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FIGURE 3. MASS CHROMATOGRAM OF A STANDARD CONTAINING 0.1 µg/L ClO 4 - AND 1.0 µg/L INTERNAL STANDARD <strong>332</strong>.0-42
FIGURE 4. MASS CHROMATOGRAM OF AN LFSSM CONTAINING 1.0 µg/L ClO 4 - AND 1.0 µg/L INTERNAL STANDARD <strong>332</strong>.0-43
Page 1 and 2: EPA Document #: EPA/600/R-05/049 ME
Page 3 and 4: atio and relative retention time ar
Page 5 and 6: and processed like a field sample (
Page 7 and 8: eluent strength or modifying the el
Page 9 and 10: 5.2 Pure ClO 4 - salts are classifi
Page 11 and 12: ate (>15 L/min), liquid nitrogen or
Page 13 and 14: 7.1.2 ACETONITRILE - ACN, CASRN 75-
Page 15 and 16: 7.2.3 CALIBRATION STANDARDS (CAL) -
Page 17 and 18: 9.1.1 METHOD MODIFICATIONS - The an
Page 19 and 20: 9.2.4.3 The target MRL is validated
Page 21 and 22: more than ±30 percent from the are
Page 23 and 24: 9.3.8 LABORATORY DUPLICATE OR LABOR
Page 25 and 26: counts for ClO 4 - at m/z 99 while
Page 27 and 28: 11. PROCEDURE 10.4.3 After every te
Page 29 and 30: 11.5 COMPOUND IDENTIFICATION - Iden
Page 31 and 32: 12.4.1 Calculations must utilize al
Page 33 and 34: 17. TABLES, DIAGRAMS, FLOWCHARTS AN
Page 35 and 36: TABLE 3. SAMPLE ANALYSIS BATCH Inje
Page 37 and 38: TABLE 5. DETECTION LIMIT AND LCMRL
Page 39 and 40: TABLE 8. ON-GOING QUALITY CONTROL R
Page 41: FIGURE 1. IC-ESI/MS Configuration U
Page 45 and 46: Procedure 1. Prepare and inject, in
Page 47 and 48: APPENDIX A TABLE A1. SAMPLE DATA CO

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