GEMS/Food Instructions for Electronic Submission of Data on ...
GEMS/Food Instructions for Electronic Submission of Data on ...
GEMS/Food Instructions for Electronic Submission of Data on ...
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2.2.22 Field No. 22: Remarks/References<br />
1 <str<strong>on</strong>g>Data</str<strong>on</strong>g> are c<strong>on</strong>fidential. Specific permissi<strong>on</strong> must be obtained<br />
be<str<strong>on</strong>g>for</str<strong>on</strong>g>e using the data <str<strong>on</strong>g>for</str<strong>on</strong>g> the purposes <str<strong>on</strong>g>of</str<strong>on</strong>g> the <str<strong>on</strong>g>GEMS</str<strong>on</strong>g>/<str<strong>on</strong>g>Food</str<strong>on</strong>g><br />
Programme.<br />
Field size: AN250 (up to 250 alphanumeric characters)<br />
Field c<strong>on</strong>tents: This field is used <str<strong>on</strong>g>for</str<strong>on</strong>g> noting remarks and/or references relevant to the<br />
data represented.<br />
2.3 Worked Examples<br />
2.3.1 Example 1<br />
This is a hypothetical example. <str<strong>on</strong>g>Data</str<strong>on</strong>g> to be submitted was generated by a laboratory under<br />
c<strong>on</strong>tract to the New Zealand WHO Collaborating Centre <str<strong>on</strong>g>for</str<strong>on</strong>g> <str<strong>on</strong>g>Food</str<strong>on</strong>g> C<strong>on</strong>taminati<strong>on</strong> M<strong>on</strong>itoring.<br />
Sampling was carried out between April 1997 and December 1997, and the record is being<br />
prepared <strong>on</strong> 2 November 1998. Samples <str<strong>on</strong>g>of</str<strong>on</strong>g> dried figs were analysed as received <str<strong>on</strong>g>for</str<strong>on</strong>g> their<br />
cadmium c<strong>on</strong>tent. The samples were <str<strong>on</strong>g>of</str<strong>on</strong>g> domestic origin and represent the supply <str<strong>on</strong>g>of</str<strong>on</strong>g> dried figs<br />
to the whole country. Analytical results are to be expressed <strong>on</strong> an “as is” basis. A total <str<strong>on</strong>g>of</str<strong>on</strong>g> 100<br />
samples were analysed by a single laboratory, with an analytical limit <str<strong>on</strong>g>of</str<strong>on</strong>g> detecti<strong>on</strong> (LOD) <str<strong>on</strong>g>of</str<strong>on</strong>g><br />
0.0005 mg/kg. The laboratory does not use a separate limit <str<strong>on</strong>g>of</str<strong>on</strong>g> quantificati<strong>on</strong> and reports<br />
quantitatively all results at or above the LOD. Of the 100 samples, 5 were below the limit <str<strong>on</strong>g>of</str<strong>on</strong>g><br />
detecti<strong>on</strong>. The best statistical estimates (using results below the LOD with values equal to<br />
LOD/2) <str<strong>on</strong>g>for</str<strong>on</strong>g> the median, mean, 90 th percentile and standard deviati<strong>on</strong> values were 0.024, 0.032,<br />
0.125 and 0.1 mg/kg respectively. The range <str<strong>on</strong>g>of</str<strong>on</strong>g> quantified analytical results was from 0.002 to<br />
0.483 mg/kg. Internati<strong>on</strong>ally recognized certified reference materials and internal quality<br />
c<strong>on</strong>trol standards were used as quality c<strong>on</strong>trol procedures. However, the laboratory does not<br />
have <str<strong>on</strong>g>for</str<strong>on</strong>g>mal accreditati<strong>on</strong> <str<strong>on</strong>g>for</str<strong>on</strong>g> cadmium testing. The data are freely available in the public<br />
domain.<br />
The following string, using a comma-delimited <str<strong>on</strong>g>for</str<strong>on</strong>g>mat would represent this in<str<strong>on</strong>g>for</str<strong>on</strong>g>mati<strong>on</strong>:<br />
01980001,2-NOV-98,NEZ,DF297,NEZ,04/1997-12/1997,SW,1,SP,012,1,.0005,.0005,<br />
.0005,.0005,A,100,5,.002,.483,.032,.032,.032,.024,.125,.1,0,LOQ was equal to the LOD<br />
The following spreadsheet would represent this in<str<strong>on</strong>g>for</str<strong>on</strong>g>mati<strong>on</strong> according to the template supplied<br />
with this document:<br />
Serial No Date <str<strong>on</strong>g>of</str<strong>on</strong>g> rec. Country <str<strong>on</strong>g>Food</str<strong>on</strong>g> id. <str<strong>on</strong>g>Food</str<strong>on</strong>g> orig. Time sampl<br />
1980001 2-Nov-98 NEZ DF297 NEZ 04/1997-12/1997<br />
Represen. No. <str<strong>on</strong>g>of</str<strong>on</strong>g> labs QA C<strong>on</strong>t id. Unit LOD min<br />
SW 1 SP 012 1 0.0005<br />
15