Synthesis and Characterization of Various Amino Acids Complexes ...

signal cnhdccm.lt by o.olumn Iluorcm.lric derction in ctadiett 'lution of d$/
mino eids in liquid chFn.ro8rapnv h6 be..aft.d out bv Grkdchi dd Miwa' l9t)
IlSl. Ft@maric {hcclio. in lhe p!!$e of .5:tari6{v Phe ws tppli'd !o sddidr
.lurion of d.ntyl die &ids in liquid chomtoSrlphv- A l-5 nn d qunz tub' p&k'd
'
$ith rh€ s. datcdals 6 the rPd.tion @luin M dplov'd for $' no* @ll
conv.ntionalsiz. @lumns see @ploy.d Thc pe6,li h.i8]t of s'l)tcs incrc$ed Nilh
i@ing ercntion owing lo fausins ed mvnomdtd ed4!t of thc sttdonary pbe'
leding to inprovddts i. ssitiviiv, *ttich B po.ouced fq ealtr"ludng l.re TrF
low dt. glrdihq $. la4p. lhe inpmv.mdr i! sitivnv 3'hia€d Dcr'ajo linils w@
inpmwn by ! f&tor ofnp to 51 bv fllorcddrc det*ti@ usins $' prk'd ltow cll'
comp&ed with thoe achi.ved 6ing a @nmon .mPlv flow 4u
Deleminarion of mino &i& sd eino $ge bv dcivlti4tio! widt 6
dinoguindylN+'dbrt5@ininid/c&b@e (AQC) follo*€d bt hid p"roIllne
liquid chm.bgnphy (HPLC) with ouq.3@e derM, 6 rcpon'd (Diu cl al 1996)
Il9l. A n.thod for th. dei@lizltim of dino &ids with lhe cit'd @npolnd (AQc)' for th'
N of HPLC *6 lcsrcd Repodlcibility, lii.ditv dd limits of detdion rcE simih lo
those ohain.d wilh olhd melhods, ech s lhe @phdal'ld'hvds dd 9_
n@Enyln.rhoxycdhontlchldi.L icthods.
Thc n lhod dcv.l@ for ddmindon ofddiE *6 cpon'd eliB bv us (Kdi
eta1.,1997) 1201. R.elioi oltldin€{ilh oxin undB onlol ldp@turc al60 "c fot l0 min
Ms €tu1cd, ft. nuoMt Pmduct {6 obbincd ud debren al lB 330 'h dd }'h 420
m by tuoiiE.try. M.ihod m be agpli.d fot d.t mination ofal$inc in biologictl fluids'
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