PHYS01200704032 Debes Ray - Homi Bhabha National Institute

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Dedicated To My Parents and Brother vi
Acknowledgements I would like to express my deep sense of gratitude to my thesis supervisor Dr. V.K. Aswal, Solid State Physics Division, Bhabha Atomic Research Centre, for his guidance, continuous support and encouragement throughout the period of my work. It is also my great pleasure to thank Dr. S.L. Chaplot, Head, Solid State Physics Division and Dr. A.G. Wagh, Former Head, Optics and Small Angle Scattering Section, Solid State Physics Division, for their support and encouragement. I am also thankful to all the members of my doctoral committee for their guidance and support. I would like to thank Dr. P.A. Hassan, Chemistry Division, Bhabha Atomic Research Centre, for many fruitful discussions and help during dynamic light scattering measurements. My thanks are also attributable to Dr. J. Kohlbrecher, for his help in small-angle neutron scattering experiments at the SINQ, Paul Scherer Institute, Switzerland, and Dr. G. Kumaraswamy and Mr. E. Venugopal, in carrying out small-angle X-ray scattering experiments at the National Chemical Laboratory, Pune. I am grateful to Dr. D. Srivastava and Mr. A.P. Srivastava, Materials Science Division, Bhabha Atomic Research Centre, for their support and help during transmission electron microscopy experiments. I am also thankful to Dr. P.U.M. Sastry, Mr. A.K. Patra, Dr. D. Sen, Dr. S. Abbas and Mr. J. Bahadur, for their constructive support during the period of my thesis work. I have benefitted immensely from the many fruitful discussions with colleagues Dr. Shirish Chodankar, Mr. Akshay J. Chinchalikar and Mr. Sugam Kumar. Also my special thanks to friends Nazir, Arvind, Sandip, Sourav, Madhumita, Tista, Ripandeep, Neetika, Anuvab, Pankaj, Rohit, Naveen, Sunil, Siba, Lokesh, Sanat, Rajib, Siddharth, Preyoshi, Indu, Anup, Palash and others who directly or indirectly have helped me in achieving my goals. I take this opportunity especially to thank my parents, brother and all the family members for being supportive in my endeavour and extending encouragement in spite of remaining aloof from my responsibilities towards them. Without their patience and constant encouragement this would not have been easy. vii
Page 1 and 2: SYNTHESIS AND CHARACTERIZATION OF B
Page 3 and 4: STATEMENT BY AUTHOR This dissertati
Page 5: DECLARATION I, hereby declare that
Page 9 and 10: 2. BLOCK COPOLYMER-MEDIATED SYNTHES
Page 11 and 12: 5. CORRELATING BLOCK COPOLYMER SELF
Page 13 and 14: SYNOPSIS OF THE THESIS TO BE SUBMIT
Page 15 and 16: synthesis for its dependence on gol
Page 17 and 18: interactions between the templating
Page 19 and 20: utilized in the formation of nanopa
Page 21 and 22: nanoparticle-protein conjugate conf
Page 23 and 24: LIST OF FIGURES Figure 1.1. The len
Page 25 and 26: Figure 4.2. UV-visible absorption s
Page 27 and 28: Figure 5.9. (a) Absorbance (Abs max
Page 29 and 30: Figure 7.5. Integrated absorbance o
Page 31 and 32: Chapter 1 Synthesis, Characterizati
Page 33 and 34: Chapter 1: Synthesis, Characterizat
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Chapter 1: Synthesis, Characterizat
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Chapter 2 Block Copolymer-mediated
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Chapter 2: Block Copolymer-mediated
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Time-dependent Absorbance Chapter 2
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Chapter 3: Multi-Technique Approach
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d/d (Q) (cm -1 ) S(Q) P(Q) Chapter
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d/d (cm -1 ) P(Q) Chapter 3: Multi-
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Chapter 4 Optimization of the Block
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Chapter 4: Optimization of the Bloc
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SPR Peak Absorbance Absorbance Chap
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Absorbance Integrated Absorbance /
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Absorbance Chapter 4: Optimization
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SPR peak absorbance Chapter 4: Opti
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d/d (cm -1 ) Chapter 4: Optimizatio
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g I ()-1 Integrated Scattering Inte
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Relative number (%) Chapter 4: Opti
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Chapter 5 Correlating Block Copolym
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Chapter 5: Correlating Block Copoly
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d/d (cm -1 ) Chapter 5: Correlating
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Absorbance Absorbance Chapter 5: Co
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Integrated Absorbance / Yield Absor
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Absorbance Absorbance Chapter 5: Co
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Chapter 6 High-Yield Synthesis of G
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Chapter 6: High-Yield Synthesis of
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Absorbance Chapter 6: High-Yield Sy
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Absorbance Chapter 6: High-Yield Sy
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d/d (cm -1 ) Chapter 6: High-Yield
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d/d (cm -1 ) Chapter 6: High-Yield
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Intensity (a.u.) Chapter 6: High-Yi
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g I ()-1 Chapter 6: High-Yield Synt
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Absorbance Integrated Absorbance /
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Chapter 7: Interaction of Gold Nano
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d/d (cm -1 ) Absorbance Chapter 7:
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Integrated Absorbance / Yield (a.u.
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Absorbance Absorbance Chapter 7: In
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d/d (cm -1 ) Chapter 7: Interaction
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d/d (cm -1 ) d/d (cm -1 ) Chapter 7
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Chapter 8: Summary Chapter 1 introd
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Chapter 8: Summary hence synthesis.
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Chapter 8: Summary irrespective of
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24. R. Elghanian, J.J. Storhoff, R.
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69. J.F. Hainfeld, D.N. Slatkin, T.
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119. N.S. Cameron, M.K. Corbierre a
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165. J.H. Lambert, Photometria sive
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210. D. Ray and V.K. Aswal, Confere
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9. SANS Studies of Temperature-depe
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14. Multi-technique Approach for th
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PHYS01200704032 Debes Ray - Homi Bhabha National Institute

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