Fluensulfone ... - IR-4 Project
Fluensulfone ... - IR-4 Project
Fluensulfone ... - IR-4 Project
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PTRL West <strong>Project</strong> No. 1977W<br />
Report 2 Page 30<br />
Table II. Summary of Method Validation Recoveries of MCW-2, Butene<br />
Sulfonic Acid and Thiazole Sulfonic Acid in Pepper.<br />
Quantitation ions<br />
Fortification Level Percent Recovery<br />
Sample (ppm) MCW-2 M-3625 M-3627<br />
Controls NA NA NA NA<br />
Fort 1A 0.01 106 99 79<br />
Fort 1B 0.01 92 98 78<br />
Fort 1C 0.01 92 88 88<br />
Fort 1D 0.01 119 108 88<br />
Fort 1E 0.01 106 108 88<br />
Average 103 100 84<br />
Standard Deviation 11 8 5<br />
% Rel. Std. Dev. 11 8 6<br />
Fort 2A 0.10 106 94 95<br />
Fort 2B 0.10 107 94 95<br />
Fort 2C 0.10 110 92 91<br />
Fort 2D 0.10 112 95 95<br />
Fort 2E 0.10 96 93 100<br />
Average 106 94 95<br />
Standard Deviation 6 1 3<br />
% Rel. Std. Dev. 6 1 3<br />
Overall Average 105 97 90<br />
Overall Standard Deviation 9 7 7<br />
Overall Average %RSD 9 7 8<br />
NA =Not Applicable<br />
M-3625 = Thiazole sulfonic acid<br />
M-3627 = Butene sulfonic acid
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