SAF-RC- 107 100-H Remaining Sites Burial Grounds ... - Hanford Site

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Client: Washington Closure Hanford Matrix Spike/lehd:81 Matrix Spike Duplicate Recovery Report - Batch: 280-16087 Preparation: 3550C Quality Control Results Job Numberi 280-3571-1 Sdg Number J00790 MS Lab Sample ID: 280-3571-3 Analysis Batch: 280-17785 Instrument ID: HPLC_G Client Matrix: Solid Prep Batch: 280-16087 Lab File ID: 012-1301.D Initial Weight/Volume: 30.7 g Dilution: 1,0 Date Analyzed: 06/01/2010 2252 FnlWih/oue 00u Date Prepared: 05/18/2010 1800 Injection Volume: Column ID: PRIMARY MSD Lab Sample ID: 280-3571-3 Analysis Batch: 280-17785 Instrument ID: HPLCG Client Matrix: Solid Prep Batch: 280-16087 Lab File ID: 013-1401.0 Initial Weight/Volume: 30.2 g Dilution: 1.0 egtou :400 L Date Analyzed: 06/01/2010 2322Fia Date Prepared: 05/18/2010 1800 Injection Volume: Column ID: PRIMARY % Rec. Analyte MVS MSD Limit RPD RPD Limit MS Qual MSD Qual Acenaphthene 93 69 72 -1 1b 28 20N Acenaphthylene 105 79 60-115 27 21 Anthracene 96 77 61 - 115 21 20 Benzo[a]anthracefle 101 83 76- 115 19 20 Benzo[a]pyrene 99 79 69- 115 21 20 Benzo[blfluoranthene 99 81 81 - 115 19 20 Benzo[g,hilperyiene 103 82 71 -115 21 20 Benzo[klfluoranthene 102 83 85 - 115 19 20N Chrysene 103 83 70-115 19 20 Dibenzo(ah)anthracene 102 82 79-115 19 20 Fluoranthene 101 82 67- 115 19 20 Fluorene 94 71 72 -115 27 20N Indeno[1,2,3-cdlpyrene 98 77 76- 115 22 20 Naphthalene 96 71 77 -115 28 20N Phenanthrene Pyrene Surrogate 97 76 79-115 22 20N 103 83 77- 115 20 20 MS % Rec MSD % Rec Acceptance Limits Terphenyl-d 14 (SUR) 92 75 72-115 TestAmerica Denver Page 45 of 58 06/07/2010
Quality Control Results Client: Washington Closure Hanford Job Number: 280-3571-1 Sdg Number: J00790 Method Blank - Batch: 280-16899 Method: 60108 Preparation: 3050B Lab Sample ID: MB 280-16899/1 -A Analysis Batch: 280-17589 Instrument ID: MT_025 Client Matrix: Solid Prep Batch: 280-16899 Lab File ID: 25A3052810.txt Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 1.00 g Date Analyzed: 05/28/2010 1904 Final Weight/Volume: 100 mL Date Prepared: 05/27/2010 1600 Analyte Result Qual MDL RL Aluminum 1.6 U 1.6 5.0 Antimony 0.38 U 0.38 0.60 Arsenic 0.66 U 0.66 1.0 Barium 0,076 U 0.076 0.50 Beryllium 0.033 U 0.033 0.20 Boron 0.98 U 0.98 2.0 Cadmium 0.041 U 0.041 0.20 Calcium 14.1 U 14.1 50.0 Chromium 0.058 U 0.058 0.20 Cobalt 0.10 U 0.10 1.0 Copper 0.22 U 0.22 1.0 Lead 0.27 U 0.27 0.50 Magnesium 3.7 U 3.7 20.0 Manganese 0.10 U 0.10 1.0 Molybdenum 0.26 U 0.26 2.0 Nickel 0.12 U 0.12 4.0 Potassium 41.0 U 41.0 300 Selenium 0.86 U 0.86 1.0 Silver 0.16 U 0.16 0.20 Sodium 59.0 U 59.0 120 Vanadium 0.094 U 0.094 2.0 Zinc 0.40 U 0.40 1.0 Method Blank - Batch: 280-16899 Method: 6010B Preparation: 30506 Lab Sample ID: MB 280-16899/1 -A Analysis Batch: 280-17754 Instrument ID: MT_025 Client Matrix: Solid Prep Batch: 280-16899 Lab File ID: 25A1 0601 10.txt Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 1.00 g Date Analyzed: 06/01/2010 1659 Final Weight/Volume: 100 mL Date Prepared: 05/27/2010 1600 Analyte Result Qual MDL RL Iron 4.34 B 3.8 5.0 Silicon 2.1 U 2.1 10.0 TestAmerica Denver Page 46 of 58 06/07/2010
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SAF-RC- 107 100-H Remaining Sites B
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THE LEADER IN ENVIRONMENTAL TESTING
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Washington Closure Hanford June 17,
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Sample Results Summary Date: 17-Jun
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Sample Results Summary Date: 17-Jun
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Page 66 and 67: ANALYTICAL REPORT Job Number: 280-3
Page 68 and 69: CASE NARRATIVE Client: Washington C
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Page 72 and 73: METHOD SUMMARY Client: Washington C
Page 74 and 75: SAMPLE SUMMARY Client: Washington C
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Page 86 and 87: Client: Washington Closure Hanford
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