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The Students' Guide in Quantitative Analysis - Free Ebooks Library

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KEI'ORXJjNG ANALYSES.<br />

E. Report<strong>in</strong>g Analyses.—<br />

Analyses may be reported on blank forms pr<strong>in</strong>ted on let-<br />

ter paper 8" x lo", hav<strong>in</strong>g follow<strong>in</strong>g head<strong>in</strong>gs :<br />

.<br />

GRAMMES<br />

<strong>The</strong>se<br />

Hakti'okd, , !S8 . Report of<br />

OF . DliXEKMlNATJON OF .<br />

. Metiiod of <strong>Analysis</strong> ,<br />

<strong>Analysis</strong><br />

TAKEN<br />

head<strong>in</strong>gs are<br />

pr<strong>in</strong>ted <strong>in</strong> vertical colim<strong>in</strong> ; <strong>in</strong> one horizontal l<strong>in</strong>e<br />

are placed follow<strong>in</strong>g head<strong>in</strong>gs: Pkecii'ITATes, Actual<br />

Weights, Constituents, Calculated Weights, Per-<br />

centages, <strong>The</strong>oretical Percentages; under each a blank<br />

space is left of 2 1-2 <strong>in</strong>ches. Under "precipitates" place<br />

formulas of precipitates obta<strong>in</strong>ed; under "actual weights"<br />

place actual weighL-i of precipitates; under "constituents "<br />

place forniDlcC of constituents to be reported; under "cal-<br />

culated weights ' place the amounts of constituents exist<strong>in</strong>g<br />

<strong>in</strong> precipitates; under " percentages" place percentages of<br />

constituents actually obta<strong>in</strong>ed — <strong>in</strong> short, the results of<br />

analyses. <strong>The</strong> last column, "theoretical percentages," can<br />

be fdled only <strong>in</strong> the case of few pure chemical salts.<br />

<strong>The</strong> words special remarks are pr<strong>in</strong>ted about two <strong>in</strong>ches<br />

from the bottom of the sheet, leav<strong>in</strong>g room for remarks on<br />

processes employed, etc.*<br />

Notes to the <strong>Analysis</strong> of Barium Chloride,<br />

Reactions. (I) BaCL -f H,SO, = EaSO, + 2HCI<br />

(2) BaCI, -\- -AgNO^ = 2AgCl+ Ba(NO,),.<br />

<strong>The</strong> chloride of silver precipitate changes color on expos-<br />

ure to light, los<strong>in</strong>g chlor<strong>in</strong>e and form<strong>in</strong>g AgjCl ; the change,<br />

however, is only superficial, but Mulder says the loss of<br />

weight is appreciable.<br />

* Sec scccimcs blaok ai the end of this beok.

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