Synthesis and Characterization of Various Amino Acids Complexes ...

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Synthesis and Characterization of Various Amino Acids Complexes by Different Analltical Techniques izVei al,/-i A t frz';' tu,sirkl b t6. ,Ul e$iq ,J Sn 4 i^ portialj,tfhrd J.r tfre d?Btu oJ aocr'/ ofefritosoptry in Chanirtr| Raja Adil Sarfraz National Center ofErcellence in Analytical Chemistry University ofSindh, Jamshoro - PAKISTAN June 2008
Page 1: Synthesis and Characterization of V
Page 5 and 6: ACKNOWLEDGEMENTS I bow oy held b.fo
Page 7 and 8: DEDICATION lfuis Eatcopors Is Adraa
Page 9 and 10: H,C N rrd'.turstcd-r.dl,}||lid. htn
Page 11 and 12: ft. d&dns :llrlMof A 'd 3. Dirpr@d
Page 13 and 14: 3.t J.2 3.3 3,5 CEAPTER 2 Amino Aci
Page 15: d....................,.........,...
Page 18 and 19: 7. (ri. T,C.. Adn. M.B., Jddi, M.K.
Page 20 and 21: spocrophotom.lryi Opimiation sudy".
Page 22 and 23: Irtroductior Chapter - 1 Anino *i&
Page 24 and 25: ADim ..lL @rt irhS u idlo grelp Hyd
Page 26 and 27: s "-9--F E-9-N{l /N-fEl | ,q"i. I d
Page 28 and 29: It is also kroM s 8.qui.olinol (ont
Page 30 and 31: a us€d ESulsly a FEc.r.lls$ 1251.
Page 32 and 33: $b3l!d6 clldlz.d by naal e ofboth s
Page 34 and 35: dim.tnybed ma.bolir6, brtinS mdlyl$
Page 36 and 37: Olns po$ibL binding 3it s n.y .le b
Page 38 and 39: l , sitlmr, s, E., BoF, A., Roitm,
Page 40 and 41: 24. (a) a, Md, H, ohlo, H. N raK Te
Page 42 and 43: 50. R- Albdro, in CodPr.hdsivc C@rd
Page 44 and 45: Chepter -2
Page 46 and 47: Ano$6 worL Egon d bv us (Kdi .t.l-
Page 48 and 49: m dd .nission 45oin. [tv.loted neth
Page 50 and 51: signal cnhdccm.lt by o.olumn Iluorc
Page 52 and 53:
@lutr. fte ndhod d.sib.d is als $ii
Page 54 and 55:
Eedilddd for lm$ *ith dhdelmsis cd
Page 56 and 57:
pr@ss, Oul of diffa..i Edu.ibl€ s
Page 58 and 59:
L C,H, Kdi. T.lqbal. ddZ,A ZAidi, J
Page 60 and 61:
3l. A. woli C. Zalpor, c Tneilrci.r
Page 62 and 63:
5?. T. Nateq S. Uhsq Y.Kiio, Y- l3h
Page 64 and 65:
Chrphr - 3
Page 66 and 67:
Erp.ribertrl IctEn n|.iio., CheEh.h
Page 68 and 69:
At l& 375. 360 m .rd la43l,, rl40 d
Page 70 and 71:
AD r60 1@ 140 1m 81@ d, 4 6 0 &. t
Page 72 and 73:
Thc @mpsitiv€ study of 0uoFslxM '
Page 74 and 75:
Si E! FsD (!)v (A) l0 t0 92 0t 0.1
Page 76 and 77:
Trble .1, (.) Comp.d'E sEdy b.il{6
Page 78 and 79:
ng. E {r): Fl@cac.c .P.cm of !.nE c
Page 80 and 81:
Trbl. a. O) Del.ctio Linn or conplq
Page 82 and 83:
(wL. a4 - l3%) Bp€rivcly. Mo@vd,
Page 84 and 85:
(.r-..-ld (r5cd.+rFqdir- r|. lc Dsr
Page 86 and 87:
€.t-a+lydq{qr5- t; n.Ihqm-oftg&6.
Page 88 and 89:
cy.bln -l-Hyddyqlln.ldrn Er, rr.lbd
Page 90 and 91:
T.th l0 hdisr€d th.6dpr6rivc nudy
Page 92 and 93:
ibh U indi€i.rl th. Erutt! of i.t
Page 94 and 95:
T.U. 12 indics.d th. nsultt obt inc
Page 96 and 97:
Nuclar Mas.ttc Re3oD.ncc Sp..trorco
Page 98 and 99:
T.bL ld Nlcld masrdic l!$@e spd:l b
Page 100 and 101:
o Plotms di@{y linLd wnh entdc tuch
Page 102 and 103:
toLcd.? ron Fr..rq ao3 I 2t t( Ft l
Page 104 and 105:
2-M.tty!&hydmryqrtrolin - glubDi .c
Page 106 and 107:
Rotir c.s L 3. 5. 6. G}l rad, T. Iq
Page 108 and 109:
Chapter - 4
Page 110 and 111:
!o iipov. ehdoth.lial tuftdd in min
Page 112 and 113:
Strlhgn ofchok t.rel crd.i..lc Abol
Page 114 and 115:
R€sults and Discursio! Fluor.lcon
Page 116 and 117:
na,3, nr* tda.addtl si- Ctd*rt rdid
Page 118 and 119:
Tb. *ilrlid .nd .nisiod wlcrgths fo
Page 120 and 121:
T.bl.:2 TGA / DTA Srudi6 ofcho!6lDl
Page 122 and 123:
.U.4. rCA / DTA Slvdi.s of Chol.stb
Page 124 and 125:
T.bl. 6. TGA / DTA Studies of Chol6
Page 126 and 127:
T.bL: t Cbolc{.yl cy{GiMre 120 w Cr
Page 128 and 129:
426=l,E1( M.l Peak=457 3E5'10o% Prc
Page 130 and 131:
I iE 9.M6+..rr!n ric sbdi*ofch6l.n
Page 132 and 133:
Cnobtnlsir. d.tta.ttE (CroL.o..yl x
Page 134 and 135:
. Abujryylb, AbduL.nin, It 6th sci.
Page 136 and 137:
SunD.ry ADiDo Acids Complerca of Os
Page 138 and 139:
h pr6.nr $rdi.q w illu{ra.d l|r. sy
Page 140 and 141:
IlM solulioo obtaincd m iho Etigq.r
Page 142 and 143:
ed B foud ro haw s psqd@teiralEdrd
Page 144 and 145:
atohs, The omplexatior ws conpleted
Page 146 and 147:
In both of $* c6, th. Osmiun ooordi
Page 148 and 149:
T.H. a, crys!.| d.i. rd *udrE .luci
Page 150 and 151:
C{ od C=O but upon th. hindde of C=
Page 152 and 153:
W. havc also t!i.d to siudy in emc
Page 154 and 155:
I P. McMom sd G..1. Hutchines. Cn?u
Page 156 and 157:
S||pponing Informltlons CrFrcll,ogr
Page 158 and 159:
_diftn dd.@ t@_'sl_ll@ 8.2 _diltr c
Page 160 and 161:
02 O 0,1189204) 0,13415( l3) 0..191
Page 162 and 163:
03 C10 2.2032(15) . ? os cu xal r9(
Page 164 and 165:
c14 c13 03 70.25(9). . ? cl7Cl3 os
Page 166 and 167:
stm.dr'-.q!ivls,a-42 eu-iBu'ld EnFn
Page 168 and 169:
_cfir L_widtr&sdE* olc 'cdc Fr 4v^2
Page 170 and 171:
c30 c 0.756r(t {.035(.)0.r6.4qe)0 0
Page 172 and 173:
t47
Page 174 and 175:
t49
Page 176 and 177:
ls_hid_M_siF_hb.r_a ls_bnr_d! .y.!6
Page 178 and 179:
Puhtrieations
Page 180 and 181:
^|!6fu!d6l.d#rso|'qs(hicsb!4hm t ;;
Page 182 and 183:
MgH.."-. ffiffiijl#' #{trffi iH3 s*
Page 184 and 185:
fubi@obdn d t odd.dd orqdoFsn.(.! d
Page 186 and 187:
Enecl ofultrrsound Agititios or the
Page 188 and 189:
original adicle Datalmlnation of le
Page 190 and 191:
a E I a i I a'i'c.'i.ot e E*dtu t c
Page 192 and 193:
ffi EI,SEVIER ':;;'sci",tceDirec Ea
Page 194 and 195:
AUTIIOR'S PROOF Potnrlln, Cddun, !,
Page 196 and 197:
ffi EI.SEVIER ':i;'scienceDirect Ta
Page 198 and 199:
22 TiD. lvirg oodin .I BCR *qualti.
Page 200:
n \n lrR d.dhe|d.r!.|.idid Ecotodco
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