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2008 Pittcon Final Program - Pittcon Web Archives

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(470-5 P) Development of Robust NIR Models for Complex<br />

Pharmaceutical Formulations KRYSTYNA POBLOCKA, Novopharm, Thierry<br />

Granger, Rod Ross, Tiffany Mills<br />

(470-6 P) Novel Application of Berthelot Reaction for the Determination of<br />

Antihypertensive Drug Lisinopril AFRAIM KOTY, Chemistry Department,<br />

Mukul Sharma, Bindu Khare, Ashutosh Srivastava<br />

(470-7 P) Residual Solvents By HT-3 Headspace in Reference to USP 467<br />

JAMES COX, Teledyne/Tekmar<br />

(470-8 P) Application of Chemiluminescent Nitrogen Detector for<br />

Pharmaceutical Compounds LILI ZHOU, Merck & Co., Inc., Terri Natishan<br />

(470-9 P) Development of a Dot-Blot Assay for Screening Monoclonal<br />

Antibodies to Immunosuppressant Drugs Sirolimus, Cyclosporine and<br />

Tacrolimus RAD NAIR, Abbott Laboratories, Larissa Harwick, Felicia Bogdan,<br />

Gangamani Beligere, Kevin Rupprecht, Jeffrey Fishpaugh<br />

(470-10 P) Determination and Validation of N-Methylpyrrolidine in<br />

Cefepime for Injection by Capillary Electrophoresis SIGAMANI JOHN<br />

PRASANNA, APL Research Centre, Hemant K Sharma, K Mukkanti<br />

(470-11 P) A Novel Method for Simultaneous Determination of Peptides,<br />

Lipids and Lipid-Impurities in the Synthetic Pulmonary Surfactant<br />

Formulation DARWIN J ASA, ESA Biosciences, Rosa Bonilla, John Rech,<br />

Victoria Scott, Charlotte Baker, Gerald Orehostky, Michelle DeCrosta<br />

(470-12 P) Application of Micro X-Ray Fluorescence (Application of Micro<br />

X-Ray Fluorescence (µXRF) for the Analysis of Pharmaceutical Materials<br />

RORY DAVID SARGEANT, Merck & Co., Inc.<br />

(470-13 P) Nontraditional Application of HS/GC/FID: Evaluation of Solvent<br />

Ratios in Pharmaceutical Manufacturing ALICIA V DURAN-CAPECE,<br />

Schering-Plough Research Institute, Douglas D Richardson, Randi Smith<br />

(470-14 P) Evaluation of Silver-Coated Substrates for Improving Surface-<br />

Enhanced Raman Scattering Signals NGEE-SING CHONG, Middle<br />

Tennessee State University, Ramamoorthy Subathra, Sunil Setti, Beng Guat<br />

Ooi<br />

(470-15 P) Kinetic Spectrophotometric Methods for Determination of<br />

Ciprofloxacin in Pharmaceutical Preparations SERAP SAGLIK ASLAN,<br />

Istanbul University, Betul Demir<br />

(470-16 P) Diffusion Measurement Using Raman Microscopy: An<br />

Application in Pharmaceutical Sciences JUN HUANG, University of<br />

Wisconsin, Madison, Ye Sun, Lian Yu<br />

(470-17 P) Effect of Sample Introduction on the Detection of Nonmetals as<br />

Chromatographic Eluents ADAM DILL, Northern Illinois University<br />

(470-18 P) Multivariate Analysis of Deep Sub-Surface Raman Spectra<br />

NEIL ANGUS MACLEOD, Rutherford Appleton Laboratory<br />

(470-19 P) Comparative Studies of Quercetin Interactions with<br />

Monophosphate Nucleotides SAMUEL N KIKANDI, SUNY-Binghamton<br />

POSTER SESSION Session 480<br />

All posters are to be mounted by 9:00 AM and remain on display until<br />

4:30 PM. Authors must be present from 9:30 AM to 11:30 AM. Location<br />

of the posters is on the Exposition Floor - Hall C, Aisles 3000-3400.<br />

Bioanalytical Chemistry: Separation Based<br />

Monday Morning<br />

(480-1 P) A “Global” Method for the Determination of Tissue Thiols,<br />

Disulfides and Thioethers Using an HPLC System Incorporating a Novel<br />

Boron-Doped Diamond Detector IAN N ACWORTH, ESA Biosciences, Inc.,<br />

Bruce Bailey, Darwin J Asa, John Christensen, Eddie Goodall, John Waraska<br />

(480-2 P) Validated HPLC-Fluorescence Method for the Determination of<br />

Valsartan in Human Plasma WIYADA AKARAWUT, Bureau of Drug and<br />

Narcotic, Sumate Thiangthum<br />

(480-3 P) Determination of Thiol Compounds in Human Blood Sample by<br />

Hydrophilic Interaction Chromatography with Electrospray Ionization Mass<br />

Spectrometry YUSUKE IWASAKI, Hoshi University, Hiroko Tezuka, Rie Ito,<br />

Koichi Saito, Hiroyuki Nakazawa<br />

(480-4 P) Sensitivity Comparison of HILIC and RPLC for Bioanalytical<br />

LC/MS/MS Analysis of Polar Drug Compounds MONIKA MITAL KANSAL,<br />

Phenomenex, A Carl Sanchez, Art Dixon, Ismail Rustamov<br />

(480-5 P) Simple HPLC Method for the Quantification of Quetiapine in Rat<br />

Plasma and Brain Tissue BATTA NEELIMA, Suven Life Sciences Limited,<br />

Gopinadh Bhyrapuneni, Koteshwara Mudigonda, Vishwottam Kandikere,<br />

Ramakrishna Nirogi<br />

(480-6 P) Vydac MS RP-HPLC Columns Provide Unique Selectivity and<br />

High Recovery for Peptide and Protein Separations RENO T NGUYEN,<br />

Grace Davison Discovery Sciences, Scott Anderson, Wendy Luo<br />

(480-7 P) Effect of the Nitration on Generation of the Reactive Oxygen<br />

Species ATSUSHI OGARA, Hoshi University, Yusuke Iwasaki, Yuji Ishii, Rie<br />

Ito, Koichi Saito, Akiyoshi Nishikawa, Hiroyuki Nakazawa<br />

(480-8 P) Using Self Interaction Chromatography to Predict the Physical<br />

Stability of Therapeutic Proteins JAIMIE M VANBUREN, Colorado State<br />

University, Charles S Henry<br />

(480-9 P) Methods for the Analysis of 3,3’,4,4’-Tetrachloroazobenzene in<br />

Rat Liver and Lung Using GC with Electron Capture Detection STEPHEN<br />

D COOPER, RTI International, Dolores R Brine, Trevor B Hoke, Calliandra B<br />

Harris, Bradley J Collins<br />

(480-10 P) Determination of Methyl Mercury in Blood and Urine Samples<br />

with Automated Dynamic Headspace Sampling and Plasma Emission<br />

Detection EIKE KLEINE-BENNE, GERSTEL GmbH & Co. KG, Oliver Lerch,<br />

Hans-Wolfgang Hoppe<br />

(480-11 P) Detection of Volatiles in the Uropygial Secretions of Grey<br />

Catbirds by Headspace Sampling SPME-GC-MS REBECCA J WHELAN,<br />

Oberlin College, Mary Garvin, Tera Levin<br />

(480-12 P) Determination of Glycols and Alcohols in Fermentation Broths<br />

by Ion-Exclusion Chromatography and Pulsed Amperometric Detection<br />

TERRI T CHRISTISON, Dionex Corporation, Jeffrey S Rohrer<br />

(480-13 P) Ultra-Fast Separations of Peptides and Proteins Using Large<br />

Pore, Sub-Two Micron Columns RENO T NGUYEN, Grace Davison<br />

Discovery Sciences, Scott Anderson, Ian Chappell, Wendy Luo<br />

(480-14 P) Characterization and Profiling of N- and O-linked<br />

Oligosaccharides from Glycoproteins with the Corona CAD<br />

DARWIN J ASA, ESA Biosciences<br />

(480-15 P) Guanosine Gels for Polymorphic ssDNA Separations in Slab<br />

Gel Electrophoresis SAMUEL LABARGE, Rensselaer Polytechnic Institute,<br />

William S Case, Linda B McGown<br />

(480-16 P) Development of Aptamers that Bind Specific VEGF Peptide<br />

Variants KUAN-LIN HUANG, Santa Clara University, Daniel J Daugherty,<br />

Steven W Suljak, Terrence E O'Brien<br />

(480-17 P) Electrocatalytic Microelectrode Enzyme Detectors for Capillary<br />

Electrophoresis JHINDAN MUKHERJEE, University of Toledo, Jon R<br />

Kirchhoff<br />

(480-18 P) Derivatization of PET by Alkaline Hydrolysis: Effects of Physical<br />

and Chemical Properties, and the Chromatographic Efficiency of a<br />

Synthetic Protein Suite CHRISTINE M STRAUT, Clemson University, R T<br />

Bostic, R Kenneth Marcus<br />

(480-19 P) Post-Source Decay Analysis of Underivatized Oligosaccharides<br />

in Negative Ion MALDI-TOF Mass Spectrometry: Simultaneous<br />

Determination of Both Linkage Types and Anomeric Configurations BING<br />

GUAN, University of New Orleans, Richard B Cole<br />

(480-20 P) LFII Advanced Technology: Vertexing GARY TAYLOR, deltaDOT<br />

(480-21 P) Therapeutic Monoclonal Antibodies MEI-AN SUNG, deltaDOT<br />

(480-22 P) Simultaneous Quantification of NADH and NAD(+) from Single<br />

Cell by Capillary Electrophoresis WENJUN XIE, Iowa State University,<br />

Edward S Yeung<br />

(480-23 P) Use of Micellar Electrokinetic Chromatography for the<br />

Separation of Cholinesterase Inhibitors IRINI NIKOLAOU, University of<br />

Cyprus, Constantina Kapnissi-Christodoulou<br />

(480-24 P) Characterization of Oligonucleotide-Modified Fused Silica<br />

MALDI Probe Surfaces Using Atomic Force Microscopy ASHLEY<br />

TENNYCK, Rensselaer Polytechnic Institute, Jacquelyn R Cole, Linda B<br />

McGown<br />

(480-25 P) Determination of Sphingosine Kinase Activity for Cellular<br />

Signaling Studies by Capillary Electrophoresis SIMON M MWONGELA,<br />

Kent State University, Katherine J Lee, Allison R Neslon, Christopher E Sims,<br />

Laura M Borland, Sumith Kottegoda, Nancy L Allbritton<br />

(480-26 P) Development of a Novel Platinum-Coated Nanoporous<br />

Membrane for the Separation of Analytes NGUYEN THI THANH BINH,<br />

National University of Singapore, Cheow Pui Sze, Toh Chee-Seng<br />

(480-27 P) Automated Solid Phase Extraction of Lipids In Biological Tissue<br />

Extracts LANDON A WIEST, Brigham Young University, Katherine N Biggs,<br />

Josiah Moulton, Steven Wood, Craig Thulin, Matthew R Linford

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