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SAF-RC- 107 100-H Remaining Sites Burial Grounds ... - Hanford Site

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Washington Closure Hantford<br />

June 17, 2010<br />

The requested analyses were:<br />

Alpha Spectroscopy<br />

Plutonium-238, -239/240 by method RL-ALP-002 (RICH-<strong>RC</strong>-5O 10)*<br />

Gas Proportional Counting<br />

Strontium-90 by method RL-GPC-003 (RICll-<strong>RC</strong>-5O06)*<br />

Gamma Spectroscopy<br />

Gamma Spec by method RL-GAM-001I (RJCII-<strong>RC</strong>-5017)*<br />

Liquid Scintillation Counting<br />

Tritium by method RL-LSC-005 (RICI I<strong>RC</strong>-5007)*<br />

Carbon-14 by method RL-LSC-008 (RICH-<strong>RC</strong>-5022)*<br />

Nickel-63 by method RL-LCS-017 (RICHl-<strong>RC</strong>-5069)*<br />

*SOPj ID's changed effective 7-01-2008. Attached is a cross reference until SOP ID's are changed in all systems.<br />

IV. Quality Control<br />

Thc analytical results for each analysis performed includes a minimum of one laboratory control sample<br />

(LCS), one method (reagent) blank, and one duplicate sample analysis. Any exceptions have been noted<br />

in the "Comments" section.<br />

QC and sample results are reported in the same units.<br />

V. Comments<br />

Alphia Spectroscopy<br />

Plutonium-238. -239/240 by method RL-ALP-002 (RICH-<strong>RC</strong>-50 10):<br />

'The LCS, batch blank, samples and sample duplicate (JI9YB6) results are within contractual<br />

requirements.<br />

Gas Proportional Counting<br />

Strontium-90 by method RL-QPC-003 (RICH-<strong>RC</strong>-5006):<br />

'[he L.CS, batch blank, samples and sample duplicate (J I9Y-B5) results are within contractual<br />

requirements.<br />

Gamma Spectroscopy<br />

Gamma Spec by method RL-GAM-00lI (RICI I-<strong>RC</strong>-50 17):<br />

There was insufficient volume for a duplicate. Sample JI19YB34 was recounted on a different detector for<br />

the duplicate (J19YB4 DUP).<br />

The count times were reduced to meet the priority turn around time. The following samples and the LCS<br />

do not meet the CRDL for Eu-152, Eu-154 & Eu-155 due to reduced count times.<br />

JI9YB4 Jl9Y136 JI9YB7<br />

Except as noted, the LCS, batch blank, samples and sample duplicate (JI9YB4) results are within<br />

contractual requirements.<br />

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