Chemical Reference Standards AccuStandard®
Chemical Reference Standards AccuStandard®
Chemical Reference Standards AccuStandard®
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Petrochemical ASTM <strong>Standards</strong><br />
ASTM D-5599 EPA Gasoline Refinery Oxygenates Calibration Curves<br />
Originally designed for D-5599-95<br />
EPA O-FID Oxygenate Petrochemical <strong>Standards</strong><br />
This second oxygenate version has been formulated to meet the specific analyte requirements set forth in the EPA methodology.<br />
EPA O-FID Quantitative Calibration Mixes (without Internal Standard)<br />
M-GRO-CAL-EPA-SET-10ML<br />
$ 350 / set of 5 x 10 mL<br />
5 comps.<br />
Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />
Calibr. range Wt. % Wt. % Wt. % Wt. % Wt. %<br />
Methanol 0.30 - 12.00 6.00 12.00 3.00 0.30 9.00<br />
Ethanol 0.30 - 12.00 0.30 3.00 6.00 9.00 12.00<br />
t-Butanol 0.30 - 12.00 0.30 6.00 9.00 12.00 3.00<br />
MtBE 0.30 - 15.00 15.00 7.50 11.25 3.75 0.30<br />
RFA Gasoline 78.40 71.50 70.75 74.95 75.70<br />
EPA O-FID Quantitative Calibration Mixes (with Internal Standard)<br />
M-GRO-CAL-IS/EPA-SET<br />
$ 175 / set of 5 x 1 mL<br />
6 comps.<br />
Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />
Calibr. range Wt. % Wt. % Wt. % Wt. % Wt. %<br />
Methanol 0.29 - 11.40 5.70 11.40 2.85 0.29 8.55<br />
Ethanol 0.29 - 11.40 0.29 2.85 5.70 8.55 11.40<br />
t-Butanol 0.29 - 11.40 0.29 5.70 8.55 11.40 2.85<br />
MtBE 0.29 - 14.29 14.25 7.13 10.69 3.56 0.29<br />
1,2-Dimethoxyethane (ISTD) 5.00 5.00 5.00 5.00 5.00<br />
RFA Gasoline 74.48 67.93 67.31 71.20 71.92<br />
ASTM <strong>Standards</strong><br />
EPA O-FID Quantitative Calibration<br />
Check Standard<br />
(without Internal Standard)<br />
M-GRO-EPA-CC-10ML<br />
M-GRO-EPA-CC-10ML-PAK<br />
Wt./Wt. %<br />
Methanol 4.0<br />
Ethanol 8.0<br />
tert-Butanol 5.0<br />
Internal Standard<br />
M-GRO-IS-5ML<br />
M-GRO-IS-5ML-PAK<br />
Wt./Wt. %<br />
Methyl tert-butyl ether 12.0<br />
RFA gasoline 71.0<br />
EPA O-FID Spiking Solution<br />
M-GRO-EPA-SP-5ML<br />
M-GRO-EPA-SP-5ML-PAK<br />
Wt./Wt. %<br />
Methanol 14.3<br />
Ethanol 28.6<br />
$ 50 / 1 x 10 mL<br />
SAVE $ 200 / 5 x 10 mL<br />
5 comps.<br />
$ 50 / 1 x 5 mL<br />
SAVE $ 200 / 5 x 5 mL<br />
4 comps.<br />
Wt./Wt. %<br />
tert-Butanol 14.3<br />
Methyl tert-butyl ether 42.8<br />
$ 10 / 1 x 10 mL<br />
SAVE $ 40 / 5 x 10 mL<br />
EPA O-FID Quantitative Calibration<br />
Check Standard<br />
(with Internal Standard)<br />
M-GRO-EPACC/IS-5ML<br />
M-GRO-EPACC/IS-5ML-PAK<br />
Wt./Wt. %<br />
Methanol 3.80<br />
Ethanol 7.60<br />
tert-Butanol 4.75<br />
Wt./Wt. %<br />
Methyl tert-butyl ether 11.40<br />
RFA gasoline 67.45<br />
DME (internal standard) 5.0<br />
Oxygenate Free Gasoline Refinery<br />
Blank<br />
M-GRO-BLNK-10ML<br />
M-GRO-BLNK-10ML-PAK<br />
RFA Gasoline (neat)<br />
$ 35 / 1 x 5 mL<br />
SAVE $ 150 / 5 x 5 mL<br />
6 comps.<br />
$ 10 / 1 x 10 mL<br />
SAVE $ 40 / 5 x 10 mL<br />
Technical Note<br />
Additional Oxygenate<br />
calibration, check standards,<br />
and independent reference<br />
standards can be found in<br />
ASTM method D-4815 or<br />
D-5622. The required QA/QC<br />
procedures in EPA methods<br />
stipulate a calibration check<br />
standard be used once per<br />
analytical batch or per 10<br />
sample set. AccuStandard has<br />
bulk packaged check standards<br />
to meet this increased usage.<br />
1,2-Dimethoxyethane (ISTD)<br />
Cross <strong>Reference</strong> Table<br />
ASTM IP ISO DIN JIS AFNOR sorted by<br />
ASTM Method see page 145<br />
164<br />
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