The Students' Guide in Quantitative Analysis - Free Ebooks Library
The Students' Guide in Quantitative Analysis - Free Ebooks Library
The Students' Guide in Quantitative Analysis - Free Ebooks Library
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KEI'ORXJjNG ANALYSES.<br />
E. Report<strong>in</strong>g Analyses.—<br />
Analyses may be reported on blank forms pr<strong>in</strong>ted on let-<br />
ter paper 8" x lo", hav<strong>in</strong>g follow<strong>in</strong>g head<strong>in</strong>gs :<br />
.<br />
GRAMMES<br />
<strong>The</strong>se<br />
Hakti'okd, , !S8 . Report of<br />
OF . DliXEKMlNATJON OF .<br />
. Metiiod of <strong>Analysis</strong> ,<br />
<strong>Analysis</strong><br />
TAKEN<br />
head<strong>in</strong>gs are<br />
pr<strong>in</strong>ted <strong>in</strong> vertical colim<strong>in</strong> ; <strong>in</strong> one horizontal l<strong>in</strong>e<br />
are placed follow<strong>in</strong>g head<strong>in</strong>gs: Pkecii'ITATes, Actual<br />
Weights, Constituents, Calculated Weights, Per-<br />
centages, <strong>The</strong>oretical Percentages; under each a blank<br />
space is left of 2 1-2 <strong>in</strong>ches. Under "precipitates" place<br />
formulas of precipitates obta<strong>in</strong>ed; under "actual weights"<br />
place actual weighL-i of precipitates; under "constituents "<br />
place forniDlcC of constituents to be reported; under "cal-<br />
culated weights ' place the amounts of constituents exist<strong>in</strong>g<br />
<strong>in</strong> precipitates; under " percentages" place percentages of<br />
constituents actually obta<strong>in</strong>ed — <strong>in</strong> short, the results of<br />
analyses. <strong>The</strong> last column, "theoretical percentages," can<br />
be fdled only <strong>in</strong> the case of few pure chemical salts.<br />
<strong>The</strong> words special remarks are pr<strong>in</strong>ted about two <strong>in</strong>ches<br />
from the bottom of the sheet, leav<strong>in</strong>g room for remarks on<br />
processes employed, etc.*<br />
Notes to the <strong>Analysis</strong> of Barium Chloride,<br />
Reactions. (I) BaCL -f H,SO, = EaSO, + 2HCI<br />
(2) BaCI, -\- -AgNO^ = 2AgCl+ Ba(NO,),.<br />
<strong>The</strong> chloride of silver precipitate changes color on expos-<br />
ure to light, los<strong>in</strong>g chlor<strong>in</strong>e and form<strong>in</strong>g AgjCl ; the change,<br />
however, is only superficial, but Mulder says the loss of<br />
weight is appreciable.<br />
* Sec scccimcs blaok ai the end of this beok.