SAF-RC- 107 100-H Remaining Sites Burial Grounds ... - Hanford Site

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Quality Control Results Client: Washington Closure <strong>Hanford</strong> Job Number: 280-3571-1 Sdg Number: J00790 Method Blank - Batch: 280-16084 Method: 8082 Preparation: 3546 Lab Sample ID: MB 280-16084/5-A Analysis Batch: 280-17564 Instrument ID: GCSW Client Matrix: Solid Prep Batch: 280-16084 Lab File ID: 063F6301.D Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 31.9 g Date Analyzed: 05/28/2010 2200 Final Weight/Volume: 5000 uL Date Prepared: 05/18/2010 1720 Injection Volume: 1 uL Column ID: PRIMARY Analyte Result Qual MDL RL Aroclor 1016 2.6 U 2.6 9.4 Aroctor 1221 7.5 U 7.5 16 Aroclor 1232 1.9 U 1.9 9.4 Aroctor 1242 4.4 U 4.4 9.4 Aroclor 1248 4.4 U 4.4 9.4 Aroclor 1254 2.4 U 2.4 9.4 Aroclor 1260 2.4 U 2.4 9.4 Surrogate % ec Acceptance Limits Decachlorobiphenyl 105 59-130 Tetra ch loro-m-xyle ne 97 53-128 Lab Control Sample - Batch: 280-16084 Method: 8082 Preparation: 3546 Lab Sample ID: LCS 280-16084/6-A Analysis Batch: 280-17564 Instrument ID: GCSW Client Matrix: Solid Prep Batch: 280-16084 Lab File ID: 064F6401.D Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 32.0 g Date Analyzed: 05/28/2010 2232 .Final Weight/Volume: 5000 uL Date Prepared: 05/18/2010 1720 Injection Volume: 1 uL Column ID: PRIMARY Analyte Spike Amount Result % Rec. Limit Qual Aroclorl1016 31.2 22.1 71 54-132 Aroclor 1260 31.2 26.5 85 62- 129 Surrogate % Rec Acceptance Limits Decachlorobiphenyt 94 59-130 Tetra chloro-m-xylene 86 53-128 TestAmerica Denver Page 37 of 58 06/07/2010
Quality Control Results Client: Washington Closure <strong>Hanford</strong> Job Number: 280-3571-1 Sdg Number: J00790 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 280-16084 Method: 8082 Preparation: 3546 MS Lab Sample ID: 280-3571-4 Analysis Batch: 280-17564 Instrument ID: GCSW Client Matrix; Solid Prep Batch: 280-16084 Lab File ID: 070F7001.D Dilution: 1.0 Initial Weight/Volume: 31.3 g Date Analyzed: 05/29/2010 0143 Final WeightlVolume: 5000 uL Date Prepared: 05/18/2010 1720 Injection Volume: 1 uL Column ID: PRIMARY MSD Lab Sample ID: 280-3571-4 Analysis Batch: 280-17564 Instrument ID: GCSW Client Matrix: Solid Prep Batch: 280-16084 Lab File ID: 071 F7101.D Dilution: 1.0 Initial Weight/Volume: 31.3 g Date Analyzed: 05/29/2010 0215 Final Weight/Volume: 5000 uL Date Prepared: 05/18/2010 1720 Injection Volume: 1 uL Column ID: PRIMARY % Rec, Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Arocorl10l6 32 19 54- 132 53 26 N J N Aroclor 1260 38 22 62- 129 50 26 N J N Surrogate MS % Rec MSD % Rec Acceptance Limits Decachlorobiphenyl 43 34 59- 130 Tetrachloro-m-xylene 53 45 *53- 128 TestAmnerica Denver Page 38 of 58 06/07/2010
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SAF-RC- 107 100-H Remaining Sites B
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THE LEADER IN ENVIRONMENTAL TESTING
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Washington Closure Hanford June 17,
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~ ~ ~ ~ enr Definfi itions _ ______
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Richland Old Richland Isotope SOP I
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Sample Results Summary Date: 17-Jun
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Sample Results Summary Date: 17-Jun
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TestAmerica Data Review/Verificatio
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Clouseau TestAmerica Nonconformance
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Page 66 and 67: ANALYTICAL REPORT Job Number: 280-3
Page 68 and 69: CASE NARRATIVE Client: Washington C
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Page 72 and 73: METHOD SUMMARY Client: Washington C
Page 74 and 75: SAMPLE SUMMARY Client: Washington C
Page 76 and 77: Analytical Data Client. Washington
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Page 86 and 87: Client: Washington Closure Hanford
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Page 96 and 97: TestAmerica Denver QUALITY CONTROL
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