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and a kinetic study should be earned out at temperatures below 250°C since the reaction is slower at these temperatures. In fitting a model 10 the experimental data, a fixed value was used for the heal capacity ofthe reaction based on the estimated value for that of SNHP. Ifa sufficiently pure sample ofSNHP could be synthesized, an experimental value for Cp
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1"'1 National Library of Canada Bib
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y thcnnally dc
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Gregory for his kindness and making
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LIST OF TABLES Table 1.1 Corrosion
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single crystals ofquartz (Nacken, 1
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phosphate control in the 19&Os was
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the standard Gibbs energies and ent
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consist ofortnophospllatcs. The bou
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2 FcIlFc[[J204(S) + 26 Na+(aq) + 12
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solubility and phase relations ofpr
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where 11 equals the ionic state ofh
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'", g :£ 30
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1.10 Project Objectives The objecti
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II - "7 /'7"7L 41 J n
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2.3.2 Single Crystal X-Ray Dif'frac
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2.4 Synthesis and Characterization
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Several solid starting materials we
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FeUlNTA(aq) + HPOl(aq) + NH/(aq) __
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All runs lasted up to to days at a
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0.0 l--l_-L_l-....J.._-L_l-....J..-
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dissolution orSNHP and allowed the
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(a) (b) Figure 3.1a and b: Scanning
Page 87 and 88: and the equilibrium constant for ma
Page 89 and 90: groups. Oxidizing agents were previ
Page 91 and 92: and reacted with aqueous sodium pho
Page 94 and 95: (al (b) Figure 3.5a and b: Scanning
Page 97 and 98: Figure 3.7: Scanning electron micro
Page 99: Table 3.1: Positional parameters fo
Page 104: Figure 3.10: Scanning electron micr
Page 107 and 108: pattern is listed in Table A.LI3. E
Page 109: 4.0 SOLUBILITY AND REACTION KINETIC
Page 117 and 118: Table 4.1 Experimental C
Page 119: Table 4.3 Standard slale properties
Page 126 and 127: Table 4.6 HKF equation ofstate coef
Page 128 and 129: Equilibrium constants are listed in
Page 130: Table 4.9 Equilbrium constants for
Page 136: Table 4.10 Standard state propertie
Page 143 and 144: 6.0 BIBLIOGRAPHY Alexander J.H., an
Page 146 and 147: Ivanov V.A., Simonoy M.A., and Bela
Page 148: Quinlan S, (1996) Thcnnochcmistry o
Page 151 and 152: APPENDICES 132
Page 153 and 154: TABLEA.l.l: X-Ray Diffraction Resul
Page 155: TABLE A.I.2 (continued) Quinlan(199
Page 158 and 159: TABLEA.I.4: X-Ray Diffraction Resul
Page 160: TABLEA.1.5: X-Ray Diffraction Resul
Page 163 and 164: TABLEA.I.G: X-Ray Diffraction Resul
Page 165: TABLEA.I.7: X-Ray Diffraction Resul
Page 169 and 170: TABLEAJ.9: X-Ray Diffraction Result
Page 171 and 172: TABLE A.1. 10: X-Ray Diffraction Re
Page 173 and 174: TABLEA.I.l1: X-Ray Diffraction Resu
Page 176 and 177: TABLE A,1.I2: X-Ray Diffraction Res
Page 178: TABLE A.I.l3: X-Ray Diffraction Res
Page 182 and 183: X-ray Strocture Report Fo' Dr. P. T
Page 185: (I) SIR92: Altomare, A., Cascarano,
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110
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APPENDIX III: Kiodie aod Solubility
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TABLE A.m.1 (continued) stock 501'n
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TABLE A.m.l (continued) Time m(Na,
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TABLE A.m.2 (continued) Time m(Na+)
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TABLE A.IIL2 (continued) Time m(Na
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TABLE A.1Il.3: Experimental Data fo
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Canada - Memorial University of Newfoundland

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