the production of thymoquinone from thymol and carvacrol

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We approve the thesis of Alev GÜNE Date of Signature ........................................................... 22 July 2005 Asst. Prof. Dr. O uz BAYRAKTAR Supervisor Department of Chemical Engineering zmir Institute of Technology .......................................................... 22 July 2005 Assoc. Prof. Dr. Selahattin YILMAZ Co-Supervisor Department of Chemical Engineering zmir Institute of Technology ........................................................... 22 July 2005 Asst. Prof. Dr. Fehime ÖZKAN Department of Chemical Engineering zmir Institute of Technology ........................................................... 22 July 2005 Asst. Prof. Dr. Ali ÇA IR Department of Chemistry zmir Institute of Technology ........................................................... 22 July 2005 Prof. Dr. Devrim BALKÖSE Head of Department zmir Institute of Technology ........................................................... Assoc. Prof. Dr. Semahat ÖZDEM R Head of Graduate School
ACKNOWLEDGEMENTS I would like to acknowledge the people who have helped to make this work possible. My sincere gratitude is first for my thesis advisor Assist. Prof. O uz BAYRAKTAR for his consistent and thoughtful advice, continuous encouragement and help during the course of this work. I am also grateful to my other advisor Assoc. Prof. Selahattin YILMAZ for his valuable comments and recommendations. I also wish to thank to personnel of IZTECH Centre for Material Research for their help during my material characterization studies. I would like to appreciate deeply to my roommates, Bahar BOZKURT, Gözde GENÇ for their friendships, supports and encouragements. I am grateful to my friends for assisting me with my research and offering advice and discussion. I also present my deepest thanks to Burç YERKES KL because of not only his friendship but also his kind of efforts and endless support. Finally, I would like to express my heartfelt gratitude to my parents, Ne e and Mehmet Ali GÜNE and brother, Batuhan GÜNE for their continuous support and encouragement, which enabled me to overcome difficulties.
Page 1: THE PRODUCTION OF THYMOQUINONE FROM
Page 5 and 6: ÖZET Bu tezde, genel esnek ligand
Page 7 and 8: 5.4. Catalytic Monoterpene Oxidatio
Page 9 and 10: LIST OF FIGURES Figure Page Figure
Page 11 and 12: LIST OF TABLES Table Page Table 2.1
Page 13 and 14: of thymoquinone are limited only to
Page 15 and 16: advantages compared to homogeneous
Page 17 and 18: NH4 +2 generates the acid sides. Ca
Page 19 and 20: homogeneous internal structures whi
Page 21 and 22: CHAPTER 3 TRANSITION METALS AND COO
Page 23 and 24: not determined by orbital energy al
Page 25 and 26: 3.3.1. Oxidation State The transiti
Page 27 and 28: it surrounds the metal, forms very
Page 29 and 30: metal complexes catalyze the reacti
Page 31 and 32: Figure 4.1. Flexible ligand method:
Page 33 and 34: included in the synthesis mixture.
Page 35 and 36: CHAPTER 5 OXIDATION OF MONOTERPENES
Page 37 and 38: In the GC-MS analysis of the oil of
Page 39 and 40: There are few studies on monoterpen
Page 41 and 42: Homolytic Pathways: Heterolytic Pat
Page 43 and 44: 6.1. Materials CHAPTER 6 EXPERIMENT
Page 45 and 46: inductively coupled plasma spectrom
Page 47 and 48: These tests were performed in detai
Page 49 and 50: Table 7.1. Metal content of encapsu
Page 51 and 52: 7.1.3. X-ray Diffraction (XRD) Anal
Page 53 and 54:
Figure 7.2 (cont.) 42
Page 55 and 56:
ands observed in the region 1200-16
Page 57 and 58:
Figure 7.5. IR spectra ligand (H2 s
Page 59 and 60:
Figure 7.6. DSC analysis result sho
Page 61 and 62:
7.2. Catalytic Activities 7.2.1. De
Page 63 and 64:
eaction products, among which TQ wa
Page 65 and 66:
carvacrol conversion (%) 16 14 12 1
Page 67 and 68:
e 11.6% with a small amount of THQ.
Page 69 and 70:
during the oxidation process and th
Page 71 and 72:
leaching of Cr (salpn) complexes fr
Page 73 and 74:
7.3.2. Effect of Temperature Four d
Page 75 and 76:
7.4. Oxidation of Thymol Carvacrol
Page 77 and 78:
at 60 o C. Essentail oil contained
Page 79 and 80:
REFERENCES Anthony, F., 1999. Advan
Page 81 and 82:
Martin, R.R.L., Neves, G. 2001. “
Page 83 and 84:
APPENDIX A DETERMINATION OF HYDROGE
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