<strong>Chromatography</strong><strong>Chromatography</strong> columns/GC columnsLLG CHROMATOGRAPHY CATALOGUE11OPTIMA ® 5 MS Accent capillary columns for GCsilarylene phaseMACHEREY-NAGELwith polarity similar to a 5 % diphenyl -95 % dimethylpolysiloxane phase.USP G27, G36lowest column bleed, nonpolar phase, ideal for ion trap and quadrupol MS detectors solvent rinsing for removalof impurities applicableapplication areas: all-round phase for environmental analyses, trace analyses, EPA methods, pesticides, PCB,food and drug analysessimilar phases: DB-5 MS, HP-5 MS, Ultra-2, Equity-5, CP-Sil 8 CB low bleed/MS, Rtx-5SIL-MS, Rtx-5 MS, 007-5 MS,BPX5, MDN-5S, AT-5 MS, VF-5 MSmax. temperature for isothermal operation: 340°C,max. temperature for short isotherms in a temperature programme: 360°Cfor cloumns with film thicknesses > 5.5 µm the max. temperatures are 320 and 340°CInt.Ext. Film Length PK Cat. No.diam.diam. thicknessmm mm µm m0.250.250.250.250.250.250.320.320.320.320.320.40.40.40.40.40.40.50.50.50.50.50.250.501.000.250.501.001.000.250.500.251.003030306060602530306060111111111114.003 0174.003 0194.003 0214.003 0184.003 0204.003 0224.003 0114.003 0094.003 0134.003 0104.003 012Each column is individually tested and supplied with test certificate and test chromatogram, but without fittings or ferrules. Column ends are melted or closedwith septa, and thus protected from atmospheric oxygen.Additionally, we supply the corresponding test mixture with each column.The bleed comparison test of the OPTIMA ® 5-MS Accentwith a conventional 5-MS phase shows the outstandingperformance of the silarylene phase.Background noise at 340 °CThe unmatched low background level of the OPTIMA ®5 MS Accent, which is approximately three times lowercompared to a 5 MS brand column, provides significantlyincreased sensitivity and allows the application in traceanalyses particularly of high-boiling compounds.107.890.2FID Signal in mV107.6107.4107.2Standard 5 MS Phase9089.889.6OPTIMA ® 5 MS Accent0 10 20 30 s0 10 20 30 s90E & OE.
LLG CHROMATOGRAPHY CATALOGUE<strong>Chromatography</strong><strong>Chromatography</strong> columns/GC columns1Optima ® 17 capillary columns for GCphenylmethylpolysiloxane (50 % phenyl)medium polar phasepreferred applications: steroids, pesticides, drug analysesUSP G3similar phases: OV-17, DB-17, HP50+, HP17, SPB-50, SP-2250, Rtx-50, CP-Sil 24 CB, 007-17, ZB50MACHEREY-NAGEL1max. temperature for isothermal operation: 320°C, max. temperature for short isotherms in a temperatureprogramme: 340°C, for 0.53mm ID columns the max. temperatures are 300 and 320°C, resp.Int.Ext. Film Length PK Cat. No.diam.diam. thicknessmm mm µm m0.100.250.250.250.250.250.250.250.250.250.250.250.250.320.320.320.320.320.320.320.320.320.320.320.320.320.530.530.40.40.40.40.40.40.40.40.40.40.40.40.40.50.50.50.50.50.50.50.50.50.50.50.50.50.80.80.100.150.250.500.150.250.500.150.250.500.150.250.500.250.350.500.150.250.350.500.250.350.500.250.350.501.001.001025252530303050505060606025252530303030505050606060253011111111111111111111111111114.003 2364.003 1814.003 0264.003 0464.003 1824.003 0274.003 0474.003 1834.003 0284.003 0484.003 1844.003 0294.003 0494.003 1124.003 1944.003 1854.003 1934.003 1134.003 1954.003 1864.003 1144.003 1964.003 1874.003 1154.003 1974.003 1884.003 1914.003 192In addition to this standard programme we will be happy to supply columns custom-made to your specifications.Column:Sample:Inj. volume:Carrier gas:Temperature:Analysis of pesticidesOPTIMA ® 17, 0.20 μm film,25 m x 0.20 mm ID,max. temperature 320/340 °C,pesticide standard of the cantonallaboratory Schaffhausen (Switzerland),0.1 mg/ml or 0.01 mg/ml each1.0 μlHe, 25 cm/s, 3 s without split100 °C (3 min), 8 °C/min → 250 °C,10 °C/min → 320 °CDetector: MSD HP 5971MN Appl. No. 2009301 2 5 10133 467 8 911 1210 20 30 minPeaks:1. Dichlorphos2. Naled3. Vinclozolin4. Chlorthalonil5. Chlorpyrifos6. Dichlofluanid7. Procymidon8. Captan9. Folpet10. Carbophenothion11. Iprodion12. Captafol13. CoumaphosE & OE.91
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Alphabetical indexLLG CHROMATOGRAPH
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ChromatographyVials/Ampoules, Septa
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ChromatographyVials/Ampoules, Septa
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ChromatographyVials/Ampoules, Septa
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ChromatographyVials/Ampoules, Septa
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ChromatographyVials/Ampoules, Septa
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ChromatographyVials/Ampoules, Septa
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ChromatographyVials/Ampoules, Septa
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ChromatographyVials/Ampoules, Septa
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ChromatographyVials/Ampoules, Septa
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ChromatographySyringes/Microlitre S
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ChromatographySyringes/Microlitre S
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ChromatographySyringes/Microlitre S
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