2008 Pittcon Final Program - Pittcon Web Archives
2008 Pittcon Final Program - Pittcon Web Archives
2008 Pittcon Final Program - Pittcon Web Archives
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ORGANIZED CONTRIBUTED<br />
Session 1410<br />
SESSION<br />
Current Status and Trends in the Application of Liquid<br />
Chromatography (LC and UHPLC) Hyphenated with Tandem<br />
Mass Spectrometry for Pharmaceutical Analysis - arranged by<br />
Arindam Roy, Covidien<br />
Tuesday Afternoon, Room 245<br />
Arindam Roy, Covidien, Presiding<br />
1:30 (1410-1) Tandem MS with Evaporative Light Scattering<br />
Detection (ELSD): A Powerful Analytical Combination for the Analysis of<br />
Select Pharmaceuticals JOHN EDWIN GEORGE, Varian, Inc., Fran Lai<br />
1:50 (1410-2) Application of LC/MS as an Everyday Tool in the<br />
Analytical Process Development of API YANQUN ZHAO, Abbott<br />
Laboratories, Wayne A Pritts, Shuhong Zhang<br />
2:10 (1410-3) The LTQ Orbitrap: Defining Its Place in the Drug<br />
Development and Impurity Analysis Workflows BRENDA KESLER, Thermo<br />
Fisher Scientific<br />
2:30 (1410-4) Addressing the NEED for SPEED: High Throughput<br />
and High Confidence with Novel LC-MS/MS Solutions ROBERT IAN ELLIS,<br />
Applied Biosystems/MDS Sciex<br />
2:50 Recess<br />
3:05 (1410-5) The Application of Capillary LC/MS Using Nanospray<br />
for the Profiling of Impurities and Degradants ROBYN A ROURICK,<br />
Kalypsys, Inc., John P Walsh, Gary Valaskovic, Mike Lee<br />
3:25 (1410-6) Automated Sample Enrichment and High Sensitivity<br />
Analysis of DMPK Samples Using HPLC-Chip QQQ MS GEORGES L<br />
GAUTHIER, Agilent Technologies, Stephan Buckenmaier, Martin Vollmer<br />
3:45 (1410-7) Realizing the Benefits of Sub 2µm Particle LC<br />
Hyphenated with MS/MS for Pharmaceutical Analysis ROBERT S PLUMB,<br />
Waters Corporation<br />
4:05 (1410-8) Effective Use of LC-MSn Molecular Fingerprinting for<br />
the Rapid Structural Identification of Pharmaceutical Impurities MIN LI,<br />
Schering-Plough, Abu M Rustum<br />
ORGANIZED CONTRIBUTED<br />
Session 1420<br />
SESSION<br />
Pharmaceutical Analysis: Latest Trends in Taste and Flavor<br />
Assessment in Drug Product Formulations (Half Session) -<br />
arranged by Kenneth J Norris, Pfizer<br />
Tuesday Afternoon, Room 261<br />
Kenneth J Norris, Pfizer, Presiding<br />
1:30 (1420-1) Analytical Methods for the Analysis of Flavors in<br />
Pharmaceuticals KENNETH J NORRIS, Pfizer<br />
1:50 (1420-2) Improving the Manufacturing Quality Consistency of<br />
Food and Soft Drink Products Using the Electronic Nose and Tongue<br />
JEAN-CHRISTOPHE MIFSUD, Alpha MOS, Vincent Schmitt<br />
2:10 (1420-3) Drug Product Characterization by Macropixel<br />
Analysis of Chemical Images MAZEN L HAMAD, U.S. Food and Drug<br />
Administration, Christopher D Ellison, Mansoor A Khan, Lyon C Robbe<br />
2:30 (1420-4) Overview of Electronic Tongue and Nose<br />
Applications for Improving the Taste and Flavor Acceptance of<br />
Pharmaceutical Products VINCENT SCHMITT, Alpha MOS<br />
ORAL SESSION Session 1430<br />
Bioanalytical Separations II<br />
Tuesday Afternoon, Room 263<br />
Mary Ellen P McNally, DuPont Crop Protection, Presiding<br />
1:30 (1430-1) Superoxide Production in Mitochondria XIN XU,<br />
University of Minnesota, Edgar A Arriaga<br />
1:50 (1430-2) Separation and Quantification of Modified<br />
Nucleosides in Urine Samples by Capillary Electrophoresis with Laserinduced<br />
Fluorescence Detection YONGQING JIANG, University of Missouri,<br />
Rolla, Heng Liang, Yinfa Ma<br />
2:10 (1430-3) Cation Separations by Capillary Electrophoresis<br />
Using Organic Salts and Modifiers in the Background Electrolyte STEVEN<br />
A STEINER, University of Wisconsin, Platteville, James S Fritz<br />
2:30 (1430-4) Possibilities in the Identification and Quantification<br />
of Flavonoids Simultaneously with Acids, Sugars and Sugar Alcohols in<br />
Natural Matrices by GC-MS(MS) IBOLYA MOLNÁR-PERL, L. Eötvös<br />
University<br />
2:50 Recess<br />
3:05 (1430-5) On-line Method for Determining In Vitro Amino Acid<br />
Flux in Sub-Minute Time Scales Using Fast Micellar Electrokinetic<br />
Chromatography JASON GREENE, Vanderbilt University, John P Wilkswo<br />
3:25 (1430-6) Isolation and Detection of Calcium Phosphate<br />
Crystals from Synovial Fluid Using Bisphosphonate-Modified Magnetic<br />
Beads AARON HERNANDEZ-SANTANA, Dublin City University, Adedayo<br />
Oyinloye, Alexander I Yavorskyy, Geraldine M McCarthy, Alastair D Smith,<br />
Gillian P McMahon<br />
3:45 (1430-7) Water-Soluble Vitamin and Amino Acid Analysis in<br />
Cell Culture Media Using Separation Technology JO-ANN M JABLONSKI,<br />
Waters Corporation, Thomas E Wheat, Paula Hong, Diane M Diehl<br />
4:05 (1430-8) High-Speed Amino Acid Analysis (AAA) on 1.8<br />
Micron Reversed-Phase (RP) Columns JOHN W HENDERSON, Agilent<br />
Technologies, Cliff Woodward, Todd Wielgos<br />
ORAL SESSION Session 1440<br />
Clinical/Toxicology<br />
Tuesday Afternoon, Room 264<br />
Dutt V Vinjamoori, Martek Biosciences Corporation, Presiding<br />
1:30 (1440-1) A New Method for the Analysis of Physiological<br />
Amino Acids PAULA HONG, Waters Corporation, Thomas E Wheat, Diane M<br />
Diehl<br />
1:50 (1440-2) Rapid and Facile Detection of Stimulants and Their<br />
Metabolites in Urine Using Solid Phase Extraction-Thermal Desorption-Ion<br />
Mobility Spectrometry with Alternating Least Squares YAO LU, Ohio<br />
University, Peter de B Harrington<br />
2:10 (1440-3) Rapid Measure of Drug-Drug Interaction Utilizing<br />
Generic Gradient Ultra Performance Liquid Chromatography and Tandem<br />
Mass Spectrometry PAUL D RAINVILLE, Waters Corporation, Robert S<br />
Plumb<br />
2:30 (1440-4) Determination of Ratio of Testosterone and Epi-<br />
Testosterone by SPME/LC/MS Method YANWEI ZHAN, University of<br />
Waterloo, Janusz Pawliszyn<br />
2:50 Recess<br />
3:05 (1440-5) Assessment of Current Atomic Spectrometric<br />
Methods for the Determination of Lead in Blood via Performance in the<br />
New York State Proficiency Testing <strong>Program</strong> PATRICK J PARSONS, New<br />
York State Dept of Health, Ciaran Geraghty, Miles Lewis, Christopher Palmer,<br />
Mary F Verostek<br />
3:25 (1440-6) Gradation of Gliomas: A 1H NMR Metabolic Study<br />
VERONIQUE GILARD, University Paul Sabatier, Myriam Malet-Martino, Olivier<br />
Robert, Jean Sabatier, Robert Martino<br />
3:45 (1440-7) Monitoring of Propofol Concentrations in Breath and<br />
Blood by SPME-GC-MS and PTR-MS: Chance and Limitations of a New<br />
Clinical Tool WOLFRAM MIEKISCH, University of Rostock, Patricia Fuchs,<br />
Svend Kamysek, Maren Mieth, Jochen Schubert<br />
4:05 (1440-8) Functional Groups: A Major Deciding Factor for<br />
Analytical Method Development PADINJAREKUTTU RAMAN PILLAI<br />
RAVIKUMAR, Public Health Laboratories/NYC DOH, Sara B Beatrice<br />
ORAL SESSION Session 1450<br />
Development and Applications of Nanotechnology and<br />
Microscopy<br />
Tuesday Afternoon, Room 271<br />
James Manner, Retired - PPG Industries, Inc., Presiding<br />
1:30 (1450-1) Nano-Structured Scaffolds as Synthetic Models of<br />
Enzyme Complexes JACQUELINE KEIGHRON, The Pennsylvania State<br />
University, Lisa M Dominak, Christine Keating