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TABLEA.I.4: X-Ray Diffraction Results for SrnP from FeNTA Decomposition Quinlan (1996) Product $IHPfrom JCPDS database JCPDS database RGH60A FeP04 Na3P04 FezPOs d"., 1/1'00 doo. 111'00 doo. 111'00 doo. IIII(JO 13.9757 21.0 7.7593 19.2 7.769 78 7.3563 19.9 7.367 73 5.3410 28.3 5.343 32 5.2500 20 4.8533 29.9 4.8800 20 4.3350 40 4.2830 11.9 4.2750 50 3.6900 20 3.6346 29.7 3.637 7 3.4260 3.3223 14.4 13.1 3.432 3.323 15 /. 3.3200 100 3.2200 20 2.9520 19 2.7440 70 2.6685 100.0 2.668 100 2.6550 30 2.6183 72.6 2.624 6 2.6250 100 2.6220 15 2.5528 52.2 2.557 8 2.450 13 2.4300 28 2.3570 19 2.3170 50 2.2510 20 2.2376 11.2 2.2290 15 2.1336 9.1 2.116 2.1390 10 2.081 1.9940 2.0620 25 1.9415 18.9 /.940 60 1.935 34 1.876 4 1.8530 30 1.8640 19 1.8373 13.3 /.837 38 1.832 13 1.7731 11.7 1.779 4 1.7180 1.7080 1.6580 1.6530 25 139
TABLE A.1.4 (continued) Quinlan (1996) Product SIHP from JCPDS database JCPDS database RGH60A FeP04 NaJP04 Fe2POS
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1"'1 National Library of Canada Bib
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y thcnnally dc
Page 11 and 12:
Gregory for his kindness and making
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LIST OF TABLES Table 1.1 Corrosion
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single crystals ofquartz (Nacken, 1
Page 23 and 24:
phosphate control in the 19&Os was
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the standard Gibbs energies and ent
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consist ofortnophospllatcs. The bou
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2 FcIlFc[[J204(S) + 26 Na+(aq) + 12
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solubility and phase relations ofpr
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where 11 equals the ionic state ofh
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'", g :£ 30
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1.10 Project Objectives The objecti
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II - "7 /'7"7L 41 J n
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2.3.2 Single Crystal X-Ray Dif'frac
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2.4 Synthesis and Characterization
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Several solid starting materials we
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FeUlNTA(aq) + HPOl(aq) + NH/(aq) __
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All runs lasted up to to days at a
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0.0 l--l_-L_l-....J.._-L_l-....J..-
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dissolution orSNHP and allowed the
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(a) (b) Figure 3.1a and b: Scanning
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and the equilibrium constant for ma
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groups. Oxidizing agents were previ
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and reacted with aqueous sodium pho
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(al (b) Figure 3.5a and b: Scanning
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Figure 3.7: Scanning electron micro
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Table 3.1: Positional parameters fo
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Figure 3.10: Scanning electron micr
Page 107 and 108: pattern is listed in Table A.LI3. E
Page 109: 4.0 SOLUBILITY AND REACTION KINETIC
Page 117 and 118: Table 4.1 Experimental C
Page 119: Table 4.3 Standard slale properties
Page 126 and 127: Table 4.6 HKF equation ofstate coef
Page 128 and 129: Equilibrium constants are listed in
Page 130: Table 4.9 Equilbrium constants for
Page 136: Table 4.10 Standard state propertie
Page 142 and 143: lower NalP04 mole ratio than the re
Page 144: Broadbent D., Lewis G.G., and Wetto
Page 147 and 148: Marshall W.L. (1982) Two-liquid-pha
Page 150 and 151: Welton E.A.M. (1981) Phase equilibr
Page 152 and 153: APPENDIX I: Powder X-ray Diffractio
Page 154 and 155: TABLE A.l.l: X-Ray Diffraction Resu
Page 157: TABLE A,I.3 (continued) Quinlan JCP
Page 162 and 163: TABLE A.l.S (continued) JCPDS Quinl
Page 164 and 165: TABLE A.1.6 (continued) Quinlan (19
Page 168 and 169: TABLE A.L8 (continued) Boudin JCPDS
Page 170 and 171: TABLE A.I.9 (continued) Product RGH
Page 172 and 173: TABLE A.I.IO (continued) Ziemniak a
Page 174: TABLE AJ.11 (continued) Zicmniak an
Page 177 and 178: TABLE A.T.I2 (continued) Zicmniak a
Page 180: TABLE A.I.13 (continued) Ziemniak a
Page 183: Experimental A colorless irrcg.plal
Page 188 and 189: Slfuc!ure Solution Refinemenl Funct
Page 190 and 191: 111
Page 192 and 193: TABLE A.1II.1: Summary of ICP ES Re
Page 194 and 195: TABLE A.lll.2: KinclicData Time m(N
Page 196 and 197: TABLE A.III.2 (continued) Time m(Na
Page 198 and 199: TABLE A.lll.2 (continued) Time m(Na
Page 200 and 201: TABLE A.lIl.l (continued) Time m(Na
Page 202: TABLE A.III.3 (continued) t "C m(p0
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