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Petrochemical ASTM Standards ASTM D-5599 Oxygenates in Gas by GC & O-FID Oxygenates Calibration Curve with Internal Standard M-GRO-CAL/IS-SET M-GRO-CAL/IS-SET-PAK $ 250 / set of 8 x 1 mL $ 1,000 / 5 x (8 x 1) mL of 15 Comp. Mix Originally designed for D-5599-94 Every analyte in each solution is individually weighed Actual weights and weight percents are provided with all ASTM/EPA Solutions Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7 Std. 8 Calibration range Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Methanol 0.1 - 5.0 --- 0.1 2.5 --- 5 0.5 1 --- Ethanol 1.0 - 12.0 12 --- 3 --- 8 5 1 --- Isopropanol 0.1 - 2.0 2 1 --- 0.1 0.3 --- 0.5 --- t-Butanol 0.1 - 2.0 0.5 0.1 1 --- 2 0.3 --- --- Propanol 0.2 - 2.0 2 --- 0.7 0.2 1 --- 0.4 --- MtBE 1.0 - 17.0 5 17 --- --- 1 2.5 10 --- sec-Butanol 0.1 - 2.5 1 --- 0.5 0.1 --- 2.5 0.7 --- Diisopropyl ether 0.1 - 2.0 --- 0.5 0.3 0.1 2 1 --- --- iso-Butanol 0.1 - 2.0 2 0.5 --- 1 0.1 0.3 --- --- EtBE 1.0 - 18.0 --- 3.5 18 7.5 --- 1 12 --- t-Pentanol 0.1 - 2.0 0.3 1 --- 0.5 0.1 2 --- --- Butanol 0.1 - 2.0 1 --- 0.3 --- 0.5 0.1 2 --- TAME 1.0 - 18.0 --- 3.5 1 18 7.5 12 --- --- 1,2- Dimethoxyethane (ISTD) 4 4 4 4 4 4 4 --- RFA Gasoline 70.2 68.8 68.7 68.5 68.5 68.8 68.4 100 Total oxygenates & ISTD 29.8 31.2 31.3 31.5 31.5 31.2 31.6 0 Technical Note Oxygenate Calibration Curves ISTD-Free and Larger Packaging Size AccuStandard has received requests from the Petroleum Industry to formulate our D-5599 Oxygenate product without internal standard (ISTD) and package it in a larger volume. We have met those requests by introducing the M- GRO-CAL-SET calibration curve. This curve is manufactured without incorporating an internal standard and is packaged in Ready-to-Use 10 mL sample volume. The certified oxygenate calibration curve can be used in combination with other aromatic standards for combined oxygenate/aromatic analysis, to change the amount of internal standard added, or to incorporate alternative internal standard analytes. ASTM Standards Oxygenates Calibration Curve with Internal Standard M-GRO-CAL/IS-R1-SET$ 250 / set of 8 x 1 mL M-GRO-CAL/IS Analyte 01-R1 02-R1 03-R1 04-R1 05-R1 06-R1 07-R1 08-R1 Calibration range Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Methanol 0.1 - 5.0 -- 0.1 2.5 -- 5 0.5 1 -- Ethanol 1.0 - 12.0 12 -- 3 -- 8 5 1 -- Isopropanol 0.1 - 2.0 2 1 -- 0.1 0.3 -- 0.5 -- t-Butanol 0.1 - 2.0 0.5 0.1 1 -- 2 0.3 -- -- Propanol 0.2 - 2.0 2 -- 0.7 0.2 1 -- 0.4 -- MtBE 1.0 - 17.0 5 17 -- -- 1 2.5 10 -- sec-Butanol 0.1 - 2.5 1 -- 0.5 0.1 -- 2.5 0.7 -- Diisopropyl ether 0.1 - 2.0 -- 0.5 0.3 0.1 2 1 -- -- Isobutanol 0.1 - 2.0 2 0.5 -- 1 0.1 0.3 -- -- EtBE 1.0 - 18.0 -- 3.5 18 7.5 -- 1 12 -- tert-Pentanol 0.1 - 2.0 0.3 1 -- 0.5 0.1 2 -- -- Butanol 0.1 - 2.0 1 -- 0.3 -- 0.5 0.1 2 -- tAME 1.0 - 18.0 -- 3.5 1 18 7.5 12 -- -- 1,2-Dimethoxyethane (ISTD) 4 4 4 4 4 4 4 -- RFA Gasoline 74.2 72.8 72.7 72.5 72.5 72.8 72.4 100 NEW Oxygenates Calibration Curve without Internal Standard M-GRO-CAL-SET $ 850 / set of 8 x 10 mL of 14 Comp. Mix Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7 Std. 8 Calibration range Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Methanol 0.1 - 5.0 --- 0.1 2.5 --- 5 0.5 1 --- Ethanol 1.0 - 12.0 12 --- 3 --- 8 5 1 --- Isopropanol 0.1 - 2.0 2 1 --- 0.1 0.3 --- 0.5 --- t-Butanol 0.1 - 2.0 0.5 0.1 1 --- 2 0.3 --- --- Propanol 0.2 - 2.0 2 --- 0.7 0.2 1 --- 0.4 --- MtBE 1.0 - 17.0 5 17 --- --- 1 2.5 10 --- sec-Butanol 0.1 - 2.5 1 --- 0.5 0.1 --- 2.5 0.7 --- Diisopropyl ether 0.1 - 2.0 --- 0.5 0.3 0.1 2 1 --- --- iso-Butanol 0.1 - 2.0 2 0.5 --- 1 0.1 0.3 --- --- EtBE 1.0 - 18.0 --- 3.5 18 7.5 --- 1 12 --- t-Pentanol 0.1 - 2.0 0.3 1 --- 0.5 0.1 2 --- --- Butanol 0.1 - 2.0 1 --- 0.3 --- 0.5 0.1 2 --- TAME 1.0 - 18.0 --- 3.5 1 18 7.5 12 --- --- RFA Gasoline 74.2 64.8 64.7 64.5 64.5 64.8 64.4 100 D5599 Meets EPA Guidelines for RFG Analysis Technical Note AccuStandard’s M-GRO oxygenate calibration curve has been successfully used by Petroleum Refineries and supporting laboratories for both ASTM Method D-5599 and ASTM Method D-4815. In addition, AccuStandard’s certified oxygenate chemical reference materials provide the following features and benefits for superior performance and value. Total oxygenates 25.8 27.2 27.3 27.5 27.5 27.2 27.6 0 162 AccuStandard’s Quality System is Certified to comply with the International ISO 9001:2000 Quality Standard
Petrochemical ASTM Standards ASTM D-5599 (Continued) Oxygenates in Gas by GC & O-FID ASTM/EPA Oxygenate Quality Control Standards Originally designed for D-5599-95 D5599 Meets EPA Guidelines for RFG Analysis Daily Quality Control Standard (without Internal Standard) M-GRO-QC-10ML M-GRO-QC-10ML-PAK Compound Target Oxygenate Wt. % Methanol 1 Ethanol 1 Isopropanol 1 t-Butanol 1 Propanol 1 MtBE 3 sec-Butanol 1 Di-isopropyl ether 3 $ 100 / 1 x 10 mL SAVE $ 400 / 5 x 10 mL Compound Target Oxygenate Wt. % iso-Butanol 1 EtBE 3 t-Pentanol 1 Butanol 1 TAME 3 RFA Gasoline 79 14 comps. 100 Daily Quality Control Standard (with Internal Standard) M-GRO-QC/IS-5ML $ 75 / 1 x 5 mL M-GRO-QC/IS-5ML-PAK SAVE 27% $ 275 / 5 x 5 mL Revised Daily Quality Control Standard (without Internal Standard) M-GRO-QC-R-10ML M-GRO-QC-R-10ML-PAK Compound Target Oxygenate Wt. % Methanol 1 Ethanol 1 Isopropanol 1 t-Butanol 1 Propanol 1 MtBE 3 sec-Butanol 1 Di-isopropyl ether 1 $ 100 / 1 x 10 mL SAVE $ 400 / 5 x 10 mL Compound Target Oxygenate Wt. % iso-Butanol 1 EtBE 3 t-Pentanol 1 Butanol 1 TAME 3 RFA Gasoline 81 14 comps. 100 Revised Daily Quality Control Standard (with Internal Standard) M-GRO-QC-R/IS-5ML $ 75 / 1 x 5 mL M-GRO-QC-R/IS-5ML-PAK SAVE 27% $ 275 / 5 x 5 mL Technical Note The Daily Quality Control Standard M-GRO-QC-R was developed in response to your requests for a QC mix bracketed by the Calibration Curve. AccuStandard reduced the diisopropyl ether content from 3 Wt. % to 1 Wt. % to meet the method specifications. Compound Target Oxygenate Wt. % Methanol 1 Ethanol 1 Isopropanol 1 t-Butanol 1 Propanol 1 MtBE 3 sec-Butanol 1 Compound Target Oxygenate Wt. % Di-isopropyl ether 3 iso-Butanol 1 EtBE 3 t-Pentanol 1 Butanol 1 TAME 3 RFA Gasoline 79 15 comps. 100 1,2-Dimethoxyethane (ISTD) is combined with the above 14 comps. in a 4 to 100 weight ratio Compound Target Oxygenate Wt. % Methanol 1 Ethanol 1 Isopropanol 1 t-Butanol 1 Propanol 1 MtBE 3 sec-Butanol 1 Compound Target Oxygenate Wt. % Di-isopropyl ether 1 iso-Butanol 1 EtBE 3 t-Pentanol 1 Butanol 1 TAME 3 RFA Gasoline 81 1,2-Dimethoxyethane (ISTD) is combined with the above 14 comps. in a 4 to 100 weight ratio 15 comps. 100 ASTM Standards Gasoline Refinery Blank (with Internal Standard) M-GRO-BLNK/IS-10ML M-GRO-BLNK/IS-10ML-PAK Wt. % 1,2- Dimethoxyethane (ISTD) 4 RFA Gasoline 96 $ 15 / 1 x 10mL SAVE $ 60 / 5 x 10mL 2 comps. O-FID Gasoline Refinery Blank M-GRO-BLNK-10ML M-GRO-BLNK-10ML-PAK RFA Gasoline (neat) $ 10 / 1 x 10mL SAVE $ 40 / 5 x 10mL O-FID/EPA Gasoline Refinery Internal Standard M-GRO-IS-5ML $ 10 / 1 x 5 mL M-GRO-IS-5ML-PAK SAVE $ 40 / 5 x 5 mL 1,2- Dimethoxyethane (ISTD) Benefits from AccuStandard’s Oxygenates Features: Benefits: Analytes checked for chemical purity & water content The use & validation of the highest purity neats enhance the integrity of the standard. Analyzed by Independent Laboratories Certified method specific calibration standards Elimination of standards preparation Internal Standards incorporated Weights and weight percents provided All necessary solutions included Various sizes available Economical Independent product validation of certified values. Increased confidence in analytical results. Time is utilized quantifying samples. Ready-to-Inject Standards. Ease of use in performing back calculations. Provides single source for sample analysis. Meet laboratory sample volumes. Time is spent on analysis rather than preparing stds. 7 standards used to generate 5 point curve Generate a 5 point curve in 30% less time than competitors' 10 standard set. For MSDSs visit our website at www.AccuStandard.com 163
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PRINTED ON RECYCLED PAPER Table of
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AccuStandard, At Your Service Inter
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PCBs AccuStandard is known througho
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PCB Congeners Individual PCB Congen
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PCB Congeners EU Formulations PCB C
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PCB Congeners Mixtures for Congener
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PCB Congeners PCB Congener Calibrat
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PCB Metabolites & Derivatives Indiv
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Aroclors Individual Aroclors (in 1
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Flame Retardants Individual PBDEs S
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Flame Retardants Method 1614 Polybr
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Flame Retardants Other Flame Retard
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Dibenzofurans Individual Dibenzofur
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PAHs & Derivatives Individual PAHs
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Nitroaromatics Individual Nitroarom
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Aliphatic & Aromatic Amines & Deriv
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Nitrogen Containing Compounds Nitro
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Pesticides & Herbicides Pesticides,
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Pesticides & Herbicides The followi
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Pesticides & Herbicides Method 531
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Volatiles Volatile Organic Compound
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Volatiles Volatiles (in 1 mL of sol
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Volatiles Chlorinated Organic Volat
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Volatiles USEPA Method 503.1 Purgea
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Volatiles USEPA Method 8010, 8010A
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Volatiles USEPA Method 8021B Purgea
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Volatiles USEPA Method 8240 & 8260
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Volatiles VOC Selected Target Compo
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Phenols & Derivatives Phenols & Der
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Phenols & Derivatives Method 8040A
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Alcohols Alcohols (in 1 mL of solve
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