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2. Single crystal growth of sodium sulfate heptahydrate 23 background LEDs a air bubble growing hepthahydrate crystal b c x2 y1 y2 x1 5 mm Fig. 2.6: Images of sodium sulfate heptahydrate growth in a 100 µl droplet with an initial concentration of c 0 = 3.4 mole/kg. (a) Initially, the holder is filled with a sodium sulfate solution at approx. 33 ◦ C. (b) Precipitation of sodium sulfate heptahydrate is observed upon cooling when the supersolubility line is reached. (c) Crystal growth stops as the concentration reaches the heptahydrate solubility line.
2. Single crystal growth of sodium sulfate heptahydrate 24 x2 y1 a y2 x1 5 mm b growth from center [mm] time [s] c growth from center [mm] time [s] Fig. 2.7: (a) Image of a single sodium heptahydrate crystal grown at 4.8 ◦ C in a 100 µl droplet with an initial concentration c 0 = 2.5 mole/kg. (b) Measured dimensions of a crystal grown in a solution with initial concentration c 0 = 2.5 mole/kg. (c) Measured dimensions in four directions of a crystal grown in a solution with initial concentration c 0 = 3.4 mole/kg. The error of the measurement is ±0.2 mmole/kg.
Page 2 and 3: Sodium sulfate heptahydrate in weat
Page 4: To my family
Page 8 and 9: CONTENTS 1. Introduction . . . . .
Page 10 and 11: 1. INTRODUCTION 1.1 Introduction Sa
Page 12 and 13: 1. Introduction 11 This phenomenon
Page 14 and 15: 1. Introduction 13 1 2 initial mass
Page 16 and 17: 1. Introduction 15 However, our pre
Page 18 and 19: 2. SINGLE CRYSTAL GROWTH OF SODIUM
Page 20 and 21: 2. Single crystal growth of sodium
Page 32 and 33: 3. CRYSTALLIZATION UNDER WETTING/NO
Page 34 and 35: 3. Crystallization under wetting/no
Page 44 and 45: 4. NUCLEATION ON MINERAL SUBSTRATES
Page 46 and 47: 4. Nucleation on mineral substrates
Page 52 and 53: 5. SODIUM SULFATE HEPTAHYDRATE FORM
Page 54 and 55: 5. Sodium sulfate heptahydrate form
Page 62 and 63: 6. CRYSTALLIZATION OF SODIUM SULFAT
Page 64 and 65: 6. Crystallization of sodium sulfat
Page 72 and 73: M 6. Crystallization of sodium sulf
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7. THERMODYNAMIC AND POROMECHANIC C
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7. Thermodynamic and poromechanic c
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8. NMR COMBINED WITH ACCELERATED WE
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8. NMR combined with accelerated we
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∆ 8. NMR combined with accelerate
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9. CONCLUSIONS AND OUTLOOK This cha
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9. Conclusions and Outlook 107 Soft
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APPENDIX: CALCULATION OF SALT CRYST
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Appendix: Calculation of salt cryst
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Bibliography 113 [15] L.M. Luquer,
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Bibliography 115 [47] D. Rosenblatt
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Bibliography 117 [78] H.P. Huinink,
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LIST OF PUBLICATIONS Published: •
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ACKNOWLEDGMENT This thesis would no
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CURRICULUM VITAE Tamerlan Saidov wa
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