SAF-RC- 107 100-H Remaining Sites Burial Grounds ... - Hanford Site

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Quality Control Results Client: Washington Closure Hanford Job Number: 280-3571-1 Sdg Number: J00790 Lab Control Sample - Batch: 280-16899 Method: 6010B Preparation: 3050B Lab Sample ID: LCS 280-16899/2-A Analysis Batch: 280-17589 Instrument ID: MT_025 Client Matrix: Solid Prep Batch: 280-16899 Lab File ID: 25A3052810.txt Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 1.00 g Date Analyzed: 05/28/2010 1906 Final Weight/Volume: 100 mL Date Prepared: 05/27/2010 1600 Analyte Spike Amount Result % Rec. Limit Qual Aluminum 200 176.3 88 82-116 Antimony 50.0 46.58 93 82-110 Arsenic 100 100.5 100 85-110 Barium 200 190.0 95 87-112 Beryllium 5.00 4.47 89 84-114 Boron 100 89.93 90 81 -110 Cadmium 10.0 9.67 97 87-110 Calcium 5000 4519 90 82-114 Chromium 20.0 19.52 98 84-114 Cobalt 50.0 46.95 94 87-110 Copper 25.0 25.54 102 88-110 Lead 50.0 49.12 98 86- 110 Magnesium 5000 4758 95 90-110 Manganese 50.0 48.76 98 88-110 Molybdenum 100 95.97 96 86-110 Nickel 50.0 47.45 95 87-110 Potassium 5000 4769 95 89-110 Selenium 200 195.7 98 83-110 Silver 5.00 5.02 100 87-114 Sodium 5000 5032 101 90-112 Vanadium 50.0 49.64 99 88-110 Zinc 50.0 49.82 100 76-114 Lab Control Sample - Batch: 280-16899 Method: 6010B Preparation: 30506 Lab Sample ID: LCS 280-16899/2-A Analysis Batch: 280-17754 Instrument ID: MT_025 Client Matrix: Solid Prep Batch: 280-16899 Lab File ID: 25A1 060110O.txt Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 1.00 g Date Analyzed: 06/01/2010 1702 Final Weight/Volume: 100 mL Date Prepared: 05/27/2010 1600 Analyte Spike Amount Result % Rec. Limit Qual Iron 100 103.0 103 87-120 Silicon 1000 217.7 22 10-70 TestAmerica Denver Page 47 of 58 06/07/2010
Quality Control Results Client: Washington Closure Hanford Job Number: 280-3571-1 Sdlg Number: J00790 Matrix Spike - Batch: 280-16899 Method: 6010B Preparation: 3050B Lab Sample ID: 280-3571-1 Analysis Batch: 280-17589 Instrument ID: MT_025 Client Matrix: Solid Prep Batch: 280-16899 Lab File ID: 25A3052810.txt Dilution: 1.0 Units: mg/Kg initial Weight/Volume: 1.07 g Dale Analyzed: 05/28/2010 1913 Final Weight/Volume: 100 mL Date Prepared: 05/27/2010 1600 Analyte Sample Result/Qual Spike Amount Result % Rec. Limit Qual Aluminum 7900 195 9547 844 50 -200 4 Antimony 0.39 U 48.7 27.39 56 20 -200 Arsenic 6.4 97.3 93.05 89 76 -111 Barium 66.4 195 236.9 88 52-159 Beryllium 0.30 4.87 4.10 78 72 -105 Boron 1.4 B 97.3 77.25 78 75- 107 Cadmium 0.073 B 9.73 8.51 87 40- 130 Calcium 3780 4870 8152 90 43-165 Chromium 11.8 19.5 29.11 89 70 -200 Cobalt 6.8 48.7 46.65 82 72 -106 Copper 13.5 24.3 36.93 96 37-187 Lead 14.7 48.7 56.01 85 70- 200 Magnesium 4190 4870 8449 88 64-145 Manganese 303 48.7 353.0 103 40- 200 4 Molybdenum 0.27 U 97.3 81.44 84 75-103 Nickel 11.6 48.7 51.92 83 61 -126 Potassium 1510 4870 5760 87 56-172 Selenium 0.88 U 195 167.2 86 76- 104 Silver 0.16 U 4.87 4.42 91 75 -141 Sodium 165 4870 4250 84 78-111 Vanadium 44.3 48.7 90.48 95 50- 169 Zinc 39.5 48.7 83.04 89 70 -200 Matrix Spike - Batch: 280-16899 Method: 6010B Preparation: 3050B Lab Sample ID: 280-3571-1 Analysis Batch: 280-17754 Instrument ID: MT_025 Client Matrix: Solid Prep Batch: 280-16899 Lab File ID: 25A1 060110O.txt Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 1.07 g Date Analyzed: 06/01/2010 1709 Final Weight/Volume: 100 mL Date Prepared: 05/27/2010 1600 Analyte Sample Result/Qual Spike Amount Result % Rec. Limit Qual Iron 19200 97.3 19340 ill 70-200 4 Silicon 390 973 460.4 7 20 -200 N TestAmnerica Denver Page 48 of 58 06/07/2010
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SAF-RC- 107 100-H Remaining Sites B
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THE LEADER IN ENVIRONMENTAL TESTING
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Washington Closure Hanford June 17,
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~ ~ ~ ~ enr Definfi itions _ ______
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Richland Old Richland Isotope SOP I
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Sample Results Summary Date: 17-Jun
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Sample Results Summary Date: 17-Jun
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TestAmerica Data Review/Verificatio
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TestAm erica Data Review/Verificati
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Clouseau TestAmerica Nonconformance
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TestAmerica THE LEADER IN ENVIRONME
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Page 66 and 67: ANALYTICAL REPORT Job Number: 280-3
Page 68 and 69: CASE NARRATIVE Client: Washington C
Page 70 and 71: DATA REPORTING QUALIFIERS Client: W
Page 72 and 73: METHOD SUMMARY Client: Washington C
Page 74 and 75: SAMPLE SUMMARY Client: Washington C
Page 76 and 77: Analytical Data Client. Washington
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Page 86 and 87: Client: Washington Closure Hanford
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Page 96 and 97: TestAmerica Denver QUALITY CONTROL
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Page 110 and 111: Client: Washington Closure Hanford
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Page 122 and 123: TestAmerica THE LEAE NEVIOMENTAL. T
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