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Organic Chemistry Semester 1 LABORATORY MANUAL - Moravian ...

Organic Chemistry Semester 1 LABORATORY MANUAL - Moravian ...

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PART I:<br />

1<br />

TABLE OF CONTENTS<br />

Pages<br />

Introduction:<br />

Weekly Schedule 3-7<br />

Philosophy and Administrative Details 8-11<br />

PART II:<br />

PART III:<br />

PART IV:<br />

Laboratory Rules and Regulations<br />

General Rules and Daily Routines 11-12<br />

Safety Regulations 12-13<br />

Laboratory Equipment List 14<br />

Laboratory Record & Report Formats<br />

Laboratory Notebook Format 15-17<br />

Data Binder Organization 17-18<br />

Laboratory Report Format 19-20<br />

Collaboration and Academic Honesty 21<br />

Experiments<br />

Experiment 1 How is the Boiling Point of a Molecule Related to Its Structure 22-23<br />

Experiment 2<br />

How is Solubility Related to the Structures of the Solute and Solvent<br />

Molecules<br />

Experiment 3 How Does the pH of Aqueous Solutions Affect the Solubilities of<br />

<strong>Organic</strong> Compounds<br />

Part A: What can solubility in acidic and/or basic aqueous solutions<br />

tell us about structures of organic molecules<br />

Part B: How can we use pH effects on solubility to separate<br />

mixtures of compounds<br />

Experiment 4 How is the Melting Point of a Mixture of Two Solids Related to the<br />

Melting Points of the Pure Solids<br />

Experiment 5 How Can an Impure Solid Substance Be Purified<br />

Part A: How can we judge the purity of a sample of an unknown<br />

solid compound<br />

Part B: How can we choose an appropriate solvent to recrystallize<br />

an unknown solid compound<br />

Experiment 6 How Can We Tell if Two Solid <strong>Organic</strong> Compounds Are the Same or<br />

Different What measurements can allow us to distinguish one<br />

compound from another<br />

Experiment 7 How Can We Determine the Structure of an <strong>Organic</strong> Compound<br />

A: How Do <strong>Organic</strong> Compounds Interact with High Energy<br />

Electrons and What Structural Information Can We Obtain from<br />

the Results<br />

B: How Do <strong>Organic</strong> Compounds Interact with Light and Magnetic<br />

Fields and What Structural Information Can We Obtain from the<br />

Results<br />

24<br />

25<br />

26<br />

27-28<br />

29-31<br />

32-33<br />

34-35<br />

36-38<br />

39-40

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