amounts<br />

The medium is automatically refilled from the<br />

reservoir. During the refilling-stage, the flow is<br />

optionally kept consistent or suspended.<br />

GraviDos with feed tank<br />

Distillate Weighing<br />

During fractioned distillation, the fractions are<br />

supposed to be weighed and individually bottled.<br />

The distillate is lead into a GraviDos receiver, and<br />

after the collection of a fraction, is bottled into<br />

vessels via a distribution valve. This assembly<br />

operates under vacuum and pressure.<br />

Distillate weighing and separate bottling of the fractions:<br />

on the left: collection vessels, center: GraviDos distillate scales,<br />

right: rectification column<br />

Further information about GraviDos weighing<br />

cells can be found in the chapter balances.<br />

Technical Data<br />

Resolution Approx. 0.01% v.E.<br />

Measurement<br />

Approx. 0.1% v.E.<br />

uncertainty<br />

Dimensions load cell 200x40x50mm<br />

(without linkages)<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Components<br />

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266<br />

GraviDos ® suspended balance<br />

Dosing Systems and Pumps<br />

The GraviDos dosing system is<br />

basde upon a GraviDos<br />

suspended balance. In direct<br />

comparison to a lab balance it is<br />

extremely compact an suitable for<br />

process application.<br />

GraviDos ® pressure resistant<br />

With the pressure<br />

resistant GraviDos<br />

tank the system<br />

can be operated up<br />

to 345 bar.<br />

GraviDos ® Standing Feed Tank<br />

With the GraviDos desktop scales<br />

standing containers can also be<br />

used as feed tanks.<br />

For further information see chapter<br />

Equipment and Components.<br />

GraviDos ® heating jacket<br />

GraviDos ® - Control Device for Stand-Alone Operation<br />

The GraviDos-Stand-Alone System enables a<br />

gravimetric dosing control even without automation<br />

system. The setpoint flow rate, the final weight, and<br />

the dosing period can be preset via the installed<br />

operator interface as well as via serial or analogue<br />

interface.<br />

The two-way valve necessary for flow control and<br />

the suspended scales of the GraviDos-System are<br />

connected directly.<br />

The device is both suited for batch and continuous<br />

dosing. In addition, it also supports automatic<br />

refilling.<br />

The optional Ex-adapter enables the deployment of<br />

the GraviDos load cells in explosive environments.<br />

Blast protection category inherent control [EEx ia]<br />

IIC for zone 0,1 or 2.<br />

With the GraviDos heating jacket it is<br />

possible to heat up the GraviDos<br />

receiver containers.<br />

The heating jacket is connected to a<br />

switching socket. The heating output<br />

can be adjusted from 0 to <strong>10</strong>0%.<br />

If the interior temperature is<br />

supposed to be controlled, it is<br />

necessary to install a temperature socket in the<br />

cover or an additional optional socket.<br />

Technische Daten<br />

Power Supply 230 V, 1A<br />

Weight approx. 900 g<br />

Max. Temperature 200 °C<br />

Order Code Description<br />

IL-GRAVIDOSST1 GraviDos control device for stand-alone operation<br />

IL-GRAVIRS Optional RS232 interface<br />

IL-GRADOEX Ex equipment of the GraviDos weighing module for zones 0.1 or 2<br />

The GraviDos control device for Stand-Alone Operation is compatible with all components and accessories<br />

of the GraviDos-System.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Dosing Systems and Pumps<br />

Order Code Description<br />

IL-GRADO<strong>10</strong>00D Digital suspeded balance 1.000 g for receiver tanks up to 500ml, incl. bracket, cable<br />

IL-GRADO3000D Digital suspeded balance 3.000 g for receiver tanks up to 2000ml, incl. bracket, cable<br />

IL-GRADO7000D Digital suspeded balance 7.000 g for custom made receiver tanks, incl. bracket, cable<br />

IL-GRADO<strong>10</strong>000D Digital suspeded balance <strong>10</strong>.000 g for custom made receiver tanks, incl. bracket, cable<br />

IL-GRADO15000D Digital suspeded balance 15.000 g for custom made receiver tanks, incl. bracket, cable<br />

IL-GRADO<strong>10</strong>00 Suspended balance with tank mounting <strong>10</strong>00 g, for feed tanks up to <strong>10</strong>00 ml, incl. cable<br />

IL-GRADO3000 Suspended balance with tank mounting 3000 g, for feed tanks up to 2000 ml, incl. cable<br />

IL-GRADO7000 Suspended balance 7000 g, for customized feed tank, incl. cable<br />

IL-GRADO<strong>10</strong>000 Suspended balance <strong>10</strong>000 g, for customized feed tank, incl. cable<br />

IL-GRADO15000 Suspended balance 15000 g, for customized feed tank, incl. cable<br />

HK-GRADOMV1 Measuring amplifier 1 channel external measuring amplifier to connect to an analogue input<br />

HK-GRADOMV1D External digital measuring amplifier, 1 channel to connect to RS232 V24 interface<br />

HK-GRADOMV1D-SN Power supply for digital measuring amplifier HK-GRADOMV1D<br />

HK-AD24DMS4PTR Measurement system 4 channels, card w/o connection board for GraviDos suspended scales<br />

LP-DMS4DA4PT connection board with 4 channels for GraviDos, 4 digital inputs<br />

LP-DMSP8 connection board with 8 strain-gauge channels for GraviDos (requires 2 times HK-AD24DMS4)<br />

IL-GRAVLBB250 Feed tank* 250 ml, borosilicate glass, PTFE tap, GL 14 connection, weight: 250g<br />

IL-GRAVLBB500 Feed tank* 500 ml, borosilicate glass, PTFE tap, GL 14 connection, weight: 350g<br />

IL-GRAVLBB<strong>10</strong>00 Feed tank* <strong>10</strong>00 ml, borosilicate glass, PTFE tap, GL 14 connection, weight: 550g<br />

IL-GRAVLBB2000 Feed tank* 2000 ml, borosilicate glass, PTFE tap, GL 14 connection, weight: 900g<br />

IL-GRAVLBGRAD Grading of a feed tank (ml-scale)<br />

IL-GRAVLBS150 Receiver tank 150 ml, 345 bar, high-grade steel 316L/ DOT-3A 5000 TC-3ASM<br />

IL-GRAVLBS300 Receiver tank 300 ml, 345 bar, high-grade steel 316L/ DOT-3A 5000 TC-3ASM<br />

IL-GRAVLBS500 Receiver tank 500 ml, 345 bar, high-grade steel 316L/ DOT-3A 5000 TC-3ASM<br />

IL-GRAVIHEAT250 Heating jacket for GraviDos feed tank 250 ml<br />

IL-GRAVIHEAT500 Heating jacket for GraviDos feed tank 500 ml<br />

IL-GRAVIHEAT<strong>10</strong>00 Heating jacket for GraviDos feed tank <strong>10</strong>00 ml<br />

IL-GRAVIHEAT2000 Heating jacket for GraviDos feed tank 2000 ml<br />

IL-GRAVIHEATSON Heating jacket for GraviDos custom design<br />

IV-MB-FK1-2-1,5-UNF-ea Universal 2/2 way lab valve ETFE, FFKM, nominal diameter of 1.5 mm, Kv 0,06 m³/h, 0 to approx.<br />

3 l/h media connector 1/4" UNF with cables of 3 m for the connection to LAB-PI or MSR-PI<br />

VL-KB-MB-FK1 Fixing element to connect small and medium sized HITec <strong>Zang</strong> valves to LAB-kit-ALU-system.<br />

Please state exact valve type when ordering .<br />

IV-MP-UK1-2-0,8-ma-ea 2/2 way proportional magnetic control valve, FPM, nominal diameter of 0.8 mm, Kv 0.02 m³/h,<br />

with cables of 1.5 m for the connection to LAB-PI or MSR-PI<br />

IV-MB-UM2-2 2/2-way- high-pressure-valve, 420 bar, 24V, 4 A<br />

IV-MB-UM2-PS Power supply for 2/2-way- high-pressure-valve, 24V, 4 A, with auxillary relay<br />

VL-KB-MB-UM2 Valve-connection piece to connect one V-MB-UM2-2 valve to LabKit-ALU-system<br />

IL-GRADOADV Adapter round measurement cell reducing adapter to 12 mm tube construction systems<br />

IL-GRADOADR12 Adapter-round manifold for measuring cell on to 12 mm tube construction system<br />

IL-GRADOADR14 Adapter-round manifold for measuring cell on to 14 mm tube construction system<br />

IL-GRAVI-KAL<strong>10</strong>00 Calibration weight <strong>10</strong>00g<br />

IL-GRAVI-KAL2000 Calibration weight 2000g<br />

IL-GRAVIDOSST1 GraviDos control device for stand-alone operation<br />

IL-GRAVIRS Optional RS232 interface<br />

IL-GRADOEX Ex equipment of the GraviDos weighing module for zones 0.1 or 2<br />

IS-W-GRAVISTAND Table stand with leveling screws<br />

IS-W-GRAVIPLATE Weighing plate diameter 140mm<br />

IS-W-GRAVICRANE Three element pivot lift crane for tube guidance into open weighing containers<br />

SL-GOPGRAVITARI HiBatch basis operation: Taring a load cell<br />

SL-GOPDOSIGRAVI1 HiBatch basis operation: gravimetric dosing without refilling option<br />

*with additional Gl14 connection above for venting or pressure compensation ** higher Kv values and other materials upon request<br />

ma = Medienanschluss:<br />

SN4/6 Verschraubung für Schlauch mit<br />

Durchmesser innen/außen 4,0/6,0 mm<br />

GMG1/8 Gewindemuffe G 1/8“<br />

ea = Elektrischer Anschluss<br />

T Tuchel-Stecker für LAB-PI<br />

O offene Enden für MSR-PI<br />

Automatic<br />

Laboratory<br />

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Hardware<br />

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Software<br />

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Technology<br />

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268<br />

Dosing Systems and Pumps<br />

Controlled Dropping Funnel AlfaDos<br />

The dosing system AlfaDos functions like the<br />

classic dropping funnel according to the force of<br />

gravity principle or supported with pressure and, like<br />

these, does not need any pumps. Due to this, the<br />

problems, which always occur with pumps, such as<br />

media incompatibility, suction problems, bubbles,<br />

etc. are eliminated.<br />

In addition, it leads to a considerable saving of<br />

expense since no expensive balances and pumps<br />

are needed. The flow is controlled via a magnetic<br />

valve. As there is no measurement or control of the<br />

flow rate, the dosing rate is not particularly accurate.<br />

In some cases, for example during the pHadjustment,<br />

the consistent compliance to a specific<br />

dosing-rate is however not so important. In this case<br />

AlfaDos is the absolute the lowest-cost solution.<br />

Application fields<br />

� Simple dosing tasks<br />

� pH-control<br />

� RedOx-adjustment<br />

� Titration<br />

� Dosing depends on process sizes<br />

An AlfaDos system consists of a supply vessel of<br />

glass, stainless steel, or synthetic material. The<br />

drain occurs due to the force of gravity or applied<br />

pressure and is controlled via a magnetic valve.<br />

Dosing under pressure or vacuum is possible if<br />

pressure compensation pipe is provided..<br />

Applications:<br />

The classical dropping funnel or dosing mechanisms<br />

with pumps and balances are replaced by AlfaDos, if<br />

the requirements regarding the stability of the dosing<br />

rate are modest, or the dosing is adjusted in<br />

dependency to another variable, for example the pH<br />

value or the RedOx potential, or if a controlled<br />

variable, such as the temperature, is deployed as a<br />

process signal.<br />

In the standard version, any material in contact with<br />

media is made glass, PTFE and PVDF. Special<br />

versions in other materials are also possible.<br />

An AlfaDos dosing device occupies a channel for the<br />

valve on a digital-output-board.<br />

Properties<br />

� Low-cost<br />

� Compact and robust<br />

� Does not need pumps<br />

� Resistant to aggressive media<br />

� Easy to clean<br />

Technical data<br />

Viscosity range 0,1...<strong>10</strong>0 mPa s<br />

Pressure range 0...1 bar abs.<br />

(for overpressure on<br />

request)<br />

H2O flow range up to <strong>10</strong>0 ml / min<br />

(di=2 m³, h=50cm, no<br />

pressure)<br />

H2O flow range up to 20 ml / min<br />

(di=1 m³, h=50cm, no<br />

pressure)<br />

H2O flow range up to 500 ml / min<br />

(di=2 m³, auxiliary<br />

pressure of 1 bar)<br />

Order Code Description<br />

IL-GRAVLBB250 Feed tank* 250 ml, Borosilicate glass, PTFE tap, GL 14 connection, 250 g<br />

IL-GRAVLBB500 Feed tank* 500 ml, Borosilicate glass, PTFE tap, GL 14 connection, 350 g<br />

IL-GRAVLBB<strong>10</strong>00 Feed tank* <strong>10</strong>00 ml, Borosilicate glass, PTFE tap, GL 14 connection, 550 g<br />

IL-GRAVLBB2000 Feed tank* 2000 ml, Borosilicate glass, PTFE tap, GL 14 connection, 900 g<br />

IV-MB-FK1-2-1,5-UNF-ea Universal 2/2 way lab valve PVDF, FFKM, nominal diameter of 1,5 mm, Kv 0,06 m³/h, 0 to<br />

approx. 3 l/h, media connector 1/4“ UNF, 3m cables for the connection to LAB-PI or MSR-PI<br />

VL-KB-MB-FK1 Valve to valve fixing element for LAB-kit-ALU-system<br />

*with additional Gl14 connection above for aeration or pressure compensation ** higher Kv values and other materials on request<br />

ea = Electrical connection T Tuchel plugs for LAB-PI<br />

O open ends for MSR-PI<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Pumps, dosing pumps<br />

Pumps, just as valves, have an important role in<br />

laboratories and pilot plant stations. Their variety is<br />

nearly unmanageable as they are needed for<br />

conveying, circulating or detailed volume dosing of<br />

the smallest to bigger material flows, across a large<br />

scale of viscosity values even with solids or for<br />

emulsions. Also the dosing of gases and the<br />

evacuating of plants belongs to the application area.<br />

Here, you can also expect our competent advice and<br />

individual lay out design especially for your<br />

application. Our know-how stretches over the most<br />

famous manufactures like: <strong>HiTec</strong> <strong>Zang</strong> Prominent,<br />

Lang, Gather, Ismatec, Speck, Lewa and many<br />

more, so that we can also help you with realising<br />

special tasks.<br />

Areas of Application<br />

� Circulation of heating and cooling media<br />

� Dosing of ingredients<br />

� Transport of ingredients, intermediate and final<br />

products<br />

� Generation of pressure, e.g. in pressure reactors,<br />

for filtering<br />

� Generation of vacuum<br />

� Ex-area zone 1 and 2 with pressure enclosed exthree-phase<br />

motor, respectively special versions.<br />

Which Pump for which Application?<br />

For the most important tasks in the laboratories and<br />

pilot plant stations, you can find approved standards<br />

under “First Choice”, which will help you to make<br />

your choice. With help of the following table, you can<br />

find the appropriate pump for various applications.<br />

In case of doubt, clarify with our project department<br />

which application you need.<br />

Here you will find:<br />

� Peristaltic pumps<br />

� Pneumatic pumps<br />

� Magnetic membrane dosing pumps<br />

Dosing Systems and Pumps<br />

Advantages, performances<br />

� All pumps are directly controllable from<br />

<strong>HiTec</strong>-PIs<br />

� Feedback from operation parameters to<br />

monitor when required<br />

� Cables and plugs for the direct connection<br />

with your LAB-xxx or MSR-xxx PI available<br />

� Hydraulic design and tuning to the media in<br />

your plant, available auxiliary power etc. by<br />

our engineering department<br />

� Special modifications to your control tasks by<br />

variable displace volumes, frequency<br />

converter…<br />

� We search and deliver also special<br />

accessories and we deliver your pump as a<br />

ready to use device<br />

� On request, bonding into your application<br />

program by our application programmer<br />

� On request, design, construction and<br />

parameterising of your control circuit by our<br />

engineering department<br />

� Advise and adjustment to your existing<br />

automation devices completely from one<br />

source<br />

� Magnetic piston dosing pumps<br />

� Positive displacement dosing pumps<br />

� Syringe dosing<br />

� High pressure double piston dosing pumps<br />

� Eccentric spiral pumps<br />

� Tooth ring pumps<br />

� Micro-tooth ring pumps<br />

� Centrifugal pumps<br />

� Membrane vacuum pumps<br />

� Rotary valve vacuum pump<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

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technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

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Technology<br />

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270<br />

Dosing Systems and Pumps<br />

IP-P-SM1..<br />

IP-P-M1..<br />

IP-P-P1..<br />

IP-P-M2..<br />

IP-P-m³..<br />

IP-P-LabDos-P..<br />

Application \ Type<br />

dosing<br />

fluids + + + + + + + + + + + + + +<br />

aggressive + + + + + + + + o + o o o +<br />

suspensions + + + o + o +<br />

viscous + o + + o + o o + +<br />

abrasive + + o o +<br />

outgassing + + o o o<br />

high pressure o o + o + +<br />

very high pressure +<br />

in vacuum + o + o + + o o o + o +<br />

volumetric + + + + + + + + + + + o + +<br />

gravimetric in control circuit + + + + + o o o + + + + +<br />

small quantities + + + + o + + o + + o<br />

multi-channel + +<br />

melting o o + +<br />

gases + o o o + o<br />

conveying / circulation<br />

fluids + + o o o o o o o + + + + + + +<br />

aggressive + + o o o o o o o + + o o + + +<br />

abrasive + o o +<br />

viscous + o + o + o o +<br />

heat carrier o + o<br />

flammable (solvent) + + o o o o o + o o + o + o o<br />

high temperatures o o + +<br />

gases + o o o +<br />

vacuum<br />

+<br />

rough + + +<br />

fine o + o<br />

aggressive vapours + + o +<br />

general characteristics<br />

self-priming + + + + + + o + o + +<br />

pulsation free o o o + + + + + + +<br />

bi-directional flow +<br />

warming up + o o +<br />

steriliseable +<br />

ex-application o + o o o o<br />

+ = well suitable, o = conditional suitable, upon request<br />

First Choice Types for Laboratories and Pilot Plants<br />

In the following you can find a suitable pump for<br />

every application.<br />

To make clear which pump you need, we need some<br />

information from you. It is also possible to consult<br />

one of our engineers and find out together the<br />

needed information.<br />

What we will ask you:<br />

Applications:<br />

� Dosing: volumetric, gravimetric in a control circuit<br />

...<br />

� Circulation, conveying: cooling- heating media,<br />

solvents...<br />

Convey media:<br />

Particular features: density, viscosity, flammable,<br />

explosive, conductibility, aggressive, emulsion,<br />

suspension, abrasive, crystallise...<br />

IP-SYRDOS..<br />

IP-P-LabDos-T..<br />

IP-P-P3..<br />

IP-P-E1..<br />

IP-P-S1..<br />

IP-P-S2..<br />

IP-P-Rx..<br />

IP-P-Z1..<br />

IP-B-K1..<br />

IP-B-K2..<br />

IP-B-V1..<br />

Convey quantity / range<br />

Media temperature / range<br />

Vapour pressure at operation temperature<br />

Self-priming / supply / primary pressure<br />

Ambient temperature<br />

IP-B-V2..<br />

IP-B-VPS..<br />

Connections:<br />

used / wished piping, tubes, and connecting parts?<br />

Bonding in a control circuit:<br />

Actual value – signal transmitter, control accuracy,<br />

control velocity, noise magnitudes, linking with other<br />

control circuits / controllers...<br />

Particular requirements:<br />

Safety aspects, cleaning possibilities, CIPcompatible<br />

etc.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


LabDos Peristaltic Pump<br />

Dosing Systems and Pumps<br />

Superios dosing technology: One fits all!<br />

Selection criteria for pumps are their dosing range,<br />

precision of dosing, media compatibility, viscosity<br />

range, interface types etc. The LabDos laboratory<br />

dosing pump fulfils many different criteria at a<br />

remarkable low price. LabDos is suited for dosing<br />

into reaction systems, transferring between tanks,<br />

sampling from vessels, for automatic sample<br />

drawing and for other liquid handling processes.<br />

The path breaking SofDrive drive technology<br />

combines the advantages of a servo motor and the<br />

step motor. The drive disposes of the robustness,<br />

the extremely broad revolution range, the absolute<br />

precision and the high durability of a step motor, but<br />

does however not show the pulsating running<br />

characteristics of the same. The SofDrive builds a<br />

perfect team with Watson Marlow and Masterflex.<br />

Large pushbuttons allow changing settings even<br />

with thick gloves. The wide display is illuminated, a<br />

wide viewing angle is ensured. It is suited both for<br />

stand-alone operation, as well as within automation<br />

systems.<br />

Properties of LabDos dosing pumps:<br />

� Universal use<br />

� Extremely large dosing range<br />

� Pulsation free high-precision drive<br />

� Revolution direction reversible<br />

� May be calibrated in g/min and ml/min<br />

� Robust and compact stainless steel housing<br />

� Optional separated pump head<br />

� Fast mode for aspiration, drain, flushing<br />

� Manual and external control<br />

� Ergonomic and intuitive handling<br />

� Stackable<br />

The simple functional principle of a peristaltic pump<br />

enables its cost efficient use from pumping to<br />

complex fluid handling requirements. The pump<br />

head is mounted on a sloped front for easy handling<br />

and maintenance.<br />

The LabDos peristaltic pump is a displacement<br />

pump, where outer rolls will drive the liquid through a<br />

hose.The conveyed media will therefore not touch<br />

any metal, the hose is the only media touching<br />

material. A contamination of pump and media is<br />

impossible.<br />

The gentle functionial principle assures a safe<br />

conveying of high viscous, abrasive, aggressive,<br />

scher-sensitive, foaming, gas or solid loaded, pure<br />

and valuable as well as explosive liquids and gases.<br />

Advantages of the LabDos peristaltic pump:<br />

� Free of dead storage<br />

� Self priming<br />

� Direct displacement against pressure<br />

� Low pulsation<br />

� High viscosity range<br />

� No valves or seals<br />

� Suction from 50 mbar vacuum<br />

� High media resistance, inert, hygienic<br />

� Suitable for media with solid particles<br />

� Dosing of shear strain sensitive fluids<br />

� No problems with bubbles<br />

� Fluid path visible<br />

� Easy to clean, easy maintenance<br />

� Monitoring of hose run time<br />

� Exchangeable pump head (optional)<br />

In combination with a GraviDos system, LabDos<br />

pumps may be used for gravimetric dosing.<br />

At the LabDos-Vario, it is possible to exchange the<br />

pump head without having to use any tools.<br />

Available are single head, double head, as well as 5<br />

and <strong>10</strong>-fold cassettes.<br />

FDA and USP23 Class VI conform hoses are<br />

available. With the development of new hose<br />

material the life expectancy was highliy increased<br />

eg. HPT-Ultra hose times fifty. The HPT-Ultra hose is<br />

suitable for nearly all aggressive chemicals,<br />

including organic solvants like MEK, THF and Toluol<br />

or acetone.<br />

The following comparative matrix illustrates that the<br />

LabDos peristaltic pump posseses more advantages<br />

than any other pump and is therefore universally<br />

deployable!<br />

Automatic<br />

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The following comparative matrix illustrates that the<br />

LabDos peristaltic pump posseses more advantages<br />

than any other pump and is therefore universally<br />

deployable!<br />

Pump characteristics compared<br />

Dosing Systems and Pumps<br />

Peristaltic Diaphragm Gear Plunger<br />

pump pump pump pump<br />

Dosing range ++ o ++ +<br />

Exact dosing of small volumes ++ o o +<br />

Direct displacement against pressure + + - ++<br />

Bidirectional pumping ++ - - ++ o<br />

Pumping of shear strain sensitive fluids ++ ++ - o<br />

Fluids containing abrasive solids ++ - - -<br />

High viscous media ++ - - ++ -<br />

Self-priming ++ - - - - ++<br />

Dosing from/to vacuum ++ o - - ++<br />

Without dead storage ++ - - - - - -<br />

Self locking ++ - - - - - -<br />

Safe dry running ++ o - - - -<br />

Autoclavable (dependent on hose) ++ - - - - - -<br />

Chemically persistant + + o +<br />

<strong>10</strong>0% decontamination ++ - - - - - -<br />

Easy maintenance ++ o o o<br />

Price/performance ratio ++ + o - -<br />

LabDos is available with various pump heads.<br />

Technical Data<br />

Pump head P30 P<strong>10</strong>0 Easy-Load Vario4(3)<br />

Dosing range 1 μl to 30 ml/min <strong>10</strong> μl to <strong>10</strong>0 0,2ml to 1,1 l/min 0,1ml to 1(1,2)<br />

ml/min<br />

l/min<br />

Hose inner diameter 0,25 to 2,4 mm 0,5 to 4 mm 0,8 to 8 mm 0,5 to 8 mm<br />

Wall thickness 0,85 mm 1,6 mm 1,6mm 1,6mm<br />

Supply preasure 0..2 bar 0..2 bar 0..2,5 bar 0..2,5 bar<br />

Revolution speed 0,01.. 300 rpm 0,01.. 200 rpm 0,01.. 300 rpm 0,01.. 250 rpm<br />

Viscosity 0...150.000 cps, 0...150.000 cps, 0...150.000 cps, 0...150.000 cps,<br />

newt.<br />

newt.<br />

newt.<br />

newt.<br />

Communication Interfaces RS232. optionally RS485 (ModBus or CAN) and analogue (0–5V/4–20mA)<br />

RS485 Mod-bus (opt.) Up to 32 pumps using one serial interface<br />

Digital input (TTL) Start/Stop, revolution direction<br />

Drive Pulsation-free SofDriveTM precision drive<br />

Power Supply 24V DC, 600 mA , Easy-Load Vario: 24V DC, 1A<br />

Protection Class IP 20<br />

Dimensions D / W / H 250 x 165 x 1<strong>10</strong> mm<br />

Weight approx. 2 kg<br />

The projected values are maximum values. They are dependend on tubing material, pressure and viscosity. Other pump heads are<br />

available on request.<br />

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Dosing Systems and Pumps<br />

LabDos P<strong>10</strong>0, with adjustable hose fitting<br />

LabDos-vario drive with fast exchangeable<br />

and stackable pumpheads<br />

LabDos-P-Easy-Load pump<br />

Vario-4 pumphead open<br />

Stack of Vario-3 and Vario-3E pump heads LabDos-P30 pump with fast-loading mini pump head<br />

The LabDos-Easy-Load pumps allows the use of a<br />

further Easy-Load for parallel dosing.<br />

With the stackable extension pump head VARIO-4E<br />

and VARIO-3E it is possible to extend the LabDosvario<br />

to multiple traces.<br />

Hint: By parallel dosing with two stackable<br />

Vario3/Vario3-E or two Easy-Load pump heads, an<br />

outstanding pulsation free feeding over the total<br />

feeding amount can be achieved.<br />

Automatic<br />

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Order Code Description<br />

IP-P-LABDOS-P30 LabDos Pump with mini pump head max. 30 ml/min, RS232 Interface<br />

IP-P-LABDOS-P<strong>10</strong>0 LabDos Pump with single pump head max. <strong>10</strong>0 ml/min, RS232 Interface<br />

IP-P-LABDOS-P-EASYLOAD LabDos Pump with pump head Easy-Load, 3 rolls, max. revolution speed 300 rpm<br />

IP-P-LABDOS-P-EASY-E Extension pump head Easy-Load, 3 rolls, max. revolution speed 300 rpm<br />

IP-P-LABDOS-P-EASY-TC Twin chanal pump head Easy-Load, 3 rolls, max. revolution 300 rpm, max. 500ml/min<br />

IP-P-LABDOS-P-VARIO LabDos Basic unit without pump head, RS232 Interface<br />

IP-P-LABDOS-P-VARIO-3 Peristaltic pump head for vario, 3 rolls<br />

IP-P-LABDOS-P-VARIO-3E Peristaltic stackable extension pump head for LabDos vario, 3 rolls<br />

IP-P-LABDOS-P-VARIO-4 Peristaltic pump head for vario, 4 rolls<br />

IP-P-LABDOS-P-VARIO-4E Peristaltic stackable extension pump head for LabDos vario, 4 rolls<br />

IP-P-LABDOS-P-MULTI-4-5 Pump head 5-fold maximum revolution speed <strong>10</strong>0 rpm, 4 rolls<br />

IP-P-LABDOS-AE Analogue interface/input revolution control (0–5 Volt and 4–20mA)<br />

IP-P-LABDOS-SK Flexible protection caps for push buttons<br />

CZ-USB-RS232 USB/RS232 converter cable USB/Sub-D9, 3 m, connects USB and RS232 interface<br />

IP-P-LABDOS-RS232BA RS232-T-bus adapter for a pump, max. 4 pumps at a single RS232 interface possible<br />

ZK-P-HI36-BS-R2-I-01 RS232 cable Sub-D9/Sub-D9, 3 m, to connect a LAB- or MSR-PI or PC<br />

ZK-P-HI36-BS-R2-I-02 RS232-bus cable Sub-D9/Sub-D9, 0,3 m, to connect of a RS232-bus adapter<br />

IP-P-LABDOS-RS485 RS485 bus connector, control of up to 32 pump via a serial interface<br />

IP-P-LABDOS-RS485BA RS485-T-bus adapter for a pump<br />

ZK-P-HI36-BS-R4-I-01 RS485 cable Sub-D9/Sub-D9, 3 m, to connect a LAB- or MSR-PI or PC<br />

ZK-P-HI36-BS-R4-I-02 RS485-bus cable Sub-D9/Sub-D9, 0,3 m, to connect a RS485-bus adapter<br />

IP-P-LABDOS-DISPENS Optional dispenser mode for LabDos, dosage of predefined volumina and amounts<br />

IP-P-LABDOS-DISPPB Pushbutton for LabDos, to trigger dosage start<br />

IP-P-LABDOS-DOMAS DosiMaster Software for dosage profiles and graphical charts<br />

CG-LABCOMMANDER LabCommander mini-terminal for laboratory devices<br />

Order Examples:<br />

LabDos basic unit with four-wheel pump head plus<br />

extension head and analogue interface.<br />

LabDos Extensions<br />

The LabDos Bus System<br />

All LabDos pumps are bus-compatible. The user is<br />

able to choose between a RS232-based or a<br />

RS485-based bus system. With the basic RS232<br />

bus, up to four pumps can be connected to a normal<br />

RS232 or, using the converter cable CZ-USB-<br />

RS232, to a USB interface.<br />

RS232 Bus for up to four Pumps<br />

Subsequently, a LABDOS-RS232BA bus adaptor<br />

and a RS232 cable is required for each pump.<br />

IP-P-LabDos-P-VARIO<br />

IP-P-LabDos-P-VARIO4<br />

IP-P-LabDos-P-VARIO4E<br />

IP-P-LabDos-AE<br />

The optional RS485 Bus IP-P-LABDOS-RS485<br />

enables the connection of up to 32 pumps to a<br />

RS485 interface. Subsequently, a IP-P-LABDOS-<br />

RS485BA bus adaptor is required for each pump.<br />

The bus adaptors are connected to each other with<br />

a bus cable of the required length.<br />

RS485 Bus for up to 32 Pumps<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


LabDos Dispenser<br />

With the Dispenser extension, a LabDos pump<br />

becomes an independent dispenser. This enables<br />

the dosing of pre-set volumes or amounts. A<br />

dispensing process can be started using an external<br />

push-button (IP-P-LABDOS-DISPPB). This means<br />

that the set amount is dosed at the set dosing rate<br />

with every actuation of the push-button.<br />

LabDos PC Software<br />

With the DosiMaster software, it is possible to<br />

establish dosing profiles in an easy manner.<br />

The dosed amount is logged and graphically<br />

presented as a cumulative curve.<br />

The software can be extended through additional<br />

functions such as protocol print-out or data export to<br />

LIMS.<br />

Dosing Systems and Pumps<br />

Multi-Component-Mixer<br />

The Component-Mixer-Function is an extension of<br />

the DosiMaster software. It enables multicomponent<br />

mixing in batch and continuous<br />

operation through simultaneous activation of up to<br />

eight LabDos pumps.<br />

In batch operation mode, a mixture of up to eight<br />

components is established upon the actuation of a<br />

button. Hereby, it is possible to pre-set the amounts<br />

of the individual components or the mixing ration<br />

and the total amount.<br />

In continuous operation mode, the flows of the<br />

components intended for mixing, as well as the<br />

ratios in percent of the individual components, are<br />

preselected.<br />

LabCommander – Mini-Bedienstation<br />

Das LabCommander mini-Notebook ermöglicht die<br />

platzsparende Realisierung von Dosier-, Dispensierund<br />

Mischstationen auf dem Labortisch.<br />

Order Code Description<br />

CZ-USB-RS232 USB/RS232 Converter Cable USB/Sub-D9, 3 m to connect USB and RS232 interface<br />

IP-P-LABDOS-RS232BA RS232-T-Bus Adaptor for one Pump, max. 4 pumps possible at a RS232 interface<br />

ZK-P-HI36-BS-R2-I-01 RS232 Cable Sub-D9/Sub-D9, 3 m for connection to LAB- or MSR-PI or PC<br />

ZK-P-HI36-BS-R2-I-02 RS232-Bus Cable Sub-D9/Sub-D9, 0,3 m, for connection of RS232 Bus Adaptors<br />

IP-P-LABDOS-RS485 RS485 Bus Connection, activation of up to 32 pumps via a serial interface<br />

IP-P-LABDOS-RS485BA RS485-T-Bus Adaptor for one pump<br />

ZK-P-HI36-BS-R4-I-01 RS485 Cable Sub-D9/Sub-D9, 3 m for connection to LAB- or MSR-PI or PC<br />

ZK-P-HI36-BS-R4-I-02 RS485-Bus CableSub-D9/Sub-D9, 0,3 m, or connection of RS485 Bus Adaptors<br />

IP-P-LABDOS-DISPPB Dispensing-Option for LabDos wih push button to trigger dispensing processes<br />

SA-P-LABDOS-DOMAS DosiMaster Software for dosing profiles and graphical presentation of the cumulative curve<br />

SA-P-LABDOS-DOMASM DosiMaster Extension: Mixer Function<br />

CG-LABCOMMANDER LabCommander Mini-Control Station for Laboratory Devices<br />

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Maximum delivery rates in ml/min, dependant of hose diameter and pump:<br />

Di/<br />

mm<br />

P30 (at 290<br />

rpm)<br />

P<strong>10</strong>0 (at<br />

200rpm)<br />

VARIO-3<br />

(at 250<br />

rpm)<br />

VARIO-4<br />

(at 250<br />

rpm)<br />

Easy-<br />

Load<br />

(at<br />

300rpm)<br />

P30<br />

(per rev)<br />

P<strong>10</strong>0<br />

(per rev)<br />

VARIO-3<br />

(per rev)<br />

VARIO-4<br />

(per rev)<br />

Easy-Load<br />

(per rev)<br />

0,25 0,73 -- -- -- -- 0,0025 -- -- -- --<br />

0,5 2,8 3 7,5 7,5 -- 0,0095 0,015 0,03 0,03 --<br />

0,8 5,8 7 15 15 18 0,025 0,035 0,06 0,06 0,06<br />

1,6 20 22 65 62 75 0,07 0,13 0,26 0,25 0,21<br />

2,4 35 48 125 <strong>10</strong>0 113 0,12 0,25 0,5 0,4 0,35<br />

3,2 -- 82 250 212 240 -- 0,41 1 0,85 0,8<br />

4,0 -- 118 325 275 3<strong>10</strong> -- 0,52 1,3 1,1 1,0<br />

4,8 -- -- 550 475 500 -- -- 2,2 1,9 1,7<br />

6,4 -- -- 900 750 850 -- -- 3,6 3 2,8<br />

8,0 -- -- 1250 <strong>10</strong>00 1150 -- -- 5 4 3,8<br />

All value are depended on hose material and media. All values are only for orientation pusposes.<br />

IP-P-LabDos-P-MULTI-4-5.<br />

Maximum delivery rates in ml/min:<br />

Di/ mm IP-P-LabDos-P-MULTI-4<br />

(in ml at 1<strong>10</strong>rpm) approx.<br />

0,13 0,1<br />

0,25 0,5<br />

0,59 2,5<br />

0,63 3<br />

0,89 7<br />

1,02 9<br />

1,3 16<br />

1,42 18<br />

1,52 20<br />

2,06 33<br />

2,54 47<br />

2,79 55<br />

If in doubt please get in touch with us. We will<br />

Compatibility of Hose Materials<br />

advice you which hose are best suited for you<br />

media.<br />

Samples can be sent upon request.<br />

Hose Acid Base Solvent Others Remarks<br />

Name<br />

weak<br />

Mid<br />

strong<br />

weak<br />

Mid<br />

HPT-Silicon<br />

(Platin) + o - + + + - - - o - + o<br />

HPT-PVC + + - + + + - - - - - + o<br />

HPT-FuelOil + o - + o - + - - + - + -<br />

HPT-Neopren o o - + o o - - - o - + o<br />

HPT-Chem + + + + + + - - - + o + +<br />

strong<br />

aliphatic<br />

aromatic<br />

halogenated<br />

alcohols<br />

aldehyde/ketone<br />

salt<br />

oxidants<br />

*) These first class attributes do not<br />

guarantee a resistance to all<br />

chemicals. Some solvents cause<br />

swelling of the hose (e.g. Hydrocarbon,<br />

amine, CHC and other solvents). In<br />

case of doubt please order test probes.<br />

Bio compatible, very good<br />

mechanical attributes, not solvent<br />

resistant. transparent<br />

very inexpensive, very good<br />

mechanical attributes, contains<br />

diluent. Non solvent resistant. clear<br />

Special hose for motor fuels and<br />

oils. yellowish<br />

pressure/vacuum resistant, high<br />

lifetime expectancy, inexpensive black<br />

Flexibiliser free, inexpensive.<br />

Limited resistance to ketone. clear<br />

HPT-Viton® + + + + + + + + + + - + + Highly resistant, inexpensive. black<br />

pressure/vacuum resistant, high<br />

HPT-Pharm o o - + o o - - - o - + o<br />

lifetime expectancy, FDA, USP, cell<br />

culture. light beige<br />

HPT-Ultra* + + + + + + + + + + + + +<br />

Extremely high life cycle and highly<br />

resistant, expensive. dimm white<br />

+ Resistant: None or only minimal swelling, None or only minimal restriction of life span.<br />

o Limited resistance: Moderate swelling, restriction of life span. Must be tested in individual case.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Dosing Systems and Pumps<br />

- Not resistant: Strong restriction of life span or complete destruction of the hose.<br />

Availability with 1.6 mm wall thickness<br />

For LabDos P<strong>10</strong>0, Vario and Easy-Load, not suitable for P30 and MULTI-4<br />

Di/ HPT-Silicon HPT-PVC HPT-FuelOil HPT-Neopren HPT-MHL HPT-Viton® HPT-Ultra coupling<br />

mm<br />

(2 pcs.)<br />

0,8 + + + + + + -- +<br />

1,6 + + + + + + *** +<br />

2,4 + + + + + + -- +<br />

3,2 + + + + + + *** +<br />

4,0 + + + + + + -- upon request<br />

4,8 + + + + + + *** upon request<br />

6,4 + + + + + + -- upon request<br />

8,0 + + + + + + *** upon request<br />

+ available, stock article, *** only pre configured as pieces of 15cm available<br />

Availability with 0.8 mm wall thickness<br />

For P30 and MULTI-4, not suitable for LabDos P<strong>10</strong>0, Vario and Easy-Load<br />

Di/ HPT-Silicon HPT-PHARM HPT-FuelOil Tygon® Lab HPT-Viton® HPT-Ultra coupling<br />

mm<br />

(2 pcs)<br />

0,19 + upon request<br />

0,25 + + *** upon request<br />

0,51 + + + + upon request<br />

0,63 + + upon request<br />

0,89 + + + + upon request<br />

1,3 + + + upon request<br />

1,42 + + + + + upon request<br />

2,06 + + + + + upon request<br />

2,79 + + + + + upon request<br />

+ available, stock article, *** only pre configured as pieces of 15cm available<br />

The coupling element for the transition from the pump hose to other hose material is made of PVDF.<br />

All hoses are available as products sold by meter (except HPT-Ultra) or as pre configured 15 cm pieces per<br />

dozen.<br />

Analytics hoses for P30 pump heads (stock artikles):<br />

Order Code Description<br />

IP-P-HPT-PHARM-08-005-m Hose Pharmed, inner diameter 0.51 mm, wall thickness 0.8 mm<br />

IP-P-HPT-PHARM-08-009-m Hose Pharmed, inner diameter 0.89 mm, wall thickness 0.8 mm<br />

IP-P-HPT-PHARM-08-028-m Hose Pharmed, inner diameter 2.79 mm, wall thickness 0.8 mm<br />

IP-P-HPT-SILP-08-006-m Hose Silikon (platinum), inner diameter 0.64 mm, wall thickness 0.8 mm<br />

IP-P-HPT-SILP-08-013-m Hose Silikon (platinum), inner diameter 1.3 mm, wall thickness 0.8 mm<br />

IP-P-HPT-SILP-08-028-m Hose Silikon (platinum), inner diameter 2.79 mm, wall thickness 0.8 mm<br />

IP-P-HPT-PVC-08-003-m Hose PVC, inner diameter . 0,25 mm, wall thickness 0,8 mm<br />

IP-P-HPT-PVC-08-009-m Hose PVC, inner diameter . 0,89 mm, wall thickness 0,8 mm<br />

IP-P-HPT-PVC-08-028-m Hose PVC, inner diameter . 2,75 mm, wall thickness 0,8 mm<br />

IP-P-VITON-08-009-m Hose Viton®, inner diameter 0.89 mm, wall thickness 0.8 mm<br />

IP-P-VITON-08-014-m Hose Viton®, inner diameter 1.42 mm, wall thickness 0.8 mm<br />

IP-P-VITON-08-028-m Hose Viton®, inner diameter 2.79 mm, wall thickness 0.8 mm<br />

IP-P-HPT-FUELOIL-08-005-m Hose fuels and oils, inner diameter 0.51 mm, wall thickness 0.8 mm<br />

IP-P-HPT-FUELOIL-08-014-m Hose fuels and oils, inner diameter 1.42 mm, wall thickness 0.8 mm<br />

IP-P-HPT-FUELOIL-08-028-m Hose fuels and oils, inner diameter 2.79 mm, wall thickness 0.8 mm<br />

Hoses for other pumping heads can be found on the next page.<br />

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278<br />

Dosing Systems and Pumps<br />

Order Code Description<br />

IP-P-HPT-SILP-16-008-x Hose silicone (platinum), inner diameter 0.8 mm, wall thickness 1.6 mm<br />

IP-P-HPT-SILP-16-016-x Hose Silikon (platinum), inner diameter 1.6 mm, wall thickness 1.6 mm<br />

IP-P-HPT-SILP-16-032-x Hose Silikon (platinum), inner diameter 3.1 mm, wall thickness 1.6 mm<br />

IP-P-HPT-SILP-16-048-x Hose Silikon (platinum), inner diameter 4.8 mm, wall thickness 1.6 mm<br />

IP-P-HPT-SILP-16-064-x Hose Silikon (platinum), inner diameter 6.4 mm, wall thickness 1.6 mm<br />

IP-P-HPT-SILP-16-080-x Hose Silikon (platinum), inner diameter 7.9 mm, wall thickness 1.6 mm<br />

IP-P-HPT-PVC-16-008-x Hose PVC, inner diameter 0.8 mm, wall thickness 1.6 mm<br />

IP-P-HPT-PVC-16-016-x Hose PVC, inner diameter 1.6 mm, wall thickness 1.6 mm<br />

IP-P-HPT-PVC-16-032-x Hose PVC, inner diameter 3.1 mm, wall thickness 1.6 mm<br />

IP-P-HPT-PVC-16-048-x Hose PVC, inner diameter 4.8 mm, wall thickness 1.6 mm<br />

IP-P-HPT-PVC-16-064-x Hose PVC, inner diameter 6.4 mm, wall thickness 1.6 mm<br />

IP-P-HPT-PVC-16-080-x Hose PVC, inner diameter 7.9 mm, wall thickness 1.6 mm<br />

IP-P-HPT-NEOPR-16-016-x Hose Neopren, inner diameter 1.6 mm, wall thickness 1.6 mm<br />

IP-P-HPT-NEOPR-16-032-x Hose Neopren, inner diameter 3.1 mm, wall thickness 1.6 mm<br />

IP-P-HPT-NEOPR-16-048-x Hose Neopren, inner diameter 4.8 mm, wall thickness 1.6 mm<br />

IP-P-HPT-NEOPR-16-064-x Hose Neopren, inner diameter 6.4 mm, wall thickness 1.6 mm<br />

IP-P-HPT-VITON-16-016-x Hose Viton®, inner diameter 1.6 mm, wall thickness 1.6 mm<br />

IP-P-HPT-VITON-16-032-x Hose Viton®, inner diameter 3.1 mm, wall thickness 1.6 mm<br />

IP-P-HPT-VITON-16-048-x Hose Viton®, inner diameter 4.8 mm, wall thickness 1.6 mm<br />

IP-P-HPT-VITON-16-064-x Hose Viton®, inner diameter 6.4 mm, wall thickness 1.6 mm<br />

IP-P-HPT-FUELOIL-16-016-x Hose fuels and oils, inner diameter 1.6 mm, wall thickness 1.6 mm<br />

IP-P-HPT-FUELOIL-16-032-x Hose fuels and oils, inner diameter 3.1 mm, wall thickness 1.6 mm<br />

IP-P-HPT-FUELOIL-16-048-x Hose fuels and oils, inner diameter 4.8 mm, wall thickness 1.6 mm<br />

IP-P-HPT-FUELOIL-16-064-x Hose fuels and oils, inner diameter 6.4 mm, wall thickness 1.6 mm<br />

IP-P-HPT-CHEM-16-016-x Hose Chem (Tygon® chemical), inner diameter 1.6 mm, wall thickness 1.6 mm<br />

IP-P-HPT-CHEM-16-032-x Hose Chem (Tygon® chemical), inner diameter 3.1 mm, wall thickness 1.6 mm<br />

IP-P-HPT-CHEM-16-048-x Hose Chem (Tygon® chemical), inner diameter 4.8 mm, wall thickness 1.6 mm<br />

IP-P-HPT-CHEM-16-064-x Hose Chem (Tygon® chemical), inner diameter 6.4 mm, wall thickness 1.6 mm<br />

IP-P-HPT-ULTRA-16-016-x Hose High Performance, inner diameter 1.6 mm, wall thickness 1.6 mm<br />

IP-P-HPT-ULTRA-16-032-x Hose High Performance, inner diameter 3.1 mm, wall thickness 1.6 mm<br />

-x: m = product sold by meter , k = 12 pcs 15 cm segments<br />

Other hoses and couplings are available on request.<br />

Order information hose couplings (stock articles):<br />

Order Code Description<br />

IP-P-FIT-I-PV-1/8 Hose coupling 1/8", PVDF<br />

IP-P-FIT-I-PV-3/16 Hose coupling 3/16", PVDF<br />

IP-P-FIT-I-PV-1/4 Hose coupling 1/4", PVDF<br />

IP-P-FIT-I-PV-1/16 Hose coupling 1/16", PVDF<br />

IP-P-FIT-I-PV-1/8 Hose coupling 1/8", PVDF<br />

IP-P-FIT-I-PV-3/16 Hose coupling 3/16", PVDF<br />

IP-P-FIT-I-PV-1/4 Hose coupling 1/4", PVDF<br />

IP-P-FIT-R-PV-1/16-1/8 Hose coupling as reduction piece 1/16 auf 1/8", PVDF<br />

IP-P-FIT-R-PV-3/16-1/8 Hose coupling as reduction piece 3/16 auf 1/8", PVDF<br />

IP-P-FIT-R-PV-1/4-1/8 Hose coupling as reduction piece 1/4 auf 1/8", PVDF<br />

IP-P-FIT-R-PV-3/8-1/4 Hose coupling as reduction piece 3/8 auf 1/4", PVDF<br />

Other hose couplings, T- and Y-couplings are available on request.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


LabDos Gear Pumps<br />

Annual gear pumps for the pulsation-free conveying<br />

and dosing within the control circuit of particle-free<br />

liquids of low to higher viscosity with medium flow.<br />

Heating is possible.<br />

Special Characteristics:<br />

� Low-Noise Run<br />

� Valveless Design<br />

� High Pressure<br />

� Accurate and reliable<br />

� Long Term Stability<br />

� Extensive Operational Range<br />

� Small Dead Volume<br />

For operation at a LAB-PI, a RS232 interface is<br />

required.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Pump Heads:<br />

Type Maximum Delivery<br />

Rate<br />

280ML80B 280 ml/min<br />

070ML30B 70 ml/min<br />

018ML<strong>10</strong>B 18 ml/min<br />

Mode of Operation Magnet-coupled Annual Gear Pump<br />

Delivery Rate 0,05...280 ml/min / 0,012..70 ml/min / 0,03...18 ml/min<br />

Max. Pump Pressure 80 bar /30 bar / <strong>10</strong> bar<br />

Media Connections Di 4mm Da 6mm / Di 1/16" Da 8"/ Di 1/16" Da 1/8"<br />

Speed 0 to 6000 Rev/min. Speed is load-independent.<br />

System Pressure <strong>10</strong>0 bar<br />

Dosing into Vacuum No<br />

Suction Height Self-priming up to a low suction height depending on media.<br />

Materials in Contact<br />

with Media<br />

High Grade Steel 316L<br />

Media Temperature -5 ..60°C . Higher temperatures are available upon request.<br />

Activation RS232, optional 4..20mA<br />

Operational Voltage/ 230V AC, 150W<br />

Power<br />

Media Compatibility Many chemicals. Please verify individual cases.<br />

Protection Class IP 30<br />

EX Version No. If required, please contact us.<br />

Delivery Scope: Annual Gear Pump with RS232 Interface<br />

Order Code Description<br />

IP-P-Z1-280ML80B-E Gear Pump with 0,05...280 ml/min, Differential Pressure 80 bar, High Grade Steel 316L<br />

IP-P-Z1-070ML30B-E Gear Pump with 0,012..70 ml/min, Differential Pressure 30 bar, High Grade Steel 316L<br />

IP-P-Z1-018ML<strong>10</strong>B-E Gear Pump with 0,03...18 ml/min, Differential Pressure <strong>10</strong> bar, High Grade Steel 316L<br />

IP-P-Z1-HEAT Heating System for Annual Gear Pump Z1, Tmax = 60 °C<br />

ZK-IT-HI01-BS-R2-I-03 RS232 Cable Sub-D9/Sub-D9, 3 m for connection to a LAB- or MSR-PI or PC<br />

IP-P-LABDOS-RS485 RS485 Bus. Activation of up to 32 pumps via serial interface.<br />

Further accessories can be found in the Chapter „ LabDos Peristaltic Pumps“.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

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Construction and<br />

Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


280<br />

LabDos Piston Dosing Pump<br />

Valveless positive displacement piston pumps<br />

enables the precise dosing and pumping of small<br />

quantities of aggressive, viscous and crystallising<br />

media within the medium pressure and temperature<br />

range.<br />

The piston dosing pump LabDos-T is suited for<br />

varied dosing tasks even below the microlitre range<br />

(sub-microlitre).<br />

Particular Features:<br />

� Valveless Design<br />

� Chemically inert due to use of ceramic<br />

� Precise and reliable<br />

� Long term stability<br />

� Great working range<br />

� Only one moving part<br />

� Reversible<br />

� Small dead storage<br />

The displaced volume and the stroke frequency can<br />

be independently adjusted. This leads to an enormous<br />

working range. The displaced volume can be<br />

adjusted in <strong>10</strong>00 steps at the calibrating ring. The<br />

stroke frequency can be varied from 0,01 to 500 /<br />

min.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Pump Heads:<br />

Type Max.<br />

Displaced<br />

Volume<br />

Maximum<br />

Delivery Rate<br />

T-2 0 - 5 µl 0 – 2,5 ml/min<br />

T-12 0 - 25 µl 0 – 12,5 ml/min<br />

T-25 0 - 50 µl 0 – 25 ml/min<br />

T-50 0 -<strong>10</strong>0 µl 0 – 50 ml/min<br />

Operating mode Valveless positive displacement piston pump with adjustable drive<br />

Max. flow rate up to 3000 ml/h<br />

Max. discharge pressure 6,9 bar<br />

Dosing in vacuum possible<br />

Stroke frequency up to 500/min<br />

Max. Displaced Volume 5 – <strong>10</strong>0 μl<br />

Suction Lift Self-priming, dependent of media<br />

Media affecting materials PVDF/ceramic piston and bushing<br />

Media connection Hose/plastic tube inner /outer diameter = 4/6 mm<br />

Media temperature Max. <strong>10</strong>0 °C<br />

Activation serial connector RS232<br />

Power supply 230 V AC<br />

Media compatibility Various chemicals, necessity to examine in individual cases<br />

Protection Category IP20<br />

Ex-version No<br />

Delivery Scope: Piston dosing pump with RS232 interface.<br />

Order Code Description<br />

IP-P-LABDOS-T-2 LabDos pump with piston pump head, 0 – 2,5 ml/min<br />

IP-P-LABDOS-T-12 LabDos pump with piston pump head, 0 – 12,5 ml/min<br />

IP-P-LABDOS-T-25 LabDos pump with piston pump head, 0 – 25 ml/min<br />

IP-P-LABDOS-T-50 LabDos pump with piston pump head, 0 – 50 ml/min<br />

IP-P-LABDOS-AE Analogue interface /input rpm control (0–5 Volt and 4–20mA)<br />

ZK-IT-HI01-BS-R2-I-03 RS232 Cable sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />

IP-P-LABDOS-RS485 RS485 Bus, activation of up to 32 pumps via a serial interface<br />

media connection:<br />

SN4-6 Tube fitting I.D./OD 4/6mm On request deliverable:<br />

� Other flow rates<br />

� Other materials: high grade steel, carbon<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Dosing Systems and Pumps<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 281


282<br />

SyrDos2 Syringe Doser<br />

The SyrDos2 pump offers extended application<br />

options.<br />

The integrated control panel with a LC-Display also<br />

enable the operation as independent pump.<br />

It supports, in addition to the LabDos-compatible<br />

RS232 protocol, the standardised MODBus-RTU<br />

protocol. The power supply for the two pumps is<br />

integrated.<br />

If two pumps are accordingly connected with the<br />

-CONT option, continuous conveying is also<br />

possible. Shock-free change-overs are reached with<br />

a special algorithm.<br />

Due to the robust high grade steel casing, it is also<br />

suited for deployment in rouh process conditions.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

SyrDos2 Syringe Doser with 2/3-Way Valves<br />

Mode of Operation Syringe Doser with step motor drive with up to <strong>10</strong>.000 steps/s.<br />

Max. Delivery Rate Depending on syringe, 50/<strong>10</strong>0/250/500 µl and 1/2,5/5/<strong>10</strong>/25/50 ml in<br />

2,5/4,9 s<br />

Max. Pump Pressure <strong>10</strong> bar, depending on syringe. Higher pressures (up to 28 bar) are<br />

available upon request.<br />

Dosing into Vacuum Possible up to <strong>10</strong> mbar (consider the vapour pressure)<br />

Resolution 24.000/48.000 Steps<br />

Suction Height Self-priming, media-dependent<br />

Materials in Contact with Media Glass, PTFE, Kel-F or PPF, optional Ceramic<br />

Media Connections UNF ¼“ 28G<br />

Media Temperature 15 to 40°C<br />

Activation Serial Interface RS232 or RS485 (MODBus-RTU Protocol)<br />

Operational Voltage (SYRDOS2) 230V AC, <strong>10</strong>0VA<br />

Media Compatibility Many chemicals. Please verify individual cases.<br />

Protection Class IP 20<br />

Dimensions (WxHxD) 223 x 270 x 180 mm<br />

Weight approx. <strong>10</strong> kg<br />

EX Version No<br />

Order Code Description<br />

IP-SYRDOS2-ss-V2/3 SyrDos2 Syringe Doser for 50µl to 50ml Syringes, RS232, RS485, 2/3-Way Valve<br />

IP-SYRDOS2-ss-VDxx SyrDos2 Syringe Doser for 50µl to 50ml Syringes, RS232, RS485, mutliway-valve (distr)<br />

IP-SYRDOS2-ss-VNDyy Syringe Doser for 50µl to 50ml Syringes, RS232, RS485, mutliway-valve (non distribution)<br />

IP-SYRDOS-VCER Extra Charge for Ceramic Version for 2/3-Way or Multi-Way Valve (1 required per valve)<br />

IP-SYRDOS-VHPR Extra Charge for max. Pressure 28 bar for 2/3-Way or Multi-Way Valve (1 required per valve)<br />

IP-SYRDOS-SYRG-vol Syringe for Syringe Doser, Glass<br />

IP-SYRDOS-CONT SyrDos Extension for continuous conveying with two pumps<br />

IP-SYRDOS-CHCKVAL 1 Pair of nonreturn valves for SyrDos, moisted material: PEEK, Spring: Gold-plated High Grade<br />

Steel<br />

ZK-IT-HI01-BS-R2-I-03 RS232 Cable Sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />

ss = Resolution, Steps 24 = 24.000, 48 = 48.000<br />

xx = Number of Positions, 2 to12<br />

yy = Number of Ways, 3 or 4<br />

vol = 50U, <strong>10</strong>0U, 250U, 500U, <strong>10</strong>00U, 2500U, 5M,1M, 25M, 50M<br />

accordingly 50/<strong>10</strong>0/250/500 μL and 1/2/2,5/5/<strong>10</strong>/25/50 ml<br />

Example Order:<br />

Duplex-Syringe Doser, Resolution: 48.000 Steps,<br />

12-Way-Distribution Valve, Media Connection UNF<br />

1/4-28, Activation RS232, 3 m RS232 Cable for<br />

connection to LAB- or MSR-PI, 1 ml Syringe.<br />

Special Design for higher pressure. Special materials<br />

etc. are available upon request..<br />

Please do not hesitate to request more detailed<br />

information, if required.<br />

Order Codes: IP-SYRDOS-48-VD12 and IP-SYRDOS-SYRG-<br />

<strong>10</strong>00U<br />

Other delivery rates are available upon request.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Dosing Systems and Pumps<br />

Diaphragm Doser with Step Motor Control<br />

MembraneDoser and PTFE-Pump Head<br />

This pump is particularly suited for the low-pulsation<br />

conveyance of aggressive fluids within the range<br />

0‚002 L/h - 48L/h at up to 18 bar<br />

the membrane pump doser combines all features<br />

and functions of conventional dosing pumps and<br />

makes dosing so uncomplicated that you can take<br />

Dosing Heads<br />

PP Type DME PP<br />

VA (high grade steel) Type DME VA<br />

VA (electrically heated) Optional<br />

PTFE Type DME PTFE<br />

PTFE / externally cooled Optional<br />

PTFE / externally heated Optional<br />

PTFE /electrically heated<br />

Accessories<br />

Optional, with/without<br />

control for heating<br />

jackets<br />

Pulsation Absorber PTFE Optional<br />

Pulsation AbsorberVA Optional<br />

Pressurised Valve PTFE Optional<br />

(Prel.) Filter PTFE Optional<br />

Connections PTFE Optional in GL14B or<br />

GL18B<br />

Connections high grade Optional in Swagelok or<br />

steel<br />

Gyrolok<br />

Heating/cooling f. pump<br />

head/feeding<br />

Optional<br />

Vaccuum application Optional<br />

high precision for granted.<br />

The main functional principle of the pump is based<br />

on the direct connection of motor and diaphragm<br />

over a slide crank gear transmission with a tooth belt<br />

transmission. With this method, in contrary to to<br />

conventional dosing pumps, the position and the<br />

speed of the diaphragm are controlled via an<br />

electronic system with a microprocessor throughout<br />

the whole pressure/suction cycle.<br />

The stroke frequency and the duration of the<br />

pressure stroke are controlled via a microprocessorcontrolled<br />

step motor according to the required<br />

dosing quantity. This drive is unique in this category<br />

and can only found here.<br />

Alternatively, the diaphragm doser is available with<br />

PP / VA or PTFE dosing heads and / or heatable or<br />

cooled dosing units.<br />

Interfaces<br />

4-20mA yes<br />

RS232 Optional with digitalanalogue<br />

converter<br />

External Pulse yes<br />

Internal Timer yes<br />

Fieldbus-Interface yes<br />

NAMUR-Interface<br />

Technical Data<br />

Optional<br />

Operating Mode step motor- diaphragm<br />

dosing pump<br />

Flow Rate 0,002 l/h bis 48 l/h<br />

Adjustable Range Flow<br />

Rate<br />

1:<strong>10</strong>00<br />

Maximum Output 18 bar<br />

Pressure<br />

Dosing in Vacuum no<br />

Suction Lift 5 m<br />

Dosing Faults ± 1% of the set value<br />

Max. Viscosity 500 mPas<br />

In contact with Media VA or PP orPTFE<br />

Activation serial connector RS232,<br />

4-20 mA, 2-<strong>10</strong> V, single<br />

stroke control<br />

Power supply <strong>10</strong>0-230 V AC<br />

Order Code Description<br />

IP-P-SM1-VA -mc Precision step motor dosing pump, VA pump head, RS232<br />

IP-P-SM1-PP -mc Precision step motor dosing pump, PP pump head, RS232<br />

IP-P-SM1-PTFE -mc Precision step motor dosing pump, PTFE pump head, RS232<br />

ZK-IT-HI01-BS-R2-I-03 RS232 Cable sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />

mc=Model Code:<br />

Model Code Dosing Rate Max. Pressure<br />

2-18 2,5 l/h 18 bar<br />

8-<strong>10</strong> 7,5 l/h <strong>10</strong> bar<br />

12-6 12 l/h 6 bar<br />

48-3 48 l/h 2,6 bar<br />

Order example:<br />

Precision step motor dosing pump, 2,5 L/h, 18 bar,<br />

pump head PTFE,<br />

Order code: IP-P-SM1-PTFE-2-18<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

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technology<br />

Automation<br />

Hardware<br />

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Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 283<br />

Equipment and<br />

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Process Analytics<br />

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Dosing Systems,<br />

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Stirring and<br />

Dispersing<br />

Services


284<br />

Pneumatic Dosing Pumps<br />

Modotec ® Dosing system; pneumatic dosing of<br />

liquids and gases.<br />

Modular constructed dosing system consisting of a<br />

control unit and diaphragm dosing head with<br />

positively controlled diaphragm valves.<br />

The pneumatic activation ensures that the pump<br />

heads are especially suited for the Ex-range.<br />

Module Control<br />

� Autonomous Control Unit<br />

� Externally controllable<br />

� Direct control through PLS via<br />

Type C<br />

� Power Supply220V / 24 V<br />

� Compressed Air 3 – 6 bar<br />

Autonomous Control with integrated pneumatic Valve Terminal<br />

Valve Terminal for Activation via LabBox/manager or SPS<br />

Dosing Systems and Pumps<br />

Module Dosing Head<br />

� Compact Dosing Head<br />

� Small Dimensions<br />

� Version with low dead storage<br />

� No mechanically moved parts<br />

� Low wear, low-maintenance<br />

� Corrosion-resistant materials<br />

� Simple assembly and cleaning<br />

� Option: Ex-version<br />

Special Features Dosing Head Type T<br />

� Controllable Diaphragm Valves<br />

� Position-independent installation<br />

� Dosing directly into the vacuum<br />

� Optional Ex-version<br />

Special Features Dosing Head Type S<br />

� Ball Valves<br />

� Twin Dosing Heads<br />

� Optional Ex-version<br />

Special Features Dosing Head Type P<br />

� Dosing Head with additional controllable multifunction<br />

valves for automated sample drawing<br />

� Multi-Component Dosing<br />

� Multi-way Dosing Head<br />

� Optional Ex-version<br />

Special Features Dosing Head Type V<br />

� Conveyance out of the vacuum into the normal<br />

pressure range<br />

� Controlled valves combined with ball valves<br />

Pump Heads Dimensions<br />

A<br />

mm<br />

B<br />

mm<br />

C<br />

Depth<br />

mm<br />

Process<br />

Connection<br />

mm<br />

Pneumatic<br />

Connection<br />

mm<br />

Type 1T 78 38 45 1,6/3,2 4<br />

Type 2T 88 48 55 3,2 4<br />

Type 4T <strong>10</strong>9 69 55 3,2 4<br />

Type 6T 160 120 75 6 4<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Pump Heads<br />

Pneumatic Pressure<br />

Supply<br />

Process Pressure<br />

Suction Lift(mWs)<br />

Delivery Height<br />

(mWs)<br />

Process Temperature<br />

(if necessary, heating<br />

module **)<br />

Max. Displaced<br />

Volume<br />

Head Size 1<br />

Head Size 2<br />

Head Size 4<br />

Head Size 6<br />

Max. Delivery Volume<br />

Head Size 1<br />

Head Size 2<br />

Head Size 4<br />

Head Size 6<br />

*) in flooded con<br />

**) Heating with Thermostat<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Type T Type S<br />

Type P Type V<br />

3 – 6 bar 3 – 6 bar 3 – 6 bar 3 – 6 bar<br />

4<br />

50<br />

4<br />

50<br />

4<br />

50<br />

< <strong>10</strong>0 °C < <strong>10</strong>0 °C < <strong>10</strong>0 °C<br />

40 µl<br />

500 µl<br />

1800 µl<br />

8000 µl<br />

<strong>10</strong>0 ml/h<br />

1800 ml/h<br />

4000 ml/h<br />

8000 ml/h<br />

upon request<br />

500 µl<br />

1800 µl<br />

upon request<br />

upon request<br />

2000 ml/h<br />

8000 ml/h<br />

upon request<br />

upon request<br />

250 µl<br />

900 µl<br />

upon request<br />

upon request<br />

250 µl<br />

900 µl<br />

upon request<br />

Operating mode Piston dosing pump with pneumatic gear<br />

Max. flow rate see table<br />

Dosing in vacuum Models with pressure-keeping and closing valve<br />

Stroke Frequency 0 - 180/min<br />

Stroke length variable 0 - <strong>10</strong>0%<br />

Suction Lift 5 m Ws<br />

Materials in contact with media PTFE/carbon/ceramic<br />

Media connection Tube/Pipe ID/OD = 4/6 mm<br />

Ambient temperature -<strong>10</strong> ... 45°C<br />

Control Voltage 4 ... 20 mA<br />

Power supply 230 V AC<br />

Display Strokes/min, after calibration l/h either<br />

Media compatibility Almost all chemicals<br />

Protection Category IP 65<br />

Ex-version No<br />

Order Code Description<br />

IP-P-N1-PK-mc Pump head pneumatic diaphragm dosing pump<br />

IP-P-N1-PK-STRG-E Autonomous control, pneumatic diaphragm dosing pump<br />

IP-P-N1-PK-STRG-VI Valve terminaldiaphragm dosing pump for binary activation<br />

mc = Model Code: T,S,P,V<br />

ec=electrical connection:<br />

T Tuchel connector LAB-PI<br />

O Open ends for MSR-PI<br />

<strong>10</strong> *)<br />

50<br />

upon request<br />

upon request<br />

upon request<br />

900 µl<br />

1500 µl<br />

upon request<br />

upon request<br />

2000 ml/h<br />

6000 ml/h<br />

Order example:<br />

Pneumatic diaphragm dosing pump Type P,<br />

autonomous control:<br />

Order Code: IP-P-N1-PK-mc und IP-P-N1-PK-STRG-E<br />

Automatic<br />

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286<br />

Magnetic dosing pump<br />

Magnetic dosing pumps are driven by an electric<br />

magnet. These generate a short and forceful dosing<br />

stroke. The dosing rate is controlled via the stroke<br />

frequency. The dosing stroke can additionally be<br />

adjusted manually.<br />

Magnetic membrane dosing pump<br />

Robust, calibratable membrane dosing pump with a<br />

magnetic drive for volumetric dosage or gravimetric<br />

dosage with a receiver on the balance in the control<br />

circuit.<br />

Technical data<br />

Operating mode Membrane dosing pump<br />

with magnetic gears<br />

Max. flow rate 1,1 l/h<br />

Max. discharge pressure 16 bar<br />

Dosing in vacuum Only with pressurised<br />

blocking valve<br />

Stroke frequency 0 - 180/min<br />

Stroke length variable 0 - <strong>10</strong>0%<br />

Suction height 5 m Ws<br />

Material in contact with PTFE/carbon/ceramic<br />

media<br />

Media connection Tube/pipe ID/OD = 4/6<br />

mm<br />

Ambient temperature -<strong>10</strong> to 45°C<br />

Activation 4 to 20 mA<br />

Power supply 230 V AC<br />

Display Strokes/min, after<br />

calibration also l/h<br />

Media compatibility Almost all chemicals<br />

Protection class IP 65<br />

Ex-version ---<br />

Order Code Description<br />

IP-P-M1-1<strong>10</strong>0M-<br />

PTFE/C/KER-SN4/6-ea<br />

ea=electrical connection:<br />

T Tuchel connector LAB-PI<br />

O Open ends for MSR-PI<br />

Order example:<br />

Magnetic membrane dosing pump, 1,1 l/h, 16 bar<br />

self-priming, Materials PTFE/Carbon/Ceramic, 180<br />

strokes/min, Activation 4 - 20mA, with 1 x 1,5m<br />

Cable for connection with a LAB-PI.<br />

Dosing Systems and Pumps<br />

Magnetic membrane dosing pump, 1.1 l/h, 16 bar self-priming, materials<br />

PTFE/carbon/ceramic, 180 strokes/min, Activation 4 - 20mA, with 1 x 1,5m cable for<br />

connection at a LAB- or MSR-PI (please indicate which one)<br />

Order Code: IP-P-M1-1<strong>10</strong>0-PTFE/C/KER-SN4/6-T<br />

On request deliverable:<br />

� PP,acrylic glass, stainless steel 1.4571<br />

� Dosing monitoring, self bleeding head for<br />

outgassing media<br />

� Other flowrate<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Magnetic piston dosing pump<br />

Robust, accurate piston dosing pump for liquids with<br />

a magnetic drive for precise, pressure-independent<br />

volumetric dosage. This pump is primarily suitable<br />

for precisely dosing small quantities.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Operating mode Piston dosing pump with magnetic gears<br />

Flow rate 0,06 ... 150 ml/h<br />

Max. discharge<br />

pressure<br />

40 bar<br />

Pressurised valve 2,5 bar<br />

Dosing in vacuum yes<br />

Stroke frequency 0 - 50/min<br />

Displace volume 1 - 50 μl, by micrometer button<br />

Stroke length variable 0 - <strong>10</strong>0%<br />

Suction Lift 6 m Ws<br />

Materials in contact with<br />

media<br />

PTFE/ceramic or stainless steel 1.4571/ceramic<br />

Media connection Capillaries da =1,75 mm or 1/16“ accords to 1,58 mm<br />

Ambient temperature 5 to 45°C<br />

Reproducibility better ± 0,5%<br />

Activation 4 - 20 mA<br />

Power supply 230 V AC<br />

Media compatibility Almost all chemicals<br />

Protection Category IP 65<br />

Ex-version Possible, on request<br />

Order Code Description<br />

IP-P-P1-0150M-PTFE/KER-SN17-ea Magnetic piston dosing pump, 0,06 - 150 ml/h, 40 bar self-priming, materials<br />

PTFE/Ceramic, 0 - 50 strokes/min, activation 4 - 20mA, with 1 x 1,5m cable for<br />

connection at a LAB- or MSR-PI (please indicate which one)<br />

IP-P-P1-0150M-VA/KER-SN16-ea Magnetic piston dosing pump, 0,06 - 150 ml/h, 40 bar self-priming, materials<br />

1.4571/ceramic, 0 - 50 strokes/min, activation 4 - 20mA, with 1 x 1,5m cable for<br />

connection at a LAB- or MSR-PI (please indicate which one)<br />

ma=media connection:<br />

SN17 Capillary screw connection OD =<br />

1,75mm, only in PTFE<br />

SN16 Capillary screw connection OD =<br />

1/16“ according 1,58mm, only in<br />

stainless steel<br />

ea=electrical connection:<br />

T Tuchel connector LAB-PI<br />

O Open ends for MSR-PI<br />

Order example:<br />

Magnetic piston dosing pump, 150 ml/h, 40 bar<br />

self-priming, materials stainless steel/ceramic, 0 -<br />

50 strokes/min, activation 4 - 20mA, with 1 x 1,5m<br />

cable for connection with a LAB-PI.<br />

Order Code: IP-P-K1-0150M-VA/KER-SN16-T<br />

available on request:<br />

� Ex-version<br />

� Greater discharge flows<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

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288<br />

Ex-Magnetic Membrane Dosing Pump<br />

Explosion-proof, robust membrane dosing pumps<br />

with a magnetic drive for volumetric dosage,<br />

gravimetric dosage with a receiver on a balance in a<br />

control circuit .<br />

The standard type, made of PTFE/carbon/ ceramic<br />

materials are particularly suitable for aqueous media<br />

with a certain electrical conductivity.<br />

When using flammable media we recommend the<br />

stainless steel model.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Operating mode Membrane dosing pump with magnetic gears<br />

Max. flow rate 1,0 l/h<br />

Max. discharge<br />

pressure<br />

16 bar<br />

Dosing in vacuum Only with pressurised blocking valve<br />

Stroke frequency 0 - 120/min<br />

Stroke length variable 0 - <strong>10</strong>0%<br />

Suction height 6 m Ws<br />

Materials in contact with<br />

media<br />

PTFE/carbon/ceramic<br />

Media connection Tube/Pipe6 x 4 mm<br />

Ambient temperature -<strong>10</strong> ... 45°C<br />

Activation 4 - 20 mA, input inherently safe „ia“<br />

Power supply 230 V AC<br />

Media compatibility Almost all chemicals<br />

Protection Category IP 65<br />

Ex-version EEx ia d IIC T6<br />

Order Code Description<br />

IP-P-M2-<strong>10</strong>00M-<br />

PTFE/C/KER-SN4/6-ea<br />

ma=media connection:<br />

SN4-6 Tube fitting I.D./OD 4/6mm<br />

ea=electrical connection:<br />

T Tuchel connector LAB-PI<br />

O Open ends for MSR-PI<br />

Ex-magnetic diaphragm dosing pump, 1,0 l/h, 16 bar self-priming, materials<br />

PTFE/carbon/ceramic, 120 strokes/min, activation 4 - 20mA, with 1 x 1,5m cable for<br />

connection at a LAB- or MSR-PI (please indicate which one)<br />

Order example:<br />

Ex-Magnetic membrane dosing pump, 1,0 l/h, 16 bar<br />

self-priming, materials PTFE/carbon/ceramic, 120<br />

strokes/min, activation 4 - 20mA, with 1 x 1,5m cable<br />

for connection at a LabManager.<br />

Order Code: IP-P-M2-<strong>10</strong>00M-PTFE/C/KER-SN4/6-T<br />

available on request:<br />

Materials:<br />

� PP,acrylic glass, stainless steel 1.4571<br />

� self-venting head for outgassing media<br />

� Model for higher viscosity<br />

� further discharge flows<br />

Notice: When using flammable media, use electrical<br />

grounding at stainless steel models and metal<br />

conductors, because of electrostatic discharge.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Dosing Systems and Pumps<br />

Precision Motor Membrane Dosing Pump<br />

Accurate membrane dosing pumps with positively<br />

controlled valves are used for precise dosing of<br />

gases and liquids. They can also dose small<br />

quantities of aggressive, abrasive, and viscous<br />

media. The inlets can be thermostatically heated and<br />

cooled. Stroke frequency and displaced volumes<br />

can be controlled separately.<br />

Due to the special construction (controlled cam<br />

valves, valve closing and opening during diaphragm<br />

standstill, through overlapping of the closing<br />

conditions no uncontrolled flow) this doser has an<br />

extremely high precision and repeat accuracy. It can<br />

convey into vacuum and convey out of vacuum.<br />

Through the forced drive of the valves, a secure<br />

valve function and a high impermeability is also<br />

achieved. This makes the reliable dosing of gases<br />

possible.<br />

Technical Data<br />

The dosing of gases should take place without<br />

pressure. Principally, the dosing with other pressure<br />

ratios is also possible. But the pressure difference<br />

range is limited due to the densification ratio. The<br />

flow rates must be calculated by calibration runs.<br />

Operating mode Motor diaphragm dosing pump with cam-controlled valves<br />

Flow rate 0 - 1800 ml/h<br />

Max. input compression 5 bar<br />

Max. pressure<br />

1 bar<br />

difference<br />

Dosing in vacuum Yes, till 0,001 mbar abs.<br />

Stroke frequency 0 - 60/min<br />

Displace volume <strong>10</strong> - 500 μl<br />

Suction Lift Self-priming, till 30 mbar abs. primary pressure<br />

Materials in contact with Post-compressed PTFE<br />

media<br />

Media connection PTFE, tube/plastic pipe I.D./OD = 4/6mm<br />

Media temperature up to <strong>10</strong>0 °C<br />

Activation serial connector RS232, 4-20 mA, 2-<strong>10</strong> V, single stroke control<br />

Power supply 230 V AC<br />

Power consumption 70 W<br />

Media compatibility Almost all chemicals<br />

Ex-version upon request<br />

Order Code Description<br />

IP-P-M3-1800M-PTFE-SN4/6 Precision motor diaphragm dosing pump, 36 - 1800 ml/h, 1 bar, materials PTFE, 0 - 60<br />

strokes/min, activation RS232<br />

ZK-P-TL02-BS-R2-I-01 RS232 Cable Sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />

ma=media connection:<br />

SN4-6 Tube fitting I.D./OD 4/6mm<br />

Order example:<br />

Precision motor diaphragm dosing pump, 36 - 1800<br />

ml/h, 1 bar, materials PTFE, 0 - 60 strokes/min,<br />

activation RS232, with 3m serial cable for<br />

connection at a LabBox or LabManager.<br />

Order Code: IP-P-M2-1800M-PTFE-SN4/6 and ZK-P-HZ01-<br />

BS-R2-I-01<br />

available on request:<br />

� Other flowrates<br />

� Heating and cooling of the pump head and feed<br />

lines<br />

� Vacuum applications<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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Automation<br />

Hardware<br />

Automation<br />

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Construction and<br />

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290<br />

Dosing Systems and Pumps<br />

High Pressure Double Piston Dosing Pump<br />

The high pressure double piston pump is made out<br />

of resistant materials and has a pulsations free flow.<br />

It is suited for dosing under high pressure in high<br />

pressure reactor systems and micro-reactor<br />

systems.<br />

Technical Data<br />

Operating mode Motor double piston pump for high pressure<br />

Max. flow rate 6 - 599,4 ml/h<br />

Max. discharge<br />

pressure<br />

500 bar<br />

Dosing in vacuum possible<br />

Materials in contact with<br />

media<br />

Stainless steel 1.4571, Aluminum oxide ceramic, carbon reinforced PTFE<br />

Media connection Capillary OD = 1/16“ equivalent 1,58mm<br />

Activation 0-<strong>10</strong> V DC, 2 x digital, RS232<br />

Power supply 230 V AC<br />

Media compatibility Almost all chemicals, besides chlorine-containing materials, hydrochloric acids<br />

Ex-version --<br />

Order Code Description<br />

IP-P-P3-0600M-VA/KER-<br />

SN16-ea<br />

ma=media connection:<br />

SN16 Screw connection for capillary 1/16“<br />

(1,58mm)<br />

ea=electrical connection:<br />

T Tuchel connector LAB-PI<br />

O Open ends for MSR-PI<br />

High pressure double piston dosing pump, 6 - 599,4 ml/h, 500 bar, materials 1.4571/ceramic,<br />

activation 0 - <strong>10</strong>V DC, 2 digital outputs with 3 x 1,5m cable for connection at a LAB- or MSR-<br />

PI, RS232<br />

Order example:<br />

High pressure double piston dosing pump, 6 - 599, 4<br />

ml/h, 500 bar, materials 1.4571/ceramic, activation 0<br />

- <strong>10</strong>V DC, 2 digital outputs with 3 x 1,5m cable with<br />

Tuchel plugs for connection to a LabManager<br />

Order Code : IP-P-K3-0600M-VA/KER-SN16-T<br />

available on request:<br />

� Increased discharge pressure up to 800 bar<br />

� Flow rates from <strong>10</strong> to <strong>10</strong>00ml/min<br />

� Other packing materials<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Eccentric screw pump<br />

Self-priming, pulsation free motor dosing pump for<br />

dosing and conveying for:<br />

� Media with different viscosities up to the pasty<br />

range<br />

� Suspensions, for instance sauces<br />

� abrasive suspensions, for instance soldering<br />

paste, polishing paste<br />

� Polymer, high viscous and crystal-containing preproducts,<br />

for example: lacquer, glue and melts<br />

� Viscous materials and granulated suspensions of<br />

the foods and pharmaceutical industry<br />

The pump is easy to disassemble and to clean.<br />

It is well suitable for speed regulated operations at a<br />

frequency converter.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Normally for connection at a LAB-PI an analogue<br />

output (LP-AAP8 or LP-AEAP), an passive digital<br />

output (LP-DAP8) for releasing and a digital input<br />

(LP-DEP8x) for the fault report are needed.<br />

Operating mode Eccentric screw pump with rotary current motor<br />

Flow rate 0 ... 24 l/h, depending on viscosity<br />

Max. discharge<br />

pressure<br />

12 bar<br />

Dosing in vacuum upon request<br />

Speed 0 ... <strong>10</strong>00 rpm, depending on viscosity<br />

Metered volume per rev. 0,40 ml<br />

Suction height Self-priming, media dependent<br />

Materials in contact with<br />

media<br />

Stainless steel 1.4571 hard chrome plated /perfluor rubber/PTFE<br />

Viscosity 1 ... 2.000.000 mPas<br />

Media connection Suction sided G ½“, pressure sided Rp ¼“, equivalent transitions available on<br />

request<br />

Media temperature up to 200 °C<br />

Metered accuracy Normally < ± 1%<br />

Control Frequency converter<br />

Power Input 0,25 kW<br />

Power supply 230 V AC<br />

Media compatibility Most chemicals beside chlorine-containing materials, hydrochloric acids<br />

Protection class IP 54<br />

Ex-version possible<br />

Order Code Description<br />

IP-P-E1-2700M-VA/FKM-ea Eccentric spiral pump with rotary current – asynchronous motor 0,25KW and frequency<br />

converter, 0-14 l/h, 12 bar, materials 1.4571 hard-chromium plated/fluorine rubber/PTFE, 0-<br />

<strong>10</strong>00 rpm, with cables to connect to a PI<br />

ea=electrical connection:<br />

T Tuchel connector LAB-PI<br />

O Open ends for MSR-PI<br />

Order example:<br />

Eccentric spiral pump with rotary current<br />

asynchronous motor 0,25KW und frequency<br />

converter, 0 - 24 l/h, 12 bar, materials 1.4571 hard<br />

chrome plated/fluorine rubber/PTFE, 0-<strong>10</strong>00 rpm,<br />

with cable for connection at a LabManager<br />

Order Code: IP-P-E1-2700M-VA/FKM-T<br />

available on request:<br />

� Other flowrate<br />

� Adjustable revolution gear<br />

Other materials:<br />

� Hastelloy<br />

� Pump head heating<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

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Technology<br />

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Toothed Ring Pumps<br />

Toothed ring pumps are suitable for pulsation poor<br />

conveyance and dosing of particle-free and not<br />

lubricating fluids of lower to high viscosity at low flow<br />

rates. They distinguish themselves by small dead<br />

storage and high dynamics.<br />

Low pressure pump<br />

Low pressure pumps distinguish themselves by a<br />

small construction volume and a favorable price. It<br />

makes pulsation free and highly precise conveying<br />

of small quantities, also not lubricating media<br />

possible.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Applications:<br />

� Small quantity dosage<br />

� Analysis technology<br />

� Biotechnology<br />

� Medical technology<br />

Operating mode Directly coupled toothed ring pump<br />

Flow rate 0,15 - 9 ml/min and 0,3 - 18 ml/min continuous<br />

Pulsation 1.5% and 6%<br />

Revolution <strong>10</strong>0 to 6000 rpm, DC motor, revolution load independent<br />

Max. discharge 0 ... 3 bar<br />

pressure<br />

Viscosity 0.5 ... 20mPas<br />

Dosing in vacuum conditional<br />

Suction Lift Self-priming up to low lift, media dependent<br />

Materials in contact with Hard metal (tungsten carbide), nickel bronze, PTFE<br />

media<br />

Media connection Tube nipple OD = 2 mm<br />

Media temperature 5 ... 50°C<br />

Activation 0-<strong>10</strong>V, (4-20mA, RS232 opt.)<br />

Revolution feedback 0-<strong>10</strong>V, (4-20mA, RS232 opt.)<br />

Power supply / 230 V AC, 50 W<br />

Performance<br />

Media compatibility Watery solutions, solvents, low viscous oil and lubricants<br />

Ex-version ---<br />

Order Code Description<br />

IP-P-R1-9M-HM-SN2-ea Micro toothed ring pump with controllable DC motor, 0.15 - 9 ml/min, max. pressure<br />

difference 3 bar, materials: hard metal/nickel bronze/PTFE, with cable for connection at a<br />

<strong>HiTec</strong> <strong>Zang</strong>-PI<br />

IP-P-R1-18M-HM-SN2-ea Micro tooth ring pumps with controllable DC motor, 0.3 - 18 ml/min, max. pressure<br />

difference 3 bar, materials hard metal/nickel bronze/PTFE, with cable for connection at a<br />

<strong>HiTec</strong> <strong>Zang</strong>-PI<br />

ea=electrical connection:<br />

T Tuchel connector LAB-PI<br />

O Open ends for MSR-PI<br />

Order example:<br />

Toothed ring pumps with controllable DC motor, 0.15<br />

- 9 ml/min, Max. pressure difference 3 bar, materials<br />

hard metal/nickel bronze/PTFE, cable with Tuchel<br />

connectors for connection at a LabManager.<br />

Order Code: IP-P-R1-9M-HM-SN2-T<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


High Performance Pump<br />

This high performance toothed ring pump<br />

distinguishes itself by good suction behaviour, less<br />

dead volumes, less pulsation and a very large<br />

viscosity range, and high dynamics.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Operating mode Direct coupled toothed ring pump<br />

Pulsation 6%<br />

Revolution <strong>10</strong>0 up to 6000 R/min, DC motor, Revolution load independent<br />

Viscosity 0.5 ... 50.000 mPas<br />

Dosing in vacuum conditional<br />

Suction Lift Self-priming, media dependent<br />

Material in contact with hard metal (tungsten-carbide), stainless steel 316L, PTFE<br />

media<br />

Media connection Screw fitting for 6/4mm plastic tube<br />

Media temperature 0 bis 50 °C (-126 bis –140°C upon request)<br />

Activation 0-<strong>10</strong>V, (4-20mA, RS232 opt.)<br />

Revolution feedback 0-<strong>10</strong>V, (4-20mA, RS232 opt.)<br />

Power supply / Leistung 230V AC, 50W<br />

Media compatibility Media compatibility Watery solutions, solvent, low viscous oil and lubricants<br />

Ex-version --<br />

For a safe operation a particle filter is required.<br />

Order Code Description<br />

IP-P-R2-18M-HM-SF1/8-ea High performance pump 0,003 - 18 ml/min, Delta-p max. 30 bar, max. 50.000 mPas<br />

IP-P-R2-72M-HM-SF1/8-ea High performance pump 0,012 – 72 ml/min, Delta-p max. 50 bar, max. 50.000 mPas<br />

IP-P-R2-288M-HM-SF1/8-ea High performance pump 0,048 – 288 ml/min, Delta-p max. 40 bar, max. 1.000.000 mPas<br />

IP-P-R2-<strong>10</strong>152M-HM-SF1/8-ea High performance pump 0,192 – 1.152 ml/min, Delta-p max. 00 bar, max. 150.000 mPas<br />

ea=electrical connection:<br />

T Tuchel connector LAB-PI<br />

O Open ends for MSR-PI<br />

Order example:<br />

Toothed ring pump with controllable DC motor, 0,3 -<br />

18 ml/min, max. pressure difference 30 bar,<br />

materials hard metal/stainless steel/PTFE, cable<br />

with Tuchel connectors for connection at a<br />

LabManager.<br />

Order Code: IP-P-R2-18M-HM-SF1/8-T<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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294<br />

Centrifugal Pumps<br />

Centrifugal Pump for High Pressure<br />

This magnet coupled centrifugal pump without shaft<br />

seal is particularly suitable for recirculation of heat<br />

carriers up to 350°C. The conveying of chemicals<br />

with higher temperature is also possible within the<br />

range of stability. It is also possible to provide<br />

systems and control vales with high flow<br />

resistances. Due to the complete separation of the<br />

media and drive, this pump is also very robust at<br />

extreme application conditions.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Operating mode Small magnet coupled centrifugal pump<br />

Delivery Rate water 840 l/h at 3 bar<br />

Max. flow rate 1800 l/h<br />

Max. pressure difference 5 bar<br />

Revolution 2800 rpm<br />

max. System pressure 25 bar<br />

Suction Lift No, influent<br />

Materials in contact with Stainless steel 1.4408, 1.4571, 1.4581<br />

media<br />

Particularly in multi reactor and parallel reactor<br />

systems with a joint thermostat control in mixing<br />

operations (large temperature changing rates,<br />

emergency cooling at exothermically reactions) the<br />

thermostat installed in the pump is often not<br />

sufficient. In this case, our pump is an appropriate<br />

solution.<br />

Media connection Internal thread G ½“<br />

Media temperature Up to 350 °C heat transfer oil, aqueous media up to 200°C possible<br />

Activation Over switching sockets (LP-DA230V2) or (HP-B230V8A)<br />

Power supply 230V AC 1 Ph, 0,5 kW. 400V AC 3 Ph possible<br />

Media compatibility Many chemicals, no chlorine-containing materials and hydrochloric acids.<br />

Protection Category IP 54<br />

Ex-version Possible, upon request<br />

Order Code Description<br />

IP-B-K1-1800L-VA-GMG1/2-ep Centrifugal pump, 0,5 kW, 2800 rpm at 50 Hz, up to 1800 l/h max. pressure difference 5<br />

bar, system pressure max. 25 bar, material stainless steel<br />

ep=<strong>Main</strong>s Power connection:<br />

230V 230V AC 1 Ph<br />

400V 400V AC 3 Ph<br />

Accessories for electrical connection of the pump<br />

like switching sockets (HP-B230V8A), protection etc.<br />

upon request.<br />

Order example:<br />

Centrifugal pump with three-phase asynchronous<br />

motor 0,5 kW,230V AC, 2800 rpm at 50 Hz, up to<br />

1800 l/h Max. pressure difference 5 bar, system<br />

pressure max. 25 bar, material: stainless steel.<br />

Order Code: IP-B-K1-1800L-VA-GMG1/2-400V<br />

We can offer you a complete spectrum of similar<br />

pumps for similar applications. Please contact us!<br />

available on request:<br />

� Other rotor material: PEEK<br />

� Controllable model with frequency converter<br />

� Model complete with frequency converter and<br />

difference pressure measuring for difference<br />

pressure control<br />

� Model with IDM measuring orifice plate for mass<br />

flow control<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Centrifugal Pump for Chemicals<br />

Magnet coupled chemical centrifugal pump without<br />

shaft seal for conveying and recirculation of pure<br />

and aggressive chemicals like acids, bases and<br />

solvents....<br />

Typical applications:<br />

� Extraction<br />

� Distillation in pilot plant, mini plant<br />

� Recirculation of baths: galvanic industry, photo<br />

industry...<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Usually, a digital output (LP-DAP8...) is required for<br />

start and stop at a LAB-PI. In individual cases a<br />

revolution controller (e.g. pressure difference<br />

controller) can be useful. In this case, an analogue<br />

output (LP-AAP8UI or LP-AEAP8I) for activation of a<br />

frequency converter will be needed.<br />

If needed, please additionally order the frequency<br />

converter.<br />

Operating mode Small magnet coupled centrifugal pump for chemical engineering<br />

Delivery Rate Water: 3000 l/h at 0,4 bar<br />

Max. flow rate 3900 l/h<br />

Max. pressure<br />

0,78 bar (7,8m discharge height, water)<br />

difference<br />

Revolution 2800 rpm<br />

max. Density 1300 kg/m³<br />

Suction Lift No, influent<br />

Material in contact with CFRETFE (Carbon fiber PE/PTFE-compound), silica carbide, FKM<br />

media<br />

Media connection External screw thread 1“<br />

Media temperature Up to 80°C<br />

Activation Over switching sockets (LP-DA230V2) or (HP-B230V8A)<br />

Power supply / 230V AC 1 Ph, 170W. three-phase current possible.<br />

Performance<br />

Media compatibility Media compatibility. Most chemicals, acids and bases.<br />

Ex-version Possible, upon request. Please inquire when using not conductive, flammable<br />

liquids because of the static charge.<br />

Order Code Description<br />

IP-B-K2-3900L-ETFE/SIC Chemical centrifugal pump with alternating current motor 170W, 230V AC, up to 3900 l/h Max.<br />

pressure difference max. 0,78 bar, materials CFRETFE/SiC/FKM<br />

We can offer you a complete spectrum of similar<br />

pumps for further applications. Please inquire.<br />

available on request:<br />

� Other flowrates and pressure difference<br />

� Other materials: PP...<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

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technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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296<br />

Reaction Proportioning Pumps<br />

Reaction proportioning pumps are especially suited<br />

for the production of nanoparticles and to test the<br />

reaction conditions for mixing or mass transfer tasks.<br />

The pumps dispose of peripheral wheel- typical<br />

pressure cells. In these, the liquid educt is<br />

compressed and flushed over the mixing rotor due to<br />

the generated turbulences. The subsequently<br />

generated circulation flows lead to especially<br />

homogenous and stable mixtures.<br />

Depending on the material, the mixers are<br />

chemically highly resistant and are able to handle<br />

system pressures up to 350 bar and temperatures of<br />

up to 450 °C.<br />

Reaction proportioning pumps are basically<br />

peripheral wheel pumps with several inlet nozzles<br />

for the fluid and gas feed.<br />

There is a separate inlet opening for each<br />

component in the diameter wall of the mixing<br />

chamber, the flow section of which is especially<br />

constructed according to the viscosity of the fluid,<br />

the projected mixing ratio or the expected reaction. A<br />

gaseous component can be fed into the mixing<br />

chamber between the inlet opening of the liquid<br />

component and the outlet/discharge opening of the<br />

mixture.<br />

Dosing Systems and Pumps<br />

Characteristics:<br />

� Robust and Safe<br />

� Simple Test Equipment<br />

� Safe test conditions, e.g. for phosgene<br />

transformation<br />

� Total volume is continuously regulable<br />

� Represents an alternative to stirred reactors or<br />

micro-mixers<br />

� Especially homogenous and stable mixtures due<br />

to intensive mixing<br />

In order to ensure a high chemical stability, the<br />

reaction mixers are constructed in Hasteloy, Tantal<br />

or silicon carbide for the part in contact with the<br />

products as well as with PTFE or Perfluorelastomer<br />

gaskets. Plastic linings with antistatic PTFE or PFA<br />

are also deployed. The drive of the mixer is magnetcoupled.<br />

In case of toxic or corrosive substances, it<br />

is possible to deploy double separating cans.<br />

The wear due to solid material content in the fluid,<br />

e.g. due to precipitation during a reaction, is<br />

countered with a suited selection of materials and<br />

design of the wheel, separating can and the shaft<br />

bearing. The separating can and the bearing, if<br />

necessary, can be flushed with a suited liquid.<br />

Depending on the respective reaction conditions, the<br />

chemical objectives, or the process-related basic<br />

conditions, special equipment is available for the<br />

reaction mixers.<br />

If exothermal o endothermal reactions are to be<br />

expected, the pumps can be equipped with heated<br />

or cooled pump heads. It is, for instance,<br />

subsequently possible to run a reaction isothermally<br />

or to prevent a melt from sulphuring. For this<br />

purpose, pump heads with a heating chamber or<br />

with a heatable separating can are available.<br />

When producing nanoparticles, the peripheral<br />

conveying system ensures fast mixing and a short<br />

holding time. As the nanoparticles are specifically<br />

produced in the reaction chamber, there is no<br />

increased risk of blockage or wear for the bearing or<br />

separating can.<br />

Due to the dosing pumps and the speed regulation,<br />

there is a high variance of possible test parameters.<br />

Order Code Description<br />

IP-B-REAKT1-4P Reaction Proportioning Pump, three inlets, one outlet, three phase motor<br />

IP-B-REAKT1-FU Frequency Converter for Reaction Proportioning Pump<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Dosing Systems and Pumps<br />

Multi-Channel Dosing Systems<br />

Flexible gravimetric dosing systems can be realised<br />

by combining the accordingly suited components.<br />

Here are just a few of the possible combinations:<br />

� Four-fold Dosing System with GraviDos<br />

LabBox1with GraviDos weighing card and 4<br />

magnetic valves or PFM-controlled pumps ,<br />

HiBuilder custom software for dosing profiles and<br />

simple records and protocoling.<br />

Options:<br />

Special cable for the connection of the dosing<br />

pumps to 4..20mA digital outputs (PWM), further<br />

RS232 interfaces for connection of dosing<br />

pumps.<br />

� Four-fold Dosing System with Laboratory<br />

Scales:<br />

LabBox1 with 4 RS232 interfaces for laboratory<br />

scales and 8 digital outputs for connection of the<br />

magnetic valves or PFM-controlled pumps,<br />

HiBuilder custom software for dosing profiles and<br />

simple records and protocoling.<br />

� Four-fold Dosing System with Notebook<br />

acting as Control Unit:<br />

Notebook, USB to RS232 Converter, four-fold<br />

DMS-Card RS232, 4 GraviDos modules, 4<br />

LabDos with RS232-Bus, HiBuilder custom<br />

software for dosing profiles and simple records<br />

and protocoling.<br />

� Mehrfachdosiersystem mit SyrDos<br />

Spritzendosierer<br />

Notebook, USB an RS232 Converter, LabBox1,<br />

2 SyrDos Systeme, DosiMaster Spezialsoftware<br />

für Dosierprofile und einfache Aufzeichnung u.<br />

Protokollierung.<br />

Options:<br />

Special cable for the connection of the dosing<br />

pumps to 4..20mA digital output (PWM), further<br />

RS232 interfaces for connection of LabDos and<br />

other dosing pumps.<br />

Custom Design, mobile 4-fold Dosing Station<br />

Kundenspezifisch gefertigte SyrDos-Dosierstationen<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

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Construction and<br />

Technology<br />

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298<br />

Vacuum pumps<br />

Membrane vacuum pump<br />

Dry running vacuum pump for neutral, highly<br />

aggressive and corrosives gases and vapours.<br />

Applications:<br />

� Evacuate in a raw vacuum range with or without<br />

cryo trap<br />

� Rotary evaporator<br />

� Evacuation of dehydrator<br />

� Substitute of water jet pumps<br />

� Discharge of process gases<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Operating mode Two phase membrane vacuum pump for the chemistry<br />

Suction capacity 1200 l/h<br />

Final vacuum 8 mbar abs.<br />

Media affecting PTFE/FFKM<br />

materials<br />

For the connection at a LAB-PI a digital output (LP-<br />

DAP8) and a switching sockets (HP-B230V8A) or a<br />

digital output 230V (LP-DA230V2) are needed.<br />

Media connection Tube nipple for vacuum tube I.D. = 6mm, OD = <strong>10</strong>mm<br />

Activation Over switching sockets (LP-DA230V2) or (HP-B230V8A)<br />

Power supply / Leistung 230V AC 1 Ph, 120W<br />

Current consumption 0,7A<br />

Media compatibility Almost all chemicals, gases and vapours<br />

Ex-version ---<br />

Order Code Description<br />

IP-B-V1-1200L-PTFE/FPM Chemical vacuum pump with alternating current motor 120W, 230V AC, 1200 l/h, final vacuum<br />

8 mbar, materials PTFE/FFKM<br />

On request deliverable:<br />

� Other flowrate<br />

� Final vacuum 2 ... <strong>10</strong>0 mbar<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Two phase rotary valve vacuum<br />

pump<br />

Two phase oil sealed rotary valve membrane pump<br />

for generating fine vacuum.<br />

Applications:<br />

� Evacuating of small up to middle reactor systems<br />

up to the higher fine vacuum range<br />

� Lyophilization / freeze drying<br />

� Vacuum distillation<br />

By condensing aggressive media a cryo trap shall<br />

be provided.<br />

For the connection at a LAB-PI a digital output (LP-<br />

DAP8) and a switching sockets (HP-B230V8A) or a<br />

digital output 230V (LP-DA230V2) are needed.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

Operating mode Two phase oil sealed rotary valve vacuum pump<br />

Suction capacity 5600 l/h<br />

End partial pressure or<br />

gas ballast<br />

4 x <strong>10</strong>-4 mbar abs.<br />

End total pressure or.<br />

Gas ballast<br />

2 x <strong>10</strong>-3 mbar abs.<br />

End partial pressure<br />

with gas ballast<br />

6 x <strong>10</strong>-3 mbar abs.<br />

Media connection Tube nipple for vacuum tube I.D. = 6mm or clamped flange DN <strong>10</strong><br />

Activation Over switching sockets (LP-DA230V2) or (HP-B230V8A)<br />

Power supply /<br />

Performance<br />

230V AC 1 Ph, 0,30kW<br />

Media compatibility Neutral gases, low quantities condensing and corroding vapors, apply cryo trap<br />

Ex-version ---<br />

Order Code Description<br />

IP-B-V2-5600L-SN6 Two phase rotary vacuum pump with alternating current motor 0,30kW, 230V AC, 5600 l/h,<br />

final vacuum 2 x <strong>10</strong>-3 mbar abs.<br />

On request deliverable:<br />

� Other flowrate<br />

� One-level version<br />

� Hybrid pump with better compatibility for<br />

aggressive vapors<br />

Automatic<br />

Laboratory<br />

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300<br />

Vacuum Pump Stand<br />

These laboratory vacuum systems are equipped<br />

with a controller. The control of the pressure is<br />

distinguished by a connection, respectively<br />

disconnection of the diaphragm pump. It is possible<br />

to suppress the connection of the pump motor a<br />

selective setting of the pressure rise rate or through<br />

an active Teach-Function. This means, that the<br />

system will only activate if a potential load is<br />

connected.<br />

Advantages<br />

� equipped with a vacuum controller, chemical<br />

resistant diaphragm pump with control<br />

� Vacuum control through revolution control<br />

� Consistent operational readiness<br />

� reduced operational costs<br />

� increased service life and longer maintenance<br />

intervals of the diaphragm pump<br />

� simple programming of the controller, directly<br />

or via PC<br />

� Storage of all program and measurement<br />

values possible<br />

Laboratory vacuum systems offer you an automatic<br />

cost-effective operation without additional charge.<br />

You do not need to supervise the operation of the<br />

pump. The integrated intelligent vacuum controller<br />

economically controls the revolutions of the pump. A<br />

suction-side separator ensures the protection of the<br />

vacuum pump by retaining particles and liquid<br />

droplets.<br />

Technical Data<br />

Dosing Systems and Pumps<br />

The pressure-side emission condenser ensures nonpolluting<br />

operation by regaining and collecting<br />

solvent remains.<br />

All components in contact with gas are made of top<br />

quality, chemically resistant materials. This even<br />

enables the evacuation of acids and solvent<br />

vapours. All glass parts are coated with a<br />

transparent shatter protection coating which<br />

preserves visibility of the processes. The coolers are<br />

insulated.<br />

Operating mode Chemical-resistant diaphragm pump, separator<br />

Suction capacity 2,2 / 4,9 / 9,1 m³/h<br />

Final Pressure or gas<br />

ballast<br />

< 2 mbar<br />

Media connection DN16KF-1/4 inch / DN16KF-1/4 inch / DN25KF-1/4 Zoll<br />

Activation RS232<br />

Power supply 230V AC<br />

Media compatibility Neutral gases, small quantities of condensing and corroding vapors<br />

Ex-version No<br />

For the connection to a LAB-PI, a RS232 cable is required.<br />

Order Code Description<br />

IP-B-VPS-mc Vacuum pump stand with chemical-resistant diaphragm pump and separator<br />

ZK-P-VB01-BS-R2-I-01 Rs232 cable for IP-B-VPS-mc<br />

mc=Model Code:<br />

Model Final Suction<br />

Code vacuum capacity<br />

2-2.2 < 2 mbar 2,2 m³/h<br />

2-4.0 < 2 mbar 4,9 m³/h<br />

2-9.1 < 2 mbar 9,1 m³/h<br />

Other delivery rates and final pressures are available on request.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Solid Matter Dosing System<br />

Dosing Systems and Pumps<br />

Load Lock Conveying System for Powders, Granulates, Crystalls....<br />

Fields of application<br />

The SoliDos solid matter<br />

dosing system is suitable<br />

for the dosing of powdery<br />

and granular solid matters.<br />

For the laboratory<br />

technician, the manual<br />

adding of solid educts at<br />

specific times, or the adjustment<br />

of the pH-value<br />

through solid matter addition<br />

are a time-consuming<br />

matter.<br />

With SoliDos You can<br />

now automate these operation<br />

steps. SoliDos is<br />

also suitable at best for<br />

the automatic seeding<br />

procedure of crystallization<br />

processes.<br />

Thanks to its especially<br />

slim design, SoliDos ideally<br />

fits into the reactor<br />

installation.<br />

� Dosing of solid matter<br />

� pH-adjustment with solid matter<br />

� Seeding of crystallization processes<br />

SoliDos can be run through a specific control device<br />

or directly through a PFM (pulse frequency module)<br />

modulated digital output of the LabManager.<br />

SoliDos can also be run through an optionally<br />

available, separate control device.<br />

The dosing rate can be adjusted via the rotation<br />

speed and the volume of the lock chamber.<br />

Optionally, a nitrogen flushing connection and a side<br />

refilling nozzle can be provided.<br />

SoliDos is built out of resistant materials. The<br />

standard model is made of borosilicate glass,<br />

stainless steel, and POM. Alternatively the material<br />

PTFE is available.<br />

Technical Data<br />

Diameter: approx. 70 mm<br />

Length: approx. 330 mm<br />

Connection: NS29/32<br />

Weight approx. 1300 g<br />

Dosage amount max. 200 ccm<br />

For assembly, the SoliDos is directly mounted on to<br />

a NS 29/32 standard grinding socket. The dosing<br />

matter, also during the running operation, can be<br />

refilled manually or automatically through the lateral<br />

refill-socket by a mounted storage container. A<br />

rinsing/flushing connection for inert gas is provided<br />

between the lock chamber and the socket.<br />

Advantages<br />

� Resistant to most chemicals<br />

� Suitable for powder and granular materialdosing<br />

� Large range for the dosing rate<br />

� Novel mechanics prevents fusing and dome<br />

formation<br />

� Minimum floor space required, very simple<br />

installation<br />

� Can be completely dismounted for cleaning<br />

� Combination with GraviDos gravimetric<br />

dosing is possible<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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302<br />

Versions<br />

Dosing Systems and Pumps<br />

Version (SoliDos2 - x ) -12 -25 -50 -<strong>10</strong>0 -200 -400<br />

Dosing rate approx. [ccm/min] 12 25 50 <strong>10</strong>0 200 400<br />

Dosed amount (per pulse) approx. [ccm] 0,12 0,25 0,50 1 2 4<br />

Max. dosing amount: 200 ccm, unlimited by refilling through the side nozzle<br />

Delivery Scope Doser with 1,5 m connection cable for active digital output of a LabManager<br />

or-box-PI, respectively Stand-Alone-control unit<br />

Order Code Description<br />

IL-SOLIDOS2-x Solid dosing basis device for LAB-PI<br />

IL-SOLIDOS2-x-ST Solid dosing basis device for stand-alone device<br />

IL-SOLIDOS2-SK-x SoliDos dosage valve<br />

IL-SOLIDOS2-HEIZ Electrical heating element for heating of the socket to prevent condensation<br />

IL-SOLIDOS2-KF Cold trap to prevent condensation in socket, NS29/32<br />

x=version according to table-12 to -400<br />

SoliDos Options<br />

An inert gas is pressed through the drive casing via<br />

the inerting connection on the drive casing in order<br />

to protect the drive from aggressive gases and to<br />

keep the dosing matter dry.<br />

Order Code Description<br />

IL-SOLIDOS1IN Inerting Connection for SoliDos solid doser on the drive<br />

Adapter for GraviDos for gravimetric dosing.<br />

Order Code Description<br />

IL-SOLIDOSADGD SoliDos/GraviDos adapter for gravimetric dosing<br />

Special designs and adapters for reactor nozzles are available on request.<br />

Screw Conveyor<br />

The SoliDos-s conveys powdery and granulate-like<br />

solids out of a storage container. A knocking mechanism<br />

prevents possible stowage in the screw.<br />

The SoliDos is available as vacuum and pressureresistant<br />

(-<strong>10</strong>00 up to 300 mbar) version.<br />

Special designs are available on request.<br />

The devices are available as client-specific custom<br />

designs in various sizes. The length of the screw, in<br />

Size 1, can be up to 500 mm.<br />

Technical Data<br />

Volumen 500 ml<br />

Dimensions without 300x300x400 mm<br />

Screw<br />

max. Length of Screw 500 mm<br />

Diameter of Screw <strong>10</strong> mm<br />

Weight approx. 2000 g<br />

Max. Dosing Rate 1 ccm/min<br />

Other dosing rates available on request.<br />

Required as PI-interfaces are:<br />

2 digital outputs<br />

Content of<br />

delivery<br />

Order Code Description<br />

IL-SOLIDOS-SF-V-1 SoliDos screw conveyor 500ml, volumetric<br />

Doser with 1,5 m connection<br />

cable for active digital outputs of a<br />

LabManager or -box-PI.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Gravimetric Solid Doser<br />

The SoliDos-s screw conveyor can be completed as<br />

gravimetric dosing unit. In the course of this, the<br />

weight reduction is registered by a precision<br />

scales.<br />

Dosing Systems and Pumps<br />

Technical Data<br />

Volume 500 ml<br />

Dimensions 300x300x400 mm<br />

max. Length of Screw: 500 mm<br />

Diameter of Screw: <strong>10</strong> mm<br />

Weight approx. 3500 g<br />

Max. Dosing Rate 1 ccm/min<br />

approx.<br />

Order Code Description<br />

IL-SoliDos-SF-G-1 Gravimetric solid doser with SoliDos screw conveyor Size 1<br />

Gravimetric frictional filler<br />

Max. Dosing Fault ±<strong>10</strong> mg<br />

Required as PI-interfaces are:<br />

2 digital outputs and one RS232 interface for the<br />

scales.<br />

Other dosing rates available on request.<br />

Delivery Scope Doser with 1,5 m connection<br />

cable for active digital outputs of a<br />

LabManager or -box-PI.<br />

The SoliDos-td frictional filler is suitable for precise<br />

dosing of solid matters.<br />

Technical data<br />

Volume 1500 ml<br />

Dimension Höhe: 600mm<br />

Durchmesser: 180 mm<br />

Materials metallfreie Ausführung in PP,<br />

optional Edelstahlausführung<br />

Weight (approx.) 4500 g<br />

Max. dosing rate 220 ccm/min<br />

Max. dosing rate 5 ccm/min<br />

As PI-interfaces are needed:<br />

Digital output (DAP8T) at the Lab/MSR-PI or<br />

GraviDos dosing control.<br />

Other dosing rates upon request.<br />

We also construct custom made systems.<br />

Delivery Scope Doser with 1,5 m connection<br />

cable for active digital outputs of a<br />

LabManager or -box-PI.<br />

Order Code Description<br />

IL-SOLIDOS-TD-V-1 frictional filler 1, volumetric<br />

IL-SOLIDOS-TD-G-1 frictional filler 1, gravimetric<br />

IL-SOLIDOS-TD-G SoliDos control device for standalone operation (combinable with IL-SOLIDOS-TD-G-1)<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Dispersing<br />

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304<br />

Dosing Systems and Pumps<br />

SoliDos - Control Device for Stand-Alone Operation<br />

The SoliDos control device offers the best<br />

functionality for the operation of the SoliDos solid<br />

doser.<br />

The device can both be controlled via the keypad<br />

and the serial (optional) or analogue interface. As it<br />

disposes of 5 dosing modes, this compact device<br />

can also be deployed everywhere without automation<br />

system.<br />

Dosing mode<br />

The SoliDos supports five Dosing modes, that can<br />

be selected from the parameter menu. The setpoint<br />

values can either be entered manually via the<br />

keypad or analogue determined via the analogue<br />

interface or serially via the RS232 interface.<br />

Delivery Scope Control device and manual.<br />

rp : pulse rate<br />

In the mode rp, a pulserate is predetermined. As<br />

soon as the SoliDos is started, it doses with the set<br />

pulse rate.e.g. 1 dosing stroke.<br />

rw: weight rate<br />

In the mode rw, a weight rate in g is predetermined.<br />

The weight rate operation mode requires a<br />

calibration run.<br />

sp: pulse sum<br />

In the mode sp, a pulse sum is predetermined. As<br />

soon as the SoliDos is started, it doses with the<br />

adjusted pulse rate until the adjusted pulse number<br />

is reached.<br />

sw: weight sum<br />

In the mode sw, a weight sum in g is predetermined.<br />

Exactly like in the mode rw, a calibration run of<br />

the appliance is necessary. As soon as the SoliDos<br />

is started, it commences dosing with the preset<br />

weight rate until the set weight sum is reached.<br />

p: single pulse<br />

In the mode p, the SoliDos can be driven in single<br />

step operation. If the UP button is actuated, a single<br />

dosing stroke will be triggered.<br />

Order Code Description<br />

IL-SOLIDOSST1 SoliDos control device for standalone operation (combinable with IL-SOLIDOS2-X-ST)<br />

IL-SOLIDOS-RS Option RS232 interface<br />

ZK-IT-HI01-BS-R2-I-03 RS232 Cable sub-D9/Sub-D9, 3 m, for connection to LAB- or MSR-PI or PC<br />

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Here you will find:<br />

Liquid Handling and Autosampler<br />

� Sampling Systems and Pipetting Robots<br />

� AutoSam Sample Collector and Sample Dispensers<br />

� LiquiDos Peristaltic Pump<br />

� SyrDos Syringe Doser<br />

� LiquidMaster Control Software<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 305<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


306<br />

Liquid Handling and Autosampler<br />

Sample Drawing Systems and Pipetting Robots<br />

24 Hour Reactor Sampling<br />

AutoSam is a fully automatic sample handling<br />

system with varied application possibilities. The<br />

robust construction enables deployment in rough<br />

plant environment.<br />

Applications<br />

� Bottling of Samples<br />

� Provision of reactants<br />

� Quenching, Mixing, Diluting<br />

� Derivatising with several Reactants<br />

� Liquid/Liquid Extraction<br />

� Creation of Backup samples<br />

In connection with an automation device or a control<br />

PC with the LiquiMaster control software, it is<br />

possible to realise any procedures time or processcontrolled<br />

according to specification of test period,<br />

time etc.<br />

Flexibility:<br />

� For Batch and Continuous Processes<br />

� For Upstream and Downstream Processes<br />

� Fully adequate Liquid Handling System<br />

� Optional interfaces for magnetic valves,<br />

pumps and switches for automation devices<br />

� Optional Stirring and Tempering Function<br />

� Interfaces for process automation<br />

Occurring sample waste and rinsing solutions are<br />

collected in a separate waste container. Due to the<br />

utilisation of inert materials and freely programmable<br />

rinsing cycles is eliminated and sterility ensured in<br />

bioprocesses.<br />

The AutoSam can be deployed as sample dispenser,<br />

respectively as a multicomponent collector, as the<br />

needle can be lowered right down to the bottle base.<br />

The precise control allows selective liquid/liquid<br />

phase separation through siphoning off to phase<br />

limit level.<br />

Optionally, it is possible to assemble digital inputs<br />

and outputs to switch external valves or pumps or to<br />

query monitors for filling level, pressure, etc. This<br />

enables easy realisation of liquid handling systems.<br />

Bottles with septa can be used as sample vessels.<br />

Vessels (e.g. 1.5 and 2ml-E-Caps) sealed with<br />

plastic covers or thin membranes are suited. By<br />

exchanging the sample tray, it is possible to switch<br />

to different vessel sizes.<br />

AutoSam300 as a fully integrated Process Component<br />

The AutoSam is connected to the <strong>HiTec</strong> <strong>Zang</strong><br />

LabManager or any other control system via serial<br />

interface. The control is easily conducted via HiText-<br />

Program or HiBatch basis operations. This ensures<br />

uncomplicated integration into the <strong>HiTec</strong> <strong>Zang</strong> LUIit<br />

and MultiLab systems.<br />

The module IL-AUTOSAM-SA enables an optional<br />

connection of an internal 2/3 way valve or an<br />

external pump a stand-alone sampling without<br />

external control device.<br />

The parameters sample amount, intervall and filling<br />

time can be set via the AutoSam control panel.<br />

For stand-alone application, the „LiquiMaster“<br />

Software is available, which enables table or scriptbased<br />

schedule control for AutoSam with two/threeway<br />

valve in combination with our peristaltic and<br />

syringe pumps.<br />

The sample tray can be exchanged by merely lifting<br />

the old one and fitting the new one.<br />

The devices are automatically able to identify an<br />

exchange of the sample tray and the number of<br />

sample positions of the sample tray.<br />

We advise to order the devices with at least two<br />

sample trays in order to prevent the necessity to<br />

individually change the sample bottles.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Liquid Handling and Autosampler<br />

As a component of the LabVision/LabManager<br />

laboratory automation, the control and protocoling<br />

can be arranged flexibly:<br />

� Process and time controlled methods<br />

� Control of the sample tray position and the<br />

injection needle<br />

� Simple integration into the plant and recipe<br />

control<br />

� Free programmable handling methods<br />

� Free programmable rinsing cycles and needle<br />

rinsing programs<br />

� Data exchange with existing LIMS-systems is<br />

possible<br />

� Protocoling in the laboratory journal and LIMS, as<br />

sample ticket etc.<br />

We also manufacture customer-specific sample tray<br />

for any sample vessels.<br />

Properties and Functions:<br />

� Materials in contact with media are made of<br />

PTFE or PVDF and glass<br />

� Vessel with septum seal are also reliably<br />

processed<br />

� Bottling under inert gas is possible<br />

� Exchangeable sample tray<br />

� Separate, big waste container<br />

� Control via serial RS232 interface, optional<br />

RS485 with ModBus or CanBus protocol, USB,<br />

Ethernet or SPS I/O<br />

� sample collector, fraction collector,<br />

multicomponent dispenser<br />

� Multicomponent mixer, phase separator<br />

� Fully automated sample handling<br />

� Options: magnetic stirrer, tempering system,<br />

tandem needle system<br />

Tandem Assembly Double Needle with Fixture<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

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Stirring and<br />

Dispersing<br />

Services


308<br />

AutoSam300<br />

Liquid Handling and Autosampler<br />

The AutoSam 300 is the basic device of the<br />

AutoSam type series. It is chargeable with sample<br />

tray for sample bottles reaching from 2 ml to <strong>10</strong>0 ml<br />

and, if necessary, fits well into a cooling incubator.<br />

At the zero position of the sample tray, the needle is<br />

able to deliver into the waste. At the rear panel of the<br />

device, there is a tube connection used for<br />

connection to the waste container (waste).<br />

With the control panel, it is possible to<br />

� move to zero position<br />

� move to next position<br />

� move needle downwards<br />

� move needle upwards<br />

� open/close valve<br />

� control stirrer rpm<br />

� exchange sample tray manually.<br />

The LC-Display presents<br />

� position of the sample tray<br />

� position of the needle<br />

� etc.<br />

Technical Data<br />

Sample tray Speed Max. 5 Rev/min.<br />

Reproducibility x-pos. ±1 mm<br />

Traverse Path Needle Drive 80 mm<br />

Power Needle Drive <strong>10</strong> N<br />

Reproducibility y-pos. ±0,1 mm<br />

Dimensions WxDxH 31x41x46 cm<br />

Diameter Sample tray 30 cm<br />

Protection Category IP20<br />

Bottle Size ml Diameter mm Number of Septum Type<br />

Bottles possible<br />

2 12,0 49 (+1) yes AutoSam300-T-12-50<br />

5 a. 8 17,2 31 (+1) yes AutoSam300-T-17-32<br />

<strong>10</strong> a. 20 23,0 24 (+1) yes AutoSam300-T-23-25<br />

50 46,0 14 (+1) yes AutoSam300-T-46-15<br />

50 30,2 22 (+1) yes AutoSam300-T-30-23<br />

<strong>10</strong>0 56,0 <strong>10</strong> (+1) yes AutoSam300-T-56-11<br />

Note: (+1) means the usually assigned waste position.<br />

Order Code Description<br />

IL-AUTOSAM300 Automatic sampler for 300mm sample tray with sample bottles reaching from 2 to <strong>10</strong>0 ml<br />

IL-AUTOSAM300-T-12-50 AutoSam300 sample tray for 50 pieces 2ml, D = 12mm sample bottles<br />

IL-AUTOSAM300-T-17-32 AutoSam300 sample tray for 32 pieces 5 and 8 ml, D = 17,2mm sample bottles<br />

IL-AUTOSAM300-T-23-25 AutoSam300 sample tray for 25 pieces <strong>10</strong> and 20ml, D = 23 mm sample bottles<br />

IL-AUTOSAM300-T-46-15 AutoSam300 sample tray for 15 pieces 50ml, D = 46mm sample bottles<br />

IL-AUTOSAM300-T-30-23 AutoSam300 sample tray for 23 pieces 50ml, D = 30,2mm sample bottles<br />

IL-AUTOSAM300-T-56-11 AutoSam300 sample tray for 11 pieces <strong>10</strong>0ml, D = 56mm sample bottles<br />

You will find further auxiliary modules at the end of the chapter.<br />

Other bottle sizes are available upon request.<br />

The casings can be made of satin or polished high-grade steel.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


AutoSam360<br />

Liquid Handling and Autosampler<br />

The AutoSam 360 is chargeable with sample trays<br />

for sample bottles reaching from 2 ml to <strong>10</strong>0 ml.<br />

At the zero position of the sample tray, the needle is<br />

able to deliver into the waste. At the rear panel of the<br />

device, there is a tube connection leading for<br />

connection to the waste container..<br />

With the operator buttons, it is also possible to<br />

� move to zero position<br />

� move to next position<br />

� move needle downwards<br />

� move needle upwards<br />

� open/close valve<br />

� control stirrer rpm<br />

� exchange sample tray manually.<br />

The LC-Display presents<br />

� position of the sample tray<br />

� position of the needle<br />

� etc.<br />

Technical Data<br />

Sample tray Speed Max. 5 Rev/min.<br />

Reproducibility x-pos. ±1 mm<br />

Traverse Path Needle Drive 80 mm<br />

Power Needle Drive <strong>10</strong> N<br />

Reproducibility y-pos. ±0,1 mm<br />

Dimensions WxDxH 31x47x46 cm<br />

Diameter Sample tray 36 cm<br />

Protection Category IP20<br />

Bottle Size ml Diameter mm Number of Septum Type<br />

Bottles possible<br />

2 12,0 79 (+1) yes AutoSam360-T-12-80<br />

5 a. 8 17,2 48 (+1) yes AutoSam360-T-17-49<br />

<strong>10</strong> a. 20 23,0 40 (+1) yes AutoSam360-T-23-41<br />

50 46,0 17 (+1) yes AutoSam360-T-46-18<br />

<strong>10</strong>0 56,0 14 (+1) yes AutoSam360-T-56-15<br />

Note: (+1) means the usually assigned waste position.<br />

Order Code Description<br />

IL-AUTOSAM360 Automatic sampler for 360mm sample tray with sample bottles reaching from 2 to <strong>10</strong>0 ml<br />

IL-AUTOSAM360-T-12-80 AutoSam360 sample tray for 80 pieces 2ml, D = 12mm sample bottles<br />

IL-AUTOSAM360-T-17-49 AutoSam360 sample tray for 49 pieces 5 and 8 ml, D = 17.2mm sample bottles<br />

IL-AUTOSAM360-T-23-41 AutoSam360 sample tray for 41 pieces <strong>10</strong> and 20ml, D = 23mm sample bottles<br />

IL-AUTOSAM360-T-46-18 AutoSam360 sample tray for 18 pieces 50ml, D = 46mm sample bottles<br />

IL-AUTOSAM360-T-56-15 AutoSam360 sample tray for 15 pieces <strong>10</strong>0ml, D = 56mm sample bottles<br />

You will find further auxiliary modules at the end of the chapter.<br />

Other bottle sizes are available upon request.<br />

The casings can be made of satin or polished high-grade steel.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

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Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


3<strong>10</strong><br />

AutoSam495<br />

Liquid Handling and Autosampler<br />

The device is chargeable with 495 mm sample trays<br />

for sample bottles reaching from 2 ml to <strong>10</strong>0 ml.<br />

At the zero position of the sample tray, the needle is<br />

able to deliver into the waste. At the rear panel of the<br />

device, there is a tube connection leading for<br />

connection to the waste container (waste).<br />

With the operator buttons, it is also possible to<br />

� move to zero position<br />

� move to next position<br />

� move needle downwards<br />

� move needle upwards<br />

� open/close valve<br />

� control stirrer rpm<br />

� exchange sample tray manually.<br />

The LC-Display presents<br />

� Position of the Sample tray<br />

� Position of the Needle<br />

� etc.<br />

Technical Data<br />

Sample tray Speed Max. 5 Rev/min.<br />

Reproducibility x-pos. ±1 mm<br />

Traverse Path Needle Drive 80 mm<br />

Power Needle Drive <strong>10</strong> N<br />

Reproducibility y-pos. ±0,1 mm<br />

Dimensions WxDxH 31x57x40 cm<br />

Diameter Sample tray 49,5 cm<br />

Protection Category IP20<br />

Bottle Size ml Diameter mm Number of Septum Type<br />

Bottles possible<br />

5 and 8 17,2 59 (+1) yes AutoSam495-T-17-60<br />

12 and 15 19,0 59 (+1) yes AutoSam495-T-19-60<br />

<strong>10</strong> 23,0 49 (+1) yes AutoSam495-T-23-50<br />

25 28,0 39 (+1) yes AutoSam495-T-28-40<br />

2 12,0 2x 49 (+1) yes AutoSam495-T-12-<strong>10</strong>0<br />

5 15,2 2x 49 (+1) yes AutoSam495-T-15-<strong>10</strong>0<br />

Order Code Description<br />

IL-AUTOSAM495 Automatic sampler for 495mm sample tray with sample bottles reaching from 2 to <strong>10</strong>0 ml<br />

IL-AUTOSAM495-T-17-60 AutoSam495 sample tray for 60 pieces 5 and 8 ml, D = 17.2mm sample bottles<br />

IL-AUTOSAM495-T-19-60 AutoSam495 sample tray for 60 pieces 12 and 15ml, D = 19mm sample bottles<br />

IL-AUTOSAM495-T-23-50 AutoSam495 sample tray for 50 pieces <strong>10</strong>ml, D = 23mm sample bottles<br />

IL-AUTOSAM495-T-28-40 AutoSam495 sample tray for 40 pieces 25ml, D = 28mm sample bottles<br />

IL-AUTOSAM495-T-12-<strong>10</strong>0 AutoSam495 Tandem sample tray for 2x50 pieces 2ml, D = 12mm sample bottles<br />

IL-AUTOSAM495-T-15-<strong>10</strong>0 AutoSam495 Tandem sample tray for 2x50 pieces 5ml, D = 15.2 mm sample bottles<br />

Other bottle sizes are available upon request.<br />

You will find accessories and further options under Auxiliary Components for Liquid Handling<br />

The casings can be made of satin or polished high-grade steel.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


AutoSam200<br />

Liquid Handling and Autosampler<br />

The AutoSam 200 is constructed very compact and<br />

is particularly suited for application within<br />

biotechnology. The sample tray can accommodate<br />

up to 24 standard 1.5 ml or 2.0 ml sample vessels.<br />

With the control panel, it is possible to<br />

� move to zero position<br />

� move to next position<br />

� move needle downwards<br />

� move needle upwards<br />

� open/close valve<br />

� control stirrer rpm<br />

� exchange sample tray manually.<br />

The LC-Display presents<br />

� Position of the Sample tray<br />

� Position of the Needle<br />

� etc.<br />

Technical Data<br />

Sample tray Speed Max. 5 Rev/min.<br />

Reproducibility x-pos. ±1 mm<br />

Traverse Path Needle Drive 80 mm<br />

Power Needle Drive <strong>10</strong> N<br />

Reproducibility y-pos. ±0.1 mm<br />

Dimensions WxDxH 20x25x46 cm<br />

Diameter Sample tray 16 cm<br />

Protection Category IP20<br />

Bottle Size<br />

ml<br />

Number of<br />

Samples<br />

Septum possible<br />

1.5 (E-caps) 24 yes<br />

2 (E-caps) 24 yes<br />

Order Code Description<br />

IL-AUTOSAM200 Automatic Sampler for 200mm sample tray<br />

IL-AUTOSAM200-T-11-32 Automatic Sampler for 32 pieces 1.5 or 2 ml D = 11mm sample bottles and E-caps<br />

Other bottle sizes are available upon request.<br />

You will find accessories and further options under Auxiliary Components for Liquid Handling<br />

The casings can be made of satin or polished high-grade steel.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 311<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


312<br />

Accessories, Options<br />

2/3-Way Valve<br />

Liquid Handling and Autosampler<br />

This 2/3 way valve for AutoSam sample collectors is<br />

mounted on the needle sliding carriage.<br />

The needle is directly attached at the valve fitting so<br />

that there is no tube between needle and valve. This<br />

leads to minimum dead volume and accordingly<br />

minimal flushing losses.<br />

For activation, the valve requires one of the three<br />

possible digital switching outputs.<br />

Material in contact with media: PTFE. Other<br />

materials are available upon request.<br />

Tube diameter 3 to 3.2 mm.<br />

Order Code Description<br />

IL-AUTOSAM-MB-2-3-P 2/3- way valve with needle holder wetted parts made of PTFE, steam-sterilisable<br />

IL-AUTOSAM-MB-2-3-K 2/3- way valve with needle holder wetted parts made of KEL-F steam-sterilisable<br />

IL-AUTOSAM-DA24 Digital switching output, 24V, 0.5 A<br />

Other bottle materials are available upon request.<br />

Multi-way valves can be found under Equipment and Components, Multi-way valves.<br />

Magnetic Stirrer Drive<br />

Beneath the needle position, a magnetic stirrer drive can be integrated in order to be able to drive magnetic<br />

stir bars in the sample bottles without contact.<br />

Order Code Description<br />

IL-AUTOSAM-R Magnetic stirrer drive for AutoSam<br />

IL-AUTOSAM-RF-d-l Magnetic stir bars for sample bottles, Teflon outer cover, 1VPE=<strong>10</strong> pieces<br />

d-l = Dimensions of the magnetic stir bar<br />

d-l: 3-6 6-<strong>10</strong> 6-15<br />

Diameter/mm 3 6 6<br />

Length/mm 6 <strong>10</strong> 15<br />

Tandem Equipment<br />

At devices and trays with tandem equipment there<br />

are always two sample bottles at every position<br />

which can be separately filled, respectively emptied.<br />

Out of the first vessel, e.g. an reactant can be<br />

provided whilst a product sample is filled into the<br />

second vessel.<br />

The needles always move in parallel.<br />

Order Code Description<br />

IL-AUTOSAM-TAN Tandem Equipment, Double Bottle Line<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Contact Guard<br />

Liquid Handling and Autosampler<br />

The contact guard prevents unintentional contact<br />

with the needle point.<br />

It is made of transparent Plexiglas and does not<br />

influence vision.<br />

Order Code Description<br />

IL-AUTOSAM-BSCHU Contact guard for needle<br />

Cooling Incubator<br />

The devices of the type series AutoSam200, 300,<br />

and 360 fit into the cooling incubator. The required<br />

electrical and fluidic connections are passed<br />

outwards through the rear panel. The cooling<br />

incubator is assembled ready for connection for<br />

AutoSam sample collector.<br />

� Glass Door<br />

� High-Grade Steel Casing<br />

� Interior Lighting<br />

� Ready to install connections for AutoSam devices<br />

Please note: Not all devices fit into the cooling<br />

incubator. In case of the AutoSam360, the plugs on<br />

the side panels and the waste connection must be<br />

relocated into the base tray.<br />

Technical Data<br />

Temperature Range 0 to +15 °C<br />

Interior Dimensions W x H x D 52 x 70 x 44 cm<br />

Exterior Dimensions W x H x D 60 x 85 x 60 cm<br />

Interior Material Plastic (silver), grids are zinc-trayd<br />

Order Code Description<br />

IL-AUTOSAM-KL Cooling Incubator for AutoSam Sample Collector<br />

Consumable Material<br />

Order Code Description<br />

IL-AUTOSAM-EN-6-x Needles for AutoSam, inside diam.= 0.6mm, outside diam.= 1.0mm 1VPE = 6 pieces<br />

IL-AUTOSAM-DN-6-x-x AutoSam double needle for venting and gassing function 1VPE = 6 pieces<br />

x = Needle length. The standard length for single needles is 50mm (x = 50). In case of double needles, the<br />

transport needle is 50mm, the venting needle is 25mm long (x-x = 50-25). Please request for other lengths.<br />

Custom designs are possible. Other inside and outside diameters on request.<br />

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314<br />

Stand-alone use<br />

Liquid Handling and Autosampler<br />

The module IL-AUTOSAM-SA enables an optional<br />

connection of an internal 2/3 way valve or an<br />

external pump a stand-alone sampling without<br />

external control device.<br />

Order Code Description<br />

IL-AutoSam-SA AutoSam module for stand-alone sample taking<br />

Miscellaneous Options<br />

The parameters sample amount, intervall and filling<br />

time can be set via the AutoSam control panel.<br />

Order Code Description<br />

IL-AUTOSAM-SA AutoSam module for stand-alone sample taking<br />

IL-AUTOSAM-SPPS SPS Interface for AutoSam, control via 4 binary signals<br />

IL-AUTOSAM-DA24 Digital switching output, 24V, 0.5 A (maximum number 3 pieces)<br />

IL-AUTOSAM-FEACON Feature Connector 2 inputs 5-24V, 2 inputs 5V with internal Pull-up resistor , 5V<strong>10</strong>0mA<br />

IL-AUTOSAM-RS485 Bus-compatible RS485-Interface for AutoSam<br />

IL-AUTOSAM-TVERL Extension of the tower, e.g. in case bottles are higher than 70mm<br />

IL-AUTOSAM-B-DN Connecting element for double needle<br />

IL-AUTOSAM-WASBO Passing of the waste connection into the base tray<br />

IL-AUTOSAM-STLI Relocation of the plugs to the left casing side<br />

IL-AUTOSAM-STRE Relocation of the plugs to the right casing side<br />

IL-AUTOSAM-POLI Casing made of polished high-grade steel<br />

Further Options are available upon request. The devices are also available in the OEM version.<br />

Additional Components for Liquid Handling<br />

Liquid Handling applications are laborious and timeconsuming,<br />

if conducted manually. With the<br />

AutoSam liquid handlers, it is possible to realise<br />

liquid handling processes efficiently and precisely<br />

and consequently significantly reduce the amount of<br />

work.<br />

AutoSam Liquid handlers are flexibly deployable<br />

and, next to the precise and fast bottling of samples,<br />

enable applications such as:<br />

� Dispensing<br />

� Multiple Dispensing<br />

� Diluting and<br />

� Pipetting.<br />

Due to the possibility to control the processes with<br />

HiText, it is also possible to realise complex systems<br />

with integrated sensor systems and integration into<br />

plant automation etc. A liquid handling system<br />

consists of an AutoSam, an electrical pump unit, a<br />

LabBox/manager system, and further optional<br />

peripheral equipment. As pumps, the LiquiDos and<br />

LabDos peristaltic pumps or the SyrDos syringe<br />

pump with 2/3 way valve are particularly suited.<br />

Single and double needles with inerting and venting<br />

connections are available as feeding needles.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


LiquiDos Peristaltic Pump<br />

Liquid Handling and Autosampler<br />

Pump/valve unit for liquid handling applications, in<br />

particular within the biotechnological sector.<br />

The LiquiDos pump can be applied to realise sterile<br />

systems (tubes are auto clavable).<br />

Technical Data<br />

Tube Diameter interior 0.25 to 2.06 mm<br />

Wall Thickness 0.85 mm<br />

Maximum Delivery Rate 20 ml/min<br />

Maximum Delivery Pressure 2 (1.5 at Di = 2mm) bar<br />

Control RS232 Interface V24<br />

LiquiDos Precision Dosing Pump with integrated 2/3-way Valve<br />

(tube squeeze valve)<br />

Order Code Description<br />

IL-LIQUIDOS1 Pump unit with 2/3 way valve for Liquid-Handling with AutoSam, Control: RS232, with 3 m<br />

serial cable for connection to LAB- or MSR-PI<br />

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316<br />

Liquid Handling and Autosampler<br />

LiquiMaster Control Software<br />

The LiquiMaster Software is intended for the<br />

realisation of stand-alone liquid handling<br />

applications with AutoSam devices.<br />

With the LiquidMaster, it is possible to realise<br />

spreadsheet or script-based schedule control for<br />

AutoSam with 2/3 -way valve in combination with<br />

our LabDos and LiquiDos peristaltic pumps and the<br />

SyrDos syringe pumps.<br />

LiquiMaster can control the sampling optionally by<br />

the integrated 2/3 way valve or/and with a LabDos<br />

peristaltic pump.<br />

Timings for valves and pumps, the pumpheads<br />

rotational speed and delivery volume as well as the<br />

cleaing time/volume can be parameterised.<br />

Sampling times will be managed be the timetable<br />

element.<br />

The programm creates a protocol of all executed<br />

sampling.<br />

With the ight version (SL-LIQUIML) an AutoSam can<br />

be used for standard samplings.<br />

The LiquiMaster full version uses the additional<br />

freely programmable HiText syntax, with which<br />

additional valves and pumps can be controlled and<br />

sensors can be integrated.<br />

The optional AutoSam feature.connector (IL-<br />

AUTOSAM-FEACON) enables the connection of two<br />

additional valves and two binary sensors at the<br />

AutoSam. With the RS232 interface additional<br />

sensors and devices can be integrated.<br />

The possibilities<br />

� Control of the position of the sample tray and the<br />

injection needle<br />

� Control of the 2/3-way valve and one pump<br />

� Free programmable rinsing cycles and needle<br />

rinsing programs<br />

� Protocoling as sample tickets etc.<br />

� Data exchange with existing LIMS systems<br />

The software is based on HiBuilder and can be<br />

extended with much ease for instance to<br />

send/receive data to/from a LIMS.<br />

It is a Microsoft Windows based software that runs<br />

on a LabCommander - Mini-Terminal.<br />

LabCommander - Mini-Terminal<br />

The LabCommander mini-terminal enables to space<br />

saving realisation of dosing-, dispering and mixing<br />

stations on the laboratory bench.<br />

Order Code Description<br />

SL-LIQUIM LiquidMaster Software for spreadsheet supported and freely programmable liquid handling<br />

SL-LIQUIML LiquiMaster Software light, for spreadsheet supported liquid handling<br />

CG-LABCOMMANDER LabCommander Mini-terminal for laboratory devices<br />

<strong>HiTec</strong> <strong>Zang</strong> also establishes ready-to-use sampling and liquid handling systems according to your<br />

specifications!<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Type Series AutoSam xl<br />

Liquid Handling and Autosampler<br />

The type series AutoSam xl is suited for the bottling<br />

of the total reactor content into containers up to 2<br />

litres. The permanently mounted high-grade steel<br />

nozzle moves to a waste position when in wait state,<br />

so that dripping rests can be directly disposed and<br />

can not cause spoilage.<br />

Bottle Size ml Number Septum Type<br />

of Bottles possible<br />

2000 8 yes AutoSam2000-8<br />

<strong>10</strong>00 12 yes AutoSam<strong>10</strong>00-12<br />

500 14 yes AutoSam500-14<br />

Technical Data<br />

Sample tray Speed max. 6 Rev/min<br />

Reproducibility x-pos. ±3 mm<br />

Traverse path needle drive approx. 80 mm<br />

Power Needle Drive approx. <strong>10</strong>0 N<br />

Reproducibility y-pos. ±3 mm<br />

Dimensions WxDxH 70x90x80 cm<br />

Order Code Description<br />

IL-AUTOSAM-XL-2000-8 Automatic Sampler for 8 x 2000ml sample bottles<br />

IL-AUTOSAM-XL-<strong>10</strong>00-12 Automatic Sampler for 12 x <strong>10</strong>00ml sample bottles<br />

IL-AUTOSAM-XL-500-14 Automatic Sampler for 14 x 500ml sample bottles<br />

Other bottles are available upon request.<br />

You can find accessories under Additional Components for Liquid Handling.<br />

XY-Pipetting Robots<br />

This pipetting robot is suited for „Liquid Handling“ of<br />

a greater number of samples. The control is easily<br />

conducted via HiText.<br />

Samples can be filled in containers, substances can<br />

be dosed out of containers, and substances can be<br />

filled from one container into another container.<br />

Optionally, sensors, e.g. pH sensors, can be moved<br />

from container to container and submerged for<br />

measuring.<br />

� For filling, sampling and pipetting<br />

� Container height up to 200 mm<br />

� RS232 Interface for <strong>HiTec</strong> UI<br />

Product Description Pipetting robot with serial interface for connection to the UI (workstation). Is<br />

assigned to one serial interface of the UI.<br />

Delivery Scope Pipetting robot with PI driver, cable, and manual.<br />

Order-Code Description<br />

IL-PIPET1 Pipetting Robot with serial interface, with cable and PI driver<br />

As pumps, the LiquiDos and SyrDos pumps are particularly suited.<br />

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Liquid Handling and Autosampler<br />

SciLab Laboratory Robot<br />

<strong>HiTec</strong> <strong>Zang</strong> manufactures the SciLab Laboratory<br />

Robot exactly to the specifications of your special<br />

application. As the devices are smoothly integrated<br />

into the <strong>HiTec</strong> <strong>Zang</strong> Automation Environment, the<br />

coupling with online analytics is possible. Therefore,<br />

the prerequisite for the realisation of automated<br />

intelligent experiments is established.<br />

Features and Functions<br />

� Flexible Liquid Handling Platform<br />

� Optional sterilisable (24h at 90°C)<br />

� Integratable additional Sensor 'Technology<br />

� Integratable additional Actuators<br />

� Simple Integration in Up and Downstream<br />

Applications<br />

Typical Applications<br />

� Up Stream Processing<br />

� Down Stream Processing<br />

� Screening<br />

� Liquid Handling<br />

� Formulations<br />

� Cell Cultures in Microtitration Plates<br />

Example 1: Robot for Cell Culture<br />

Features and Functions<br />

� Sterilisable(24h at 90°C)<br />

� Compact Construction, Incubator Operation<br />

� Detection of Liquid Surfaces<br />

� Simultaneous Handling also of Microtitration<br />

Plates of different Formats<br />

Example 2: Robot for Formulation<br />

Special Features<br />

Product Description XYZ-Pipetting Robot with serial Interface<br />

Delivery Scope Robot with Cable and Manual<br />

� Blending out of up to 12 Components<br />

� Individual Stirring Functions for all Positions<br />

� Integrated gravimetric liquefied Material Dosing<br />

Order Code Description<br />

IL-SCIBOT-x Customer-specific XYZ-Robot<br />

IL-SCIBOTBIB Software Library for HiText and HiBuilder for Liquid Handling and Pipetting Tasks<br />

x: Specification according to functional requirements.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Here you will find:<br />

� ViscoPakt ® Torque Measuring Stirrer Drive<br />

Stirring and Dispersing<br />

� ViscoTrol Control Module for Three Phase Stirrer Drive<br />

� Stirring Accessories (Stirring Blades, Lead-Throughs, Magnetic Couplings....)<br />

� Drives and Tools for Dispersing and Homogenisation<br />

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320<br />

Stirring and Dispersing<br />

Measuring Stirrer ViscoPakt ®<br />

The Visco-Pakt measuring stirrer is a strong stirring<br />

an torque measuring system with speed regulation<br />

and state-of-the-art torque measurement sensitivity.<br />

Fields of Application<br />

� System stirrer for automatic laboratory reactor<br />

� Identification of reaction phases<br />

� Detection of stirrer dissipation in the reaction<br />

calorimeter<br />

� Measurement of rheological material properties<br />

� Scale-up experiments<br />

� Process monitoring<br />

The drive unit requires only a fraction of the space<br />

needed by usual measuring stirrers, allowing more<br />

valuable space for the reactor head. Due to its<br />

compact construction, it also fits into a small<br />

apparatus, e.g. a 250 mL reactor system. The small<br />

dimensions of the drive were achieved by separating<br />

the stirrer from its control unit. The separate<br />

controller has a keypad and an LC display, which<br />

shows the torque and rotational speed.<br />

The measured torque is automatically corrected<br />

using the speed dependent “zero torque”.<br />

In many applications, ViscoPakt delivers important<br />

additional information. For polymerization and polycondensation,<br />

the initiation or completion of a<br />

reaction, which cause a change in the viscosity, can<br />

be read off and identified via the torque.<br />

The power dissipated from stirring, which is of<br />

interest for reaction calorimetry, can be determined<br />

from the torque and speed of rotation.<br />

As the design has no gearing, an extraordinarily<br />

large range of torque can be continuously achieved<br />

with no switching.<br />

Glass stirrers are protected from breaking by softstart<br />

and torque limiters.<br />

Characteristics and Functions<br />

� Powerful and compact<br />

� High measuring precision<br />

� High measuring sensitivity<br />

� Robust measurement technique<br />

� Measurement of rotational speed and torque<br />

� Wide and continuous range of rotational<br />

speeds<br />

� Smooth start-up, adjustable gradient<br />

� Automatic correction of the zero torque<br />

� Adjustable soft-start ramp<br />

� Adjustable rotational speed and torque<br />

limitation<br />

� Quick catch chuck<br />

� Low noise operation<br />

ViscoPakt rheo was developed for applications for<br />

which the exact torque, viscosity, or the dissipated<br />

energy and a precise keeping of the rotational speed<br />

are needed.<br />

The measurement sensitivity is impressive.<br />

Viscosity variations in the order of the viscosity of<br />

water are still resolved.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


ViscoPakt ®<br />

The standard design is equipped with a simple<br />

torque output which reflects the viscosity's trends.<br />

Variations of the rotational speeds due to load<br />

fluctuations are electronically compensated.<br />

Technical data<br />

Stirring and Dispersing<br />

ViscoPakt model - 27 - 57 - 1<strong>10</strong> Unit<br />

Maximum torque 27 57 1<strong>10</strong> Ncm<br />

Resolution 0,07 0,1 0,2 Ncm<br />

Reproducibility 1,5 3 5 Ncm<br />

Minimum speed 150 150 150 rpm<br />

Maximum speed 2200 2000 2000 rpm<br />

Speed uncertainty 2 1,5 1,5 %<br />

Chuck size 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> mm<br />

Type of protection<br />

controlling device<br />

20 20 20 IP<br />

Type of protection<br />

drive<br />

51 51 51 IP<br />

Approx. Weight 2 3 4 kg<br />

Motor Diameter 55 70 83 mm<br />

Length across axis<br />

(approx.)<br />

2<strong>10</strong> 230 270 mm<br />

Extension<br />

diameter/length<br />

16 / 220 16 / 220 16 / 220 mm<br />

Max. viscosity <strong>10</strong>.000 40.000 70.000 mPas<br />

Max. Mixing quantity<br />

(H2O)**<br />

15 30 50 Liter<br />

* Control Unit /Drive<br />

** Reference values for propeller stirrer in H2O<br />

Interfaces<br />

Analogue:<br />

Required rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />

Actual rotational speed (= required value or 0) 0 - <strong>10</strong> V, 0/4-20mA<br />

Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />

The setpoint rotational speed can be pre-set via an<br />

analogue input or the serial interface. The torque<br />

and the setpoint rotational speed are issued via the<br />

analogue outputs and the serial interface.<br />

RS232:<br />

Send: Setpoint rotational speed<br />

Received: Setpoint rotational speed, actual torque value<br />

Delivery Scope Measuring-stirrer drive and control unit with 2.3 m cable<br />

Order Code Description Specifications<br />

IR-VIPA27 ViscoPakt-27 27 Ncm<br />

IR-VIPA57 ViscoPakt-57 57 Ncm<br />

IR-VIPA1<strong>10</strong> ViscoPakt-1<strong>10</strong> 1<strong>10</strong> Ncm<br />

IR-VIPARS Optional RS232 Interface Setpoint rotational speed and actual torque<br />

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322<br />

ViscoPakt ® -rheo<br />

The ViscoPakt-Rheo model series is equipped with<br />

precision-torque measuring. The zero torque, which<br />

depends on the rotational speed, is registered by an<br />

automatic calibration process and is used to correct<br />

the actual torque signal. This allows the on-line<br />

determination of the viscosity (via a calibration table)<br />

as well as of other rheological parameters.<br />

Technical Data<br />

Stirring and Dispersing<br />

ViscoPakt Model rheo - X7 - 16 - 27 - 57 -1<strong>10</strong> Unit<br />

Maximum torque 7 16 27 57 1<strong>10</strong> Ncm<br />

Resolution 0.003 0.01 0.02 0.04 0.08 Ncm<br />

Reproducibility 0.05 0.1 0.2 0.4 0.8 Ncm<br />

Minimum speed 40 40 40 40 40 rpm<br />

Maximum speed 3000 2200 2200 2000 2000 rpm<br />

Speed uncertainty 0.1 0.1 0.1 0.1 0.1 %<br />

Chuck size 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> mm<br />

Type of protection<br />

controlling device<br />

20 20 20 20 20 IP<br />

Type of protection<br />

drive<br />

54 54 54 54 54 IP<br />

Approx. Weight 0.9 1.7 2.6 3.9 6 kg<br />

Motor Diameter 70 45 55 70 83 mm<br />

Length above axis<br />

(approx.)<br />

250 245 250 255 295 mm<br />

Extension<br />

diameter/length<br />

16/220 16/220 16/220 16/220 16/220 mm<br />

Max. viscosity 5,000 6,000 <strong>10</strong>,000 40,000 70,000 mPas<br />

Max. Mixing quantity<br />

(H2O)**<br />

2 8 15 30 50 Litres<br />

* Control Unit /Drive<br />

** Reference values for propeller stirrer in H2O*<br />

Interfaces<br />

Analogue:<br />

Required rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />

Actual rotational speed (= required value or 0) 0 - <strong>10</strong> V, 0/4-20mA<br />

Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />

Changes to the rotational speed which are caused<br />

by load fluctuations are registered by a digital<br />

revolution counter and are electronically regulated.<br />

The rotational speed can be pre-set via an analogue<br />

input or the serial interface. The actual rotational<br />

speed and the torque are issued via the analogue<br />

outputs and the serial interface.<br />

RS232:<br />

Send: Required rotational speed<br />

Received: Required rotational speed, actual rotational speed, actual torque value<br />

Delivery Scope Measuring-stirrer drive and control unit with 2.3 m cable<br />

Order Code Description Specifications<br />

IR-VIPARHX7 ViscoPakt-Rheo-X7 7 Ncm<br />

IR-VIPARH16 ViscoPakt-Rheo-16 16 Ncm<br />

IR-VIPARH27 ViscoPakt-Rheo-27 27 Ncm<br />

IR-VIPARH57 ViscoPakt-Rheo-57 57 Ncm<br />

IR-VIPARH1<strong>10</strong> ViscoPakt-Rheo-1<strong>10</strong> 1<strong>10</strong> Ncm<br />

IR-VIPARS Option RS232 Interface Setpoint and actual rotational speed and<br />

actual torque<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


ViscoPakt ® -rheo+<br />

The model series ViscoPakt-Rheo+ is based on<br />

most modern brushless drives. Consequently, they<br />

are absolutely maintenance-free and the friction<br />

moment caused by the brush is no longer existent at<br />

precision torque measurements. The speeddependant<br />

zero torque is captured in the course of<br />

an automatic calibration procedure and utilised for<br />

the correction of the torque signal. Herewith, it is<br />

Technical Data<br />

Stirring and Dispersing<br />

Type ViscoPakt-rheo+ -40 -75 -150 -220 Einheit<br />

Maximum torque 40 75 150 220 Ncm<br />

Resolution 0,01 0,03 0,04 0,05 Ncm<br />

Reproducibility 0,1 0,2 0,3 0,4 Ncm<br />

Minimum speed 40 40 40 40 rpm<br />

Maximum speed 2200 2000 2000 2000 rpm<br />

Speed uncertainty 0,01 0,01 0,01 0,01 %<br />

Chuck size 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> 1 - <strong>10</strong> mm<br />

Type of protection 20 20 20 20 IP<br />

controlling device<br />

Type of protection drive 54 54 54 54 IP<br />

Approx. Weight 1,5 2,5 3,5 5 kg<br />

Motor Diameter 43 87 87 87 mm<br />

Length above axis 200 180 180 2<strong>10</strong> mm<br />

(approx.)<br />

Extension diameter/length <strong>10</strong> / 200 13 / 200 13 / 200 13 / 200 mm<br />

Max. viscosity <strong>10</strong>.000 40.000 70.000 70.000 mPas<br />

Max. Mixing quantity** 15 40 60 80 Liter<br />

* Steuergerät/Antrieb<br />

** Richtwerte für Propellerrührer in H2O<br />

Schnittstellen<br />

RS232, RS485 interface with Modbus Protocol (opt.)<br />

Send: Rotational speed desired value<br />

Receive: Rotational desired/actual value, torque actual value<br />

Analogue:<br />

Required rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />

Actual rotational speed (= required value or 0) 0 - <strong>10</strong> V, 0/4-20mA<br />

Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />

possible to establish the viscosity (per calibration<br />

table) and other rheological parameters online.<br />

Speed changes caused by load variations are<br />

captured by a digital speed sensor and electronically<br />

compensated. The speed can be predefined via an<br />

analogue input or the serial interface. The actual<br />

speed and the torque are issued via analogue<br />

outputs and the serial interface.<br />

Delivery Scope Measuring-stirrer drive and control unit with 2.3 m cable<br />

Bestellcode Beschreibung<br />

IR-VIPARHP40 ViscoPakt-Rheo+-40 precision-stirrer actuator, 40 Ncm<br />

IR-VIPARHP75 ViscoPakt-Rheo+-75 precision-stirrer actuator, 75 Ncm<br />

IR-VIPARHP150 ViscoPakt-Rheo+-150 precision-stirrer actuator, 150 Ncm<br />

IR-VIPARHP220 ViscoPakt-Rheo+-220 precision-stirrer actuator, 220 Ncm<br />

IR-VIPARHPRS485 Option RS485 ModBus Interface<br />

IR-VIPARHPUI Option Current and voltrage interface<br />

Automatic<br />

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324<br />

ViscoPakt ® -mini-rheo-35<br />

Stirring and Dispersing<br />

The ViscoPakt-mini is a<br />

precision measuring stirrer<br />

disposing of an especially<br />

compact design. It is<br />

deployed where torques<br />

must be generated in most<br />

limited spaces. These are<br />

mainly small reactors with a<br />

nominal volume below 500<br />

ml with many mounted<br />

sockets at the same time,<br />

as such are frequently<br />

deployed for parallel<br />

syntheses.<br />

The ViscoPakt-mini,<br />

amongst other utilisations,<br />

is deployed in our LabKit<br />

and MultiLab parallel<br />

reactor systems.<br />

Interfaces<br />

Analogue:<br />

Order Code Description<br />

IR-VIPA-MINI-RHEO-35 ViscoPakt-mini-rheo stirrer drive, 35 Ncm<br />

Ministirrer<br />

The MiniStirrer is the economic<br />

alternative to the ViscoPakt-mini<br />

with a lower maximum torque<br />

and simple torque measurement<br />

(current measurement).<br />

It can be deployed everywhere<br />

where a qualitative torque signal<br />

is sufficient and relatively lowviscous<br />

substances are stirred.<br />

Order Code Description<br />

IR-MINISTIRR<strong>10</strong> Mini-stirrer-<strong>10</strong> stirrer drive<br />

<strong>HiTec</strong>-<strong>Zang</strong> naturally also offers all necessary<br />

accessories, e.g. flexible stirrer shafts, stirrer shaft<br />

protection, special stirrer receptacles, and also a<br />

wide array of mixing elements made of glass, high-<br />

Setpoint rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />

Actual rotational speed (=<br />

setpoint value or 0)<br />

0 - <strong>10</strong> V, 0/4-20mA<br />

Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />

RS232:<br />

Send: Setpoint rotational speed<br />

Received: Setpoint rotational speed, actual<br />

rotational speed, actual torque value<br />

ViscoPakt Type mini-rheo-35 Unit<br />

Maximum torque 35 Ncm<br />

Resolution 0.01 Ncm<br />

Reproducibility 0.1 Ncm<br />

Minimum speed 15 rpm<br />

Maximum speed 800 rpm<br />

Diameter 45 mm<br />

Length across axis 230 mm<br />

Interfaces<br />

Analogue:<br />

Setpoint rotational speed 0 - <strong>10</strong> V, 0/4-20mA<br />

Actual rotational speed (=<br />

Setpoint value or 0)<br />

0 - <strong>10</strong> V, 0/4-20mA<br />

Actual torque value 0 - <strong>10</strong> V, 0/4-20mA<br />

ViscoPakt Type Mini-strirrer-<strong>10</strong> Unit<br />

Maximum torque 17 Ncm<br />

Resolution 0.07 Ncm<br />

Reproducibility 0.5 Ncm<br />

Minimum speed 60 rpm<br />

Maximum speed 1900 rpm<br />

Diameter 50 mm<br />

Length across axis 195<br />

*only current measurement!<br />

mm<br />

grade steel PTFE and other materials. Our experts<br />

will gladly help you to arrange the mixing elements<br />

and stirrers that exactly accord to your requirements.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Stirring and Dispersing<br />

ViscoTrol Control Unit for Three-Phase Stirrer Drive<br />

The ViscoTrol control units enable an electronically<br />

controlled variation of the rotational speed of three<br />

phase stirrer drives and the electronic collection of<br />

the torque. Due to this, adjustable gear units and<br />

and measuring shafts are no longer necessary.<br />

The standard ViscoTrol family meets simple<br />

requirements in regard to precision.<br />

Higher demands to precision are met by the<br />

ViscoTrol rheo family.<br />

Due to unsufficiant cooling when in low rpm mode it<br />

is recommended to adjust the motor via the set point<br />

of the control device or adding an additional cooler.<br />

ViscoTrol<br />

The control units dispose of a Start-Stop switch and<br />

a setpoint potentiometer for manual operation.<br />

Interfaces:<br />

Analogue Interfaces: 4...20mA, E = setpoint<br />

rotational speed,<br />

A = Torque and actual rotational speed<br />

RS485 interface with Modbus Protocol<br />

Digital Release<br />

Notice<br />

A MODBUS interface requires the option<br />

PNKMODBUS and a free RS485 interface at the PI.<br />

The activation via 4-20 mA requires an 4-20mA<br />

analogue output for the setpoint rotational speed, as<br />

Delivery Scope Control Unit with power cable.<br />

Technical Data<br />

Performance 0.35 up to 2.2 kW<br />

Rotational Speed 1:250 (at sufficient<br />

Variation<br />

cooling of motor)<br />

Start Ramp Adjustable<br />

Torque Limiting Adjustable<br />

RPM Limiting Adjustable<br />

Resolution<br />

Torque Measurement<br />

5% (differentiated)<br />

Casing Protection<br />

Category<br />

IP54<br />

Power Supply Single phase supply 200 -<br />

240V<br />

Dimensions LxWxH 192x215x277mm<br />

well as respectively one analogue input 4-20mA for<br />

the actual rpm and torque. In addition, a digital<br />

output is required for the digital release.<br />

Order Code Description<br />

IR-VISCOTROL350 ViscoTrol350 control unit for three phase drives, 0,35 kW<br />

IR-VISCOTROL550 ViscoTrol550 control unit for three phase drives, 0,55 kW<br />

IR-VISCOTROL1<strong>10</strong>0 ViscoTrol1<strong>10</strong>0 control unit for three phase drives, 1,1 kW<br />

IR-VISCOTROL2200 ViscoTrol2200 control unit for three phase drives, 2,2 kW<br />

IR-VISCOTROL-MOT055 Asynchronous 0,55 kW motor for Viscotrol<br />

IR-VISCOTROL-MOT075 Asynchronous 0,75 kW motor for Viscotrol<br />

IR-VISCOTROL-MOT1<strong>10</strong> Asynchronous 1,<strong>10</strong> kW motor for Viscotrol<br />

IR-VISCOTROL-MOT150 Asynchronous 1,5 kW motor for Viscotrol<br />

IR-VISCOTROL-MOT300 Asynchronous 3,0 kW motor for Viscotrol<br />

IR-VISCOTROL-FAN Additional fan for ViscoTrol asynchrous motor<br />

ZK-R-HI30-BK-IX-Y-01 ViscoTrol cable for LabManager/box, 4...20mA rotational speed set point and current value,<br />

digital disengange<br />

ZK-R-HI30-BS-R4-I-01 ViscoTrol cable RS485<br />

Automatic<br />

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Automation<br />

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Equipment and<br />

Components<br />

Process Analytics<br />

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326<br />

ViscoTrol rheo<br />

The activation via 4-20 mA<br />

requires an 4-20mA<br />

analogue output for the<br />

setpoint rotational speed, as<br />

well as one analogue input 4-<br />

20mA for the torque The<br />

checkback signal of the<br />

actual rotational speed via the<br />

device-internal PFM-output<br />

requires an additional digital<br />

input. In addition, a digital<br />

output is required for the digital release. Notice: The<br />

deployment of the RS485 requires an additional<br />

RS485 interface module in the PI and a device<br />

component for binary protocoling.<br />

Note: For a MODBUS-interface the option<br />

PNKMODBUS and a single free RS485 at the PI is<br />

needed.<br />

Delivery Scope Control Unit (box) with power<br />

supply line<br />

Stirring and Dispersing<br />

Technical Data<br />

Order Code Description<br />

IR-VISCOTROL350-RHEO ViscoTrol350 control unit for three phase drives. 0,35 kW<br />

IR-VISCOTROL550-RHEO ViscoTrol550control unit for three phase drives, 0,55 kW<br />

IR-VISCOTROL750-RHEO ViscoTrol750 control unit for three phase drives, 0,75 kW<br />

IR-VISCOTROL-MOT075 Asynchronous 0,75 kW motor for Viscotrol<br />

IR-VISCOTROL-MOT1<strong>10</strong> Asynchronous 1,<strong>10</strong> kW motor for Viscotrol<br />

IR-VISCOTROL-FAN Additional fan for ViscoTrol asynchrous motor<br />

Cable<br />

Performance 0.35 to 0.75 kW<br />

Rotational Speed 1:250 (if motors sufficiently<br />

Variation cooled)<br />

Start Ramp Adjustable<br />

Torque Limiting Adjustable<br />

RPM Limiting Adjustable<br />

Resolution Torque 0.5%<br />

Measurement<br />

Casing Protection<br />

Category<br />

IP 20, IP54 at connection<br />

Power Supply 400V Rotating current<br />

Interfaces:<br />

Analogue interfaces 4...20mA, I = set point rpm, O =<br />

torque<br />

RS485 interface with Modbus RTU protocol<br />

Digital disengage<br />

Bestellcode Beschreibung<br />

ZK-R-HI31-BK-IA-Y-01 Cable for LabManager/box, rotational speed setpoint value, actual value torque actual value<br />

4...20mA., release via digital output, 3m<br />

ZK-R-HI31-BK-IP-Y-01 Cable for LabManager/box, rotational speed setpoint value, actual value torque actual value<br />

4...20mA., release via digital output, 3m<br />

Accessories for the ViscoPakt®-Family<br />

Cable<br />

Order Code Description<br />

ZK-R-HI02-BA-UP-Y-03 Cable for LabManager/box, Setpoint speed and actual value,<br />

torque current value, 0...<strong>10</strong>V, 3m<br />

ZK-R-HI02-BA-IP-Y-02 Cable for LabManager/box, Setpoint speed required and actual value,<br />

torque actual value, 0/4...20mA, 3m<br />

ZK-R-HI02-BS-R2-I-01 RS232 cable, Setpoint speed and actual value,<br />

torque actual value, On/Off, 3m<br />

Mounting Elements<br />

Bilateral mounting element for LabKit square<br />

aluminum profiles.<br />

In comparison to standard mounting elements with<br />

round rod, this element defines all axes of the stirrer<br />

drive.<br />

Order Code Description<br />

IR-VPMONT2 Mounting element for ViscoPakt stirrer drives on to LabKit aluminum profiles<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Stirrer Couplings<br />

These stirrer shaft coulings are made of POM, a<br />

mechanically stable light-weight plastic. The power<br />

transmission is conducted via a novel internally<br />

located construction with high-grade steel ball<br />

bearings.<br />

Standard version<br />

Version for magnetic stirrer heads<br />

Stirring and Dispersing<br />

The individual advantages are:<br />

� low-weight but highly stable construction<br />

� extremely low centrifugal forces due to the<br />

low weight<br />

� suited for stirrer shafts jacketed with glass,<br />

metal or PTFE<br />

� Rotational direction-independent (anti- and<br />

clockwise rotation equally possible)<br />

� version free of play (no vibration development<br />

or resonance)<br />

� suited for speeds up to 1200 rpm<br />

� high-power transmission up to 3 Nm<br />

� uncomplicated mounting of the stirring shaft<br />

in a Ø 8 mm and Ø <strong>10</strong> mm receptacle (clamp<br />

ring connection)<br />

� extra-long receptacle pin with Ø <strong>10</strong> mm,<br />

respectively 8 mm hexagon head, and a<br />

length of 90 mm, generates space (length can<br />

be shortened by user)<br />

� Temperature stability maximal +1<strong>10</strong>°C and<br />

minimal -20°C, respectively without stress<br />

Technical Data<br />

Stirring shaft receptacle,<br />

below<br />

8 mm and <strong>10</strong> mm<br />

Upper receptacle Ø <strong>10</strong><br />

Total length 190 mm<br />

Maximum axis offset <strong>10</strong> mm<br />

Technical Data<br />

Stirring shaft receptacle Interior-square<br />

SW6<br />

Upper receptacle Female hexagon<br />

SW8<br />

Total Length 190 mm<br />

Maximum axis offset <strong>10</strong> mm<br />

Order Code Description<br />

IR-VIPARK-BF-POM Light-weight, highly stable stirring coupling made of POM, standard version for stirrer shafts Ø<br />

8mm or <strong>10</strong>mm<br />

IR-VIPARK-VK-POM Light-weight, highly stable stirring coupling made of POM, for magnetic stirrer heads with interiorsquare<br />

SW5 for magnetic coupling<br />

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328<br />

Bellows couplings<br />

In order to be able to bridge longer distances<br />

between the stirrer drive and stirring lead-through,<br />

we offer our flexible stirring shaft extensions. They<br />

consist of bellows couplings and high-grade steel<br />

shafts.<br />

Stirring and Dispersing<br />

Order Code Description Specifications<br />

IR-VIPARWV15019 Flexible stirring shaft extension made of 19 cm, shaft Ø 6mm, 2 bellows coupling max.<br />

high-grade steel<br />

150Ncm<br />

IR-VIPARWV45020 Flexible stirring shaft extension made of 20 cm, shaft Ø <strong>10</strong>mm, 2 bellows coupling max.<br />

high-grade steel<br />

450Ncm<br />

IR-VIPARWV45028 Flexible stirring shaft extension made of 28 cm, shaft Ø <strong>10</strong>mm, 2 bellows coupling max.<br />

high-grade steel<br />

450Ncm<br />

IR-VIPARWV<strong>10</strong>0021 Flexible stirring shaft extension made of 21 cm, shaft Ø <strong>10</strong>mm, 2 bellows coupling max.<br />

high-grade steel<br />

<strong>10</strong>00Ncm<br />

IR-VIPARWV<strong>10</strong>0029 Flexible stirring shaft extension made of 29 cm, shaft Ø <strong>10</strong>mm, 2 bellows coupling max.<br />

high-grade steel<br />

<strong>10</strong>00Ncm<br />

Magnetic stirrer heads<br />

Technical Data<br />

For stirring shafts-Ø 8 mm <strong>10</strong> mm<br />

Square connection<br />

for coupling<br />

Female<br />

square<br />

adapter<br />

SW6<br />

With grinding<br />

Female<br />

square<br />

adapter<br />

SW6<br />

Guide Tube<br />

(glas)<br />

NS 29/32<br />

max. torque 50 Ncm 50 Ncm<br />

max. rpm 1500 rpm 1500 rpm<br />

max. media temp. 250°C 250°C<br />

With grinding<br />

NS 29/32<br />

Advantages<br />

Order Code Description<br />

IR-RDFMAG8 magnetic stirrer head for 8 mm stirring shafts<br />

IR-RDFMAG<strong>10</strong> magnetic stirrer head for <strong>10</strong> mm stirring shafts<br />

� high performance power transmission 50<br />

Ncm<br />

� metal–free, no lubricants<br />

� easy-to-clean due to easy-to-access and<br />

smooth components<br />

� compact construction, low outer dimensions -<br />

Ø 35 mm, generates space on the lid<br />

� high rotational speed up to max. 1.500 rpm<br />

� high working temperature up to +250°C<br />

� excellent chemical stability (comparable with<br />

PTFE)<br />

� Suited for dry run<br />

� Sealed rotor prevents leakages<br />

� smooth, non-porous rotor prevents memory<br />

effects<br />

� extremely durable due to exchangeable<br />

durable wear parts<br />

Miscellaneous Accessories<br />

Order Code Description Specifications<br />

IB-SIND Inductive rotation speed monitor 3...300 Impulse /min, dimensions: M30 thread x 81 mm<br />

IR-VIPASFG Chuck size for glass stirrer with shaft Diameter 8mm, 2 bellows couplings<br />

IR-VIPARWS Stirring shaft protection, half-shell Adjustable length: 19 to 30 cm<br />

Special designs and further accessories available upon request.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Stirrer Blades<br />

According to the desired application, some stirrer<br />

blades are more suited than others to perform the<br />

task. In laboratories close to production, it is often<br />

preferred to use the same stirrer type as in<br />

production in order to reach maximum comparability.<br />

Anchor Stirrer Propeller<br />

Stirrer<br />

Turbine Stirrer Cross-Arm<br />

Stirrer<br />

Stirring and Dispersing<br />

Plane Stirrer /<br />

Turbo Stirrer<br />

Slanted Blade<br />

Stirrer<br />

We are able to produce and supply stirrer blades<br />

according to your specifications made of stainless<br />

steel, glass and other materials.<br />

Stirrer blades out of metal can be provided with a<br />

thin glass coating in order to increase media<br />

compatibility.<br />

Impeller Stirrer MIG-Stirrer Toothed Disc/<br />

Dissolver<br />

Stirrer<br />

Grating Stirrer Paddle Stirrer Spiral Ribbon<br />

Stirrer<br />

Stirrer type Recommended Application Speed Range Principal Viscosity Limit Diameter Ratio D/<br />

approx. rpm** Current approx. mPas (cSt) d<br />

Anchor stirrer In case of crust<br />

development, good<br />

exchange of heat,<br />

strong shear flow,<br />

medium to high-viscous<br />

20 ... 500 tangential 50,000 1.05 ... 1.1<br />

Propeller stirrer Good mixing effect,<br />

stirring of light solid<br />

matters, thickening<br />

agents<br />

200 ... 1800 axial 4,000 3 ... 6<br />

Pane stirrer Dispersing, dispersion 300 ... 1500 radial 1,000 2 ... 4<br />

(with blades)/ of gases, strong shear<br />

Turbo stirrer flow<br />

Impeller stirrer Good mixing effect 500 ... 1500 radial <strong>10</strong>,000 1.5 ... 2<br />

MIG-stirrer high mixing effect,<br />

strong shear flow for<br />

low to medium<br />

viscosities<br />

200 ... <strong>10</strong>00 axial <strong>10</strong>,000 1.05 ... 1.5<br />

Toothed disc/<br />

dissolver stirrer<br />

Particle break-up <strong>10</strong>00 ... 3000 radial <strong>10</strong>0,000 2 ... 5<br />

Turbine stirrer Highly viscous media,<br />

lacquers, medium to<br />

high rotation speeds<br />

400 ... 2200 axial 200,000 3 ... 6<br />

Automatic<br />

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Components<br />

Process Analytics<br />

and Sensors<br />

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Stirring and Dispersing<br />

Stirrer type Recommended Application Speed Range Principal Viscosity Limit Diameter Ratio<br />

approx. rpm** Current approx. mPas (cSt) D/d<br />

Cross-arm stirrer Shea flows in several<br />

fields, medium viscous<br />

liquids, good exchange of<br />

heat<br />

400 ... 800 tangential <strong>10</strong>,000 1.1 ... 2<br />

Slanted blade good axial mixing effect , 500 ... 2500 radial 1,000 2.5 ... 3.5<br />

stirrer<br />

shear flow, prevention of<br />

layer build-up<br />

Grating stirrer Medium viscosity, strong<br />

shear flow, good<br />

exchange of heat<br />

200 ... 700 tangential 5,000 1.4 ... 2<br />

Paddle stirrer Low rotation speed, strong 20 ... <strong>10</strong>0<br />

shear flow, very sparing at<br />

low rotation speeds<br />

tangential <strong>10</strong>0 1.5 ...3<br />

Helical ribbon Powerful shear flow, for 50 ... 200 axial 50,000 1.1 ... 1.5<br />

stirrer<br />

high-viscous liquids,<br />

suspensions, pastes<br />

**with D of approx. 20 cm<br />

The stated values do strongly vary within literature<br />

by more than one order of magnitude and are used<br />

for a first orientation. Our project department will<br />

gladly help you to find a suitable stirrer-drive.<br />

To help you, we require the following information<br />

Order Code Description<br />

IR-RBL-rt-rd-ws-wl-wd Stirrer blade<br />

rt = stirrer type:<br />

AN Anchor stirrer<br />

PR Propeller stirrer<br />

SC Plane or turbo stirrer<br />

IP Impeller stirrer<br />

MI MIG-stirrer<br />

ZA Toothed disc stirrer<br />

TU Turbine stirrer<br />

KR Cross arm stirrer<br />

ST Slant blade stirrer<br />

GI Grating stirrer<br />

BL Paddle stirrer<br />

SP Spiral stirrer<br />

rd = blade diameter in mm (d)<br />

ws = material:<br />

ES Stainless steel<br />

EG Glass coated stainless steel<br />

GL Glass<br />

wl = shaft length<br />

wd = shaft diameter<br />

Ordering example:<br />

Anchor stirrer of glass, diameter 15 cm, shaft<br />

diameter <strong>10</strong> mm, shaft length 30cm<br />

Order code: IR-RBL-AN-150-GL-300-<strong>10</strong><br />

from you:<br />

Stirrer type used, rotation speed, viscosity (or<br />

comparative information like water, motor oil,<br />

honey ...), mixing pot D, used stirrer D.<br />

Projecting Aide:<br />

Estimation of Viscosity<br />

Material Viscosity in mPas<br />

approx. at 20 ° C<br />

Acetone 0.33<br />

Alcohol 0.6<br />

Benzene 0.65<br />

Water 1<br />

Liqueur 3<br />

Condensed milk 7,5% 12<br />

Condensed milk <strong>10</strong>% 45<br />

Olive oil 80<br />

Edible oil 85<br />

Apple juice concentrate 300<br />

Egg liqueur 600<br />

Yogurt 900<br />

Glycerine 1,500<br />

Honey 2,000-<strong>10</strong>,000<br />

Mustard 11,000<br />

Print colours <strong>10</strong>0,000 – <strong>10</strong>0 Mill.<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Stirring and Dispersing<br />

ViscoGraph – Automation of Stirring Tests<br />

ViscoGraph allows the automation of stirringtechnological<br />

tests with the ViscoPakt Torque<br />

Measurement Stirrer.<br />

The Programme enables:<br />

� Measurement of the torque in dependency of the<br />

speed<br />

� User-defined Torque Profiles<br />

� Measurement of the Viscosity<br />

� Zero Torque Calibration<br />

With the buttons on the left, it is possible to call up<br />

the various functions of ViscoGraph. The current<br />

values of the test period, rotation speed etc., are<br />

presented in the view boxes.<br />

The diagrams present the procedure of speed and<br />

torque via the time.<br />

The speed profile can be defined via up to <strong>10</strong><br />

sampling points:<br />

it is possible to select for each speed sampling point,<br />

if the speed is approached via a jump or a ramp:<br />

The data is stored in the *.csv format and can<br />

undergo further processing with programmes such<br />

as MS-Excel.<br />

The measurement system can be extended by<br />

further measurement variables with the help of the<br />

digital measuring amplifier.<br />

The additionally captured measurement curves<br />

receive an own Y-axis in the diagram.<br />

Order Code Description<br />

SL-VISCOGRAPH ViscoGraph Control Software for automated Operation of ViscoPakt Measuring Stirrers<br />

SL-VISCOGRAPHAI ViscoGraph Control Software Upgrade for Voltage Measurement with IL-AINAMP1D<br />

SL-VISCOGRAPHPT ViscoGraph Control Software Upgrade for Temperature Measurement with I IL-PTAMP1D<br />

IL-AINAMP1D Digital Measuring Amplifier for -<strong>10</strong>...+<strong>10</strong>V, 0/4...20mA, RS232 V24 /RS485 Interface<br />

IL-PTAMP1D Digital Measuring Amplifier for Pt<strong>10</strong>0 Four-Wire Technology, RS232 V24 /RS485 Interface<br />

IL-MV1D-SN Power Supply Plug for digital Amplifier<br />

Customer-specific adjustments and extensions are possible.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 331<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


332<br />

Stirring and Dispersing<br />

Dispersing and Homogenising<br />

Drives<br />

These high-performance drives for laboratory<br />

applications meet all requirements to modern and<br />

compact laboratory drives and represent a<br />

guarantee for safe and successful working in the<br />

laboratory.<br />

Together with the accessories, you already dispose<br />

of a wide application range:<br />

� Homogenisation<br />

� Dispersing<br />

� Emulsifying<br />

� Suspending<br />

This can be utilised for the preparation of analyses<br />

as well as in reactor acceleration.<br />

The rotational speed of the drives can be adjusted<br />

continuously up to 35,000 rpm.<br />

The exchange of tools is fast and uncomplicated<br />

with the patented tool receptacle system.<br />

Tools<br />

The tools consist of rotor and stator. The rotor<br />

geometry generates a strong pumping effect. Due to<br />

this, the media is suctioned into the operational<br />

range between rotor and stator. Here, high<br />

frequency vertical and horizontal pulsations are<br />

generated. Due to the high exit speeds, ultrasonic<br />

frequencies are generated at the stator slits. This<br />

leads to cavitation.<br />

A balanced interaction between shear forces and<br />

percussion effects transfers the the liquid media<br />

intended for processing into the finest state. This<br />

significantly shortens process periods and reduces<br />

the heat input.<br />

The tools are made of acid-resistant high-grade<br />

steel 316L. They can be sterilised and are<br />

autoclaveable.<br />

The special shaft geometry enables fast tool<br />

exchange. PTFE rings prevent the medium from<br />

rising into the shaft tube.<br />

Drive 350 Watt Drive 1400 Watt Tool<br />

Order Code Description<br />

IR-DISPANTR350 Drive 350Watt, up to 35,000 rpm, for dispersing tools<br />

IR-DISPANTR750 Drive 750Watt, up to 35,000 rpm, for dispersing tools<br />

IR-DISPANTR850 Drive 850Watt, up to 35,000 rpm, for dispersing tools<br />

IR-DISPANTR1400 Drive 1400Watt, up to 35,000 rpm, for dispersing tools<br />

IR-DISPWZ040 Dispersing tool with quick coupling, diameter 4 mm<br />

IR-DISPWZ063 Dispersing tool with quick coupling, diameter 6.3 mm<br />

IR-DISPWZ140 Dispersing tool with quick coupling, diameter 14 mm<br />

IR-DISPWZ200-G Dispersing tool with quick coupling, coarse, diameter 20 mm<br />

IR-DISPWZ40-F Dispersing tool with quick coupling, fine, diameter 20 mm<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Here you will find:<br />

� Customised Application Programs<br />

� Seminars and Training Offers<br />

� <strong>Main</strong>tenance Contracts<br />

� Order Guide for Product Manuals<br />

Services<br />

Services<br />

Phases<br />

Services<br />

Planning Establishment<br />

/ Assembly<br />

Commissioning Operation<br />

Consultancy �� ��<br />

Training �� �� ��<br />

Realisation �� �� ��<br />

Support �� �� �� ��<br />

Service/<strong>Main</strong>ten<br />

ance<br />

��<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 333<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


334<br />

Services<br />

<strong>HiTec</strong> <strong>Zang</strong> - Your competent Project Partner !<br />

The company <strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong>, in addition to<br />

being a system retailer supplying systems and<br />

components, also offers a wide range of services.<br />

We are able to support you with our know-how<br />

gained in 30 years of project work for the process<br />

engineering industry covering all project phases:<br />

Services<br />

Phases<br />

Planning Establishment /<br />

Assembly<br />

Commissioning Operation<br />

Consultancy �� ��<br />

Training �� �� ��<br />

Realisation �� �� ��<br />

Support �� �� �� ��<br />

Service/<br />

<strong>Main</strong>tenance<br />

Our Service Portfolio in detail:<br />

� PMC technical consultancy,<br />

� Procedural consultancy,<br />

� Plant design for laboratory and<br />

� Mini-plants,<br />

� PMC, planning of basic version, realisation<br />

� and planning of application -oriented details,<br />

� Component selection for special<br />

� Problem solutions,<br />

� PMC, application establishment,<br />

� Control-oriented support,<br />

� Support for Commissioning,<br />

� Fault diagnosis and analysis,<br />

� Device coupling,<br />

� Sensor calibration,<br />

� Seminars and training,<br />

� Remote maintenance,<br />

� Order development.<br />

��<br />

Take advantage of our widespread know-how for<br />

your projects:<br />

� Research Process Control Systems,<br />

� Automated Laboratory Reactor Systems,<br />

� Mini- und Bench-Plant-Technology,<br />

� NAMUR-basis Operations,<br />

� Instrumenting, Sensors,<br />

� Spectrometry,<br />

� High-Precision Temperature Measurement,<br />

� Reaction Calorimetry,<br />

� Weighing and Dosing Technology,<br />

� Measuring and Control Technology,<br />

� Process Control Technology, PLC Technology,<br />

� LIMS-Systems,<br />

� Device Interfaces,<br />

� CAN-Bus, Profi-Bus-DP,<br />

� Remote Data Transmission, Remote<br />

<strong>Main</strong>tenance,<br />

� Remote Alarming via Phone, E-Mail or SMS,<br />

� Computer Networks<br />

� Quality Assurance Systems.<br />

Our experienced project engineers and technicians<br />

will support you all the way until your project is<br />

ideally realised. Whether you merely require<br />

consultancy, or you wish to couple an analysis<br />

device with a special protocol with a control system,<br />

or you require a complete ready-to-use plant,<br />

whatever it may be, you can count on our support.<br />

Just talk to us!<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Services<br />

Customised Application Programs<br />

<strong>HiTec</strong> <strong>Zang</strong> establishes application programs<br />

according to customer specifications. If required,<br />

we will gladly establish a duty record book<br />

Collection and Administration of Stirrer-related Data<br />

GyroDat is a program package for the projecting<br />

and realisation of tests applying a stirrer. The work<br />

environment includes the process control of the<br />

test progression, the collection, evaluation, the<br />

presentation, and archiving of the data.<br />

GyroDat consists of two modules. The<br />

administration, projecting, and evaluation were<br />

realised in the <strong>HiTec</strong> <strong>Zang</strong> HiBuilder, the process<br />

control programmed in the <strong>HiTec</strong> <strong>Zang</strong> -<br />

Labvision and HiText.<br />

Systematic Examinations:<br />

� Influence of the Stirrer Design<br />

� Influence of Flow Interrupters<br />

� Influence of Vessel Design<br />

� Properties of Media<br />

The Sequence of Operation<br />

Stirrer type, vessel type, flow interrupters, and<br />

revolutions are specified by the user and transferred<br />

by GyroDat to Labvision for automatic execution.<br />

The data collected in the course of the stirring test is<br />

transferred by Labvision to GyroDat for evaluation.<br />

GyroDat calculates the process characteristics and<br />

establishes the result diagrams.<br />

Calculated Data:<br />

� Re = f(Ne)<br />

� Md = f(n)<br />

� Idle time data of the stirrer drive<br />

containing the product requirement specifications<br />

in the forefront. The following shows an example<br />

based on the HiBuilder.<br />

Administration of the Project Data<br />

The user interface/work station of the GyroDat is<br />

designed for the graphic evaluation and simple<br />

comparison of various test data.<br />

Up to ten project steps can be parameterised in the<br />

project data window. A change of media during the<br />

test is taken into account. Data storage is<br />

conducted automatically.<br />

Administrated are:<br />

� 200 Project Template<br />

� <strong>10</strong>0 Stirrer Stands<br />

� <strong>10</strong>0 Stirrer<br />

� <strong>10</strong>0 Container<br />

� <strong>10</strong>0 Flow Interruptor<br />

� 50 Reference Media<br />

Presentation of the Data<br />

A freely designable protocol page (with HiBuilder)<br />

containing graphics, values, and comments can be<br />

printed out.<br />

Order Code Description<br />

SA-GYRODAT Program for the collection and administration of stirrer data<br />

Please also consider our precision measurement stirrer ViscoPakt-rheo, which is ideally suited to conduct<br />

stirring tests.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 335<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


336<br />

Seminars and Training<br />

The continuous vocational and advanced training<br />

for personnel is the most important investment for<br />

the future of your enterprise. Profound knowledge<br />

is an essential prerequisite for the successful<br />

realisation of your products. Our seminar training<br />

portfolio in regard to the selection of the topics and<br />

content is the result of our many years of practical<br />

experience in deploying laboratory automation and<br />

mini-plant technology.<br />

Due to the fact that we are aware that learning<br />

something is accomplished the fastest by actually<br />

doing something yourself in practice, our training<br />

mainly consists of practical training at our systems.<br />

The participants mainly conduct clearly set tasks<br />

independently.<br />

The training is conducted on our premises and, in<br />

the ideal case, is rounded off by support during the<br />

commissioning at the client plant.<br />

Your advantages:<br />

� Reduction of the Project Preparation Period<br />

� Reduction of the Project Running Period<br />

� Better Results<br />

� Optimal Utilisation of the Equipment<br />

� Staff Satisfaction<br />

Training Modules<br />

the training program is principally aligned to your<br />

individual requirements. The training schedule is<br />

arranged out of the following modules. A user<br />

introduction approximately requires ½ to 1 day, a<br />

complete training program between 5 and 8 days,<br />

depending on the existent knowledge of the<br />

participant.<br />

Up to four participants may participate without<br />

additional charge. The provision of the equipment<br />

for two participants is included in the price. For<br />

Services<br />

each of the other two participants, extra equipment<br />

is required.<br />

Level 1: User Training<br />

Introduction into the Lab/MSRmanager System<br />

Prerequisites: Windows experience, basic<br />

chemical-process-oriented experience.<br />

Introduction of the UI Software LabVision<br />

� Configuring and Parameterising<br />

� Multiplotter<br />

� Online-Graphics<br />

� Monitoring and Operating in PLS Images<br />

� Programming<br />

User Training at the UI/Work Station of a<br />

simulated Plant<br />

� Administration and Starting of the Project<br />

� Configuring and Parameterising<br />

� Monitoring and Operating<br />

� Establishment and Realisation of a recipe with<br />

HiBatch<br />

� Discussion, open issues<br />

Level 2: Project Manager Training<br />

Project Establishment in LabVision<br />

Prerequisites: Windows experience, basic<br />

knowledge of PMC technology.<br />

PMC-Basic Knowledge<br />

� Connection and Parameterisation of Sensors<br />

and Actors<br />

� Data Storage in the History Data Base<br />

� Setting up of the Plotters<br />

� Establishment and Dynamisation of PLS-<br />

Images<br />

� Linking of Signals<br />

� Process Report<br />

� Message Report<br />

� Data Export<br />

� Routing of Message Events<br />

� Visualisation of Message Events<br />

� Project Establishment with Project Modules<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


The following topics can be combined to form an<br />

individually aligned training program:<br />

� HiText, Control and Online Evaluation<br />

� Programming of Recipe Element Programs<br />

Services<br />

� Setting Up and Parameterisation of Controllers<br />

� Programming in IEC 61131 I<br />

� System Administration<br />

� Advanced Training<br />

� Applied Control Technology<br />

Order Code Description<br />

DS-SCHULTAS One daily rate, content according to prior agreement<br />

DS-SCHULQUIP Provision of the training equipment, one work station, maximum two participants per day<br />

<strong>Main</strong>tenance Contracts<br />

Software-Upgrade-Contract<br />

An Update is an improved program version with<br />

unmodified functional range, After the purchase of<br />

any of our software, the customer, upon request, will<br />

receive updates free of charge for the duration of<br />

one year.<br />

An upgrade is a further developed version which<br />

usually contains an extended functional range.<br />

Without a software upgrade contract (after expiry of<br />

the first year), an upgrade for any consecutive year<br />

costs 15 % of the catalogue price. The upgrade<br />

option expires 4 years after the initial purchase,<br />

respectively the last update.<br />

Order Code Description<br />

DS-UPGR Software Upgrade<br />

Hardware <strong>Main</strong>tenance Contract<br />

If a Hardware <strong>Main</strong>tenance Contract is concluded,<br />

we will annually check and calibrate your devices<br />

and upgrade them to the current state of technology.<br />

Faulty parts will be exchanged free of charge either<br />

in our works or directly at the location. Only the<br />

travelling expenses will be charged. Damage due to<br />

external influences is excluded.<br />

Order Code Description<br />

DS-VHW Hardware <strong>Main</strong>tenance Contract<br />

Support and Remote <strong>Main</strong>tenance Contract<br />

If a Support Contract is concluded, our Hotline is<br />

available for the answering of your queries, when<br />

establishing applications or for the quick solution of<br />

software problems.<br />

Order Code Description<br />

DS-VSW Support and Remote <strong>Main</strong>tenance Contract<br />

Upon request, we will conduct the installation<br />

subject to the charge of the according expenditures.<br />

Example: If a software was purchased 2 ½ years<br />

ago (no existing software upgrade contract) and the<br />

catalogue prices is stated as, e.g., 2800€, the price<br />

for the update amounts to 2 x 15% (due to the fact<br />

that the first year is free) of 2800€, therefore 840€.<br />

With a Software-Upgrade-Contract, you are entitled<br />

to the respectively most recent version. The annual<br />

costs amount to 15 % of the current catalogue price.<br />

If required, we will conduct remote maintenance.<br />

The contract will be aligned to your individual<br />

requirements.<br />

Automatic<br />

Laboratory<br />

Reactor Systems<br />

Reaction<br />

Calorimetry<br />

Fermentation<br />

technology<br />

Automation<br />

Hardware<br />

Automation<br />

Software<br />

Plant<br />

Construction and<br />

Technology<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 337<br />

Equipment and<br />

Components<br />

Process Analytics<br />

and Sensors<br />

Dosing Systems,<br />

Pumps<br />

Liquid-Handling,<br />

Autosampler<br />

Stirring and<br />

Dispersing<br />

Services


338<br />

Product Manuals<br />

The manuals to our products are usually delivered<br />

together with the product on a data carrier. If<br />

required, they can also be acquired as a printed<br />

paper version.<br />

Application Software<br />

Services<br />

Order Code Description<br />

ZH-LABVIS LabVision Manual<br />

ZH-HIBUILDER Manual to the evaluation program HiBuilder<br />

ZH-GYRODAT Manual to the evaluation program GyroDat<br />

ZH-KALDAS Manual to the evaluation program KalDas<br />

ZH-SOLIDOS SoliDos Manual<br />

ZH-VISCOPAKT ViscoPakt Manual<br />

ZH-RAMOS RAMOS Manual<br />

ZH-LABDOS LabDos Manual<br />

ZH-GRAVIDOS GraviDos Manual<br />

ZH-AUTOSAM AutoSam Manual<br />

ZH-ALFADOS AlfaDos Manual<br />

ZH-REGLER Manual Controllers and Controller Parameterisation<br />

ZH-HICON Manual to the adaptive Controller HiCon<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


018ML<strong>10</strong>B.............................................................279<br />

070ML30B.............................................................279<br />

280ML80B ............................................................279<br />

CG-ABK1C............................................................136<br />

CG-ABK1D............................................................136<br />

CG-ABK1I..............................................................136<br />

CG-ABK1M...........................................................136<br />

CG-ABK2C............................................................137<br />

CG-ABK2D............................................................137<br />

CG-ABK2I..............................................................137<br />

CG-ABK2M...........................................................137<br />

CG-ABKEX............................................................137<br />

CG-LABCOMMANDER.........................................275<br />

CG-LABCOMMANDER.........................................274<br />

CG-OMNIFERM-ABK..............................................42<br />

CK-RAID1..............................................................137<br />

CK-RAM2x<strong>10</strong>24....................................................137<br />

CK-RAM2x2048....................................................137<br />

CK-RAM2x512......................................................137<br />

CP-BCS232...........................................................140<br />

CP-DIGICAM1.......................................................158<br />

CP-DIGICAM2.......................................................158<br />

CP-DRUHPDJC....................................................140<br />

CP-DRUHPLJ.......................................................140<br />

CP-DRUHPLJC.....................................................140<br />

CP-INMON ...........................................................138<br />

CP-ISDNAD..........................................................175<br />

CP-M17TFT..........................................................139<br />

CP-M190TFT........................................................139<br />

CP-M20TFTWS ....................................................139<br />

CP-M22TFTWS.....................................................139<br />

CP-MODEM2........................................................175<br />

CP-MODEM4........................................................175<br />

CP-USV7...............................................................138<br />

CP-USV7O............................................................138<br />

CP-USV7O............................................................136<br />

CS-RS2322-PCI....................................................139<br />

CS-RS2324-PCI....................................................139<br />

CS-RS4852-PCI....................................................139<br />

CS-RS4854-PCI....................................................139<br />

CZ-EXMAUS.........................................................137<br />

CZ-USB-RS232.....................................................275<br />

CZ-USB-RS232.....................................................274<br />

DS-LVPROG.........................................................174<br />

DS-SCHULQUIP ..................................................337<br />

DS-SCHULTAS ....................................................337<br />

DS-UPGR..............................................................337<br />

DS-VHW ...............................................................337<br />

DS-VSW ...............................................................337<br />

HA-COMSERV<strong>10</strong>01..............................................132<br />

HA-MODEM4........................................................132<br />

HA-RS485 ............................................................131<br />

HA-V24LINK2 .......................................................131<br />

HA-V24LINKKLA...................................................131<br />

HA-V24LINKKLI....................................................131<br />

HD-RS2329 ............................................................92<br />

HD-RS2329(P)L....................................................130<br />

HD-RS2329L.........................................................<strong>10</strong>3<br />

HD-RS2329PL......................................................<strong>10</strong>3<br />

HD-RS485P..........................................................<strong>10</strong>3<br />

HE-EEXID.............................................................121<br />

HE-EEXII...............................................................121<br />

HE-EEXIPT<strong>10</strong>0.....................................................121<br />

HE-EEXIRS232.....................................................121<br />

Order Codes<br />

HE-EEXITH...........................................................121<br />

HE-EEXIU.............................................................121<br />

HK-AD20N.............................................................121<br />

HK-AD20NMUX16................................................123<br />

HK-AD20NMUX8..................................................123<br />

HK-AD24DMS4.....................................................255<br />

HK-AD24DMS4.....................................................253<br />

HK-AD24DMS4.....................................................206<br />

HK-AD24DMS4.....................................................125<br />

HK-AD24DMS4PTR..............................................267<br />

HK-AD24PKAL......................................................124<br />

HK-AD24PX8........................................................124<br />

HK-DA812UI.........................................................125<br />

HK-DEA16N..........................................................126<br />

HK-GRADOMV1...................................................267<br />

HK-GRADOMV1...................................................255<br />

HK-GRADOMV1...................................................253<br />

HK-GRADOMV1...................................................206<br />

HK-GRADOMV1D.................................................267<br />

HK-GRADOMV1D.................................................255<br />

HK-GRADOMV1D.................................................206<br />

HK-GRADOMV1D-SN...........................................267<br />

HK-GRADOMV1D-SN...........................................255<br />

HK-GRADOMV1D-SN...........................................206<br />

HK-HMUX..............................................................122<br />

HK-PHAMP.............................................................92<br />

HK-SER16ECB.....................................................127<br />

HK-SER16ECB.....................................................<strong>10</strong>4<br />

HK-SER8ECB.......................................................127<br />

HK-SER8ECB.......................................................<strong>10</strong>4<br />

HK-SER8ECB.........................................................72<br />

HP-B230V16H ......................................................128<br />

HP-B230V16R.......................................................128<br />

HP-LABCOM1 ......................................................130<br />

HP-SITEMPBEG1.................................................257<br />

HP-SITEMPWAE1 ...............................................256<br />

HP-WDOGEXT1-pa .............................................131<br />

HS-NGS153SN.....................................................133<br />

HS-NGS241A........................................................132<br />

HS-NGS241S........................................................132<br />

HS-NGS242..........................................................133<br />

HS-NGS242............................................................69<br />

HS-NGS243..........................................................133<br />

HS-NGS248..........................................................133<br />

HS-NGS248E........................................................133<br />

HS-NGS248S........................................................132<br />

HX-SIMPT1...........................................................134<br />

IB-FGVE-120-GMG3/4-ea....................................257<br />

IB-FVGE-1200-GMG1/4-ea..................................259<br />

IB-FVGE-60-GMG3/4-ea......................................257<br />

IB-LWDRU-NC-ea.................................................262<br />

IB-LWE-<strong>10</strong>0-sk-ea.................................................260<br />

IB-LWE-250-NC-ea...............................................261<br />

IB-LWE-250-sk-ea.................................................260<br />

IB-LWE-300-sk-ea.................................................260<br />

IB-PRKO-6-ma-ea.................................................258<br />

IB-SIND.................................................................328<br />

IB-SIND.................................................................262<br />

IFN-IV-MW1..........................................................223<br />

IFN-IV-MW2..........................................................223<br />

IL-AINAMP1D........................................................331<br />

IL-AINAMP1D........................................................135<br />

IL-AINAMP1D........................................................134<br />

IL-ALCOTECT-AIRS...............................................47<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 339


340<br />

IL-ALCOTECT-d-l....................................................47<br />

IL-AOUT1D...........................................................135<br />

IL-AOUT1D...........................................................134<br />

IL-AUTOSAM-B-DN..............................................314<br />

IL-AUTOSAM-BSCHU..........................................313<br />

IL-AUTOSAM-DA24..............................................314<br />

IL-AUTOSAM-DA24..............................................312<br />

IL-AUTOSAM-DN-6-x-x.........................................313<br />

IL-AUTOSAM-EN-6-x............................................313<br />

IL-AUTOSAM-FEACON........................................314<br />

IL-AUTOSAM-KL...................................................313<br />

IL-AUTOSAM-MB-2-3-K........................................312<br />

IL-AUTOSAM-MB-2-3-P........................................312<br />

IL-AUTOSAM-POLI...............................................314<br />

IL-AUTOSAM-R....................................................312<br />

IL-AUTOSAM-RF-d-l.............................................312<br />

IL-AUTOSAM-RS485............................................314<br />

IL-AUTOSAM-SPPS.............................................314<br />

IL-AUTOSAM-STLI...............................................314<br />

IL-AUTOSAM-STRE.............................................314<br />

IL-AUTOSAM-TAN................................................312<br />

IL-AUTOSAM-TVERL...........................................314<br />

IL-AUTOSAM-WASBO..........................................314<br />

IL-AUTOSAM-XL-<strong>10</strong>00-12....................................317<br />

IL-AUTOSAM-XL-2000-8......................................317<br />

IL-AUTOSAM-XL-500-14......................................317<br />

IL-AUTOSAM200...................................................311<br />

IL-AUTOSAM200-T-11-32.....................................311<br />

IL-AUTOSAM300..................................................308<br />

IL-AUTOSAM300-T-12-50.....................................308<br />

IL-AUTOSAM300-T-17-32.....................................308<br />

IL-AUTOSAM300-T-23-25.....................................308<br />

IL-AUTOSAM300-T-30-23.....................................308<br />

IL-AUTOSAM300-T-46-15.....................................308<br />

IL-AUTOSAM300-T-56-11.....................................308<br />

IL-AUTOSAM360..................................................309<br />

IL-AUTOSAM360-T-12-80.....................................309<br />

IL-AUTOSAM360-T-17-49.....................................309<br />

IL-AUTOSAM360-T-23-41.....................................309<br />

IL-AUTOSAM360-T-46-18.....................................309<br />

IL-AUTOSAM360-T-56-15.....................................309<br />

IL-CLARKAMP1D..................................................135<br />

IL-CLARKAMP1D..................................................134<br />

IL-DIN1D...............................................................135<br />

IL-DIN1D...............................................................134<br />

IL-DOUT1D...........................................................135<br />

IL-DOUT1D...........................................................134<br />

IL-Gmix-S-RAMP....................................................47<br />

IL-GMIX21...............................................................47<br />

IL-GMIX21-X...........................................................47<br />

IL-GMIX31...............................................................47<br />

IL-GMIX31-X...........................................................47<br />

IL-GMIX31-XET.......................................................47<br />

IL-GMIX41...............................................................47<br />

IL-GMIX41-X...........................................................47<br />

IL-GMIX41-XET.......................................................47<br />

IL-GRADO<strong>10</strong>00.....................................................267<br />

IL-GRADO<strong>10</strong>000...................................................267<br />

IL-GRADO<strong>10</strong>000D................................................267<br />

IL-GRADO<strong>10</strong>00D..................................................267<br />

IL-GRADO15000...................................................267<br />

IL-GRADO15000D................................................267<br />

IL-GRADO3000.....................................................267<br />

IL-GRADO3000D..................................................267<br />

Order Codes<br />

IL-GRADO7000.....................................................267<br />

IL-GRADO7000D..................................................267<br />

IL-GRADOADR.....................................................206<br />

IL-GRADOADR12.................................................267<br />

IL-GRADOADR12.................................................255<br />

IL-GRADOADR14.................................................267<br />

IL-GRADOADR14.................................................255<br />

IL-GRADOADV.....................................................267<br />

IL-GRADOADV.....................................................255<br />

IL-GRADOADV.....................................................206<br />

IL-GRADOAMP1D................................................135<br />

IL-GRADOAMP1D................................................134<br />

IL-GRADOAMP1D................................................<strong>10</strong>6<br />

IL-GRADOAMP1D-SN..........................................<strong>10</strong>6<br />

IL-GRADOEX........................................................267<br />

IL-GRADOEX........................................................266<br />

IL-GRADOMV1.....................................................<strong>10</strong>6<br />

IL-GRAVI-KAL<strong>10</strong>00...............................................267<br />

IL-GRAVI-KAL2000...............................................267<br />

IL-GRAVIDOSST1.................................................267<br />

IL-GRAVIDOSST1.................................................266<br />

IL-GRAVIHEAT<strong>10</strong>00..............................................267<br />

IL-GRAVIHEAT2000..............................................267<br />

IL-GRAVIHEAT250................................................267<br />

IL-GRAVIHEAT500................................................267<br />

IL-GRAVIHEATSON..............................................267<br />

IL-GRAVIRS..........................................................267<br />

IL-GRAVIRS..........................................................266<br />

IL-GRAVLBB<strong>10</strong>00.................................................268<br />

IL-GRAVLBB<strong>10</strong>00.................................................267<br />

IL-GRAVLBB2000.................................................268<br />

IL-GRAVLBB2000.................................................267<br />

IL-GRAVLBB250...................................................267<br />

IL-GRAVLBB250 ..................................................268<br />

IL-GRAVLBB500...................................................268<br />

IL-GRAVLBB500...................................................267<br />

IL-GRAVLBGRAD.................................................267<br />

IL-GRAVLBS150...................................................267<br />

IL-GRAVLBS300...................................................267<br />

IL-GRAVLBS500...................................................267<br />

IL-HISENSE-c-2......................................................51<br />

IL-HISENSE-c-4......................................................51<br />

IL-HISENSE-c-8......................................................51<br />

IL-HISENSE-c-x......................................................42<br />

IL-HISENSE-m-1.....................................................50<br />

IL-HISENSE-m-2.....................................................50<br />

IL-HISENSE-m-3.....................................................50<br />

IL-HISENSE-m-5.....................................................50<br />

IL-HISENSE-m-5.....................................................50<br />

IL-HISENSE-m-x.....................................................42<br />

IL-KALHEIZE50.......................................................34<br />

IL-KALHEIZES<strong>10</strong>0..................................................34<br />

IL-KALHEIZG50......................................................34<br />

IL-KALHEIZGL<strong>10</strong>0..................................................34<br />

IL-KALHEIZP<strong>10</strong>0.....................................................34<br />

IL-KALHEIZP50.......................................................34<br />

IL-KALKALIB<strong>10</strong>0.....................................................34<br />

IL-KALKALIB50.......................................................34<br />

IL-LIQUIDOS1.......................................................315<br />

IL-MV1D-SN..........................................................331<br />

IL-MV1D-SN..........................................................135<br />

IL-ODFERM-l...........................................................42<br />

IL-OXYTECT-l.........................................................48<br />

IL-OXYTECT-l.........................................................42<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


IL-PHADEC...........................................................235<br />

IL-PHADEC-PTFE.................................................235<br />

IL-PHADEC-SE.....................................................235<br />

IL-PHADEC-X.......................................................235<br />

IL-PHAMP1...........................................................<strong>10</strong>5<br />

IL-PHAMP1D.........................................................135<br />

IL-PHAMP1D.........................................................134<br />

IL-PHAMP1D.........................................................<strong>10</strong>5<br />

IL-PHAMP1D-SN..................................................<strong>10</strong>5<br />

IL-PHASEP............................................................211<br />

IL-PHFERM-l...........................................................48<br />

IL-PHFERM-l...........................................................42<br />

IL-PIPET1..............................................................317<br />

IL-PTAMP1D.........................................................331<br />

IL-PTAMP1D.........................................................135<br />

IL-PTAMP1D.........................................................134<br />

IL-RFT-SV-1..........................................................212<br />

IL-RFT-SV-MAG....................................................212<br />

IL-RFT-TR-1..........................................................212<br />

IL-RFT-TR-MAG....................................................212<br />

IL-SCIBOT-x..........................................................318<br />

IL-SCIBOTBIB.......................................................318<br />

IL-SOLIDOS-RS....................................................304<br />

IL-SoliDos-SF-G-1.................................................303<br />

IL-SOLIDOS-SF-V-1..............................................302<br />

IL-SOLIDOS-TD-G................................................303<br />

IL-SOLIDOS-TD-G-1.............................................303<br />

IL-SOLIDOS-TD-V-1.............................................303<br />

IL-SOLIDOS2-HEIZ...............................................302<br />

IL-SOLIDOS2-KF..................................................302<br />

IL-SOLIDOS2-SK-x...............................................302<br />

IL-SOLIDOS2-x ....................................................302<br />

IL-SOLIDOS2-x-ST ..............................................302<br />

IL-SOLIDOSADGD................................................302<br />

IL-SOLIDOSST1...................................................304<br />

IL-VERDA-THEL...................................................213<br />

IL-VERDA-TREG..................................................213<br />

IL-VERDA120........................................................213<br />

IP-B-K1-1800L-VA-GMG1/2-ep............................294<br />

IP-B-K2-3900L-ETFE/SIC.....................................295<br />

IP-B-REAKT1-4P..................................................296<br />

IP-B-REAKT1-FU..................................................296<br />

IP-B-V1-1200L-PTFE/FPM...................................298<br />

IP-B-V1-1200L-PTFE/FPM.....................................16<br />

IP-B-V2-5600L-SN6..............................................299<br />

IP-B-VPS-mc.........................................................300<br />

IP-P-E1-2700M-VA/FKM-ea..................................291<br />

IP-P-LABDOS-AE.................................................280<br />

IP-P-LABDOS-AE.................................................274<br />

IP-P-LABDOS-DISPENS......................................274<br />

IP-P-LABDOS-DISPPB.........................................275<br />

IP-P-LABDOS-DISPPB.........................................274<br />

IP-P-LABDOS-DOMAS.........................................274<br />

IP-P-LABDOS-P-EASY-E......................................274<br />

IP-P-LABDOS-P-EASY-TC...................................274<br />

IP-P-LABDOS-P-EASYLOAD...............................274<br />

IP-P-LABDOS-P-MULTI-4-5..................................274<br />

IP-P-LABDOS-P-VARIO........................................274<br />

IP-P-LABDOS-P-VARIO-3....................................274<br />

IP-P-LABDOS-P-VARIO-3E..................................274<br />

IP-P-LABDOS-P-VARIO-4....................................274<br />

IP-P-LABDOS-P-VARIO-4E..................................274<br />

IP-P-LABDOS-P<strong>10</strong>0..............................................274<br />

IP-P-LABDOS-P30................................................274<br />

Order Codes<br />

IP-P-LABDOS-RS232BA......................................275<br />

IP-P-LABDOS-RS232BA......................................274<br />

IP-P-LABDOS-RS485...........................................280<br />

IP-P-LABDOS-RS485...........................................279<br />

IP-P-LABDOS-RS485...........................................275<br />

IP-P-LABDOS-RS485...........................................274<br />

IP-P-LABDOS-RS485BA......................................275<br />

IP-P-LABDOS-RS485BA......................................274<br />

IP-P-LABDOS-SK.................................................274<br />

IP-P-LABDOS-T-12...............................................280<br />

IP-P-LABDOS-T-2.................................................280<br />

IP-P-LABDOS-T-25...............................................280<br />

IP-P-LABDOS-T-50...............................................280<br />

IP-P-M1-1<strong>10</strong>0M-PTFE/C/KER-SN4/6-ea..............286<br />

IP-P-M2-<strong>10</strong>00M-PTFE/C/KER-SN4/6-ea..............288<br />

IP-P-M3-1800M-PTFE-SN4/6...............................289<br />

IP-P-N1-PK-mc.....................................................285<br />

IP-P-N1-PK-STRG-E.............................................285<br />

IP-P-N1-PK-STRG-VI............................................285<br />

IP-P-P1-0150M-PTFE/KER-SN17-ea...................287<br />

IP-P-P1-0150M-VA/KER-SN16-ea........................287<br />

IP-P-P3-0600M-VA/KER-SN16-ea........................290<br />

IP-P-R1-18M-HM-SN2-ea.....................................292<br />

IP-P-R1-9M-HM-SN2-ea.......................................292<br />

IP-P-R2-<strong>10</strong>152M-HM-SF1/8-ea............................293<br />

IP-P-R2-18M-HM-SF1/8-ea..................................293<br />

IP-P-R2-288M-HM-SF1/8-ea................................293<br />

IP-P-R2-72M-HM-SF1/8-ea..................................293<br />

IP-P-SM1-PP -mc..................................................283<br />

IP-P-SM1-PTFE -mc.............................................283<br />

IP-P-SM1-VA -mc..................................................283<br />

IP-P-Z1-018ML<strong>10</strong>B-E............................................279<br />

IP-P-Z1-070ML30B-E............................................279<br />

IP-P-Z1-280ML80B-E............................................279<br />

IP-P-Z1-HEAT.......................................................279<br />

IP-SYRDOS-VCER...............................................282<br />

IP-SYRDOS-VCER...............................................281<br />

IP-SYRDOS-VHPR...............................................282<br />

IP-SYRDOS-VHPR...............................................281<br />

IP-SYRDOS1........................................................281<br />

IP-SYRDOS1-ss-V2/3...........................................281<br />

IP-SYRDOS1-ss-VDxx..........................................281<br />

IP-SYRDOS1-ss-VNDyy.......................................281<br />

IP-SYRDOS2-ss-V2/3...........................................282<br />

IP-SYRDOS2-ss-VDxx..........................................282<br />

IP-SYRDOS2-ss-VNDyy.......................................282<br />

IR-DISPANTR1400...............................................332<br />

IR-DISPANTR350.................................................332<br />

IR-DISPANTR750.................................................332<br />

IR-DISPANTR850.................................................332<br />

IR-DISPWZ040.....................................................332<br />

IR-DISPWZ063.....................................................332<br />

IR-DISPWZ140.....................................................332<br />

IR-DISPWZ200-G.................................................332<br />

IR-DISPWZ40-F....................................................332<br />

IR-MINISTIRR<strong>10</strong>...................................................324<br />

IR-RBL-rt-rd-ws-wl-wd ..........................................330<br />

IR-RDFMAG<strong>10</strong>......................................................328<br />

IR-RDFMAG8........................................................328<br />

IR-RDFMAG8..........................................................16<br />

IR-VIPA-MINI-RHEO-35........................................324<br />

IR-VIPA-MINI-RHEO-35..........................................19<br />

IR-VIPA-MINI-RHEO-35..........................................16<br />

IR-VIPA1<strong>10</strong>............................................................321<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 341


342<br />

IR-VIPA27..............................................................321<br />

IR-VIPA57..............................................................321<br />

IR-VIPARH1<strong>10</strong>.......................................................322<br />

IR-VIPARH16........................................................322<br />

IR-VIPARH27........................................................322<br />

IR-VIPARH57........................................................322<br />

IR-VIPARHP150....................................................323<br />

IR-VIPARHP220....................................................323<br />

IR-VIPARHP40......................................................323<br />

IR-VIPARHP75......................................................323<br />

IR-VIPARHPRS485...............................................323<br />

IR-VIPARHPUI......................................................323<br />

IR-VIPARHX7........................................................322<br />

IR-VIPARK-BF-POM.............................................327<br />

IR-VIPARK-VK-POM.............................................327<br />

IR-VIPARS.............................................................322<br />

IR-VIPARS.............................................................321<br />

IR-VIPARWS.........................................................328<br />

IR-VIPARWV<strong>10</strong>0021.............................................328<br />

IR-VIPARWV<strong>10</strong>0029.............................................328<br />

IR-VIPARWV15019...............................................328<br />

IR-VIPARWV45020...............................................328<br />

IR-VIPARWV45028...............................................328<br />

IR-VIPASFG..........................................................328<br />

IR-VISCOTROL-FAN............................................326<br />

IR-VISCOTROL-FAN............................................325<br />

IR-VISCOTROL-MOT055.....................................325<br />

IR-VISCOTROL-MOT075.....................................326<br />

IR-VISCOTROL-MOT075.....................................325<br />

IR-VISCOTROL-MOT1<strong>10</strong>......................................326<br />

IR-VISCOTROL-MOT1<strong>10</strong>......................................325<br />

IR-VISCOTROL-MOT150.....................................325<br />

IR-VISCOTROL-MOT300.....................................325<br />

IR-VISCOTROL1<strong>10</strong>0.............................................325<br />

IR-VISCOTROL2200.............................................325<br />

IR-VISCOTROL350...............................................325<br />

IR-VISCOTROL350-RHEO...................................326<br />

IR-VISCOTROL550...............................................325<br />

IR-VISCOTROL550-RHEO...................................326<br />

IR-VISCOTROL750-RHEO...................................326<br />

IR-VPMONT2........................................................326<br />

IS-F-0000.P.X.P.01.CX..........................................242<br />

IS-F-0045.P.H.0.00.CX..........................................242<br />

IS-F-0045.P.X.P.01.DL..........................................241<br />

IS-F-0045.P.X.P.01.DL..........................................241<br />

IS-F-0045.P.X.P.01.DX..........................................241<br />

IS-F-0045.P.X.P.01.DX..........................................241<br />

IS-F-0045.S.B.P.01.XX..........................................242<br />

IS-F-0045.S.N.P.01.XX.........................................242<br />

IS-F-0045.T.H.0.00.DX..........................................241<br />

IS-F-0045.T.H.0.00.DX..........................................241<br />

IS-F-0045.T.H.P.01.DL..........................................241<br />

IS-F-0045.T.H.P.01.DX..........................................241<br />

IS-F-0045.T.H.P.01.XL..........................................242<br />

IS-F-0045.T.H.P.01.XX..........................................242<br />

IS-F-0045.T.N.0.00.DX..........................................241<br />

IS-F-0045.T.N.0.00.DX..........................................241<br />

IS-F-0045.T.N.P.01.DL..........................................241<br />

IS-F-0045.T.N.P.01.DX..........................................241<br />

IS-F-0045.T.N.P.01.XL..........................................242<br />

IS-F-0045.T.N.P.01.XX..........................................242<br />

IS-F-0045.X.X.X.00.CX.........................................242<br />

IS-F-0085.P.H.0.00.CX..........................................242<br />

IS-F-0085.P.H.P.01.CX..........................................242<br />

Order Codes<br />

IS-F-0085.P.X.P.01.DL..........................................241<br />

IS-F-0085.P.X.P.01.DL..........................................241<br />

IS-F-0085.P.X.P.01.DX..........................................241<br />

IS-F-0085.P.X.P.01.DX..........................................241<br />

IS-F-0085.S.B.P.01.XX..........................................242<br />

IS-F-0085.S.N.P.01.XX.........................................242<br />

IS-F-0085.T.H.0.00.DX..........................................241<br />

IS-F-0085.T.H.0.00.DX..........................................241<br />

IS-F-0085.T.H.P.01.DL..........................................241<br />

IS-F-0085.T.H.P.01.DX..........................................241<br />

IS-F-0085.T.H.P.01.XL..........................................242<br />

IS-F-0085.T.H.P.01.XX..........................................242<br />

IS-F-0085.T.N.0.00.DX..........................................241<br />

IS-F-0085.T.N.0.00.DX..........................................241<br />

IS-F-0085.T.N.P.01.DL..........................................241<br />

IS-F-0085.T.N.P.01.DX..........................................241<br />

IS-F-0085.T.N.P.01.XL..........................................242<br />

IS-F-0085.T.N.P.01.XX..........................................242<br />

IS-F-0085.X.X.X.00.CX.........................................242<br />

IS-F-0125.S.B.P.01.XX..........................................242<br />

IS-F-0125.S.N.P.01.XX.........................................242<br />

IS-F-0125.T.B.P.01.XX..........................................242<br />

IS-F-0125.T.N.P.01.XL..........................................242<br />

IS-F-6300.BA.CON.DC.XX...................................243<br />

IS-F-6700-DA-CON-DC........................................244<br />

IS-F-LABTUC........................................................243<br />

IS-F-S601-P2........................................................242<br />

IS-F-S601-P20......................................................242<br />

IS-F-S601-P40......................................................242<br />

IS-F-TDMMV-AK-F..................................................35<br />

IS-F-TDMMV-AK-I...................................................35<br />

IS-F-TDMtc-tb-sa..................................................245<br />

IS-F-TDMtc-tb-sa....................................................35<br />

IS-FM-L30 0,0.......................................................246<br />

IS-FM-L30C2I........................................................246<br />

IS-FM-L30C5.........................................................246<br />

IS-FM-M12............................................................248<br />

IS-FM-M12V1NI....................................................248<br />

IS-FM-M13............................................................248<br />

IS-FM-M13V1NI....................................................248<br />

IS-FM-M14............................................................248<br />

IS-FM-M14V1NI....................................................248<br />

IS-FV-GAS-DISP...................................................249<br />

IS-FV-GAS-IG.......................................................249<br />

IS-FV-GAS-IGEX...................................................249<br />

IS-FV-GAS-MAN...................................................249<br />

IS-FV-GAS-tc-au...................................................249<br />

IS-FV-GAS-THG....................................................249<br />

IS-FV-GAS-THS....................................................249<br />

IS-G-IND1..............................................................254<br />

IS-G-REFL1..........................................................254<br />

IS-L-FA-ea.............................................................236<br />

IS-M-FEU1............................................................254<br />

IS-MOLECULEEYE...............................................228<br />

IS-MOLECULEEYEMUX......................................228<br />

IS-P-A-025-ma-ea.................................................251<br />

IS-P-A-1,6-ma-ea..................................................251<br />

IS-P-A-2,5-ma-ea..................................................251<br />

IS-P-A-6-ma-ea.....................................................251<br />

IS-P-R-6-ma-ea.....................................................251<br />

IS-P-TUBE-sd.......................................................253<br />

IS-P-Z-AA..............................................................252<br />

IS-P-Z-AA..............................................................251<br />

IS-PARTICLEYE- 2D-l...........................................232<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


IS-PARTICLEYE- 3D-l-t........................................232<br />

IS-PARTICLEYE- WV...........................................232<br />

IS-PARTICLEYE-AA6...........................................232<br />

IS-PARTICLEYE-EEX...........................................232<br />

IS-PARTICLEYE-S- l.............................................232<br />

IS-PTOT-A-16-ea..................................................252<br />

IS-PTOT-R-16-ea..................................................252<br />

IS-T-NICRNI-d-l.....................................................250<br />

IS-T-PT<strong>10</strong>0 1/5-VA-d-l...........................................250<br />

IS-T-PT<strong>10</strong>0-1/1-VA -d-l..........................................250<br />

IS-T-PT<strong>10</strong>0-1/1-VA-d-l...........................................250<br />

IS-T-PT<strong>10</strong>0-1/<strong>10</strong>-VA-d-l.........................................250<br />

IS-T-PT<strong>10</strong>0-1/3-VA-d-l...........................................250<br />

IS-T-PT<strong>10</strong>003B.......................................................90<br />

IS-T-PT<strong>10</strong>015G.......................................................90<br />

IS-T-PTKAL.............................................................90<br />

IS-TRUB-O-ea.......................................................233<br />

IS-TRUB-ORF-ea..................................................234<br />

IS-W-GRAVICRANE.............................................267<br />

IS-W-GRAVICRANE.............................................207<br />

IS-W-GRAVIPLATE...............................................267<br />

IS-W-GRAVIPLATE...............................................207<br />

IS-W-GRAVISTAND..............................................267<br />

IS-W-GRAVISTAND..............................................207<br />

IS-W-KMZ<strong>10</strong>00......................................................255<br />

IS-W-KMZ<strong>10</strong>00D...................................................255<br />

IS-W-KMZ<strong>10</strong>00k....................................................255<br />

IS-W-KMZ<strong>10</strong>0k......................................................255<br />

IS-W-KMZ15000...................................................255<br />

IS-W-KMZ15000D.................................................255<br />

IS-W-KMZ200k......................................................255<br />

IS-W-KMZ3000......................................................255<br />

IS-W-KMZ30000...................................................255<br />

IS-W-KMZ30000D.................................................255<br />

IS-W-KMZ3000D...................................................255<br />

IS-W-KMZ500k......................................................255<br />

IS-W-KMZ50k........................................................255<br />

IS-W-KMZ7500......................................................255<br />

IS-W-KMZ7500D...................................................255<br />

IV-DRUMIN16/1......................................................16<br />

IV-MB-FK1-2-1,5-UNF-ea.....................................268<br />

IV-MB-FK1-2-1,5-UNF-ea.....................................267<br />

IV-MB-FK1-2-1,6-GMG1/8-ea...............................216<br />

IV-MB-FK1-3-1,6-GMG1/8-ea...............................216<br />

IV-MB-FK2-2-1,5-UNF-ea.....................................216<br />

IV-MB-FK2-2-nw-ma-ea........................................217<br />

IV-MB-FK2-3-1,5-UNF-ea.....................................216<br />

IV-MB-FK2-3-nw-ma-ea........................................217<br />

IV-MB-GM1-2-nw-ma-ea.......................................218<br />

IV-MB-UM1-2-3-ma-ea..........................................219<br />

IV-MB-UM1-3-3-ma-ea..........................................219<br />

IV-MB-UM2-2........................................................267<br />

IV-MB-UM2-2........................................................219<br />

IV-MB-UM2-PS......................................................267<br />

IV-MB-UM2-PS......................................................219<br />

IV-MP-ELBU1........................................................222<br />

IV-MP-ELBU2........................................................222<br />

IV-MP-UG1-2-6-ma-ea..........................................222<br />

IV-MP-UK1-2-0,8-ma-ea.......................................267<br />

IV-MP-UK1-2-0,8-ma-ea.......................................222<br />

IV-MP-UM1-2-2-ma-ea..........................................222<br />

IV-MP-UM2-2-4-ma-ea..........................................222<br />

IV-MW1-wa-ma-ea................................................223<br />

IV-MW2-wa-1/4.....................................................223<br />

Order Codes<br />

IV-PB-FG1-2-15-ma-ea.........................................219<br />

IV-PB-FG2-2-15-ma-ea.........................................219<br />

IV-PB-FG3-3-20-ma-ea.........................................219<br />

IV-PP-FG1-3-20-ma-ea.........................................222<br />

IV-PP-UG1-2-13-ma-ea.........................................222<br />

IV-PP-UX1-2-ma-ea-kv.........................................222<br />

IW- GRAVIPF15000..............................................207<br />

IW- GRAVIPF3000................................................207<br />

IW- GRAVIPF7000................................................207<br />

IW-572-35..............................................................208<br />

IW-572-49..............................................................208<br />

IW-GRAVIREAKW.................................................208<br />

IW-GRAVITS<strong>10</strong>00.................................................207<br />

IW-GRAVITS<strong>10</strong>00D...............................................206<br />

IW-GRAVITS15000...............................................206<br />

IW-GRAVITS15000D............................................206<br />

IW-GRAVITS3000.................................................207<br />

IW-GRAVITS3000.................................................206<br />

IW-GRAVITS30000...............................................206<br />

IW-GRAVITS30000D............................................206<br />

IW-GRAVITS3000D...............................................206<br />

IW-GRAVITS7500.................................................207<br />

IW-GRAVITS7500.................................................206<br />

IW-GRAVITS7500D...............................................206<br />

IW-LP4200S..........................................................209<br />

IW-ME414S...........................................................209<br />

IW-PLS 4000-2......................................................208<br />

IW-PLS 5<strong>10</strong>-3........................................................208<br />

IW-QKE 36K0.5.....................................................208<br />

L-SONSCHR-1......................................................212<br />

LB-LABBOX1B........................................................77<br />

LB-LABBOX2B........................................................78<br />

LB-LABMAN1B.......................................................80<br />

LB-LABMAN2B.......................................................81<br />

LG-LABBOX1..........................................................72<br />

LG-LABBOX2-1.......................................................73<br />

LG-LABBOX2-2.......................................................73<br />

LG-LABMAN1.........................................................74<br />

LK-LABBOX1K........................................................69<br />

LK-LABBOX2K-1.....................................................70<br />

LK-LABBOX2K-2.....................................................70<br />

LK-LABMAN1K.......................................................71<br />

LP-AAP8UI..............................................................94<br />

LP-AE4PT4P...........................................................91<br />

LP-AE4PT4PA.........................................................91<br />

LP-AEAP8I..............................................................95<br />

LP-AEAP8IA............................................................95<br />

LP-AEAP8U.............................................................95<br />

LP-AEAP8UA..........................................................95<br />

LP-AEP8..................................................................88<br />

LP-AEP8A...............................................................89<br />

LP-DAP8.................................................................98<br />

LP-DAP8A...............................................................99<br />

LP-DAP8T.............................................................<strong>10</strong>0<br />

LP-DE4DA4P........................................................<strong>10</strong>0<br />

LP-DE4DA4PA......................................................<strong>10</strong>1<br />

LP-DEP8.................................................................96<br />

LP-DEP8A...............................................................97<br />

LP-DMS4DA4PT...................................................267<br />

LP-DMS8.................................................................93<br />

LP-DMSP8............................................................267<br />

LP-LP-DA4HZ4PA.................................................<strong>10</strong>1<br />

LP-PEAP...............................................................<strong>10</strong>4<br />

LP-PEAPSK15......................................................<strong>10</strong>4<br />

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344<br />

LP-PEAPSK24......................................................<strong>10</strong>4<br />

LP-PHRED24..........................................................92<br />

LP-PHRED24B........................................................92<br />

LP-PTP8..................................................................89<br />

LP-PTPRP8...........................................................124<br />

LP-PTPRP8.............................................................90<br />

LP-SER99.............................................................<strong>10</strong>2<br />

LP-THP8..................................................................92<br />

LZ-AKLES1.............................................................93<br />

LZ-AKLES1.............................................................93<br />

LZ-AKLES1.............................................................92<br />

LZ-AKLES1.............................................................90<br />

LZ-AKLES1.............................................................89<br />

LZ-AKPH.................................................................92<br />

LZ-AKRS9.............................................................<strong>10</strong>2<br />

LZ-AKTUB.............................................................<strong>10</strong>1<br />

LZ-AKTUB.............................................................<strong>10</strong>1<br />

LZ-AKTUB.............................................................<strong>10</strong>0<br />

LZ-AKTUB...............................................................97<br />

LZ-AKTUB...............................................................96<br />

LZ-AKTUB...............................................................89<br />

LZ-AKTUB...............................................................88<br />

LZ-AKTUB ..............................................................95<br />

LZ-AKTUB ..............................................................94<br />

LZ-AKTUB ..............................................................93<br />

LZ-AKTUS.............................................................<strong>10</strong>1<br />

LZ-AKTUS.............................................................<strong>10</strong>0<br />

LZ-AKTUS.............................................................<strong>10</strong>0<br />

LZ-AKTUS...............................................................99<br />

LZ-AKTUS...............................................................98<br />

LZ-BEFW19.............................................................83<br />

LZ-GRIFFLU............................................................83<br />

LZ-GRIFFRO...........................................................83<br />

LZ-PR19Z3HE.........................................................82<br />

LZ-PR7....................................................................82<br />

LZ-PRx....................................................................82<br />

LZ-USTAT5M...........................................................82<br />

LZ-USTAT6..............................................................82<br />

LZ-USTAT7..............................................................82<br />

MB-AAB8UI...........................................................118<br />

MB-AEB16VP........................................................118<br />

MB-DAB8R............................................................119<br />

MB-DAB8T_0.5A...................................................120<br />

MB-DEB8...............................................................119<br />

MG-MSRBOX1......................................................117<br />

MG-MSRBOX2......................................................117<br />

MG-MSRBOX2s....................................................117<br />

MG-MSRMAN .......................................................115<br />

P-USV7O...............................................................137<br />

SA-GYRODAT.......................................................335<br />

SA-KALDAS3..........................................................33<br />

SA-KALDAS3..........................................................31<br />

SA-KALDAS3..........................................................29<br />

SA-P-LABDOS-DOMAS.......................................275<br />

SA-P-LABDOS-DOMASM....................................275<br />

SD-HIBUILDER ....................................................191<br />

SF-ANWTAB.........................................................179<br />

SF-ANWTAB.........................................................179<br />

SF-ANWTAB.........................................................178<br />

SF-ANWTAB.........................................................178<br />

SF-ANWTAB.........................................................178<br />

SF-ANWTAB.........................................................177<br />

SF-ANWTAB.........................................................177<br />

SF-ANWTAB.........................................................177<br />

Order Codes<br />

SF-ANWTAB.........................................................146<br />

SF-ANWTAB ........................................................189<br />

SF-AWL.................................................................146<br />

SF-AWL ................................................................188<br />

SF-AWLPLUS.......................................................188<br />

SF-AWLPLUS.......................................................146<br />

SF-DATLOG..........................................................179<br />

SF-DATLOG..........................................................179<br />

SF-DATLOG..........................................................178<br />

SF-DATLOG..........................................................178<br />

SF-DATLOG..........................................................178<br />

SF-DATLOG..........................................................177<br />

SF-DATLOG..........................................................177<br />

SF-DATLOG..........................................................177<br />

SF-DATLOG..........................................................146<br />

SF-DATLOG .........................................................189<br />

SF-HICON ............................................................186<br />

SF-HICONx...........................................................146<br />

SF-HITUNE...........................................................178<br />

SF-HITUNE...........................................................146<br />

SF-HITUNE ..........................................................185<br />

SF-HITUNE ..........................................................179<br />

SF-HITUNE ..........................................................179<br />

SF-NAMSER128...................................................189<br />

SF-NAMSER16.....................................................189<br />

SF-NAMSER32.....................................................189<br />

SF-NAMSER4.......................................................189<br />

SF-NAMSER4.......................................................179<br />

SF-NAMSER4.......................................................179<br />

SF-NAMSER4.......................................................178<br />

SF-NAMSER4.......................................................178<br />

SF-NAMSER4.......................................................178<br />

SF-NAMSER4.......................................................177<br />

SF-NAMSER4.......................................................177<br />

SF-NAMSER4.......................................................177<br />

SF-NAMSER64.....................................................189<br />

SF-NAMSER8.......................................................189<br />

SF-NAMSERxx.....................................................146<br />

SF-PID16...............................................................185<br />

SF-PID16 ..............................................................177<br />

SF-PID16 .............................................................179<br />

SF-PID24...............................................................185<br />

SF-PID32...............................................................185<br />

SF-PID4.................................................................177<br />

SF-PID4...................................................................16<br />

SF-PID4.....................................................................7<br />

SF-PID4 ................................................................185<br />

SF-PID4 ...............................................................178<br />

SF-PID4 ...............................................................178<br />

SF-PID8.................................................................185<br />

SF-PID8.................................................................177<br />

SF-PID8...................................................................31<br />

SF-PID8...................................................................29<br />

SF-PID8.....................................................................9<br />

SF-PID8 ...............................................................179<br />

SF-PID8 ...............................................................178<br />

SF-PIDxx...............................................................146<br />

SF-PNKMSR.........................................................146<br />

SL-ACTIONTRACK...............................................163<br />

SL-ACTIONTRACK...............................................145<br />

SL-ALRRUF..........................................................158<br />

SL-ALRRUF..........................................................145<br />

SL-ANWINT..........................................................174<br />

SL-ANWINT..........................................................145<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


SL-BENRECH.......................................................173<br />

SL-BENRECH.......................................................145<br />

SL-BERICHT.........................................................165<br />

SL-BERICHT.........................................................149<br />

SL-BERICHT.........................................................145<br />

SL-BIBRILK...........................................................192<br />

SL-BIBRILK...........................................................156<br />

SL-BIBRILK...........................................................146<br />

SL-CLONLV ..........................................................145<br />

SL-DESIGN...........................................................152<br />

SL-DESIGN...........................................................145<br />

SL-DESIGNL.........................................................152<br />

SL-DESIGNL.........................................................146<br />

SL-DIAPROT.........................................................161<br />

SL-DIAPROT.........................................................145<br />

SL-EASYBATCH...................................................163<br />

SL-EASYBATCH...................................................145<br />

SL-EMLRUF..........................................................159<br />

SL-EMLRUF..........................................................145<br />

SL-EXPORT..........................................................172<br />

SL-EXPORT..........................................................145<br />

SL-FREMDPNK....................................................174<br />

SL-FREMDPNK....................................................174<br />

SL-FREMDPNK....................................................146<br />

SL-GOPBEFUEL...................................................167<br />

SL-GOPBIB...........................................................166<br />

SL-GOPBIB...........................................................165<br />

SL-GOPBIB...........................................................146<br />

SL-GOPBIBL.........................................................166<br />

SL-GOPBIBL.........................................................165<br />

SL-GOPDEST.......................................................167<br />

SL-GOPDOSI........................................................167<br />

SL-GOPDOSIGRAVI1...........................................267<br />

SL-GOPDOSIGRAVI1...........................................167<br />

SL-GOPDPWERT.................................................167<br />

SL-GOPDRUCK....................................................167<br />

SL-GOPDRUCKHALTEN......................................167<br />

SL-GOPEINWIEG.................................................167<br />

SL-GOPEND.........................................................167<br />

SL-GOPGRAVITARI..............................................267<br />

SL-GOPGRAVITARI..............................................167<br />

SL-GOPINERT......................................................167<br />

SL-GOPINERTHERST..........................................167<br />

SL-GOPKALOHEIZ...............................................167<br />

SL-GOPKALOONL ...............................................167<br />

SL-GOPKONTIDOS..............................................167<br />

SL-GOPMENGENDOS.........................................167<br />

SL-GOPPHREGELUNG.......................................167<br />

SL-GOPPROGRAMM...........................................167<br />

SL-GOPRATENDOS.............................................167<br />

SL-GOPREKTIF....................................................167<br />

SL-GOPRUECKDEST..........................................167<br />

SL-GOPRUEHR....................................................167<br />

SL-GOPSIEDEP...................................................167<br />

SL-GOPSTART.....................................................168<br />

SL-GOPSTOSSDOS.............................................168<br />

SL-GOPTEMP.......................................................168<br />

SL-GOPTEMPHALTEN.........................................168<br />

SL-GOPVAKHALTEN............................................168<br />

SL-GOPVAKU.......................................................168<br />

SL-GOPWAAGETARI...........................................168<br />

SL-GOPWARTET..................................................168<br />

SL-GOPWARTEZ..................................................168<br />

SL-GOPWBEDIENER...........................................168<br />

Order Codes<br />

SL-GOPWBEDINGUNG.......................................168<br />

SL-GOPWIEDERH................................................168<br />

SL-HIBATCH.........................................................165<br />

SL-HIBATCH.........................................................145<br />

SL-HIBATCHAP....................................................165<br />

SL-HIBATCHL.......................................................165<br />

SL-HIBATCHL.......................................................146<br />

SL-HIBATCHRT....................................................165<br />

SL-HILIMS.............................................................165<br />

SL-HILIMS.............................................................145<br />

SL-HILIMSL...........................................................165<br />

SL-HILIMSL...........................................................146<br />

SL-HILIMSSQL.....................................................145<br />

SL-HITEXT............................................................160<br />

SL-HITEXT............................................................145<br />

SL-HITEXTL..........................................................160<br />

SL-HITEXTL..........................................................146<br />

SL-JOURNAL........................................................171<br />

SL-JOURNAL........................................................165<br />

SL-JOURNAL........................................................145<br />

SL-KALDAS3........................................................145<br />

SL-LABCAM..........................................................158<br />

SL-LABCAM..........................................................145<br />

SL-LABVIPBAT.....................................................179<br />

SL-LABVIPBAT.......................................................71<br />

SL-LABVIPBAT.......................................................16<br />

SL-LABVIPBATE.....................................................31<br />

SL-LABVIPBATE.....................................................29<br />

SL-LABVIPBATE ..................................................178<br />

SL-LABVIPBATE ......................................................9<br />

SL-LABVIPBATL.....................................................70<br />

SL-LABVIPBATL.......................................................7<br />

SL-LABVIPBATL .................................................178<br />

SL-LABVIPBATP ..................................................179<br />

SL-LABVIPEASY .................................................178<br />

SL-LABVIPKON....................................................177<br />

SL-LABVIPKON......................................................71<br />

SL-LABVIPKONL..................................................177<br />

SL-LABVIPKONL....................................................70<br />

SL-LABVIPKONP..................................................177<br />

SL-LABVIS............................................................147<br />

SL-LABVIS..............................................................69<br />

SL-LABVOICE.......................................................145<br />

SL-LIQUIM............................................................316<br />

SL-LIQUIML..........................................................316<br />

SL-MICROBIB ......................................................146<br />

SL-MODBIBALR...................................................155<br />

SL-MODBIBALR...................................................155<br />

SL-MODBIBALR...................................................146<br />

SL-MODBIBALRL.................................................155<br />

SL-MODBIBALRL.................................................155<br />

SL-MULTIBATCH..................................................169<br />

SL-MULTIBATCH..................................................145<br />

SL-MULTIBATCH....................................................16<br />

SL-MULTIPROJ....................................................173<br />

SL-MULTIPROJ....................................................145<br />

SL-ONLGRA.........................................................150<br />

SL-ONLGRA.........................................................145<br />

SL-ONLGRAL.......................................................150<br />

SL-ONLGRAL.......................................................146<br />

SL-PNKDDE..........................................................174<br />

SL-PNKDDE..........................................................146<br />

SL-PNKLASENTEC..............................................174<br />

SL-PNKLASENTEC..............................................146<br />

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346<br />

SL-PNKMBUSSER...............................................146<br />

SL-PNKMODBUS.................................................174<br />

SL-PNKMTRx........................................................174<br />

SL-PNKMTRx........................................................146<br />

SL-PNKNAMSERA...............................................189<br />

SL-PNKOPC.........................................................174<br />

SL-PNKOPC.........................................................146<br />

SL-PNKPERF........................................................174<br />

SL-PNKPERF........................................................146<br />

SL-PNKSIM...........................................................145<br />

SL-PNKSPS..........................................................174<br />

SL-PNKSPS..........................................................146<br />

SL-PROJMOD.......................................................155<br />

SL-PROJMOD ......................................................145<br />

SL-REZGEN..........................................................168<br />

SL-RICAD..............................................................192<br />

SL-RIEDIT.............................................................156<br />

SL-RIEDIT.............................................................145<br />

SL-RIEDITL...........................................................156<br />

SL-RIEDITL...........................................................146<br />

SL-SCHANA..........................................................148<br />

SL-SCHANA..........................................................145<br />

SL-SCHANAL........................................................148<br />

SL-SCHANAL........................................................146<br />

SL-SCHERE..........................................................165<br />

SL-SCHERE..........................................................149<br />

SL-SCHERE..........................................................145<br />

SL-SCHEREL........................................................149<br />

SL-SCHEREL........................................................146<br />

SL-SCHPHA..........................................................165<br />

SL-SCHPHA..........................................................149<br />

SL-SCHPHA..........................................................145<br />

SL-SCHPHAL........................................................149<br />

SL-SCHPHAL........................................................146<br />

SL-SELFIL.............................................................172<br />

SL-SELFIL.............................................................145<br />

SL-SWITCHER ....................................................145<br />

SL-TELES.............................................................175<br />

SL-UEBMEL..........................................................157<br />

SL-UEBMEL..........................................................145<br />

SL-VISCOGRAPH.................................................331<br />

SL-VISCOGRAPHAI.............................................331<br />

SL-VISCOGRAPHPT............................................331<br />

SL-WEBVIS...........................................................173<br />

SL-WEBVIS...........................................................145<br />

SL-WEBVISL.........................................................173<br />

SL-WEBVISL.........................................................146<br />

SP-RQFEED-AC.....................................................52<br />

VA-FESTBETT........................................................53<br />

VA-HIFERM-FCU....................................................44<br />

VA-OMNIFERM-AIRPUM........................................42<br />

VA-OMNIFERM-BGR..............................................42<br />

VA-OMNIFERM-CHILL...........................................42<br />

VA-OMNIFERM-COOL...........................................42<br />

VA-OMNIFERM-ETOH............................................42<br />

VA-OMNIFERM-FE-<strong>10</strong>00........................................42<br />

VA-OMNIFERM-FE-2000........................................42<br />

VA-OMNIFERM-FE-250..........................................42<br />

VA-OMNIFERM-FE-600..........................................42<br />

VA-OMNIFERM-FOAM...........................................42<br />

VA-OMNIFERM-FOLE............................................42<br />

VA-OMNIFERM-GAS1............................................42<br />

VA-OMNIFERM-GASMF.........................................42<br />

VA-OMNIFERM-GASMF2.......................................42<br />

Order Codes<br />

VA-OMNIFERM-GASMF4MUX...............................42<br />

VA-OMNIFERM-LEV...............................................42<br />

VA-OMNIFERM-REDOX.........................................42<br />

VA-OMNIFERM-RQFEED.......................................42<br />

VA-RAMOSCON8...................................................40<br />

VA-RAMOSCTR......................................................39<br />

VA-RAMOSFI1........................................................39<br />

VA-RAMOSFTT8.....................................................40<br />

VA-RAMOSINKSHA................................................39<br />

VA-RAMOSMK250..................................................39<br />

VA-RAMOSMKX......................................................39<br />

VA-RAMOSOTR......................................................39<br />

VA-RAMOSTKS4....................................................39<br />

VA-RAMOSTKSE....................................................39<br />

VL-BAVA-GKB.......................................................2<strong>10</strong><br />

VL-BAVA-HWS<strong>10</strong>..................................................2<strong>10</strong><br />

VL-BAVA-HWS20..................................................2<strong>10</strong><br />

VL-BAVA-HWST....................................................2<strong>10</strong><br />

VL-BAVA-NOR<strong>10</strong>..................................................2<strong>10</strong><br />

VL-BAVA-NOR15..................................................2<strong>10</strong><br />

VL-BAVA-NOR25..................................................2<strong>10</strong><br />

VL-BAVM-GKB......................................................2<strong>10</strong><br />

VL-EDDEST............................................................21<br />

VL-EDDOSFL..........................................................21<br />

VL-EDDOSPU.........................................................21<br />

VL-EDSIM...............................................................21<br />

VL-EDUQUIP..........................................................21<br />

VL-EDVAK...............................................................21<br />

VL-HICLAVE-ABKPNK1..........................................12<br />

VL-HICLAVE-ABKPNK2..........................................12<br />

VL-HICLAVE-ABKPNK4..........................................12<br />

VL-HICLAVE-COOLP..............................................12<br />

VL-HICLAVE-GRAVI150.........................................12<br />

VL-HICLAVE-HEABAN-vol......................................12<br />

VL-HICLAVE-HYDR................................................12<br />

VL-HICLAVE-MAGHEAT.........................................12<br />

VL-HICLAVE-SC-n..................................................12<br />

VL-HICLAVE-STIRR-20..........................................12<br />

VL-HICLAVE-STIRR-50..........................................12<br />

VL-HICLAVE-ws-vol................................................12<br />

VL-KB-FK2-UM1...................................................217<br />

VL-KB-MB-FK1.....................................................268<br />

VL-KB-MB-FK1.....................................................267<br />

VL-KB-MB-FK1.....................................................216<br />

VL-KB-MB-GM1....................................................218<br />

VL-KB-MB-UM2....................................................267<br />

VL-KB-MB-UM2....................................................219<br />

VL-LABKIT-SP........................................................22<br />

VL-LABKIT-SP-FOCON..........................................22<br />

VL-LABKIT-SP-PHCON..........................................22<br />

VL-LABKITALR1........................................................7<br />

VL-LABKITALR2........................................................9<br />

VL-LABKITALR2-AWE..............................................9<br />

VL-LABKITALR2-RFT...............................................9<br />

VL-LABKITED.........................................................21<br />

VL-LABKITRCB1.....................................................31<br />

VL-LABKITRCF1.....................................................29<br />

VL-LABKITRCMDM................................................31<br />

VL-LABKITRCONLB...............................................31<br />

VL-LABKITRCONLF...............................................29<br />

VL-MINILAB-BU......................................................19<br />

VL-MINILAB-GRV125.............................................19<br />

VL-MINILAB-GRV250.............................................19<br />

VL-MINILAB-GRV75...............................................19<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


VL-MULTILAB-ABKPNK1.......................................16<br />

VL-MULTILAB-ABKPNK2.......................................16<br />

VL-MULTILAB-ABKPNK4.......................................16<br />

VL-MULTILAB-ABKPNK6.......................................16<br />

VL-MULTILAB-ABKPNK8.......................................16<br />

VL-MULTILAB-BU...................................................16<br />

VL-MULTILAB-CHILL-20.........................................16<br />

VL-MULTILAB-CHILL-40.........................................16<br />

VL-MULTILAB-CHILL-60.........................................16<br />

VL-MULTILAB-DEST..............................................16<br />

VL-MULTILAB-GRAVI500ml...................................16<br />

VL-MULTILAB-GRV250..........................................16<br />

VL-MULTILAB-GRV400..........................................16<br />

VL-MULTILAB-INERT.............................................16<br />

VL-MULTILAB-REKT ..............................................16<br />

VL-MULTILAB-RFC ................................................16<br />

VL-MULTILAB-VAKU...............................................16<br />

VL-SOLIDOS-BIN.................................................2<strong>10</strong><br />

W-GRAVIPF30000................................................207<br />

ZH-ALFADOS........................................................338<br />

ZH-AUTOSAM.......................................................338<br />

ZH-GRAVIDOS......................................................338<br />

ZH-GYRODAT ......................................................338<br />

ZH-HIBUILDER ....................................................338<br />

ZH-HICON ............................................................338<br />

ZH-KALDAS .........................................................338<br />

ZH-LABDOS..........................................................338<br />

ZH-LABVIS ...........................................................338<br />

ZH-RAMOS ..........................................................338<br />

ZH-REGLER ........................................................338<br />

ZH-SOLIDOS .......................................................338<br />

ZH-VISCOPAKT ...................................................338<br />

ZK-HM-HI01-OD-XA-I-01......................................212<br />

ZK-IT-HI01-BS-R2-I-03.........................................304<br />

ZK-IT-HI01-BS-R2-I-03.........................................283<br />

ZK-IT-HI01-BS-R2-I-03.........................................282<br />

ZK-IT-HI01-BS-R2-I-03.........................................281<br />

Order Codes<br />

ZK-IT-HI01-BS-R2-I-03.........................................280<br />

ZK-IT-HI01-BS-R2-I-03.........................................279<br />

ZK-LAB-HI01-IA-IA-O-01 .......................................89<br />

ZK-LAB-HI01-IA-IA-O-02........................................89<br />

ZK-LAB-HI01-IA-IP-O-01........................................89<br />

ZK-LAB-HI01-IA-IP-O-01........................................88<br />

ZK-LAB-HI01-IA-UA-O-01.......................................89<br />

ZK-LAB-HI01-IA-UP-O-01.......................................89<br />

ZK-LAB-HI01-IA-UP-O-01.......................................88<br />

ZK-LAB-HI06-OD-XX-I-01.....................................128<br />

ZK-LAB-HI99-IA-XA-Y-0.1.....................................254<br />

ZK-P-HI36-BS-R2-I-01..........................................275<br />

ZK-P-HI36-BS-R2-I-01..........................................274<br />

ZK-P-HI36-BS-R2-I-02..........................................275<br />

ZK-P-HI36-BS-R2-I-02..........................................274<br />

ZK-P-HI36-BS-R4-I-01..........................................275<br />

ZK-P-HI36-BS-R4-I-01..........................................274<br />

ZK-P-HI36-BS-R4-I-02..........................................275<br />

ZK-P-HI36-BS-R4-I-02..........................................274<br />

ZK-P-TL02-BS-R2-I-01.........................................289<br />

ZK-P-VB01-BS-R2-I-01.........................................300<br />

ZK-R-HI02-BA-IP-Y-02..........................................326<br />

ZK-R-HI02-BA-UP-Y-03........................................326<br />

ZK-R-HI02-BS-R2-I-01..........................................326<br />

ZK-R-HI30-BK-IX-Y-01..........................................325<br />

ZK-R-HI30-BS-R4-I-01..........................................325<br />

ZK-R-HI31-BK-IA-Y-01..........................................326<br />

ZK-R-HI31-BK-IP-Y-01..........................................326<br />

ZK-SF-KM01-IA-IA-I-01.........................................245<br />

ZK-SF-KM01-ID-XA-I-01 ......................................245<br />

ZK-SFV-RI01-ID-XX-I-01......................................249<br />

ZK-W-KE04-BS-R2-I-02........................................208<br />

ZK-W-KE06-BS-R2-I-01........................................208<br />

ZK-W-SA01-BS-R2-I-03........................................209<br />

ZK-W-SA01-BS-R2-I-03........................................209<br />

ZK-X-HI05-IA-IA-O-01...........................................131<br />

ZK-X-HW01-OD-XA-I-01.......................................212<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 347


348<br />

Table of Content<br />

New in this Edition.............................................................................................................................................4<br />

Automatic Laboratory Reactor Systems..........................................................................................................5<br />

Standard Laboratory Reactor Systems..........................................................................................................................6<br />

Parallel Reactor Systems............................................................................................................................................13<br />

LabKit- Small Reactor Systems for Education..........................................................................................................20<br />

Automated Laboratory Clarification Unit .....................................................................................................................22<br />

Modular Micro-Reaction Technology............................................................................................................................23<br />

Reaction Calorimetry.......................................................................................................................................26<br />

Reaction Calorimeters.................................................................................................................................................27<br />

Calorimetry Evaluation Program KalDas.................................................................................................................32<br />

Components for Reaction Calorimetry.........................................................................................................................34<br />

Fermentation Technology...............................................................................................................................36<br />

RAMOS® Bioprocess Optimisation in Shaking Flasks ...............................................................................................37<br />

Feeding and Sample Drawing in Shaking Flasks ........................................................................................................40<br />

OmniFerm® - Mini Fermentation System....................................................................................................................41<br />

HiFerm-FCU Customer-specific Fermenter Control Systems .................................................................................43<br />

Gmix – Gas Mixing Device.......................................................................................................................................45<br />

AlcoTect Alcohol Probe ...........................................................................................................................................47<br />

OxyTect Optical Dissolved Oxygen Probe ...............................................................................................................48<br />

Autoclavable pH-Probe ...............................................................................................................................................48<br />

HiSense Emission Analysis System ........................................................................................................................49<br />

RQFeed Feeding Algorithm .....................................................................................................................................52<br />

Packed Bed Reactor ...................................................................................................................................................53<br />

Laboratory Automation Hardware..................................................................................................................54<br />

LabManager®-System.................................................................................................................................................55<br />

MSRmanager-System............................................................................................................................................112<br />

Interface Cards..........................................................................................................................................................121<br />

PI Additional Devices ................................................................................................................................................128<br />

Display and Operating Elements ..............................................................................................................................135<br />

Laboratory Automation Software.................................................................................................................141<br />

LabVision®................................................................................................................................................................142<br />

HiLIMS Laboratory Information Management-System...........................................................................................180<br />

PI-Firmware-Modules................................................................................................................................................184<br />

HiBuilder Data Evaluation and Presentation..........................................................................................................190<br />

RI-CAD the CAD-Software for P&ID-flow diagrams...............................................................................................192<br />

Plant Construction and Miniplant Technology............................................................................................193<br />

LabKit Custom Reaction Equipment ....................................................................................................................198<br />

Custom Parallel Reactor System...............................................................................................................................200<br />

Custom Reaction Calorimeters .................................................................................................................................201<br />

Formulation and Handling Stations ...........................................................................................................................203<br />

Equipment and Components........................................................................................................................205<br />

Laboratory Scales......................................................................................................................................................206<br />

Electrical Base Discharge Valves ............................................................................................................................2<strong>10</strong><br />

Automatic Liquid Phase Separation ..........................................................................................................................211<br />

Glass Components ...................................................................................................................................................212<br />

Low Pulsation Total Evaporator ................................................................................................................................213<br />

Valves and Stop-Cocks ............................................................................................................................................214<br />

Process Analytics and Sensors....................................................................................................................224<br />

30 Years of Excellence in Lab Scale Technology · Over 1.000 Products around the Laboratory Reactor


Table of Content<br />

MoleculeEye® ATR-FTIR-Spectroscopy....................................................................................................................225<br />

ParticleEye Particle Sizer.......................................................................................................................................229<br />

Turbidity Probe .........................................................................................................................................................233<br />

Fibre-Optic Submersible Reflection Probes ..............................................................................................................234<br />

Phase boundary Detector .........................................................................................................................................235<br />

Level Sensor..............................................................................................................................................................236<br />

Teflon® Flow Sensors ..............................................................................................................................................237<br />

Turbine Flow Sensor for Heat carrier Oil....................................................................................................................244<br />

Thermal Mass Flowmeters and Controllers ..............................................................................................................245<br />

Coriolis Mass Flowmeters and Controllers ...............................................................................................................247<br />

Laboratory Gas Counter............................................................................................................................................248<br />

Temperature Sensors ...............................................................................................................................................250<br />

Pressure Transmitters ...............................................................................................................................................251<br />

Hose Pressure Transmitter........................................................................................................................................253<br />

Humidity Sensors .....................................................................................................................................................254<br />

Distance and Rotational Speed Measurement..........................................................................................................254<br />

Weight Measuring and Load Cells ...........................................................................................................................255<br />

Monitors.....................................................................................................................................................................256<br />

Dosing Systems and Pumps.........................................................................................................................263<br />

Controlled Dropping Funnel GraviDos®....................................................................................................................264<br />

Controlled Dropping Funnel AlfaDos......................................................................................................................268<br />

Pumps, dosing pumps...............................................................................................................................................269<br />

Multi-Channel Dosing Systems .................................................................................................................................297<br />

Vacuum pumps..........................................................................................................................................................298<br />

Solid Matter Dosing System......................................................................................................................................301<br />

Liquid Handling and Autosampler................................................................................................................305<br />

Sample Drawing Systems and Pipetting Robots........................................................................................................306<br />

Stirring and Dispersing.................................................................................................................................319<br />

Measuring Stirrer ViscoPakt®....................................................................................................................................320<br />

ViscoTrol Control Unit for Three-Phase Stirrer Drive ............................................................................................325<br />

ViscoGraph – Automation of Stirring Tests ...........................................................................................................331<br />

Dispersing and Homogenising ..................................................................................................................................332<br />

Services..........................................................................................................................................................333<br />

<strong>HiTec</strong> <strong>Zang</strong> - Your competent Project Partner !..........................................................................................................334<br />

Customised Application Programs ............................................................................................................................335<br />

Seminars and Training ............................................................................................................................................336<br />

<strong>Main</strong>tenance Contracts ...........................................................................................................................................337<br />

Product Manuals ......................................................................................................................................................338<br />

<strong>HiTec</strong> <strong>Zang</strong> <strong>GmbH</strong> · Tel: +49(0)2407/9<strong>10</strong> <strong>10</strong>0 · info@hitec-zang.de · http://www.hitec-zang.com 349

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