Fluensulfone ... - IR-4 Project
Fluensulfone ... - IR-4 Project
Fluensulfone ... - IR-4 Project
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PTRL West <strong>Project</strong> No. 1977W<br />
Report 2 Page 31<br />
Table II (cont.). Summary of Method Validation Recoveries of MCW-2, Butene<br />
Sulfonic Acid and Thiazole Sulfonic Acid in Pepper.<br />
Confirmation ions<br />
Fortification Level Percent Recovery<br />
Sample (ppm) MCW-2 M-3625 M-3627<br />
Controls NA NA NA NA<br />
Fort 1A 0.01 99 69 79<br />
Fort 1B 0.01 92 69 79<br />
Fort 1C 0.01 79 78 78<br />
Fort 1D 0.01 99 98 88<br />
Fort 1E 0.01 86 88 88<br />
Average 91 80 82<br />
Standard Deviation 9 13 5<br />
% Rel. Std. Dev. 10 16 6<br />
Fort 2A 0.10 103 85 92<br />
Fort 2B 0.10 108 85 94<br />
Fort 2C 0.10 110 88 90<br />
Fort 2D 0.10 109 85 93<br />
Fort 2E 0.10 90 95 96<br />
Average 104 88 93<br />
Standard Deviation 8 4 2<br />
% Rel. Std. Dev. 8 5 2<br />
Overall Average 98 84 88<br />
Overall Standard Deviation 11 10 7<br />
Overall Average %RSD 11 12 8<br />
NA =Not Applicable<br />
M-3625 = Thiazole sulfonic acid<br />
M-3627 = Butene sulfonic acid
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