Catalytic Reductive Coupling Reactions - Michigan State University
Catalytic Reductive Coupling Reactions - Michigan State University
Catalytic Reductive Coupling Reactions - Michigan State University
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Screening Pd(2+) CatalystsEEEEcatalystsolventHHEEentry catalyst solvent temperature time (h) yield (%)1 (Ph3P)4Pd THF reflux 12 02 Pd(OAc)2 THF room temp.notreported503 (Ph3P)2Pd(OAc)2 THF 64 ° C 1.5 704 (Ph3P)2Pd(OAc)2 C6D6 60 ° C 1.5 85Trost, B.; Lautens, M. J. Am. Chem. Soc. 1985, 107, 1781—1783.